HomeMy WebLinkAboutHISTORICALBarber, Jim
From:
Hardee, Ed
Sent:
Monday, November 02, 2009 9:36 AM
To:
Barber, Jim
Cc:
stolson@cheraw.com
Subject:
RE: FW: WQ0014248
Jim,
Payment was received 10-27-09 from the Town of Cheraw, check number 4598.
Ed Hardee
Aquifer Protection Section
Land Application Unit
1636 Mail Service Center
Raleigh, NC 27699-1636
Phone (919) 715-6189
Fax (919) 715-0588
DISCLAIMER: Per Executive Order No. 150, all e=mails sent�to and from
this'account are subject to the North Carolina Public Records Law and
;may be disclosed to third parties.
From: Barber, Jim
Sent: Monday, November 02, 2009 8:53 AM
To: Hardee, Ed
Subject: FW FW: WQ0014248
Ed;
Here's the reply from the Town of Cheraw relative to my email about their annual permit fee being late. Can you help
Ms. Tolson? .
Thanks
Jim Barber
From: stolson@cheraw.com [mailto:stolson@cheraw.com]
Sent: Thursday, October 29., 2009.10:03 AM
To: Barber, Jim
Subject: RE: FW: WQ0014248
Hi Jim,
I spoke with our clerk after our conversation yesterday.
A check was sent with the original invoice. The check was'dated 8/25/2009.
When we were sent. the second notice, we found out that check had not yet cleared. A second check,
dated 10/20/2009 has been sent. Do you think we should wait 30'days to see what happens?
Thanks for your help,
Sherry
--------- Original Message --------
Subject: FW: WQ0014248
From: "Barber; Jim" <jim.barber(d)ncdenr.aov>
Date:, Wed, October 28, 2009 2:20 pm
1
#To: "stolson(a)cheraw.com" <stolson(abcheraw.com>
Ms. Tolson;
Thanks for the information provided during our phone call this.afternoon concerning the Town of
Cheraw Class "A" residuals program. As discussed, the above attachments are provided. The last
document, page 3, is the panel from DWQ's database that indicates the annual permit
administration fee is late. Once you have the opportunity to see if the town has received notice
(cancelled check or notification from NC DWQ by receipt) that the bill has been resolved, please
email me.
If you have any questions relating to this issue, don't hesitate to call me at 910-433-3340 or Mr.
Ed Hardee in our Raleigh Central office at 919-715-6189.
Thanks again
Jim Barber
DWQ-Fayetteville Regional Office
E-mail correspondence to and from this address may be subject to the North Carolina Public
Records Law and may be disclosed to third parties.
2
N
Barber, Jim
From:
Bernard, Jane
Sent:
Thursday, October 15, 2009 3:12 PM
To:
Barber, Jim
Subject:
W00014248
Jim,
I've got an annual report that shows distribution of Biosolids in a field located on -the
Scotland/Roberson line Allan Baucom Site. Matt Fleahman suggested I to pass this to you.
The file is here but there is very little in it. You may get more information from central
files if you need it.
Jane
(note: new e-mail address - iane.bernard(@ncdenr.gov )
Jane R. Bernard
Environmental Specialist
------------------------------------ --
Aquifer Protection Section, DWQ
Phone 919-791-4200
Fax 919-571-4718 -
E-mail correspondence to and from this address may be subject to the North Carolina Public
Records Law.and may be disclosed to third parties-
1
rM
CHERAW
I
Mr. Daryl Merritt
DENR/DWQ/Water Quality Section
1617 Mail Service Center
Raleigh, NC 27699-1617
Dear Mr. Merfitt:
Enclosed. is the annual Biosolids marketing and distribution report.
Please contact me if you'have any questions or comments.
Sin cerely�/2 /� 3 S�
SheTolson
Industrial. Pretreatment Coordinator
QA/QC Director
/110 fz Q) (-C— � 2 Uk- flr-:---
S-, C
Cheraw Public Utility Department
Post Office Box 219, Cheraw, South Carolina 29520
843.537.8440, Fax 843.537.8442
www.chera-,v.com,
zz
MV 9
LG
7'A"
I . NI- OFFICE
�10N
Jnit
ANNUAL LAND APPLICATION CERTIFICATION FORM
Permit#: W40014248 County: Chesterfield ,- = Yey ark'„ 2008
Facility Name (as shown on permit):. Town of Cheraw
Land Application Operator: Phone: (843)537-8440
Land application of residual solids as allowed by the permit occurred during the past calender year?
® Yes ❑ No If No; skip Part A, and Part B and proceed to -the certification. Also, if residuals were
generated but not land ,applied, please attach an explanation on how the residuals were handled.
Part A:
Total number of application fields in permit:
Total number of fields land application occurred during the year:
_ 1
Total amount of dry tons applied during the year for all application sites:
92
Total number of acres land application occurred during the ear:1
100
Part B:
Facility was compliant during calendar year 2008 with all conditions of the land application permit
(including but not limited -to items 1-12 below) issued by the Division of Water Quality. ® Yes 0 No
If no please, provide a written description why the facility was not compliant, the dates, and explain
corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at
least 6.0 or the limit specified in the permit.
3. Annual soils analysis were.performed on each site, receiving residuals during the past calendar year and three
(3) copies of laboratory results are attached.
4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required
and three (3) copies of certified laboratory results are attached.
6. The facility did not exceed. any of the Pollutant Concentration Limits in Table 1, of 40 CFR Part 503.13 or the
Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated, facilities).
7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were
complied with (applicable to 40 CFR Part 503 regulated facilities).
8. All operations and maintenance requirements in the. permit were complied with or, in the case of a deviation,
prior authorization was received from the Division of Water Quality.
9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of
violations are attached to include appropriate actions and remediations.
10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed
in accordance with the crop management plan.
11. No. runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
12. All buffer requirements as. specified on the permit were maintained during ti f residuals.
"I certify, under penalty of law, that the above information is, to the best oIm nowe nd belief, true,
accurate, and complete. I am aware that there are significant penalties for flti��ffige information,
including the possibility of fines and imprisonment for knowing violat' nsY�R.ctuHLHr Jac rioN
Information Processing unit q
Ricky Ingram/Public Utility Director
Permittee Name and Title (type or print) Sig re of larmittee Date
Signature of Preparer* Date Signiture, of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
Preparer is defined in 40 CFR Part 503.9 (r)
Author Daryl D. Merritt DENR FORM ACF 17/9nn91
TOWN OF CHERAW WASTEWATER TREATMENT FACILITY
BIOSOLIDS REPORT 2008
PRESS DRY CAKE TONS LIME % TOTAL LIME $/ POLY $/ ;LBS. POLY/ LBS. POLY
MONTH HOURS SOLIDS T. USED LIME DRY PROD. TON PROD. TON CAKE TON CAKE USED
JAN
189.30
85.77
99.26
53.65
185.03
73.45
, 8.62
4.66
400.00
FEB
137.70
77.18
71.77
48.18
148.95
65.89
10.91
5.51
425.00
MAR
145.10
83.94
55.27
39.70
139.21
59.41
12.38
6.25
525.00
APR
118.50
73.92
' 30.56
- 29.25
104.48
40.35
5.37
2.71
200.00
MAY
168.30
77.54
99.75
56.26
177.29
77.55
11.48
5.80
450.00
JUN
165.00
74.21
77.96
'51.23
152.17
73.63
13.35'
6.74
500.00
JUL
181.90
93.60
73.26
43.91
166.86
65.73
11.64
5.88
550.00
AUG -
155.00
88.72
65.46
42.46
154.18
63.71
11.72
5.92
525.00
SEP
102.50
53.87
36.87
45.67
80.74.
_ 49.25
10.10
5.10
275.00
OCT
116.80
57.42
33.86
37.09
91.28
.54.70
14.65
7.40
425.00
NOV
4.10
2.13
2.28
51.70
4.41
76.24
26.86
11.73
25.00
DEC
27.90
14.31
15.08
51.31
29.39
75.67
16.01
6.99
100.00
TO
1512.10
782.61'
661.38
1,443.99
775.58
153.09
74.69
4,400.00-
AVG
126.01
65.22
55.12'
45.87
120.33
64.63
12.76
10.71
366.67
MIN
4.10
2.131
2.28
29.25
4.41
40.35.
.5.37
2.71
25.00
MAX
189.30
93.601
99.75
56.261
185.03
77.55
26.86
11.73
550.00
ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
PERMIT #: W00014248 FACILITY NAME: Town of Cheraw
PHONE: (843) 537-8440 COUNTY:' Chesterfield -OPERATOR:
.FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
® Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? ® - Yes-- ❑No No If No skip parts A; B, C and certify -form below _
Part A*:
Part B*:
Month
-
Sources s (include NPDES # if
applicable)
Volume (dry tons)
Admendment/
Bulking Agent Residual In Product Out
Recipient Information
Name(s) Volume (dry tons) Intended use(s
_.
January
SC0020249
99.26
85.77
185.03
Allan Baucom
92
so beans
February
SCO020249
71.77
77.18
148.95
March
SCO020249
55.27
83.94
139.21
April
SCO020249
30.56
73.9.2
104.48
May
-SC0020249
99.75
'77.54
177.29
June
SC0020249,
77:96
74.21
152.17
July
SCO020249
73.26
93.60
166.86
August
SCO020249
65.46
88.72
154.18.-
September
S00020249
36.87
53.87
80.74
October
SCO020249
33.86
.57.42
91.28
November
SCO020249
2.28
2.13
4.41
December
SCO020249
15.08
14.31
29.39
Totals:
Annual (dry tpns)-.T
661.38
782.61
1443'.99 `
Admendment(s) used:
I Lime
Bulking Agent s) used:
*If more space than given is. required, please attach additional information sheet(s). ❑ Check box if additional sheet(s) are attached
Part C:
Facility was compliant during calendar year 2007 with all conditions of the permit (including but not limited to items 1-3 below) issued by the
Division of Water Quality. ® Yes [INo If No, please provide a written description why the facility was not compliant.
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization'was received from the Division of Watei
Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware
th the a are si ificant penalties for submitting false, informaiton, including the possibility of fines and imprisonment for knowing violations."
2 /.0- d 9
Sig a of Pe ee Date Signature of Preparer** Date
(if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r)
Author Daryl D. Merritt DENR FORM DMSDF (7/2002)
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters. to be analyzed than those required to be summarized on this form.
Permit Number: WQ0014248
Facility Name: Town of ' Cheraw
NPDES # or
WQ#: SCO020249
WWTP Name: Town of Cheraw wwTP
Residual Analysis Data
Laboratory: 1) Davis & Brown
2) .Clemson University.
3)
4)
5) ,
Sample or
Composite Date
1/16/08
1./1.6/08
8/09/08
3/19/08
5/21 /08
5/21 /08
7/15/08
7/15/08
9/17/08
9/17/08
11 /19/0
11 /19/0
Percent Solids
47.00
46.32-
55.94
58.00
52.10
54.02
46.10-
48.25
70.90
72.90
52.00
52.98
Arsenic
1.30
.1.11
2.19
1.14
2.04
0.959
Cadmium
0.212
1.11
0.219
1.14
2.04
0.9
Chromium
14.9
97.6
16.1
.13.9
125.0 '
41.6
23.2
Copper
28.6
-48.0
30.1
15.4
42.7_
Lead
1.80
1.64
2.02
1.14
2.04
0.959
Mercury
0.049 '
0.091
0.099
0.039
0.115
0.190
Molybdenum
1.40
1.46
10.1
4.58
2.52
3.84
Nickel
11.7
29.0
12.9
15.3
25.7
18.2
Selenium
1.30
1:1.1
2.19
1.14
.2.04
0.959
Zinc
81.7
170.0
97.7
62.7
128.0
78.3
TKN
1.7973
2.1049
-
1.6429
2.2218
1.1159
1.2269
Ammonia -Nitro a
0.6477
0.1251
0.0370
0.1036
0.2058
0.0566
Nitrate and Nitrite
Total Phosphorus
0.0.381
1 .213_j 3.
0.0604
1 .1682
0.0037
1.1218
D.0016.
1.0767
0.0001
0.8471
0.0098
0.9390
661 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to'assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant en dfl s for submitting false information, including the possibility of fines and imprisonment for knowing violations.
Signatur Prepa Date
Author Daryl D. Merritt DENR FORM RSSF (7/2002)
CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT
CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES
BIOSOLIDS SAMPLE DATE-.WWn y 1e :20Q8
Biosolids Maximum Maximum Maximum
Maximum
Metal Allowable Allowable, Application
Application
Content, Metal App. Rate, Rate,
Rate..
METALS ow Content Dom r1/Acre/Yr. OT/Acre/Yr.
WT/AcrdYr.
Arsenic, Total 1.38 • 41.00 1A0 325.38 660.77
Cadmium, Total 0.23 ` 39.00 1.70 1884.43 3768.87
Chromium, Total 15.85 1200.00 134.00 2113:42 4226.85
Copper, Total 30.43 1500.00 67.00 550.52 1101.05
Lead, Total ' 1.91 300.00 13.00 1697.22 3394.44
Mercury,`Totel 0.05 17.00 0.75 3596.94 7193.88
Molybdenum, Total 1.49 18.00 0.60 134.29 268.57 ,
Nickel, Total 12.45 420.00 18.70 375.60 751.20
Selenium, Total 1.38 36.00 . 4.50 813.46 1626.92
Zinc, Total 88.91 1525.00 ' 125.00 359.65 719.09
PCB 0.70 1.60
' Actual metal content less than amount indicated.-
Biosolids Biosolids Maximum Maximum
Nutrient Nutrient Crop/Soil Application Application
Content, Content, Requirement, Rate, Rate,
oom % INAcre •' DT/Acre/Yr. WT/Acre/Yr.
Ammonium Nitrogen 323.83 0.03
Organic Nitrogen 8662.58 . 0.87
Incorporated Available Nitrogen 5758.85 0.58 120:00 5.21 10A2
Surface Available Nitrogen 5601.70 0.67 120.00 5.30 10.60
Phosphorus as P205 6088.49. 0.61 80.06 3.30 6.59
Potassium as K20 .723.23 0.07 - 50.00 17.28 34.57
Calcium, Total 144257.34 14.43
Calcium as CaO, 201960.28 20.20
Calcium as CaCO3 (CCE) 359515.33 35.95 2000.00 1.39 2.78
Magnesium, Total 2450.35 0.25
Manganese 75.56 0.01
Sulfur 1300.13 0.13
Percent Masture 50.00 •
These are typical values, and must be adjusted based upon specific site conditions -
DT is Dry Tons of Biosolids. - WT is Wet Tons of Biosolids.
CERTIFICATION: This blosoiid product has been produced by the Tam of CheraWs Wastewater .
Treatment Plant by a beab. ant process that pasteurized plant residual solids using high temperature
and lime (calcium oxide). The Town of Cheraw certifies that this biosolid complies with the
Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A product and has a metal
and nutrient content as presented above.
DIRECTIONS FOR USE This bioaolid is intneded to be used as a soil amendment The blosolid
land application race shall not exceed the most restrictive Maximum Application Rate as indicated in.
the table above. The application rate for nitrogen, phosphorus, potassium, and calcium is dependent
upon the crop gram and site soil characteristics. The user should contact the Clemson Extension
Service (843-623-2134) and/or the Sal Conservation Service (843.823-2187) for aasistanoe in
determining the proper application rate for each crop and site. In no case shall the land application
rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension
Service Circular N478 titled "Lime and Fertilizer Recommendations."
THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY.
AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES.
THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS
BIOSOLID PRODUCT.
Mr. Ricky D. Ingram, Public Utlllty Director
P. 0. Box 219; Cheraw, SC 29520
Telephone: 843-537-8440
FAX: 843-537-8442
Davis & Brown
PO Box 15038
Quin6y, SC 29506
(843) 665-6746 FAX: (843) 629-1444
Certificate of Analysis
Client: CHERAW, TOWN OF South Carolina Certification Number: 21117
P.O. BOX 219
CHERAW, SC 29520
Client #: 168 Receipt Date: 17-Jan-08
Contact: SHERRY TOLSON • Report Date: 31-Jan-08
Sample Date: 16-Jan-08 ,
SDG.#: SDG-058820 Approved By:�_,ir A.;.
Van Ward
Lab Director
Reporting
Parameter Result Limit Unit 'Method Flag Date Time Analyst
LSID-130336
1iu-5 ,o8= 00
Acid Digestion (Solids)
YES
EPA 200.2
1/18/2008
9:30
DH
pH (Waste)
12
S.U.
EPA�90451)
S16
1/22/2008
9:45
RBS
TCLP
PASS
P/F
SW-846 '
1/30/2.008
WSF
Ignitability
>170
Deg. F.
SW846 1010
S16
1/25/2008
10:30
KPB
Percent Moisture
53.0
0.1
wt%
SW846 3540
1/15/2008
17:15
BW
Aluminum, Total
5060
0.425
mg/kg
SW846 6010A
1/23/2008
16:29
DH
Arsenic, Total
<1.30
1.3
mg/kg
SW846 6010A
1/24/2008
0:00
JR
Cadmium, Total'
<0.212
0.212
mg/kg
SW846 601OA
1/22/2008
12:16
DH
Chromium, Total
14.9
0.212
mg/kg
SW846 6010A
1/22/2008
12:16
DH
Copper, Total
28.6
0.212
mg/kg
SW846 6010A
1/22/2008
12:16
DH
Lead, Total
1.80
1.1
mg/kg
SW846 6010A
1/21/2008'
15:18
DH
Molybdenum, Total
1.40
0.85
mg/kg
SW846 601OA
1/23/2008
16:29
DH
Nickel, Total
11.7
0.212
mg/kg
SW846 6010A
1/22/2008
12:16
DH
Zinc, Total
81.7
0.212
mg/kg
SW846 601OA
1/22/2008
12:16
DH
Mercury, Total
<0.049
0.049
mg/kg
SW846 7470A
1/18/2008
13:28
DH
Selenium, Total
<1.30
1.3
mg/kg
SW846 7741A
1/29/2008
13:11
JR
PCB
0.66
mg/kg
SW846 8080
S16
1/20/2008
22:20
CSU
Reactivity, Cyanide
<0.125
0.125
mg/kg
SW846 9010
S16
1/24/2008
12:34
LEM
Reactivity, Sulfide
<25
25
mg/kg
SW846 9030
S16
1/24/2008
10:15
LJN .
Paint Filter
PASS
P/F
SW8469095
S16
1/24/2008
7:00
KPB
Page 1
12065 Lebanon Rd.
0 Mt. Juliet, TN 37122
ENVIRONMENTAL i-800 767-5859
SCIENCE CORP. Fax (615) 756-5859
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Scott Fields January 29,2008
Davis 6 Brown
P.O. Box 15038
Quinby, SC 29506
ESC Sample #
L328165-02
Date Received January
18, 2008
Description
Site ID
Sample ID 130336
Project
#
Collected By
Collection Date 01/16/08
14:30
Parameter
Result
Det. Limit
Units
Method
Date/Time
Analyst
Dil.
Ignitability
See Footnote
Deg. F -
D93
01/25/08
1030
KPB
1`
pH
12.
su
9045D
01/22/08
0945
RBS
1
Paint Filter Test
See Footnote
9095B
01/24/080700
KPB
1
Reactive.CN (SW846 7.3.3.2)
BDL
0.125
mg/kg
9012B
01/24/08
1234
LEM
1
Reactive 'Sulf.(SW846'7.3.4.1)
BDL
25.
mg/kg
9034/9030
01/24/08
1015
KPB
1
TCLP Extraction
-
1311
01/21/08
1015
LJN
1
Mercury
BDL
0.0010
mg/1
7470A
01/22/08
1907
KBW
1
Arsenic
BDL
0.050
mg/1
6010B
01/21/08
1658
LRL
1
Barium
0.31
0.050
mg/1
6010B
01/21/08
1658
LRL
1
Cadmium
BDL
0.050
mg/1
6010B
01/21/08
1658
LRL
1
Chromium
BDL
0.050
mg/1
6010B
�01/21/08
1656
LRL
1
Lead
BDL
0.050
mg/1
6010E
01/21/08
1658
LRL
1
Selenium
0.092
0.050
mg/1
6010B
01/21/08
1658
LRL
1
Silver
BDL
0.050
mg/1
6010B
01/21/08
1658
LRL
1
TCLP ZHE Extraction
-
1311
01/19/08
1113
MVE
1
TCLP Volatiles
Benzene
BDL
0.050
mg/1
8260B
01/22/08
0325
BRW
1
Carbon tetrachloride
BDL
0.050
mg/1
8260B
01/22/08
0325
BRW
1
Chlorobenzene
BDL
0.050
mg/1
8260B
01/22/08
0325
BRW
1
Chloroform
BDL
0.25
mg/1
8260B
01/22/08
0325
BRW
1
1,2-Dichloroethane
BDL
0.050
mg/1
8260B
01/22/08
0325
BRW-
1
1,1-Dichloroethene
BDL
0.050
mg/1
8260B
01/22/08
0325
BRW
1
2-Butanone (MEK)
BDL
0.50
mg/1
8260B
01/22/06
0325
BRW
1
Tetrachloroethene
BDL
0.050
mg/1
8260B
01/22/08
0325
BRW
1
Trichloroethene
BDL
0.050
mg/l
8260B
01/22/08
0325
BRW
I
Vinyl chloride
BDL
0.050
mg/l
8260B
01/22/08
0325
BRW
1
Surrogate Recovery
Dibromofluoromethane
ill.
9 Rec.
8260B
01/22/08
0325
BRW
1
Toluene-d8
108.
9 Rec.
8260E
01/22/08
0325
BRW
1
4-Bromofluorobenzene
102.
8 Rec.
8260E
01/22/08
0325
BRW
1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL) .
Notes:
The reported analytical results relate only to the sample submitted
This report shall not be reproduced, except in full, without the written approval from ESC.
L328165-02 (IGNITABILITY)'- Did Not Ignite @ 170
L328165-02 (PAINT) - Contains No Free Liquid
Page 3 of 6
0
ENVIRONMENTAL
SCIENCE CORP.
REPORT OF ANALYSIS
Mr. Scott Fields
Davis 6 Brown
P.O. Box 15030
Quinby, SC 29506
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-761-5859
Fax (615) 758-5859
Tax I.D. 62-0814-189
Est. 1970
January 29,2008
ESC Sample #
L328165-02
Date Received January 18,
2008
Description
Site ID
Sample ID 130336
Project
#
Collected By
Collection Date 01/16/08 14:30
Parameter
Result
Det. Limit
Units
Method
Date/Time
Analyst
Dil.
TCLP Pesticides
Chlordane
BDL
0.0050
mg/l
8081A
01/24/08_2130
CSU
1
Endrin
BDL
0.0050
mg/l
8081A
01/24/08
2130
CSU
1
Heptachlor
BDL
0.0050
mg/1
8081A
01/24/08
2130
CSU
1
Lindane
BDL
0.0050
mg/1
8081A
01/14/08
2130
CSU
1
Methoxychlor
BDL
0.0050
mg/l
8081A
O1/24/08
2130
CSU
1
Toxaphene
BDL
0.010
mg/l
8081A
01/24/08
2130
CSU
1
Surrogate Recovery
Decachlorobiphenyl
67.6
% Rec.
6081A
01/24/08
2130
CSU
1
Tetrachloro-m-xylene
61.8
% Rec.
8081A
01/24/08
2130
CSU
1
TCLP Herbicides
2,4,5-TP (Silvex)
BDL
0.020
mg/1
8151A
01/28/OB
1351
JSW
10
2,4-D
BDL
0.020
mg/l
8151A
01/28/08
1351
JSW
10
Surrogate Recovery
2,4-Dichlorophenyl Acetic Acid
156.
% Red.
8151A
01/28/08
1351
JSW
10
TCLP Semi-Volatiles
1,4-Dichlorobenzene
BDL
0.10
mg/l
8270C
01/23/08
1629
CMJ
1
2,4-Dinitrotoluene
BDL
0.10
mg/l
8270C
01/23/08
1629
CMJ
1
Hexachlorobenzene
BDL
0.10
mg/1
8270C
01/23/08
1629
CMJ
1
Hexachloro-1,3-butadiene
BDL
0.10
mg/l
8270C
01/23/OB
1629
CMJ
1
Hexachloroethane
BDL
0.10
mg/l
8270C
01/23/08
1629
CMJ
1
Nitrobenzene
BDL
0.10
mg/l
8270C
01/23/08
1629
CMJ
1
Pyridine
BDL
0.10
mg/l
82,70C
01/23/08
1629
CMJ
1
m&p-Cresol
BDL
0.10
mg/1
8270C
01/23/08
1629
CMJ
1
o-Cresol
BDL
0.10
mg/l
8270C
01/23/00
1629
CMJ
1 .
Pentachlorophenol
BDL
0.10
mg/1
9270C
01/23/08
1629
CMJ
1
2,4,5-Trichlorophenol
BDL
0.10
mg/l
8270C
01/23/08
1629
CMJ
1
2,4,6-Trichlorophenol
BDL
0.10
mg/l
8270C
01/23/08
1629
CMJ
1
Surrogate Recovery
Nitrobenzene-d5
58.3
% Rec.
8270C
01/23/08
1629
CMJ
1
2-Fluorobiphenyl
53.1
% Rec.
8270C
01/23/08
1629
CMJ
1
p-Terphenyl-dl4
72.3
% Rec.
8270C
01/23/08
1629
CMJ
1
Phenol-d5
35.8
% Rec.
8270C
01/23/09
1629
CMJ
1
2-Fluorophenol
45.1
% Rec."
8270C
01/23/08
1629
CMJ
1
2,4,6-Tribromophenol
97.4
% Rec.
8270C
01/23/08
1629
CMJ
1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Notes:
The reported analytical results relate only to the sample submitted
This report shall not be reproduced, except in full, without the written approval from ESC.
All samples analyzed in adcordance with 40 CFR, Part 136.3
Reported: 01/29/08 14:06 Printed: 01/29/08 15:00
L328165-02 (IGNITABILITY) - Did Not Ignite @ 170
L328165-02, (PAINT) - Contains No Free Liquid
Page 4 of 6
Attachment A
List of Analytes with QC'Qualifiers
Sample # Analyte Qualifier
L328165-02 2,4,5-TP (Silvex) 0
2,4-D OJ5
2,4-Dichlorophenyl Acetic Acid J1
Methoxychlor J3
Page 5 of 6
Attachment B
Explanation of QC Qualifier Codes
Qualifier Meaning
J1 Surrogate recovery limits have been exceeded; values are outside,upper
control limits
J3 The associated batch QC was outside the established quality control range
for precision.
O (ESC) Sample diluted due to matrix interferences that impaired the ability
to make an accurate analytical determination. The detection limit is
elevated in order to reflect the necessary dilution.
J5 The sample matrix interfered with the ability to make any accurate
determination; spike value is high
Qualifier Report Information
ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and
as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted
by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical
results. Each qualifier is designated in the qualifier explanation as either EPA or ESC.
Data qualifiers are intended to provide the ESC client with more detailed information concerning
the potential bias of reported data. Because of the wide range of constituents and variety of
matrices incorporated by most EPA methods,it is common for some compounds to fall outside of
established ranges. These exceptions are evaluated and all reported data is valid and useable
unless qualified as 'R' (Rejected).
Definitions
Accuracy - The relationship of the observed value of a known sample to the
true value of a known sample. Represented by percent recovery and
relevant to samples such as: control samples, matrix spike recoveries,
surrogate recoveries, etc.
Precision - The agreement between a set of samples or between duplicate samples.
Relates to how close together the results are and is represented by
Relative Percent Differrence.
Surrogate - Organic compounds that are similar in chemical composition, extraction,
and chromotography to analytes of interest. The surrogates are used to
determine the probable response of the group of analytes that are chem-
ically related to the surrogate compound. Surrogates are added to the
sample and carried through all stages of preparation and analyses.
TIC - Tentatively Identified Compound: Compounds detected in samples that are
not target compounds, internal standards, system monitoring compounds,
or surrogates.
Page 6 of 6
DAVIS & BROWN
Data Qualifiers
Within the attached report, some analytical data may be reported as "Qualified
Data" .as indicated by a "Data Qualifier" or "flag" next to the result. The.data
qualifier "S" indicates that the analysis was performed by another SC
certified Lab. This table summarizes the South Carolina Lab Certification
Numbers for those laboratories.
S
South Carolina Lab Certification Number:
99040001
S1
South Carolina Lab Certification Number:
96031
S2
South Carolina Lab Certification Number:
23105
S3
South Carolina Lab Certification Number:
10120 ".
S4
South Carolina Lab Certification Number:
84002
S5
South Carolina Lab Certification Number:
3211.7
S6
Agricultural Service Laboratory Clemson University
S7
South Carolina Lab Certification Number:
36001
S8
**********
S9
South Carolina Lab Certification Number:
94014001; 94014002
S 10
South Carolina Lab Certification Number:
84009
S 11
South Carolina Lab Certification Number: 96023; 96026; 96031; 9800 1;73006
S12
AASHTO R18 Certified
S 13
South Carolina Lab Certification Number:
96012
S 14
South Carolina Lab Certification Number:
89002 -
S15
**********
S16
South Carolinalab Certification Number:
84004
S 17
South Carolina Lab Certification Number:
96037001
S 18
South Carolina Lab Certification Number:
95005
S 19
South Carolina Lab Certification Number:
23104
S20
South Carolina Lab Certification Number:
96027001
S21
South Carolina Lab Certification Number:
21005
S22
South Carolina Lab Certification Number:
24110
S23
South Carolina Lab Certification Number:
84001001
S24
South Carolina Lab Certification Number: 82014001
S25
Sam levas analyzed by Microsee s, Inc Laboratory
S26
North Carolina Lab Certification Number:
21 Wilson Division NC00120)
S27
South Carolina Lab Certification Number: 40569 I i'
Revision 06/05 Dataqual (SubLabs) .wpd
CHAIN
Page of __L__
OF CUSTODY RECORD
DAVIS & BROWN
Post Office an Ism 124 West McIver Road
Ouift South CamMa 29506 Florence. South Carotins 2M1
Telephone (843) 665-6746
5'8a2D
Use Codes in the boxes to indicate
whether sample was filtered or preserved.
�mmiiiilllllllllll
Neill
I
I
low M,.gm-.M-
Inn
M.-
I Mfj,
���Lq
"*its
R MINE
I NA/
"-'J-
WOW
• Program Area: D - Drinking Water / G - Grouodwator / S - Solid / W - Waste Water / N - NPDES / O - Other
A N I M A L W A S T E A N A L Y S I S R E P O R T
Agricultural Service Laboratory
LAB No. 10110 Clemson University
TOLSON, SHERRY ACCOUNT COCHSFL
PO BOX 219 DATE 02-01-2008
CHERAW SC 29520 CHERAWTO.WNOF656@BELLSOUTH.NET
SAMPLE NO. 0116085:OMANURE: OTHER STORAGE: UNCOVERED
-----------------RESULTS REPORTED ON AN AS -SAMPLED BASIS----------------------
lbs/ton
Ammonium Nitrogen 0.03 % 0.60
Organic Nitrogen .0.80 % 16.05
Nitrate Nitrogen 176.49 ppm 0.35
---------------------------------------------------------------'
INCORPORATED AVAILABLE NITROGEN ESTIMATE
10.67
SURFACE AVAILABLE
NITROGEN ESTIMATE
10.49
---------------------------------------------------------------
Phosphorus as P205
0.56
%
11.24
Potassium as K20
0.07
%
1.34
Calcium
13.36
%
267.28
Magnesium
0.23
%
4.54
Sulfur
0.12
%
2.41
Zinc
100.52
ppm
0.20
Copper
33.35
ppm
0.07
Manganese
70.87
ppm
0.14
Sodium
'123.68
ppm
0.25
Moisture
53.68
%
Calcium Carbonate
Equivalency 33.31
%
666.11
------------------------------------------------------------------------------
INCORPORATED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of
organic-N, and 100% of.nitrate-N (if determined). Assumes the manure will be
incorporated into the soil within hours of application. Assumes some loss of
ammonium-N during application and prior to incorporation.
SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
left on the surface of the soil with no incorporation by plowing or irrigation.
Available nitrogen calculations are estimates and if nitrate-N was not re-
quested the amount of available nitrogen may be slightly more than reported.
Also, the actual amount may be more or less than the estimate depending on the
composition of the manure, soil type, and environmental conditions.
All of the potash in the animal waste should be plant available in the first
year of application. Although not all of the phosphorous is available in the.
first year, its availability should be comparable to that in commercial
fertilizers.
The rate of animal waste to apply for crop production is dependent on the
nutrient content of the waste, method of application and incorporation, soil
test, crop to be grown, and previous manure applications. In most cases, the
plant available nitrogen content of the waste is used to determine the rate of
application.
The Agricultural Service Laboratory is a public service of Clemson University,
an affirmative action and equal opportunity educational institution.-
http://www.clemson.edu/aglabresultsICOCHSFLTOLSON,%20SHERRY0802011538451.htm 2/4/08
% moisture
% solids
lbs. solids/ton
lbs. solids/500 tons
53.68
46.32
926.4
463200
%
ppm
lbs/ton
%
ppm
Ibsfton
as -sampled
as-dampled
as -sampled
dry ton
dry ton
dry
Ammonium Nitrogen
0.03
300
0.6
0.064767
647.6684
1.295337
Organic Nitrogen
0.8025
8025
16.05
1.732513
17325.13
34.65026
Nitrate Nitrogen
0.017649
176.49
0.35298
0.038102
381,0233
0.762047
Incorporated Available Nitrogen Estimate
0.5335
5335
10.67
1.15177
11517.7
23.03541
Surface Available Nitrogen Estimate
0.5245
5245
10.49
1.13234,
11323.4
22.6468
Phosphorus as P205
0.562
5620
11.24
1,213299
12132.99
24.26596
Potassium as K20
0.067
670
1.34
0.144646
1446.459
2.892919
Calcium
13.364
133640
267.28
28.85147
288514.7
577.0294
Magnesium
0.227
2270
4.54
0.490069
4900.691
9.801382
Sulfur
0.1205
1205
2.41
0.260147
2601.468
5.202936
Zinc
0.010052
100.52
0.20104
0.021701
217.0121
0.434024
Copper
0.003335
33.35
0.0667
.0.0072
71.99914
0.143998
Manganese
0.007087
70.81
0.14174
0.0153
153.0009
0.306002
Sodium
0.012368
123.68
0.24736
0.026701
267.0121
0.534024
Calcium Carbonate Equivalency
33.3055
333055
666.11
71.90307
719030.7
1438.061
CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT
CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES
BIOSOLIDS SAMPLE DATEr,! _arc 9; 2008
Biosolids
Maximum
Maximum
Maximum
Maximum.
Metal
Allowable
Allowable
Application
Application
Content,
Metal
App. Rate,
Rate,
Rate,
METALS
ppm
Content, ppm
WAcre/Yr.
DT/AcrefYr.
WT/Acre/Yr.
Arsenic, Total
0.96 •
41.00
1.80
470.27
940.54
Cadmium, Total
0.96 •
39.00
1.70
444.14
888.29
Chromium, Total
84.14
1200.00
134.00
398.16
796.31
Copper, Total
41.38
1500.00
67.00
404.79
809.58
Lead, Total
1.41
300.00
, 13.00
2298.78
4597.56
Mercury, Total
0.08
17.06
0.75
2390.11
4780.22
Molybdenum, Total
1.26
18.00
0.80
158.90
317.81
Nickel, Total
25.00
420.00
18.70
167.00
374.00
Selenium, Total
0.96
36.00"
4.50
1175.68
2351.35
Zinc, Total
146.55
1525.00
- 125.00
213.24
426.47
PCB
BDL
1.60
• Actual metal content less than amount Indicated.
Biosdids
Nutrient
Content,
ppm
Biosdids
Nutrient
Content,
%
Crop/Soil
Requirement,
#/Acre ••
Maximum
Application
Rate,
DT/Acre/Yr.
Maximum
Application
Rate,
WT/Acre/Yr.
Ammonium Nitrogen
625.67
, 0.06
Organic Nitrogen
9899.00
0.99
Incorporated Available Nitrogen
6922.60
0.69
120.00
4633
8.67
Surface Available Nitrogen
6734.89
0.67
120.00
4.45
8.91
Phosphorus as P205
5841.08
0.58
80.00
3.42
6.85
Potassium as K20
1264.75
0.13
" 50.00
9.88
19.77
Calcium, Total
131051.13
13.11
Calcium as C20
183471.58
18.35.
Calcium as CaCO3 (CCE)
337705.58
33.77
2000.00
1.48
2.96
Magnesium, Total
2301.57
0.23
Manganese
67.04
0.01
Sulfur
1202.18
0.12
Percent Moisture
50.00
•• These are typical values and must be adjusted based upon specific site conditions
DT is Dry Tons of Blosdids. WT is Wet Tons of Blosdids.
CERTIFICATION: This biosdid product has been produced by the Town of Cho w's Wastewater
Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature
and lime (calcium oxide). The Town of Cheraw certifies that this biosdid complies with the
Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has a metal
and nutrient content as presented above.
DIRECTIONS FOR USE: This biosdid is intneded to be used as a sail amendment. The biosdid
land application rate shalt not exceed the most restrictive Maximum Application Rate as indicated in
the table above. The application rate for nitrogen, phosphorus, potassium, and calcium is dependent
upon the prop grown and site soil characteristics. The user should contact the Clemson Extension
Service (843-623-2134) and/or the Soil Conservation Service (843-623-2187) for assistance in
determining the proper application rate for each crop and site. in no case shall the land application
rate exceed the agronomic rate for the crop grown. •User should also refer to the Clemson Extension
Service Circular #476 titled "Lime and Fertilizer Recommendations."
THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY. ..
AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES.
THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING"OF THIS
BIOSOLID PRODUCT.
Mr. Ricky D. Ingram, Public Utility Director
P. O. Box 219; Cheraw, SC 29520
Telephone: 843-537-8440
FAX: 843-537-8442
Davis & Brown
PO Box 15038
Quinby, SC 29506
(843) 665-6746 FAX: (843) 629-1444
Certificate of Analysis
Client: CHERAW, TOWN OF
P.O. BOX 219
CHERAW, SC 29520
Client #: 168
Contact: SHERRY TOLSON
South Carolina Certification Number: 21117
Receipt Date: 20-Mar-08
Report Date: 15-Apr-08
Sample Date: 19-Mar-08 v
SDC #: SDG-059817
Approved By: f 'A- IZ/ �_.._.
Lab Sample ID: LSID-132469 Van Ward
Sample ID: B107S01,IDS_03=.F9'-08-500' Lab Director
Parameter
Result
Reporting
Limit
Unit
Method
Flag Date
Time
Analyst
Acid Digestion (Solids)
YES
EPA 200.2,
3/20/2008
10:50
DH
Percent Moisture
42.0
0.1
wt%
SW846 3540
3/24/2008
16:30
BW
Aluminum, Total
7040
0.558
mg/kg
SW846 6010B
4/7/2008
16: I8
DH
Arsenic, Total
<1.11
1.1 1
mg/kg
SW846 6010B
3/28/2008
12:03
DH
Cadmium, Total
<1.11
1.11
mg/kg
SW846 6010B
3/27/2008
16:01
DH
Chromium, Total
97.6
1.11
mg/kg
SW846 6010B
N27/2008
16:.01
DH
Copper, Total
48.0
1.11
mg/kg
SW846 6010B
3/27/2008
16:01
DH
Lead, Total
1.64
1.11
mg/kg
SW846 6010B
3/27/2008
16:01
DH
Molybdenum, Total
1.46
1.12
mg/kg
SW846 6010B
4/7/2008
16:18
DH
Nickel, Total
29.0
I. i l
mg/kg
SW846 6010B
3/27/2008
16:01
DH
Zinc, Total
170
0.14
mg/kg
SW846 6010B
4/10/2008
1 1:44
DH
Mercury; Total .
0.091
0,037
mg/kg
SW846 7470A
4/10/2008
9:24
DH
Selenium, Total
<l.l 1
1.1 1
mg/kg
SW846 7741A
3/28/2008
12:03
DH
PCB
BDL
mg/kg
SW846 8080
S16 3/28/2008
16:13
CSU
Page 3
1'2065 Lebanori Rd.
0
Mt. Juliet, TN 37122
ENVIRONMENTAL
(61'.) 758-5
-
1-800-767-S858
59
SCIENCE CORP.
Fax (615) 758-5659
Tar. I.D. 62-0814289
'
Est. 1970
REPORT
OF ANALYSIS
Mr. Scott Fields
March 31,2008
Davis 6 Brown
P.O. Box 15038
Quinby, SC 29506
#
ESC Sample L337765-01
Date Received March
25, 2008
Description 132469
Site ID
Sample ID 132469
Project
#
Collected By
Collection Date 03/19/08
13:20
Parameter
Dry Result
Det. Limit
Units
Method
Date
Analyst
Total Solids
47.5
8
254OG
03/29/08 1513
JDW
Polychlorinated Biphenyls
PCB 1016
BDL
0.18
mg/kg
8082
03/28/08 1613
CSU
PCB 1221
BDL
0.18
mg/kg
8082
03/28/08 1613
CSU
PCB 1232
BDL
0.18
mg/kg
8082
03/28/08 1613
CSU
PCB 1242
BDL
0.18
mg/kg
8082
03/28/OB 1613
CSU
PCB 1248
BDL
0.18
mg/kg
8082
03/28/08 1613
CSU
PCB 1254
BDL
0.18
mg/kg
8082
03/28/08 1613
CSU
PCB 1260
BDL
0.18
mg/kg
8082
03/28/08 1613
CSU
Results listed are dry weight basis.
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Laboratory Certification Numbers:
AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
AZ -0612, MN - 047-999-395, NY - 11742, NJ - TNO02, WI - 998093910
Note:
This report shall not be reproduced, except in full, without the written approval .from ESC.
The reported analytical results relate only to the sample submitted
Reported: 03/31/08 13:44 Printed: 03/31/08 13:45
Page 2 of 2
- —b— a va a
A N I M A L W A S T E A N A L Y S I
S R E P O R T
Agricultural Service Laboratory
LAB No. 30593
Clemson *University
TOLSON, SHERRY
ACCOUNT
COCHSFL
PO BOX 219
DATE
04-01-2008
CHERAW SC
29520 CHERAWTOWNOF656@BELLSOUTH.NET
SAMPLE N0.�03;0=9085.Q MANURE:
OTHER STORAGE: UNCOVERED
-----------------RESULTS
REPORTED ON AN AS -SAMPLED BASIS---------------
lbs/ton
Ammonium Nitrogen
0.07 %
1.40
Organic Nitrogen
1.11 %
22.15
Nitrate Nitrogen
---------------------------------------------------------------
337.88 ppm
0.68
INCORPORATED AVAILABLE NITROGEN ESTIMATE
15.49
SURFACE AVAILABLE
---------------------------------------------------------------
NITROGEN ESTIMATE
15.07
Phosphorus'as P205 0.65 %
13.07
Potassium as K20
0.14 %
2.83
Calcium
14.66 %
293.24
Magnesium
0.26 %
5.15
Sulfur
0.13 %
2,69
Zinc
109.64 ppm
0.22
Copper
36.92 ppm
0.07
Manganese
72.72 ppm
0.15
Sodium
190.20 ppm
0.38
Moisture
44.06 %
Calcium Carbonate
Equivalency 37.78 %
755.65
------------------------------------------------------------------------------
INCORPORATED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
incorporated into the soil within hours of application. Assumes some loss of
ammonium-N during application and prior to incorporation.
SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
left on the surface of the soil with no incorporation by plowing or irrigation.
Available nitrogen calculations are estimates and if nitrate-N was not re-
quested the amount of available nitrogen may be slightly more than reported.
Also, the actual amount may be more or less than the estimate depending on the
composition of the manure, soil type, and environmental conditions.
All of the potash in the animal waste should be plant available in the first
year of application. Although not all of the phosphorous is available in the
first year, its availability should be comparable to that in commercial
fertilizers.
The rate of animal waste to apply for crop production is dependent on the
nutrient content of the waste, method of application and incorporation, soil
test, crop to be grown, and previous manure applications. In most cases, the
plant available nitrogen content of the waste is used to determine the rate of
application.
The Agricultural Service Laboratory is a public service of Clemson University,
an affirmative action and equal opportunity educational institution.
** http://www.clemson.edu/agsrvlb **
http://www. clemson. edu/aglabresults/C OCHSFLT'OLSON,%20SHERRY0804010925 5 93 .h... 4/2/200R
% moisture _
% solids
lbs. solids/ton
lbs. solids/500 tons
44.06
55.94
1118.8
559400
%
ppm , .
lbstton.
%
ppm
Ibstton -
as -sampled
as -sampled
is -sampled
dry ton
dry ton
dry
Ammonium Nitrogen,
0.07
' 700
1.4
.0.125134
1251.341
2.502681
Organic Nitrogen
1.1075
11075
22.15
1.9798
19798
- 39.596
Nitrate Nitrogen
0.033788
337.88
0.67576
0.0604
604.0043
1.208009
Incorporated Available Nitrogen Estimate
07745
7745
15.49
1.384519
13846.19
27.69038
Surface Available Nitrogen Estimate
0.7635
7535
15.07
1.346970
13469.79
26.93958
Phosphorus as P205
0.6535
6535
13.07
1.168216
11682.16
23.36432
Potassium as K20
0.1415
1415
- 2.83
0.25295
2529.496
5.058992
Calcium
14.662
146620
293.24
26.21023
262102.3
524.2045
Magnesium
0.2575
2575
5.15
0.460315
4603.146
9.206292
Sulfur
0.1345
1345
2.69
0.240436
2404.362.4.808724.
Zinc
0.010964
109.64
0.21928
0.0196
195.9957
0.391991
Copper
0.003692
36.92
0.07384
0.0066
65.99928
0.131999
Manganese
0.007272
72.72
0.14544
0.013
129.9964
0.259993
Sodium
0.01902
190.2
0.3804
0.034001
340.0072
0.680014
Calcium Carbonate Equivalency
37.7825
377825
755.65
67.54112
675411.2.
1350.822
�March2008
CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT
CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES
BIOSOLIDS SAMPLE DATE^Mav: 12 2008�
Biosolids
Maximum '
Maximum Maximum
Maximum
Metal
Allowable
Allowable Application
Application
Content,
Metal
App. Rate, ' Rate, `
Rate,
METALS ppm
Content, ppm
#/Acre/Yr. DT/Acre/Yr.
WT/Acre/Yr.
Arsenic, Total
2.10 '
41.00
1.80
214.11
428.22
Cadmium, Total
6.21 •
39.00
1.70
2022.15
4644.29
Chromium, Total
15.45
1200.00
134.00
2168.14
4336.27
Copper, Total
28.89
1500.00
67.00
579.85
1159.70
Lead, Total
1.94
300.00
13.00
1676A9
-3352.97
Mercury, Total
0.10
17.00
0.75
1973.48
3946.97
Molybdenum, Total
9.69
18.00
0.80
20.63
41•.27
Nickel, Total
12.38
420.00
18.70
377.62
755.25
Selenium, Total
2.10
36.00
4.50
535.27
1070.55
Zinc, Tote)
93.78
1525.00
125.00
333.29
666.58
PCB
BDL
1.60
"Actual metal content less than amount Indicated.
Biosolids
Biosolids
Maximum
Maximum
Nutrient
Nutrient
Crop/Soil Application
Application
Content,
Content,
Requirement, Rate,
Rate,
ppm
%
IWAcre" DT/Acre/Yr.
WT/Acre/Yr. .
Ammonium Nitrogen
Organic Nitrogen
Incorporated Available Nitrogen
Surface Available Nitrogen
Phosphorus as P205
Potassium as K20
Calcium, Total
185.12
0.02
8029.43
0.80
4998.15
0.50
120.00
4942.61
0.49
120.00
5609.03
0.56
80.00
1082.93
0.11
50.00
144400.22
14.44
6.100 12.00
6.07 12.14
3.57 7.13
11.54 23.09
Calcium as Ca0
202160.31
20.22
Calcium as CaCO3 (CCE)
354452.05
35.45 2000.00 1.41 2.82
Magnesium, Total
2448.17
.0.24
Manganese
83.30
0.01
Sulfur
1147.72
0.11
Percent Moisture
50.00
These are typical values and must be adjusted based upon specific site conditions
DT is Dry Tons of Blosdids. ; WT is Wet Tons of Biosdids:
CERTIFICATION: This biosolid product has been produced by the Town of Cheraw's Wastewater
Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature
and lime (calcium oxide). The Town of Cheraw certifies that this biosolid compiles with the
Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has a metal
and nutrient content as presented above.
DIRECTIONS FOR USE: This biosclid is intneded to be used as a soil amendment. The biosdid
land application rate shall not exceed the most restrictive Maximum Application Rate as indicated in
the table above. The application rate for nitrogen, phosphorus, potassium, and calcium is dependent
upon the crop grown and site soil characteristics. The user should contact the Clemson Extension
Service (843-623-2134) and/or the Sal Conservation Service (843- i23-2187) for assistance in
determining the proper application rate for each crop and site. In no case shall the land application
rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension
Service Circular #476 titled "Lime and Fertilizer Recommendations."
THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY.
AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES.
THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS
BIOSOLID PRODUCT.
Mr. Ricky D. Ingram, Public Utility Director
P.O. Box 219; Cheraw, SC 29520
Telephone: 843-53741440
FAX: 843-537-8442
PRODUCT USER NAME:
Davis & Brown
PO Box 15038
Quinby; SC 29506
(843) 665-6746 FAX: (843) 629-1444
Certificate of Analysis
Client: CHERAW, TOWN OF South Carolina Certification Number: 21117
P.O. BOX 219
CHERAW, SC 29520
Client #: 168 Receipt Date: 22-May-08
Contact: SHERRY TOLSON Report Date: • 13-.tun-08
Sample. Date: 21-May-08
SDG #: SDG-06081 1 Approved By:
Lab Sample ID: LSID-134706 Van Ward
a Lab Director
r'(1 MQ
Sample ID: W 20,-
BL0 SOLIDS -
Parameter
Result
Reporting
Limit
Unit
Method
Flag Date
Time
Analyst
Acid Digestion (Solids)
YES
EPA 200.2
5/28/2008.
9:30
DH
Percent Moisture
47.9
0.1
wt%
SW846 3540
5/27/2008
16:40
BW
AILInllnunl, Total
4'180
438
mg/kg
SW846 601 OB
5/29/2008
1 1:30
DH
Arsenic, Total
<2.19
2.19
nlg/kg
SW846 601 OB
5/30/2008
1 1:20
DH
CadnliLim, Total
<0.2.19
0.219
nlg/kg
SW846 6010B
6/3/2008
13:51
DH
Chromium. Total
16.1
0.219
nlg/kg
SW846 601OB
6/3/2008
13:51
DH
Copper, Total
30.1 _
0.219
nlg/kg
SW846 601 OB
6/3/2008
13:51
DH
Lead. Total
2.02
1.3
mg/kg
SW846 601 OB
6/5/2008
14:23
DH
Molybdenum, Total
<10.1
10.1
mg/kg
SW846 6010E
6/10/2008 .
9:53
DH
Nickel, Total
12.9
0.219
mg/kg
SW846 601 OB
6/3/2008
13:51
DH
Zinc, Total
97.7
0.219
mg/kg
SW846 601 OB
6/3/2008
13:51
DH
Mercury, Total
0:099
0.014
nlg/kg
SW846 7470A
6/6/2008
10:27.
DH
Selenium, Total
<.2.19
2.19
mg/kg
SW846 7741A
5/30/2008
1 1:20
DH
PCB
BDL
nlg/kg
SW8468080
S16 5/29/2008
22:58
LSB
Page 1
0 1
ENVIRONMENTAL
SCIENCE CORP.
REPORT OF ANALYSIS
[Ar. '."co-t Fields
Dac'is & Brown
F.U. Box 15038
Quinby, SC 29506
.nilie[, TIJ t?I.
T.I:: I.h. A--'1F14
Eot . I.1-71,
June 02,2008
ESC Sample #
L347131-01
Date Received
May
23, 2008.
Description
Site ID
Sample ID
134706
Project
#
Collected By.
Collection Date
05/21/08
10:00
Parameter
Dry Result
Det. Limit
Units
Method
Date
Analyst
Total Solids
48.2
•.
2540C
05,130/08
1001
JDW
Polychlorinated
Biphenyls
PCB 1016
BDL
0.18
mg/l:g
8082
05/29/08
2258
LSB
FCB 1221
BDL
0.18
mg/kg
8082
05/29/08
2258
LSB
PCB 1232
BDL
0.18
mg/kg
8082
05/29/OB
2258
LSB
PCB 1243
BDL
0.18
mg/kg
8082
05/29/08
22258
LSB
PCB 1248
BDL
0.18
mg/l:g
8082
05/29/08
2258
LSB
PCB 1254
BDL
0.18
mg/kg
8082
05/29/08
2=58
LSB
PCE 1260
BDL
0.18
mg/kg
808Z
05/29/08
2258
LSB
Re:;ults listed are dry weight basis.
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Laboratory Certification Numbers:
AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
17Y - 90010, 1:YUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
AZ -0612, MN - 047-999-395, NY - 11742, NJ - TNO02, WI - 998093910
Nnte:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
P.eporr.ed: 061 02/OS 09:38 Printed: 06/02/08 09:38
Page 2 of 2
DAVIS & BROWN
Data Qualifiers
Within the attached report, some analytical data may be reported as "Qualified
Data" as indicated by a "Data Qualifier" or "flag" next to the result. The data
qualifier "S" indicates that the analysis was performed by another SC
certified Lab. This table summarizes the South Carolina Lab Certification
Numbers for those laboratories.
S
South Carolina Lab Certification Number:
23101
S 1
South Carolina Lab Certification Number:
93013
S2
South Carolina Lab Certification Number:
23105
S3
South Carolina Lab Certification Number:
10120
S4
South Carolina Lab Certification Number:
84002
S5
South Carolina Lab Certification Number:
32117
S6
Agricultural Service Laboratory Clemson University
S7
South Carolina Lab Certification Number:
36001
S8
**********
S9
South Carolina Lab Certification Number:
94014001; 94014002
S 1 O
South Carolina Lab Certification Number:
84009
S1 1
South Carolina Lab Certification Number: 96023; 96026; 96031; 98001, 73006
S 12
AASHTO R18 Certified
S 13
South Carolina Lab Certification Number:
96012
S 14
South Carolina Lab Certification Number:
89002
S15
*********
S 16
South Carolina Lab Certification Number:
84004
S 17
South Carolina Lab Certification Number:
96037001
S 18
South Carolina Lab Certification Number:
95005
S 19
South Carolina Lab Certification Number:
23104
S20
South Carolina Lab Certification Number:
96027001
S21
South Carolina Lab Certification Number:
21005
S22
South Carolina Lab Certification Number:
24110
S23
South Carolina Lab Certification Number:
84001001
S24
South Carolina Lab Certification Number: 82014001
S25
Sample was analyzed by Microsee s, Inc Laboratory
S26
North Carolina Lab Certification Number:
21 (Wilson Division NC00120)
S27
South Carolina Lab Certification Number: 40569
RC%iswn (K)A)? 1XIMLI of (SUTA1111R) .wpd
CHAIN OF CUSTODY RECORD
Nge_L of _L
DAVIS & BROWN
Post Office Boot 15M 124 WON Mckw Road
OWnby. S011M Carolina WM mle ". scum cam= moll
Tammnm gak.6"'m
L-11-1 NAM/ Facility Nam
TOWAI Of
SAMEANALYSIS REQUIRED (z)—m temttka Dirt to specify tpeube compounds ar tegbods,
Use Codes in the boxes to indicate
I
011mv1
whether sample was filtered or preserued.
Code. HNO3 w A H2SO4 = D
AMA
5
JS
EE
€
HCLol L& A&,., Ff
NAOH.0 ZINCACETATE G
SAMPLE ID
DATE
TE
W
REMARKS
LAB ID
0,
fill
Rd' NATW)- Date Time Rdinquisbed by (SiGNKIURl:�• DaceRdWW�by (S�IGNATUREI-
TIM
Recci IS NATURE? Due Tuve by (SIGNATURE .
raw Rccd%vd by (SIMM—URE)e
ICED Lk:o
746S MID
t
6 a4m commen s elf
(;� C3 NO a N=
Redalamry
• Pr mm Am2. A.
A N I M A L W A S T E A N A L Y S I S R E P O R T
Agricultural Service Laboratory
LAB No. 50992 Clemson University
TOLSON, SHERRY ACCOUNT COCHSFL
PO BOX 219 DATE 06-04-2008
CHERAW SC 29520 CHERAWTOWNOF656@BELLSOUTH.NET
SAMPLE NO'y Qr521V8'S,0 MANURE: OTHER STORAGE: UNCOVERED
-----------------RESULTS REPORTED ON AN AS -SAMPLED BASIS----------------------
lbs/ton
Ammonium Nitrogen
0.02
%
0.40
Organic Nitrogen
0.87
%
17.35
Nitrate Nitrogen
-----------------------------------------=---------------------
19.99
ppm
0.04
INCORPORATED AVAILABLE NITROGEN ESTIMATE
10.80
SURFACE AVAILABLE
---------------------------------------------------------------
NITROGEN ESTIMATE
10.68
Phosphorus as P205
0.61
%
12.12
Potassium as K20
0.12
%
2.34
Calcium
15.60
%
312.02
Magnesium
0.26
%
5.29
Sulfur
0.12
%
2.48
Zinc
102.64
ppm
0.21
Copper
55.64
ppm
0.11
Manganese
89.67
ppm
0.18
Sodium
231.21
ppm
0.46
Moisture
45.98
%
Calcium Carbonate
Equivalency 38.30
%
765.90
------------------------------------------------------------------------------
INCORPORATED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
incorporated into the soil within hours of application. Assumes some loss of
ammonium-N during application and prior to incorporation.
SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N'(if determined). Assumes the manure will be
left on the surface of the soil with no incorporation by plowing or irrigation.
Available nitrogen calculations are estimates and if nitrate-N was not re-
quested the amount of available nitrogen may be slightly more than reported.
Also, the actual amount may be more or less than the estimate depending on the
composition of the manure, soil type, and environmental conditions.
All of the potash in the animal waste should be plant available in the first
year of application. Although not all of the phosphorous is available in the
first year, its availability should be comparable to that in commercial
fertilizers.
The rate of animal waste to apply for crop production is dependent on the
nutrient content of the waste, method of application and incorporation, soil
test, crop to be grown, and previous manure applications. In most cases, the
plant available nitrogen content of the waste is used to determine the rate of
application.
The Agricultural Service Laboratory is a public service of Clemson University,
an affirmative action and equal opportunity educational institution.
http://www.clemson.edu/aglabresults/COCHSFLTOLSON,%20SHERRY0806041.638041.htm 6/6/08
% moisture
% solids
lbs. solids/ton
lbs. solids/500 tons
45.98
54.02
1080.4
540200
%
ppm
lbs/ton
% .
ppm
lbs/ton
as -sampled
as -sampled -
as -sampled
d ton
d ton
dry
Ammonium Nitrogen
0.02
200
0.4
0.037023
370.2332
0.740466
Organic Nitrogen
0.8675
8675
17.35
1.605881
16058.87
32.11773
Nitrate Nitrogen
0.001999
19.99
0.03998
0:0037
37.00481
0.07401
Incorporated Available Nitrogen Estimate
0.54
5400
10.8
0.99963
9996.298
19.9926
Surface Available Nitrogen Estimate
0.534
5340
10.68
0.988523
9885.228
19.77046'
Phosphorus as P205 .
0.606
6060
12.12
1.121807
11218.07
22.43613
Potassium as K20
0.117
1170
2.34
0.216586
2165.864
4.331729
Calcium
15.601
156010
•312.02
28.88004
288800.4
577.6009
Magnesium
0.2645
2645•
5.29
0.489633
4896.335
9.792669
Sulfur
0.124
1240
2.48
0.229545
2295.446
4.590892
Zinc
0.010264
102.64
0.20528
0.019
190.0037
0.380007
Copper
0.005564
55.64
0.11128
• 6.0103
102.9989
0.205998
Manganese
0.008967
89.67
0.17934
0.016599
165.9941
0.331988
Sodium
0.023121
231.21
0.46242
0.042801
428.0081
0.856016
Calcium Carbonate Equivalency
38.295
382950
.765.9
70.89041
708904.1
1417.808
Mayw200
CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT
CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES
BIOSOLIDS SAMPLE DATE,•. y 15 200
Biosolids
Maximum
Maximum
Maximum
Maximum
Metal
Allowable
Allowable
Application
Application
Content,
Metal
App. Rate,
Rate,
Rate,
METALS ppm
Content, ppm
#/Acre/Yr.
DT/Acre/Yr.
WT/Acre/Yr.
Arsenic, Total 1.24 '
41.00
1.80
363.95
727.89
Cadmium, Total 1.24 '
39.00
1.70
343.73
687.46
Chromium, Total 15.08
1200.00
134.00
2222.09
4444.17
Copper, Total 16.70
1500.00
67.00
1002.82
2005.65
Lead, Total 1.24 '
300.00
13.00
2628.51
5257.02
Mercury, Total 0.04 '
17.00
0.75
4432.69
8865.38
Molybdenum, Total 4.97 '
18.00
0.80
40.26
80.52
Nickel, Total 16.59
420.00
18.70
281.72
563.44
Selenium, Total 1.24 '
36.00
4.50
909.87
1819.74
Zinc, Total 68.00
1525.00
125.00
459.53
919.06
PCB BDL
1.60
' Actual metal content less than amount indicated.
Biosolids
Biosolids
Maximum
Maximum
Nutrient
Nutrient
Crop/Soil
Application
Application
Content,
Content,
Requirement,
Rate,
Rate,
ppm
%
#/Acre "
DT/Acre/Yr.
WT/Acre/Yr.
Ammonium Nitrogen
518.13
0.05
Organic Nitrogen
10590.67
1.06
Incorporated Available Nitrogen
6782.38
0.68
120.00
4.42
8.85
Surface Available Nitrogen
6626.94
0.66
120.00)
4.53
9.05
Phosphorus as P205
5383.42
0.54
80.00
' 3.72
7.43
Potassium as K20
1989.64,
0.20
50.00
6.28
12.57
Calcium, Total
126005.18
12.60
Calcium as CaO
176407.25
17.64
Calcium as CaCO3 (CCE)
279067.36
27.91
2000.00
1.79
3.58
Magnesium, Total
2202.07
0.22
Manganese
129.53
0.01
Sulfur
1150.26
0.12
Percent Moisture
.50.00
" These are typical values and must be adjusted based upon specific site conditions
DT is Dry Tons of Biosolids. WT is Wet Tons of Biosolids.
CERTIFICATION: This biosolid product has been produced by the Town of Cheraw's Wastewater
Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature
and lime (calcium oxide). The Town of Cheraw certifies that this biosolid complies with the
Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has a metal
and nutrient content as presented above.
DIRECTIONS FOR USE: This biosolid is intneded to be used as a soil amendment. The biosolid
land application rate shall not exceed the most restrictive Maximum Application Rate as indicated in
the table above. The application rate for nitrogen, phosphorus, potassium, and calcium is dependent
upon the crop grown and site soil characteristics. The user should contact the Clemson Extension
Service (843-623-2134) and/or the Soil Conservation Service (843-623-2187) for.assistance in
determining the proper application rate for each crop and site. In no case shall the land application
rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension
Service Circular #476 titled "Lime and Fertilizer Recommendations."
THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY.
AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES.
THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS
BIOSOLID PRODUCT.
Mr. Ricky D. Ingram, Public Utility Director
P. O. Box 219; Cheraw, SC 29520
Telephone: 843-537-8440
FAX: 843-537-8442
PRODUCT USER NAME:
ADDRESS:
INTENDED USE:
LOCATION OF USE:
QUANTITY RECEIVED:
RECEIVED BY:
.Davis & Brown
PO Box 15038
Quiuby, SC 29506
(843) 665-6746 FAX: (843) 629-1444
Certificate of Analysis
Client: ('FIERA W. TOWN OF South Carolina Certification Number: 21117
1'.0.B0X 219
C'HRRA W. SC29520
Client #: 168
Contact: SHERRY TOLSON
Sample Date:
SDC #: SDG-06171 1
Receipt Date: 17-.ILII-08
Report Date: 04-Aug-08
Approval By:
Van Ward
Lab Director
Reporting
Parameter Result Limit Unit 'Method Flag Date Time Analyst
LSID-136477 1001-F
fluoride- IC 3.09 0.2 mg/L EPA 300.0 S 1 1 7/23/2008 15:25 JEM
LSID-136478 1001-C
Acid Di-estion ( Liquids)
YES
EPA 200.2
7/22/2008
10:00
DH
Chromium. TOtal
-c0,005
0.005
m/L
EPA 200.7
W25/2005
17:18
DH
Copper. "I'utal
0.045
0.005
mg/L
EPA 200.7
7/25/2008
17:1 S
DH
Mun-ancse, 'total
0.026
0.005
nig/L
EPA 200.7
7/25!2008
17: I S
DH
Zinc, Tot:ll
0.041
0.005
mg!L
EPA 200.7
7/25/2008
17:1 S
DH
LSID-136479
E F F. 7-15-08-001
lcid Digestion (Liquids)
YES
EPA 200.2
7/2212008
10:00
DH
Silver. Total
=•0.005 0.005
mg/L
EPA 200.7
7/29/2008
12:16
DH
LSID-136480
IOUSOR I US-67=15=08=50
Acid Dicc,; ion (Solids)
YES
EPA 200.2
7/22/2008
10:00
DH
PUCCnt N1101Snu-c
53.9 0.1
wt'%I
SW8403540
7/15,12008
16:45
BW
Aluminum. Total
2750 4.0
mg/k;,
SW840 601 OB
7/23/2008
1 1:56
DH
Arsenic. Total
•.-.1.14 1.14
mg/kg
SW840 601 OB
7/25/200S
14:00
DH
Page 2
Davis & Brown
PO Box 15038
Quimby, SC 29506
(843) 665-6746 FAX: (843) 629-1444
Certificate of Analysis
Client: CHERAW, TOWN OF South Carolina Certification Number: 21117
P.0.130X 219 t
CH ERA W. SC 29520
Client #:
16\
Receipt Date:
17-.1u1-08
Contact:
SHERRY TOLSON
Report Date:
04-Aag-08
Sample Date:
15-Jul-08
'
SDC #:
SD(.;-()6 171 I
Approved By:
N1:1II
.Ward
Lab Director
Reporting
Parameter
Result
Limit
Unit
Method Flag Date
Time
Analyst
C'admiunt, focal
•--,1.14
1.14
mg/kg
SWS46601013
7/25/2008
17:I8
DH
C'hrontiunt. "Total
13.9
1.14
mg/kg
SW846 601OB
7/25/2008
17: I S
DH
{'olthcr.'fnlal.
15.4
1.14
mg/kg
SW840601OB
7/25/2008
17:I8
DH
Lead. "total
•c1.14
1:14
ntg/kg '
SW840 GOIOB
7/251'2008
17:I8
DH
Mo IVIIdcnunt. Tol:tl
Z#ice 4s,10
4.6
mg!kg.
SWS46 601013
7/23/2008
11:56
DH
Nickel. Total
15.3
1.14
mg/kg
SW8406010B
7/25/2008
17:I8
DH
Zinc. Toml
62.7
1.14
mg/kg
SW846 601 OB
7/25/2008
17:1 S
DH
Mercury.] owl
:0.039
0.039
mill/kg
SWS46 7470A
7/22/2008
14:10
DH
Selenium, Tidal
=1.14
1.14
ma 11(g
SW846 7741A
7/25/2008
14:00
DH
PCC13
BDL
mg/kg
SWS46 SOSO S16
7/24/2008
0:45
LSB
Page 3
12,11.�. L.�t,.ot ,i r:•I.
ENVIRONMENTAL
SCIENCE CORP.
REPORT OF ANALYSIS
Hi.. Scott Fields July 24,2008
Davis L Brown
P.O. Lax 15038
Qllinby, SC :Ci506
ESC ample # L.355817-01
P,:te Received July
18, 2008
Description
Site
ID
,:ample ID 13t;480
Project # .
Collected By
Coll,>r_tion Date 07/15/08
13:40
Pai.Imeter
Dry Result Det..Limit
Units
Method
Date
Analyst
Total solid::
43.9
254OG
07/23/08 2101
JDW
Pol_hlor_aated Eiphenyls
F'Cc 101r;
BDL
0.39
mg/kg
8010--
07/24/08 0045
LSB
FCc 1221
EDL
0.39
mg/kg
8082
07/-24/08 0045
LSE
PCB 1232
BDL
0.39
mg/kg
8082
07/24/08 0045
LSE
PCE6 1214:'
EDL
0.39
mg/kg
8062
07/_-'/08 004S
LSP.
PCL 11--40
BDL
0.39
mg/kg
8082
07,124/08 0045
L:E
PCF.. 1254
EDL
0.39
mg/kg
808,
07/24/08 9045
L_'B
BDL
0.39
mg/kg
8082
07/24/03 0045
LSE
P.e!'uLts listed are dry weight basis.
BDL Blow Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Laboratory Certification Numbers:
AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
E'' - 90010, EYOST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
blote: AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - !)98093910
This: Leport shall not be reproduced, except in full, without the written approval from ESC.
Thy Lehorted analytical results relate only to the sample submitted
F-pnrt�[I: 07/24/08 17:28 Printed: 07/2--4/08 17:29
L�S5817-01 rPCBSt - IS/SUP.R failed on lower dilution.
Page of 4
Attachment A
List of Anal yt es with QC Qualifiers
Analyte Qualifier.
PCB 1016
PCB 12 2 1
PCB 1232 C)
PCB 1242 0
PCB 1248 0
PCB 12154 0
PCB 1260 0
9
P,ige 3 of 4
Attachment !
Explanation of QC Qualifier Codes
I
uilrfier Meaning
(ESC) Sample diluted due to matrix; interferences that impaired the ability
to make an accurate analytical determination. The detection limit is
ele•rated in order to reflect the necessary dilution.
Qualifier Report Information '
utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and
.i.,: required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted
Yr, ESC:, we have implemented ESC qualifiers to provide more information pertaining to our analytical
re>ult::. Each Qualifier is designated in the qualifier explanation as either EPA or ESC.
Mitzi qualifiers, are intended to provide the ESC client with more detailed information concerning.
the pr.tential bias of reported data. Because of the wide range of constituents and variety of
matrices'incorporated by most EPA methods,it is common for some compounds to fall outside of
established ranges. These exceptions are evaluated and all reported data is valid and useable
unlss qualified as 'R' (Rejected).
Definitions
c'::irric,, - The :e_sitionr,hip of the observed value of a known example to the
tree value of a known sample. Represented by percent recovery and
_+>levant to samples such as: control samples, matrix spike recoveries,
.,Arrogate recoveries, etc.
PsFcie,_or. - The agreement between a set of samples or between duplicate samples.
Relates to how close together the results are and is represented by
Felatcve Percent Differrence.
._eog.,%e - organic compounds that are similar ,n chemical compos_t;.on, extract --on.,
ond.chromotography to analytes of interest. The surrogates are u:,ed to
d,�term,ne the probable response of the group of analytes that are Chem-
ically related to the surrogate compound. Surrogates are added to the
jatiple and Carried through all stages of preparation and analyzes.
i
- Te:•:tatively Ident-,fied Compound: Compounds detected it. ,--ample:, that are
not'target compounds, infernal standards, system monitoring co:rpo.:ndz;,
Page 4 of 4
DAVIS & BROWN
r Data Qualifiers
Within the attached report, some analytical data may be reported as "Qualified
Data" as' indicated by "Data Qualifier" or "flag" next to the result: The. data.
qualifier "S" indicates that the analysis was performed by another -SC
certified Lab. This table summarizes the South Carolina_ Lab Certification
Numbers for those laboratories.
S
South Carolina Lab Certification Number:
23101
S 1
South Carolina Lab Certification Number:
93013
S2
South Carolina Lab Certification Number:
23105
S3
SoUth Carolina Lab Certi ficati on'Number:
10120 .
S4
South Carolina Lab Certification Nurriber:
84002
S5
South Carolina Lab Certification Number:
32117
96,
Agricultural Service Laboratory Clemson Uhiversit
ST
South Carolina Lab, Certificatioh' Number:
_
36001
S8
S9
South Carolina Lab Certification Number:
94014001; 94014002
S 10
South Carolina Lab Certification Number:
84009
S I 1
South Carolina Lab.Certif cation :Number: 96023; 96026; 96031; 98001: 73006
S 12
AASHTO R 18 Certified
S 13
SOL th Carolina Lab Certification Number:
96012
S 14
South Carolina Lab Certification Number:
89002.
S15
********
S 16
South Carolina Lab Certification:Niunber:
84004 .
S 17
South Carolina Lab Certification Number:
96037001
S18
South Carolina Lab Certification Number:
95005
S 19
South Carolina Lab Certification Number:
23104
S20
`South Carolina Lab Certification Number:.
96027001
S21
South Carolina Lab Certification Number:
2100.5 -
S22
South Carolina.Lab Certification Number:
24110
S23
South Carolina Lab Certification Number:
840.01001
S24
South Carolina Lab Certification Number: 82014001
-S25
Sam le was analyzed by _Microsee s, Inc Labora'tory
S26
North Carolina Lab Certifi.cation.Number:
21 (Wilson Division NC001"20)
S27
South Carolina Lab Certification Number: 40569
Revision tNv'05 Dataguul ISuhLabsl .wpd
CHAIN OF CUSTODY RECORD
Page__L__ of I
DAVIS & BROWN
Pose Olf1w Box 15M 124 West McIver Road
t wft South CamkM 2V" Flm m*. South Cmulkm 2tl I
Taleph= (M) 60.6748
_ CQ lit 1
Em� �_ MII
M�
Use Codes in the boxes to indicate
"Mr'
dtered or preserved.
PO
M�W
MORM
M-11i�
"°��
wd-f
ilk
- Program Area: D - Drinking Wata / G - Groundwater / S - Solid / W - Waste Water / N - NPDES / O - Other
Page 1 of 1
A N I M A L W A S
T E A
N A L Y S I
S R E P O R T
Agricultural
Service
Laboratory
LAB No. 71184 Clemson University
TOLSON, SHERRY
ACCOUNT
c
COCHSFL
PO BOX 219
DATE
07-29-2008
CHERAW SC 29520
CHERAWTOWNOF656@BELLSOUTH.NET
SAMPLE NO.07fi.5Q 58 MANURE: OTHER STORAGE:
UNCOVERED
--RESULTS REPORTED ON
AN AS -SAMPLED BASIS----------------------
lbs/ton
Ammonium Nitrogen
0.05
%
1.00
Organic Nitrogen
1;02
%
20.44
Nitrate Nitrogen
---------------------------------------------------------------
7.72
ppm
0.02
INCORPORATED AVAILABLE NITROGEN ESTIMATE
13.09
SURFACE AVAILABLE NITROGEN ESTIMATE
.12.79
---------------------------------------------------------------
Phosphorus as P205
0.52
%
10.39
Potassium as K20
0.19
%
3.84
Calcium
12.16
%
243.19
Magnesium
0.21
%
4.25
Sulfur
0.11
%
2.22
Zinc
75.27
ppm
0.15
Copper
30.40
ppm
0.06
Manganese
125.46
ppm
0.25
Sodium
185.29
ppm
0.37
Moisture
51.75
%
Calcium Carbonate Equivalency
26.93
%
538.60
------------------------------------------------------------------------------
INCORPORATED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined)., Assumes the manure will be
incorporated into the soil within hours of application. Assumes some loss of
ammonium-N during application and prior to incorporation.
SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
left on the surface of the soil with no incorporation by plowing or irrigation.
Available nitrogen calculations are estimates and if nitrate-N was not re-
quested the amount of available nitrogen may be slightly more than reported.
Also, the actual amount may be more or less than the estimate depending on the
composition of the manure, soil type, and environmental conditions.
All of the potash in the animal waste should be plant available in the first -
year of application . Although not all of the phosphorous is available in the
first year, its availability should be comparable to that in commercial
fertilizers.
The rate of animal waste to apply for crop production is dependent on the
nutrient content of the waste, method of application and incorporation, soil
test, crop to be grown, and previous manure applications. In most cases, the
plant available nitrogen content of the waste is used to determine the rate of
application.
The Agricultural Service Laboratory is a public service of Clemson University,
an affirmative action and equal opportunity educational institution.
** http://www.clemson.edu/agsrvlb **
I'AA . //, .....,ao.....,,.., mnT cnt,r ,A, .,�,..�..�...,
% moisture
• solids
lbs. solids/ton
lbs. solids/500 tons'
51.75
48.25
965
482500
% ppm
lbs/ton
%
ppm
Ibs/ton
as -sampled as -sampled
as -sampled
dry ton
dry ton
dry
Ammonium Nitrogen
0.05
500
1
0.103627
1036.269
2.072539
Organic Nitrogen
1.022
10220
20.44
2.118135
21181.35
42.36269
Nitrate Nitrogen
0.000772
7.72
0.01544
0.0016
16
0.032
Incorporated Available Nitrogen Estimate
0.6545
.6545
13.09
1.356477
13564.77
27.12953
Surface Available Nitrogen Estimate
0.6395
6395
12.79
1.325389
13253.89
26:50777
Phosphorus as-P205
0.5195
5195
10.39
1.076684
10766.84
21.53368
Potassium as K20
0.192.
1920
3.84
0.397927
3979.275
7.958549
Calcium
12.1595
121595
243.19
25.20104
252010.4
504.0207
Magnesium
0.2125
2125
14.25
0.440415
4404.145
8.80829
Sulfur
0.111
1110
2.22
0.230052
2300.518
4.601036
Zinc
0.007527
75.27
0.15054
0.0156
156
0.312
Copper
0.00304
30.4
.0.0608
0.006301
63.00518
0.12601
Manganese
0.012546
125.46
0.25092
0.026002
260.0207
0.520041
Sodium
0.018529 •
185.29
0.37058
0.038402
384.0207
0.768041
Calcium Carbonate Equivalency
26.93
269300
538.6
55.81347
558134.7
1116.269
V-
,luly 2008=:
CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT
CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES
BIOSOLIDS SAMPLE DATE,$eptenitier;l.7;2008
Biosolids
Maximum
Maximum
Maximum
Maximum
Metal
Allowable
Allowable
Application •
Application
Content,
Metal
App. Rate,
Rate,
Rate,
METALS
ppm
Content, ram
N/AcrelYr.
DT/Acre/Yr.
WT/Acre/Yr.
Arsenic, Total
1.44 "
41.00
1:86
312.79
625.59
Cadmium, Total
1.44 •
39.00
1.70
295.42
590.83
Chromium, Total
88.15 .
1200.00
134.00
380.02
760.05
Copper, Total
30.11
1500.00
67.00
556.24
1112.48
Lead, Total
1.44 •
300.00
13.00
2259.07
4518.14
Mercury, Total •
0.08 •
17.00
0.75
2311.96
4623.91
Molybdenum, Total
1.78
18.00
0.80
112.54
225.08
Nickel, Total
18.12
420.00
18.70
257.94
515.89
Selenium, Total
1.44
_ 38.00
4.50
781.99
1563.97
,.Zinc, Total
90.27
1525.00
125.00
346.19
692.38
PCB
BDL
1.60
Actual metal content less than amount Indicated.
Biosolids
Biosollds
Maximum,
Maximum
Nutrient
Nutrient
Crop/Soil
Application
'Application
Content,
Content,
Requirement,
Rate,
Rate,
aam
%
#/Acre "
DT/Acre/Yr.
WT/Acn31Yr.
Ammonium Nitrogen
1028.81
0.10
Organic Nitrogen
4550.75
" 0.46
Incorporated Available Nitrogen
3552.61
0.36
120.00
8.44
'16.89
Surface Available Nitrogen
3244.17
0.32
_ 120.00
9.25
18.49
Phosphorus as P205
4235.25
0.42
80.00
4.72
9.44
Potassium as K20
723.59
0.07
50.00
17.27
34.55
Calcium, Total
119694.79
11.97
Calcium as COO
167572.70
16.76
Calcium as CaCO3 (CCE)
304187.24
30.42
2000.00
1.64
3.26
Magnesium, Total
1899.86
0.19
Manganese
78.88
0.01
Sulfur
896.49
0.09
Percent Moisture
50.00
These are typical values and must be adjusted based upon specific site conditions
DT is Dry Tans of Biosolids. WT is Wet Tons of Biosoiids.
CERTIFICATION: This biosolid product has been produced by the Town of Cheraw's Wastewater
Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature
and lime (calcium o)dde). The Town of Cheraw certifies that this blosolld complles.with the
Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has a metal
and nutrient content as presented above.
DIRECTIONS FOR USE: This blosoiid Is intneded to be used as a soil amendment. The biosoild
land application rate shall not exceed the most restrictive Maximum Application Rate as indicated in
the table above. The application rate far nitrogen, phosphorus, potassium, and calcium is dependent
upon the crop grown and site soil characteristics. The user should contact the Clemson Extension
Service (843-623-2134) and/or the Soil Conservation Service (843-623-2187) for assistance In
determining the proper application rate for each crop and site. In no case shall the land application
rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension
Service Circular #476 titled "Lime and Fertilizer Recommendations."
THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY.
AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES.
THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS
BIOSOLID PRODUCT.
Mr. Ricky D. Ingram, Public Utility Director
P. 0. Bar 219; Cheraw, SC 29520
Telephone: 843-537-8440
FAX: 843-5374442
Davis & Brown
PO Box 15038
Quiuby, SC 29506
(843) 665-6746 FAX: (843) 629-1444
Certificate of Analysis
Client: CHERAW, TOWN OF South Carolina Certification Number: 21117
P.O.130X 219
CHERAW. SC 29520
Client #: 168 Receipt Date: 18-Sep-08
Contact: SHERRY TOLSON Report Date: 08-Oct-08
Sample Date: I 71--sep-08
Approved By:
Lab tiamplc ID: I.SID-135704
Van Ward
'Sample II): f)'tiUL D ?)f7=G)S� -5 0 ~
Lab Director
Reporting
Parameter
Result
Limit
Unit
Method
Flag Date
Time
Analyst
\cnl I)i_x:unn !S ,lids!
YES
EPA 200.2
9/22/2008
1 1:00
DH
I',rccn! \•Ini:aurc
29.1
(l.l
��t:„
SW8403540
9/23/2008
17:00
13\V
0310
164
mg/kg
SWS466010B
9!29!-?()OS
I0:47
DH
Al-scn!c. fatal
2.04
2.04
mg/kg
SW846 601OB
9/22/2008
16:44
DH
('aLlmium. total
-:2.04
2.04
mg/kg
SW846 601OB
9/23/2008
10:45
DFI
('11f„mltttt). •f,,lal
125
2.04
mpg/kg
SWS46 601 OB
9/23/2008
10:45
DH
('opper.'I'olal
42.7
2.04
mg/kg
SW846601OB
9/23/2008
10:45
DH
I.cail. Total
2.04
2.04
mgikg
SW846 601OB
9/23/2008
10:45
DH
mt,d),hdcnum. Total
2.52
1.64
mg/kg
SW846 601013
9/29/2008
16:47
DH
N''icku•I.'I'n!al
25.7
2.04
mg/kg
SW846601OB
9/23/2008
10:45
DFI
zinc. Towl
128
.1.04
mg/kg
SWS46 601OB
9/23:'2008
10:45
DH
VIcrcurN. Total
�0.1 15
0.1 15
mg/kg
SW846 7470A
10/1/2008
14:23
DH
S, Irninm. I'ntal
�.04
�.04
mg/kg
SWS46 7741A
9'22/2008
16:44
DFI
1'('[1
C3DL
mg/kg
SW846 8080
S16 9/27/2008
5:12
AD1=
Page 2
ENVIRONMENTAL
SCIENCE CORP.
REPORT OF ANALYSIS
September 30,2008
ESC Sample 4 : L366100-01
September 19, 2008
Site ID
::a111J.A- JD
136704
Project
#
By
09/17/08 12:45
Dry
Result
Det. Limit
Units
Method
Date
Analyst
73.0
09/25/08
1141
TRR
BDL
2.3
mg/l:g
8082
09/27/08
0512
ADF
BDL
2.3
mg/kg
8082
09/27/08
0512
ADF
BDL
-
mg/kq
01082
09/27/08
0512
ADF
BDL
2.3
mg/kg
3002
09/27/08 0512
ADF
BDL
2.3
mg/kg
30`2
'09/27/05
0 1. 12
?LIF
BDL
2.31
rrig/l-.g
8082
09/27/08
05121
ADF
BDL
2
-.3
mg/hg
E082
0 9 /21 7 /;1 ""
0512
T. DF
i,;t-d are dry weight basis.
Limit
-,iwi.r. Preict)-,--al Quantitation Limit(PQL)
Laboratory Certification Numbers:
:%iH'-. - 1007bcJ, AL - 40660, CA - 1-2327, CT- PH-0197, FL E87487,_ GA - �42-i, 10 C-TN-01
FY115T - (1016, MC 7 ENV375,DW21704, ND R-140,SC- 84004, TN 2006, VA 00109, WV 233
AZ -0612, MN - 047.-999-395, HY 11742, NJ TN002-j WI 998093910
Thi-.; :;h,ill not be reproduced, except in full, without the written approval from ESC-.
analvtical results 'relate only to the sample submitted
ol,/21-1/08 -11:14 Revised: 09/30/08 12:00
1, t--10( -0i Dilution due to matri-..
Page 2 of 4
Attachment A
List of Anal7tes with QC Qualifiers
1 If Anal_ r.e
Qualifier
PCB 1016
PCB 1221
0
PCB 12-32
0
PCB 1242
a
PCB 12.38
C)
PCE, 1254
P�---B 1260
Pa (I F. 3 .) f 4
E!
E_-:planatic-n of Code_-,
tESC) Sample diluted due to matxix, interferences O-iat ijnl:;;iired thr. ability
t,., mal:e an- accurate analytical determination. The detection limit is
e1,:,7ated in,order to reflect the necessary dilution. _
Qualifier Report Information
:111d result qualifiers as set forth by the EPA Contract Laboratory Program and
h-v most i.:&rtifying' bodies including NELAC. In addition to the EPA qualifiers adopted
implemented ESC qualifiers to provide more information' pertaining to our analytical
E-:ich qualifier is designated in the qualifier e_xplanation as either. -EPA or ESC.
tiel.-S are intended to provide the ESC client with more detailed information concerning
bias of reported data. because of the wide range of constituents and variety of
by most -EPA methods, it is common for some compounds t---, fall out-ni-le of
1-111ries. These e%-ceptions are evaluated and all reported data it, valid and useable
I'ILI,;Iifilaa .,s IR' (Rejected)
Definitions
The, relationship of the observed Salue of a ):nown sample to, the
i:Lle value of a known sample. Repre.sented by .percent recovery and
-levant to samples such as: control .5antl5les, inatri-.: spike recoveries,
etc.
between ci set of samples or between duplicate sa.mplL-
-o how close together the results are and is represented by
Percent Differrence.
compounds that are similar in chemical
..!.,Ci .-:i:z-)wOtoCriphy to cine-Ilytes of int-rest. The surroaate.s al-e "Ised to
r - thfF p_,ob.=.b.Le responre of -Le group of analyre!, .,he�.t c*hem-
--ed to tsurrogatehe icomi:o.ind. S,irroc1
ates circ added co r:!-
arid al -cages o_prepira.-on and-
- identified Compound: detected in
:!.:r rompo"zr. cis, internal standard:.,, system moni-..orin.7
1 1: f C g;, t e -
4 of 4.
ENVIRONMENTAL
C-1
L)CIENCE CORP.
Report Summary
Tuesday September 30, 2008
Report Number: L366100
Samples Received: 09/19/08
Client Project:
Description:
T..:. 1, . D. - —, . il �,; 0,
in this report based upon ini,**.
rnAFlf - -1 01, pp1ied
i, Vhe -:J-Jent, and are for your exclusive use.
r-garding this data package, please do
Entire Report Reviewed By: T. Alan harviii, Eou Rep
CeftifiClqdO17 M1117bei-s
-ALJ(-,1-01, AIHA - 09227, AL -'40660, CA - 1-2327, CT - EIII-0197'FL - E87487
IN - C.-TN-01, KY - 90010, KYUST - 0016, NC - ENV375,DW-'?1704, ND R-140
THJf'0,', :-7',C' 84004, TN - 2006,.VA - 00109, WV - 233
12 [IN 047-999-39 5,'NY 11742, WI 998093910
I L I - u, Ei i .,j -i an E
1 . 1 f, V i
DAVIS & BROWN
Data Qualifiers
Within the attached report, some analytical data may be reported as "Qualified
Data" as indicated by a "Data Qualifier" or "flag" next to the result. The data
qualifier "S" indicates that the analysis was performed by another SC
certified Lab. This table summarizes the South Carolina Lab Certification
Numbers for those laboratories.
S
South Carolina Lab Certification Number:
23101
S 1
South Carolina Lab Certification Number:
93013
S2
South Carolina Lab Certification Number:
23 105-
S3
South Carolina Lab Certification Number:
10120
S4
South Carolina Lab Certification Number:
84002
S5
South Carolina Lab Certification Number:
32117
S6
Agricultural Service Laboratory Clemson University
S7
South Carolina Lab Certification Number:
36001
S8
****
S9
South Carolina Lab Certification Number:
94014001; 94014002
S10
South Carolina Lab Certification Number:
84009
S11
South Carolina Lab Certification Number: 96023; 96026; 96031; 98001; 73006
S 12
AASHTO R18 Certified
S 13
South Carolina Lab Certification Number:
96012
S 14
South Carolina Lab Certification Number:
89002
S 15*****
S 16
South Carolina Lab Certification Number:
84004
S17
South Carolina Lab Certification Number:
96037001
S 18
South Carolina Lab Certification Number:
95005
S 19
South Carolina Lab Certification Number:
23104
S20
South Carolina Lab Certification Number:
96027001
S21
South Carolina Lab Certification Number:
21005
S22
South Carolina Lab Certification Number:
24110
S23
South Carolina Lab Certification Number:
84001001
S24
South Carolina Lab Certification Number: 82014001
S25
Sam le was analyzed by Microsee s, Inc Laboratory
S26
North Carolina Lab Certification Number:
21 (Wilson Division NC00120)
S 2 7
South Carolina Lab Certification Number: 40569
Revision (X)-05 Da[ayual ISuKabsl .wpd
CHAIN OF CUSTODY RECORD
Page____ of
DAVIS & BROWN
Post Office Box 15038 124 West McIver Road
Quinby, South Carolina 29506 Florence, South Carolina 29501
Telephone (m3) 665.6746 f
""
Use Codes in the boxes to indicate
A ether sample was filtered or preserved.
o
„ter
In�
Him
F, ,
r
14,�
jjjjjjjj,
iNONNI!
n
eiiiiieii
loii�
o•-••• - - . .wng u - c,rounawater / 3 - Solid / W - Wade Water / N - NPDES / 0 - Other
A N I M A L W A S T E A N A L Y S I S R E P O R T
Agricultural Service Laboratory
LAB No. 91496 Clemson University
TOLSON, SHERRY ACCOUNT COCHSFL
PO BOX 219 DATE 09/26/2008
CHERAW SC 29520 CHERAWTOWNOF656@BELLSOUTH.NET
SAMPLE NO. VP170:&5;_O_-jMANURE : OTHER STORAGE: UNCOVERED
-----------------RESULTS REPORTED ON AN AS -SAMPLED BASIS----------------------
lbs/ton
Ammonium Nitrogen
0.15
%
3.00
Organic Nitrogen
0.66
%
13.27
Nitrate Nitrogen
---------------------------------------------------------------
0.73
ppm
0.00
INCORPORATED AVAILABLE NITROGEN ESTIMATE
10.36
SURFACE AVAILABLE NITROGEN ESTIMATE
---------------------------------------------------------------
9.46
Phosphorus as P205
0.62
%
12.35
Potassium as K20
0.11
%
2.11
Calcium
17.45
%
349.03
Magnesium
0.28
%
5.54
Sulfur
0.13
%
2.62
Zinc
159.64
ppm
0.32
Copper
42.28
ppm
0.08
Manganese
117.36
ppm
0.23
Sodium
885.70
ppm
1.77
Moisture
27.10
%
Calcium Carbonate Equivalency
44.35
%
887.01
------------------------------------------------------------------------------
INCORPORATED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
incorporated into the soil within hours of application. Assumes some loss of
ammonium-N during application and prior to incorporation.
SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50%of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
left on the surface of the soil with no incorporation by plowing or irrigation.
Available nitrogen calculations are estimates and if nitrate-N was not re-
quested the amount of available nitrogen may be slightly more than reported.
Also, the actual amount may be more or less than the estimate depending on the
composition of the manure, soil type, and environmental conditions.
All of the potash in the animal waste should be plant available in the first
year of application. Although not all of the phosphorous is available in the
first year, its availability should be comparable to that in commercial
fertilizers.
The rate of animal waste to apply for crop production is dependent on the
nutrient content of the waste, method of application and incorporation, soil
test, crop to be grown, and previous manure applications. In most cases, the
plant available nitrogen content of the waste is used to determine the rate of
application.
The Agricultural Service Laboratory is a public service of Clemson University,
an affirmative action and equal opportunity educational institution.
http://www.clemson.edu/aglabresults/COCHSFLTOLSON,%20SHERRY0810201153231.htm 2/9/09
% moisture
% solids
lbs. solidstton
lbs. solidsJ500 tons
27.1
72.9
1458
729000
%
ppm
Ibstton
%
ppm
Ibstton
as -sampled
as -sampled
as -sampled
dry ton
dry ton
d
Ammonium Nitrogen
0.15
1500
3
0.205761
2057.613
4.115226
Organic Nitrogen
0.6635
6636
13.27
0.910151
9101.509
18.20302
Nitrate Nitrogen
7.3E-05
0.73
0.00146
0.0001
1.001372
0.002003
Incorporated Available Nitrogen Estimate
0.518
5180
10.36
0.710562
7105.624
14.21125
Surface Available Nitrogen Estimate
0.473
4730
9.46
0.648834
6488.34
12.97668
Phosphorus as P205
0.6175
6175
12.35
0.847051
8470.508
16.94102
Potassium as K20
0.1055
1055
2.11
0.144719
1447.188
2.894376
Calcium
17.4515
174515
349.03
23.93896
239389.6
478.7791
Magnesium
0.277
2770
5.54
0.379973
3799.726
7.599451
Sulfur
0.131
1310
2.62
0.179698
1796.982
3.593964
Zinc
0.015964
159.64
0.31928
0.021898
218.9849
0.43797
Copper
0.004228
42.28
0.08456
0.0058
57.99726
0.115995
Manganese
0.011736
117.36
0.23472
0.016099
160.9877
0.321975
Sodium
0.08857
885.7
1.7714
0.121495
1214.952
2.429904
Calcium Carbonate Equivalency
44.3505
443505
887.01
60.83745
608374.5
1216.749
�"September>208
CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT
CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES_
BIOSOLIDS SAMPLE DATE:14q,v mi5er19 20Q8
Biosolids
Maximum
Maximum
Maximum
Maximum
Metal
Allowable
Allowable
Application
Application
Content,
Metal
App. Rate,
Rate,
Rate,
METALS
ppm
Content, ppm
#/Acre/Yr.
DT/Acre/Yr.
WT/Acre/Yr.
Arsenic, Total
0.92 '
41.00
1.80
488.01
976:02
Cadmium, Total
0.92 •
39.00
1.70
460.90
921.79
Chromium, Total
40.00
1200:00
134.00
837.50
1675.00
Copper, Total
22.31
1500.00
67.00
750.86
1501.72
Lead,'Total
0.92 `
300.00
13.00
3524.50
7049.01
Mercury, Total
0.18
17,00
0.76
1026.32
2052.63
Molybdenum, Total
3.69
18.00
' 0.80
54.17
108.33
Nickel, Total
17.50
420.00
18.70
267.14
534.29
Selenium, Total
0.92
36.00
4.50
1220.02
2440.04
Zinc, Total -
75.29
1525.00
125.00
415.07
830.14
PCB
BDL
1.60
Actual metal content less than amount indicated.
Biosolids
Biosolids
Maximum
Maximum
Nutrient
Nutrient
Crop/Soil
Application
Application
Content,
Content,
Requirement,
Rate,
Rate,
ppm
%
#/Acre"
DT/Acre/Yr.
WT/Acre/Yr.
Ammonium Nitrogen
283.13
0.03
Organic Nitrogen
5861.26
0.59
Incorporated Available Nitrogen
3817.48
- 0.38
120.00
7.86
15.72
Surface Available Nitrogen
3732.54
0.37
120.00
8.04
16.07
Phosphorus as P205
4695.17
0.47
80.00
4.26
8.52
Potassium as K20
721.97
0.07
50.00
17.31
34.63
Calcium, Total
154147.79-
15.41
Calcium as CaO
215806.91
21.58
Calcium as CaCO3 (CCE)
441586.45
44.16
2000.00
1.13
2.26
Magnesium, Total
2850.13
0.29
Manganese.
84.94
0.01
,Sulfur
948.47
' 0.09
Percent Moisture
50.00
" These are typical values and must be adjusted based upon specific site conditions
DT is Dry Tons of Biosolids. WT is Wet Tons of Biosolids.
CERTIFICATION: This biosolid product has been produced by the Town of Cheraw's Wastewater
Treatment Plant by a treatment process that pasteurized plant residual•solids using high temperature
and lime (calcium oxide). The Town of Cheraw certifies that this biosolid complies with the
Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has meta_ I
.and nutrient content as presented above.
DIRECTIONS FOR USE: This biosolid is intneded to be used as a soil amendment. The biosolid
land application rate shall not exceed the most restrictive Maximum Application Rate as indicated in
the table above. The application rate fix nitrogen, phosphorus, potassium, and calcium is dependent
upon the crop grown and site soil characteristics. The user should contact the Clemson Extension
Service (843-623-2134) and/or the Soil Conservation Service (843-6234187) for assistance in
determining the proper application rate for each crop and site. In no case shall the land application
rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension
Service Circular #476 titled "Lime and Fertilizer Recommendations."
THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY.
AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES.
THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS
BIOSOLID PRODUCT.
Mr. Ricky D. Ingram, Public Utility Director
P. 0. Box 219; Cheraw, SC 29520
Telephone: 843-537-Wo
FAX: 843-537-8442
PRODUCT USER NAME:
Davis & Brown
PO Box 15038
Quinby, SC 29506
(843) 665-6746 FAX: (843) 629-1444
Certificate of Analysis
Client: CHERAW, TOWN OF,
P.O.BOX 219
CHERAW, SC 29520
Client #: 168
Contact: SHERRY TOLSON -
Sample Date: 19-Nov-08
SDG #: SDG-063870
Lab Sample ID: LSID-141 193
Sample ID: B10` D9 1-1:-19-08-50
South Carolina Certification Number: 21117
Receipt Date: 21-Nov-08
Report Date: 05-Dec-08
Approved By: F •� _ a: !f
Van Ward
Lab Director
Reporting
Parameter
Result
Limit
Unit
Method
Flag Date
Time
Analyst
Acid Digestion (Solids)
YES
EPA 200.2
11/24/2008
8:00
DH
Percent Moisture
48.0
0.1
wt%
SW846 3540
11/20/2008
16:30
BW
Aluminum. Total
3640
38.4
mg/kg
SW846 6010B
12/l/2008
15:37
DH
Arsenic, Total
<0.959
0.959
mg/kg
SW846 601013
12/2/2008
10:51
DH
Cadmium, Total
<0.959
0.959
mg/kg
SW846 6010B
11/25/2008
10:00
DH
Chromium. Total
41.6
0.959
mg/kg
SW846 6010E
11/25/2008
10:00
DH
Copper, Total
23.2
0.959
mg/kg
SW846 6010E
11/25/2008
10:00
DH
Lead, Total
_<0.959
0.959
mg/kg
SW846 6010B
11/25/2008
10:00
DH
Molybdenum, Total
<3.84
3.84
mg/kg
SW846 6010B
11/25/2008
14:38
DH
Nickel, Total
18.2
0.959
mg/kg
SW846 6010B
11/25/2008
10:00
DH
Zinc, Total
78.3
0.959
mg/kg
SW846 601013
11/25/2008
10:00
DH
Mercury, Total
<0.190
0.19
mg/kg
SW846 7470A
. 11/25/2008
14:53
DH
Selenium, Total
<0.959
0.959
mg/kg
SW846 7741A
12/2/2008
10:51
DH
PCB
BDL
mg/kg
SW846 8080
S16 11/28/2008
13:52
ADF
Page 1
ENVIRONMENTAL
SCIENCE CORP.
Mr. Scott Fields
Davis & Brown
P.O. Box 15038
Quinby, SC 29506
REPORT OF ANALYSIS
IIt. .Tali=-, T14
I - , i GI 75t:-S','',ti
7-Y;nfi-7n.7-S
Ta': I.D. r._-iiIli 14_r',9
E::t . 197U
December,03,2008
ESC Sample #
L376626-01
Date Received
November
25, 2008
Description
Site ID
Sample ID
141193
Project
#
Collected By
,
Collection Date
11/19/08
13:00
Parameter
Dry Result
Det. Limit
Units
Method
Date
Analyst
Total Solids "•
51.3
2540G
12/03/08
1016
JDW
Polychlorinated
Biphenyls
PCB 1016
BDL
0.033
mg/kg
8082
11/28/08
1352
ADF
PCB 1221
BDL
0.033
mg./kg
8082
11/28/08
1352
ADF
PCB 1232
BDL
`0.033
mg/kg
8082
11/28/08
1352
ADF
PCB 1242
BDL
0.033
mg/kg
8082
11/28/08
1352
ADF
PCB 1248
BDL
0.033
mg/kg
8082-
11/28/08
1352
ADF
PCB 1254
BDL
0.033
mg/kg
8082
11/28/08
1352
ADF
PCB 1260
BDL
0.033
mg/kg
8082
11/28/08
1352
ADF
Results listed are dry weight basis.
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Laboratory Certification Numbers:
AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0'197, FL - E87487, GA - 923, IN - C-TN-01
F-Y - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
Note: AZ -0612, MN - 047-999-395, NY - 11742, NJ - TNO02, WI - 998093910
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 12/03/08 14:14 Printed: 12/03/08 14:14
Page 2 of 2
DAVIS & BROWN
Data ,Qualifiers
Within the attached report, some analytical data may be reported as "Qualified
Data" as indicated by a "Data Qualifier" or "flag" next to the result. The data
qualifier "S" indicates that the analysis was performed by another SC
certified Lab. This table summarizes the South Carolina Lab Certification
Numbers for those laboratories.
S
South Carolina Lab Certification Number:
23101
S 1
South Carolina Lab Certification Number:
93013
S2
South Carolina Lab Certification Number:
23105
S3
South Carolina Lab Certification Number:
10120
S4
South Carolina Lab Certification Number:
84002
S5
South Carolina Lab Certification Number:
32117
S6
Agricultural Service Laboratory Clemson University
S7
South Carolina Lab Certification Number:
36001
S8
**********
S9
South Carolina Lab Certification Number:
94014001; 94014002
S 10
South Carolina Lab Certification Number:
84009
S11
South Carolina Lab Certification Number: 96023; 96026; 96031; 98001; 73006
S12
AASHTO R1.8 Certified
S 13
South Carolina Lab Certification Number:
96012
S 14
South Carolina Lab Certification Number:
89002
S15
**********
S 16
South Carolina Lab Certification Number:
84004
S17
South Carolina Lab Certification Number:
96037001
S 18
South Carolina Lab Certification Number:
950.05
S 19
South Carolina Lab Certification Number:
23104
S20.
South Carolina Lab Certification Number:
96027001
S21
South Carolina Lab Certification Number:
21005
S22
South Carolina Lab Certification Number:
24110
S23
South Carolina Lab Certification Number:
84001001
S24
South Carolina Lab Certification Number: 82014001
S25
Sample was analyzed by Microsee s, Inc Laboratory
S26
North Carolina Lab Certification Number:
21 Wilson Division NC00120
S27
South Carolina Lab Certification Number: 40.569
Revision 06/05 Dataqual (SubLabs) .wpd
CHAIN OF CUSTODY RECORD #1
Page of
DAVIS & BROWN
PM OEM Box i s= 124 wea4 Mckw Reed
OWnW. South CMMa 2=6 %rem. South C Mm 2MI
TONAMe (M) 665$746
Bee���e�III�
Ba�B��ee
f�l�f��Yi
� fe37�i� i��lYi
- o i - aue aw / N - NPDESO-Odier
Salmm Bu�lnesa sDaIn Me=
form No. 811• 156 2104 1g1-W
A N I M A L W A S T E A N A L Y S I S R E P 0 R T
Agricultural Service Laboratory
LAB No. 121916 Clemson University
TOLSON, SHERRY ACCOUNT COCHSFL
PO BOX 219 DATE 12/09/2008
CHERAW SC 29520 CHERAWTOWNOF656@BELLSOUTH.NET
SAMPLE NO. 1`'1=1;9Q:85z0 MANURE: OTHER STORAGE: UNCOVERED
-----------------RESULTS REPORTED ON
AN AS -SAMPLED BASIS----------------------
lbs/ton
Ammonium Nitrogen
0.03
%
0.60
Organic Nitrogen
0.62
%
12.40
Nitrate Nitrogen
---------------------------------------------------------------
51.92
ppm
0.10
INCORPORATED AVAILABLE NITROGEN ESTIMATE
8.09
SURFACE AVAILABLE NITROGEN ESTIMATE
--------------------------------
7.91
Phosphorus as P205
-------------------------------
0.50
%
9.95
Potassium as K20
0.08
%
1.53
Calcium
16.33
%
326.67
Magnesium,
0.30
%
6.04
Sulfur
0.10
%
2.01
Zinc
81.59
ppm
0.16
Copper
31.26
ppm
0.06
Manganese
87.94
ppm
0.18
Sodium
113.90
ppm
0.23
Moisture
47.G2
%
Calcium Carbonate Equivalency
46.79
%
935.81
INCORPORATED PLANT,AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
incorporated into the soil within hours of application.' Assumes some loss of
ammonium-N during application and prior to incorporation.
SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
left on the surface of the soil with no incorporation by plowing or irrigation.
Available nitrogen calculations are estimates and if nitrate-N was not re-
quested the amount of available nitrogen may be slightly more than reported.
Also, the actual amount may -be more or less than the estimate depending on the
composition of the manure, soil type, '.and environmental conditions.
All of the potash in the animal waste should be plant available in the first
year of application. Although not all of.the phosphorous is available in the
first year, its availability should be comparable to that in commercial
fertilizers.
The rate of animal waste to apply for.crop production is dependent on the
nutrient content of the waste, method of application and, incorporation, soil
test, crop to be grown, and previous manure applications. In most cases, the
plant available nitrogen content of the waste is used to determine the rate of
application,
The Agricultural Service Laboratory is a public service of Clemson University,
an affirmative action and equal opportunity educational institution.
** http://www.clemson.edu/agsrvlb **
http://www.clemson.edu/aglabresults/COCHSFLTOLSON,%20SHERRY081209085435... 12/11 /2008
% moisture ----
% solids
lbs. solidsiton
lbs. solids/500 tons
- 47.02
52.98
1059.6
529800
%
ppm
lbs/ton
%
PI)m
Ibs/ton
as -sampled
as -sampled
as -sampled
dry ton
dry ton
d
Ammonium Nitrogen
0.03
300
0.6
0.056625
566.2514
1.132503
Organic Nitrogen
0.62
6200
12.4
1.170253
11702.53
23.40506
Nitrate Nitrogen
0.005192
51.92
0.10384
0.0098
97.99924
0.195998
Incorporated Available Nitrogen Estimate
0.4045
4045
8.09
0.763496
7634.957
15.26991
Surface Available Nitrogen Estimate .
0.3955
3955
7.91
0.746508
7465.081
14.93016
Phosphorus as P205
0.4975
4975
9.95
0.939034
9390336
18.78067
Potassium as K20
0.0765
765
1.53
0 .144394
1443.941
2:887882
Calcium
16.3335
.163335
326.67
30.82956
308295.6
616.5912
Magnesium
0.302
3020,
6.04
0.570026
5700.264
11.40053
Sulfur
0.1005
1005
2.01
0.189694
1896.942
3.799884
Zinc
0.008159
81.59
- 0.16318
0.0154
154.0015
0.308003
Copper
0.003126
31.26
0.06252
0.0059
59.0034
0.118007
Manganese
0.008794
87.94
0.17588
0.016599
165.9872
0.331974
Sodium
0.01139
113.9
0.2278
0.021499
214.9868
0.429974
Calcium Carbonate Equivalency
.46.7905
467905
935.81
88.31729
883172.9
1766.346
November,2008� '
Davis & Brown
PO Box 15638
Quinby, SC 29506
(843) 665-6746 FAX: (843) 429-1444
Certificate` of Analysis
Client: CHERAW, TOWN, OF South Carolina Certification Number: 21117
P.O. BOX 219
CHERAW, SC 29520
Client #:
168
Receipt Date:
17-Jan-08•
Contact:
SHERRY TOLSON
Report Date:
31-Jan-08
Sample Date:
16-Jan-08
By:
VIxI+_.�,•c.-:
SDG #:
SD6-058820
Approved
Van Ward
Lab Director
Reporting
Parameter
Result
'Limit
Unit
Method
Flag
Date
Time
Analyst
LSID-130336
"_--I6' 5080 01
Acid Digestion (Solids)
YES
EPA 200.2
1/18/2008
9:30
DH
pH (Waste)
12
S.U.
EPA 9045D
S16'
1/22/2008
9:45
RBS
11*9TINPPWA
iP sSA
'P/F`
SW-846
1/30/2008
WSF
Ignitability
. >170
Deg. F;
SW846 1010
S16
1/25/2008
10:30
KPB
Percent Moisture
53.0
0.1
Wt%
SW846 3540
l/15/2008
17:15
BW ,
Aluminum, Total
5060
0.425
mg/kg
SW846 6010A
1/23/2008
16:29
DH
Arsenic, Total
<1.30
1.3
mg/kg,
SW846.6010A
1/24/2008, '.
0:00
JR
Cadmium, Total
<0.212
0.212
mg/kg
SW846 60110A
1/22/2008
12:16
,, DH'
Chromium, Total
14.9
0.212
mg/kg
SW846 6010A
1/22/2008
•12:16
DH
Copper, Total
28.6
0.212
mg/kg.
SW846 6010A
1/22/2008
12:16
DH
Lead, Total-
1.80
• 1.1
mg/kg
SW846 6010A
1/21/2008
15:18
DH
Molybdenum, Total
1.40
0.85 _
mg/kg
SW846 6010A ,
1/23/2008
16:29
DH
Nickel, Total
11.7
0.212
mg/kg
SW846 6010A
1/22/2008
1.2:16
DH
Zinc, Total
817
0.212
mg/kg
SW846 6010A
1/22/2008
12:16
DH.
Mercury, Total
<0.649
0.049
mg/kg
SW846 7470A
1/18/2008
13:28.
DH
Selenium, Total'.
<1.30
1.3
mg/kg
SW846 7741A
1/29/2008
13:11
JR
PCB
0.66
mg/kg
9W846 8080
S16
1/20/2008
22:20
CSU
Reactivity, Cyanide
<0.125
0.125
mg/kg
SW846 9010
S16
1/24/2008
12:34
LEM
Reactivity, Sulfide
<25
25
mg/kg
SW846 9030
S16
1/24/2008
10:15
LJN
Paint Filter
PASS
P/F
SW846.9095
S16;'
1/24/2008 .
7:00
KPB
-Page 1
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name: Town of Cheraw Permit Number:
WWTP Name: Town of Cheraw WWI'P NPDES Number:
Monitoring Period: From 01 /01 /08 To 12/31 /08
WQ0014248
SCO020249
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
Alternative 40
T Alternative 5 El I
Alternative 6 ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization IM
Class B:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Level in
Pathogen Density
g y
Number o
Excee-
encts
Frequency
of Analysis
Sample
Type
Analytical
Tech-niqu
inimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 et6th
power MPN per
gram of total
solids or 2 x 10 to
the 6th power
CFU per gram of
1000 mpn per
gram of total solid
(dry weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4
grams total solid
(dry weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Option 1 ❑ Option 2 ❑ Option 3 ❑ Option 4 ❑ Option 5 ❑
Option 6 ® Option 7 ❑ Option 8 ❑ Option 9 ❑ Option 10 ❑
No vector attraction reduction options were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
® "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
.attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "1 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate the information
used to determine that the pathogen and vector attraction reduction requirements have been met. I
am aware that there are significant penalties for false certification including fine and imprisonment."
Ricky'Ingram/Public Utility Director
Preparer Name nd Title (type or print) Land Applier Name and Title (if applicable)(type or print)
2 a,7
Signade of PlWarer Date Signature of Land Applier (if applicable) Date
Author Daryl D. Merritt DENR FORM RF (7/2002)
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A-1 Medium
Double Strength Single Strength
10 ' dilution/ 10 ml sample l 0-' dilution i 1.0 ml sample
Single Strength
10-2 dilution ! 1.0 ml sample
Single Strength
10` dilution / 0.1 ml sample
Date.'T•ime Test Set -Up: - - Q8' ,?,'30 ,,r... Date! Time Test Read: -1708
Time Placed in Incubator: 3. AO,o,,r, , Incubator Te rnp: 3 �D
Time Transferred to Water Bath: A A'00, -2 Water Bath Temp: sG
Operator Media Lot # : Q
% Solids Sample # :I i
DQ
MPN Fecal Coliform = lox MPN Index i 100 atl
Per Gram Total Solids Largest Volume'x' % Dry Solids
NOTE + indicates positive results ; - indicates negative results
FORMULA:
Where:
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE
% Total Solids = (A - B) x 100
C-B
A = Weight of dried residue + dish (mg)
B = Weight of empty dish (mg)
C = Weight of wet sample + dish (mg)
Sample # : %—/e - 6 ff Saa
Weight of dried residue + dish: ,
Duplicate weight of dried residue .+ dish:
Weight of empty dish
Weight of wet sample + dish' ;
% Total Solids
a a. 39 9P2
a,a�io
.aGI f�X /DD
a6x14.06
$;. 67
0
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A-1 Medium
Double Strength Single Strength ,
l 0-' dilution i' 1,0 nil sample 10-' dilution i 1.0 ml sample
Single Strength "- Single Strength
10-2 dilution',, 1.0 ml sample, I V, dilution / 0.1 ml sample
Date:Time Test SetooT : oZ�.ZO /, • Date:' Time Test Read:
Time Placed in Incubator:
Incubator- Temp: . Jr. L C-
Time Transferred to Water Bath: /'-`/ °
Water Bath Temp: TT
Operator Media Lot #
% Solids —a. Sample #
-otD- 08- ,41616
MPN Fecal Coliforrn 10 x MEN Index i 160 ml
Per Gram Total Solids Largest Voltime `x % Dry Solids
NOTE: + indicates..positive results`; - indicates negative results
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE
FORMULA:
% Total Solids
_ (A-B)xI00
C-B
A = Weight of dried residue + dish (mg)
B = Weight of empty dish (mg)
C = Weight of wet sample + dish (mg)
Sample # : ? - 20 - a F- S,46
Weight of dried residue + dish:
Duplicate weight of dried residue + dish :
Weight of empty dish
Weight of wet sample + dish :
% Total Solids = �.
0? / 1 {/ 4-!
7,D
39.1513
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A- l Medium
Date "Time Test Set-LTp; - d $ : 3Q date.' Time Test Read:
Time Placed in Incubator: L.s o,,�
Incubator Temp:
Time Transferred to Water Bath: °
. i'►'►. Water Bath Temp:
Operator r�
JAI Media Lot # . •
% Solids. 7D Sample #
MPN Fecal Coliform = 10 x' MPN Index / 100 ml = Q
per Gram"Total Solids Largest Volume x % Dry Solids
NOTE: + indicates positive results ; - indicates negative results
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE
FORMULA:
% Total Solids . (A - B) x 100
C-B
Where:
A = Weight of dried residue + dish (mg)
B = Weight of empty dish (mg)
C = Weight of wet sample + dish -(mg)
Sample # : 3 ' % - Q $ Oro D
Weight of dried residue + dish: 016 • S 3 /Q
Duplicate weight of dried residue + dish: aZ U 0 3
Weight of empty dish *I . Q 3 / oZ
Weight of wet sample + dish
% Total Solids = 7 p, .7 =
D.g003-X-039'� XlOD
I qm,
44
FECAL COLIFORM FOR MUNICIPAL, BIOSOLIDS
A-1 Medium
Double Strength Single Strength
10-' dilution / 10 ml sample 10-' dilution / 1.0 ml sample
t—
Single Strength Single Strength
10'2 dilution ' 1.0 ml sample. 10-2 dilution 10A ml sample
Date.rI'ime Test Set-LTp:
d0 Date. Time Test Read — _ Q 8 •
Time Placed in Incubator:3��,� ,
Incubator Temp:
Time Transferred to Water Bath: : 30 Water Bath Te
nix
Operator f �[A i' Media Lot _ 3 3 ?
Solids 'S, Sample # 4 r AA
MPN Fecal Coliform = 10 x MPN In / l00 ml per Gram Total Solids.' Largest Volume x % D
r} Solids
NOTE: + indicates positive results ; - indicates negative results
FORMULA:
Where:
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE
% Total Solids = (A - B) x 100
C-B
A = Weight of dried residue + dish (mg)
B = Weight of empty dish (mg)
C = Weight of wet sample + dish (mg)
Sample #: 5�-Jl -h9-5100
Weigi. ,f dned residue + dish:
Duplicate weight of dried residue + dish
Weight ,ji empty dish
Weight of wet sample + dish
%-Total Solids
,23r 3 9 r S
a3.39.!W
a 3. 3q�o—a.oGo� 1C Sao
J
a133.�6
�F 9�9G 0
r
FECAL'COLIFORM FOR MUNICIPAL BIO SOLIDS
` A=1 Medium
. Double Strength
107' dilution i 10 ml sample
Single Strength
10-' dilution / 1.0 ml sample
Single Strength
l 0-' dilution / 1.0 ml sample
Single Strength
10` dilution / 0.1 ml sample
Date."Time Test Set -Up: a-Vate.' Time Test Read: - D8
Time Placed in Incubator: Incubator Temp: Sd G
Time Transferred to Water Bath: .3� .r• Water Bath Temp:
Operator Media Lot # 3
3 fir
% Solids . 3 D Sample. #
S
MPN Fecal Coliform = 10 x MPN Index / 100 ml =
Per Gram Total Solids Largest Volume x % Dry Solids
NOTE: + indicates positive results ; - indicates negative results
FORMULA:
Where:
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE
% Total Solids
(A-B)x 100
C-B
A = Weight of dried residue + dish (mg)
B = Weight of empty dish (mg)
C = Weight of wet sample + dish (mg)
Sample # : �— a f — Q ?- �o
Weight of dried residue + dish:
Duplicate weight of dried residue + dish:
Weight of empty dish
Weight of wet sample + dish :
% Total Solids = L 3. 3 A
a.DS. 4
5?, SS3D?
c2 3 0 - � 43. 3
5/. qq.ST
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A-1 Medium
Single Strength
10-2 dilution! 1.0 ml sample
Single Strength
10-: dilution / 0.1 ml sample
Date,!Time Test Set-LTp: A; Date.! Time Test Read: !p - —Q • •3,$ •
Time Placed in Incubator:
�3•S /►'` • Incubator Temp:
Time Transferred to Water Bath: ; .3 S� Water Bath Temp: C
Operator
Media Lot # 73 3 / p
b
% Solids T o Sample #
MPN Fecal Coliform = 10 x MPN Index / 100 ml = Q
per Gram Total Solids Largest Volume x % Dry Solids
NOTE: + indicates positive results; - indicates negative results
FORMULA:
Where:
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE
% Total. Solids = (A - B) x 100
C-B
A = Weight of dried residue + dish (mg)
B = Weight of empty dish (mg)
C = Weight of wet sample + dish (mg)
Sample # : �o - i ff— o S _ Soo
Weight of dried residue + dish:
Duplicate weight of dried residue + dish:
Weight of empty. dish
Weight of wet sample + dish :
% Total Solids
53.1/G�—a•aGGo
30
S/. osaa
FECAL COLIFORM FOR MUNICIPAL:BIOSOLIDS
A-1 Medium.'.
Single Strength
10-2 dilution 1.0 ml sample
Single Strength
10-: dilution ! 0.1 ml sample
Date,rrime Test Set -Up: - Q 8 %' 14okpate! Time Test Read: 10
Time Placed in Incubator: ; Q Incubator Temp: 3 ,5, Q
Time Transferred to Water Bath: Water Bath Temp:
Operator Media Lot #. % 1 3 R
% Solids ��s Sample # — Q
MPN Fecal .Coliform 10 x MPN Index/ 100 ml
Per Gram Total Solids Largest Volume x % Dry Solids -
NOTE: + indicates positive results ; - indicates negative results
FORMnA:
Where:
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE
% Total Solids = (A B) x 100
C-B
A = Weight of dried residue + dish (mg)
B = Weight of empty dish (mg)
C = Weight of wet sample + dish (mg)
Sample#:
Weight of dried residue + dish:
Duplicate weight of dried residue + dish:
Weight of empty dish
Weight of wet sample + dish
% Total Solids
70/0
/07C x MO
------------
w
N
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A-1 Medium
Double Strength
10'' dilution / 10 ml sample
Single Strength
10 2 dilution / 1.0 ml sample
Single Strength
10-' dilution / 1.0 ml sample
Single Strength
10-= dilution / 0.1 mi sample
r ,
Date. 'rime Test Set -Lip:
�[� C7 R' Date. Time Test Read:
Time Placed in Incubator:'; Incubator Temp: 0 a
' C
Time Transferred to Water Bath. o
Water Bath Temp:
Operator Media Lot
Solids : �'��j Sample #
MPN Fecal Coliform = 10 x MPN In i 100 ml = V
Per Gram Total Solids Largest Volume x- % Dry Solids
NOTE: + indicates positive results ; = indicates negative results
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE
FORMULA:
% Total Solids
(A-B)x100
C-B
A = Weight of dried residue + dish (mg)
B = Weight of empty dish (mg)
C = Weight of wet sample + dish (mg)
Sample # : g-- 01;6-0 2- C a 6
Weight of dried residue + dish:
Duplicate weight of dried residue + dish :
Weight of empty dish
Weight of wet sample + dish
% Total Solids =
0 09 O'C'
o
Sg�
�S��
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A-1 Medium
Double Strength Single Strength-
10-1 dilution /, 10 ml sample l 0` dilution / 1.0 ml sample
Single Strength Single Strength
10'' dilution / 1.0 ml sample 10-2 dilution / 0.1 ml sample
Date.rFime Test Set -Up: 7 - i / " Q
• 41- Date! Time Test Read: L9-d
•
Time Placed in Incubator: . 3Q Incubator. Te
Time Transferred to Water Bath:
PW Water Bath Temp:
Operator Media Lot
3, D
% Solids Sam le #
p
MFN Fecal Coliform ' 10 x MPN Index/* 100 ml =
Per Gram Total Solids Largest Volume x %DrySolids
NOTE: + indicates positive results ; - indicates negative results
FORMULA:
Where:
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE
% Total Solids = (A - B) x 100
C-B
A = Weight of dried residue + dish (mg)
B = Weight of empty dish (mg) ,
C = Weight of wet sample + dish (mg)
Sample #
Weight of dried residue + dish:
Duplicate weight of dried residue .+ dish:
Weight of empty dish
Weight of wet sample + dish :
% Total Solids = �' 3 • ��
a�a q I
a 91x �aa
3 q.584 9
�s
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A- I Medium
Double Strength
10` dilution / 10 ml sample
Single Strength
10`2 dilution / 1.0 ml sample
Single Strength
10-1 dilution / 1.0 nil sample
Single Strength
10-: dilution / 0.1 nil sample
Date:rTime Test Set -Up:
Time Test Read: —/ - wh�
��•+•�
Time Placed in Incubator: �: ,,� , C
Incubator. Temp: SQ
Time Transferred to Water at:
. BhQ �'"• Water Bath Temp:
Operator p
Media Lot # _7 3 3 9 �O
% Solids �, / /O Sample #
p _/D-/S•-D -SDD
MPN Fecal Coliforin = 10 x MPN Index / 100 m[ _
Per Gram Total Solids Largest 1Jolume x % Dry Solids
NOTE: + indicates positive results ; -indicates negative results
FORMULA:
Where:
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE
% Total Solids
(A-B)x100
C-B
A = Weight of dried residue + dish (mg)
B = Weight of empty dish (mg)
C =. Weight of wet sample + dish (mg)
Sample #
Weight of dried residue + dish:
Duplicate weight of dried residue + dish
Weight of empty dish
Weight of wet sample + dish
% Total Solids
oz Fl �CIDa
s3. �970
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS .
A-1 Medium
Double Strength Single Strength
_ 1,0'' dilution / 1 O.ml sample 10-' dilution / l .0 ml sample
Single Strength Single Strength
10'' dilution / 1.0 ml sample 10' dilution ! 0.1 ml sample
Date/Time Test Set -Up: �V ; QQ , Date! Time Test Read: -,26
— 4?
Time Placed in Incubator: %.'3D�0,� Incubator Temp:,
Time Transferred to Water Bath: .'30 Water Bath Temp: S O
Operator '
I Al
Media Lot #.3 q 8
Solids 49 4—.
Sample #
MPN Fecal Coliform. = 10 x MPN Index / 100 nil = Q
Per Gram Total Solids Largest Volume x % Dry Solids '
NOTE: + indicates positive results ; - indicates negative results
FORMULA:
Where:
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE
% Total Solids = (A - B) x 100
C-B
A = Weight of dried residue + dish (mg)
B = Weight of empty dish (mg)
C = Weight of wet sample + dish (mg)
Sample # :
Weight of dried residue + dish:
Duplicate weight of dried residue + dish:
Weight of empty dish .
Weight of wet sample + dish
33.19 S.�
33,67 9f
% Total Solids = .
33.-07
3r00.so_iq.5°fo
4a.s76 /
FECAL COLIFORM FOR MUNICIPAL BIOSOLDS
A-1 Medium
Date/Time Test Set -Up: — Q ; A Date! Time Test Read:
M
Time Placed in Incubator:
• • � Incubator Temp:
Time Transferred to Water Bath: 0 Water Bath Temp: S
I.
Operator
Media Lot ## Q S
% Solids r%. �p Sample # IJ — — A0
MPN Fecal Coliform — 10 x MPN Index 1100 ml. _ Q
per Gram Total Solids Largest Volume x % Dry Solids
NOTE: + indicates positive results ; - indicates negative results
FORMULA:
Where:
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS-SAMPLE
% Total Solids
_ (A-B)x100
C -B
A = Weight of dried residue + dish (mg)
-B = Weight of empty dish (mg)
C = Weight of wet sample + dish (mg)
Sample # : 162-1 % - b V — soo
Weight of dried residue + dish:
Duplicate weight of dried residue + dish:
Weight of empty dish
Weight of wet sample + .dish
% Total Solids
�.0L
Sl, 8 80
H4. 93.3 1
Pasteurization vessel operates on a constant speed with an in/out
time duration of 30 minutes.
-
MINIMUM
MINIMUM
DATE
2 HOUR pH
24 HOUR pH
TEMP IN
TEMP OUT
01 /02/08
12.34
12.24
159
164
01/03/08
12.57'
12.31
157
178
01 /07/08
12.38'
12.19
160
163
01 /08/08
12.27
12.11
163
168
01 /09/08
12.21
12.08
159
164
01/10/08
12.35
12.15
166
160
01/11/08
12.22 ,
12.09
166
163
01 / 14/08
12: 39
12.20
161
164
01/15/08
12.46
12.22
- 160
161
01 /16/08
12.28
12.12
160
158
01 / 17/08
12.39
12.22
159
171
01 /18/08
12.39
12.19
158
158
01 /22/08
12.41
12.22
159
160
01 /23/08
12.34
12.13
159
166
01 /24/08
12.17
12.03
161
166
01 /28/08
12.23
12.09
159 ,"
176
01 /29/08
12.37
12.18
158
168
. 01 /30/08
12.22
12.08
159
161
01 /31 /08
12.29
12.13
159
169
02/01 /08
12.26
12.09
161
172
02/04/08
12.21
12.13
164
156
02/06/08
12.28
12,12
159
164
02/06/08
12.34 .
12.18
160
170
02/07/08
12.22
12.12
159
164
02/08/08 ,
12.28
12.14
163
174
02/11 /08
12.23
12.09
164
171
02/ 12/08
12.24
12.18
163
178
02/ 13/08
12.26
12.14
161
172
02/20/08
.12.29
12.04
159
172
02/21 /08
12.15
12.05
159
158
02/25/08
12.25
12.14
163
167
02/26/08
12.27
12.16.
164
169
02/28/08
12.25
12.16
159
160
02/29/08 -
12.24 "
12.07
160
166
03/03/08
12.18
12.11
161
157
03/04/08
12.32
12.18
164
170
03/05/08
12.20
12.13
160
168
03/06/08
12.33
12.17
159
157
03/07/08
12.31
12.13
160
168 '
03/ 10/08
12.24
12.12
159
164
03/11 /08
12.06 .
11.87
159
. 161
03/ 12/08
12.08
12.01
160
158
03/13/08
1-2.31
12.18
160
158
03/14/08
12.05
11.96
'158
167
03/ 17/08.
12.17
12.06
161.
164
03/ 18/08
12.31
12.16
165
'168
03/ 19/08
12.24
12.01
161
169
03/20/08
12.22
12.13
165
159
03/21 /08
12.26
12.17
159
162
03/25/08
12.21
12.04
160
169
03/26/08
12.23
12.11
159,
161
03/27/08
12.24
12.07
160
167
03/28/08
12.08,
12.01
160
169
Pasteurization vessel operates on a constant speed with an, in/out
time duration of 30. minutes.
MINIMUM MINIMUM
DATE
2 HOUR pH
24 HOUR pH
TEMP IN
TEMP OUT
04/01 M
12.21
12.06
155
162
04/02/08
12.21
12.07
159
160
04/03/08
12.19
12.04
159
158
04/04/08
12.20
12.06
159
162
04/07/08
12.22.
12.09
159
158
04/08/08
12.27
12.12
159
162
04/09/08
12.23
12.09
162
168
04/10/08
12.16
12.08
161
160
04/11 /08
12.24
12.13
158
164
04/14/08
12.18
12.01
158
163
04/15/08
12.21
12.03
157
160
04/16/08
.12.08
12.04
157
162
04/25/08
12.23
12.17
161
167
04/28/08
12.17
12.04-
161
-160
04/29/08
12.22
12.04
159
158
04/30/08
12.23
12.08
159
163
05/01 /08
12.24
12.09
161
.166
05/02/08
12.31
12.17
161
158
' 05/05/08
. 12.28
12.09
162
160
05/06/08
12.24
12.09
159
167,
05/07/08
12.15
12.08
159
165
05/08/08
12.16
12.09
159
162
05/09/08
12.11
12.01
164
162
05/12/08
12.20
12.08
159
167
05/13/08
12.18
12.04
159
164
05/14/08
12.30
12.20
'159
166
05/15/08
12.22
12.14
160,
169
05/16/08 '
12.27
12.13
160
158
05/19/08'
12.20
12.06
160
160
05/20/08
12.23
12.09
159
162
05/21/08
12.37
1.2.19
-159
162
05/22/08
12.30
12.23
160
170
05/23/08
12.31
12.09
159
'1'60
05/27/08
12.29
12.07
159
168
05/28/08
12.09
12.04
161
159
05/29/08
12.19
12.10
159
167 -
05/30/08
12.26
12.13
163
171
06/02/08
12.08
11.92
159
167
06/03/08
12.14
12.06
160
166
06/04/08
12.13
12.00
159
164
06/05/08
12.10 ,
11.96
165
160
06/06/08
12.17
12.03
159
1.59
06/09/08
12.09
11.94
161
164
06/10/08
12.21
12.07
159
159
06/11 /08
12.25
12.08
159
162
06/12/08
12.20
12.03
159
160
06/13/08
12.18
12.00
160
160
06/16/08
12.20
12.05
162
170
06/17/08
12.31
12.25
157
158
06/18/08
12.27
12.12
167
169
06/ 19/08
12.07..
11.96
159
156
06/20/08
12.11
12.01
159
155
06/23/08
12:27
12.06
166
167
06/24/08
12.25
12.18.
159
161
06/25/08
12.23
12.13
163
160
06/26/08
12.21
12.03
159
161
06/27/08
12.26
12.06
159
159
06/30/08
12.27
12.08
162
159
Pasteurization vessel operates on a constant speed with an in/out
time duration of 30 minutes.
DATE
2 HOUR pH
24 HOUR pH
MINIMUM
TEMP IN
MINIMUM
TEMP OUT
07/01 /08
12.27
12.08
160
162
07/02/08
12.18
12.11
159
164
07/03/08
12.21
12.13
159
169
07/07/08
12.23
12.09
161
167
07/08/08
12.26
12.11
162
158
07/09/08
12.17
12.05
161
161
07/10/08
12.19
12.08
161
161
07/11 /08
12.28
12.17
159
159
07/14/08
12.24
12.12
159
1.60
07/15/08
12.19
12.06
164
167
07/16/08
12.18
12.10
160
173
07/17/08
12.25
12.13
159
162
07/18/08
12.21
12.11
1.60
164
07/21 /08
12.11
12.02
163
168
07/22/08
12.30
12.04
159
162
07/24/08
12.27
12.06
167
161
07/25/08
12.23
12.09
159
160
07/28/08
12.09
12.04
163
165
07/29/08
12.25
12.12
160
163
07/30/08
12.27
12.14
160
168
07/31 /08
12.24
12.08
160
163
08/01/08
12.12
12.01
159
161
08/04/08
12.28
12.09
159
164
08/05/08
12.17
12.09
164
165
O8/06/08
12.24
12.06
164
161
08/07/08
12.08
12.04
160
172
08/08/08
12.26
12.13
161
168
08111 /08
12.19
12.09
164
172
08/12/08
12.25
12.10
160
170
08/ 13/08
12.20
12.03
159
159
08/ 14/08
12.21
12.08
162
159
08/ 15/08
12.26
12.11
161
159
08/ 19/08
12.18
12.09
159
180
08/20/08
12.28
12.03
166
162
08/21 /08
12.29
12.12
160
170
08/22/08
12.23
12.14
170
181
08/25/08
12.20
12.12
165
168
08/26/08
12.23
12.03
171
181
08/28/08
12.27
12.16
161
160
08/29/08
12.06
12.01
160
170
09/02/08
12.20
12.09
162
170
09/03/08
12.24
12.21
161
174
09/05/08
12.30
12.19
159
160
09/08/08
12.18
12.07
165
168
09/09/08
12.23
12.03
160
181
09/ 10/08
12.27
12.13
161
186
09/ 12/08
12.23
12.09
161
186
09/ 15/08
12.21
12.11
.16 5
174
09/16/08
12.19
12.07
162
175
09/ 17/08
12.31
12.12
160
172
09/18/08
12.25
12.12
160
170
09/19/08
12.28
12.09
170
182
09/22/08
12.33
12.18
160
160
09/24/08
12.30
12.16
161
155
09/26/08
12.28
12.06
169
159
Pasteurization vessel operates on a constant.speed with an in/out
time duration of 30 minutes.
DATE
2 HOUR pH
24 HOUR pH
MINIMUM
TEMP IN
MINIMUM
TEMP OUT
10/02/08
12.19
12.05
158
160
10/07/08
12.17
12.07
160
168
10/08/08
12.27
12.08
159'
172
10/09/08
12.21
12.18
157
174
10/ 10/08
12.34
12.23
161
163
10/ 13/08
12.21
12.09
159
177
10/ 14/08
12.31
12.16
150
172
10/ 15/08
12.29
12.20
159
162
10/16/08
12.33
' 12.14
168
176
10/17/08
12.18
12.07
161
163
10/20/08
12.22
12.11
161
174
10/21 /08
12.29
.12.13
164
162
10/22/08
12.21
12.15
172
172
10/23/08
12.19
12.08
159
162
11 / 17/08
12.18.
12.08
169
179
12/ 18/08
12.08
12.01
181
183
12/19/08
12.09
12.03
160
159
12/30/08
12.22
12.07
160
160
12/31 /08
12.13
12.03
160
159
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Cheraw
Total Dry Tons Applied (Annual): 92
WQ0014248 Cation Exchange Capacity (non 503 only):
Allan Baucom Owner: Allan Baucom
100 'Acres Permitted: Site #: 106 Field #:
Residual, Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Total
Phos-
_phorusEMENEEMENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
'
t
Me
Phos-
phorusTotal
"I certify, under penalty of law, that this -document was prepared under my- direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware'that there are significant penalties for submitting false information,
including the possibility of fines and imprison or knowing violations".
Z o 0
Signature o Lan Applier Date "
Author Daryl D. Merritt DENR FORM"MFLSF (7/2002)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. 1
'PLACE A- "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
.Facility Name: Town of Cheraw Permit #: WQ0014248 Annual Dry Tons Applied:
Owner: Allan Baucan Operator: Allan Baucom ' Cation Exchange Capacity (non 503):
Site #: 106 Field #: Acres Utilized:, 100 Acres Permitted:
�
Q
SGalf
Totals
Per
Acre
Solids
As
Deci-
Dry
Tons
Per
Acre
Residual
Sou �rces
(Summarize)
site
Cond.
Dry,
Wet,
Inches
Preci
Past 24
Hrs.
Appli-
cation
Meth-
od**
Voli-
tila-
zation
Rate*
Miner-
ala-
zatiop' n.
Rate
TKN
Ammo
nia-
Ni-
trogen
Ni-
trate-
Ni-
trogen
PAN 1
PAN 2
Must Select
Cro 1 or Cro
p P
2
Cu.Yd.
Report
Totals
in Gal.Moist
Crop 1
Crop 2
April-
N/A - '
N A
0.509
0.92
S
0.5
17973
648
381
10776
X
TOTALSt
'
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Ap
lied
Annuallbs/acre
.0047
.0008
.0539
.1034
.0065
.0002
.0051
.0423
.0047
.2953
43.86
38.95.1
Date
.lbs/ac
Current Cumulative lbs/acre
.0111, .0042 .2002 .3428- .0270 .001.2 1.0216 .1793' .0095 .8156
- 0064 .0034 1.1463 1.2394 1.0205 .0010 .0165 .1370 .0048 1.5203
Prior Years Cumulative lbs/acre
Permitted C., P. L. R. *-*
Permit PAN Limit 1 st/2nd Crop
..1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that -there are, -
significant penalties fo r.sabmitting false information, including the possibility of fines and imprisonment for knowing violations."
too *Application Method: S - Surface, IN - Injection, INC - Incorporation,
Signature of Land Applier Date **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
***C.P.L.R.:.Cumulative Pollutant Loading.Rate
Author Daryl D. Merritt DENR FORM FSF (7/2002)
74
_
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Ah-
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raw
Allan Baucom site
„ 106
N34043.110 ' - 100 acres
..., :`: _'�%
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N3442-
3-D lapoquub Copprigh! 0 1999 DeLom,e Tareoath, 1R 0096 Sonya Data: USGS 900 ft Scale: 1 : 22,100 Detail: 13-2 Daum: MSSI
ANNUAL LAND APPLICATION CERTIFICATION FORM
Permit#: WQ0014248 Couvty:
Facility Name (as shown on permit):
Land Application Operator:
Chesterfield Year: 2006
Town of Cheraw
Land application of residual solids afi allowed by the permit occurred during the past calender year? �
® Yes ❑ No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A:
Total number of application fields in permit:
Total number of fields land application occurred during the year:
4
Total amount of dry tons applied during the year for all application sites:
1510
Total number of acres land application occurred during the year:
1265
Part B:
Facility was compliant during calendar year 2006 with all conditions of the land application permit
(including but not limited to items 1-12 below) issued by the Division of Water Quality. M Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain
corrective action taken.
1. Only residuals approved for this permit were applied to the permi
2. Soil pH was adjusted as specified in the permit and lime was app i
least 6.0 or the limit specified in the permit.
3. Annual soils analysis were performed on each site receiving residl `
(3) copies of laboratory results are attached.
4. Annual TCLP analysis was performed and three (3) copies of certi
5. All other monitoring was performed in accordance with the permit)
and three (3) copies of certified laboratory results are attached. , V
6. The facility did not exceed any of the Pollutant Concentration Lim
Pollutant Loading Rates- in Table 2 of 40 CFR part 503.13 (applica
7.- All general requirements in 40 CFR Part 503.12 and management I -
complied with (applicable to 40 CFR Part 503 regulated facilities). / �rr✓1 ��� P..
8. All operations and maintenance requirements in the permit were c
prior authorization was received from the Division of Water Qualit� - J
9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of
violations are attached to include appropriate actions and remediations.
10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed
in accordance with the crop management plan.
11. No runoff of residuals from the application sites .onto adjacent property or nearby surface waters has occurred.
12. All buffer requirements as specified on the permit were maintained during each application of residuals.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there -are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
-----, �
Ricky Ingram/Public Utility Director fr W"4- o
Permittee Name. and Title (type or print) FEB Z 3 2007 Signature of l4rrnittee Date
I
[DEhIn-FAMTE,4) I P RCPrno.fAI
Signature of Preparer* Date _-Signiture of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r)
Author Daryl D. Merritt DENR FORM ACF (7/2002)
ANNUAL DISTRIBUTION AND MARKETING/ SURFACE. DISPOSAL CERTIFICATION AND SUMMARY FORM.
PERMIT #: WQ0014248 FACILITY NAME.: Town of Cheraw
PHONE: (843) 537-8440 COUNTY: Chesterfield OPERATOR•
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
® Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar _year? ® Yes ❑No No If No ckin nnrtc -A R V and t,nrtwv, f.., _ hpi_'
Part A*: _
t B*: Par -.
Month
Sources s
O (include<NPDES-# if
applicable)
Volume (dry tons)
Recipient Information
Admendment/
Bulking Agent
Residual In
Product Out
Names)
Volume (dry tons)
Intended use s
O ,
January
February.
March
SCO020249
SC0020249
SCO020249
27.54
88.76
113.31
38.43
68.47
101.31
65.97
157.23
214.62
Allan'Bauccm
Allan Baucom
71717
948
crop fert.
crop fert.
April.
SCO020249
89.62
97:98.
187..60
May
SCO020249
64:00
68.1-5
131.90_
June
SCO020249
6 00
6.82
12'.82
July
SCO020249
54 55
45.60
100.15
August
SC0020249 _ .
- . 110.77
.81.. 43
192..20
September
SC0020249
28.18.,
24.32
52.50
r
October
SCO020249' —
101.46
' 61.11 --
162. 57 -
November
Sd0020249.74,09.74.
09
148.18 `
December
SC0020249
75 64
86.07,
161.71
Totals:,
Annual (dry: tons):
753 78
.1587 45'
Admendment(s) used:
Lime
Bulking Agents) used: 1 none
* If more space than given is required, please attach additional information sheet(s). [3 Check box if additional sheets) are attached .-
Part C:
Facility, was compliant during -,calendar year . 2006 .:with all conditions of the permit (including but -not limited to items 1-3 below), issued. by the
Division of Water Quality. ® Yes ❑ No If No, please provide a written description' why the facility was not compliant,
1. All monitoring was done, in' accordance with the permit and.reported for the year as'required and three (3) copies of certified laboratory results are attached
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the -Division of Water
Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law; that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware
that here are significant penalties for submitting false informaiton,,including the possibility.of fines and imprisonment for knowing violations."
Signatur of P ttee' Date Signature of Preparer** Date
(if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r)
Author Darvl D. Merritt DFNR FnRm nm.gnF (7/9nroi
TOWN OF CHERAW WASTEWATER TREATMENT FACILITY
BIOSIOLIDS REPORT'
MONTH
PRESS
HOURS
DRY CAKE
SOLIDS T.
TONS LIME
USED
%
LIME
TOTAL
DRY PROD.
LIME $/
TON PROD.
POLY $/
TON CAKE
LBS. POLY/
TON CAKE
LBS. POLY
USED
JAN 06
85.80
38.43
27.54
41.75
65.97
50.37"
28.11
13.99
537.50
FEB
152.50
68.47
88.76
56.45
157.23
68.21
16.15
8.15
550.00
MAR
192.50
101.31
113.31
52.80
214.62
63.82
15.38
7.65
775.00
APR
181.50
97.98
89.62
47.77
187.60
57.80
13.33
6.63
650.00,
MAY
_ 143.50
, .68.15
64
.48.33
_ 131.90
58.64
15.48
7.70
525.00
JUN
15.50
6.82
6.00
46.80
12.82
56.78
14.74
7.33
50.00
JUL
97.50
45.60
54.65
54.47
100.15
66.53
15.43
7.68
350.00
AUG
212.00
81.43
110.77
57.63
192.20
70.40
20.36
10.13
825.00
SEP-
73.50
24.32
28.18
53.68
--52.50
65.74
'20.66
10.28
250.00
OCT
171.50
61.11
101.46
62.41 '
'162.57
76.44
16.45
8.18 '
500.00
NOV.
159.00
74.09
74.09 '
50.00
148.18
60.52 ,
5:43
2.70
200.00
DEC
173.50
86.07
75.64
' 46.78
161.71
56.59
8.17
4.07
350.00
TOT
1,658.30
753.78
833.67
1,587.45
751.84
189.69
94.49
5,562.50
AVG
138.19
62.82
3.00
51.57
132.29
62.65
15.81
7.87
463.54
MIN
15.50
6.82
.6.00
41.75,
12.82
50.37
5.43.
2.70
50.00
MAX
212.00
101.31
113.31
62.41
214.62
76.44
28.11
13.99
825.00
ANNUAL,.RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report'
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ001'4248 Laboratory: 1) Davis &Brown ,
Facility Name: Town of Cheraw 2) Clemson University - .
NPDES # or 3)
WQ#: SCO020249
4)
.WWTP Name: Town of Cheraw WWTP, 5)
Residual Analvciic Data
Sample or
Composite Date .
1 /05/06
1 /05/06
3/09/06
3/09/06
5/04/06
5/01/06
7/13/06
7/13/06
9/07/06
9/67/06
11 /6/06
11 /6/06
Percent Solids
42.80
-44.98
44..30
47.04
53.40
.45.30
.40.50
- 51 .84
34.00
- 29.51
54.00
47.18
Arsenic
.230, _
.446
.1 .48
:230 '
1-.05
1 .35
Cadmium
. 292
: 307
4.295 _
: 410, :
. 210
4.269 .
Chromium
13.2. ,
13.7
20. 9 '
24:7
15.8`
22.4
Copper
21.. 8
22.9
25. 2 -
36. 2 �
40.0
48.6
Lead
1'.92
2.34
1:84
2.20
2.22.
3.43
A
Mercury
.156
.021
.150
.084
.044
.182
`1Vlolybdenum
1:62
1.35
, 1..40 .
2.54
_
1 77
<.885
Nickel.,
9.45
6.5E
9.07
10.E
18.E
20.0
77. Selenium
.131
:125
<1.48
.205
1.05
1.35
Zinc
40.2
44:7
64-
:.3
67.1
64.4
91.1
._....
TKN
14550'.9
22193.9
21578.4
16425.5
-
34378.2
16553.6
Ammonia-Nitroge
1333. 9;
1062..9
441.5
771.E
3727.5
847.8
_Nitrate and Nitrite
187.0
363.0j
459:0
845._0
958.1
1200.1
FTotal Phosphorus
6869..7
10533.E
11445.9`
11217.2
19241.1
12823.2
"I certify', under penalty of law; that ;this document was prepared under my direction or supervision in accordance With a system
designed .to assure that qualified personnel,properly gathered and evaluated the in submitted: I, am aware that there are
significant. penalties for submitting false information, including the_possibility of fines and imprisonment for knowing violations."
Signatu of P eparer Date
Author Darvl D. Merritt. nFniR FnPKA Rcc;: MOWWN
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name: Town of Cheraw, Permit Number: - WQ0014248
WWTP Name: Town "of Cheraw WWTP, NPDES Number: SCO020249
Monitoring Period: _ From 01 /01 /06 To ' 12/31 /06 _
Pathogen .Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: '
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
Alternative 4❑ ,
. ,Altemadve 5 ®F
-(� Alternative 6 _ ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑ 71
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
'Pasteurization
Class B:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
If applicable .to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization -; ❑
Air Drying ❑ '
Coinposting
erobic Digestion ❑
Anaerobic Digestion❑
If applicable to alternative performed (Class A or Class -B) complete the'following monitoring data:
Parameter '
-
Level in
Pathogen Density
- g Y
um er o
-Excee- _
deuces
Frequency
of Analysis
.Sarriple
'Type "
Analytical
Tech-nique'
MinimumGeo.
Mean
aximu
Units
Fecal Coliform
2 x 10 to the 6th
power MPN per
gratn.of total
solids or 2 x 1'0 to
the 6th power
CFU per grain, of
1000 mpn per
gram of total solid
(dry, weight)
0
0
!,
0
MPN
0
Monthly
Grab
multi -
tube
Salmonella bacteria
(in lieu of fecal
coliform)
' 3 MPN per 4
grams total solid
(dryweight)
Vector Attraction Reduction (40- CFR 50333) - Please indicate option performed:
Option 1- 1.0ption 2 [11 Option 3, 10ption 4 ❑ Option 5 ❑
Option 6 El Option T ElOption 8 ❑. Option 9 ❑ Option 10 ❑
,PNo vector attraction reduction options were performed - E3.
ERTIFICATION STATEMENT (please check the appropriate statement) ;
® "I certify, under penalty of law; that the pathogen requirements. in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have. been met."
❑ `;, "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector,
attraction reduction requirement in 40 CFR. 503.33 have not been met." (Please note if you check
this statement attach an explanation why, you have not met one or •both of the requirements.)
"This. determination has been made under my direction and supervision in accordance with the •
'-system designed to ensure "that qualified personnel properly gather and evaluate the information
used to determine that the pathogen and vector attraction reduction requirements have been met: I
am aware that there are significant penalties for -false -certification including fine. and imprisonment."
Ricky Ingram/Public Utility Director
Preparer Name and Title (type or print) Land. Applier Naive and Title (if applicable)(type or print)
Signs a of P parer Date* .'Signature of Land Applier (if applicable) Date
Author Daryl D. Merritt DENR FORM. RF (7/2002)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Cheraw
Owner: Allan . Baucom
Site #: 104 Field #:
Permit #: WQ0014248 Annual Dry Tons Applied: * 400
Operator: Allan Baucom Cation Exchange Capacity (non 503):
Acres Utilized: 330 Acres Permitted:
A
S'Galf
Totals
Per
Acre
Solids
As
Deci-
1
Dry
Tons
' Per
Acre
Residual
Sources
(Summarize)
Site
Cond.
C
Dry,
Wet,
ois
Inches
Preci
Past 24
Hrs.
Appli-
cation
Meth-
od**
Voli-
tila-
zation
Rate*
Miner-
ala-
zation
Rate
TKN
Ammp'
nia-
Ni-
trogen
Ni-
trate-
Ni-
trogen
PAN 1
PAN 2
Must Select
Crop
P 1 or Crop
2
Cu.Yd.
Report
Totals .
in Gal.
Crop 1
Crop 2
Jan.
N/A
N/A
.4389
13.21
S
0.5
114551
1334
187
8117
g
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Ap lied
Annual lbs/acre
0.0013
0.0016
0.0728
0.1202
0.0106
0.0009
0.0089
0.0521
0 0007
0,2217
37,8781
44 755
Date
lbs/ac
Current Cumulative lbs/acre
0.0096 0.0033 0.1467 0.3160 0.0223 0.0012 0.0138 0.1116 0.0073 0.4323
0.0083 0.0017 0. 0739 0.1958 0. 0117 0:1.0003 0,0049 0.0595 0.0066 0.2106
Prior Years Cumulative lbs/acre
Permitted C. P. L. R.***
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and, evaluated the information submitted. I am aware that there are
significa gnial 'es bmitting false information, including the possibility of fines and imprisonment for knowing violations."
2 Q *Application Method: S - Surface, IN - Injection, INC - Incorporation
ignature of Land Applier Date **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
Author Daryl D. Merritt DENR FORM FSF (7/2002)
------- ----- 1'Vl\L1•
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Cheraw
Total Dry Tons Applied (Annual):
W00014248 Cation Exchange Capacity (non 503 only):
Allan Baucom Owner: Allan Baucom
330 Acres Permitted:
Site #: 104 Field #:
400
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg. % Solids use Raiv PPrrant ttl.
..
•
.:. •
..
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
•
e e .
__�_®____®_
Elms
were e •
eee •
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
includin he possibilit fines and imprisonment for knowing violations"
2 lZ o 7
Signature of Land Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)
.s✓
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120
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3-D RopoNads Copyright 0 1999 DeUrme Yarmouth, W 04096 Source Data: DSCS i --I900 ft Scale: 1 : 22,400 Detail: 13-2 Datum: UGS94
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM .TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Cheraw
Owner: Allan Baucom
Site #: 105 Field #:
Operator:
Permit #: WQ0014248
Allan Baucom
Acres Utilized:- 210
Annual Dry Tons Applied: 250
Cation Exchange Capacity (non 503):
Acres Permitted:
"
A
Specify
Totals
Per
Acre
Solids
As
Deci-
D
Dry
Tons
Per
Acre
Residual
Sources
(Summarize)
Site
Cond.
Dry,
Wet,
Moist
Inches
Preci p'
Past 24
Hrs.
pp .-
A li
cation -
Meth-
od**
Voli-
tila-
zation
Rate*
Miner-
ala-
zation
Rate
TK1V
Ammo
nia-
Ni-
trogen
Ni-
trate-
Ni-
trogen
PAN 1
PAN 2
Must Select
Crop 1 or Cro
P F
2
f
Cu.Yd.
Report
Totals
in Gal.mal
Crop 1
Crop 2
Jan.
N/A
N/A .
.4389
1.19
S
0.5
14551
1334
187
8117
X
TOTALS:
As
Cd
Cr
Cu
Pb
HR
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
.0012
.0016
.07116
J182
.01-04
.0008
.0088
.0512
.0007
.2180
37..252
44.02
Date
lbs/ac
Current Cumulative lbs/acre
.0092 .0034 .1525 .3326 .0231 .0011 .0140 .1157 .0070 .4452
.0080 .0018 .0809 .2144 .0127 :0003 .0052 .0645 .0063 :2272
Prior Years Cumulative lbs/acre
Permitted C. P. L. R. * * *
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated,the information submitted. I am aware that there are
signrtt enalties for submitting false information, including the possibility of fines and' imprisonment for knowing violations."
2 l?r o 7 *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of Land Applier bate **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.6
***C.P.L.R.: Cumulative Pollutant Loading Rate
Author Daryl D. Merritt . DENR FORM FSF (7/2002)
l al • 1 . V AL 1.11� 1 ALV 1' a1:/LJl L V ALll \ l7 U lJ lTlITJLt&1\ 1 l %-J JLNl\'1
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Cheraw Total Dry Tons Applied (Annual): 250
Permit #: WQ0014248 Cation Exchange Capacity {non 503 only):
Operator: Allan Baucom Owner: Allan Baucom
Acres Used: 210
Acres Permitted: Site #: 105 - Field #:
Residual Analysis Data (Heavy Metals and Total Phosphorus use m % Solids use Raw
Total
Phos-
..
.:. •
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
tal
Phos-
phorusIMENEEMENEEMEN
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
includi the possibility of fines and imprisonment for knowing violations"
ztzo�
Signs re of and Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)
f {+v .� _ .. --�'
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3-D Topoquads Copyright ® 1999 DeLorme Yarmouth, HE 04096 Source Data: DSGS i 900 ft Scale: I : 22,400 Detail: 13-2 Datum: WGS84
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Cheraw
Owner: Allan Baucom
Site #: 106 Field #:
Permit #: WQ0014248
Operator: Allan Baucom
Acres Utilized: 306
Annual Dry Tons Applied: • 360
Cation Exchange Capacity (non 503):
Acres Permitted:
A
S'Galf
Totals
Per
Acre
Solids
As
Deci-
mal
Dry
Tons
Per
Acre
Residual
Sources
(Summarize)
Site
Cond.
Dry,
Wet,
Moist
Inches
Preci p'
Past 24
Hrs.
Appli-
cation
Meth-
od**
Voli-
tila-
zation
Rate*
Miner-
ala-
zation
Rate
TKN
Ammo
nia-
Ni-
trogen
Ni-
trate-
Ni-
trogen
PAN 1
PAN 2
Must Select
Crop 1
p or Cro 1
2
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop
Feb.
N/A
N/A
.41-89
1.18
S
0.5
14551
11334
187
8117
g
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Ap lied
Annuallbs/acre
.0012
.0016
.0710
.1172
.0,1103
.0008
.0087
.0508
.0007
.2162
36.939
43.646
Date
lbs/ac
Current Cumulative Ibs/acre
.0041 .0029 .1226 .2136 .0171 .0009 .0152 .1140 .0025 .4464
.0029 .0013 .0516 1.0964 .0068 1 .0001 .0065 .0632 .0018 .2302
Prior Years Cumulative lbs/acre
Permitted C. P. L. R. * * *
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
signi cant penalties forsubmitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of Land Applier Date **Volitilization Rate: Surface - 0.5, Injection/Incorporation 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
Author Daryl D. Merritt DENR FORM FSF (7/2002)
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Cheraw Total Dry Tons Applied (Annual): 360
Permit #: WQ0014248 Cation Exchange Capacity (non 503 only):
Operator: Allan Baucom Owner: Allan Baucom
Acres Used: 305 Acres Permitted: Site #: .
Residual Analvsis Data (Heavv Metals and Total Phncnhnrnc i,qP mo/ko
106
Field #:
% gr%HrIL nen 1Do—r D^ ...4 al\_
Total
Phos-
phorusEWEEMENEEMEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Mr. M.
NMI
Total
. os-
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fine and imprisonment for knowing violations"
vrzo7
f6atuof Lan Applier Date
Author Daryl D. Merritt DENR FORM, MFLSF (7/2002)
W;ta
1?1�
I'l-,
i. At
I ; .
t
41.
1
It
4"
NTIA
At.,
u
NA
C•
it-
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24
n
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Cheraw
Owner: Allan Baucom Operator: Allan
Site #: 113 Field #:
Permit #: W00014248 Annual Dry Tons Applied: * 500
Baucom Cation Exchange Capacity (non 503):
Acres Utilized: 420
Acres Permitted:
Q
S�Galf
Totals
Per
Acre
Solids
As
Deci-
mal
Dry
Tons
Per
Acre
Residual
Sources
(Summarize)
Site
Cond.
Dry,
Wet,
Moist
Inches
Preci p'
Past 24
Hrs.
Appli-
cation
Meth-
od**
Voli-
tila-
zation
Rate*
Miner-
ala-
zation
Rate
TKN
Ammo
nia-
Ni-
trogen
Ni-
trate-
Ni-
trogen
�
PAN 1
PAN 2
Must Select
Crop 1 or Cro
P F
2
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
Feb.
N/A
N/A
.43891
500
S
1 0.5
14551
1334
187
81177
X
L
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Ap lied
Annuallbs/acre
.0012
.0016
.0716
.1182
.0104
.0008
.0088
.0512
.0007 1.2180
37.25
44.02
Date
lbs/ac
Current Cumulative lbs/acre
.0051 .0034 .2152 .3237 .0222 .0011 .0221 .1657 .0016 .6504
.0039 .0018 .1436 1.2055 .0118 .0003 .0133 .1145 .0009 .4324
Prior Years Cumulative lbs/acre
Permitted C. P. L. R. * *
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant enalties fors mitting false information, including the possibility of fines and imprisonment for knowing violations."
4e4d►z(b7 *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of Land Applier Date **Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
Author Daryl D. Merritt
DENR FORM FSF (7/2002)
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Owner: Allan Baucom
Acres Used: 420 Acres Permitted: Site #: 113 Field #:
Residual Analysis Data (Heavy Metals and Total Phosnhnrnc nce mofk4_ a/,� Cnlirlc ncn RQ.0 po,., _+ 4N.
Town of Cheraw
WQ0014248
Allan Baucom
500
Sample
-
---- - --
----- ••.
or Com-
1 /5/
1 /5/
06
06
posite
Date
% Solids
42.80
44.98
Arsenic
0.23
Cadmium
0.292
Chromium
13.2
Copper
21.8
Lead
1.92
Mercury
0.156
Molyb-
1.62
denum
Nickel
9.45
Selenium
0.131
Zinc
40.2
Total
Phos-
6869.7
horus
Annual Heavy Metal Field Loadings (Calculated in lhs/acre):
y�
y
3
a
y
s�
Arsenic
.0012
.0012
Cadmium
.0016
.0016
hromiu
.0716
.0716
Copper
.1182
.1182
Lead
.0104 ,
.010404
Mercury
.0008
.0008
Molyb-
, 0088
denum
.0088
Nickel
.0512
.0512
Selenium
.0007
.0007
Zinc
.2180
.2180
Total
37.25
Phos-
37.252
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
includine,the possibility of fines and imprisonment for knowing violations"
f2 ni
ignature o La Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)
3-D TopoQoads Copyright ® 1999 DeLome Yarmouth, NE 04096 Source Data: DSGS f-- �900 ft Scale: 1 : 22,400 Detail: 13-2 Datum: AGS84
CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT
CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES
BIOSOLIDS SAMPLE DATEJ'Jaituary 542006
Biosolids
Maximum
Maximum
Maximum
Maximum
Metal
Allowable
Allowable
Application
Application
Content,
Metal
App. Rate,
Rate,
Rate,
METALS
ppm
Content, ppm
#/Acre/Yr.
DT/Acre/Yr.
WT/AcrelYr,
Arsenic, Total
0.27
41.00
1.80
1674.78
3349.57
Cadmium, Total
0.34 '
39.00
1.70
1245.89
2491.78
Chromium, Total
15.42
1200.00
134.00
2172.42
4344.85
Copper, Total
25.47
1500.00
67.00
657.71
1315.41
Lead, Total
2.24
300.00
13.00
1448.96
2897.92
Mercury, Total.
0.18
17.00
0.75
1028.85
2057.69
Molybdenum, Total
1.89
18.00
0.80
105.68
211.36
Nickel, Total
11.04
420.00
18.70
423.47
846.94
Selenium, Total
0.15
36.00
4.50
7351.15
14702.29
Zinc, Total
46.96
1625.00
125.00
665.42
1330.85
PCB
BDL
1.60
' Actual metal content less than amount indicated.
Blosolids
Biosolids
Maximum
Maximum
Nutrient
Nutrient
Crop/Soil
Application
Application
Content,
Content,
Requirement,
Rate,
Rate,
ppm
%
#/Acre"
DT/Acre/Yr.
WT/Acre/Yr.
Ammonium Nitrogen
666.96
0.07
Organic Nitrogen
6608.49
0.66
Incorporated Available Nitrogen
4646.51
0.46
120.00
6.46
12.91
Surface Available Nitrogen
4446.42
0.44
120.00
6.75
13.49
Phosphorus as P205
3434.86
0.34
80.00
5.82
11.65
Potassium as K20
844.82
0.08
50.00
14.80
29.59
Calcium, Total
152767.90
15.28
Calcium as CaO
213875.06
21.39
Calcium as CaCO3 (CCE)
219972.77
22.00
2000.00
2.27
4.55
Magnesium, Total
2751.22
0.28
Manganese
77.81
0.01
Sulfur
1000.44
0.10
Percent Moisture
50.00
'* These are typical values and must be adjusted based upon spec site conditions
DT is Dry Tons of Biosolids. WT is Wet Tons of Biosolids.
CERTIFICATION: This biosolid product has been produced by the Town of Cheraw's Wastewater
Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature
and lime (calcium oxide). The Town of Cheraw certifies that this biosolid complies with the
Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has a metal
and nutrient content as presented above.
DIRECTIONS FOR USE: This biosolid is intneded to be used as a soil amendment. The biosolid
land application rate shall not exceed the most restrictive Maximum Application Rate as indicated in
the table above. The application rate for nitrogen, phosphorus, potassium, and calcium is dependent.
upon the crop grown and site soil characteristics. The user should contact the Clemson Extension
Service (843-623-2134) and/or the Soil Conservation Service (843-623-2187) for assistance in
determining the proper application rate for each crop and site. In no case shall the land application
rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension
Service Circular #476 titled "Lime and Fertilizer Recommendations."
THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY.
AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES.
THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS
BIOSOLID PRODUCT.
Mr. Ricky D. Ingram, Public Utility Director
P.O. Box 219; Cheraw, SC 29520
Telephone: 843-537-8440
FAX: 843-537-8442
QUANTITY RECEIVED:
RECEIVED BY:
Davis & Brown
PO Box 15038
Quinby, SC 29506
(843) 665-6746 .FAX: (843) 629-1444
Certificate of Analysis
Client: CHERAW, TOWN OF South Carolina Certification Number: 21117
P.O.BOX 219 North Carolina Certification Number: 612
CHERAW, SC 29520
Client #: 168 Receipt Date: 06-Jan-.06
Contact: SHERRY TOLSON Report Date: 27-Jan-06'
Sample Date: 05-Jan-06
SDG #: - SDG-046340
Parameter
Lead, Total
Nickel, Total
Zinc, Total
Reporting
Result
Limit
Unit
<0.656
0.05
mg/L
0.037
0.01
mg/L
0.468
0..01
mg/L,
Approved By:
Van Ward
Lab Director
Method
Flag Date
Time
Analyst
EPA 200.7
1/11/2006
10:45
DH
EPA 200.7
1/9/2006
17:38
DH
EPA 200.7
1/9/2006
17:38
DH
LSID-104212 1001-X
Cyanide <0.005 0.005 mg/L EPA 335.2 1/10/2006 8:00 MLL
LSID-104213
1002-X
Cyanide
<0.005
0.005
mg/L.
EPA 335.2
1/10/2006
8:00
MLL
LSID-104214
Be IO:&O.LIDS is0&201
Acid Digestion (Solids)
YES
EPA 200.2
1/9/2006
10:00
DH
TCLP
PASS
P/F
SW-846
S16 1/13/2006
WSF
Ignitability
>170
Deg. F.
SW846 1010
'S16 1/9/2006
10:00
_ CWP
Percent Moisture
57.2
0.1
Wt%
SW846 3540
1/10/2006
12:30
JR
Aluminum, Total
3840
0.584
mg/kg
SW846 6010A
1/12/2006
14:46
DH
Arsenic; Total
0.230
0.131
mg/kg
SW846-6010A
1/25/2006
16:40
JR
Cadmium, Total .
<0.292
0.292
mg/kg
SW846 6010A
1/9/2006
17:38
DH
Chromium, Total
13.2
0.292
rng/kg
SW846 6010A
1/9/2006
17:38
DH
Copper, Total
2.1.8
0.292
mg/kg
SW846 6010A
1/9/2006
17:38
DH
Lead, Total
1.92
1.46
mg/kg
SW846 6010A
1/11/2006
10:45
DH-
Page 2
Davis & Brown
PO Box 15038
Quinby, SC 29506
(843) 665-6746 FAX: (843) 629-1444
Certificate of Analysis
Client:. CHERAW, TOWN. OF 'South Carolina Certification Number: 21117
P.O.BOX 219 _ North Carolina Certification Number: 612
CHERAW, SC 29520
Client #: 168 Receipt Date: . 06-Jan-06
Contact: SHERRY. TOLSON Report Date: 27-Jan-06
Sample Date: 05-Jan-06
SDG #: SDG-046340
Approved By:
VanVard
Lab Director
Reporting
Parameter
Result
Limit
Unit
Method
Flag Date
Time .
Analyst'
Molybdenum, Total
1.62
1.2
mg/kg
SW846 6010A
1/12/2006
' 14:51
DH
Nickel,- Total
9.45
0.292
mg/kg
SW846 6010A
1/9/2006
17:38
DH
Zinc, Total
40.2
0.292-
mg/kg
SW846 6010A:.
1./9/2006
.17:38.
DH
Mercury, Total
0.156,
0.053'
mg/kg.
SW846 7470A
1%12%2006
15:26
DH
Selenium, Total
<0.131
0.131
mg/kg
SW846 7741A
1/17/2006
12:04 .
JR
PCB
BDL
1.4
mg/kg
SW846 8080.
S16 1/10/2006
S:23
JSW
Reactivity, Cyanide
<0.12
0.12
mg/kg
SW846 9610
S16 1/11/2006
11:45
DJS
Reactivity, Sulfide
29
25
mg/kg
SW846 9030
1/9/2006
15:00
CWP
pH (Solids)
10.6'
S.U.
SW846 9045 :
1/16/2006
14:40
LM
Paint Filter
PASS
P/F
SW8469095
S16 1/9/2006
11:30
CWP
LSID-104215 1-5-06-102
Acid Digestion (Liquids)
Aluminum, Total
YES
0.040
0.02 mg/L
EPA 200.2
'EPA-200.7
1/9/2006
1/12/2006
1:00
14:46
DH
DH
LSID-104216 1001-0
Total Toxic Organics
0.154
0.01 mg/L
8260/8270.
S11 1/10/2006
15:11
VMW
LSID-104217 1002-0
Total Toxic Organics
0.209
0.01 mg/L
8260/8270
Sl l 1/11/2006
17:08
JCK
0
Page 3
ANIMALWAS TEANALYSISREPO RT Page l of
A N I M A L W A S T E A N A L Y S I S R E P O R T
Agricultural -Service Laboratory
LAB No. 10092 'Clemson.University-
TOLSON, SHERRY ACCOUNT COCHSFL
PO BOX 219 DATE 01-30-2006
CHERAW SC 29520 CHERAWTOWNOF656@BELLSOUTH..NET
SAMPLE NO. 012,5952:0_ MANURE : OTHER STORAGE: UNCOVERED
-----------------RESULTS
REPORTED ON AN AS-SAMPLED-BASIS----------------------
lbs/ton
Ammonium Nitrogen
0.06
%
1.20
Organic Nitrogen
0.59
%
11.89
Nitrate Nitrogen
---------------------------------------------------------------
84.12
ppm
0.17•
INCORPORATED AVAILABLENITROGEN ESTIMATE
8.36
SURFACE AVAILABLE
NITROGEN ESTIMATE
8.00
---------------------------------------------------------------
Phosphorus as P205
0.31
%
6.18
Potassium as K20•
0.08
%
1.52
Calcium
13.74
%
274.86
Magnesium
0.25
%
4.95
Sulfur
0.09
%
1.80
Zinc
43.64
ppm
0.09
Copper
21.59
ppm
0.04
Manganese
68.83
ppm
0.14
Sodium
161.95
ppm
0.32
Moisture
55.02
Calcium Carbonate
Equivalency 39.58
%
791.55
-------------------------------------- 7---------------------------------------
INCORPORATED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure, will be
incorporated into the soil within'hours of application. Assumes some loss of
ammonium-N during application and prior to incorporation.,
SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of
organic-N, and 100% of•nitrate-N (if determined). Assumes the manure will be
left on the surface•of the soil with no incorporation by plowing or irrigation.
Available nitrogen calculations are estimates and if nitrate-N was not re-
quested the amount of .available nitrogen may be slightly more than reported.
Also, the actual amount may be more or less than the estimate depending on the
composition of the manure, soil type, and environmental conditions.
All of the potash in the animal waste should be plant available in the first
year of application. Although not all of.the phosphorous is available in the
first year, its availability should -be comparable to that in commercial
fertilizers.
The rate of animal.waste to apply for crop production is dependent on the
nutrient content of the waste, method of application and incorporation,•soil,
test, crop to be grown, and previous manure applications. In most cases, the
plant available nitrogen content of the waste is used to determine the rate of
application.
The Agricultural Service Laboratory is a public service of Clemson University,
an affirmative action and equal opportunity educational institution.
** http://www.clemson.edu/agsrvlb **
http://www.Clemson.edu/aglabresults/COCHSFLTOLSON,%20SHERRY0601300000001.... , 1/31/2006
%moisture
% solids
lbs. solids/ton
lbs. solids/500 tons
44.98
899.E
449800
%
ppm lbs/ton
%
ppm
lbs/ton
as -sampled
as-sam led as -sampled-
dry,ton
dry ton
d
Ammonium Nitrogen
0.06
" 600 1, 2
0.133393
1333.926
2.667852
Organic Nitrogen
0.5945
" 5945 �u 11 $9
1.321699
13216.99,
26.43397
Nitrate Nitrogen
0.008412
84`1:2 0 16824.
0.018702
'.187.0165
0.374033
Incorporated.Available Nitrogen Estimate
0.418
4180 8 36:
0.929302
9293,01.9
18.58604
Surface Available Nitrogen Estimate
0.4
4000 '8;
0.889284
8892.841
17.78568
Phosphorus as P205
0.309
3090 6 18
0.686972
6869.72
13.73944
Potassium as K20
0.076
760 ^ 1 52
0.168964
1689.64
3.37928
Calcium
. .13.743
,
137430 : ' x ` 274 86
30.55358
305535.8
611.0716
Magnesium
0.2475
2475 4:95
0.550245
5502.446
11.00489
Sulfur
0.09
900
0.200089
2000.889
4.001779.
Zinc .
0.004364
43 64 0.08728
0.009702
97.0209
0.194042
Copper
0.002159
r ` , 21 59 0.04318
- 0.0048
47.99911
0.095998
Manganese
0.006883
ti
6&83 i 0.13766
0.015302
153.0236
0.306047
Sodium
0.016195
a 161 95, 0.3239
0:036005
360.0489,
0.720098.
Calcium Carbonate Equivalency
39.5775
395776 k 1 791 55
87.98911
879891 A
1759.782�
CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT
CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES
BIOSOLIDS SAMPLE DATE:VOC- 2006P
METALS
Biosolids
Metal
Content,
ppm
Maximum
Allowable
Metal
Content, ppm
Maximum
Allowable
App. Rate,
#/Acre/Yr.
Maximum
Application
Rate,
DT/Acre/Yr.
Maximum
Application
Rate,
WT/AcrelYr.
1
Arsenic, Total
0.50
41.00
1.80
893.95
17a7.89
Cadmium, Total
0.35
39.00
1.70
1226.55
2453.09
Chromium,.Total
15.46
1200.00
134.00
2166.50
4332.99
Copper, Total
25.85
1500.00
67.00
648.06
1296.11
Lead, Total
2.64
300.00
13.00
1230.56
2461.11
Mercury, Total
0.02
17.00
0.75
7910.71
15621.43
Molybdenum, Total
1.52
18.00
0.80
131.26
262.52
Nickel, Total
7.40
420.00
18.70
631.41
1262.82
Selenium, Total
0.14
. 36.00
4.50
7974.00
15948.00
Zinc, Total
50.45
1525.00
125.00
619.41
1238.81
PCB .
BDL
1.60
' Actual metal content less than amount indicated.
Biosolids
Nutrient
Content,
ppm
Biosolids
Nutrient
Content,
%
Crop/Soil
Requirement,
#/Acre "
Maximum
Application
Rate,
DT/Acre/Yr.
Maximum
Application
Rate,
W'f/AcrelYr.
Ammonium Nitrogen
531.46
0.05
Organic Nitrogen
10565,48
1.06
-
Incorporated Available Nitrogen
7057.82
0.71
120.'00
4.25
8.50
Surface Available Nitrogen
6898.38
0.69
120.00
4.35
8.70
Phosphorus as P205
6266.79
0.63
80.00
3.80
7.59
Potassium as K20
1626.28
0.16
50.00
7.69
15.37
Calcium, Total
140896.05
14.09
,
Calcium as CaO
197254.46
19.73
Calcium as CaCO3 (CCE)
176392.43
17.64
2000.00
2.83
5.67
Magnesium, Total
2800.81
0.28
Manganese
47.83
0.00,
Sulfur
1349.91
0.13
Percent, Moisture
60.00
- `rhese are typical values and must be adjusted based upon specific site conditions
DT is. Dry Tons of Biosolids. WT is Wet Tons of Biosolids..
CERTIFICATION: This biosolid product has been produced by the Town of Cheraw s Wastewater
Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature
and lime (calcium, oxide). The Town of Cheraw certifies that this biosolid complies with the
Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has a metal
and nutrient content as presented above.
DIRECTIONS FOR USE: This biosolid is intneded to be used as a soil amendment. The biosolid
land application rate shall not exceed the most restrictive Maximum Application Rate as indicated In
the table above. The application rate for nitrogen, phosphorus, potassium, and calcium Is dependent
upon the crop grown and site soil characteristics. The user should contact the Clemson Extension
Service (843-623-2134) and/or the Soil Conservation Service (843-623-2187) for assistance in
determining the proper application rate for each crop and site. In no case shall the land application
rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension
Service Circular #476 titled "Lime and Fertilizer Recommendations."
THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY.
AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES.
THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS
BIOSOLID. PRODUCT.
Mr. Ricky D. Ingram, Public Utility Director
P.O. Box 219; Cheraw, SC 29520
Telephone: 843-537-8440
FAX: 843-537-8442
PRODUCT USER 14AME:
ADDRESS:
UUhltl 11I I nr_l,M VCU:
RECEIVED BY:
Davis & . Brown
PO Box 15038
Quinby, SC 29506
(843) 665-6746 FAX: (843) 629-1444
Certificate of Analysis
Client: CHERAW, TOWN OF
P.O.BOX 219
CHERAW., SC 29520
Client #: 168
Contact: SHERRY TOLSON
Sample Date: 09-Mar-06
SDG #: SDG-047386
Reporting
Parameter Result Limit Unit
South Carolina Certification Number: 21117
North Carolina Certification Number: 612
Receipt Date: 10-Mar-06
Report Date: 30-Mar-06
Approved By:
Van Ward
Lab Director
Method Flag Date Time Analyst
LSID-106258
SLI SO IL DS 3 9 06=500 V
Acid Digestion (Solids)
YES
EPA 200.2
3/14/2006
13:00
DH
Percent Moisture
55.7
0.1
wt%
SW846 3540
3/14/2006
16:30
JR
Aluminum, Total
3800
0.5
mg/kg
SW846 6010A_
3/24/2006
11:37
`DH
Arsenic, Total
0.446
0.125
mg/kg
SW846 6010A
3/13/2006
18:14
JR
Cadmium, Total
<0.307
0.307
mg/kg
SW846 6010A
3/13/2006
16:08
DH
Chromium, Total
13.7
0.307
mg/kg
SW846 6010A
3/1372006
16:08
DH
Copper, Total
22.9
0.307
mg/kg
SW846 6010A
3/13/2006
16:08
DH
Lead, Total
2.34
1.5
r-ig/kg
SW846 6010A
3/14/2006
16:10
DH
Molybdenum, Total
1.35
1.2
mg/kg
SW846 6010A
3/15/2006
17:21
DH
Nickel, Total
6.56 '
0.307
mg/kg
SW846 6010A
3/13/2006
16:08
DH
Zinc, Total
44.7
0.307
mg/kg
SW846 6010A
3/13/2606
16:08
DH
Mercury, Total
<0.021
0.021
mg/kg
SW846 7470A
3/21/2006
9:35
DH
Selenium, Total
<0.125
0.125
mg/kg
SW846-7741A
3/14/2006
14:14
JR
PCB
BDL
6.273
mg/kg
SW846 8080
S16 3/16/2006
11:47
TLW
i
Page 2
ANIMAL WAS TEANALYSISREPORT
Page 1 of 2
A N:.I M A L W A S
T E A N A L Y S I
S R E P O R T
Agricultural
Service Laboratory
LAB No. 30500 Clemson University
TOLSON,, SHERRY
ACCOUNT
COCHSFL
PO BOX 219
DATE
03-29=2006
CHERAW SC 29520
CHERAWTOWNOF@BELLSOUTH.NET
SAMPLE NO.R0�3000-Q5. NURE: OTHER STORAGE: UNCOVERED
-----------------RESULTS REPORTED ON
AN AS -SAMPLED BASIS------------------=---
lbs/ton
Ammonium Nitrogen
0.05 %
1.00
Organic Nitrogen
0.99 %
19.88
Nitrate Nitrogen
-------------------------------------------------------------
170.75 ppm
0.34
INCORPORATED AVAILABLE NITROGEN ESTIMATE
13.28
SURFACE AVAILABLE NITROGEN ESTIMATE
-----------------------------------------------------
12,98
Phosphorus as 'P205
0.50 %
7---------
9.91
Potassium as K20
0.15 %
3.06
Calcium
13.26 %
265.11
Magnesium
0.26 %
5.27
Sulfur
0.13 %
2.54
Zinc
67.74 ppm
0.14
Copper
35.75 ppm
0.07
Manganese
45..16 ppm
0.09
Sodium
166.99 ppm
0.33
Moisture 52.96 %
Calcium Carbonate Equivalency 33.19 %
663.80
------------------------------ 7-----------------------------------------------
INCORPORATED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
incorporated into the soil within hours of application. Assumes some loss of
ammonium-N during application .and prior to incorporation.
SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of
organic-N, and 100%.of nitrate-N (if determined). Assumes the manure will be
left on the surface of the soil with no incorporation by plowing or irrigation.
Available nitrogen calculations are estimates and if nitrate-N was not re-
quested the amount of available -nitrogen may be slightly more than reported.
Also, the actual amount may be more or less than the estimate depending on the
composition of the,manure, soil type, and environmental conditions.
All of the potash in the animal waste should be plant available in the. first
year of application. Although not all of the phosphorous is available in the
first year, its availability should be comparable to that in commercial
fertilizers.
The rate of animal waste to apply for crop production is dependent on the
nutrient content of the waste, method of application and incorporation, soil
test, crop to be grown, and previous manure applications. In most cases, the
plant available nitrogen content of the waste is used to determine the rate of
application.
The Agricultural Service Laboratory is a public service of Clemson University,
an affirmative action and equal opportunity educational institution.
** http://www.clemson.edu/agsrvlb **
http://www.clemson.edu/aglabresults/COCHSFLTOLSON,%20SHERRY0603290000005.... 3/30/2006
% moisture
% solids
lbs. solids/ton
lbs. solidst500 tons
.-47.04
940.8
470400
%
PPm lbs/ton
%g
ppm
lbstton
as-sam led
as -sampled as -sampled
dry, ton
dry ton
d -
Ammonium Nitrogen
0.05
500 , 1:.0.106293
1062.925
2.12585
Organic Nitrogen
0.994
9940 19:88
2.113095
21.130.95
. 42.261,9
Nitrate. Nitrogen
0.017675
r 170 75,, 0.3415
0.036299.
362.9889
0.725978
Incorporated Available Nitrogen Estimate
0.664
6640 13 28
1.411565
141,15.65
28.23129
Surface Available Nitrogen Estimate
: 0.649.
6490 1298
1.379677
13796.77
27.59354
Phosphorus as P205
0.4955
4%5 9 91''
1.053359
10533.59
21.06718
Potassium as It20
0.1.53
1530 3:06.
0.325255
3252.551
6.505102
Calcium
13.2555
132555 265;1=1'
28.17921
281192.1
563.5842
Magnesium
0.2635
2635 ;- , 5z2i
0.660162
5601.616
11.20323
Sulfur
0.127
1270 2.54.
0.269983
2699.83
5.39966
Zinc
0:066774
67 74; 0.13548
.0.014401
144.0051
0.28801
Copper.
0.003575
35 75`-; , 0.0715
0.0076
75.99915
0.151998
Manganese
0.004516
,' 4516+ . 0.09032
0.0096
96.0034
0.192007
Sodium
0.016699
166 99 ° 0.33398
0.0355
354.9957
0.709991
Calcium Carbonate E uivalenc,y
33.19
331900 - L 6638
'70.55697
705569.7
1411.139
CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT
CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES
BIOSOLIDS SAMPLE DATE: May-1,-2006-
Biosolids
Maximum
Maximum
Maximum
Maximum
Metal
Allowable
Allowable
Application
Application
Content,
Metal
App. Rate,
Rate,
Rate,
METALS ppm
Content, ppm
#/AcrefYr.
DT/Acre/Yr.
WT/Acre/Yr.
Arsenic, Total
1.39
41.00
1.80
324.73
649.46
Cadmium, Total
0.28 '.
39.00
1.70
1538.64
3077.29
Chromium, Total
19.57
1200.00
134.00
1711.87
3423.73
Copper, Total
23.60
1500.00
67.00
709.88
1419.76
Lead, Total
1.72
300.00
13.00
1886.41
3772.83
Mercury, Total,
0.14
17.00
0.75
1335.00
2670.00
Molybdenum, Total
1.31
18.00
0.80
152.57
305.14
Nickel, Total
8.49
420.00
18.70
550.49
1100.97
Selenium, Total
1.39
36.00
4.50
811.82
1623.65
Zinc, Total
60.21
1525:00
125.00
519.05
1038.10
PCB
BDL
1.60
" Actual metal content less than amount indicated.
Biosolids
Biosolids
Maximum
Maximum,
Nutrient
Nutrient
Crop/Soil Application
'Application
Content,
Content,
Requirement, Rate, ,
Rate,
ppm
%
#/Acre *° DT/Acre/Yr.
WT/Acre/Yr.
Ammonium Nitrogen
220.75
0'02
Organic Nitrogen
10568.43
1.06
Incorporated Available Nitrogen
6887.42
0.69
120.00
4.36
8.71
Surface Available Nitrogen
6821.19
0.68
120.00
4.40
8.80
Phosphorus as P205
5722.96
0.57
80.00
3.49
6.99
Potassium as K20
1385.21
0.14 '
50.00
9.02
18.05
Calcium, Total
139034.22
13.90
Calcium as C60
194647.90
19.46
Calcium as CaCO3 (CCE)
183907.28
18.39
2000.00
2.72
5.44
Magnesium, Total
2500.00
0.25
Manganese
77.26
0.01
Sulfur
1302.43
0.13
Percent Moisture
50.00
These are typical values and must be adjusted based upon specific site conditions
DT is Dry Tons of Biosolids. WT is Wet Tons of Biosolids.
CERTIFICATION: This biosolid product has been produced by the Town of Cheraw s Wastewater
Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature
and lime (calcium oxide). The Town of Cheraw certifies that this biosolid complies with the
Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has a metal
and nutrient content as presented above.
DIRECTIONS FOR USE: This biosolid is intneded to be used as a soil amendment. The biosolid
land application rate shall not exceed the most restrictive Maximum Application Rate as indicated in
the table above. The application rate for nitrogen, phosphorus, potassium, and calcium is dependent
upon the crop grown and site soil characteristics. The user shouldcontact the Clemson Extension .
Service (843-623-2134) and/or the Soil Con va sertion Service (843-623-2187) for assistance in
determining the proper application rate for each crop and site. In no case shall the land application
rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension .
Service Circular #476 titled "Lime and Fertilizer Recommendations."
THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY.
AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES.
THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS
BIOSOLID PRODUCT.
Mr. Ricky D. Ingram, Public Utility Director
P. 0. Box219; Cheraw, SC 29520
Telephone: 843-537-8440
FAX: 843-537-8442
PRODUCT USER NAME:
ADDRESS:
INTENDED USE:
LOCATION OF USE:
QUANTITY RECEIVED:
RECEIVED BY:
Davis & Brown
PO Box 15038
Quinby, SC 29506
(843) 665-6746 FAX: (843) 629-1444
Certificate of Analysis
Client: CHERAW, TOWN OF South Carolina Certification Number: 21117
P.O.BOX 219 North Carolina Certification Number: 612
CHERAW, SC 29520
Client #: 168 Receipt Date: 05-May-06
Contact: SHERRY TOLSON L" ReportDate: 01-Jun-06
Sample Date: 26-Apr-06
SDG #: SDG-048280
Approved By:
Van Ward,
-Lab Director
Reporting
Parameter Result Limit Unit Method
LSID-108152 5-4-06-F
Flag Date Time Analyst
Fluoride 0.96 0.2 mg/L SM 4500FC 5/16/2006 15:00 MLL
LSID-108153 SOURCE 050406
Total Organic Carbon 2.9 .0.5, mg/L EPA 415.1 5/17/2006 9:30 SM
LSID408154 FINISHED 050406
Total Organic Carbon <0.50 0.5 mg/L EPA 415.1 5/17/2006 9:30 SM
LSID-108155
Xr5_B-4W0-e-50TJUW
Acid Digestion (Solids)
YES
EPA 200,2
5/10/2006
9:00
DH
Percent Moisture
46.6
0.1
Wt%
SW846 3540
5/5/2006
15:30
JR
Aluminum, Total
3340
0.59
mg/kg
SW846 6010A
-5/15/2006
12:06
DH
Arsenic, Total
<1.48
1.48
mg/kg
SW846 6010A
5/15/2006
14:29
JR
Cadmium, Total
<0.295
0.295
mg/kg
SW846 6010A
5/10/2006
14:07
DH
Chromium, Total
20.9
0.295
mg/kg
SW846 6010A
5/10/2006
14:07
DH
Copper, Total
25.2
0.295
mg/kg
SW846 6010A
5/10/2006
14:07
DH
Lead, Total
1.84
1.5
mg/kg
SW846 6010A
5/10/2006
16:38
DH
Molybdenum, Total
1.40
0.981
mg/kg
SW846 6010A
5/31/2006
10:09
DH
Nickel, Total
9.07
0.295
mg/kg
SW846 6010A
5/10/2006
14:07
DH
Page 2
a
Davis & Brown
PO Box 15038
Quinby, SC 29506,
(843) 665-6746 FAX: (843) 6294444
Certificate of, Analysis
Client: CHERAW, TOWN OF South Carolina Certification Number:-21117
P.O.BOX 219 North Carolina Certification Number: 612
CHERAW, SC 29520
Client #: 168 Receipt Date:' 05-May-06
Contact: SHERRY TOLS'ON Report Date: 01-Jun-06
Sample Date: 04-May-06
SDG #: SDG-048280
Approved By: G ,
Van Ward
Lab Director
Reporting
Parameter
Result
Limit
Unit .
Method
Flag, Date
Time
Analyst
Zinc, Total
64.3
0.295
mg/kg
SW846 6010A
5/10/2006
14:07
DH
Mercury, Total
0.150
6.053
mg/kg
SW846 7470A
5/24/2006
14:18
DH
Selenium, :Total
<1.48
1.48
mg/kg
SW846 7741A
5/16/2006
13:39
JR
PCB
BDL
1.6
mg/kg
SW846 8080
S16 5/15/2006
9:42
JSW
LSID-108156 5-4-06-001
Acid Digestion (Liquids)
YES .
EPA 2002
5/8/2006
1:00
DH
Lead; Total
<0.050
0.05
mg/L
EPA200.7
5/10/2006
16:38
DH
Arsenic, Total
<0.005
0.005
mg/L
SM 3113B
5/15/2006
14:29
JR
Page 3
12065 Lebanon Rd.
Mt. Juliet, TN 37122
ENVIRONMENTAL
1-800 767-5859
SCIENCE CORP.
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
-REPORT OF ANALYSIS
Mr. Scott -Fields,
May
15,2006
Davis & Brown
P.O. Box 15038
Quinby, SC 29506 '
ESC
Sample #.: L244348-02
Date Received May
69, 2006
Description
Site
ID
Sample ID 108155 .
Project #
Collected By
Collection Date :, 05/04/06
13:00
Parameter
Dry Result
Det. Limit
Units
Method
Date
Analyst
Total Solids
44.9
%
25400-
05/13/.06 0834
MAS
Polychlorinated Biphenyls
PCB 1016
BDL
0.038
mg/kg
8082
05/15/06 0942
JSW
PCB 1221
BDL,'
0.038
mg/kg
8082
05/15/06 0942
JSW
PCB 1232
BDL
0.038
mg/kg
8082
05/15/06 0942
JSW
PCB•1242
BDL
0.038
mg/kg
8082
05/15/06 0942
JSW-
PCB 1248
BDL
0.038
mg/kg
B082
05/15/06 0942
JSW
PCB-1254
BDL
0.038
mg/kg
8082
05/15/06 0942
JSW
PCB 1260
BDL
0.038
mg/kg
8082
05/15/06 0942
JSW
Jeff Carr, ESC Representative
Results listed are dry weight basis.
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL) -
Laboratory Certification Numbers:
AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923,. IN - C-TN-01
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC-'84004, TN - 2006; VA - 00109, WV - 233
AZ -0612, MN - 047-999-395, NY - 11742, NJ.- 81002, WI - 998093910
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 05/15/06 16:01 Printed- 05/15/06 16:01
Page 2 of 5 '
0
ANIMAL WA91 LANAL Y J19KrFUK.1 rage 1 OIL
A N I M A L' W A S T-E A N A L Y S I S R E P O R T
Agricultural Service Laboratory
LAB No. -50771 Clemson University
TOLSON', SHERR ACCOUNT. COCHSFL
PO BOX 219 DATE 05-08-2006
CHERAW SC 29520 CHERAWTOWNOF656@BELLSOUTH.NET
SAMPLE N0. 5t0}]04� MANURE: OTHER STORAGE: UNCOVERED
-= SULTS REPORTED ON AN•AS-SAMPLED BASIS --------------
lbs/ton
Ammonium Nitrogen
0.02
%
0.40
Organic Nitrogen
0.96 .
%
19.15
Nitrate Nitrogen
207.91
ppm
0.42
INCORPORATED AVAILABLE NITROGEN
ESTIMATE
12.48
SURFACE AVAILABLE NITROGEN ESTIMATE
12.36
---------------------------------------------------------------
Phosphorus as P205
0.52
%
10.37
Potassium as K20
0.13
%
2.51
Calcium
12.60
%
251.93
Magnesium
0.23
%
4.53
Sulfur
0.12
%
2.36
Zinc
77.00
ppm
0.15
Copper
33.97
ppm
0.07
Manganese
72.47
ppm
0.14,
Sodium
167.14
ppm
0.33
Moisture
54.70
%
Calcium.Carbonate Equivalency
33.32
%
666.48
- - - - - - - - - - - - - - - - - - - - - 1- - - - - - - - - - - - - - - -----------------------------------------
INCORPORATED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
incorporated into the,soil within hours of application. Assumes some loss of
ammonium7N during application and prior to incorporation. -
SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be.
.left on the surface of the soil with no incorporation by plowing or irrigation.
Available nitrogen calculations are estimates and if nitrate-N was not re-
quested the amount of available nitrogen may be slightly more than reported.
Also, the actual amount may be more or less than the estimate depending on the
composition of.the manure, soil type, and environmental conditions.
All of the potash in the animal waste should be plant available in the first
year of application. Although not all of the phosphorous is available in -the
first year, its -availability shouldbe comparable to that in commercial
fertilizers.
The rate of animal waste to apply for crop,production is dependent on the
nutrient content of the waste, method of•application and incorporation, soil
test, crop to be grown, and previous manure applications. In most cases, the
plant available nitrogen content of the waste is used to determine the rate of
application.
The Agricultural Service Laboratory is a public service of Clemson University,
an affirmative action and equal opportunity educational institution.
** http://www.clemson.edu/agsrvlb **
http://www.clemson.edu/aglabresults/COCHSFLTOLSON,%2OSHERRO60508000000111tm • 5/9/2006
% moisture
% solids
lbs. solids/ton
lbs. solids/500 tons
547.
45.3
906
453000
ppm
lbs/ton
%
ppm
lbs/ton .
as -sampled
as -sampled
as=sam led ,
dry ton
dry ton
dry
Ammonium Nitrogen
0.02
200
b 4:
0.04415
441.6011
0.883002
Organic'Nitrogen
0.9575
9575
rr 19 15
2.113687,
21136.87
42.27373
Nitrate Nitrogen
0.020791
`;20T91
041582
0.045896
.458.9625
-,0.917925
Incorporated Available Nitrogen Estimate
0.624
: 62401.377483
13774.83
27.54967
Surface Available Nitrogen Estimate
0:618
6180
< F ' 12:36
1.364238
13642.38
27.28477
Phosphorus as P205
0.5185
5185
10.37
1.144592
11445.92
-22.89183
Potassium as 1C20
A1255
1255
`" 2 51'
0.277042
; 2770.419
5.540839
Calcium
12-.5965
125965
"; 25,1 s93
27.80684
278068.4
556.1369
Magnesium
0.2265
2265
A'53
` 0.5
5000
10
Sulfur
0.'118.
1180
`' 2:36
0.260486
2604.857
5.209713
Zinc
0.007,7
77;
0.154
0.016998
169.9773
0.339956
Copper
0.003397
y 33 97
0.06794
0.0.07499
74.98896
0.149978.
Manganese
0 007247,
" . 72
0.14494
0.015998
159.9779
0.319956
Sodium
0.016714
-'`16714:
.114
0.33428
0.036896
368.9625
0.737925
Calcium Carbonate Equivalency
33.324
333240 66648
73.56291
735629.1
1471.258
CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT
CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES
BIOSOLIDS SAMPLE DATE:" 13, 2005'V
Biosolids
Maximum
Maximum
Maximum
Maximum
Metal
Allowable
Allowable
Application
Application
Content,
Metal
App. Rate,
Rate,
Rate,
METALS porn
Content, ppm
#/Acre/Yr.
DT/Acre/Yr.
WT/AcrefYr.
Arsenic, Total
0.28
41.00
1.80
1584.78
3169.57
Cadmium, Total
0.51
39.00
1.70
839.63
1679.27
Chromium, Total
30.49
1200.00
134.00
1098.58
2197.17
Copper, Total
44.69
1500.00
67.00
374.19
749.59
Lead, Total
2.72
300.00
13.00
1196.59
2393.18
Mercury, Total
0:10
17.00
0.75
1808.04
3616.07
Molybdenum, Total
3.14
18.00
0.80
63.78
127.56
Nickel, Total
13.09
420.00
18.70
357.24
714.48
Selenium, Total
0.25 * "
36.00
4.50
4445.12
8890.24
Zinc, Total
82.84
1525.00
125.00
377.24
754.47
PCB
BDL
1.60
* Actual metal content less than amount indicated.
Biosolids
Biosolids
Maximum
Maximum
Nutrient
Nutrient
Crop/Soil
Application
Application
Content,,
Content,
Requirement,
.Rate,
Rate,
ppm
%
#/Acre'°
DT/Acre/Yr.
WT/Acrn1Yr.
Ammonium Nitrogen
385.80
0.04
Organic Nitrogen
7826.97
0.78
Incorporated Available Nitrogen
$680.94
0.57
120.00
5.28
10.56
Surface Available Nitrogen
6565.20
0.56
120.00
6.39
10.78
Phosphorus as P205
5608.60
0.56
80.00
3.57
7.13
Potassium as K20
781.25
0.08
50.00
16.00
32.00
Calcium, Total
139009.45
13.90
Calcium as Ca0
194613.23
19.46
Calcium as CaCO3 (CCE)
175583.53
17.56
2000.00
2.85
5.70
Magnesium, Total
2748.84
0.27
Manganese
101.27
0.01
Sulfur
1302.08
0.13
Percent Moisture
50.00
*° These are typical values and must be adjusted based upon specific site conditions
DT is Dry Tons of Biosolids. WT is Wet Tons of Biosolids.
CERTIFICATION: This biosolid product has been produced by the Town of Cheraw's Wastewater
Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature
and lime (calcium o)dde). The Town of Cheraw certifies that this biosolid complies with the
Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has a metal
and nutrient content as presented above.
DIRECTIONS FOR USE This biosolid is intneded to be used as a soil amendment. The biosolid
land application rate shall not exceed the most restrictive Maximum Application Rate as indicated in
the table above. The application rate for nitrogen; phosphorus, potassium, and calcium is dependent
upon the crop grown and site soil characteristics. The user should contact the Clemson Extension
Service (843-623-2134) and/or the Soil Conservation Service (843-623-2187) for assistance in
determining the proper application rate for each crop and site. In no case shall the land application
rate exceed the agronomic rate for the crop grown. User should "also refer to the Clemson Extension
Service Circular #476 titled "Lime and Fertilizer Recommendations."
THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY.
AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES.
THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS
BIOSOLID PRODUCT.
Mr. Ricky D: Ingram, Public Utility Director
P.O. Box 219; Cheraw, SC 29520
Telephone: 843-537-8440
FAX: 843-537-8442
QUANTITY RECEIVED:
RECEIVED BY:
-..
Davis - & Brown
PO Box 15038
Quinby, SC 29506
(843) 665-6746 FAX: (843) 629-1444
Certificate of Analysis
Client: CHERAW, TOWN OF South Carolina Certification Number: 21117
P.O.BOX 219 North Carolina Certification Number: 612
CHERAW, SC 29520
Client #: 168 Receipt Date: 14-Jul-06
Contact: SHERRY TOLSON Report Date: 03-Aug-06
Sample Date: 12-Jul-06
SDG #: SDG-049352
Parameter
LSID-1'10454
Acid Digestion (Solids)
Percent Solids
Aluminum, Total
Arsenic, Total
Cadmium, Total
Chromium, Total
Copper, Total
Lead, Total
Molybdenum, Total
Nickel, Total
Zinc, Total
Mercury, Total
Selenium, Total
PCB
Approved By:
Van Ward
Lab Director
Reporting
Result Limit Unit Method Flag Date Time Analyst
YES
EPA 200.2
40.5
0.1
wt%
SW846 3540
2990
75.1
mg/kg
SW846 6010A
0.230
0.205
mg/kg
SW846 6010A
<0.410
0.41
mg/kg
SW846 6010A
24.7
0.41
mg/kg
SW846.6010A
36.2
0.41
mg/kg
SW846 6010A
2.20
2.1
mg/kg
SW846 6010A
2.54
1.5
mg/kg
SW846 6010A
10.6
0.41
mg/kg
SW846 6010A
67.1
0.41
mg/kg
SW846 6010A
0.084
0.023
mg/kg
SW846 7470A
<0.205
0.205
mg/kg
SW846 7741A
BDL
1.5
mg/kg
SW846 8080
7/18/2606
10:00
DH
7/20/2006 '
17:30
JR
7/24/2006
17:49
DH
7/18/2006
14:28
JR
7/19/2006
9:17
DH
7/19/2006
9:17
DH
7/19/2006
9:17
DH
7/19/2006
15:46
DH
7/24/2006
17:54
DH
7/19/2006
9:17
DH .
�7/19/2006
9:17
DH
7/24/2006
13:29
DH .
7/18/2006
20:06
JR
S16 7/20/2006
21:56
TLW
L9I13-110455 7-13-06-F
Fluoride 1.08 0.2 mg/L SM 4500FC 7/24/2006 14:00 MLL
LSID-110456 SOURCE H2O
Page 2
J
Lebanon R37
Mt. Juliet, TN 122 "
ENVIRONMENTAL
(615) 758-5858
1-800-767-58s9
-SCIENCE CORP.
Fax (615) 7 e-se59
Tax I.D. 62-0814289
Est. 1970 .
REPORT
OF ANALYSIS
Mr. Scott Fields
July 24,2006
Davis & Brown
P.O. Box 15038
Quinby, SC 29506
ESC Sample # L253316-01
Date Received July
19,: 2006
Description
Site ID
Sample ID 110454
Project
.:
#"_
Collected By
Collection Date b7/13/0:6
00:00
Parameter
Dry Result
Det. Limit
Units`
Method
Date Analyst
Total: Solids
40.4
%
2540G
07/22/06 1214 LF
Polychlorinated Biphenyls
PCB 1016
BDL
0.21
mg/kg
8082
07/20/06 2156 TLW
PCB 1221
BDL
0.2
mg/kg
8082
07/20/06 2156 TLW
PCB 1232
BDL-
0.21 -
mg/kg
8082
07/20/06 2156 TLW
PCB 1242
BDL
0.21
.mg/kg
8082
07/20/06,2156 TLW
PCB 1248
BDL
0.21
mg/kg
8082
07/20/06 2156 TLW
PCB 1254
B6L
0.21
mg/kg
8082
07/20/06 2156 TLW
PCB 1260
BDL
0.21
mg/kg
8082
07/20/06 2156 "TLW
Results listed are dry weight
basis.
BDL- Below. Detection Limit
Det,. Limit - Practical Quantitation Limit(PQL)
Laboratory
Certification
Numbers:
ANIMAL WAN 1EANALYNINKEYUK1 Page Iot2
A N I M
A L W A S T E A
N A L Y S I
S R E P O R T
Agricultural Service
Laboratory
LAB No. 71013-
Clemson University'
TOL'SON, SHERRY
ACCOUNT
COCHSFL
PO BOX 219
DATE
07-26-2006
CHERAW SC
29520
CHERAWTOWNOF656@BELLSOUTH.NET
SAMPLE NO. 7'13`'6 'MANURE: OTHER STORAGE:
UNCOVERED
-----------------RESULTS
REPORTED ON AN AS -SAMPLED BASIS ----------------------
lbs/ton
Ammonium Nitrogen
0.04
%
0.80
Organic Nitrogen
0.81
%
16.23
Nitrate Nitrogen
438.07
ppm
0.88
INCORPORATED AVAILABLE
NITROGEN ESTIMATE
11.78
SURFACE AVAILABLE
NITROGEN ESTIMATE
11.54
-------•--------------------------------------------------------
Phosphorus as P205
0.58
%
11.63
Potassium as K20
0.08
%
1.62
Calcium
14.41
%
288.25
Magnesium
0:29
%
5.70
Sulfur
0.13
%
2.70
Zinc
81.91
ppm.
0.16
Copper
34.73
ppm
0.07
Manganese
106.80
ppm
0.21
Sodium
125.98
ppm
0.25
Moisture.
48:16
%
Calcium Carbonate
Equivalency 36.41
%
728.18
--------------------------------------------------------------------------'----
INCORPORATED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure,will be
incorporated into the soil within hours of application. Assumes some loss of
ammonium-N during application and prior to incorporation.
SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
left on the surface of the soil with no incorporation by plowing or irrigation.'
Available nitrogen calculations are estimates and if nitrate-N was not re-
quested the amount of available nitrogen may slightly more than reported.
Also, the actual amount may be more or less than the estimate depending on the
composition of the manure, soil type, and environmental conditions.
All of the potash in the animal waste should be plant available in the first
year of application. Although not all of the phosphorous is available in the
first year, its availability should be comparable to that,in commercial
fertilizers.
The rate of animal waste to apply for crop production is dependent on the
nutrient content of the waste, method of application and incorporation, soil
test, crop to be grown, and previous manure applications. In most cases, the
plant available nitrogen content of the waste is used to determine ,the rate of
application.
The Agricultural Service Laboratory is a public service of Clemson University,
an affirmative action and equal opportunity educational institution.-
http://www.clemson.edu/agsrvlb
http://www.clemson.edu/agsrvlb **
http://Www.clemson.edu/aglabresults/COCHSFLTOLSON%20SHERRY0607260000001.htm 7/27/06
% moisture
% solids
lbs. solidsiton
lbs. solids1500 tons
4816
51.84
1036.8
518400
%
ppm Ibstton
'
%
ppm ., :
lbs/ton,
as -sampled-
as -sampled as-sam led
dry ton
dry ton -
dry
Ammonium Nitrogen
0.04
400 08
0.07716
771.6049
1.54321
Organic Nitrogen
' 0.8115
8115 18 23
,1.565394:
15653.94
31.30787
Nitrate Nitrogen
0.043807
438 07 0.87614
0:084504
845.0424
1.'690085
Incorporated Available Nitrogen Estimate
0.589
5890 11 78
1136188
11361.88
22.72377
Surface Available Nitrogen Estimate
0.577
5770 t11 54:
,1;11304.
11130.4
2-2.2608
Phosphorus as P205
0.5815
5815 11'63;
1.121721
11217.21
22.43441
Potassium as K20
0:081
810 1'.fi2'
0.15625
1562.5
3.125
Calcium
14.4125
144125 288.25'
27.80189-
278018.9
556.0378
Magnesium
0:285
2850 5:7
0.549169
5497.685
10.99537
Sulfur
0.135
1350 ` g 27
0.260417
2604.167
5.208333
Zinc
0.008191
0.16382
0.015801
158.0054
0.316011
Copper
0/.003473
', 34 73 0.06946
0.006699
66.9946
0.133989
Manganese
0.01068
j ,.,L ,106`8a 0.2136
0.020602
206.0185
0.412037
Sodium
0.012598
° 1{2598 0 25196
0.024302'
243.017
0.486034
Calcium Carbonate E uivalenc
36.409
364090 " 7.28:-18
70.23341
702334.1
1404.668
CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT
CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES
BIOSOLIDS SAMPLE DATE: %eptember 77.2006
Biosolids
Maximum
Maximum
Maximum
Maximum
Metal
Allowable
Allowable.
Application
Application
Content,
Metal
App. Rate,
Rate,
Rate,
METALS
pp m
Content, ppm
#/AcrelYr.
DT/Acre/Yr.
WT/Acre/Yr.
Arsenic, Total
1.54 '
41.00
1.80
291.43
582.86
Cadmium, Total
0.31' '
39.00
1.70
1376.19
2752.38
Chromium, Total
23.24
1200.00
134.00
1441.77
2883.54
Copper, Total
58.82
1500.00
67.00
284.75
569.60 ,
Lead, Total
3.26
300.00
13.00
995.50
f 1990.99
Mercury, Total
0.06
17.00
0.75
2897.73
5795.45
Molybdenum, Total
2,60
18.00
0.80
76.84
153.67
Nickel, Total
27.35
420.00
18.70
170.91
341.83
Selenium, Total
1.54
36.00
4.50
728.57
1457.14
Zinc, Total
94.71
1525.00
125.00
329.97
659.94.
PCB
BDL
1.60
"Actual metal content less than amount indicated.
Biosblids Biosolids Maximum Maximum
Nutrient Nutrient Crop/Soil Application Application
Content, Content, Requirement, Rate, Rate,
aam % #/Acre" DT/Acre/Yr. WT/Acre/Yr.
Ammonium Nitrogen
1863.77
0.19
Organic Nitrogen
15325.31
1.53
Incorporated Available Nitrogen
11453.74
1.15
120.00
2.62
5.24
Surface Available Nitrogen
10894.61
1.09
120.00
2.75
5.51
Phosphorus as P205
9623.86
0.96
80.00
2,08
4.16
Potassium as K20
1872.25
0.19
50.00
6.68
13.35
Calcium, Total
80167.74
8.02
Calcium as CaO
112234.84
11.22
Calcium as CaCO3 (CCE)
95967.47
9.60
2000.00
5.21
10.42
Magnesium, Total
-1948.49
0.19
Manganese
203.32
0.02
Sulfur
1702.81
0.17
Percent Moisture
50.00
" These are typical values and must be adjusted based upon specific site conditions
DT is Dry Tons of Biosolids. I WT is Wet Tons of Biosolids.
CERTIFICATION: This biosolid product has been produced by the Town of Cheraw's Wastewater
Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature
and lime (calcium oxide). The Town of Cheraw certifies that this biosolid complies with the
Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has a metal
and nutrient content as presented above.
DIRECTIONS FOR USE: This biosolid is intneded to be used as a soil amendment. The biosolld
land application rate shall not exceed the most restrictive Maximum Application Rate as indicated in
the table above. The application rate for nitrogen, phosphorus, potassium, and calcium is dependent
upon the crop grown and site soil characteristics. The user should contact the Clemson Extension
Service (843-623-2134) and/or the Soil Conservation Service (843-623-2187) for assistance in
determining the proper application rate for each crop and site. In no case shall the land application
rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension
Service Circular #476 titled "Lime and Fertilizer Recommendations."
THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY.
AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES.
THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS
BIOSOLID PRODUCT.
Mr. Ricky D. Ingram, Public Utility Director
P.O. Box 219, Cheraw, SC 29520
Telephone: 843-537-8440
FAX: 843-537-8442
RECEIVED BY:
Davis &'Brown
PO Box 15038
Quinby, SC 29506
(843) 665-6746 FAX: (843) 629-1444
Certificate of Analysis
Client: CHERAW, TOWN OF South Carolina Certification Number: 21117
P.O.BOX 219 North Carolina Certification Number: 612
CHERAW, SC 29520
Client #: 168 Receipt Date: 08-Sep-06
Contact: SHERRY TOLSON Report Date: 27-Sep-06
Sample Date: 06-S'ep-06
SDG #: SDG-050277 Approved By:���
Van Ward
Lab Director
Reporting
Parameter Result 'Limit Unit Method Flag Date Time Analyst
LSID-112411 1005-B
Oil and Grease 57.2 5 mg/L EPA 413.1 9/13/2006 13:00 JR
LSID-112412 1005-T
Oil• & Grease, Hydrocarbon 6.0 5 mg/L SM 503E 9/13/2006 15:00 JR
LSID-112413
1005-D
Chemical Oxygen Demand 1900
100 J
mg/L
EPA 410.4
9/15/2006
9:30
DH
LSID-112414
RIO'-``S"6LID 09-07-0' 00*
Acid Digestion (Solids)
YES
EPA 200.2
9/12/2006
-10:00
DH
Percent Moisture
66.0
0.1
wt%
SW846 3540
9/8/2006
16:30
JR
Aluminum, Total
4730
0.397
mg/kg
SW846 6010A
9/22/2006
10:01
DH
Arsenic, Total.
<1.05
1.05
mg/kg
SW846 6010A
9/13/2006
19:26
JR
Cadmium, Total
<0.210
0.21
mg/kg
SW846 6010A
9113/2006
17:51
DH
Chromium, Total
15.8
0.21
mg/kg
SW846 6010A
9/14/2006
12:42
DH
Copper, Total
40.0
0.21
mg/kg
SW846 6010A
9/13/2006
17:51
DH
Lead, Total
2.22
1.1
mg/kg
SW846 6010A
9/15/20U6
9:23
DH
Molybdenum, Total
1.77
0.794
mg/kg
SW846 6010A
9/21/2006
9:48
'DH
Nickel, Total
18.6
0.21
mg/kg
SW846 6010A
9/13/2006
17:51
DH
Zinc, Total
64.4
0.05
mg/kg
SW846 6010A
9/13/2006
17:51
DH
Page 1
Davis & Brown
PO Box 15038
Quinby, SC 29506
(843) 665-6746 FAX: (843) 629-1444
Certificate of Analysis
Client: CHERAW, TOWN OF South Carolina Certification Number: 21117
P.O.BOX 219North Carolina Certification Number: 612
CHERAW, SC 29520
Client #: 168 Receipt Date: 08-Sep-06
Contact: SHERRY TOLSON Report Date: 27-Sep-06
Sample Date: 07-Sep-06
SDG #: SDG-050277
Approved By:
Van Ward
Lab Director
Reporting
Parameter
Result
Limit
Unit
Method
Flag Date
Time
Analyst
Mercury, Total
0.044
0.019
mg/kg
SW846 7470A-
9/19/2006
12:66
DH.
Selenium, Total
<1.05
1.05
mg/kg
SW846 7741A
9/13/2006
16:59
JR
PCB
BDL
1.6
mg/kg
SW846 8080
S16 9/1-4/2006
12:06
TLW
LSID-112415 FINISHED WATER 9-7-06
Total'Organic Carbon
2.0
0.5
mg/L
EPA 415.1
9/15/2006
9:30
SF
LSID-112416 SOURCE WATER 9-7-06
Total Organic Carbon
4.5
0.5
mg/L
EPA 415.1
9/15/2006
9:30
SF
LSID-112417 .9-7-06-F
Fluoride
0.90
0.2
mg/L
SM 4500FC
9/13/2006
14:00
MLL-
Page 2
12065 Lebanon Rd.
Mt. 'Juliet, TN 7122
ENVIRONMENTAL-800-767-5859
Fax (615) 758-58,59
SCIENCE CORP .
Tax B.D.62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. 'Scott Fields September 19,2006
Davis &'Brown
P.O' Box 15038
Quinby, SC 29506
ESC Sample # L260494-03
Date Received, September 12, 2006
Description
Site ID
Sample,ID 112414
Project #
Collected By
Collection Date 09/07/06 1j,:45
Parameter- Dry Result.Det. Limit Units Method: ;Date Analyst
Total Solids 33.0' % 254OG 09/16/06 0850'.MAS
Polychlorinated Biphenyls
PCB�1016 BDL 0.26 mg/kg 8082 09/14/06 1206 TLW
PCB 1221 BDL 0.26 mg/kg 8082 09/14/06 1206 TLW
PCB 1232 BDL 0.26 mg/kg 8082 09/14/06 1206 TLW
PCB 1242 BDL0.26 mg/kg 8082 09/14/06 1206 TLW
PCB 1248 BDL 0.26 mg/kg 8082 09/14/0.6 1206 TLW',
PCB 1254 BDL 0.26 mg/kg 8082 09/14/06 1206 TLW
PCB'12'60 BDL 0.26 mg/kg 8082 09/14/06 1206 TLW
Results listed are dry weight basis.
BDL,- Below Detection Limit
'Det. Limit - Practical Quantitation Limit(PQL)•
Laboratory Certification Numbers:
AIHA - 100789, AL - 40660,'CA - I-2327," CT- PH-.0197, FL - E87487, GA - 923, IN - C-TN-01
KY'- 90010, KYUST-•0016, NC-'.ENV375,'DW21704, ND - R-1401- SC _ 84004, TN - 2006, VA'-.00109, WV - 233
A2 -0612, MN.- 047-999-395, NY - 11742, NJ - TN002, WI - 998093910..
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted ,
Reported: 09/18/06 13:43 Revised: 09/19/06 07:55
Page 3 of 5,
= A 114 1 lYl n, L YY 1-1 0 1 L 111 14 r-1 L i a 1 a 1C Z r V 1C 1
rage i of
A N I M A L W A S T E A N A L Y S I S R`E P 0 R T
Agricultural Service Laboratory
LAB No. 91224 Clemson University
TOLSON, SHERRY
PO BOX 219
CHERAW.SC 29520
ACCOUNT COCHSFL
DATE 10-02-2006
CHERAWTOWNOF656@BELLSOUTH.NET
SAMPLE NO. &Oc7,0.65:Oj INURE: OTHER
STORAGE: UNCOVERED
--------- RESULTS REPORTED
ON AN AS -SAMPLED BASIS ----------------------
lbs/ton
Ammonium Nitrogen
0.11
%
2.20
Organic Nitrogen
0.90
%
18.09
Nitrate Nitrogen
-----------------------------------------------
282.75
ppm
----------------
•0.57
INCORPORATED AVAILABLE NITROGEN ESTIMATE
13:52
SURFACE AVAILABLE NITROGEN
---------------------------------------------------------------
ESTIMATE
12.86
Phosphorus as P205
0.57
%
11.36
Potassium as K20
0.11
%
2.21
Calcium
4.73
%
94.63
Magnesium
0.12
%
2.30
Sulfur
0.10
%
2.01
Zinc
59.03
ppm
0.12
Copper
39.55
ppm
0.08
Manganese
119.83
ppm
0.24
Sodium
132.23
ppm
0.26
Moisture 70.49 %
Calcium Carbonate Equivalency 11.33 %
226.56
------------------------------------------------------------------------------
INCORPORATED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
incorporated into the soil within hours of application. Assumes some loss of
ammonium-N during application and prior to�incorporation.
SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
left on the surface of the soil with no incorporation by plowing or irrigation.
Available nitrogen calculations are estimates and if nitrate-N was not re-
quested the amount of available nitrogen may be slightly more than reported.
Also, the actual amount may be more or less than the estimate depending on the
composition of the manure, soil type, and environmental conditions.
All of the potash in the animal waste should be plant available in the first
year of application. Although not all of the phosphorous is available in the
first year, its availability should be comparable to that in commercial
fertilizers.
The rate of animal waste to apply for crop production is dependent on the
nutrient content of the waste, method of`application and incorporation, soil
test, crop to be grown, and previous manure applications. In most cases, the
plant available nitrogen content of the waste is used to determine the rate of
application.
The Agricultural Service Laboratory is a public service of Clemson University,
an affirmative action and equal opportunity educational institution.
** http://www.clemson.edu/agsrvlb **
http://www.clemson.edu/aglabresults/COCHSFLTOLSON,%2OSBERRY0610020000006.htm 10/5/06
moisture
% solids
lbs. solidsiton
lbs. solids/500 tons
::. . ',70:49
29"51
590.2
295100
ppm Ibs/ton
%
ppm.
lbs/ton
as-sam lets
as -sampled as -sampled
dry,ton
d ton
dry
Ammonium Nitrogen
0.11
1100 .2:2
0.372755
3727.55
. 7.4551
Organic Nitrogen
0.9045
9045 1'8a09:
3.065063
30650:63
61.30125
Nitrate Nitrogen
0.028275
: 282 75' 0.5655
0.095815
958.1498
1.9163
Incorporated Available Nitrogen Estimate
0.676
6760 13:52
2290749
22907.49
45.81498
Surface Available Nitrogen. Estimate
0.643
6430 12 86
2.1789"
21789.22
43-57845
Phosphorus as P205_
0.568
5680 11 36
1:924771
19247.71
38.49543
Potassium as K20
0.1105
1105 ' sF 2 2f
0.374449
3744.403
7.488987
Calcium
4.7315
47315 -, '04.63
16.03355
160335.5
320.671
Magnesium
0.115
t-,
11.50 2.3
0.389698.3896.984
7.793968
Sulfur
0.1005
1005 _` 2 01j
0.340563
3405.625
6.81125
Zinc
0.065903
59 R03 0.11806
0.020003
200.0339
0.400068
Copper
0.003955
r ; `39 55 " 0.0791
0.013402
134.0224
.0.268045
Manganese
0.011983
°' 119 83 0.23966
0.040607
406.0657
0.812131
Sodium
0.013223
' 1.32 23 0 26446
0.044809
448.0854
0.896171
Calcium Carbonate E uivalen
11.328
. 115280 s 226:56
38.38699
383869.9.
767J397
CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT
CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES
BIOSOLIDS SAMPLE DATE:'pc e-Mber-fi;,2006W'
METALS
Biosolids
Metal
Content,
ppm
Maximum
Allowable
Metal
Content, ppm
Maximum Maximum
Allowable Application
App. Rate, Rate,
#/Acre/Yr. DT/AcreJYr.
Maximum
Application
Rate,
WT/AcrelYr.
Arsenic, Total
1.25 '
41.00
1.80
360.00'
720.00
Cadmium, Total
0.25 `
39.00
1.70
1706.32
. 3412.64
Chromium; Total
20.74
1200.00
134.'00
1615.18
3230.36
Copper, Total
45.00
1500.00
67.00
372.22
744.44
Lead, Total
3.18
300.00
13'00
1023.32
2046.65
Mercury, Total
0.17
17.00
0.75
1112.64
2225.27
Molybdenum, Total
0.62 •
.18.00
0.80
244.07
488.14
Nickel, Total .
18.52
420.00
18.70
252.45
504.90
Selenium, Total
1.25 '
36.00
4.50
900.00
1800.00
Zinc, Total
84.35
1525.00
125.00
370.47
740.94
PCB
BDL
1.60
' Actual metal content less than amount indicated.
-
Biosolids
Biosolids
1
Maximum
Maximum
Nutrient
Nutrient
Crop/Soil Application
Application
Content,
Content,
Requirement, Rate,
Rate,
ppm
%
#/Acre" DT/AcrelYr.
WT/AcrafYr.
Ammonium Nitrogen
Organic Nitrogen
Incorporated Available Nitrogen
Su -dace Available Nitrogen
Phosphorus as P205
Potassium as K20
Calcium, Total
423.91
0.04
7852.90
0.79
6008.90
0.60
120.00
5881.73
0.59
120.00
6411.62
0.64
80.00
1266.43
0.13
50.00
150365.62
15.04
4.99 9.99
5.10 10.20
3.12 6.24
9.87 19.74
Calcium as Cab
210511.87
21.05
Calcium as CaCO3 (CCE)
339683.13
33.97 2000.00 1.47 2.94
Magnesium, Total
2750.11
0.28
Manganese
185.46
0.02
Sulfur
1250.53
0.13
Percent Moisture
50.00
These are typical values and must be adjusted based upon specific site conditions
DT is Dry Tons of Btosolids. WT is Wet Tons of Biosolids,
CERTIFICATION: This biosolid product has been produced by the Town of Cheraw'iWastewater
Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature
and(lime (calcium oxide). The Town of Cheraw certifies that this biosolid complies with the
Environmental Protection Agency regulations 40 CFR Part 503 for a "Class Al' product and has a metal
and nutrient content as presented above.
DIRECTIONS FOR USE: This biosolid is intneded to be used as a soil amendment.. The biosolid .
land application rate shall not exceed the most restrictive Maximum Application Rate as indicated in
the table above. The application rate for nitrogen, phosphorus, potassium, and calcium is dependent
upon the crop grown and site soil characteristics. The user should contact the Clemson Extension
Service (843-623-2134) and/or the Soil Conservation Service (843-623-2187) for assistance in
determining the proper application rate for each crop and site. In no case shall the land application
rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension
Service Circular #476 titled "Lime and Fertilizer Recommendations."
THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY.
AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES.
THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS
BIOSOLID PRODUCT.
Mr. Ricky D. Ingram, Public Utility Director
P.O. Box 219; Cheraw, SC 29520
Telephone:' 843-537-8440
FAX: 843-537-8442
Davis & Brown
PO Box 15038
Quinby, SC 29506
(843) 665-6746 FAX: (843) 629-1444
Certificate of Analysis
Client: CHERAW, TOWN OF South Carolina Certification Number: 21117
P.O.BOX 219
CHERAW, SC 29520
Client #: 168 Receipt Date: 06-Nov-06
Contact: SHERRY TOLSON Report Date: 28-Nov-06
Sample Date: 06-Nov-06
SDG SDG-051175
#: Approved By:
Van Ward
Lab Director
Reporting
Parameter Result Limit Unit Method Flag, Date Time Analyst
LSID-114251
$IOS"OLIDS'11 66=06=500
Acid Digestion (Solids)
YES
EPA 200.2
11/7/2006
10:00
DH
Percent Moisture
46.0
0.1
wt%
SW846 3540
11/8/2006
17:30
JR
Aluminum, Total
6.32
0.445
mg/kg
SW846 6010A
11/14/2006
10:57
DH
Arsenic, Total
<1.35
1.35
mg/kg
SW846 6010A
11/14/2006
16:27
JR
Cadmium, Total
<0.269
0.269
mg/kg
SW846 6010A
11/7/2006
15:56
DH
Chromium, Total
22.4
0.269
xng/kg
SW846 6010A
11/7/2006
15:56
DH
Copper, Total
48.6
0.269
mg/kg
SW846 6010A
11/7/2006'
15:56
DH
Lead, Total
3.43
1.4
mg/kg
SW846 6010A
1.1/8/2006
16:42
DH
Molybdenum, Total
<0.885
0.885
mg/kg
SW846 6010A
11/27/2006
15:55_
DH
Nickel, Total
20.0
0.269
mg/kg
SW846 6010A
11/7/2006
15:56
DH-
Zinc, Total
91.1
0.269
mg/kg
SW846 6010A
-11/7/2006
15:56
DH
Mercury, Total
0.182
0.066
mg/kg
SW846 7470A
11/20/2006
14:17
DH
Selenium, Total
<1.35
1.35
mg/kg
SW846 7741A
11/15/2006
17:15
DH
PCB
BDL
1.6
ug/kg
SW846 8080
S11 11/9/2006
18:09
KA
LSID-114252 FINISHED WATER
Chloride- IC 20.2 1 mg/L EPA 300.0 11/8/2006 11:02 SF
LSID-114253 FINISHED WATER
Page 1
AINIAlALWAalhANAL YJI�;.K_,YUKh Pagel oft
A N I M A L W A S T E, A N A L Y S I S R E P O R T
Agricultural Service.Laboratory
LAB No. 111390 Clemson University
TOLSON, SHERRY, ACCOUNT COCHSFL
PO BOX 219 DATE 11-16-2006'
CHERAW SC 29520 CHERAWTOWNOF656@BELLSOUTH.NET
SAMPLE NO. 11060;6 0 URE: OTHER STORAGE: UNCOVERED
------------
RESULTS REPORTED ON AN AS -SAMPLED BASIS--- -------- ---=_-------
lbs/ton
Ammonium Nitrogen
0.04
%
0.80
Organic Nitrogen
0.74
%
14,82
Nitrate Nitrogen
---------------------------------------------------------------
566.21
ppm
1:13
INCORPORATED AVAILABLE NITROGEN
ESTIMATE
11.34
SURFACE AVAILABLE NITROGEN ESTIMATE
11.10
Phosphorus as P205
0.61
%
12.10
Potassium as K26
0.12
%
2.39
Calcium
14.19
%
283.77
Magnesium
0.26
%
5.19
Sulfur
0.12
%
2.36
Zinc
64.64
ppm
0.13
Copper
34.44
ppm
0.07
Manganese
174.11
ppm
0.35
Sodium
203.84
ppm
0.41
Moisture
52.82
%
Calcium Carbonate Equivalency
32.05
$
.641..05
------------------------------------------------------------------------------
INCORPORATED PLANT AVAILABLE'NITROGEN ESTIMATE - 80% of ammonium-N, 60% of
organic-N, and 100% of_nitrate-N (if determined). Assumes the manure will'be
incorporated into the soil within hours of application. Assumes some loss of
ammonium-N during application and prior to incorporation.
SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 6'0% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
left.on the surface of the soil with no incorporation"by plowing or irrigation.
Available nitrogen calculations are estimates and if nitrate-N was not re-
quested the amount of'available nitrogen may be slightly more than reported.
Also, the actual amount may be more or less than the estimate depending on the
composition of the manure, soil type, and environmental conditions.
All of the potash in the animal waste should be plant available in the first
year of application. Although not all: of the phosphorous is available in the
first year,.its availability should:be comparable to that in commercial
fertilizers.
The rate of animal waste to apply for crop production is dependent on the
nutrient content of the waste, method of application and incorporation, soil
test, crop to be grown, and previous manure applications. In most cases, -the
plant available nitrogen'content of the waste is used to determine the rate of
application.
The Agricultural Service Laboratory is a public service of Clemson University,
an affirmative action and equal opportunity educational institution.
**-http://www.clemson.edu/agsrvlb **
hq://www.clemson.edu/aglabresults/COCHSFLTOLS ON,%20SHERRY0611160000001.h... 11 /17/06
% moisture
% solids
lbs. solids/ton
lbs. solids/500 tons
47.18.
"943.6
471800
%
ppm Ibst.ton .
% .;,
ppm
lbstton
"
as -sampled
as -sampled as-sam" led
ft ton
'dry tone
dry
Ammonium Nitrogen
0.04
400 , :'08
0.084782
847.8169
1.695634
Organic Nitrogen. .
0.741
7410 � - 14:82
1:570581 `
15705:81
31.41162
Nitrate Nitrogen
0;056621
=566 21' 1.13242
0:120011
1200.106
2.400212
Incorporated Available Nitrogen Estimate
0.567
5670 ;. a 11 34.
1.20178
12017.8
24.03561
Surface Available Nitrogen Estimate
0.555 .
5550 . Ir>_, , ,1.1.1,
1.176346
11763:46
23.52692
Phosphorus as P205
0.605
' 6050 , 12:1'_
1.282323
12823.23
25.64646
Potassium as K20
0.1195
.. 1195 . , >y . , 2`39
0.253285
2532.853
5.065706
Calcium
- 14.1885
141885 28347
'30.07312
3007312
601.4625
Magnesium
0.2595:.
2595 ;: 5:16
0.550021
5500.212
11.00042
Sulfur
0.118
1180 .... ,_, = . ,;2:36;
0.250106
2501.06
5.00212
Zinc
0.006464 :, 64 64, 0:.12928
0.013701
137'0072
.0.274014
Copper
0.003444
r. 3444 0.06888
0.0073
72.99703
.0.145994
_
Manganese
0.017411
t17411 034822
0.036903
'369.0335
0.738067
Sodium
0.020384
203 84 0.40768
0.043205
432.0475
0.864095
Calcium Carbonate E uivalenc
32.0525
320525 641 6
67.93663
679366.3
1358.733
Pasteurization vessel operates on a constant speed with an in/out
time duration of 30°minutes.
-
MINIMUM 'MINIMUM
DATE '
2 HOUR pH 24 HOUR pH.
TEMP IN
TEMP OUT
01/09/06
12.38
12.26
°158
157
01/12/06
12.79
12V
152
162
01/13/06
12.16.
12.08
- -156
159"
01/23/06,
12.32
12.25
160
- 160
01 /24/06 .
12.33
12.17
158
157
01 /25/06
' 12.24 '
12.07
166
165 .
01 /26/06
12.36
12.19
- 157
:. '160
01/27/06
12.01
11.87-
158
159
01/30/06
12.19
11.97
158-
158
- 01 /31 /06
- 12.03
11.86
157
157
02/01/06
1236 .
12.18-
157
158
02/06106.
12.19
12.08
160
160
' 02/07/06
12.16
12.62
169
158
02/08/06
.12.09. ,
11.92
158
160.
`02/09/06
12.17
12.10
159
160 ,
02/ 10/06
12 -"47
12.31
160
167
02/13/06
12.07 .; "
12.01
157.
159 .
02/14/06 •
. 12.32
12.10
160
164 ,
02/15/06
12.29
12.08.
158
-150 --
02/16/06
12.27:,
12.12
162
.162
02/17/06
1229
12.13
162
158,
02/20/06
12.27
12.02
,'.160
148
02/21 %06
1 i 19
12.08
160
160
02/22/06
12.28 •
' 12.13
159
. .158
02/23/06
12.27
12.04
162
- 158
02/24/06,
12.33
12.13
, ' - ' 164
160
" 02/27/06
" 12.44
12:27
160
_ 162
02/28/06
12.38
12.10158
159
03/01 /06
12.27
12.07
158
163 .
03/02/06
- 12.22
12.03
-158
160 ,
03/03/06
12.08
11.90
158
160' "
03/06/06
12.29 ..
12.0-1
163-
169
03/07/06
12.14
12.06
159
1.62"
03/06/06
12.26•
12.1.7
'161
164
03/09/06
12.32:
-12.10
-160
159
03/10/06
12.33
12.25
158
-160..
03/13/06
12.21
11.97
158
163
03/ 15/06
12.09
11.91
158
159
03/16/06
12.00
11.94
159'
164
03/17/06
12.21 "
12.03
164
160
03/20/06
12.02 '
11.91
164
164
03/21/06
12.24
' 11-88
169
162
03/22/06
12.08
11:90
160
158 -
03/23/06
12.22
12.08
. 165
,-"169
03/24/06
12.36 "
12.15
161
'160
03/27/06
12.18
12.98
167
165, -
03/28/06
12.20
12.06
158
164.
03/29/06
12t.24.
11.97
162
. " 167 :
03/30/06
12.09
12.03
166
164
03/31 /06
112.14.
12.03
160
167 '
Pasteurization vessel operates on a.constant speed vAth an in/out
time duration of 30 minutes.
MINIMUM
MINIMUM
DATE .2 HOUR pH 24 HOUR pH
TEMP IN
TEMP OUT
04/03/06
12.16
12.08
169-
168
W04/06
12.20
12.01
166
160
04/05 06
12.16 .
12.03
.160
. 160 -
04/06/06
12.21
11.69
162
100
04/07/06
12.22
12.03
166'
165 °
04/10/06
12.06
11.94
163"
166
04/11/06 -
12.02
11.89
160
164
04/12/06
12.08
.11.93
161
163 -
04/13/06
1.2.09
12.00
171
174
04/14/06
12.03
11.93
162
163 .
04/18/06
12.02
11.90
167
170
04/19/06
12.09
12.87
162
160
04/20/06
12:06
11.89
163
161
04/21 /06
12.11
11.96
162
163
04/24/06
12.04
12.59
162-
165
04/25/06
12.03
11.94
165
.166
04/26/06
12.07
11.93
161
- 160
04/27/06
12.24
11.91
158
159
04/28/06
12.09
1,1.93
164
164
05101 /06
1223
12.04
160
165
05102.106
12.22
11.98
159
160
05/03/06
12.10
11.77 -
165
163
05/05/06
12.21
11.99
165
160
05/08/06
.12.25
11.97
159
162
0 510 9/06
12.15
11.72
158
162
05/10/06
12.20
12.13
162
165
05/11 /06
12.31
12.10
163
161
05/12/06
12.26
12.03
158
159
65/15/06 .
12.16
12.03
158
163
05/16/06
12.18
12.05
162
158
05/17/06
12.17
12.04
160
158
05/18/06
12.24
. 11.93
162
159 -
05/19/06
12.21
11.99
160
158 .
05/22/06
12618
12.03
160
166
06/29/06 ,
• 12.15
11.97
163
158
06/30/06
12.17
12.00
162
160
138810
..38811
38812
38813
38814
38817
38818
38810
38820
38821
38825
38826
38827
38828
38831
38832
38833
38834
38835
38838
38839
38840
38842
38845
38846
38847
38848
38849
38852
" . 38853
38854
38855
38856'
38859
38897
38898
'Pasteurization vessel operates on a constant speed with an in/out :
time duration of 30 minutes.
MINIMUM, MINIMUM
DATE- 2 HOUR pH .24 HOUR pH TEMP:. IN TEMP OUT •
07/03/06 ' 12.23' - 11.97 162 158
07/05/06 12.14 11.09 158 159
07/06/06 12.26 12.08 161 160
: 07/07/06 12.17 12.03 162- .162
07/10/06 12.09 11.88 ; 163 •1"
07/11/06 ,... 12.19 11.98 167 168.
07/17/06 12.14 12:0.1 160 159
67/18/06 12.20 12,11 -163 163
07/19/06 ` 12.09 11.8T 102 137,
07/20/06 12.25 12.17 174 169.
07/31/06 1211, 12.03 160 -163
08/01 /06 12.08 11.92 165 166
08/02/06 12.14- 12.06: 1.64 1'62 "
08/03/06 12.13 ' 12.00 169 168
08/04/06 . , 12.10 12.03 •160 163
08/07/06 12:20 12.12 160 158 .
08/08/06 12.26 12.18 168 161 ;
08/09/06 1203 11.89 . 163 160 '
08/10/06 12.12 1,1.97 160' 165
08/12/66" 12.17 11.86 166 165
08/14/061. 12.20 12.05 -162 167
08/15/06 ' 12.12 12.02 161 158
08/16/66 12.23 12.04 . 161 168
08/17/06 12.11 12.96 164 165,
08/18/06 12.04 11.90' 120 130 _
08/21 /06 12.20 ` 12.06 160 165'
08/22/06 12.21 12.02 162 161
08/23/06 12. 22 12.03 161 166
08/24/06 ' 12.19 12.09 , 169 168
08/25/06 -12.20 - 11.94 159 _ '162
08/28/06 12.18 12.06 . 162'. 163 `
08/29/06 12.24 12.06 163 169
08/30/06 12.18 .12: 06 162 164
08/31 /06 , 12.01 11.96 165 168
' 09/05/06 12.21 11.97 158 159
09/06/06 12.08 11.86 159 158 -
09/07/06 - -12.10 12.01 160 145.
09/08/06 12:20 12.05 " 164 162 .
09/11/06 12.18 12.03 • 170 172
09/12/06 12.18 1106 162 166
09/13/06 .. 12.27 12.03 169 166
V10 �.
q�
41�o�i ��
J
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A' l Medium
Double Strength
10` dilution / 10 ml sample
-
Single Strength
10-'- dilution / 1.0 ml sample
Single Strength
10'2 dilution / 1.0 nil sample
Single Strength.,
10-2dilution / 0.1 ml sample
Date/Time Test Set -Up. A-_.30_.J.)!Datel Time Test Read:
Time Placed in Incubator: �; �d ,o, �r, , Incubator Temp: %
Time Transferred to Water Bath: Water Bath Temp: T
Operator /D-rMedia Lot : _'�lc l 736
Solids 7/D Sample #
INN Fecal Coliform = 10 x 1VIPN-Index / 100 ml .. _
per Guam Total Solids . Largest Volume x % Dry Solids
NOTE: + indicates positive results ; - indicates negative results
FORMULA:
Where:
r
CALCULATION'FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE
% Total Solids = (A - B) x 100
C-B
A = Weight of dried residue + dish (mg)
B = Weight of empty dish (mg)
C = Weight.of wet sample + dish (mg)
Sample # : f --/D -D - 340
Weight of dried residue + dish:
Duplicate weight of dried residue + dish :
Weight of empty dish
Weight of wet sample + dish :
% Total Solids = 02 3, 7 Q Q x l Q D
� 1 ly q. 71 ;=7 q-a e ? /%0
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A-1 Medium
Double Strength
10-' dilution / 10 in1 sample
Single Strength
10-' dilution / 1.0 ml sample
............. �
Single Strength
10 ^ dilution /.1.0 ml sample
Single Strength
10-2 dilution / 0.1 ml sample
Date/Time Test Set -Up: -A r , ;QQ wh , Date" Time Test Read: , 36
Time Placed in Incubator: .30 Incubator Temp: ,3 S.
PC -
Time Transferred to Water Bath: Q Water Bath Temp:'. G
Operator Media Lot #*. Y S� % q 3 6-
%Solids �. Sample # : 2- 9 D -D 6 3 66
MPN Fecal Coliform = 10: x 1v1PN Index / 100 ml
per Gram Total Solids Largest Volume x % Dry Solids _
NOTE: + indicates positive results -: indicates negative results
FORMULA:
Where:
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE
% Total Solids
(A-B)x 100
C-B
A = Weight of dried residue + dish (mg)
B = Weight of empty dish (mg)
C = Weight of wet sample + dish (mg)
.gym. � / //
Weight of dried residue + dish:
Duplicate weight of dried residue:+ dish
Weight of empty dish
Weight of wet sample + dish
/45, 7,3
Total Solids = �'3, �'
rl 67. Z7Z- x M
------------
-33.Yle4—/7)ar
/3 L, 3j--
3a.o917
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A-1 Medium
Double Strength
10-' dilution / 10 ml sample
Single Strength
10_2
dilution / 1.0 ml sample
Single Strength
10" dilution / 1.0 ml sample
Single Strength
10' dilution / 0.1 ml sample
- �' ;3D Date/ Time Test Read:
Date/Time Test Set -Up: A.
Time Placed in Incubator: .3 ; Qp, �+�: Incubator Tem
p':
Time Transferred to Water Ba (p•�Qp.rv.. Water Bath Temp: '�; C
Operator Media Lot
% Solids �' �. /0 Sample.# r
MPN Fecal Coliform = 10 x MPN Index / 100 ml = Q
per Gram Total Solids Largest Volume x % Dry, Solids
NOTE: + indicates positive results ; - indicates negative results
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE
HIM:?Tlil�
% Total Solids
(A-B)x100
C-B
A = Weight of dried residue + dish (mg)
B = Weight of empty dish (mg)
C = Weight of wet sample + dish (mg)
Sampie # :.39-t16 — `j O
Weight of dried residue + dish:
Duplicate weight of dried residue .+ dish
Weight of empty dish
Weight of wet sample + dish
% Total Solids = T 1 7
1666.
.R. ��o6
• �f13
aa, �300
TV 0
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A-1 Medium
Double Strength Single Strength;
10-' dilution / 10 ml sample 10-.1 dilution / 1.0 ml sample
Single Strength Single Strength
10-2 dilution 1.0 ml sample 10-1 dilution / 0.1 nil sample
Date/Time Test Set-U`Ly - - ;36 ,.Date! Time Test Read:
Time Placed in Incubator: °
3 ' ®d g. Ih, Incubator Temp, 34 � C.
Time Transferred to Water Bath: _ ; a0 sr , Water Bath Temp: 7 �—
Operator A&I ,aMedia Lot g . S�o
% Solids F-j . �a �6 Sample #
MPN Fecal Coliform = 10 x MFN index / 100 ml =
per Grant Total Solids Largest Volume x-% Dry Solids
NOTE: + indicates positive results ; indicates negative results
FORMULA:
1" - -
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE
% Total Solids
(A-B)x100
C-B
A = Weight of dried residue + dish (mg)
B = Weight of empty dish (mg)
C = Weight of wet sample + dish (mg)
Sample_#
Weight of dried residue + dish: $Q q S
Duplicate weight of dried residue+ dish:
Weight of empty dish a, Q � I
Weight of wet sample + dish
Total Solids ='3, 6 P6
a64 3-:3—= 43.G%a
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A-1 Medium
Double Strength
10-' dilution / 10 ml sample
Single Strength
10 dilution 1/.1.0 rn! sample
Single Strength
10-' dilution / 1.0 rnl sample
Single Strength
10-' dilution / 0.1 ml sample
Dat:.e/Time Test Set -Up: 6--0 4 4:34404te' Time Test Read:
Time Placed in Incubator: ��; D D A. r� • Incubator Temp:
Tine Transferred to Water Bath: ; dQ ,�_ Water.Bath Temp: G
Operator Media Lot # . 661173 O
Solids-3 . Sample #
WT'NT Fecal Coliform = 10 x lv N, Index / 100 ml =
per Gram Total Solids Largest Volume x % Dry Solids
V0 TE: + indicates positive results ; - indicates negative results
FORMULA:
Where:
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE
% Total Solids = (A - B)x 100
C-B
A = Weight of dried residue + dish (mg)
B = Weight of empty dish (mg)
C ; Weight of wet sample + dish (mg)
Sample # : s5 - / -- Q6 — ,-d Q
Weight of dried residue + dish:
Duplicate weight of dried residue .+ dish:
Weight of empty dish
Weight of wet sample + dish
Total Solids
I,,66 - �.dS � X
aaa9.�s _ 415�a
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A-1 Medium
Double Strength
10"1 dilution / 10 ml sample
Single Strength
10 = dilution / 1.0 m1 sample
Single Strength
10-1 dilution / 1.0 ml s
Single Strength
10-1 dilution / 0.1 ml sample
Dat:e!Time Test Set -Up: - : /d or Date! Time Test Read:
Tune Placed in Incubator: : 3 , n., Incubator Te '
mp:
Tune Transferred to Water Bath: Water Bath Temp:
Dperator Media Lot #,SAP 73d
Yo SolidsSample #
D
NDN Fecal Coliform = 10 x MPN-Index./ 100 nil = Q
per Gram Total Solids Largest Volume x % Dry Solids
90-M: + indicates positive results z -indicates negative results
FORMULA:
Where:
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE
% Total Solids = (A - B) x 100
C'B
A = Weight of dried residue + dish (mg)
B = Weight of empty dish (mg)
C = Weight of wet sample + dish (mg)
Sample#:�p—f
Weight of dried residue + dish:
Duplicate weight of dried. residue .+ dish:
Weight of empty dish
Weight of wet sample +dish :
% Total Solids
r2 4, 4 a 7v
4. 4Z A
a. 0.2
-0 P—. 4 4
d.��3
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A-1 Medium \
Single Strength Single Strength
10'dilution / 1.0 ml sample 10-' dilution / 0'.1 ml sample
Date Time Test Set -Up: I' 3"�� ��: QS Date! Time Test — •
.fir,, F.ead:
Time Placed in Incubator: d
oZ J Incubator Temp:
Time Transferred to Water Bath: 446. r Water'Bath Temp:
Operator Media Lot::
% .Solids �" / . �0 Sample # JI
MPN Fecal Coliform = `10 x WN Index / 100 fnl =
per Ceram Total Solids Largest Volume x % D.ry Solids
NOTE:' + indicates positive results; indicates negative resoles
�• .
Where:
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE
% Total Solids = (A - B) x 100
C-B
A = Weight of dried residue + dish (mg)
B = Weight of empty dish (mg)
C = Weight of wet sample + dish (mg)
Sample # :. 7— 13 0lv
Weight of dried residue + dish:
Duplicate weight of dried residue .+ dish:
Weight of empty dish
Weight of wet sample + dish :
% Total Solids = 9, /v
33. oo?(
a. os� qs
073
3 3,
LLA
6a.6y 7 �
I
FECAL COLIFORM-FOR MUNICIPAL BIOSOLIDS
A-1 Medium
Double Strength
10"' dilution / 10 ml sample
Single Strength
1 0•'-, dilution / 1.0 ml sample
Single Strength
10" dilution i 1.0 ml sample
�o
Single Strength
10-' dilution / 0.1 ml sample
Date, Time Test Set -Up: - -Q '3Q ^ date/ Time Test Read: b
Time Placed in Incubator: �; _�Q �o, A,. , Incubator Temp:.
Time Transferred to Water Bath: °
ODD,,r, ; -Water Bath Temp: ��. S , C
Operator Media Lot
% o Solids !'p�. i sd Sample
MPN Fecal Coliform = l0 x IvTN Index./ 100 ml
per Cram Total Solids Largest Volume x % Dry Solids
NOTE:. + indicates positive results ; - indicates negative results
MM
Where:
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE
% Total Solids = (A - B) x 100
C-B
A = Weight of dried residue + dish (mg)
B = Weight of empty dish (mg)
C = Weight of wet sample + dish (mg)
Sample#:
Weight of dried residue + dish:
Duplicate weight of dried residue .+ dish:
Weight of empty dish
Weight of wet sample + dish :
% Total Solids
a3.3 � JO
�3.3/18
S1.. S"9�,3
3.3118-�..o6�fS�
S/. 59.s3
a1a4.73
�9.530$
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A-1 Medium
Double Strength
10-' dilution / 10 ml sample
Single Strength
10'- dilution / 1.0 ml sample
Single Strength
10-1* dilution / 1.0 ml sample
Single Strength
10-' dilution / 0.1 ml sample
Date/Time Test Set-LTp: ''7- 66 o2'6d , vD'ate! Time Test Read: �- 8'� Q � o?.'3D �,, %
Time PIaced in Incubator: _ dZ 364,A r., > Incubator. Temp:�'-
Tune Transferred to Water Bath: Water Bath Temp:. . Sc
Operator Media Lot#
% Solids TJ • 7" /d Sample #
MPN Fecal Coliform = 1.0 x MPN Index / 100 mI =
per Gram Total Solids Largest Volume x .% Dry Solids
NOTE: + indicates positive results; - indicates negative results
CALCULATION FOR TOTAL SOLIDS IN BIOSOLID9 SAMPLE
'FORMULA:
% Total Solids = '(A' B ) x 100
-C - B
Where:
A = Weight of dried residue + dish (mg)
B Weight of empty dish (mg)
C = Weight of wet sample + dish (mg)
Sample # :
Weight of dried residue +dish:
Duplicate weight of dried residue •+ dish:
Weight of empty. dish
Weight of wet sample + dish 3► %Q .QQ -
Total Solids
01�-� X 0 76 X �a6
3q /Dao—/d7D
"FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A-1 Medium
Double Strength
10"' dilution / 10 ml sample
Single Strength
10 dilution / 1.0 ml sample
Single Strength
10-" dilution / 1.0 ml sample
Single Strength
10-1 dilution / 0.1 nil sample
Date!Time Test Set -Up: /Q - -Q� D •%,,,Date/Time Test Read:
Time Placed in Incubator: Incubator Temp: : 3. Q
Time Transferred to Water Bath:
i►•+ : Water Bath Temp: T
Li 1i
Operator Media Lot 9
%'Solids17 Sample # a'L - , S"
WN Fecal Coliform .. = 10 x MPN Index / 100 ml. = 0
per Gram Total Solids Largest Volunie x %,Dry Solids
NOTE: +indicates positive results ; - indicates negative results .
Where:
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE
% Total Solids = (A - B)x 100
C-B
A = Weight of dried residue + dish (mg)
B = Weight of empty dish (mg)
C = Weight of wet sample + dish (mg)
Sample # :1 , %4 ` D t/O .�®
Weight of dried residue + dish:
Duplicate weight of dried residue -+ dish:
Weight of empty dish
Weight of wet sample + dish
��. 1 /C
/ol. V 4 .
2 L ��
Y
36. 6)R
% Total Solids
//I//,- x AM
36,
I L�4,3. U,
33. % 6 6
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A-1 Medium
-Double Strength
10' dilution / 10 ml sample
Single Strength
10' dilution ! 1.0 ml sample
Single Strength
I07",dilution / 1.0 ml sample
- Single Strength
10-2 dilution 7 0.1 ml sample
Date/Time Test Set -Up: P Ob Date/ Time Test Read:
Time PIaced in Incubator: - -3 Op.. , Incubator Temp: 3 5; L0 C_
Time Transferred to Water Bath: Water Bath Temp:
Operator /�J� Media Lot # �� �f
�j % 4 97
% Solids 3 8.6 /0 Sample # a " �o -' EQ a
WN Fecal Coliform = 10 x MPi\? Index i' 100 ml =
per Gram Total Solids Largest Volume x % Dry Solids
NOTE: + indicates positive results ; - indicates negative results
i
FORMULA:
Where:
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE
% Total Solids = (A - B) x 100
C-B
A = Weight of dried residue + dish (mg)
B = Weight of empty dish (mg)
C = Weight of wet sample + dish (mg)
Weight of dried residue .+ dish:
Duplicate weight of dried residue -+ dish:
Weight of empty dish
Weight of wet sample + dish : /a /, C2 7
% Total Solids = 3 ! , a Z
76
�3
�0��0
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A-1 Medium
Double Strength
10' dilution / 10 ml sample
Single Strength
l 0-' dilution / 1.0 nit sample
Single Strength
10-1' dilution / 1.0 ml sample
Single Strength
10-' dilution / 0.1 ml sample
Date/Time Test Set -Up: -- -� a,'Q�D,r�te!-Time Test Read:
Time Placed in Incubator: - 30 Incubator Temp:°c-
Time Transferred to Water Bath: `I/� °
D .n� Water Bath Temp: Tr
Operator Media Lot # 44)31
% Solids g� Sample
MPN Fecal Coliform = 10 x MPN Index / 100 ml =
per Grans Total Solids Largest Volume x % Dry Solids
NOTE: + indicates positive results ; . - ihdicates negative results
FORMULA:
Where:
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE
% Total Solids
(A-B)xl00
C-B
A = Weight of dried residue + dish (mg)
B = Weight of empty dish (mg) -
C = Weight of wet sample + dish (mg)
Sample # : A_ J* -d (o - pD
Weight of dried residue + dish: o7 Ll. a 3 /D
Duplicate weight of dried residue + dish
Weight of empty dish : C/
Weight of wet sample + dish
% Total Solids3Y
3
RECEIVED IDEN R1D\NQ
AOUIFFR'PRQTFr
FEB 21 'tub/
F WATF
• OHO !QpG r Michael F. Easley, Governor
y William G. Ross Jr., Secretary
r✓ North Carolina Department of Environment and Natural Resources
=1
Alan W. Klimek, P.E.,.Director
—_ Division-of_W.ater Quality
- _ August 26, 2005
- Mr. Ricky Ingram, Public Utility Director
_Post Office Box 219
Cheraw, South Carolina 29520 --- -
Subject: Permit No. WQ0014248
_ Town of Cheraw, South Carolina
_- Town of Cheraw Residuals Distribution Program
Distribution of Class A Wastewater Residuals
- Central Office — Out of State Operation
Dear Mr. Ingram:
- In accordance with your application received on July 30, 2003 and additional information received
on February 25, 2004, we are forwarding herewith Permit No. WQ0014248, dated August 26, ,2005, to the
Town of Cheraw for the continued operation of a wastewater residuals facility for the distribution of Class
A residuals.
_ = This permit shall be effective from the date of issuance until July 31, 2010, shall void Permit No.
WQ0014248 issued August 15,,199,7; andshall be subject to the conditions and limitations as specified
therein. Please pay particular attention to the monitoring and reporting requirements contained in this
permit. Failure to establish an adequate system for collecting and maintaining the required operational
- information will.result in future compliance problems.
_ -- If any parts, requirements, or limitations contained in this permit are unacceptable, you have the
_ - right to request an adjudicatory hearing upon written request within thirty (30) days following receipt of
_ this permit. This request must be in the form of a written petition; conforming to Chapter, 150B of North
Carolina General Statutes, and filed with the'Office of Administrative Hearings, 6714 Mail Service Center,
Raleigh, NC 27699-6714. Unless such demands are made this permit shall be final and binding.
If you need additional information concerning this matter, ple e contact Duane Leith at (919)
715-6186 or email duane.leith@ncmail.net.
Sincer y.
V6Alan W. Klimek, P.E.
cc: lNCDWQ Regional Offices,_ __ater_QuaTity Secti i
Technical Assistance and Certification Unit
Water Quality Central Files
NDPU Files
- - NDPU Residuals Program Coordinator_—_
Aquifer Protection Section 1636 Mail Service Center Raleigh
Internet: http://h2o.enr.state.nc.us 2728 Capital Boulevard Raleigh
An Equal Opportunity/Affirmative Action Employer— 50% Recycled/10% Pj
,C Ciha
C) o 1
Tina
lly .
0
NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
RALEIGH
PERMIT FOR THE DISTRIBUTION OF CLASS A RESIDUALS
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as
amended, and other applicable Laws, Rules, and Regulations _
PERMISSION IS HEREBY GRANTED TO
Town of Cheraw
Chesterfield County, South Carolina
FOR THE
continued operation of a wastewater residuals facility for the distribution of Class A residuals consisting of --
the distribution of 1,800 dry tons per year of residuals from the sources listed in Condition 112, with no
discharge of wastes to the surface waters, pursuant to the application received on July 30, 2003 and in
conformity with the project plan, specifications, and other supporting data subsequently filed and approved
by the Department of Environment and Natural Resources and considered a part of this permit. _
This permit shall be effective from the date of issuance until July 26, 2010, shall -void Permit No. .
WQ0014248 issued August 15, 1997, and shall be subject to the following specified conditions and
limitations:
L. PERFORMANCE STANDARDS = _
1. The distribution -of Class A residuals program shall be effectively maintained and operated as a
non -discharge system to prevent the discharge of any wastes -resulting from the operation of
this program.
2. This permit shall become voidable in the event of^failure of the residuals program to
adequately protect the assigned water quality standards of the surface waters and
groundwaters.
3. The issuance of this permit shall not relieve the Permittee of the responsibility for damages to -
surface or groundwaters resulting from the operation of this program.
4. In the event that the residuals.program is-rio"t operated satisfactorily, including the creation of
nuisance conditions, the Permittee shall take any immediate corrective actions as may be
required by the Division of Waterquality,_(Division).
1
EIS
5. Diversion or. bypassing of the untreated residuals or leachate from the residual treatment
fa"litiesis prohibited.
6. All leachate must be reused as a wetting agent for the processing of residuals or routed to the
head of the treatment plant.
7. When wastewater residuals are sold or given away, one of the Class A pathogen requirements
in 40 CFR Part 503.32(a) and one of vector attraction reduction requirements in 40 CFR Part
503.33 must be met. Additionally, an evaluation must be performed which demonstrates the
residuals ability to comply with. this requirement. Upon request, a copy of this evaluation
must be submitted including all test results and calculations.
OPERATION AND MAINTENANCE REQUIREMENTS
1. The residuals treatment facilities shall be properly maintained and operated at all times.
2. No residuals other than.the following are hereby approved for distribution in accordance with
this permit:
Permit Volume
Source County Number (Dry Tons/Year)
Town of Cheraw Chesterfield, SC SCO020249 1,800
3. All residuals shall be adequately stored to prevent leachate runoff until treated., The finished
product may be placed on a concrete pad, placed under shelter or covered until such time as it
is distributed to the buyer. If an alternate storage site is to be used, approval must be obtained
from the Division.
4. No other residuals other than those specified under Condition H 2 above may be distributed.
The Permittee shall request and obtain a permit, amendment from the Division for each
additional residual source prior to acceptance of that residual.
5. For a Class A residual to be sold or given'away in bags or other container for application to the
land, the following must be satisfied:
The Ceiling Concentrations (Dry Weight Basis) and the Pollutant Monthly Average
Concentrations (Dry Weight Basis) must be maintained:
Ceiling Monthly Average
Concentrations Concentrations
Parameters mg/kg mg/kg
Arsenic
75
41
Cadmium
85
39
Copper
4,300
1,500
Lead
840
300
Mercury
57
17
Molybdenum
75
----
Nickel
420
420
Selenium
100
100
Zinc
7,500
2,800
2
6. Upon classification of the facility by the Water Pollution Control System Operators
Certification Commission (WPCSOCC), the Permittee shall employ a certified residuals
operator to be in responsible charge (ORC) of the residuals program. The operator must hold
a certificate of the type classification assigned to the residuals program by the WPCSOCC.
The Permittee must also employ a certified back-up operator of the appropriate type to comply
with the conditions of 15A NCAC 8G .0202.
7. Adequate provisions shall be taken to prevent wind erosion and surface runoff from conveying
pollutants from -the residuals treatment area onto the adjacent.property or into any surface
waters.
A label shall be affixed to the bag or other container in which residuals that are sold or given
away for application to the land, or an information sheet shall be provided to the person who
receives the residuals sold or given away in an other container for application to the,land. The
label or information sheet shall contain the following information:
a. The name and address of the person who prepared the residuals that is sold or given
away in a bag or other container for application to the land.
b. A statement that application of the residuals to the land is prohibited except in
accordance with the instructions on the label or information sheet.
c. A statement which identifies that this material shall be prevented from entering any
public or private water supply source (including wells) and any stream, lake, or river.
d. Residuals shall not be applied to any site that is flooded, frozen or snow-covered.
e Adequate procedures shall be provided to prevent surface runoff from carrying any
disposed or stored residuals into any surface waters.
III. MONITORING AND REPORTING REQUIREMENTS
1. Any monitoring (including groundwater, surface water, residuals, soil, or plant tissue analyses)
deemed necessary by the Division to insure protection of the environment will be established
and an acceptable sampling and reporting schedule shall be followed.
2. Proper records shall be maintained by the Permittee tracking all residual activities. These
records shall include, but are not necessarily limited to the following information:
a. source, volume and analysis of each residuals
b. name of residuals' recipient, volume received, and intended use
3
3. A residual analysis shall be conducted annually from the date of permit issuance by the
Permittee. The results of all analysis shall be maintained on file by the Permittee for a
minimum of five years. The residuals analysis shall include the following parameters:
Arsenic
Cadmium.
Copper
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Aluminum
Ammonia -Nitrogen
Calcium ,
Magnesium
Nitrate -Nitrite Nitrogen
% Total Solids_
pH
Phosphorus
Potassium
Sodium
TKN
Plant Available Nitrogen (by calculation)
4. The residuals generated by each residuals source -generating facility listed in condition 11.2.
above shall be analyzed to demonstrate that they are non -hazardous under the Resource
Conservation and Recovery Act (RCRA). A corrosivity, ignitability, and reactivity analysis as:
well as a Toxicity Characteristics Leaching Procedure (TCLP) analysis shall be conducted on
the residuals generated by each residual's source -generating facility listed in condition 11.2.
above. The analyses shall be perfonned annually, and the results shall be maintained on file
by. the Permittee for a minimum of five years. If the residuals generated by a. particular
residuals source -generating facility are land applied at a frequency less than annually, the
Analyses shall be required for each residuals land application event. The TCLP analysis shall
'include the following parameters (please note the regulatory level in mg/L in parentheses):
Arsenic (5.0)
Barium (100.0)
Benzene (0.5)
Cadmium (1.0)
Carbon tetrachloride (0.5)
Chlordane (0.03)
Chlorobenzene (100.0)
Chloroform (6.0)
Chromium (5.0)
o-Cresol (200.0)
m-Cresol (200.0)
p-Cresol (200.0)
Cresol (200.0)
2;4-D (10.0)
1,4-Dichlorobenzene (7.5)
1,2-Dichloroethane (0.5)
1;1-Dichloroethylene (0.7)
2,4-Dinitrotoluene (0.13)
Endrin (0:02)
Heptachlor (and its hydroxide) (0.008)
,
Hexachlorobenzene ,(0.13)
Hexachloro-1,3-butadiene (0.5)
Hexachloroethane (3.0)
Lead (5.0)
Lindane (0.4)
Mercury (0.2)
Methoxychlor (10.0)
Methyl ethyl ketone (200.0)
Nitrobenzene (2.0)
Pentachlorophenol (100.0)
Pyridine (5.0)
Selenium (1.0)
Silver (5.0)
Tetrachloroethylene (0.7)
Toxaphene (0.5)
Trichloroethylene (0.5)
2,4,5-Trichlorophenol (400.0)
2,4,6-Trichlorophenol (2.0)
2,4,5-TP (Silvex) (1.0)
Vinyl chloride (0.2)
After the residuals have been monitored annually for two years, the Permittee may submit a
request to the Division for a permit modification to reduce the frequency of the TCLP analysis.
In no case, however, shall the frequency of TCLP monitoring be ,less than once per permit
cycle when residuals are sold or given away.
4
5. All residuals included in this permit must be monitored annually, from the date of permit
issuance, for compliance with condition I.7. of this permit. Data to verify stabilization of the
residuals must be maintained by the Pennittee. The required data is specific to the
stabilization process utilized, but should be sufficient to clearly demonstrate compliance with
the Class A pathogen requirements in 40 CFR Part 503.32(a) and the vector attraction
reduction requirements in 40 CFR Part 503.33. In addition, the EPA certification statements
concerning compliance with pathogen requirements, vector attraction reduction requirements
and management practices must be completed annually by the proper authority or authorities if
more than one is involved, either the person who generates the residuals or the person who
prepares the residuals to be sold or given away.
6. Three copies of all required monitoring and reporting requirements as specified in conditions
III 1, III 2, 111 3, I1I 4, and 1115 shall be submitted annually on or before March 1 of the
following year to the following address.
Division of Water Quality
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
7. Noncompliance Notification:
The Permittee shall report by telephone to the appropriate DWQ Regional Office as soon as
possible, but in no case more than 24 hours or on the next working day following the
occurrence or first knowledge of the occurrence of any of the following:
a. Any occurrence with the distribution program which results in the land application of
significant amounts of wastes which are abnormal in quantity or characteristic.
b. Any failure of the distribution program resulting in a release of material to receiving
waters.
c. Any time that self -monitoring information indicates that the facility has gone out of
'compliance with the conditions and limitations of this permit or the parameters on which
the system was designed.
d. Any process unit failure, due to known or unknown reasons, that render the facility
incapable of adequate residual treatment.
e. Any spillage or discharge from a vehicle or piping system during transportation of
residuals.
Persons reporting- such occurrences by telephone shall also file a written report in letter form
within five (5) days following first knowledge of the occurrence. This report must outline the
actions taken or proposed to be taken to ensure that the problem does not recur.
IV. GROUNDWATER REQUIREMENTS
Any groundwater quality monitoring, as deemed necessary by the'Division, shall be provided.
5
V. INSPECTIONS
L . The Pern- ittee or his designee shall inspect the residuals storage, transport, and treatment
facilities to prevent malfunctions and deterioration, operator errors and discharges which may
cause or lead to the release of wastes to the environment, a threat to human health, or a
nuisance. The Permittee shall maintain an inspection log or summary including at least the
date and time of inspection, observations made, and any maintenance, repairs, or corrective
actions taken by the Permittee. This log of inspections shall be maintained by the Permittee
for a period of five years from the date of,the inspection and shall be. made available to the
Division or other permitting authority, upon request.
2. Any duly authorized officer, employee, or -representative of the Division may, upon
presentation of credentials, enter and inspect any property, premises or place on or related to
the treatment site or facility at any reasonable time for the purpose of determining compliance
with this permit; may inspect or copy any. records that must be kept under- the terms and
conditions of this permit; and may obtain samples of groundwater, surface water, or leachate.
VI. GENERAL CONDITIONS
This permit shall become, voidable unless. the distribution activities are carried out in
accordance with the conditions of this permit, the supporting materials, and in the manner
approved by this Division. .
2. This permit is effective only with respect to the nature and volume of residuals described in
the application and other supporting data.
3. This permit is not automatically transferable, In the event that there is a desire for the facilities
to change ownership or a name change of the Permittee, a formal permit request must be
submitted to the Division accompanied by an application fee, documentation from the parties
involved, and other supporting materials as may be appropriate. The approval of this request
will be considered on its merits and may or may not be approved.
4. Failure to abide by the conditions and limitations contained in this permit may subject the
Permittee to an enforcement action by the Division in -accordance with North Carolina General
Statute 143-215.6A to 143-215.6C.
5. The annual administering and compliance fee must be paid by the Permittee within thirty (30)-
days after being billed by :the Division. , Failure to pay the fee accordingly may cause the
Division to initiate action to revoke this permit as specified by 15 NCAC 2H .0205 (c)(4).
6. The issuance of this permit does not exempt the Permittee from complying with any and all,
statutes, rules, regulations, or ordinances which may be imposed by other government
agencies (local, state, and federal) which have jurisdiction, including but not limited to
applicable river buffer rules in 15A NCAC 2B.0200, erosion and sedimentation control
requirements in 15A NCAC Chapter 4 and under the Division's General Permit NCGO10000,
and any requirements pertaining to wetlands under 15A NCAC 2B .0200 and 2H .0500. , .
6
7. The Permittee, at least six (6) months prior to the expiration of this permit, shall request its
extension. Upon receipt of the request, the Commission will review the adequacy of the
facilities described therein, and if warranted, will extend the permit for such period of time and
under such conditions and limitations as it may deem appropriate.
8. This permit may be modified, or revoked and reissued to incorporate any conditions,
limitations and monitoring requirements the Division deems necessary in order to adequately
protect the environment and public health.
Permit issued this the 26t"day of August, 2005.
NORZCLINA ENVIRONMENTAL MANAGEMENT COMMISSION
✓LAlan W. Klimek, P.E., Director
Division of Water Quality
By Authority of the Environmental Management Commission
Permit Number WQ0014248.
7
NON -DISCHARGE REGIONAL WATER.QUALITY "
STAFF REPORT AND RECOMMENDATIONS
Da` 'ie I78fiO4t County: Unknown,,
To: on Dischar a Permittin "Unit
m
g Perittee: Town of Cheraw. SC
NDPU Reviewer: Duane Leith . Application No:: W00014248
Regional Login Nos W00014248-Residuals Distribution
GENERAL INFORMATION
1. -This application IS (check all that apply): ❑ New Z ;Renewal
El MiriorMWifkation'❑ Major Modification
❑ Surface Irrigation [:]-Reuse ❑ Recycle ❑ High Rate Infiltration ❑,EvaporatioWMfiltration Lagoon
❑ Land Application of Residuals , ❑ Attachment B included as appropriate Z 503 regulated ❑ 503 exempt
Z Distribution of Residuals ❑ Surface Disposal
,2.. Was a site visit conducted in order to prepare -this report? ❑ Yes or. [E No.
a. Date of site visit:
b. Person contacted'and contact information:. ;
c. Site visit conducted by;
d. Inspection Report Attached: ❑ Yes or Z,N6.
3. Is the following information entered into the BIMS°record for this application correct? '
Yes or No. " If h6;. please complete the following 'or indicate that it is correct on the current
application.
For Treatment Facilities:
a, Location: Cheraw, .SC in Chesterfield'Co
b. Driving -Directions:
a USGS Quadrangle Map name and number: Wallace'
d. Latitude: 34-41-24 Longitude: 79-52=10-
e. Regulated Activities % Type of Wastes (e.g., subdivision, food processing, municipal wastewater):
Municipal
For Disposal Sites:
into the document for each site, or attach additional- pages for each site)
a. Location(s):
b. Driving Direction's:
c. USGS, Quadrangle, Map name and number:
d. Latitude: Longitude:
FORM; NDSRR 03/02 ' 1
v
NON -DISCHARGE REGIONAL .WATER ,QUALITY
STAFF REPORT AND RECOMMENDATIONS
NEWAND MAJOR MODIFICATIONAPPLICATIONS (this_ section not needed for renewals or
minor modirications, skin to next section)
DESCRIPTION OF WASTES) AND FACILITIES
1. Please attach completed rating sheet. Facility Classification:
2. Are the new treatment facilities -adequate for the type of waste and disposal system?
❑ Yes ❑ No ❑ N/A. If no, please explain:
3.. Are the new site conditions (soils, topography, etc) consistent with what was reported by the soil
scientist and/or Professional Engineer? ❑ Yes ❑ -No ❑ N/A. If no, please explain:
4. Is the proposed residuals management plan for the adequate and/or acceptable to the Division.
❑ Yes ❑ No ❑ N/A. If no, please explain:
5. Are the proposed application rates for new sites (hydraulic or nutrient) acceptable?
❑ Yes ❑ No ❑ N/A. If no, please explain:
6: Are the new treatment facilities or any new disposal sites located in a 109-year floodplain?
❑ Yes. ❑ No ❑ N/A. If yes, please attach a map showing areas of 100-year floodplain and please
explain and recommend any mitigative measures/special conditions in Part IV:
7. Are there any buffer conflicts (new treatment facilities or new disposal sites)? ❑ Yes or ❑ No: If_ -
yes, please attach a map showing conflict areas or attach any new maps, you have received from the
applicant to be incorporated into the permit:
FORM: NDSRR 03/02 2
NON -DISCHARGE REGIONAL WATER QUALITY
STAFF REPORT AND RECOMMENDATIONS
RENEWAL AND MODIFICATIONAPPLICATIONS (use previous section for new or maior
modification systems)
DESCRIPTION OF WASTE(S) AND FACILITIES
1. Are there an appropriately certified ORCs for the facilities? ❑ .Yes or ❑ No.
Operator in Charge: Certificate #:
Back- Operator in Charge: Certificate #:
2. Is the design, maintenance and operation (e.g. adequate aeration, sludge wasting, sludge storage,
effluent storage, etc) of the treatment facilities, adequate for the -type of waste and disposal system?
® Yes or ❑ No. If no, please explain: Appears to be so.
3. Are the site conditions (soils, topography, etc) maintained appropriately and adequately assimilating
thewaste? ❑ Yes or ❑ No: If no, please explain:
4. Is the residuals management plan for the facility adequate and/or acceptable to the Division?
❑ Yes or ❑ No. If no, please explain:
5. Are the existing application rates (hydraulic or nutrient) still acceptable? ❑ Yes or ❑ No. If no,
please explain:
6. Are there any buffer conflicts (treatment facilities or disposal sites)? ❑ Yes or ❑ No. If yes, please
attach a map showing conflict areas or -attach any new maps you have received from the applicant to
be incorporated into the permit:
7. Is the type and/or volume of waste(s) as written in the existing permit correct? ❑ Yes. or ❑ No. If
no, please explain:. _
8. Is the description of the facilities as written in the existing permit correct? ❑ Yes or ❑ No. If no,
please explain:
9. Has a review of all self monitoring data been conducted? ❑ Yes or ❑ No. Please summarize any
findings resulting from this review: ,
10. Check all that apply:. ❑ No compliance. issues; ❑ Notice(s) of viol
ation.within the last permit cycle;
❑ Current enforcement action(s) ❑ Currently under SOC; El Currently under JOC; ❑ Currently.
under moratorium. If any items, checked, please explain and attach any documents that may help
clarify answer/comments (such as NOV, NOD etc): ,
11. Have all compliance dates/conditions in the existing permit, SOC, JOC, etc. been complied with?
❑ Yes or ❑ No.. If no, please explain:
12. Are there any issues related to compliance/enforcement that should be resolved before issuing this
permit? ❑ Yes or Z No. If yes, please explain:
FORM: NDSRR 03/02 3
NON -DISCHARGE REGIONAL WATER QUALITY
STAFF REPORT AND RECOMMENDATIONS
E VAL UA TION AND RECOMMENDATIONS
1. Provide any additional narrative regarding your review of the application.:
2. List any items that you would like NDPU to obtain through an additional information request. Make
sure that you provide a reason for each item:
Item •
Reason
The sample product label advises users to contact
the Clemson Extension Service and the Soil
Conversation Service, that appears to be in SC. I
will let Nondischarge Permitting decide whether
more local contact information should be provided.
3. List specific Permit conditions that you recommend to be removed from the permit when issued.
Make sure that you provide a reason for each condition:
Condition Reason
4. List specific special conditions or compliance schedules that you recommend to be included in the
permit when issued. Make sure that you provide a reason for each special condition:
Condition Reason
5. Recommendation: ❑ Hold, pending receipt and review of additional information by regional office;
❑ Hold, pending review of draft permit by regional office; Z Issue; ❑ Deny. If deny, please state
reasons:. Upon satisfactory review by Nondischarge Permitting. the WO RRO has no obiection to the
issuance of the permit.
6. Signature of report preparers
FORM: NDSRR 03/02 4
NON -DISCHARGE REGIONAL WATER -QUALITY
STAFF REPORT AND 'nlECOMM NDATIONS'
Signature of WAS re/lonal supervisor:
Date: / M142
ADDITIONAL REGIONAL STAFF REVIEW ITEMS
This request is for the renewal'of'a permit for the Distribution and'Marketing" of Residuals that
oriainate and are produced in Cheraw, SC. The information submitted in the application package
seems to be that information required for review and issuance of a renewed pemiit.
FORM: NDSRR 03/02 5
NON -DISCHARGE APPLICATION REVIEW REQUEST FORM
Dat st 18, 2003
To: ❑
Forrest Westall, ARO-WQS
❑
Paul Rawls, FRO-WQS
Rex Gleason,_MRO-WQS =
�❑
L H
,Ken Schuster, RRO-WQS.,
�^�___ ___.__v__
❑
Jim Mulligan, WaRO-WQS
❑
Rick Shiver, WiRO-WQS
❑
Steve Mauney, WSRO-WQS
From: Duane Leith, Non -Discharge Permitting Unit
Telephone: (919) 733-5083 ext. 370
E-Mail. duane.leith@ncmail.net
A. Permit Number: W00014248
B. Owner: Town of Cheraw (South Carolina)
❑ Debra Watts, COJS
2 rn- ,
Copies Sent to CO,-GWS
Copies Sent to RO-WQS: 1
❑ Distribute 0 Copies to RO-GWS
Fax: (919) 715-6048
C. Facility/Operation: Town of Cheraw Residuals Distribution Program
❑
Proposed ®, Existing
❑ Facility :
® Operation
D. Application:
1. Permit Type: ❑
CS (O&M) ❑ Surface Irrigation ❑ Reuse.
❑ H-R Infiltration
❑
Recycle ❑ I/E Lagoon
❑ GW Remediation (ND)
For Residuals:
❑ Land App.
® D&M
❑ Surface Disposal
® 503
❑ 503 Exempt
❑ Animal
2. Project Type: ❑ New ❑ Major Mod. ❑ Minor Mod. ® Renewal ❑ Renewal w/ Mod.
E. Comments/Other Information: ❑ I would like to accompany you on a site visit.
This is a new application. An earlier application was returned due to addinfo not being received.
Attached, you will find all information submitted in support of the above -referenced application for your
review, comment, and/or action. Within 30 calendar days, please take the following actions:
For RO-WQS:
® Return a Completed Form NDSRR. ❑ Attach Attachment B for Certification by the NDPU.
❑ Issue an Attachment B Certification from the RO*.
* Remember that you will be responsible for coordinating site visits, reviews, as well as additional
information requests with other RO-WQS and RO-GWS representatives in order to prepare a complete
Attachment B for certification. Refer to the RPP SOP for additional detail.
For CO-GWS:
❑ Return a Memorandum with Permit Condition Recommendations.
When you receive this request form, please write your name and dates in the spaces below, make a copy
of this sheet, and return it
to the appropriate Non- ischarge Permitting Unit contact person listed above.
RO-WQS Reviewer: Date: 49
CO-GWS Reviewer:
Date:
FORM: NDARR 09/02 Page 1 of 1
Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Alan W. Klimek, P.E., Director
Division of Water Quality
August 5, 2003
Ricky Ingram
Public Utility Director
Town of Cheraw
PO Box 219
Cheraw, SC 29520
Subject: Acknowledgement of Application No. WQ0014248
Town of Cheraw
Distribution of Residual Solids
Wake County
Dear Mr. Ingram:
The Non -Discharge Permitting Unit of the Division of Water Quality (Division) acknowledges receipt of
your permit application and supporting materials on July 30, 2003. This application package has been
assigned the number listed above and will be reviewed by Duane Leith.
The reviewer will perform a detailed review and contact you with a request for additional information if
necessary. To ensure the maximum efficiency in processing permit applications, the Division requests
your assistance in providing a timely and complete response to any additional information requests.
Please note at this time processing permit applications can take as long as 60 - 90 days after receipt of a
complete application.
If you have any questions, please contact Duane Leith at 919-733-5083, extension 370, or via e-mail at
duane.leith@ncmail.net. If the reviewer is unavailable, you may leave a message, and they will respond
promptly.
PLEASE REFER TO THE ABOVE APPLICATION NUMBER IN CORRESPONDENCE AND WHEN
MAKING INQUIRIES ON THIS PROJECT. To check the status of this permit application, go to
http://h2o.onr.state.nc.us/bims/Reports/reportsPermits.htmi and check pending permits for the Non -
Discharge program in the. pertinent region. Projects are listed (as facility) in alphabetical order.
Sincerely,
Kim H. Colson, P.E.
Supervisor
cc:. Raleigh=Regional=Gffice Water Q.uality�Section-
Permit Application File WQ0014248
Non -Discharge Permitting Unit
1617 Mail Service Center, Raleigh, NC 27699-1617
DENR Customer Service Center
An Equal Opportunity Action Employer
Internet http://h2o.enr.state.nc.us/ndpu. NCDENR
Telephone •(919) 733-5083 Fax (919) 715-6048
Telephone 1 800 623-7748
50% recycled/10% post -consumer paper
Permit Number WQ0014248
Program Category
Non -discharge
Permit Type
Distribution of Residual Solids (503)
Primary Reviewer
duane.leith
Permitted Flow
Facility Name
Town of Cheraw Residuals Distribution Program
Location Address
Post Office Box 219
Cheraw
Owner
SC 29520
08/05/03
Permit Tracking Slip
Status Project Type
In review Renewal
Version Permit Classification
Individual
Permit Contact Affiliation
Major/Minor Region
Minor Raleigh
County
Wake
Facility Contact Affiliation
Owner Name Owner Type
Town of Cheraw Government - Municipal
Owner Affiliation
Ricky Ingram
Post Office Box 219'
Cheraw, SC 29520
Dates/Events
Scheduled
Orig Issue App Received Draft Initiated Issuance Public, Notice Issue Effective Expiration
08/15/97 07/30/03
Regulated Activities Requested/Received Events
Wastewater treatment and disposal RO staff report received
RO staff report requested
Additional information requested
Additional information received
Groundwater -comments -requested ®V)%�
r Grrouadwatemrnents-received ���
Outfall NULL
,,(/Waterbody Name Stream Index
Number Current Class // Subbas-inn
A/4 / e s 7zf 5r i't Ste./co.•: �%f��l cg J� o.�/ Su�iN'! � e J'�s� �/,'c%sj7`/t�ti. �..A J� �•-�1
r
I
t,.
Department of Environment, Health and Natural Resources
Division of Environmental Management.
Non-Diisu'llaige Permit Application Form
(THIS FORM MAY BE PHOTOCOPIED FOR USE AS AN ORIGINAL)
DISTRIBUTION OF RESIDUAL SOLIDS
This application is intended for facilities which are to be regulated under 40 CFR Part 503
I. GENERAL INFORMATION:
1. Applicant's name (please specify the name of the municipality, corporation, individual, etc.): -
Town of Cheraw
2. Print owners or signing official's name and title (the person who is legally responsible for the facility and its compliance):
Ricky Ingram — Public Utility Director
3. MailinQ address: P.O. Box 219
City: Cheraw
State: SC
Zip: 29520
Telephone Dumber: ( 843 ) 537-8440
4. Application Date: 07/23/03 ,
5. Fee Submitted: S 400.00 [Tbe permit processing fee should be as specified in 15A NCAC 2H .0205(c)(5).]
6. Specify bow these residuals will be distributed: sold or giver. away in bags or other containers; lawn (bulk);
home garden (bulk); X other; Given away in bulk quantities for pasture, land
reclamation, forestry, etc.
7 If the alternative for residual disposal consists of "surface disposal" as dei:ned under 40 CFR Part 503, please complete the
application titled "SURFACE DISPOSAL OF RESIDUAL SOLIDS. Please identify if there is any storage of residuals in
a surface impoundment or disposal th.ru landfillins. Explain:
8. Is the residual process facility also the generator? X Yes; No
9. Latitude: 3404112411 Longitude: 79052' 10" of rCSidulp:oc:caa iauiiity
10. Specif; whether the process facility is owned by: federal; private; state; X local sovernment;
11. County where facility is located: Chesterfield
II. PERMIT INFORMATION:
I. Application No. (will be completed by DEM.):
2. Specify whether project is: new; X renewal"; modification
For renewals, complete all sections included in the application. Engineering Signature and Seal not required. for
renewals or if there is not any construction involved with the subject project.
3. If this application is being submitted as a result of a renewal or modification to an existing permit, list the existing permit
number WQ0014248 and its issue date August 15, 1997
FORM: DRS 06/94
Page. 1 of 8
III. FACILITY INFORMATION (attach additional pages for additional sources of residuals):
1. Name r'f fa__': ; he:e residuals a.-e generated or prepamed: Town of Cheraw WWTp
2. Facility permit number: SCO020249 ; facility permit bolder: _ Town of Cheraw
3. Specify whether facility in Section IE.1 is owned by: federal; private; state; _X local government;
4. Specify facility design flow
Type of residual storage:
4.0 mgd; facility average daily flow: 1.978 mgd;
Concrete pad with shelter
Volume of residual storage: 50,000 cubic feet
Length of residuals storage at facility: 120 days (the Division requires a minimum 30 days storage in units that
are separate from treatment system, i.e. not in clarifiers, aeration basins, etc.);
Estimated volume of residuals: 1800 (dry tons/yr.); residual plus additives
5. If the residual process facility is not the same as the generator, please specify delivery frequency and quantity of residual to
be processed: N/A
6. Facility contact (person familiar with residuals preparation): Ricky Ingram
7. Facility contact's telephone number: (
843
537-8440
S. Location of treatment fatgity:
South Carolina
State; - Chesterfield County
9. Mailing address: P.O.
Box 219 Cheraw SC
29520
P
10. Specify the source of the residuals: X treatment of domestic wastewater, X treatment of industrial wastewater;
other (explain):
Attach an explanation of either the treatment process, manufacturing process, or how the waste is generated. Provide full
and complete details of the entire process.
11. Does the facility which generates the residuals have an approved pretreatment program? X Yes; No.
This includes facilities wbicb are classified as -a "Class I" facility (any publicly owned treatment works required, under 40
CFR=03.8, to have an approved pretreatment program or any facility treating domestic sewage that is classified as "Class
I" by the appropriate federal or State authority)
IV. RESIDUALS INFORMATION (attach additional pages for additional sources of residuals):
I. Information for Hazardous Waste (RCRA) Determination. The information requested or, the limitations snecifed belo::
pertain only to those residuals that are generated from a municipal wastewater treatment facility with industrial contribution
or active pretreatment program and from any other treatment facility with wastewater sources that include industrial sources.
a. Are any of the residuals covered by this application listed in 40 CFR 261.31-261.33? Yes: X No. If Yes,
Iist the number(s):
b. Do the residuals exhibit any of the four characteristics defined by 40 CFR 261.21-261.24? Yes; _X No.
Attach laboratory results for the Toxicity Characteristic Leaching Procedure. Analyses, Reactivity, Ignitabdity, and
Corrosivin• for each residual.
FORM: DRS 06/94 Pate 2 of 8
Note: If -the following constituent levels (as determined by the Toxicity Characteristic Leaching'Procedure Analyses) are
exceeded in the residuals ,or if the pH, of _the residual is. not within the range listed below, the residual is by -
definition a Hazardous waste. Chemical analyses must be made to Minimum Detection Levels.
- PENS
REM
.Arsenic 5.0
Barium
100.0
Benzene 0s
Cadmium
1.0
Carbon tetrachloride 0.5
Chlordane
- 0.03
Chlorobenzene 100.0
Chloroform
6.0
Chromium 5.0
o-Cresol
200.0
m-Cresol 200.0
p-Cresol-
200.0
Cresol 200.0 ..
2,4-D
10.0
1,4-Dichlorobenzene 7.5
1,2-Dichloroethane
0.5
- 1,1-Dichloroethylene 0.7
2,4-Dinitrotoluene
0.13
Endrin 0.02
Heptachlor (and its hydroxide)
. 0.008
Hexachlorobenzene 0.13.
Hexachloro-1,3-butadiene
0.5
Hexachloroethane 3.0
Lead
5.0 %
'Lindane 0.4
Mercury
0.2
Methoxychlor 10.0
Methyl ethyl ketone.,.- �'
200.0
Nitrobenzene 2.0
Pentachlorophenol
100.0
Pyridine 5.0
Selenium
1.0
Silver 5.0
Tetrachloroethylene .-
0.7
Toxaphene 0.5
Trcchooroethylene '.
0.5 .
'2,4,5-Trichlorophenol 400.0 -
2,4,6-Trichlorophenol
2.0
2,4,5-TP -(Silvex) - 1.0
Vinyl chloride
0.2
pH (2:1 volJwt.): >2.0 s.u. - <12.5 s.u.
i+
-
NOTE: IF ANY OF THE RESIDUALS MEET
THE DEFINITIONS- OF A
HAZARDOUS WASTE,
AS NOTED, IN EITHER "A" OR "B"-
ABOVE; A. PERMIT CANNOT' BE -ISSUED :FOR
THAT MATERIAL AND, IT SHOULD NOT .BE INCLUDED
AS PART OF THIS
APPLICATION.
2. For each residual, please attach a complete chemical analysis of the material. This analysis must be comprehensive enough
to completely characterize the residual and must be based upon`a review of the process that generates the material. If the
facility that will. generate the -residual is not yet in operation,, the characterization must be based on similar existing
facilities and projection based on the type of facility. The analysis must include a minimum
of the following parameters
and any other known.and suspected contaminants that are tributary to the system.
Arsenic Molybdenum
Calcium
Phosphorus
Cadmium Nickel
Magnesium
Potassium
Chromium Selenium
Nitrate -Nitrite Nitrogen
Sodium
Copper Zinc
% Total Solids
TKN
Lead Aluminum
pH
Mercury Ammonia -Nitrogen
Plant Available Nitrogen
(by calculation)
FORM: DRS 06194
Page 3 of 8
3. Wastewater residuals can not be sold or given away if -the concentration of any pollutant in the residuals exceeds the ceiling
concentrations specified in the table below. Specify the pollutant concentration of these residuals (attach lab analysis):
Pollutant
Pollutant Ceiling Concentration (mg/kg)
Dry Weight Basis
Pollutant.Concentration-(mg/kg)
Dry Weight Basis
Arsenic
75
< 2.73
Cadmium
85
0.549
Chromium
3000
15.2
Copper
4300
1 4
Lead
840
11.9
Mercury
57
0.310
Molybdenum
75
2.19
Nickel
420
Selenium
100
2.73
Zinc
7500
109
4. Provide, all applicable pilot studies and any bench scale tests performed on. each residual source and the results, including
the approximate fertiliier equivalent.
5. Wastewater residuals can't be sold or Eiven away in bags or other containers for application to the land unless one of the
following options is satisfied.
A Specify either A .or B. Please be advised, if the residuals are to be sold or given away in bulk for application to
lawn or home garden then Opdon A is the only option.
A . The pollutant concentration of the residuals must be less than Pollutant Monthly Average Concentrations
listed in the table below.
Pollutant
Monthly Average Concentrations
Dry Weight Basis (mg/ke)
Pollutant Concentration
Dry Weight Basis (m ) .
Arsenic
41
< '2.73
Cadmium
- - 39
< 0,549
Chromium
1200
15.2
Copper
1500
61.4
Lead
300
111. 9
Mercury
17
0.310
Nickel
420
34.2
Selenium
36.
< 2.73
Zinc
2800
109
B . The product of the concentration of each pollutant in the residual and the annual whole residual application
rate for the residual shall not cause the Annual Pollutant Loading Rate to be exceeded.
In order for the Annual «aole Residual Application Rate (AWRAR) to be calculated the Annual Pollutant
Loading Rate (APLR) is divided by the pollutant concentration (PC) times 0.001 (a conversion factor) as
follows:
AWRAR = ARL&
PC * 0.001
FORM: DRS 06/94 Pace 4 of 8
Pollutant
Pollutant
Concentration
Dry Weight Basis
(mJk)
Annual Pollutant
Loading Rates
(APLR)
kg/hectare -
Annual Whole Residual
Application Rate
(AWRAR)
kg/hectare
Arsenic
2.0
Cadmium
1.9
Chromium
150
Copper
75
Lead
15
Mercury
0.85
Nickel
21
Selenium
5.0
..Zinc
140
The AWRAR for -the residual is the lowest AWRAR calculated. This, is the maximum rate at which the
subject residual can be applied (to convert kg/hectare to lbs/acre multiply by 0.8924). Please specify
kg/hectare or lbs/acre:
AWRAR =
V . PATHOGEN AND VECTOR ATTRACTION REDUCTION INFORMATION .(attach additional pages for
additional sources of residuals):
I. In order for the residuals to be Class A, in accordance with the pathogen requirements in 40 CFR 503.32(a), tither Part a or
Part b &rld one of the options in Part c must be completed (pleah submit all lab analysis, test results and calculations):
X a.. A Fecal coliforin density less than 1000 Mosi.. Probable Number per gram of total dry solids, or
b. A Salmonella sp. density less than 3 Most Probable Number per 4 grams of total dry solids.
fig_ c. In addition to Part a or Part b being met. one of the following alternatives must also be completed. Please
specify 1, 2, 3, 4, 5a, 5b, 5c, 5d, 5e, 5f, 5c or 6 below being met:
1. timeltemp rat it an increased residuals temperature should be maintained for a prescribed period of time, in
accordance with the following guidelines. The results (D) shall be the amount of time, in days, that the residuals
shall remain at the given temperature:
Time anti Temr entire nnirieiinPc
Total Solids
Tem rature (t)
Minimum Time
Equation
Notes
No heating of small
> or = 7%
> or = 500 C
> or = 20 minutes
D=131,700,000
particles by warmed
100.14 t
gases or immiscible
liquid.
> or = 7%
> or = 500 C
> or =15 seconds
D = 131, 00,000
Small particles heated by
100.14 t
warmed gases or -
immiscible liquid.
< 7%
> or = 500 C
> or =15 seconds
D=131,700,000
to
100.14 t.
< 30 minutes
< 7%
> or = 500 C
>or = 30 minutes
D = 50,070,000 .
100.14 t
T..
FORM: DRS 06/94 Page-5 of 8
alkaline treatment - the pH of the residuals is raised to greater than 12 for at least 72 hours. During this lime, th,
temperature of the residuals should be greater than 520 C for at least 12 hours. In addition, after the 72 hour
period, the residuals are to be air dried to at least 50% total solids.
3. prior testing for Enteric VirucNiable Helmin h Ova - the residuals are analyzed for the presence of enteric viruses
(Plaque -forming units) [pfu] and viable behninth ova. If the residuals are analyzed before the pathogen reduction
process and found to have densities of enteric virus <1 pfu/4 grams of total solids and viable helminth ova <1/4g
total solids, the residuals are Class A with respect to enteric virus and viable helminth ova until the next
monitoring episode. If the residuals are analyzed before the pathogen reduction process and found to have densities
of enteric virus > or = 1 pfu/4 g total solids or viable helminth ova > or = 1/4 g total solids, and tested again after
processing and found to meet the enteric virus and viable helminth ova levels listed under "4" below, then the
processed residuals will be Class A with respect to enteric viruses and viable helminth ova when the operating
parameters for the pathogen reduction process are monitored and shown to be consistent with the values or ranges
of values documented.
4. no prior testing for Enteric VintsNiable Helminth Ova - if the residuals are not analyzed before pathogen reduction
processing for enteric viruses and viable helminth ova, the density of enteric viruses must be less than 1 pfu/4 g of
total dry solids and the density of viable helminth ova must be less than 1/4 g of�total dry solids, -.or the residuals
must be treated by a "Process to Further Reduce Pathogens" or a"'Process to Further Reduce Pathogens" equivalent
process.
5. The "Processes to Further Reduce Pathogens" (PFRP) are described as follows:
a. Com4sting - using either the within -vessel or static.aerated pile composting methods, the temperature of the
residuals are raised to 550 C or higher for three days. ' Using the windrow composting method, the residuals are
raised to 550 C or higher for fifteen days. During the high temperature period, there will be a minimum of five
turnings of the windrow.
b. Heat Drying - residuals are dried by direct or indirect contact with hot gases to reduce the moisture content of
the residuals to 10% or lower. Either the temperature of the gas in contact with the residuals exceeds 800 C or
the wet bulb temperature of the gas in contact with the residuals, when the residuals leave the dryer, exceeds
800 C.
c. Heat Treatment - liquid residuals are heated to a temperature of 1800 C or higher for thirty minutes.
d. Thermonhilic Aerobic Dices i n - liquid residuals are agitated with air or oxygen to maintain aerobic cond:dons
at residence times of ten days at temperatures of 550 C to 600 C.
e. Beta Rav Irradiation - residuals are irradiated with beta rays from an accelerator at dosages of at least 1.0
megarad at room temperature (ca. 200 Q.
f. Gamma Rav Irradiation - residuals are irradiated with gamma rays from certain isotopes such as 60Co and
137Ce, at dosages of at least 1.0 megarad at room temperature (ca. 200 Q.
g. Pa_tet�izad - the temperature of the residuals is maintained at 700 C or higher for at least thirty minutes.
6. The residuals shall be treated in a process that is equivalent to a "Processes to Further Reduce Pathogens" (PFRP),
as determined by the permitting authority based on evaluations of the recommendations provided by the Pathogen
Equivalency Committee.
2. When residuals are to be sold or given away, one of the following vector attraction reduction requirements (a, b, c, d, e, f,
g, or h) described below must be met.
f Specify the letter of the vector attraction reduction requirement that has been met (submit lab results, test results and
calculations). Any variation of the below must be described in full detail and attached.
a. Aerobic or Anaerobic Digestion - The mass of volatile solids are reduced by at least 38%. Volatile solids reduction is
measured between the residuals, prior to stabilization, and the residuals ready for use or disposal. This criterion should
be readily met by properly designed and operated anaerobic digestors, but not as readily met by aerobic digestors.
Treatment facilities with aerobic digestors may need to meet the vector attraction reduction requirement through 19c or
19d.
FORM: DRS 06194 Page 6 of 8
b. Anaerobic D;a scion - If 38% volatile solids reduction cannot be achieved, vector attraction reduction can be L
r demonstrated by further digesting a portion of the previously digested residuals in a bench scale unit for an additional
40 days at 3U' C to 370 C. If, at the end of the 40 days, the volatile solids are reduced by less than 17%, vector
attraction reduction is achieved.
c. Aerobic Dig •ion - If 38% volatile solids reduction cannot be achieved, vector attraction reduction can be demonstrated
by further digesting'a portion of -the previously digested residuals that have a solids content of 2% or less in a bench
scale unit for an additional 30 days at 200 C. If, at the end of the 30 days, the volatile solids are reduced by less than
15%, vector artaction reduction is achieved.
d. Aerobic Dig ; ion - The specific oxygen uptake rate (SOUR) shall be equal to or less than 1.5 milligrams of oxygen
per hour per gram of total dry solids at 201 C.
e. Aerobic Processes - The temperature of the residuals for at least 14 days shall be greater than 40' C. During this time,
the average temperature shall be greater than 450 C.
f. Alkaline Stabilization - The pH of the residuals is raised to 12 or higher by alkali addition and, without the addition of
more alkali, remains at 12 or higher for 2 hours and then at 11.5 or higher for an additional 22 hours.
g. DCvi g (stabili7ed solids) - The total solids of residuals that do not contain unstabilized solids, and which are generated
in a primary wastewater treatment process, shall be equal to or greater than 75%. Blending with other materials is not
allowed to acLeve the total solids percentage.
h. ing (unstaaJiuLed solids) - The total solids of residuals that contains unstabilized solids, and which are generated in a
primary wastewater treatment process, shall be equal to or greater than 90%. Blending with other materials is not
allowed to acLeve the total solids percentage.
VI. GENERAL INFORMATION:
1. Please provide a brief narrative concerning materials handling, including the following:
�-T
a. How will the materials will be handled and transported from where the residuals were produced to where it will be
Al
b. Where will the residuals be stored until processed?
C. How will leach -ate collection be handled? t'
d. What will be he duration of treatment?
e. Where will the final product be stored?
f. How long will the final product be stored before being distributed?
a. How will the f:nal product be distributed (packaging)?
Plegse attach a marketability statement detailing destinations and approximate amounts of the final product to be
ibu distrted.
3. ,Please provide either a label which shall be affixed to the bagged processed residual or an information sheet which shall be
provided to the person who receives the processed residual. The label or information sheet shall contain, at a minimum, the
following information:
a. The name and :address of the person who prepared the residual that is sold or given away in a bag or other container for
application to the land.
b. A statement ths[ application of the residual to the land is prohibited except in accordance with the instructions on the
label or information sheet.
c. A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered.
d A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored
residuals into any surface waters.
e. Information on ail applicable buffers including a 10 foot buffer between application site and any public or private water
supply source (including wells) and any stream, lake, river, or natural drainage way.
f. The Annual "A --hole Residual Application Rate (AWRAR) for the residual that does not cause any of the annual
pollutant loadLr,, rates to be exceeded (if necessary).
FORM: DRS 06,94 Page 7 of 8
Name and Complete Address of Engineering Firm: Haves, Seav, Mattern & Mattern, Inc,
181 E. Evans Street BTC 105
City: * Florence State: Sc Zip: 29506
Telephone Number: ( 843 ) 669-4491
Professional Engineer's Certification:
I,
attest that this application for
has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge
the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal
package may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have
reviewed this material and have judged it to be consistent with the proposed design.
North Carolina Professional Engineer's Seal, Signature, and Date:
r
Applicant's Certification:
ii
I, Ricky Ingram , attest that this application for
Distribution of Residual Solids
has been reviewed by me Ln_f is accurate and complete to the best of my knowledge. I understand that if all required parts of this
application are not completed a, -id that if all required supporting information and attachments are not included, this application package
will be retuned to kne_as incomplete+
Signature 646 � � Date
THE CONIPLETED APPLICATION PACKAGE, INCLUDING ALL SUPPORTING INFOR, ATI0\ AND
iIATERIALS, SHOULD BE SE\'T TO 'THL FOLLONi'IN° ; ADDRESS:
NORTH CAROLINA DIVISION OF ENVIRONNIENTAL MANAGEMENT
WATER QUALITY SECTION
PERMITS AND ENGINEERING UNIT
POST OFFICE BOX 29535
RALEIGH, NORTH CAROLINA 27626-0535
TELEPHONE NUMBER: (9I9) 733-5083.
FORM: DRS 06194 Pace 8 of 8
Davis & Brown
PO Bog 15038
Quinby, SC 29506
(843) 665-6746 FAX: (843) 629-1444
Certificate of Analysis
Client: CHERAW, TOWN OF South Carolina Certification Number: 21117
P.O.BOX 219 North Carolina Certification Number: 612
CHERAW, SC 29520
Client"#: 168 Receipt Date: 31-Jan-03
Contact: SHERRY TOLSON Report Date: 27-Feb-03
Sample Date: 29-Jan-03
SDG #: SDG-028528 Approved By:
Van Ward
Lab Director
Reporting
Parameter Result Limit Unit Method Flag Date Time Analyst
Silver, Total <0.010 0.01 mg/l EPA 200.7 02/13/03 15:51 DH
Zinc, Total 0.089 0.01 mg/L EPA 200.7 02/10/03 10:21 DH
LSED-064172
1-27-03-300
Acid Digestion (Solids)
YES
EPA 200.2
02/03/03.
16:00
DH
TCLP
PASS
P/F
SW-846
S16
02/10/03
8:13
KK
Percent Moisture
52.1
0.1
Wt%
SW846 3540
02/11/03
16:50
LM
Aluminum, Total
9900
0.526
mg/kg
SW846 6010A
D
02/20/03
15:42
DH
Arsenic, Total
<2.73
2.73
mg/kg
SW846 6010A
D
02/03/03
14:51
DH
Cadmium, Total
<0.549
0.549
mg/kg
SW846 6010A
D "
02/10/03
10:21
DH
Chromium, Total
15.2
0.263
mg/kg
SW846 6010A
D
02/10/03
10:21
DH.
Copper, Total
61.4
0.263
mg/kg
SW846 6010A
D
02/10/03
10.-21
DH
Lead, Total
11.9
1.31
mg/kg
SW846 6010A
D
02/10/03
14:58
DH
Molybdenum, Total
<2.19
2.19
mg/kg
SW846 6010A -
D
02/06/03
17:08
DH
Nickel, Total
34.2
0.263
mg/kg
SW846 6010A
D
02/10/03
10:21
DH
Zinc, Total
109
0.263
mg/kg
8W8461601OA
D
02/10/03
10:21
DH
Mercury, Total
0.310
0.014
mg/kg .
SW846 7470A
D .
02/20/03
8:42
DH
Selenium, Total
<2.73
2.73
mg/kg
SW846 7741A
D
02/19/03
10:46
DH
PCB
BDL
2.9
mg/kg
SW846 8080
S16
02/07/03
13:38
KK
Paint Filter
PASS
P/F
SW846 9095
S16'
02/06/03
15:15
MNU
Page 4,
ENVIRONMENTAL
SCIENCE CORP.
REPORT OF ANALYSIS
Mr. Scott Fields
Davis & Brown
P.O. Box 15038
Quinby, SC 29506
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
February 12, 2003
ESC
Sample # :
L103192-03
Date Received
February
04, 2003
Description
2-3-2003
Site
ID
Sample ID
64172
Project
#
2-3-2003
Collected By
Collection Date
01/27/03
09:45
Parameter
Dry Result
Det. Limit
Units
Method
Date
Analyst
Total Solids
47.3
%
254OG
02/04/03
1311
SA
Polychlorinated
Biphenyls
PCB 1016
BDL
0.42
mg/kg
8082
02/07/03
1338
KK
PCB 1221
BDL
0.42
mg/ka
8082
02/07/03
1338
KK
PCB 1232
BDL
0.42
mg/kg
8082
02/07/03
1338
KK
PCB 1242
BDL
0.42
mg/kg
8082
02/07/03
1338
KK
PCB 1248
BDL
0.42
mg/kg
8082
02/07/03
1338
KK
PCB 1254
BDL
0.42
mg/kg
8082
02/07/03
1338
KK
PCB 1260
BDL
0.42
mg/kg
8082
02/07/03
1338
KK
i
Al 'en VUrilEerley, ESC Representative
Results listed are dry weight basis.
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 4 of 8
ENVIRONMENTAL
SCIENCE CORP.
REPORT OF ANALYSIS
Mr. Scott Fields
Davis & Brown
P.O. Box 15038
Quinby, SC 29506
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax Z.D. 62-0814289
Est. 1970
February 12,2003
ESC
Sample # :
L103192-04
Date Received February 04,
2003
Description 2-3-2003
Site
ID
Sample ID 64172
Project
#
2-3-2003
Collected By
Collection Date 01/27/03 09:45
Parameter
Result
Det. Limit
Units
Method
Date/Time
Analvst
Decachlorobiphenyl
92.
% Rec.
8081A
02/07/03
1050
KK
Tetrachloro-m-xylene
86.
% Rec.
8081A
02/07/03
1050
KK
TCLP Herbicides
2,4,5-TP (Silvex)
BDL
0.0020
mg/1
8151A
02/10/03
0813
KK
2,4-D
BDL
0.0020
mg/1
8151A
02/10/03
0813
iGC
Surrogate Recovery
2,4-Dichlorophenyl Acetic Acid
98.
% Rec.
8151A
02/10/03
0813
rK
TCLP Semi-Vclatiles
1,4-Dichlorobenzene
BDL
0.10
mg/l
8270C
02/07/03
1835
KSG
2,4-Dinitrotoluene
BDL
0.10
mg/l
8270C
02/07/03
1835
KSG
Hexachlorobenzene
BDL
0.10
mg/l
8270C
02/07/03
1835
KSG
Hexachlaro-1,3-butadiene
BDL
0.10
mg/1
8270C
02/07/03
1835
KSG
Hexachlorcethane
BDL
0.10
mg/1
8270C
02/07/03
1835
KSG
Nitrobenzene
BDL
0.10
mg/l
8270C
02/07/03
1835
KSG
Pyridine
BDL
0.10
mg/l
8270C
02/07/03
1835
KSG
m&p-Cresol
BDL
0.10
mg/1
8270C
02/07/03
1835
KSG
o-Cresol
BDL
0.10
mg/l
8270C
02/07/03
1835
KSG
Pentachlorophenol
BDL
0.10
mg/l
8270C
02/07/03
1835
KSG
2,4,5.-Trichlorophenol
BDL
0.10
mg/l
8270C
02/07/03
1835
KSG
2,4,6-Trichlorophenol
BDL
0.10
mg/l
8270C
02/07/03
1835
KSG
Surrogate Recovery
Nitrobenzene-d5
53.
% Rec.
8270C
02/07/03
1335
KSG
2-Fluorobiphenyl
48.
% Rec.
8270C
02/07/03
1835
KSG
p-Terphenyl-dl4
83.
% Rec.
8270C
02/07/03
1835
KSG
Phenol-d5
60.
% Rec.
8270C
02/07/03
1835
KSG
2-Fluoromhenol
57.
% Rec.
8270C
02/07/03
1835
KSG
2,4,6-Tribromophenol
78.
% Rec.
8270C
02/07/03
:835
KSG
AI'lenMinkerley, ESC Renresentative
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
A2LA - 1461-01, AIHA - 100789 , AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
KY - 90010, KYUST-0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
Notes:
The reported analytical results relate only to the sample submitted
This report shall not be reproduced, except in full, without the written approval from ESC.
All samples analyzed in accordance with 40 CFR, Part 136.3
L103192-04 (PAINT) - contains no free liquid
Page 6 of 8
ENVIRONMENTAL
SCIENCE CORP.
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Scott Fields February 12,2003
Davis & Brown
P.O. Box 15038
Quinby, SC 29506
ESC
Sample # :
L103192-04
Date Received February
04, 2003
Description 2-3-2003
Site ID
Sample ID 64172
Project #
2-3-2003
Collected By
Collection Date 01/27/03
09:45
Parameter
Result
Det. Limit
Units
Method
Date/Time
Analyst
Paint Filter Test
See Footnote
%
9095
02/06/03
1515
MNU
TCLP Extraction
-
1311
02/04/03
1506
TVH
Mercury
BDL
0.0010
mg/l
7470A
02/05/03
1751
RH
Arsenic
BDL
0.050
mg/l
60102
02/05/03
2339
CRF
Barium
0.56
0.050
mg/l
6010B
02/05/03
2339
CRF
Cadmium
BDL
0.050
mg/•l
6010B
02/05/03
2339
CRF
Chromium
BDL
0.050
mg/l
6010B
02/05/03
2339
CRF
Lead
BDL
0.050
mg/l
6010B
02/05/03
2339
CRF
Selenium
0.065
0.050
mg/1
6010B
02/05/03-2339
CRF
Silver
BDL
0.050
mg/1
6010B
02/05/03
2339
CRF
TCLP ZHE Extraction
-
1311
02/04/03
1507
TVH
TCLP Volatiles
Benzene
BDL
0.050
mg/l
8260B
02/06/03
1743
CH
Carbon tetrachloride
BDL
0.050
mg/l
8260B
02/06/03
1743
CH
Chlorcbenzene
BDL
0.050
mg/l
8260B
02/06/03
1743
CH
Chloroform
BDL
0.050
mg/l
8260B
02/06/03
1743
CH
1,2-Dichloroethane
BDL
0.050
mg/1
8260B
02/06/03
1743
CH
1,1-Dichloroethene
BDL
0.050
mg/l
8260B
02/06/03
1743
CH
2-Butancne (MEK)
BDL
2.5
mg/l
8260B
02/06/03
1743
CH
Tetrachloroethene
BDL
0.050
mg/l
8260B
02/06/03
1743
C4
Trichlcrcethene
BDL
0.050
mg/l
8260B
02/06/03
1743
CH
Vinyl chloride
BDL
0.050
mg/l
8260B
02/06/03
1743
CH
Surrogate Recovery
Dibromofluoromethane
98-
% Rec.
8260B
02/06/03
1743
CH
Toluene-d8
100
% Rec.
8260B
02/06/03
1743
CH
4-Bromofluorobenzene
100
% Rec.
8260B
02/06/03
1743
CH
TCLP Pesticides
Chlordane
BDL
0.030
mg/l
8081A
02/07/03
1050
KK
Endrin
BDL
0.0050
mg/l
8081A
02/07/03
1050
KK
Heptachlor
BDL
0.0050
mg/1
8081A
02/07/03
1050
KK
Lindane
BDL
0.0050
mg/l
8081A
02/07/03
1050
KK
Methoxychlor
BDL
0.0050
mg/l
8081A
02/07/03
1050
KK
Toxanhene
BDL
0.10
mg/l
8081A
02/07/03
1050
KK
Surrogate Recovery
BDL - Below Detection Limit'
Det. Limit - Estimated Quantitation
Limit(EQL)
Laboratory Certification
Numbers:
A2LA - 1461-01, AIHA - 100789
AL - 40660, CA
- I-2327, CT- PH-0197, FL - E87487,
GA -
923,
IN - C-TN-01
KY - 90010, KYUST-0016, NC
- ENV375,DW21704,
ND - R-140,
SC - 84004, TN -
2006, VA -
00109,
WV - 233
Notes:
The reported analytical results
relate only to
the sample
submitted
This report shall not be reproduced, except in
full, without the written approval
from
ESC.
L103192-04 (PAINT) - contains
no free liquid
Page 5 of 8
A N I M A L W A S T E A N A L Y S I S R E P. O R T
Agricultural Service Laboratory
LAB No. 10119 . Clemson Extension
171 Old Cherry Rd, Clemson, SC 29634
http://www.clemson.edu/agsrvlb
NAME TOLSON, SHERRY ACCOUNT COCHSFL
ADDRESS P 0 BOX 219 DATE 02-04-2003
CITY CHERAW SC CHERAWUTILITY@MINDSPRING.COM
ZIP CODE 29520
SAMPLE NO. 12703300 MANURE: OTHER STORAGE: COVERED
-----------------RESULTS REPORTED ON AN AS -SAMPLED BASIS----------------------
lbs/ton
Ammonium Nitrogen
0.03
%
0.60
Organic Nitrogen
0.74
%
14.83
Nitrate Nitrogen
---------------------------------------------------------------
60.79
ppm
0.12
INCORPORATED AVAILABLE NITROGEN ESTIMATE
9.58
SURFACE AVAILABLE
---------------------------------------------------------------
NITROGEN ESTIMATE
9.40
Phosphorus as P205
0.39
%
7.73
Potassium as K20
0.15
%
2.91
Calcium
14.72
%
294.30
Magnesium
0.22
%
4.44
Sulfur
0.12
%
2.32
Zinc
67.06
ppm
.0.13
Copper
37.15
ppm
0.07
Manganese
56.93
ppm
0.11
Sodium
184.78
ppm
0.37
Moisture
51.75
%
Calcium Carbonate
Equivalency 34.35'.
%
686.93
------------------------------------------------------------------------------
INCORPORP_TED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
incorporated into the soil within hours of application. Assumes some loss of
ammonium-N during application and prior to incorporation.
SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of
organic-N, and 100.% of nitrate-N (if determined). Assumes the manure will .be
left on the surface of the soil with no incorporation by plowing or irrigation.
Available nitrogen calculations are estimates and if nitrate-N was not re-
quested the amount of available nitrogen may be slightly more than reported.
Also, the actual amount may be more or less than the estimate depending on the
composition of the manure, soil type, and environmental conditions.
All of the potash in the animal waste should be plant available in the first
year of application. Although not all of the phosphorous is available in the
first year, its availability should be comparable to that in commercial
fertilizers.
The rate of animal waste to apply for crop production is dependent on the
nutrient content of the waste, method of application and i corpor tion, it
test, crop to be grown, and previous manure applications m s ca the
plant available nitrogen content of the waste is use rm n th r to of
application. APPROVED BY
Cooperative extension work in agriculture and home a onomics-state o
SOUTH CAROLINA, CLEMSON UNIVERSITY, and the UNITED S3ATES DEPARTMENT
of AGRICULTURE cooperating.
1 of 1 2/4/03 5:16 PM
1.0
1.1
1.2
1.3
2.0
WASTEWATER TREATMENT FACILITY .4 g
TOWN OF CHERAW, SOUTH CAROLINA .
� G
O N
FACILITY DESCRIPTION
Treatment Process
The Cheraw wastewater treatment plant is currently permitted for a capacity of 4.0 MGD.
The plant treats wastewater utilizing the activated sludge process operating in the
extended aeration mode. It includes the following treatment units: Bar screen, flow
measurement,, grit chamber; aeration basins, clarifiers, and disinfection. Excess solids are
removed from the treatment system pumped to a holding tank where the solids are mixed,
aerated, and thickened. Solids are then dewatered utilizing a belt filter press and then
further treated by the lime pasteurization process prior to a final disposal by land
application.
Current Operating Condition
The current wastewater flow to the treatment plant averages approximately 1.54 MGD of
which approximately 63 percent of this flow is from industrial users. The Town has an
Industrial Pretreatment Program which controls the discharge of toxic pollutants. During
the past year the influent and effluent BOD averaged 473 mg/1 and 12.4 mg/l respectively.
Influent and effluent suspended solids have averaged 293 mg/1 and 12.8 mg/1 respectively.
The plant's NPDES permit requires effluent BOD and TSS to be less than 30 mg/l.
Solids Production
The -quantity of solids produced by the plant is subject to many factors. During the past
year, the plant staff removed from the treatment system approximately 1728 dry tons.
Dewatered solids off the belt press are not sufficiently stabilized and must receive
additional treatment in order to comply with EPA standards for land application.
BIOSOLIDS TREATMENT AND DISPOSAL
2.1 Process Description
Dewatered solids receive additional treatment by a process developed by the RDP
Company call EnVessel pasteurization. This process utilizes quicklime and supplemental
electrical heat to elevate the pH and temperature for the sludge to that level needed to
destroy pathogens and meet vector attraction requirements. Amore detailed description
of the process is presented below.
As the sludge comes off the belt press it is conveyed to a storage hopper then on to a
mixing chamber called a "thermoblender" where quicklime is added. The mixing chamber
contains mixing rotors that blend the sludge and the quicklime. Within this chamber the
sludge is heated to approximately 70°C (158°F) by reaction with the quicklime and by
electrical heat tubes installed internal to the mixing rotors. The lime also elevates the
sludge pH to 12. The heated sludge/lime mixture is then discharged to the pasteurization
vessel where the entire mass of material is allowed to cook for approximately 30 minutes.
This vessel is an enclosed, insulated environment, maintaining the proper temperature over
time to destroy harmful pathogens. The vessel is equipped with heating elements to
compensate for any heat losses during the processing period and to ensure that the sludge
maintains the proper temperature throughout. After treatment the biosolids are conveyed
from the pasteurization vessel to a concrete pad where they are windrowed to facilitate
further dewatering after which the biosolids are moved into a covered storage area until
land application.
2.2 Significant Process Technical Features
2.2.1 General: The process of sludge treatment by the addition of lime is not new and the
technology is known and fully documented elsewhere. However, the process used in
Cheraw has several unique technical features which improve the process of lime treatment
and produces a biosolids product of superior quality. Some of those features are
presented below.
2.2.2 Lime Dosage: the Cheraw biosolids treatment system utilizes a combination of lime and
electrical heat to meet the temperature and pH requirements for pathogen destruction and
reduction in vector attraction. A lime only treatment system would require approximately
1 pound of lime per pound of dry solids to create sufficient chemical hydration to raise the
sludge temperature to 158°F. With the use of supplemental electrical heat, the Cheraw
system has been able to reduce the lime requirement to approximately 0.43 pounds of lime
per pound of dry solids. The reduction in requited lime dosage has several advantages to
include the following.
> Supplemental electrical heat allows the pH of the sludge to increase with less lime.
> Ammonia gas is produced by the reaction of sludge and lime. With a lower lime
dosage less ammonia gas is produced resulting in reduced process odors. It also
results in preserving the nitrogen content of the final biosolids.
> A lower lime dosage reduces the mass of biosolid product for final disposal.
2.2.3 Product Quality: The Cheraw system cures or cooks the sludge in an enclosed insulated
treatment vessel. This method insures that the entire mass of sludge and lime mixture is
maintained at the required temperature for complete pathogen destruction. As previously
mentioned the vessel is equipped with electrical heating elements to compensate for any
temperature loss during the treatment period.
2.2.4 Land Application R. In the Cheraw area most farmland requires the application of lime
to make up the calcium that is absorbed by the crops. Lime is typically applied to the
fields to maintain a pH of 6.5 to 7.0 generally at a rate of 2000 pounds per acre. The rate
of land application of biosolids in the Cheraw area is typically limited by its lime content.
Therefore, reducing the lime content as previously described allows a greater biosolids
application rate per acre thereby decreasing the total amount of land required for biosolids
disposal. For example, the land application rate for Cheraw's biosolids using a
conventional lime only system would be 6.25 tons of biosolids per acre. With the lime and
electrical heat system the application rate is increased to approximately 14.5 tons per acre.
Therefore, the Cheraw system has reduced land requirement by approximately 57 percent.
2.3 Biosolids Product Quality
In order to document compliance with the EPA 503 Regulation's Class A sludge pathogen
reductions requirements and vector attraction requirements continuous measurements are
made of sludge temperature and pH within the "thermoblender" and pasteurization vessel.
The pH of the biosolids is also monitored at the end of the 24-hour treatment period to
verify compliance with the EPA regulations. Since the process has been in operation,
there has been no instance where temperature and pH requirements of EPA have not been
met. Prior to hauling any biosolids off -site fecal coliform samples are taken. This
sampling has indicated no evidence of fecal coliform regrowth even after several months
of storage.
2.4 Biosolids Disposal
The Town of Cheraw is currently marketing the biosolids to farmers and others. To date
biosolids have been used for land reclamation, landfill top cover, and farmland. A research
project has been, initiated by the State Forestry Commission and Clemson University to
study the effect of Cheraw biosolids on pine tree growth at the Sandhills State Forest near
Cheraw.
Each recipient of biosolids is given a copy of a label as included. These labels describe the
quality of the biosolids and provide assistance as to its proper use.
. GENERAL INFORMATION
DISTRIBUTION OF RESIDUAL SOLIDS
TOWN OF CHERAW, SOUTH CAROLINA
1. Material Handling
a. How will the residuals be handled and transported from where the residuals are produced
to where they will be treated?
Residuals are produced and treated at the same site.
b. Where will the residuals be stored until processed?
Residuals are stored in a holding tank until they are dewatered and pasteurized.
c. How will leachate collection be handled?
Leachate from the treatment system and storage facility are collected and returned to
the head of the wastewater treatment plant.
d. What will be the duration of treatment?
Refer to attached biosolids treatment process description.
e. Where will the final product be stored?
After treatment biosolids are stored on a covered concrete pad.
f. How long will the final product be stored before being distributed?
The storage facility has the capacity to store product up to 120 days at current product
rates.
g. How will the final product be distributed?
The biosolids are hauled by truck to land application sites in bulk.
2. Product Distribution
Currently all product produced is being used by local farmers in South Carolina, North
Carolina, and at the Sandhills State Forest.
3. Product Label
Enclosed is a copy of the product label currently being used. This label is given to each
recipient of product.
�-� TOWN OF CHEQAW
July 23, 2003
North Carolina Department of Environment
and Natural Resources
Division of Water Quality
1617 Mail Service Center
Raleigh, N.C. 27699-1617
To Whom It May Concern:
RE: NPDES PERMIT NO. SCO020249
TOWN OF CHERAW
CHESTERFIELD, S.C.
PART 11, B-6 SIGNATORY REQUIREMENTS
The Town of Cheraw hereby authorizes the Town's Public Utility Director,
currently Ricky Ingram, to sign and certify all applications, reports or documents
containing information related to this permit that are submitted to the North Carolina
Department of Environment and Natural Resources. This authorization shall remain in
effect until this notice rescinds or changes this authorization and notifies. the North
Carolina Department of Environment and Natural Resources in writing.
Sincerely,
J6
J. William Taylor
Town Administrator
JWT/em
cc: , Andy Ingram, Mayor
P.O. Box 219 • Cheraw, 6S.C. 29520 • (843) 537-8400 • FAX (843) , 537-8407
E-Mail: townofcheraw@mind,3prin8.com
CHERAW-ALKALINE BIOSOLIDS SOIL AMENDMENT
CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES
BIOSOLIDS SAMPLE DATE: March 12, 2003
Biosolids
Maximum
Maximum
Maximum
Maximum
Metal
Allowable
Allowable
Application
Application
Content,
Metal
App. Rate,
Rate,
Rate,
METALS
ppm
Content, ppm
#/Acre/Yr.
DT/Acre/Yr.
WT/Acre/Yr.
Arsenic, Total
3.25
41.00
1.80
127.55
277.04
Cadmium, Total
0.63 '
39.00
1.70
623.64
1354.55
Chromium, Total
26.98
1200.00
134.00
1143.15
2482.94
Copper, Total
123.81
1500.00
67.00
124.57
270.58
Lead, Total
5.04
300.00
13.00
594.12
1290.44
Mercury, Total
0.08
17.00
0.75
2039.43
4429.69
Molybdenum, Total
4.51
18.00
0.80
40.85
88.73
Nickel, Total
36.40
420.00
18.70
118.26
256.85
Selenium, Total
3.13
36.00
4.50
330.72
718.33
Zinc, Total
223.28
1525.00
125.00
128.87
279.92
PCB
BDL
10.00
`Actual metal content less than amount indicated.
Biosolids
Biosolids
Maximum
Maximum
Nutrient
Nutrient
Crop/Soil
Application
Application
Content,
Content,
Requirement,
Rate,
Rate,
ppm
%
#/Acre"
DT/Acre/Yr.
WT/Acre/Yr.
Nitrogen, Ammonia
608.17
0.06
Organic Nitrogen
6372.72
0.64
Plant Avail. Nitrogen (PAN)
108.60
0.01
120.00
254.36
552.48
Phosphorus as P205
3570.81
0.36
80.00
5.16
11.20
Potassium as K20
1494.35
0.15
50.60
7.70
16.73
Calcium, Total
118292.79
11.83
Calcium as CaO
165609.90.
16.56
Calcium as CaCO3 (CCE)
302432.67
30.24
2000.00
1.52
3.31
Magnesium, Total
1920.07
0.19
Manganese
39.10
0.00
Sulfur
1081.67
0.11
Percent Moisture
53.96
These are typical values and must be adjusted based upon specific site conditions
DT is Dry Tons of Biosolids. WT is Wet Tons of Biosolids.
CERTIFICATION: This biosolid product has been produced by the Town of Cheraw's Wastewater
Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature
and lime (calcium oxide). The Town of Cheraw certifies that this biosolid complies with the
Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has a metal
and nutrient content as presented above.
DIRECTIONS FOR USE: This biosolid is intended to be used as a soil amendment. The biosolid
land application rate shall not exceed the most restrictive Maximum Application Rate as indicated in
the table above. The application rate for nitrogen, phosphorus, potassium, and calcium is dependent
upon the crop grown and site soil characteristics. The user should contact the Clemson Extension
Service (843-623-2134) and/or the Soil Conservation Service (843-623-2.187) for assistance in
determining the proper application rate for each crop and site. In no case shall the land application
rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension
Service Circular #476 tilled "Lime and Fertilizer Recommendations."
THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY.
AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES.
THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING. OF THIS
BIOSOLID PRODUCT.
Application of this residual is prohibited except in accordance with the instructions on this information
sheet Residuals shall not be applied to any site that is flooded, frozen or snow-covered. The applier
must provide adequate procedures to prevent surface run-off from carrying any disposed or stored
residuals into any surface waters. A minimum buffer of 10 feet must be provided between the application
site and any public or private water supply source (including wells) and any stream, lake, river or natural
drainage way.
Mr. Ricky D. Ingram, Public Utility Director
P. 0. Box 111; Cheraw, SC 29520
Telephone: 843-537-8440
FAX: 843-537-8442
PP()nl IrT I BUM NAIIAP
\O�OF W AT �RQG _ Michael F. Easley, Governor
William G. Ross Jr., Secretary
�y North Carolina Department of Environment and Natural Resources
� r
— I Alan W. Klimek, P.E., Director
Division of Water Quality
Apri] 28, 2003LIAPR 2 9 2003
RICKY D. INGRAM, PUBLIC UTILITY DIRECTOR
TOWN OF CHERAW i
POST OFFICE BOX 219 - -
CHERAW, SOUTH CAROLINA, 29520
Subject: Application No. WQ0014248
Additional Information Request
Town of Cheraw Residuals Distribution
Program
Distribution of Residual solids (503)
Chesterfield County, South Carolina
Dear Mr. Ingram:
The Non -Discharge Permitting Unit has conducted a preliminary review of the subject permit application
package. Additional information is required before we may continue our review. Please address the
following items no later than May 28, 200.3.
1: The application must be signed by an appropriate person in accordance with 15A NCAC 211
.0206. This regulation states that, for a corporation, it must be signed by a principal
executive officer of at least the level of vice-president, or his duly authorized representative.
Please sign the application following the above requirement. You may provide
documentation the signer, or any employee holding the position of the signer, is a duly
authorized representative through a letter of delegation.
2. The copy -of the information sheet intended to accompany--the-residuals-does--not--meet-the
requirements specified in item H.6 in your existing permit and our current regulations.
Please provide either a label which shall be affixed to the bagged processed residual or a
revised information sheet which shall be provided to the person who receives the processed
residual. The label or information sheet shall contain at a minimum, the following
information:
a. The name and address of the person who prepared the residual that is sold or given
away in a bog or other container for application to the land.
b. A statement that application of the residual to the land is prohibited except in
accordance with the instructions on the label or information sheet. .
c. A statement that the residuals shall not be applied to any site that is flooded, frozen or
- snow-covered.
d. A statement that adequate procedures shall be provided to prevent surface runoff from
carrying any disposed or stored residuals into any surface waters.
Non -Discharge Permitting Unit
1617 Mail Service Center, Raleigh, NC 27699-1617
DENR Customer Service Center
An Equal Opportunity Action Employer -
Internet http://h2o.enr.state.nc.us/ndpu
Telephone (919) 733-5083 Fax (919) 715-6048
Telephone 1 800 623-7748
5017o recycled/10% post -consumer paper
NCDENIR
e. Information on all applicable buffers including a 10 foot buffer between the
• application site and any public or private water supply source (including wells) and
any stream, lake, river or natural drainage way.
3. Please clarify the estimated volume of residuals listed 'as 1128 dry tons per year. Is this the
weight of residuals alone or the residuals with amendments? Please note that we need the
volume reported as weight of residuals with amendments. Your existing permit is for 1800
dry tons per year. You may provide a reasonable estimate of the .dry tons/year anticipated
over the next five years if that might be different from the actual production recorded in a
past year. Note that you are not allowed to distribute more than the dry tons/year specified in
your permit.
Please be aware that you are responsible for meeting all requirements set forth in North Carolina rules
and regulations. Any oversights that occurred in the review of the subject application package are still
the responsibility of the applicant. In addition, any omissions made in responding to the above items may
result in future requests for additional.infon-nation.
Please reference the subject application number when providing the requested information. Two copies
of all revised and/or additional documentation should be signed, sealed, dated, and submitted to my
attention at the address above. Please note that failure to provide -this additional information on or before
the above requested date may result in your application being. denied.
If you have any questions regarding this request, please do not hesitate to contact me at
duane.leith@ncmail.net or (919) 733-5083, extension 370. You may also check the future status of this
project online at http://h2o.enr.state.nc.us/bims/RQorts/reportsPermits.html. Thank you for your
cooperation.
Sincerely,
Duane Leith
Non -Discharge Permitting Unit
Cc: NCDWQ Regional Offices, Water Quality Section
Permit Application File WQ0014248
NON NPDES FACILITY AND PERMIT DATA 07/28/9}9k"07:46:41
RETRIEVE OPTION q TRXID 60U KEYWQ.0014248
PERSONAL DATA FACILITY APPLYING FOR PERMIT APP/PERMIT FEE-$ 400.00 --REGION
FACILITY NAME> CHERAW, TOWN -A SLUDGE FACILIT5 CO.UNT_Y_>. WAKE f 05
ADDRESS: MAILING (REQUIRED) • ENGINEER: HAYES SEAY MATTERN & MATT
STREET: PO BOX 111 STREET: 181 E. E.VANS ST; BTC 105
CITY: CHERAW ST SC ZIP 29520 CITY:.FLORENCE ST SC ZIP 2952
TELEPHONE 843 537 8440 TELEPHONE: 803 669 4491
STATE CONTACT> ALLEN FACILITY CONTACT JAMES T. MORRIS-
TYPE OF PROJECT> SLUDGE D&M 15 LAT: 3441240 LONG: 07952100
DATE APP RCVD 08/07/97 N=NEW,M=MODIFICATION,R=REISSUE> N'
DATE ACKNOWLEDGED 08/08/97 DATE REVIEWED 08/12/97 RETURN DATE
REG COMM REQS / / DATE DENIED / / NPDES #-
REG COMM RCVD / / DATE RETURNED / / TRIB Q .0000 MG
ADD INFO REQS / / OT AG COM REQS / / TRIB DATE-
ADD INFO RCVD / / OT AG COM RCVD /
END STAT APP P 11/05/97 DATE ISSUED 08/15/97 DATE EXPIRE 07/31/02
FEE CODE( 6 ) 1=,(>1MGD) , 2= (>10KGD) , 3= (>1KGD) ,'4= (<1KGD+SF) , 5= (S>300A) , 6= (S'<`=300A)
7=(SENDEL),8=(SEDEL),9=(CLREC),0=(NO FEE) DISC CODES 01 ASN/CHG PRM
ENG CERT DATE 11/11/11 LAST NOV DATE, / / CONBILL( )'
COMMENTS: 1,800 DT/YR. NOV STABILIZATION,TCLP&MONITORING �.
MESSAGE:
r FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
JUL Me 1999
.a 1 ii�l,ut•ion- /iR'10,i1�:,rsa gle 10-1 dilution 0l 'Sample
auo , i.i L r R I
t
XX ,LACTOSE
24 hr. 48 hr.
E C�
24 hr. 48 hr.
10_2 dilution / 1.0 ml. sample
X LACTOSE
I hr. 48 hr..
-FINAL
FINAL
X' LACTOSE
24 hr. 48 ' hr.-
E C
24 hr. F48 hr.
FINAL
Batch Production Dates.
Date Test Performed
Time. Z: OO P P1
Operator'
I.s o
%.solids
MPN of total solids = (�
MPNI from table (8M 13...9-50) .
11 x % solids
RECEIVED
-.fill to logo
WATER QUALITY SECTION .
Non-DIschargo Compliance c-'
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
10 1 dilution / 10 ■l sample. 10-1 dilution / 1.0 al sample
I
XX LACTOSE
24 hr. 48 hr.
E C
24 hr. 48 hr.
10 — dilution / 1.0 ■1 sample
FINAL.
X LACTOSE
£4 hr. 48 hr.
1— .
124E C
.
hr. 48 hr.
Batch Production Dates:
Dat T t P f d 2- f
FINAL
Ti■
Ope
% S
So
MPN
MPN
r
e es er orme
ator
of total solids =
from table (SM n. 9-50)
FINAL
FECAL COLIFORM,FOR MUNICIPAL BIOSOLIDS
_�l 1 dilution / 10-■1 sample 10-1 dilution / 1.0,ml .sample.
XX -LACTOSE
24 Fir. 48 hr.
r'
r�
X LACTOSE
4 hr. 48hr.
E C
124 hr. 48 hr.
FINAL .
X LACTOSE
24 hr, E
hr.
---------7
E C
24 hr'. 48 hr.
FINAL
-Date Test.Performed
FINAL
Time
Operator
% Solids
-- MPN of total.solids
MPN from table (SM p.--9-50)
FECAL
COLIFORM FOR'MUNICIPAL
BIOSOLIDS
10-1
dilution % 10 ■1 sample
10-1.dilution
1 1.0 m'l sample
10-2 dilution.:./ 1.0 ■1 sample. Batch Production .Dates:..
Date Test Performed
X LACT05E E C' FINAL `
-Tine
24 hr. 48 hr.- 24 hr. 48 hr.
Operator..
% Solids
MPN of total'. solids V
r, MPN from table. -(SM P. 9=50)
11 X % solids
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
dilution / 10 ■l sample 10-1 dilution./ 1.0 ml sample
I
XX LACTOSE
24 hr. 48 hr.
E C
24 hr. 48 hr.
FINAL
X LACTOSE
24 hr. 48 hr.
-E C
24 hr. 48 hr.
FINAL
Date Test Performed
FINAL
Time
Operator
X Solids S
MPN of total solids
MPN from table (SM a 9-50)
11 u 'X snI irla .
E C
24 hr. 48 hr.
FECAL
COLIFORM FOR MUNICIPAL
BIOSOLIDS
10 1
dilution / 10 ml sample
10-1 dilution
I
/ 1.0.ml sample
XX LACTOSE
24 hr. 48 hr.
10 2'dilution / 1.0 al sample Batch Production Dates:
Date Test Performed
X LACTOSE E C FINAL.
Time
24 hr. 48 hr. 24 hr. 48 hr.
Operator
c,� a J
% Solids � / /f
FINAL. X LACTOSE
'24 fir. 48 hr.
E C
24 hr. 48 hr.
MPN of total solids =
MPN from table (SM p. 9-50)
11 x % solids-
FECALCOLIFORM FOR MUNICIPAL BIOSOLIDS
_d 1 dilution / 10 a1 sample.. 10-1 di.lutiom / 1.0.m1 sample
10 2 dilution / 1.0 ml sample, Batch Production Dates:
FECAL.COLIFORM FOR.MUNICIPAL BIOSOLIDS
is ;_I
dilution / 10 al sample 10 1 dilution / .1.0 ml sample•'
10-2-dilut-ion / 1.0•■1 sample Batch Production Dates:
.FINAL
10_Z dilution /." 1.0 ■.1 sample Batch Product,i`on Dates:
FECAL,COLIFORM-FOR
MUNICIPAL--BIOSOLIDS
dilution./
.10 ml- sample
I 10-1 dilution
/ 1,.0 ml' saimple
FINAL
1
10_p dilution / 1.0 ■1,sample Batch Production Dates:'
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS*-
ad-1.dilution / 10 ml sample 10-1 dilution / 1.0 m1 sample
. I
:FINAL
10-2 dilution /..1.0 ■l sample Batch Production Dates:
•4 g
4 hr.
E;•.
hr.
Date Test Performed. _ h
.FINAL
Time . �S
Operator. Q
X Solids rd
MPN of total'_solids
.MPN'from table (SM p..9-50)
-11 u .ti en7;r1�
FECAL
COLIFORM FOR MUNICIPAL
BIOSOLIDS
10 1
dilution 110 ■1 sample
10. dilution
'/ 1.0 1.sample
FINAL ,
10 2 dilution / 1A 41 .sample Batch Production Dates 1
n, -4- Ts.} Dn"fnJMMnd I L R
Pasteuriztion vessel operates on a constant speed with an in/out
time duration of 30 minutes.
MINIMUM
MINIMUM
DATE
2 HOUR pH 24 HOUR pH
TEMP IN
TEMP OUT
07101 /98
12.40
12.32
145
144
07/02/98
12.34
12.26
152
155
07/06/98
12.33'
12.21
153
157
07/07/98
12.32
12.23
150
148
07/08/98
. 12.37
12.25
156
158
. 07/09/98
12.21
12.17
. 158
.148
07/10/98
12.38
12.32
151
157
. 07/13/98
12.31
12.25
151
153
. 07/14/98
12.41
12.37
.158
158
07/15/98
12.33
12.26
152
156
07/16/98
12.32 -
12.26
156
159 .
07/17/98
12.37
12.30
154
133
07/20/98
12.37
12.32
161
157
07/21 /98
12.14
12.11
160
156
07/23/98
12.20
12.14
160
165
07/24/98
12.22
12.18
157
157
08/07/98
12.27
12.22
166
161
08/08/98
12.30
12.26
162
167
.08/10/98
12.24
12.18
1,58
138
08/11 /98
12.38
12.33
158
158
08/12/98 .
12.41
12.32
159
160
08/13/98
12.30
12.21
160
172
08/14/98
12.26
12.18
172
173
08/17/98
12.28
12.22
158
157
08/18/98
12.34
12.28
158
134
08/19/98
12.36
12.31
158
154
08/20/98 .
. 12. 32
12.29
160
150
08/21 /98
12.28
12.22
158
140
08131 /98
1.2.38
12.33
159
161
09101 /98
12.30
12.25
160
150
09/02/98 .
12.34 -
12.26
159
164
09/03/98 -.
12.29 .
12.19
164
165
09/04/98
12.31
12.24
.158 _
159
09/08/98
.1.2.34
12.28
160
169
09/09/98
.12.37
12.30
158
148
09/10/98-
12.35- .
12.18-
.159
143
09/11/98
12:20
12.11
159
161
: 09/14/98
.12.35
12.29
158.
160
09/15/98
12: 33
12.26
158
162 .
09/16/98 .
12.29
12.24
158
A60
09/17/98
- .1.2.34 -
12.30
158`
156
09/18/68
12.29 ".:
12:22
154
155
- 09/21 /98
12.33
12.28
,
09/22/98 .
.: ;12.22
12.17
159
. 160
09/23/98
1.2.31...
12.27
158 .
151
.09/24/98. '
12.28 .
12.22
16.1
152
09/25/98 -
12.19
12.12
159
150
09/28/98
12.18
12.12
160
152
-09/29198
12.08
12.05
158
160 -
09/30/98
12.34.
12.21
160
154
Pasteuriztion vessel -operates on a constant speed with an in/out
time duration of 30 minutes.
MINIMUM
MINIMUM
DATE
2 HOUR pH 24 HOUR pH
TEMP IN
TEMP OUT' "
04/01/98
12.18
12.10
161•
158
04/02/98
12.30 .
12.22
158
159
04/03/98
12.25
12.19
140
146
04/07/98
.12.68
.12. 02
158
158
04/08/98
12.07
12.03
158
160
04%09/98
12.12
12.09
-158
158
04/ 10/98
12.16
. 12.12
158
159
04/14/98
12.18
.12.13
158
159
04/15/98
> . 12.17
12.1-1
158.
158.
04/16/98
.12.20'
12.16
160,
157
04/17/98
12.11 -
12.08
158
159
04/20/98
12.18
12.12
158 '
160-'.
04/21 /98
12.20
12.16
158
158
04/22/98
12.22
12.16
158
159
04/23/98
12.14
12.10
156
158
04/24/98
12.10
12.03
99
158
04/27/98
12.18
12.11
160.
, 159
04/28/98
-12.22
12.17
158
158
04/29/98
12.18
12.13
.: 158
163
04/30/98
12.27
12.21
158;
142
05/01/98.
12.18
12.10
158''
158
05/04/98
12:08
12.06
'160
158
05/05/98
12.22
12.18,
160
158
05/06/98
12.17-
12.14
160
158
05/08/98
. 12.26
12.20
158
158
05/11 /98
12.16
.12.10
158
158
05/12/98,
12.19
12.14
158,
158
05/13/98
12.28
12.19
153
148
05/14/98
12.21
12.16
152
.145
' 05/15/98
12.27 ,.
12.20
145
150
05/18198
12.22
12.16
155 .
156
05/19/98
12.30
12.22
148
151
05/20/98
12.23
12.20'
144
121
05/21/98
12.19
12.12
163
151
05/22/98
12.28
12.21
156
155
05/25/98
.12.20
12.15
150
147
05/26/98
12.21
12.16
157,
147
05/27/98
12.18
12.14
146
'147
05/28/98
12.12 •
12.09
139
138
06/01/98
12.14
12.1.0
150 -
153
06/02/98
12.31
12.26
144
151.
06/03/98
1218 ,
12.24
156
153
06/04/98
12.22
12.15
149
158
06/05/98
. 12.19
12.15
145
132
06/08/98
12.31
12.26
144
137
06/09/98 ..
' 12.29
12.23
149 :
149. .
- 06/`t 0/98
12.27
12.23
145
151
06/ 11 /98
12.20 :
12.15
146'*
146
06/12/98
~ 12.27
12.21
145
147
06/15/98
12.26
--.12.20
142
147
06/16/98 _
12.42 . '
12.34.
147
1.50
06/1.7/98
12.38
' 12.31
142
145
06/18/98
`12.-29 `.
12.23
141
- 143
06/19/98
12.42
12.34
148
138
06/22198.
12.39
12.'36 '
146
151
06/24/98
12.56
1.2. 49
157
153
06/25/98
12 A4
12.40
156
164
06/26/98
-12.38 -
12.29
157
156
06/29/98
.12.22
12.17
145
154
06/30/98
12;31
12.25
150.
i 140.
e Pasteuriztion vessel operates on a constant speed vvith an in/Out
time duration
�� of 30 minutes.
INiINIIVIUldi
i'viiia''MU 1
MATE;
2 HOUR pH
224 FOUR pH
TEMP" IN
I CIIAP OUT
01 /02/98
12.22
12.16
162
162
. 01, 05f 98
12. C6
12. 01
160
158
01 /06/98
12.15
2.10
158
i 58
01 /07f98
- 121.09
12.04
158
158
011A4,198
12.12
12.1 ^v
158
158
0414 5f98
12.07
12.03
158
161
011,16/98
12.09
12.0A
158
i 58
01/20/98
12.19'
1 12.12
153
158
01'21198
12.24
i 2.19
i 58
158
01 f22/98
12.16
12:10
158
158
G 1 /201
12.2 1
12.14
_ 158
.159
01f26/98
12.26
12.18
15S
161
01 /27/98
12.20
12.11
158
158
01 /28/98
12.18
12.12
1.58
160
G 1 /29/98
12: 14
12.12
1 O
158
01 /3C/98
12.18
12.11
158
153.
02/02198
12.25
12.18
158
158
02f03r,98
12.20
12.14
158
158
OZ'04f98
12.15;
12.10
158
15-8
02'05/98
12.1.1
12.08
159
159
GZ'06/98
12.15
12. G9
158
158
02109f98
12.26
111
158
458
02/10/98
12.28
12.19
158
158
OZf11f98
12.1
12.14
158
160
02/12/98
12.16
I L.10
158
158
02/13,
. 12.24
12:16
158
158
G2/i.7/98
'12.14
12.09
158
158
0111 98
12:24
12.17
159
158
12. i 9
12.13
153
158
n02119198
' 02/40/98
12.15
� 1.2.11
159
158 -
G2I23/9p8
i2.2 i
i2.15
158
158
G2/24198
12.27,
121.2G
4158
158 .
02/25/98
i2.I
12.G8
15^v
152
03102M
12.16
12.11
158
163
03/03/98
12.19
12.13
158
1001
03f04/98
12.22
12.18
163
158
03/05/98
i 2.26,
12.20
158
158
03,106,198
12.20
12.14
... 158
158
03/09/98
12.1 c6
12.12
158
155
03/12/98
12:17
12.1.0,
158
158_
03' 6/�$
12.Go
:. 12.0 i
i6 i
16 i .
C3f17f98"
.
12.11
12.06
158
160'
..
03/18195 .
12:1
12.00
- 158
158 .
03f19/98
_ 12.07
12.04
158
158
03/23/98 ..
12.09 .
12.03
158
i 5S
03/24/58
12.20
12.12
.. 158.
158
03i25198.
i2.1-5-
12.10
158
158
03/26198:
: •12.09
12.06
158
159
03/27/98
12:03
12.OG
150
158
03/30198
12.20
12.14
158
158
03/3. i /98
12.28
12. 22
158
158
Pasteuriztion vessel. operates on a constant speed with an irdout
time duration of 30 minutes.
MINIMUM
MINIMUM
DATE
2 HOUR pH
24 HOUR pH
TEMP IN
TEMP OUT
10/06/98
12.26
12.17
158
155
10/07/98
12.22
12.18
160
157
10/08/98
12.27
12.21
159
121
10/09/98
12.31
12.22'
158
160
10/12/98
2.28
12.21
158
136
10/13/98
12.26
12.19
158'
132
10/14198
12.30
12.18
158
160
10/15/98
. 12.28
12.16
158
138
10/16/98
12.34
12.22
156
156
10/19/98
. 12.28
12.22
158
138
10/20/98
12.24
12.18
161
156
10/21 /98
12.24
12.20
158
123
10/22/98
12.16
12.12
158
90 .
10/23/98
.12.20
12.16
166
120
10/26/98
12.30
12.25
158
153
10/27/98
12.22
12.18
158
151
.10.128198
12.31
12.23
.160
151
10/29/98
12.18.
12.12
158
110
' 11/02/98
12.34
12.29
158
158
11 /03%98
12.35
12.29
158
154
11 /04/98
12.26
12.19
158
153
11/05/98
12.29
'12.24
158
145
11 /06/98
12.32
12.22
161
150
11/09/98
:. 12.37 "
12.23
158
159
11 /10/98
12:25
12.19
158
158
11 /11 /98
12.23
12.20
158
142
11/12/98
12.21
12.22
158
156
11 /13/98
12.21
12.15
164
158
11 /16/98
12.25
12.19
158 .
157
11 /17/98
.12.28
12.22
158
164
11 /18198
12.30
12.24
145
135
11 /19/98
12.28
12.23
158
153
11 /20/98
12.29
12.21
158
167
11 /23/98
12.31
12.25
158
162
11/24/98
12.28
12.22
158
151
12l01 /98
12.21
12.17
1.47
147
12/02/98
12.22
12.17
143
144
12/03/98
12.28
12.1.9
150
112
12/04/98 .
12.22
12.18
161
.160
12/05/98 .
12:30
12.22
152
153
12/06/98
12.19
12.15
158
156
12/07/98
;12.22.
'12.18
158
148
12/08/98 .
12.17
12.15
158
152
12/09198
12.24
12.19
158
96
12/10/98 .
12.42
12.37
160
153
12/11 /98
12.30.
12.23
146
126
12/14/98
12.36
12.27
152
1.55
12/15/98
12.24
12.19
145
150
12/16/98
12.23
12.18
152
151
12/17/98.'
12.29
12.25
158
142
12/18/98
12.20
12.12
145
146
12/21 /98
::12.12 :
12:09
161
145
12/22/98
12.20
12.09
158
100
12/29/98
12.31.
.12.28
158
156 .
12/30/98
'12.28
12.22
158
155
12/31/98
12:27'
'12.20
152
154
Davis & Brown
PO Box 15038
Quinby, SC 29506
(803) 665-6746 FAX: (803) 629-1444
Certificate of Analysis
Client: CHERAW, CITY OF
South Carolina Certification Number: 21117
P.O.BOX I I I
CHERAW, SC 29520
Client #: 168
Receipt Date:
11-Mar-99
Contact: SHERRY LEBEL
Report Date:
12-Apr-99
Sample Date: 10-Mar-99
SDG #: SDG-009504
Approved By:
Van Ward
Lab Director
Reporting
Parameter
Result
Limit
Unit
Method Flag Date
Time
Analyst
LSID-021475 1009-Z
Cyanide
<0.010
0.01
mg/L
EPA 335.2
3/17/99
14:06
TL
LSID-021476 1010-Z
Cyanide
<0.010
0.01
mg/L
EPA 335.2
3/17/99
14:06
TL
LSID-021477 1011-Z
Cyanide
<0.010
0.01
mg/L
EPA 335.2
3/17/99
14:06
TL
LSID-021478 3-5-99-204
Aluminum, Total
0.070
0.02
mg/1
EPA 202.2
3/19/99
11:30
DH
Acid Digestion (Liquids)
YES
EPA 4.1.4
3/15/99
14:00
DH
LSID-021479 ., ` 3-8-99-200
TCLP
PASS
P/F
3/26/99
11:23
SF
Nitrogen, Nitrate- IC
635
48.5
mg/kg
EPA 300.0
D 3/18/99
12:11
SM
Nitrogen, Nitrite- IC
<121
48.5
mg/kg
EPA 300.0
D 3/18/99
12:11
SM
Nitrogen, Ammonia
578
98
mg/kg
EPA 350.3
D 4/8/99
14:30
NW
Acid Digestion (Solids)
YES
SW846 3050A
3/22/99
9:00
DH
Percent Moisture
60.0
0.1
wt%
SW846 3540
3/23/99
17:00
LM
Aluminum, Total
9550
0.397
mg/kg
SW846 6010A
D 4/6/99
12:00
DH
Page 1
Davis & Brown
PO Box 15038
Quinby, SC 29506
(803) 665-6746 FAX: (803) 629-1444
Certificate of Analysis
Client: CHERAW, CITY OF South Carolina Certification Number: 21117
P.O.BOX 111
CHERAW, SC 29520
Client #: 168 Receipt Date: 11-Mar-99
Contact: SHERRY LEBEL Report Date: 12-Apr-99
Sample Date: 08-Mar-99
SDG #: SDG-009504
Approved By:
Van Ward
Lab Director
Reporting
Parameter
Result
Limit
Unit
Method
Flag
Date
Time
Analyst
Arsenic, Total
5.18
0.1
mg/kg
SW846 6010A
D
3/23/99
15:00
DH
Cadmium, Total
<0.990
0.397
mg/kg
SW846 6010A
D
3/23/99
17:49
DH
Chromium, Total
60.0
0.397
mg/kg
SW846 6010A
D
3/26/99
11:16
DH
Copper, Total
95.0
0.993
mg/kg
SW846 6010A
.D
3/23/99
17:49
DH
Lead, Total
5.93
0.1
mg/kg
SW846 6010A
D
3/23/99
9:30
DH
Molybdenum, Total
3.18
0.497
mg/kg
SW846 6010A
D
4/1/99
10:41
DH
Nickel, Total
29.5
0.993
mg/kg
'SW846 6010A
D
3/23/99
17:49
DH
Zinc, Total
88.8
0.993
mg/kg
SW846 6010A
D
3/23/99
17:49
DH
Mercury, Total
<0.25
0.1
mg/kg
SW846 7470A
D
3/17/99
14:10
ROBI
Selenium, Total
0.15
0.04
mg/kg
SW846 7741
D
3/31/99
15:00
DH
PCB
BDL
1.6
mg/kg
SW846 8080
S10
3/18/99
20:23
KLEP
Page 2
. CHAIN OF CUSTODY RECORD
Page J__ of
Client T Name / Facility Name.
rn
SAMPLE
ANALYSIS
REQUIRED
(x) -use
remarks
area
to
specify
specific
compounds
or methods
m
o
la
la
z
o
c
0.
o
y
c
A
a`
m
Col17ted By:, L
� "y
JAM
SAMPLE ID
DATE
TIME
3bo
0
1 - z
3.716- 9 p
it
3-4 =
T,T
_LL_
R7�sh y:
Date
Time
Receiv by
R/elinpplUl shed by.
/
Date
Time
o
Re !Ived y lab by:
r+'
* Program Area: N - NPDES, H.- Haz. Waste, D - Drinking Water, G - Groundwater, O. - Other, W - Waste Water
a .
DAVIS & BROWN-A.C.
P.O. Box 15038
Quinby, SC 29506
(803) 665-6746
2121 Black Creek Road
Florence, SC 29501
Use For Pin the boxes to indicate whether
sample wasfiltered and/orpreseraed.
Remarks
Lab ID
o /i i r'LGI I U
i6,
t/�rltl/cf�rr
r f -�l
Lf'
Relinquished by:
Date
Time
Received by:
Date
Time
Circle One
ICED YES NO
Remarks
-
State of North Carolina
Department ,of Environment,
Health and .Natural Resources
Division of Water Quality
James B. Hunt; Jr., Governor
Wayne McDevitt; Secretary
A. Preston Howard, Jr., P.E., Director
James T. Morris; Public Utility Director
Town of Cheraw
Post Office Box 111
Cheraw, South,Carolina 29520
Dear Mr. Morns:
August 15, 1997 1
AUG 2 0 1991
FAYETTEVILLE
REQ. 0FRCE
Subject: Permit No .WQ001=4248
To no f Chem., .
Distribution offass AWastewater Residuals
, f, - esterfreldyCoun South Carolina
In accordance with,your application received on August, 7, 1997; we are forwarding herewith
Permit No.,WQ0014248, dated August 15, 1997, to the Town of Cheraw for the distribution of Class A
residuals in North Carolina.
This permit shall be effective from'the date of issuance until July 31, 2002, and shall be subject to
the conditions, and limitations as specified therein. Please pay particular attention to the monitoring and,
reporting requirements contained in this permit.. Failure to establish an adequate: system for collecting, and
maintaining the required operational information will result in future 'compliance problems.
If any parts, requirements, or limitations contained in this permit are unacceptable, you. have the
right to request an adjudicatory hearing upon written request within thirty (30) days following receipt of
this permit. This request must be in the form of a written petition, conforming to Chapter 150B of North
Carolina General Statutes, and filed with the Office of Administrative Hearings, P.O. Drawer 27447,
Raleigh, NC 27611-7441. Unless such demands are made this permit shall be final and binding. -
If you, need additional information concerning this mattes;, please contact Mr. Michael D. Allen at
(919)' 733-5083 extension 547.' =
Sincerell
L
�A. Preston Howard, ,Jr., P.E.
cc: NCDWQ Regional Offices, Water Quality Section
Facilities Assessment Unit
P.O. Box, 29535, Raleigh-, North Carolina 2762&0535 • Telephone (919) 733-5083 FAX (919) 733-0719
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper
NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES
RALEIGH
PERMIT FOR THE DISTRIBUTION OF CLASS A RESIDUALS
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as
amended, and other applicable Laws, Rules, and Regulations
PERMISSION IS HEREBY GRANTED TO THE
Town of Cheraw
Chesterfield County, South Carolina
FOR THE
the distribution of up to 1,800 dry tons per year of Class A wastewater residuals in North Carolina from
the sources listed in Condition II 1, with no discharge of wastes to the surface waters, pursuant to the
application received on August 7, 1997, and in conformity with the project plan, specifications, and other
supporting data subsequently filed and approved by the Department of Environment, Health and Natural
Resources and considered a part of this permit.
This permit shall be effective from the date of issuance until July 31, 2002, and shall be subject to
the following specified conditions and limitations:
I. PERFORMANCE STANDARDS
1. The distribution of Class A residuals program shall be effectively maintained and operated
as a non -discharge system to prevent the discharge of any wastes resulting from the
operation of this program.
2. This permit shall become voidable in the event of failure of the residuals program to
adequately protect the assigned water quality standards of the surface waters and
groundwaters.
3. The issuance of this permit shall not relieve the Permittee of the responsibility for damages
to surface or groundwaters resulting from the operation of this program.
4. In the event that the residuals program is not operated satisfactorily, including the creation
of nuisance conditions, the Permittee shall take any immediate corrective actions as may be
required by the Division.
5. When wastewater residuals are sold or given away, one of the Class A pathogen
requirements in 40 CFR Part 503.32(a) and one of vector attraction reduction requirements
in 40 CFR Part 503.33 must be met. Additionally, an evaluation must be performed which
demonstrates the residuals ability to comply with this requirement. Upon request, a copy
of this evaluation must be submitted to the Assistant Chief, Technical Support Branch,
Division of Water Quality, Post Office Box 29535, Raleigh, NC 27626-0535.
II:
OPERATION AND MAINTENANCE REQUIREMENTS
1. No residuals .other than the following are hereby approved for distribution in accordance
with this permit:
Permit Volume
Source County Number (Dry Tons/Year)
Town of Cheraw Chesterfield, SC SCO020249 1,800
2. The finished product shall not be stored at, the land application sites unless it is placed on a
concrete pad, placed under shelter -or covered until such time as it is land applied. If an
alternate storage site is to be used, approval must be obtained from the Division of Water
Quality.
3. No other residuals other than those specified under Condition II 2 above may be
distributed. The Permittee shall request and obtain a permit amendment from the Division
of Water Quality for each additional residual source prior to acceptance of that residual.
4. For a Class A residual to be sold or given away in bags or other container for application to
the land, the following must be satisfied:
The Ceiling Concentrations (Dry Weight Basis) and the Pollutant Mon_ thly
Average Concentrations (Dry Weight Basis) must .be maintained:
Ceiling Monthly Average
Concentrations Concentrations
Parameters mg/kg mg/kg
Arsenic
75
41
Cadmium
85
39
Copper
4,300
1,500
Lead
846
300
Mercury
57
17
Molybdenum
75
----
Nickel
420
420
Selenium
100
100
Zinc
7,500
2,800
5. Adequate provisions shall be taken to prevent wind erosion and surface runoff from
conveying pollutants from the residuals treatment area onto the adjacent property or into
any surface waters.
6. A label shall be affixed to the bag or other container in which residuals that are sold or
given away for application to the land, or an information sheet shall. be provided to the
person who receives the residuals sold or given away in an other container for application
to the land. The label or information sheet shall contain the following information:
a. The name and address of the person who prepared the residuals that is sold or given
away in a bag or other container for application .to the land.
b. A statement -that application of the residuals to the land is. prohibited except in
accordance with the instructions on the label or information sheet.
C. A statement which identifies that this material shall be prevented from entering any
public or private water supply source (including wells) and -any stream, lake, or river.
d. Residuals shall not be applied to. any site that is flooded, frozen or snow-covered.
K
e Adequate procedures shall be provided to prevent surface runoff from carrying any
disposed or stored residuals into any surface waters.
MONITORING AND REPORTING REQUIREMENTS
1. Any monitoring (including groundwater, surface water, residuals, soil, or plant tissue
analyses) deemed necessary by the Division of Water Quality to insure protection of the
environment will be established and an acceptable sampling and reporting schedule shall be
followed.
2. Proper records shall be maintained by the Permittee tracking all residual activities. These
records shall include, but are not necessarily limited to the following information:
a. source, volume and analysis of each residuals
b. name of residuals' recipient, volume received, and intended use
3. A residual analysis shall be conducted annually from the date of permit issuance by the
Permittee. The results of all analysis shall be maintained on file by the Permittee for a
minimum of five years. The residuals analysis shall include the following parameters:
Arsenic
Molybdenum
Cadmium
Nickel
Copper
Selenium
Lead
Zinc
Mercury
Aluminum
pH
Ammonia -Nitrogen
Phosphorus
Calcium
Plant Available Nitrogen (by calculation)
Magnesium
Potassium
Nitrate -Nitrite Nitrogen
Sodium
% Total Solids
TKN
4. A Toxicity Characteristics Leaching Procedure (TCLP) analysis shall be conducted by the
Permittee annually. The TCLP analysis shall include the following parameters (please note
the regulatory level in mg/L in parentheses):
Arsenic (5.0)
Benzene (0.5)
Carbon tetrachloride (0.5)
Chlorobenzene(100.0)
Chromium (5.0)
m-Cresol (200.0)
Cresol (200.0)
1,4-Dichlorobenzene (7.5)
1,1-Dichloroethylene (0.7)
Endrin (0.02)
Hexachlorobenzene (0.13)
Hexachloroethane (3.0)
Lindane (0.4)
Methoxychlor (10.0)
Nitrobenzene (2.0)
Pyridine (5.0)
Silver (5.0)
Toxaphene (0.5)
2,4,5-Trichlorophenol (400.0)
2,4,5-TP (Silvex) (1.0)
Barium (100.0)
Cadmium (1.0)
Chlordane (0.03)
Chloroform (6.0)
o-Cresol (200.0)
p-Cresol (200.0)
2,4-D (10.0)
1,2-Dichloroethane (0.5)
2,4-Dinitrotoluene (0.13)
Heptachlor (and its hydroxide) (0.008)
Hexachloro-1,3-butadiene (0.5)
Lead (5.0)
Mercury (0.2)
Methyl ethyl ketone (200.0)
Pentachlorophenol (100.0)
Selenium (1.0)
Tetrachloroethylene (0.7)
Trichloroethylene (0.5)
2,4,6-Trichlorophenol (2.0)
Vinyl chloride (0.2)
3
5. All residuals included in this permit must be monitored annually, from the date of permit
issuance, for compliance with condition 19 of this permit. Data to verify stabilization of
the residuals must be maintained by -.the Permittee. The required data is specific'to the
stabilization process, utilized, but should be sufficient to clearly demonstrate compliance
with the Class A pathogen requirements in 40 CFR Part 503.32(a) and the vector attraction
reduction requirements in 40 CFR Part 503.33. In addition, -the EPA. certification
statements concerning compliance with pathogen requirements, vector attraction reduction
requirements and management practices must be completed annually by the proper authority
or authorities if more than one is involved, either the person who generates the residuals or
the person who prepares the residuals to be sold or given away.
6. Three copies, of all required monitoring and reporting requirements as'specified in
conditions 1111, III 2,1113;11I 4, and III 5 shall be submitted annually on or before March
1 of the "following year to the following address:
NC Division of Water Quality
Water Quality Section ,
Facility Assessment Unit
PO Box 29535
Raleigh, NC 27626-0535
7. Noncompliance Notification:
The Permittee 'shall report by telephone to the appropriate DWQ Regional Office (as
outlined in attachment 1) as soon -as possible, but in no case more than 24 hours or on the
next working day following the occurrence or first knowledge of the occurrence of any of
the following:
a. Any occurrence with the distribution program which results -in the land application of
significant amounts of wastes which are, abnormal in quantity, or characteristic.
b. Any failure of the distribution program resulting in a release of material to receiving
waters.
c. Any time that self -monitoring information indicates that the facility has gone out of
compliance with the conditions and limitations of this permit or the parameters on
which the system was designed.
d. Any process unit failure, due to known or unknown reasons, that render the facility
incapable of adequate residual treatment.
e. Any spillage or discharge from a vehicle or piping system during transportation of
residuals.
Persons reporting such occurrences by telephone shall also file''a written report in letter
form within five (5) days following first knowledge of the'occurrence. This report must
outline the actions taken or proposed to be taken to ensure that the problem does not recur.
IV. INSPECTIONS
1. Any duly authorized officer, employee, or representative of the Division of Water Quality'
may, upon presentation of credentials, enter and inspect any property, premises or place on
or related to the treatment site or facility at any .reasonable time for the purpose of
determining compliance with this permit; may inspector copy any records that must be kept
under the" terms and conditions of this permit; and may obtain samples of groundwater,
surface .water, or.leachate.'
4
2. The Permittee or his designee shall inspect the residuals storage, transport, and treatment
facilities to prevent malfunctions and deterioration, operator errors and discharges which
may cause or lead to the release of wastes to the environment, a threat to human health, or a
nuisance. The Permittee shall maintain an inspection log or summary including at least the
date and time of inspection, observations made, and any maintenance, repairs, or corrective
actions taken by the Permittee. This log of inspections shall be maintained by the Permittee
for a period of five years from the date of the inspection and shall be made available to the
Division of Water Quality or other permitting authority, upon request.
V . GENERAL CONDITIONS
1. This permit shall become voidable unless the distribution activities are carried out in
accordance with the conditions of this permit, the supporting materials, and in the manner
approved by this Division:
2. This permit is effective only with respect to the nature and volume of residuals described in
the application and other supporting data.
3. This permit is not automatically transferable. In the event that there is a desire for the
facilities to change ownership or a name change of the Permittee, a formal permit request
must be submitted to the Division of Water Quality accompanied by an application fee,
documentation from the parties involved, and other supporting materials as may be
appropriate. The approval of this request will be considered on its merits and may or may
not be approved.
4. Failure to abide by the conditions and limitations contained in this permit may subject the
Permittee to an enforcement action by the Division of Water Quality in accordance with
North Carolina General Statute 143-215.6(a) to 143-215.6(c).
5. The annual administering and compliance fee must be paid by the Permittee within thirty
(30) days after being billed by the Division. Failure to pay the fee accordingly may cause
the Division to initiate action to revoke this permit as specified by 15 NCAC 2H .0205
(c)(4).
6. The issuance of this permit does not preclude the Permittee from complying with any and
all statutes, rules, regulations, or ordinances which may be imposed by other government
agencies (local, state, and federal) which have jurisdiction.
7. The Permittee, at least six (6) months prior to the expiration of this permit, shall request its
extension. Upon receipt of the request, the Commission will review the adequacy of the
facilities described therein, and if warranted, will extend the permit for such period of time
and under such conditions and limitations as it may deem appropriate.
8. This permit may be modified, or revoked and reissued to incorporate any conditions,
limitations and monitoring requirements the Division of Water Quality deems necessary in
order to adequately protect the environment and public health.
Permit issued this the fifteenth day of August, 1997
NORTH C INA ENAOAL MANAGEMENT COMMISSION
Preston Howard, Jr., P.E., Director
Division of Water Quality
By Authority of the Environmental Management Commission
Permit Number WQ0014248
5
ATTACHMENT 1
DIVISION OF WATER QUALITY REGIONAL OFFICES
Asheville Regional' WQ Supervisor
59'Woodfin Place
Asheville, NC 28801
(704)25.1-6208
Fax (704) 251-6098
Avery
Macon
Buncombe
Madison
Burke
McDowell
Caldwell
Mitchell
Cherokee
Polk
Clay
Rutherford
Graham
Swain
Haywood
Transylvania
Henderson
Yancy
Jackson
Fayetteville Regional WQ Supervisor
Wachovia Building, Suite 714
Fayetteville, NC 28301
(910)486-1541
Fax (9,10) 486-0707
Anson Moore
Bladen Robeson
Cumberland Richmond
Harnett Sampson
Hoke Scotland
Montgomery
Winston-Salem Regional WQ Supervisor
585 Waughtown Street
Winston-Salem, NC 27107
(910)771-4600
Fax (910)771-4631
Alamance Rockingham
Alleghany Randolph
Ashe Stokes
Caswell Surry
Davidson Watauga
Davie Wilkes
Forsyth Yadkin
Guilford
Washington Regional WQ Supervisor
943 Washington Square Mall
Washington, NC 27889_
(919) 946-6481
Fax (919) 975-3716
Beaufort Jones
Bertie Lenoir
CamdenMartin
Chowan Pamlico
Craven Pasquotank
Cumtuck Perquimans
Dare . Pitt
Gates Tyrell
Greene Washington
Hertford Wayne
Hyde
Mooresville Regional WQ Supervisor
919 North Main Street
Mooresville, NC 28115
(704).663-1.699
Fax (704).663-6040
Alexander
Lincoln
Cabarrus
Mecklenburg
Catawba
Rowan
Cleveland
Stanly
Gaston
Union
Iredell-
Raleigh Regional.WQ Supervisor
Post Office Box 27687
Raleigh, NC 27611
(919) 571-4700
Fax (919) 571-4718
Chatham Nash
Durham Northampton
Edgecombe Orange
Franklin Person
Granville Vance
Halifax Wake
Johnston Warren
Lee Wilson
Wilmington Regional WQ Supervisor
127 Cardinal Drive Extension
Wilmington, NC 2840.5-3845
(910) 395-3900
Fax (910)350-2004
Brunswick New Hanover
Carteret Onslow
Columbus Pender
Duplin '.
Electronic Code of Federal Regulations (e-CFR) (e-CFR Data is current as of March 20,,2007
J ...
Title 40: Protection of Environment
PART 503-STANDARDS FOR THE USE OR DISPOSAL OF SEWAGE SLUDGE
Section Contents
Subpart A-General'Provisions
§ 503.1 . Purpose and applicability.
§ 503.2 Compliance period.
§ 503.3 Permits and direct enforceability.
§ 503.4 .Relationship to other regulations.
§ 503; 5 Additional or more stringent requirements.
§ 503.6. Exclusions.,
§ 503.7 Requirement for a person who prepares'sewage sludge.
§ 503.8 Sampling and analysis.
§ 503.9 General -definitions.
Subpart B=Land Application
§ 503.10 Applicability,.
§ 503.11 Special definitions.
§ 503.12 General requirements-.
§ 503.13 Pollutant limits.
§ 503.14 Management practices.
§ 503.15 Operational standards -pathogens and vector, attraction reduction.
§ 503.16 Frequency of monitoring.
§ 503.17 Recordkeeping.
§ 503.18 Reporting.
Subpart C=Surface Disposal
§ 503.20 Applicability.
§ 503.21 Special definitions.
§ 503.22 General requirements.
§ 503.23 Pollutant limits_ (other than domestic septage).
§ 503.24 Management practices.
§ 503.25 Operational standards -pathogens and vector attraction reduction.
§ 503.26 Frequency of monitoring.
§ 503.27 Recordkeeping.
§ 503.28 Reporting.
Subpart D-Pathogens and Vector Attraction Reduction
§ 503.30 Scope'.
§ 503.31 Special definitions.'
§ 503.32 Pathogens.
§ 503.33 Vector attraction reduction.
Subpart E-Incineration
§ 503.40 Applicability.
§ 503.41 Special definitions.
§ 50142 General requirements.
§ 503.43 Pollutant limits.
§ 503.44 Operational standard -total hydrocarbons.
§ 503,45 Management practices.
§ 503.46 Frequency of monitoring.
§ 503.47 Recordkeeping.
§ 503-48 Reporting.
Appendix A to Part 503=Procedure To Determine the Annual Whole Sludge Application Rate for a Sewage
Sludge
Appendix B to Part 503-Pathogen Treatment Processes
a
V
PART 503—STANDARDS FOR THE USE OR DISPOSAL OF SEWAGE SLUDGE
Authority: Sections 405 (d) and (e) of the Clean Water Act, as amended by Pub. L. 95-217, sec. 54(d), 91
Stat. 1591 (33 U.S.C. 1345 (d) and (e)); and Pub. L. 100-4, title IV, sec. 406 (a), (b), 101 Stat., 71, 72 (33
U.S.C. 1251 et seq. ).
Source: 58 FR 9387, Feb. 19, 1993, unless otherwise noted.
Subpart A —General Provisions
§ 503.1 Purpose and applicability.
(a) Purpose. (1) This part establishes standards, which consist of general requirements, pollutant limits,
management practices, and operational standards, for the final use or disposal of sewage sludge generated
during the treatment of domestic sewage in a treatment works. Standards are included in this part for sewage
sludge applied to the land, placed on a surface disposal site, or fired in a sewage sludge incinerator. Also
included in this part are pathogen and alternative vector attraction reduction requirements for sewage sludge
applied to the land or placed on a surface disposal site.
(2) In addition, the standards in this part include the frequency of monitoring and recordkeeping requirements
when sewage sludge is applied to the land, placed on a surface disposal site, or fired in a sewage sludge
incinerator. Also included in this part are reporting requirements for Class I sludge management facilities,
publicly owned treatment works (POTWs) with a design flow rate equal to or greater than one million gallons
per day, and POTWs that serve 10,000 people or more.
(b) Applicability. (1) This part applies to any person who prepares sewage sludge, applies sewage sludge to
the land, or fires sewage sludge in a sewage sludge incinerator and to the owner/operator of a surface
disposal site.
(2) This part applies to sewage sludge applied to the land, placed on a surface disposal site, or fired in a
sewage sludge incinerator.
(3) This part applies to the exit gas from a sewage sludge incinerator stack.
(4) This part applies to land where sewage sludge is applied, to a surface disposal site, and to a sewage
sludge incinerator.
§ 503.2 Compliance period.
(a) Compliance with the standards in this part shall be achieved as expeditiously as practicable, but in no
case later than February 19, 1994. When compliance with the standards requires construction of new
pollution control facilities, compliance with the standards shall be achieved as expeditiously as practicable,
but in no case later than February 19, 1995.
(b) The requirements for frequency of monitoring, recordkeeping, and reporting in this part for total
hydrocarbons in the exit gas from a sewage sludge incinerator are effective February 19, 1994 or, if
compliance with the operational standard for total hydrocarbons in this part requires the construction of new
pollution control facilities, February 19, 1995.
(c) All other requirements for frequency of monitoring, recordkeeping, and reporting in this part are effective
on July 20, 1993.
(d) Unless otherwise specified in subpart E, compliance with the requirements in §503.41(c) through (r),
503.43(c), (d) and (e), 503.45(a)(1), (b) through (f), 503.46(a)(1), (a)(3), and (c), and 503.47(f) that were
revised on September 3, 1999 shall be achieved as expeditiously as practicable, but in no case -later than
-September 5, 2000. When new pollution control facilities must be constructed to comply with the revised
requirements in subpart.E, compliance with the revised requirements shall be achieved as expeditiously as
practicable but no later than September 4, 2001. '
[58 FR 9387, Feb. 19, 1993, as amended at 64 FR 42568, Aug. 4, 19991
§ 503.3 Permits and direct enforceability.
(a) Permits. The requirements in this part may be implemented through a permit:
(1) Issued to a "treatment works treating domestic sewage", as defined in 40.CFR 122.2, in accordance with
40 CFR parts 122 and 124 by EPA or by a State that has a State sludge management program approved by
EPA in accordance with 40 CFR part 123 or 40 CFR part 501 or
(2) Issued under subtitle C of the Solid Waste Disposal Act; part C of the Safe Drinking Water Act; the Marine
Protection, Research, and Sanctuaries Act of 1972; or the Clean Air Act. "Treatment works treating domestic
sewage" shall submit a permit application in accordance with either 40 CFR 122.21 or an approved State
program.
(b) Direct. enforceability. No person -'shall use or dispose of sewage sludge through any practice for which
requirements are established' in this part except in accordance with such requirements.
§ 503.4 Relationship to other regulations.
Disposal of sewage sludge in a municipal solid waste landfill unit, as defined in 40 CFR 258.2, that complies
with the requirements in 40 CFR part 258 constitutes compliance with section 405(d) of the CWA. Any person
who prepares sewage, sludge that, is disposed in a municipal solid waste landfill unit shall ensure that the
sewage sludge. meets the"requirements in 40 CFR part 258,concerning the quality of materials . disposed- in a
municipal solid waste landfill- unit.
§ 503.5 Additional or more stringent requirements.
(a) On a case -by -case basis, the permitting authority may impose requirements for the use or disposal.of
sewage sludge in addition to or more stringent than the requirements ih.this part when necessary'to protect
public health and the environment from any adverse effect of a pollutant in the sewage sludge.
(b) Nothing in this part precludes a State or political subdivision thereof or interstate agency from imposing
`requirements for the use or disposal of sewage sludge more stringent than the requirements in this part or
from imposing additional requirement's for the use or disposal of sewage sludge.
§ 503.6 Exclusions.
(a) Treatment processes. This part does not establish requirements for processes:used to treat domestic
sewage or for processes used to treat sewage sludge prior to final use or disposal, except as provided "in,
§503.32 and §503.33.
(b) Selection of'a use or disposal practice. This part does not require the selection of a sewage sludge -,use or
disposal practice. The determination of the manner in which sewage sludge is used or disposed is a local
determination.
(c) Co -firing of sewage sludge.'This part does not establish requirements for sewage,sludge co -fired in an
incinerator with other wastes or for the incinerator in which sewage sludge and -other wastes are co -fired.
Other wastes do not include auxiliary fuel, as defined in 40 CFR 503.41(b), fired in a sewage sludge
incinerator.
(d) Sludge generated at an industrial facility: This part does not establish requirements for the use or disposal
of sludge generated at an industrial facility during the treatment of industrial wastewater, including sewage
sludge generated during -the treatment of industrial wastewater combined with domestic sewage.
(e) Hazardous sewage sludge. This part- does not establish requirements for the use or disposal of sewage
sludge determined to be hazardous in accordance with 40 CFR'part 261.
(f) Sewage sludge with high PCB concentration. This part does not establish requirements for the use or
disposal of sewage sludge with a concentration of polychlorinated biphenyls (PCBs) equal to or greater than
50 milligrams per kilogram of total solids (dry weight basis).
(g) Incinerator ash. This part does not establish requirements for the use or disposal of ash generated during
the firing,of sewage sludge in a sewage sludge incinerator.
(h) Grit and screenings. This part does not establish requirements for the use or disposal of grit (e.g., sand,
gravel, cinders, or other materials with'a high specific gravity) or screenings (e.g., relatively large materials
such as rags) generated during preliminary treatment of domestic sewage in a treatment works.
(i) Drinking water"treatment sludge. This part does not establish requirements, for the use or disposal of
sludge generated during the treatment'of either'surface water or ground water used for drinking water.
0) Commercial and industrial septage. This part does�not establish requirements forthe use or disposal of
commercial septage, industrial septage, a mixture of domestic septage and commercial, septage, or a mixture
of domestic septage and industrial septage.
§ 503.7 Requirement for a person who prepares sewage sludge..,
Any person who prepares sewage sludge shall ensure that the applicable requirements in this.part are met
when the sewage sludge is applied to the land, placed on a surface disposal site, or fired in a sewage sludge
incinerator,
§ 503.8 Sampling and analysis.
(a) Sampling. Representative samples of sewage sludge that is applied to the land, placed on a surface
disposal site, or fired in a sewage sludge incinerator shall be collected and analyzed.
(b) Methods. The materials listed below are incorporated by reference in this part.. These incorporations by
reference were approved by the Director of the Federal Register in accordance with 5 U.S.C. 552(a) and 1
CFR part 51. The materials are incorporated as they exist on the date of approval, and notice of any change
in these materials will be published in theFederal Register.They are available for inspection at the Office of
Water Docket, room L-102, U.S. Environmental Protection Agency, 401 M St., SW., Washington, DC, and at
the National Archives and Records Administration (NARA). For information on the availability of this material
at NARA, call 202-741-6030, or go to:
http://www.archives.gov/federal_register/code of federal_regulations/ibr locations.html. Copies may be
obtained from the standard producer or publisher listed in the regulation. Methods in the materials listed
below shall be used to analyze samples of sewage sludge.
(1) Enteric viruses. ASTM Designation: D 4994-89, "Standard Practice for Recovery of Viruses From
Wastewater Sludges", 1992 Annual Book of ASTM Standards: Section 11—Water and Environmental
Technology, ASTM, 1916 Race Street, Philadelphia, PA 19103-1187.
(2) Fecal coliform. Part 9221 E. or Part 9222 D., "Standard Methods for the Examination of Water and
Wastewater", 18th Edition, 1992, American Public Health Association, 1015 15th Street, NW., Washington,
DC 20005.
(3) Helminth ova. Yanko, W.A., "Occurrence of Pathogens in Distribution and Marketing Municipal Sludges",
EPA 600/1-87-014, 1987. National Technical Information Service, 5285 Port Royal Road, Springfield,
Virginia 22161 (PB 88-154273/AS).
(4) Inorganic pollutants. "Test Methods for Evaluating Solid Waste, Physical/Chemical Methods", EPA
Publication SW-846, Second Edition (1982) with Updates I (April 1984) and II (April 1985) and Third Edition
(November 1986) with Revision I (December 1987). Second Edition and Updates I and II are available from
the National Technical Information Service, 5285 Port Royal Road, Springfield, Virginia 22161 (FB-87-120-
291). Third Edition and Revision I are available from Superintendent of Documents, Government Printing
Office, 941 North Capitol Street,, NE., Washington, DC 20002 (Document Number 955-001-00000-1).
(5) Salmonella sp. bacteria. Part 9260 D., "Standard Methods for the Examination of Water and Wastewater",
18th Edition, 1992, American Public Health Association, 1015 15th Street, NW., Washington, DC 20005; or
Kenner, B.A. and H.P. Clark, "Detection and enumeration of Salmonella and Pseudomonas aeruginosa
Journal of the Water Pollution Control Federation, Vol. 46, no. 9, September 1974, pp. 2163-2171. Water
Environment Federation, 601 Wythe Street, Alexandria, Virginia 22314.
(6) Specific oxygen uptake rate. Part 2710 B., "Standard Methods for the Examination of Water and
Wastewater", 18th Edition, 1992, American Public Health Association, 1015 15th Street, NW., Washington,
DC 20005.
(7) Total, fixed, and volatile solids. Part 2540 G., "Standard Methods for the Examination of Water and
Wastewater", 18th Edition, 1992, American Public Health Association, 1015 15th Street, NW., Washington,
DC 20005.
[58 FR 9387, Feb. 19, 1993, as amended at 69 FR 18803, Apr. 9, 2004]
§ 503.9 General definitions.
(a) Apply sewage sludge or sewage sludge applied to the land means land application of sewage sludge.
(b) Base flood is a flood that has a one percent chance of occurring in any given year ( i.e. , a flood with a
magnitude equalled once in 100 years).
(c) Class I sludge management facility is any publicly owned treatment works (POT", as defined in 40 CFR
501.2, required to have an approved pretreatment program under 40 CFR 403.8(a) (including any POTW
located in a State that has elected to assume local program responsibilities pursuant to 40 CFR 403.10(e))
and any treatment works treating domestic sewage, as defined in-40 CFR 122.2, classified as a Class I
sludge management facility by the EPA Regional Administrator, or, in the case of approved State programs,
the Regional Administrator in conjunction with the State Director, because of the potential for its sewage
sludge use or disposal practice to affect public health and the environment adversely.
(d)Cover crop is a small grain crop, such as oats, wheat, or barley, not grown for harvest.
(e) CWA means the Clean Water Act (formerly referred to as either the Federal Water Pollution Act or the
Federal Water Pollution Control Act Amendments of 1972), Public Law 92-500, as amended by Public Law
95-217, Public Law 95-576, Public Law 96-483, Public Law 97-117, and Public Law 10d-4.
(f) Domestic septage is either liquid or solid material removed from, a septic tank, cesspool, portable toilet,
Type III marine sanitation device, or similar treatment works that receives only domestic sewage. Domestic
septage does not include liquid or solid material removed from a septic tank, cesspool, or similar treatment
works that receives either commercial wastewater or industrial wastewater and does not include grease
removed .from a grease trap at a restaurant.
(g) Domestic sewage is waste and wastewater from humans or household operations that is discharged to or
otherwise enters a treatment works.'
(h) Dry weight basis means calculated on the basis of having been dried at 105 degrees Celsius until''
reaching a constant mass ( i.e. , essentially 100 percent solids content).
(i) EPA'means the United States Environmental Protection Agency.
(j) Feed crops are crops produced primarily for consumption by animals.
(k) Fiber crops are crops such as flax and cotton.
(1) Food crops 'are crops consumed by humans. These include, but are not limited to, fruits, vegetables, and
tobacco:
(m) Ground water is water below the land surface in the saturated zone.
(n)"Industrial.wa"stewater is wastewater generated in a commercial or industrial process.
(o) Municipality means a city,, town; borough, county, parish, district, association, or other public body
(including an, intermunicipal Agency of two or more of the foregoing entities) created by or under State law; an
Indian tribe or an authorized Indian tribal organization having jurisdiction over sewage sludge management; or
a designated and -approved management Agency under section 208 of the CWA, as amended, The definition
includes a special district created.under State law,.such as a water district, sewer district, sanitary'district,
utility district, drainage district, or similar entity, or an integrated waste management facility as defined in -
section 201(e) of the CWA, as amended, that has as one of its principal responsibilities the treatment,
transport, use,' or disposal of sewage sludge.
(p) Permitting authority is either EPA or a State with an EPA -approved sludge management program.
(q) Person is an individual, association, partnership, corporation, municipality, State or Federal agency, or an
agent or employee thereof.
(r) Person who prepares sewage sludge is either the person who, generates sewage sludge during the
treatment of domestic sewage in a treatment works or -the person who derives a material from sewage sludge.
(s) Place sewage sludge or sewage sludge placed means disposal of sewage sludge on a surface, disposal
site-.
(t) Pollutant is an organic substance, an inorganic substance, a combination of organic.and inorganic
substances, or a pathogenic organism that, after discharge and upon exposure, ingestion, inhalation, or
assimilation into an organism either directly from the environment or indirectly by' ingestion through the food
chain, could, on the basis of information available to the Administrator of EPA, cause death, disease' .
behavioral abnormalities, cancer, genetic mutations, physiologicalmalfunctions (including malfunction in
reproduction),` or physical deformations in either organisms or,offspring of the organisms.
(u) Pollutant limit is a numerical value,that describes the amount of a pollutant allowed per unit'amount of
sewage sludge (e.g., milligrams. per kilogram of total solids); the amount of a pollutant that can be applied -to a
unit area of land (e.g.; kilograms per hectare); or the volume of a material that can be applied to a unit area of
land (e.g., gallons per acre).
(v) Runoff is rainwater, leachate, or other liquid that drains overland on any part of a land surface and runs off
of the land surface.
(w) Sewage sludge is solid, semi -solid, or liquid residue generated during the treatment of domestic sewage
in a treatment'works. Sewage, sludge includes, but is not limited to, domestic se, ptage; scum or solids
removed in primary, secondary, or advanced wastewater treatment processes; and a material derived from
sewage sludge. Sewage sludge does not include ash generated during the firing of sewage sludge-in.'a , .
sewage sludge incinerator or grit and screenings generated during preliminary treatment of domestic` sewage
in a treatment works.
(x) State is one'of the United States of America, the District of Columbia, the Commonwealth of Puerto Rico,
the Virgin Islands, Guam, American Samoa, the Trust Territory of the Pacific Islands', the Commonwealth of
the Northern Mariana Islands, and an Indian Tribe eligible for treatment as a State: pursuant to regulations
promulgated, under the authority of section 518(e) of the CWA.
(y) Store or storage of sewage sludge is the placement of sewage sludge on land on which the sewage
sludge remains for two years -or less. This does not include the placement of sewage sludge on land for
treatment.
(z) Treat or treatment of sewage sludge is the preparation of sewage sludge for final use or disposal. This
includes, but is not limited to, thickening, stabilization, and dewatering of sewage sludge. This does -not
include storage of sewage sludge.
(aa) Treatment works is either a federally owned, publicly owned, or privately owned device or system used to
treat (including recycle and reclaim) either domestic sewage or a combination of domestic sewage and
industrial waste of a liquid nature.
(bb) Wetlands means those areas that are inundated or saturated by surface water or ground water at'a
frequency and duration to support, and that under normal circumstances do support, a prevalence bf
vegetation typically adapted for life in saturated soil conditions. Wetlands generally include swamps, marshes,
bogs, and similar areas.
Subpart B-Land Application
§ 503.10 Applicability.
(a) This subpart applies to any person who prepares sewage sludge that is applied to the land, to `any person
who applies sewage sludge to the land, to sewage sludge applied to the land, and to the land on which
sewage sludge is applied.
(b)(1) Bulk sewage sludge. The general requirements in §503.12 and the management practices in §503.14
do not apply when bulk sewage sludge is applied to the land if the bulk sewage sludge meets the ceiling
concentrations in Table 1 of §503.13 and the pollutant concentrations in Table 3 of §503.13; the Class A
pathogen requirements in §503.32(a); and one of the vector attraction reduction requirements in
§503.33(b)(1) through (b)(8).
(2) The Regional Administrator of EPA or, in the case of a State with an approved sludge management
program, the State Director, may apply any or all of the general requirements in §503.12 and the
management practices in §503.14 to the bulk sewage sludge in §503.10(b)(1) on a case -by -case basis after
determining that the general requirements or management practices are needed to protect public health and
the environment from any reasonably anticipated adverse effect that may occur from any pollutant in the bulk
sewage sludge.
(c)(1) The general requirements in §503.12 and the management practices in §503.14 do not apply when a
bulk material derived from sewage sludge is applied to the land if the derived bulk material meets the ceiling
concentrations in Table 1 of §503.13 and the pollutant concentrations in Table 3 of §503.13; the Class A
pathogen requirements in §503.32(a); and one of the vector attraction reduction requirements in
§503.33(b)(1) through (b)(8).
(2) The Regional Administrator of EPA or, in the case of a State with an approved sludge management
program, the State Director, may apply any or all of the general requirements in §503.12 or the management
practices in §503.14 to the bulk material in §503.10(c)(1) on a case -by -case basis after determining that the
general requirements or management practices are needed to protect public health and the environment from
any reasonably anticipated adverse effect that may occur from any pollutant in the bulk sewage sludge.
(d) The requirements in this subpart do not apply when a bulk material derived from sewage sludge is applied
to the land if the sewage sludge from which the bulk material is derived meets the ceiling concentrations in
Table 1 of §503.13 and the pollutant concentrations in Table 3 of §503.13; the Class A pathogen
requirements in §503.32(a); and one of the vector attraction reduction requirements in §503.33(b)(1) through
(b)(8)•
(e) Sewage sludge sold or given away in a bag or other container for application to the land. The general
requirements in §503.12 and the management practices in §503.14 do not apply when sewage sludge is sold
or given away in a bag or other container for application to the land if the sewage sludge sold or given away in
a bag or other container for application to the land meets the ceiling concentrations in Table 1 of §503.13 and
the pollutant concentrations in Table 3 of §503.13; the Class A pathogen requirements in §503.32(a); and one
of the vector attraction reduction requirements in §503.33(b)(1) through (b)(8).
(f) The general requirements in §503.12 and the management practices in §503.14 do not apply when a
material derived from sewage sludge is sold or given away in a bag or other container for application to the
land if the derived material meets the ceiling concentrations in Table 1 of §503.13 and the pollutant
concentrations in Table 3 of §503.13; the Class A pathogen requirements in §503.32(a); and one of the vector
attraction reduction requirements in §503.33(b)(1) through (b)(8). _
(g) The requirements in this subpart do not apply when a material derived from sewage sludge is sold or
given away in a bag or other container for application to the land if the sewage sludge from which the material
is derived meets the ceiling concentrations in Table 1 of §503.13 and the pollutant concentrations in Table 3
of §503.13; the Class A pathogen requirements in §503.32(a); and one of the vector attraction reduction
requirements in §503.33 (b)(1) through (b)(8).
[58 FR 9387, Feb. 19, 1993,. as amended at 64 FR 42568, Aug. 4, 1999]
§ 503.11 Special definitions.
(a) Agricultural land is land on which a food crop, a feed crop, or a fiber crop is grown. This includes range
land and land used as pasture.
(b) Agronomic rate is the whole sludge application rate (dry weight basis) designed:
(1) To provide the amount of nitrogen needed by the food crop, feed crop, fiber crop, cover crop, or vegetation
grown on the land; and
(2) To minimize the amount of nitrogen in the sewage sludge that passes below the root zone of the.crop or
vegetation grown on the land to the. ground water.
(c) Annual pollutant loading rate is the maximum amount of a pollutant that can be applied to a unit area of -
land during a 365 day period.
(d) Annual whole sludge application rate is the maximum amount of sewage sludge (dry weight basis): that
can be applied to a unit area of land during a 365 day period.
(e) Bulk sewage sludge is sewage sludge that is not sold or given away in a bag or other container:for'`'
application to the land.
(f) Cumulative pollutant loading rate is the maximum amount of an inorganic pollutant that can be applied to
an area of land.
(g) Forest is a tract of land thick with trees and underbrush.
(h) Land application is the spraying or spreading of sewage sludge onto the land surface; the injection of
sewage sludge.below the land surface; or the incorporation of sewage sludge into the soil so that the sewage
sludge can either condition the soil or fertilize crops or vegetation grown in the soil.
(i) Monthly average is the arithmetic mean of all measurements taken during the month.
0) Other container is either an open or closed receptacle. This includes, but is not limited to, a bucket; a box,
a carton, and a vehicle or trailer with a load capacity of one metric ton or less.
(k) Pasture is land on which animals feed directly on feed crops such as legumes, grasses, grain stubble,: or
stover.
(1) Public contact site is land with a high potential for'contact by the'public. This includes, but is not limited to,
public parks, ball fields, cemeteries, plant nurseries, turf farms, and golf courses.
(m) Range land is open land with indigenous vegetation.
(n) Reclamation site is drastically disturbed land that is reclaimed using sewage sludge. This includes, but is
not limited to, strip mines and construction sites.
§ 503.12 General requirements. .
(a) No person shall apply sewage sludge to the land except in accordance with the requirements in this
subpart.
(b) No person shall apply bulk sewage sludge subject to the cumulative pollutant loading rates in
§503.13(b)(2) to agricultural land, forest, a public contact site, or a reclamation site if any of the cumulative
pollutant loading rates in §503.13(b)(2) has been reached.
(c) No person shall apply domestic septage to agricultural land, forest, or a reclamationsite during a 365 day
period if the annual application rate in §503.13(c) has been reached during that period.
(d) The person who prepares bulk sewage sludge that is applied to agricultural land, forest, a public contact
site, or a reclamation site shall provide the person who applies the bulk sewage sludge written notification of
the concentration of total nitrogen (as N on a dry weight basis) in. the bulk sewage sludge.
(e)(1) The person who applies sewage sludge to the land shall obtain information needed to comply with the
requirements in this subpart.
(2)(i) Before bulk sewage sludge subject to the cumulative pollutant loading rates,i,n §503.13(b)(2) is applied
to -the land, the person who proposes to apply the bulk sewage sludge shall contact the permitting authority
for the State in;which the bulk sewage sludge will be applied to determine whether bulk sewage sludge
subject to the cumulative pollutant loading rates in §503.1.3(b)(2) has been applied to the site since July 20,
1993.
(ii) If bulk sewage sludge subject to the cumulative pollutant loading rates in §503.13(b)(2) has not been
applied to the site since July 20, 1993, the cumulative amount for each pollutant listed in Table 2 of §503.13
may be applied to the site in accordance with-§503.13(a)(2)(i).
(iii) If bulk sewage sludge subject to'the cumulative pollutant loading rates in §503.13(b)(2) has been applied
to the site since July'20, 1993, and the cumulative amount of each pollutant applied to the site in the bulk
sewage' sludge since that .date .is known, the cumulative amount of each pollutant applied to the site shall be,
used to determine the additional amount of each pollutant that can be applied to the site in accordance with
§503.13(a)(2)(i).
(iv) If bulk sewage sludge subject to. the cumulative pollutant loading rates in §503.13(b)(2) has been applied
to the site since July 20, 1993, and the cumulative amount of each pollutant applied to the site in the bulk
sewage sludge since that date is not known, an additional amount of each pollutant shall not be applied to the
site in accordance with §503.1-3(a)(2)(i).
(f) When a person who prepares bulk sewage sludge provides the bulk sewage sludge to a person who .
applies the bulk sewage sludge to the land, the person who prepares the bulk sewage sludge shall provide
the person who applies the sewage sludge notice and necessary information.to comply with the requirements
in this subpart.
(g) When a person who prepares sewage sludge provides -the sewage sludge to another person who
prepares the sewage sludge, the person who provides the sewage sludge shall provide the person who
receives the sewage sludge notice and necessary information to comply with the requirements in this subpart.
(h) The person who applies bulk sewage sludge to the land shall provide the owner or lease holder of the land
on which the bulk sewage sludge is applied notice and necessary information to comply with the requirements
in this subpart.
(i) Any person who prepares bulk sewage sludge that is applied to land in a State other than the State in
which the bulk sewage sludge is prepared shall provide written notice, prior to the initial application of bulk
sewage sludge to the land application site by the applier, to the permitting authority for the State in which the
bulk sewage sludge is proposed to be applied. The notice shall include:
(1) The location, by either.street address or latitude and longitude, of each land application site.
(2) The approximate time period bulk sewage sludge will be applied to the site.
(3) The name, address, telephone number, and National Pollutant Discharge Elimination System permit
number (if appropriate) for the person who prepares the bulk sewage sludge.
(4) The name, address, telephone number, and National Pollutant Discharge Elimination System permit
number (if appropriate) for the person who will apply the bulk sewage sludge.
0) Any person who applies bulk sewage sludge subject to the cumulative pollutant loading rates in
§503.13(b)(2) to the land shall provide written notice, prior to the initial application of bulk sewage sludge to a
land application site by the applier, to the permitting authority for the State in which the bulk sewage sludge
will be applied and the permitting authority shall retain and provide access to.the notice. The notice shall
include:
(1) The location, by either street address or latitude and longitude, of the land application site.
(2) The name, address, telephone number, and National Pollutant Discharge Elimination System permit
number (if appropriate) of the person who will apply the bulk sewage sludge.
§ 503.13 Pollutant limits.
(a) Sewage sludge. (1) Bulk sewage sludge or sewage sludge sold or given away in a bag or other container
shall not be applied to the land if the concentration of any pollutant in the sewage sludge exceeds the ceiling
concentration for the pollutant in Table 1 of §503.13.
(2) If bulk sewage sludge is applied to agricultural land, forest, a public contact site, or a reclamation site,
either:
(i) The cumulative loading rate for each pollutant shall not exceed the cumulative pollutant loading rate for the
pollutant in Table 2 of §503.13; or
(ii) The concentration of each pollutant in the sewage sludge shall not exceed the concentration for the
pollutant in Table 3 of §503.13.
(3) If bulk sewage sludge is applied to a lawn. or a home garden, the concentration of each pollutant in the
sewage sludge shall not exceed the concentration for the pollutant in Table 3 of .§503.13.
(4) If sewage sludge is sold or given away in a bag or other container for application to the land, either:
(i) The concentration of each pollutant in the sewage sludge shall not exceed the concentration for the
pollutant in Table 3 of 5503.13; or
(ii) The product of the concentration of each pollutant in the sewage sludge and the annual whole sludge
application rate for the sewage sludge shall not cause the annual pollutant loading rate for the pollutant in
Table 4 of §503.13 to be exceeded. The procedure used to determine the annual whole sludge application
rate is presented in appendix A of this part.
(b) Pollutant concentrations and loading rates —sewage sludge. —(1) Ceiling concentrations.
Table 1 of &503.13—Ceiling Concentrations
Pollutant
Ceiling concentration (milligrams per kilogram)1
Arsenic .
75
Cadmium
85
Copper
4300
Lead
840
Mercury
57
Molybdenum
175
Nickel.
420
Selenium
100
1 Dry weight basis.
(2) Cumulative 'pollutant loading rates.
Table 2 of 8503.13=Cumulative Pollutant I nnriinn Ratac
Pollutant
Cumulative pollutant loading rate (kilograms per hectare)
Arsenic
41
Cadmium
39
Copper
1500
Lead
300
Mercury
17
Nickel
420
Selenium I
100
Zinc
2800
(s) roiiutant concentrations.
Table 3 of &503-13—Pollutant Conr_entrations '
Pollutant .
Monthly average concentration (milligrams per kilogram)1
Arsenic
41
Cadmium
39
Copper.
1500
Lead
300
Mercury
17
Nickel
420
Selenium
100 "
Zinc
2800
1 Dry weight basis.
(4) Annual pollutant loading rates.
Table 4 of §503.13—Annual Pollutant Loading Rates
Pollutant
Annual pollutant loading rate (kilograms per hectare per 365 day period)
Arsenic
2.0
Cadmium
1.9
Copper
75.
Lead
15
Mercury
0.85
Nickel
21
Selenium
5.0
Zinc
140
(c) Domestic septage. The annual application rate for domestic septage applied to agricultural land, forest, or
a reclamation site shall not exceed the -annual application rate calculated using equation (1).
AAR = N Eq. (1)
0.0026
Where: ,
AAR=Annual application rate in gallons per acre per 365 day period.
N=Amount of nitrogen in pounds per acre per 365 day period needed by the crop or vegetation grown on the
land.
[58 FIR 9387, Feb. 19, 1993, as amended at 58 FIR 9099, Feb. 25, 1994; 60 FIR 54769, Oct. 25, 1995]
§ 503.14 Management practices.
(a) Bulk sewage sludge shall not be applied to the land if it is likely to adversely affect a threatened or
endangered species listed under section 4 of the Endangered Species Act or its designated critical habitat.
(b) Bulk sewage sludge shall not be applied to agricultural land, forest, a public contact site, or a reclamation
site that is flooded, frozen, or snow-covered so that the bulk sewage sludge enters a wetland or other waters
of the United States, as defined in 40 CFR 122.2, except as provided in a permit issued pursuant to section
402 or 404 of the CWA.
(c) Bulk sewage sludge shall not be applied to agricultural land, forest, or a reclamation site that is 10 meters
or less from waters of the United States, as defined in 40 CFR 122.2, unless otherwise specified by the
permitting authority.
(d) Bulk sewage sludge shall be applied to agricultural land, forest, a public contact site, or a reclamation site
at a whole sludge application rate that is equal to or less than the agronomic rate for the bulk sewage sludge,
unless, in the case of a reclamation site, otherwise specified by the permitting authority.
(e) Either a label shall be affixed to the bag or other container in which sewage sludge that is sold or given
away for application to the land, or an information sheet shall be provided to the person who receives sewage
sludge sold or given away in an other container for application to the land. The -label or information sheet shall
contain the following information:
(1) The name and address of the person who prepared the sewage sludge that is sold or given away in a bag
or other container for application to the land.
(2) A statement that application of the sewage sludge to the land is prohibited except in accordance with the
instructions on the label or information sheet.
(3) The annual whole sludge application rate for the sewage sludge that does not cause any of the annual
pollutant loading rates in Table 4 of §503.13 to be exceeded.
§ 503.15 Operational standards —pathogens and vector attraction reduction.
(a) Pathogens —sewage sludge. (1) The Class A pathogen requirements in §503.32(a) or the Class B
pathogen requirements and site restrictions in §503.32(b) shall be met when bulk sewage sludge is applied to
agricultural land, forest, a public contact site, or a reclamation site.
(2) The Class A pathogen requirements in §503.32(a) shall be met when bulk sewage sludge is applied to a
lawn or a home garden.
(3) The Class A pathogen requirements in §503.32(a) shall be met when sewage sludge is sold or given away
in a bag or other container for application to the land.
(b) Pathogens —domestic septage. The requirements in either §503.32 (c)(1) or (c)(2) shall be met when
domestic septage is applied to agricultural land, forest, or a reclamation site.
(c) Vector attraction reduction —sewage sludge. (1) One of the vector attraction reduction requirements in
§503.33 (b)(1) through (b)(10) shall be met when bulk sewage sludge is applied to agricultural land, forest, a
public contact site, or a reclamation site.
(2) One of the vector attraction reduction requirements in §503.33 (b)(1) through (b)(8) shall be met when bulk
sewage sludge is applied to a lawn or a home garden. -
(3) One of the vector attraction reduction requirements in §503.33 (b)(1) through (b)(8) shall be met when
sewage sludge is sold or given away in a bag or other container for application to the land.
(d) Vector attraction reduction —domestic septage. The vector attraction reduction requirements in
§503.33(b)(9), (b)(10), or (b)(1 2) shall be met when domestic septage is applied to agricultural land, forest, or
a reclamation site.
§ 503.16 Frequency of monitoring.
(a) Sewage sludge. (1) The frequency of monitoring for the pollutants listed in Table 1, Table 2, Table 3 and
Table 4 of §503.13; the pathogen density requirements in §503.32(a) and §503.32(b)(2); and the vector
attraction reduction requirements in §503.33 (b)(1) through (b)(4) and §503.33 (b)(7) through (b)(8) shall be
the frequency in Table 1 of §503.16.
Table 1 of §503.16—Frequency of Monitorinq—Land Application
(Amount of sewaqe sludge1(metric tons per 365 day period) IFreauencv
Greater than zero but less than 290
Once per year.
Equal to or greater than 290 but less than 1,500
Once per quarter (four times per year).
Equal to or greater than 1,500 but less than 15,000
Once per 60 days (six times per year).
Equal to or greater than 15,000
Once per month (12 times per year).
1 Either the amount of bulk sewage sludge applied to the land or the amount of sewage sludge prepared for
sale or give-away in a bag or other container for application to the land (dry weight basis).
(2) After the sewage sludge has been monitored for two years at the frequency in Table 1 of §503.16; the,
permitting authority may reduce the frequency of monitoring for pollutant concentrations and for the pathogen
density requirements in §503.32(a)(5)(ii) and (a)(5)(iii).
(b) Domestic septage. If either the pathogen requirements in §503.32(c)(2) or the vector attraction reduction
requirements in,§503.33(b)(1.2) are met when domestic septage is applied to agricultural land, forest; or a
reclamation site,•each container of domestic septage applied to the land shall be monitored for compliance
with those requirements.
(Approved by the Office of Management and Budget under control number 2040=0157)
[58 FIR 9387, Feb. 19, 1993, as amended at 64 FIR 42569, Aug. 4, 1999]
§ 503.17 Recordkeeping.
(a) Sewage sludge. (1) The person who prepares the sewage sludge in §503.10(b)(1) or (e) shall develop the
following information and shall retain the information for five years:
(i) The concentration of each pollutant listed in Table 3 of §503.13 in the sewage sludge.
(ii) The following certification statement:
I certify, under penalty of law, that the information that will be used to determine compliance with the Class A
pathogen requirements in §503.32(a), and the vector attraction reduction requirement in [insert one of the
vector attraction reduction requirements in §503.33(b)(1) through §503.33(b)(8)] was prepared under my
direction and supervision in accordance with the system designed to ensure that qualified personnel properly
gather and evaluate this information. I am aware that there are. significant penalties for false certification
including the possibility of fine and imprisonment.
(iii) A description of how the Class A pathogen requirements in §503.32(a) are met.
(iv) A description of how one of the vector attraction reduction requirements in §503.33 (b)(1) through (b)(8) is
met. -
(2) The person -who derives the material in §503.10 (c)(1) or (f) shall develop the following information and
shall retain the information for five years:
(i) The concentration of each pollutant listed in Table 3 of §503.13 in the material.
(ii) The following certification statement:
I certify, under penalty of law, that the information that will be used to determine compliance with the Class A
pathogen requirements in §503.32(a) and the vector attraction reduction requirement in (insert one:of the
vector attraction reduction requirements in §503.33(b)(1) through (b)(8)) was prepared under my direction and
supervision in accordance with the system designed to ensure that qualified personnel properly gather and
evaluate this information. I am aware that there are significant penalties for false certification including the
possibility of fine and imprisonment.
(iii) A description of how the Class A pathogen requirements in §503.32(a) are met.
(iv) A description of how one of the vector attraction reduction requirements in §503.33 (b)(1) through (b)(8) is
met.
(3) If the pollutant concentrations in §503.13(b)(3), the Class A pathogen requirements in §503.32(a), -and the
vector attraction reduction requirements in either §503.33 (b)(9) or (b)(10) are met when bulk sewage sludge
is applied to agricultural land, forest, a public contact site, or a reclamation site:
(i) The person who prepares the bulk, sewage sludge shall develop the following information and shall retain
the information for five years.
(A) The concentration of each pollutant listed in Table 3 of §503.13 in the bulk sewage sludge.
(B) The following certification statement:
I certify, under penalty of law, that the information that will be used to determine compliance with the Class A
pathogen requirements in §503.32(a) was prepared under my direction and supervision in accordance with
the system designed to ensure that qualified personnel properly gather.and evaluate this information. I am
aware that there are significant penalties for false certification including the possibility of fine and
imprisonment.
(C) A description of how the pathogen requirements in §503.32(a) are met.
(ii) The person who applies the•.bulk sewage sludge shall develop the following information and shall retain
the information for five years.
(A) The following certification statement:
I certify, under penalty of law, that the information that will be used to determine compliance with the
management practices in §503.14 and the vector attraction reduction requirement in (insert either
§503.33(b)(9) or (b)(10)) was prepared under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate this information. I am aware that
there are significant penalties for false certification including the possibility of fine and imprisonment.
(B) A description of how the management practices in §503.14 are met for each site on which bulk sewage
sludge is applied.
(C) A description of how the vector attraction reduction requirements in either §503.33(b)(9) or (b)(10) are met
for each site on which bulk sewage sludge is applied.
(4) If the pollutant concentrations in §503.13(b)(3) and the Class B pathogen requirements in §503.32(b) are
met when bulk sewage sludge is applied to agricultural land, forest, a public contact site, or a reclamation site:
(i) The person who prepares the bulk sewage sludge shall develop the following information and shall retain
the information for five years:
(A) The concentration of each pollutant. listed in Table 3 of §503.13 in the bulk sewage sludge.
(B) The following certification statement:
I certify, under penalty of law, that the information that will be used to determine compliance with the Class B
pathogen requirements in §503.32(b) and the vector attraction reduction requirement in (insert one of the
vector attraction reduction requirements in §503.33(b)(1) through (b)(8)if one of those requirements is met)
was prepared under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate this information. I am aware that there are significant'
penalties for false certification including the possibility of fine and imprisonment. '
(C) A description of how the Class B pathogen requirements in §503.32(b) are met.
(D) When one of the vector attraction reduction requirements in §503.33 (b)(1) through (b)(8) is met, a
description of how the vector attraction reduction requirement is met.
(ii) The person who applies the bulk sewage sludge shall develop the following information and shall retain
the information for five years.
(A) The following certification statement:
I certify, under penalty of law, that the information that will be used to determine compliance with the
management practices in §503.14, the site restrictions in §503.32(b)(5), and the vector attraction reduction
requirement in (insert either §503.33(b)(9) or (b)(10) if one of those requirements is met) was prepared for
each site on which bulk sewage sludge is applied under my direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate this information. I am aware
that there are significant penalties for false certification including the possibility of fine and imprisonment.
(B) A description of how the management practices in §503.14 are met for each site on which bulk sewage
sludge is applied.
(C) A description of how the site restrictions in §503.32(b)(5) are met for each.site on which bulk sewage
sludge is applied.
(D) When the vector attraction reduction requirement in either §503.33 (b)(9) or (b)(10) is met, a description of
how the vector attraction reduction requirement is met.
(E) The date bulk sewage sludge is applied to each site.
(5) If the requirements in §503.13(a)(2)(i) are met when bulk sewage sludge is applied to agricultural land,
forest, a public contact site, or a reclamation site:
(i) The person who prepares the bulk sewage sludge shall develop the following information and shall retain
the information for five years.
(A) The concentration of each pollutant listed in Table 1 of §503.13 in the bulk sewage sludge.
(B) The following certification statement:
I certify, under penalty of law, that the information that will be used to determine compliance with the
pathogen requirements in (insert either §503.32(a) or §503.32(b)) and the vector attraction reduction
.requirement in (insert one of the vector attraction reduction requirements in §503.33(b)(1) through (b)(8) if one
.of those requirements is met) was prepared under my direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate this information. I am aware
that there are significant penalties for false certification including the possibility of fine and imprisonment.
(C) A description of how the pathogen requirements in either §503.32 (a) or (b) are met.
(D) When one of the vector attraction requirements in §503.33 (b)(1) through (b)(8) is met, a description of
how the vector attraction requirement is met.
(ii) The person who applies the bulk sewage sludge shall develop the following information, retain the
information in §503.17 (a)(5)(ii)(A) through (a)(5)(ii)(G) indefinitely, and retain the information in §503.17
(a)(5)(ii)(H) through (a)(5)(ii)(M) for five years.
'(A) The location, by either street address or latitude and longitude, of each site on which:bulk sewage sludge
is applied.
(B) The number of hectares in each site on which bulk sewage sludge is applied.
(C) The date bulk. sewage sludge is applied to each site.
(D) The cumulative amount of each pollutant ( i.e. , kilograms) listed in Table 2 of §503.13 in the bulk sewage
sludge applied to each site, including the amount in §503.12(e)(2)(iii).
(E) The amount of sewage sludge ( i.e. , metric tons) applied to each site.
(F) The following certification statement:
I certify, under penalty of law, that the information that will be -used to determine compliance with the
requirement to obtain information in §503.12(e)(2) was prepared for each site on which bulk sewage sludge
was applied under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate this information. I am aware that there are significant
penalties for false certification including the possibility of fine and imprisonment.
(G) A description.of how the requirements to obtain information in §503.12(e)(2) are met.
(H) The following certification statement:
I certify, under penalty of law,'that the information that will be used to determine compliance with the:: `
management practices in §503.1.4 was prepared for each site on which bulk sewage sludge was -applied...
under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate this information. I am aware that there are significant penalties for false
certification including the possibility of fine and imprisonment.
(1) A description- of how the management practices in §503.14 are met for each site on which bulk sewage
sludge is applied.
(J) The following certification statement when the bulk sewage sludge meets the Class B pathogen
requirements in §503.32(b):
I certify, under penalty of law, that the information that will be used to determine compliance with the site
restrictions in §503.32(b)(5) for each site on which Class B sewage sludge was applied was prepared under
my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate this information. I am aware that there'are significant penalties for false
certification including the possibility of fine and imprisonment.
(K) A description of how the site restrictions in §503.32(b)(5) are met for each site on which Class B bulk
sewage sludge is applied'.
(L) The following certification statement when the vector attraction reduction requirement in either
§503.33(b)(9) or (b)(10) is met:
I certify, under penalty of law, that the information that will be used to determine compliance with the vector
attraction reduction requirement in (insert either §503.33(b)(9) or §503.33(b)(10)) was prepared under my -
direction and supervision in accordance with the system designed to ensure that qualified personnel properly
gather and evaluate this information. I am aware that there are significant penalties for false certification
including the possibility of fine and imprisonment.
(M) If the vector attraction reduction requirements in either §503.33 (b)(9) or (b)(10) are'met, a description of
how the requirements are met.
(6) If the requirements in §503.13(a)(4)(ii) are met when sewage sludge is sold or given away in a bag or
other container for application to the land, the person who prepares the sewage sludge that is sold or given
away in a bag or other container shall develop the following information and. shall retain the information for
five years:
(i) The annual whole sludge application rate for the sewage sludge that does not cause the annual pollutant
loading rates in Table 4 of §503.13 to be exceeded.
(ii) The concentration of each pollutant listed in Table 4 of §503.13 in the sewage sludge.
(iii) The following certification statement:
I certify, under penalty of law, that the information that will be used to determine compliance with the
management practice in §503.14(e), the Class A pathogen requirement in §503.32(a), and the vector
attraction reduction requirement in (insert one of the vector attraction reduction requirements in §503.33(b)(1)
through §503.33(b)(8)) was prepared under my direction and supervision in accordance with the system
designed to ensure that qualified'personnel properly gather and evaluate this_ information. I am aware that
there are significant penalties for false certification including the possibility of fine and imprisonment.
(iv) A description of how the Class A pathogen requirements in §503.32(a) are met.
(v) A description of how one of the vector attraction requirements in §503.33 (b)(1) through (b)(8) is met.
(b) Domestic septage. When domestic septage is applied to agricultural land, forest, or a reclamation site, the
person who applies the domestic septage shall develop the following information and shall retain the
information for five years:
(1) The location, by either street address or latitude and longitude, of each site on which domestic septage is
applied.
(2) The number of acres in each site on which domestic septage is applied.
(3) The date domestic septage is applied to each site.
(4) The nitrogen requirement for the crop or vegetation grown on each site during a 365 day period.
(5) The rate, in gallons per acre per 365 day period, at which domestic septage is applied to each site.
(6) The following certification statement:
I certify, under penalty of law, that the information that will be used to determine compliance with the
pathogen requirements (insert either §503.32(c)(1) or §503.32(c)(2)) and the vector attraction reduction
requirement in [insert §503.33(b)(9), 503.33(b)(10), or §503.33(b)(12)] was prepared under my direction and
supervision in accordance with the system designed to ensure that qualified personnel properly gather and
evaluate this information. I am aware that there are significant penalties for false certification including the
possibility of fine and imprisonment.
(7) A description of how the pathogen requirements in either §503.32(c)(1) or (c)(2) are met.
(8) A description of how the vector attraction reduction requirements in §503.33 (b)(9), (b)(10), or (b)(12) are
met.
(Approved by the Office of Management and Budget under control number 2040-0157)
[58 FR 9387, Feb. 19, 1993, as amended at 64 FR 42569, Aug. 4, 1999]
§ 503.18 Reporting.
(a) Class I sludge management facilities, POTWs (as defined in 40 CFR 501.2) with a design flow rate equal
to or greater than one million gallons per day, and POTWs that serve 10,000 people or more shall submit the
following information to the permitting authority:
(1) The information A §503.17(a), except the information in §503.17 (a)(3)(ii), (a)(4)(ii) and in (a)(5)(ii), for the
appropriate requirements on February 19 of each year.
(2) The information in §503.17(a)(5)(ii)(A) through (a)(5)(ii)(G) on February 19th of each year when 90 percent
or more of any of the cumulative pollutant loading rates in Table 2 of §503.13 is reached at a land application
site, i
(Approved by the Office of Management and Budget under control number 2040-0157)
[58 FR 9387, Feb. 19, 1993, as amended at 64 FR 42570, Aug. 4, 1999]
Subpart C—Surface Disposal
§ 503.20 Applicability.
(a) This subpart applies to any person who prepares sewage sludge that is placed on a surface disposal site,
to the owner/operator of a surface disposal site, to sewage sludge placed on a surface disposal site, and to a
surface disposal site.
(b) This subpart does not apply to sewage sludge stored on the land or to the land on which sewage sludge is
stored. It also does not apply to sewage sludge that remains on the land for longer than two years when the
person who prepares the sewage sludge demonstrates that the land on which the sewage sludge•remains is
not an active sewage sludge unit. The demonstration shall include the following information, which shall be
retained by the person who prepares the sewage sludge for the period that the sewage sludge remains on the
land:
(1) The name and address of the person who prepares the sewage sludge..
(2) The name and address of the person who either owns the land or leases the land.
(3) The location, by either street address or latitude and longitude, of the land.
(4) An explanation of why sewage sludge needs to remain on the land for longer than two years prior to final
use or disposal.
(5) The approximate time period when the sewage sludge will be used or disposed.
(c) This subpart does not apply to sewage sludge treated on the land or to the land on which sewage sludge
is treated.
§ 503.21 Special definitions.
(a) Active sewage sludge unit is a sewage sludge unit that has not closed.
(b) Aquifer is a geologic formation, group of geologic formations, or a portion of a geologic formation capable
of yielding ground water to wells or springs.
(c)'Contaminate an aquifer means to introduce a substance that causes the maximum contaminant level for
nitrate in 40 CFR 141.62(b) to be exceeded in the ground water or that causes the existing concentration of
nitrate in ground water to increase when the existing concentration of nitrate in the ground water exceeds the
maximum contaminant level for nitrate in 40 CFR 141.62(b).
(d) Cover is soil or other material used to cover sewage sludge placed on an active sewage sludge unit.
(e) Displacement is the relative movement of any two sides of a fault measured in any direction.
(f) Fault is a fracture or zone of fractures in any materials along which strata on one side are displaced with
respect to strata on the other side.
(g) Final cover is the last layer of soil or other material placed on a sewage sludge unit at closure:
(h) Holocene time is the most recent epoch of the Quaternary period, extending from the end of the
Pleistocene epoch to the present.
(i) Leachate collection system is a system or device installed immediately above a liner that is designed,
constructed, maintained, and operated to collect and remove leachate from a sewage sludge unit.
Q) Liner is soil or synthetic material that has a hydraulic conductivity of 1 X10-7centimeters per second 'or less.
(k) Lower explosive limit for methane gas is the lowest percentage of methane gas. in air, by volume,. that
propagates a flame at 25.degrees' Celsius and atmospheric pressure.
(1) Qualified ground -water scientist is an individual with a baccalaureate or post -graduate degree in the natural
sciences or engineering who has sufficient training and experience in ground -water hydrology and related
fields, as may be demonstrated by State registration, professional certification, or completion of accredited
university programs, to make sound professional judgments regarding ground -water monitoring, pollutant fate
and transport, and corrective action.
(m) Seismic impact zone is an area that has a 10 percent or greater probability that the horizontal ground
level acceleration of the rock in the area exceeds 0.10 gravity once in 250 years.
(n) Sewage'sludge unit island on which only sewage sludge is placed for final disposal. This does not include
land on which sewage sludge is either stored or treated. Land does not include waters of the United States,
as defined in 40 CFR 122.2.
(o) Sewage sludge unit boundary is the outermost perimeter of an active sewage sludge unit.
(p) Surface disposal site is an area of land that contains one or more active sewage sludge units.
(q) Unstable area is land subject to natural or human -induced forces that may damagethe structural
components of an active sewage sludge unit. This includes, but is not limited to, land on which the soils are
subject to mass movement.
[58 FIR 9387, Feb. 19, 1993, as amended at 64 FIR 42570, Aug. 4, 1999]
§ 503.22 General requirements.
(a) No person shall place sewage sludge on an active sewage sludge unit unless the requirements in this
subpart are met.
(b) An active sewage sludge unit located within 60 meters of a fault that has displacement in Holocene time;
located in an unstable area; or located in a wetland, except as provided in a permit issued pursuant to either
section 402 or 404 of the CWA, shall close by March 22, 1994, unless, in the case of an active sewage sludge
unit located within 60 meters of a fault that has displacement in Holocene time, otherwise specified by the
permitting authority.
(c) The owner/operator of an active sewage. sludge unit shall submit a written closure and post closure plan to
the permitting authority 180 days prior to the date that the active sewage sludge unit closes. The plan shall
describe how the sewage sludge unit will be closed and, at a minimum, shall include:
(1) A discussion of how the leachate collection system will be operated and maintained for three'years after
the sewage sludge unit closes if the sewage sludge unit has a liner and leachate collection system.
(2) A description of the system used to monitor for methane gas in the air in any structures within the surface
disposal site and in the air at the property line of the surface disposal site, as required in §503.240)(2).
(3) A discussion of how public access to the surface disposal site will be restricted for three years after the
last sewage sludge unit in the surface disposal site closes.
(d) The owner of a surface disposal site shall provide written notification to the subsequent owner of the site
that sewage sludge was placed on the land.
[58 FIR 9387, Feb. 19, 1993, as amended at 64 FIR 42570, Aug. 4, 1999]
§ 503.23 Pollutant limits (other than domestic septage).
(a) Active sewage sludge unit without a liner and leachate collection system.
(1) Except as provided in §503.23 (a)(2) and (b), the concentration of each pollutant listed in Table 1 of
§503.23 in sewage sludge placed on an active sewage sludge unit shall not exceed the concentration for the
pollutant in Table 1 of §503.28.
Table 1 of §503.23—Pollutant Concentrations —Active Sewage Sludge Unit Without a Liner and Leachate
Collection
(Pollutant lConcentration (milligrams per kilogramsl)
Arsenic 73
Chromium 600
Nickel 420
1 Dry weight basis.
(2) Except as provided in §503.23(b), the concentration of each pollutant listed in Table 1 of §503.23 in
sewage sludge placed on an active sewage sludge unit whose boundary is less than 150 meters from the
property line of the surface disposal site shall not exceed the concentration determined using the following
procedure:
(i) The actual distance from the active sewage sludge unit boundary to, the property line of the surface
disposal site shall be determined.
(ii) The concentration of each pollutant listed in Table 2 of §503.23 in the sewage sludge shall not exceed the
concentration in Table 2 of §503.23 that corresponds to the actual distance in §503.23(a)(2)(i).
Table 2 of §503.23—Pollutant Concentrations —Active Sewage Sludge Unit Without a Liner and Leachate
Collection Svstem That Has a Unit Boundary to Property Line Distance Less Than 150 Meters
Unit boundary to property line
Pollutant concentration1
Distance (meters)
Arsenic (mg/kg)
Chromium (mg/kg)
Nickel (mg/kg)
0 to less than 25
30
200
210
25 to less than 50
34
220-
240
50 to less than 75
39
260
270
75 to less than 100
46
300
320
100 to less than 125
53
360
390
125 to less than 150
62
450
420
1 Dry weight basis.
(b) Active sewage sludge unit without a liner and leachate collection system —site -specific limits.
(1) At the time of permit application, the owner/operator of a surface disposal site may request site -specific
pollutant, limits in accordance with §503.23(b)(2) for an active sewage sludge unit without a liner and leachate
collection system when the existing values for site parameters specified by the permitting authority are
different from the values for those parameters used to develop the pollutant limits in Table 1 of §503.23 and
when the permitting authority determines that site -specific pollutant limits are appropriate for the active
sewage sludge unit.
(2) The concentration of each pollutant listed in Table 1 of §503.23 in sewage sludge placed on an active
sewage sludge unit without a liner and leachate collection system shall not exceed either the concentration for
the pollutant determined during a site -specific assessment, as specified by the permitting authority, or the
existing concentration of the pollutant in the sewage sludge, whichever is lower.
§ 503.24 Management practices.
.(a) Sewage sludge shall not be placed on an active sewage sludge unit if it is likely to adversely affect a
threatened or endangered species listed under section 4 of the Endangered Species Act or its designated
critical habitat.
(b) An active sewage sludge unit shall not restrict the flow of a base flood.
-(c) When a surface disposal site is located in a seismic impact zone, an active sewage sludge unit shall be
designed to withstand the maximum recorded horizontal ground level acceleration.
(d) An -active sewage sludge unit shall be located 60 meters or more from a fault that has displacement in
Holocene time, unless otherwise specified by the permitting authority.
(e) An active sewage sludge unit shall not be located in an unstable area.
(f) An active sewage sludge unit shall not be located in a wetland, except as provided in a permit issued
pursuant to section 402 or 404 of the CWA.
(g)(1) Run-off from an active sewage sludge unit shall be collected and shall be disposed in accordance with
National Pollutant Discharge Elimination System permit requirements and any other applicable requirements.
(2) The run-off collection system for an active sewage sludge unit shall have the capacity to handle run-off
from a 24-hour, 25-year storm event.
(h) The leachate collection system for an active sewage sludge unit that has a liner and leachate collection
system shall be operated and maintained during the period the sewage sludge unit is active and for three
years after the sewage sludge unit closes.
(i) Leachate from- an active sewage sludge unit that has a liner and leachate collection system shall be
collected and shall be disposed in accordance with the applicable requirements during the period the sewage
sludge unit is active and for three years after the sewage sludge unit closes.
0)(1) When a cover is placed on an active sewage sludge unit, the concentration of methane gas in air in any
structure within the surface disposal site sliall not exceed 25 percent of the lower explosive limit for methane
gas during the period that the sewage sludge unit is active and the concentration of methane gas in.air at the
property line of the surface disposal site shall not exceed the lower explosive limit for methane gas -during the
period that the sewage sludge unit is active.
(2) When a final cover is placed on a sewage sludge unit at closure, the concentration of methane gas in air in
any structure within the surface disposal site shall not exceed 25 percent of the lower explosive limit for
methane gas for three years after the sewage sludge unit closes and the concentration of methane gas in air
at the property line of the surface disposal site shall not exceed the lower explosive limit for methane gas for
three years after the sewage sludge unit closes, unless otherwise specified by the permitting authority.
(k) A food crop, a feed crop, or a fiber crop shall not be grown-on,an active sewage sludge unit, unless the
owner/operator of the surface disposal site demonstrates to the permitting authority that through management
practices public.health and the environment are protected from any reasonably anticipated adyerse,effects of
pollutants in sewage sludge when crops are grown.
(1) Animals shall not be grazed on an' active sewage sludge unit, unless the owner/operator of the surface
disposal site demonstrates to the permitting authority that through management practices public health and
the environment are protected from any reasonably anticipated adverse effects of pollutants in sewage sludge
when animals are grazed.
(m) Public access to a surface disposal site shall be restricted for the period that the surface disposal site
contains an active sewage sludge unit and for three years after the last active sewage sludge unit in the .
surface disposal site closes.
(n)(1) Sewage sludge placed on an active sewage sludge unit shall not contaminate an aquifer.
(2) Results of a ground -water monitoring program developed by a qualified ground -water scientist or a
certification by a qualified ground -water scientist shall be used to demonstrate that sewage sludge, placed on
an active sewage sludge unit does not contaminate an aquifer.
§ 503.25 Operational standards —pathogens and vector attraction reduction.
(a) Pathogens —sewage sludge (other than domestic septage). The Class A pathogens requirements in
§503.32(a) or one of the Class B pathogen requirements in §503.32 (b)(2) through (b)(4) shall be met when -
sewage sludge is placed on an active sewage sludge unit, unless the vector attraction reduction requirement
in §503.33(b)(11) is met.
(b) Vector attraction reduction —sewage sludge (other than domestic septage). One of the vector attraction
reduction requirements in §503.33 (b)(1) through (b)(11) shall be met when sewage sludge is placed on an
active sewage sludge unit.
(c) Vector attraction reduction --domestic septage. One of the vector attraction reduction requirement in
§503.33 (b)(9) through (b)(12) shall be met when domestic septage is placed on an active sewage sludge
unit.
§ 503.26 Frequency of monitoring.
(a) Sewage sludge (other than domestic septage). (1) The frequency of monitoring for the pollutants in
Tables 1 and 2 of §503.23; the pathogen density requirements in §503.32(a) and in. §503.32(b)(2); and the
vector attraction reduction requirements in §503.33(b)(1) through (b)(4) and §503.33(b)(7) through'(b)(8) for
sewage sludge placed on an active sewage sludge unit shall be the frequency in Table 1 of §503.26.
Table 1 of §503.26—Frequency of Monitoring —Surface Disposal
Amount of sewage sludge1
(metric tons per 365 day period)
Frequency
Greater than zero but less than 290
Once per year.
Equal to or greater than 290 but less than 1,500
Once per quarter (four times per year).
Equal to or greater than 1,500 but less than 15,000
Once per 60 days (six times per year):
Equal .to or greater than 15,000
Once per month (12 times per year).
1Amount of sewage sludge placed on an active sewage sludge unit (dry weight basis).
(2) After the sewage sludge has been monitored for two years at the frequency in Table 1 of this section, the
permitting authority may reduce the frequency of monitoring for pollutant concentrations and for the pathogen
density requirements in §503.32(a)(5)(ii) and (a)(5)(iii).
(b) Domestic septage. If the vector attraction reduction requirements in §503.33(b)(12) are met when
domestic septage is placed on an active sewage sludge unit, each container of domestic septage shall be
monitored for compliance with those requirements.
(c) Air. Air in structures within a surface disposal site and at the property line of the surface disposal site shall
be monitored continuously for methane gas during the period that the surface disposal site contains an active
sewage sludge unit on which the sewage sludge is covered and for three years after a sewage sludge unit
closes when a final cover is placed on the sewage sludge.
(Approved by the Office of Management and Budget under control number 2040-0157)
[58 FIR 9387, Feb. 19, 1993, as amended at 64 FIR 42570, Aug. 4, 1999]
§ 503.27 Recordkeeping.
(a) When sewage sludge (other than domestic septage) is placed on an active sewage sludge unit:
(1) The person who prepares the sewage sludge shall develop the following information and shall retain the
information for five years.
(i) The concentration of each pollutant listed in Table 1 of §503.23 in the sewage sludge when the pollutant
concentrations in Table 1 of §503.23 are met.
(ii) The following certification statement:
I certify, under penalty of law, that the information that will be used to determine compliance with the
pathogen requirements in (insert §503.32(a), §503.32(b)(2), §503.32(b)(3), or §503.32(b)(4) when one of
those requirements is met) and the vector attraction reduction requirement in (insert one of the vector
attraction reduction requirements in §503.33 (b)(1) through (b)(8) if one of those requirements is met) was
prepared under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate this information. I am aware that there are significant penalties for
false certification including the possibility of fine and imprisonment.
(iii) A description of how the pathogen requirements in §503.32 (a), (b)(2), (b)(3), or (b)(4) are met when one
of those requirements is met. - -
(iv) A description of how one of the vector attraction reduction requirements in §503.33 (b)(1) through (b)(8) is
met when one of those requirements is met.
(2) The owner/operator of the surface disposal site, shall develop the following information and shall retain
that information for five years.
(i) The concentration of each pollutant listed in Table 2 of §503.23 in the sewage sludge when the pollutant
concentrations in Table 2 of §503.23 are met or when site -specific pollutant limits in §503.23(b) are met.
(ii) The following certification statement:
I certify, under penalty of law, that the information that will be used to determine compliance with the
management practices in §503.24 and the vector attraction reduction requirement in (insert one of the
requirements in §503.33(b)(9) through §503.33(b)(11) if one of those requirements is met) was prepared
under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate this information. I am aware that there are significant penalties for false
certification including the possibility of fine and imprisonment.
(iii) A description of how the management practices in §503.24 are met.
(iv) A description of how the vector attraction reduction requirements in §503.33 (b)(9) through (b)(1 1) are met
if one of those requirements is met.
(b) When domestic septage is placed on a surface disposal site:
(1) If the vector attraction reduction requirements in §503.33(b)(12) are met, the person who places the
domestic septage on the surface disposal site shall develop the following information and shall retain the
information for five years:
(i) The following certification statement:
I certify, under penalty of law, that the information that will be used to determine compliance with the vector
attraction' reduction requirements in §503.33(b)(12) was prepared under my direction and supervision in
accordance with the system designed to ensure that qualified personnel properly gather and evaluate this
information. I am aware that there are significant penalties for false certification including the possibility of fine
and imprisonment. i .
(ii) A description of how the vector attraction reduction requirements in §503.33(b)(12) are met.
(2) The owner/operator of the surface disposal site shall develop the following information and shall retain that
information for five years:
(i) The following certification statement:
I certify, under penalty of law, that the information that will be used to determine compliance with the.;:.
management practices in §503:24 and the vector attraction reduction requirements in (insert §5.03.33(b)(9)
through §503.33(b)(11) if one of those requirements is met) was prepared under my direction and`supervision
in accordance with the system designed to ensure that qualified personnel properly gather and evaluate this
information. I am aware that there are significant penalties for false certification including the possibility of- fine
or imprisonment. -
(ii) A description of how the management practices in §503.24 are met.
(iii) A description how the vector attraction reduction requirements in §503.33(b)(9) through §503.33(b)(11)
are met if one of those requirements is met.
(Approved by the Office of Management and Budget under control number 2040-0157)
[58 FR 9387, Feb.,19, 1993, as amended at 64 FR 42571, Aug. 4, 1999]
§ 503.28 Reporting.
Class I sludge management facilities, POTWs (as defined in 40 CFR 501.2) with a design flow rate equal to or
greater than one million gallons per day, and POTWs that serve 10,000 people or more shall submit the
information in §503.27(a) to the permitting authority on February 19 of each year.
(Approved by the Office of Management and Budget under control number 2040-0157)
Subpart D—Pathogens and Vector Attraction Reduction
§ 503.30 Scope.
(a) This subpart contains the requirements for a sewage sludge to be classified either Class A or Class B
with respect to pathogens.
(b) This subpart contains the site restrictions for land on which a Class B sewage sludge is applied.--
(c) This subpart contains the pathogen requirements for domestic septage applied to agricultural land, forest,
or a reclamation site.
(d) This subpart contains alternative vector attraction reduction requirements for sewage sludge that is
applied to the land or placed on a surface disposal site.
§ 503.31 Special definitions.
(a) Aerobic digestion is the, biochemical decomposition of organic matter in sewage sludge into carbon
dioxide and water by microorganisms in the presence of air.
(b) Anaerobic digestion is the biochemical decomposition of organic matter in sewage sludge into methane
gas and carbon dioxide by microorganisms in the absence of air.
(c) Density of microorganisms is the number of microorganisms per unit mass of total solids (dry weight) in
the sewage sludge.
(d) Land with a high potential for public exposure is land that the public uses frequently. This includes, but is
not limited to, a public contact site and a reclamation site located in a populated area (e.g, a construction site
located in a city).
(e) Land with a low potential for public exposure is land that the public uses infrequently. This includes; but is
not limited to, agricultural land, forest, and a reclamation site located in an unpopulated area (e.g., a strip
mine located in a rural area)...
(f) Pathogenic organisms are disease -causing organisms. These include, but are not limited to, certain
bacteria, protozoa, viruses, and viable helminth ova.
(g) pH means the logarithm of the reciprocal of the hydrogen ion concentration measured at 25 *Centigrade or
measured at another temperature and then converted to an equivalent value at 25 .°Centigrade.
(h) Specific oxygen uptake rate (SOUR) is the mass of oxygen consumed per unit time per unit mass of total
solids (dry weight basis) in the sewage sludge.
(i) Total solids are the materials in sewage sludge that remain as residue when the sewage sludge is dried at
103 to 105 degrees Celsius.
0) Unstabilized solids are organic materials in sewage sludge that have not been treated in either an aerobic
or anaerobic treatment process.
(k) Vector attraction is the characteristic of sewage sludge that attracts rodents, flies, mosquitos, or other
organisms capable of transporting infectious agents.
(1) Volatile solids is the amount of the total solids in sewage sludge lost when the sewage sludge is
combusted at 550 degrees Celsius in the presence of excess air.
[58 FR 9387, Feb. 19,' 1993, as amended at 64 FR 42571, Aug. 4, 1999]
§ 503.32 Pathogens.
(a) Sewage sludge —Class A. (1) The requirement in §503.32(a)(2) and the requirements in either
§503.32(a)(3), (a)(4), (a)(5), (a)(6), (a)(7), or (a)(8) shall be met for a sewage sludge to be classified Class A
with respect to pathogens.
(2) The Class A pathogen requirements in §503.32 (a)(3) through (a)(8) shall be met either prior to meeting or
at the same time the vector attraction reduction requirements in §503.33, except the vector attraction
reduction requirements in §503.33 (b)(6) through (b)(8), are met.
1((3) Class A —Alternative 1. (i) Either the density of fecal coliform in the sewage sludge shall be less than 1000
Most Probable Number per gram of total solids (dry weight basis), or the density of Salmonella sp. bacteria in
the sewage sludge shall be less than three Most Probable Number per four grams of total solids (dry weight
basis) at the time the sewage sludge is used or disposed; at the time the sewage sludge is prepared for sale
or give away in a bag or other container for application to the land; or at the time the sewage sludge or
material derived from sewage sludge is prepared to meet the requirements in §503.10 (b), (c), (e), or (f).
(ii) The temperature of the sewage sludge that is used or disposed shall be maintained at a specific value for
a period of time.
(A) When the percent solids of the sewage sludge is seven percent or higher, the temperature of the sewage
sludge §hall be 50 degrees Celsius or higher; the time period shall be 20 minutes or longer; and the
temperature and time period shall be determined using equation (2), except when small particles of sewage
sludge are heated by either warmed gases or an immiscible liquid.
__ 131,700, 000
100.1400r Eq. (2)
Where,
D=time in days.
t=temperature in degrees Celsius.
(B) When the percent solids of the sewage sludge is seven percent or higher and small particles of sewage
sludge are heated by either warmed gases or an immiscible liquid, the temperature of the sewage sludge
shall be 50 degrees Celsius or higher; the time period shall be 15 seconds or longer; and the temperature and
time period shall be determined using equation (2).
(C) When the percent solids of the sewage sludge is less than seven percent and the time period is at least
15 seconds, but less than 30 minutes, the temperature and time period shall be determined using equation
(2)
(D) When the percent solids of the sewage sludge is less than seven percent; the temperature of the sewage
sludge is 50 degrees Celsius or higher; and the time period is 30 minutes or longer, the temperature and time
period shall be determined using equation (3).
50, 070, 000
= 100.14001 Eq. (3
Where,
D=time in days.
t=temperature in degrees Celsius.
(4) Class A Alternative 2. (i) Either the density of fecal coliform in the sewage sludge shall be less than 1000
Most Probable Number per gram of total solids (dry weight basis), or the density of Salmonella sp. bacteria in
the sewage sludge shall be less than three Most Probable Number per four grams of total. solids (dry weight
basis) at the time the sewage sludge is used or disposed; at the time the sewage sludge is prepared for sale
or give away in a bag or other container for application to the land; or at the time the sewage sludge or
material derived from sewage sludge is prepared to meet the requirements in §503.10 (b), (c), (e), or (f).
(ii)(A) The pH of the sewage sludge that is used or disposed shall be raised to above 12 and shall remain
above 12 for 72 hours.
(B) The temperature of the sewage sludge shall be above 52 degrees Celsius for 12 hours or longer during
the period that the pH of the sewage sludge is above 12.
(C) At the end of the 72 hour period during which the pH of the sewage sludge is above 12, the sewage
sludge shall be air dried to achieve a percent solids in the sewage sludge greater than 50.percent.
(5) Class A —Alternative 3. (i) Either the density of fecal coliform in the sewage sludge shall be less than 1000 .
Most,Probable Number per gram of total solids (dry weight basis), or the density of Salmonella sp. bacteria in
sewage sludge shall be less than three Most Probable Number per four grams of total solids (dry weight
basis) at the time the sewage sludge is used or disposed; at the time the sewage sludge is prepared for sale
or give away in a bag or other container for application to the land; or at the time the sewage sludge or
material derived from sewage sludge is prepared to meet the requirements in §503.10 (b), (c), (e), or (f).
(ii)(A) The sewage sludge shall be analyzed prior to pathogen treatment to determine whether the, sewage
sludge contains enteric viruses.
(B) When the density of enteric viruses in the sewage sludge prior to pathogen treatment is less than one
Plaque -forming Unit per four grams of total solids (dry weight basis), the sewage sludge is Class A with
respect to enteric viruses until the next monitoring episode for the sewage sludge.
(C) When the density of enteric viruses in the sewage sludge prior to pathogen treatment is equal to or
greater than one Plaque -forming Unit per four grams of total solids (dry weight basis), the sewage slud9e.is
Class A with respect to enteric viruses when the density of enteric viruses in the sewage sludge. after;
pathogen treatment is less than one Plaque -forming Unit per four grams of total solids (dry weight basis) and..
when the values or ranges of values for the operating parameters for the pathogen treatment process that
produces the sewage sludge that meets the enteric virus density requirement are documented.
(D) After the enteric virus reduction in paragraph (a)(5)(ii)(C) of this section is demonstrated for the pathogen
treatment. process, the sewage sludge continues to be Class A with respect to enteric viruses when,the "'
values for the pathogen treatment process operating parameters are consistent with the values or ranges of
values documented in paragraph (a)(5)(ii)(C) of this section.
(iii)(A) The sewage sludge shall be analyzed prior to pathogen treatment to determine whether the sewage
sludge contains viable helminth ova.
(B) When the density of viable helminth ova in the sewage sludge prior to pathogen treatment..is,less than* one
per four grams of total solids (dry weight basis), the sewage sludge is Class A with respect to viable helminth
ova until the next monitoring episode for the sewage sludge.
(C) When the density of viable helminth ova in the sewage sludge prior to pathogen treatment is equal to or
greater than one per four grams of total solids (dry weight basis), the sewage sludge is Class A with respect
to viable helminth ova when the density of viable helminth ova in the sewage sludge after pathogen treatment
is less than one per four grams of total solids (dry weight basis) and when the values or ranges of values for
the operating parameters for -the pathogen treatment process that produces the sewage sludge that meets the
viable helminth ova density requirement are documented.
(D) After the viable helminth ova reduction in paragraph (a)(5)(iii)(C) of this section is demonstrated for the
pathogen treatment process, the sewage sludge continues to be Class A with respect to viable helminth ova
when the values for the pathogen treatment process operating parameters are consistent with the values or
ranges of values documented in paragraph (a)(5)(iii)(C) of this section.
(6) Class A Alternative 4. (i)' Either the density of fecal coliform in the sewage sludge shall be less than 1000
Most Probable Number per gram of total solids (dry weight basis), or the density of Salmonella sp. bacteria in
the sewage sludge shall be less than three Most Probable Number per four grams of total solids (dry weight
basis) at the time the sewage sludge is used or disposed; at the time the sewage sludge is prepared for'sale
or give away in a bag or other container for application to the land; or at'the time the sewage sludge or
material derived from sewage sludge is prepared to meet the requirements in §503.10 (b), (c), (e), or (f).
(ii) The density of enteric viruses in the sewage sludge shall be less than one Plaque -forming Unit per four
grams of total solids (dry weight basis) at the time the sewage sludge is used or disposed; at the time -the
sewage sludge is prepared for sale or give away in a bag or other container for application to the land; or at
the time the sewage sludge or material derived from sewage sludge is prepared to meet the requirements in
§503.10 (b), (c), (e), or (f), unless otherwise specified by the permitting authority.
(iii) The density of viable helminth ova in the sewage sludge shall be less than one per four grams of total
solids (dry weight basis) at the time the sewage sludge is used or disposed; at the time the sewage sludge is
prepared for sale or give away in a bag or other container for application to the land; or at the time the
sewage sludge or material derived from sewage sludge is prepared to meet the requirements in §503.10 (b),
(c), (e), or (f), unless otherwise specified by the permitting authority.
(7) Class A —Alternative 5. (i) Either the density of fecal coliform in the sewage sludge shall be less than 1000
Most Probable Number per gram of total solids (dry weight basis), or the density of Salmonella, sp'. bacteria in
the sewage sludge shall be less than three Most Probable Number per four grams of total solids (dry weight
basis) at the time the sewage sludge is used or disposed; at the time the sewage sludge is prepared for sale
or given away in a bag or other container for application to the land; or at the time the sewage sludge or
material derived from sewage sludge is prepared to meet the requirements in §503.10(b), (c), (e), or (f).
(ii) Sewage sludge that is used or disposed shall be treated in one of the Processes to Further Reduce
Pathogens described in appendix B of this part.
k(8) Class A Alternative 6. (i) Either the density of fecal coliform in the sewage sludge shall be less than 1000
Most Probable Number per gram of total solids (dry weight basis), or the density of Salmonella, sp. bacteria in
the sewage sludge shall be less than three Most Probable Number per four grams of total solids (dry weight
basis) at the time the sewage sludge is used or disposed; at the time the sewage sludge is prepared for sale
or given away in a bag or other container for application to the land; or at the time the sewage sludge or
material derived from sewage sludge is prepared to meet the requirements in §503.10(b), (c), (e), or (f).
(ii) Sewage sludge that is used or disposed shall be treated in a process that is equivalent to a Process to
Further Reduce Pathogens, as determined by the permitting authority.
(b) Sewage sludge —Class B. (1)(i) The requirements in either §503.32(b)(2), (b)(3), or (b)(4) shall be met for
a sewage sludge to be classified Class B with respect to pathogens.
(ii) The site restrictions in §503.32(b)(5) shall be met when sewage sludge that meets the Class B pathogen
requirements in §503.32(b)(2), (b)(3), or (b)(4) is applied to the land.
(2) Class B—Alternative 1. (i) Seven representative samples of the sewage sludge that is used or disposed
shall be collected.
(ii) The geometric mean of the density of fecal coliform in the samples collected in paragraph (b)(2)(i) of this
section shall be less than either. 2,000,000 Most Probable Number per gram of total solids (dry weight basis)
or 2,000,000 Colony Forming Units per gram of total solids (dry weight basis).
(3) Class B—Alternative 2. Sewage sludge that is used or disposed shall be treated in one of the Processes
to Significantly Reduce Pathogens described in appendix B of this part.
X. (4) Class B—Alternative 3. Sewage sludge that is used or disposed shall be treated in a process that is
equivalent to a Process to Significantly Reduce Pathogens, as determined by the permitting authority.
(5) Site restrictions. (i) Food crops with harvested parts that touch the sewage sludge/soil mixture and are
totally above the land surface shall not be harvested for 14 months after application of sewage sludge.
(ii) Food crops with harvested parts below the surface of the land shall not be harvested for 20 months after
application of sewage sludge when the sewage sludge remains on the land surface for four months or longer
prior to incorporation into the soil.
(iii) Food crops with harvested parts below the surface of the land shall not be harvested for 38 months after
application of sewage sludge when the sewage sludge remains on the land surface for less than four months
prior to incorporation into the soil.
(iv) Food crops, feed crops, and fiber crops shall not be harvested for 30 days after application of sewage
sludge.
(v) Animals shall not be grazed on the land for 30 days after application of sewage sludge.
(vi) Turf grown on land where sewage sludge is applied shall not be harvested for one year after application of
the sewage sludge when the harvested.turf is placed on either land with a high potential for public exposure
or a lawn, unless otherwise specified by the permitting authority.
(vii) Public access to land with a high potential for public exposure shall be restricted for one year after
application of sewage sludge.
(viii) Public access to land with a low potential for public exposure shall be restricted for 30 days after
-application of sewage sludge.
(c) Domestic septage. (1) The site restrictions in §503.32(b)(5) shall be met when domestic septage is applied
to agricultural land, forest, or a reclamation site; or
(2) The pH of domestic septage applied to agricultural land, forest, or -a reclamation site shall be raised to 12
or higher by alkali addition and, without the addition of more alkali, shall remain at 12 or higher for 30 minutes
and the site restrictions in §503.32 (b)(5)(i) through (b)(5)(iv) shall be met.
[58 FR 9387, Feb. 19, 1993, as amended at 64 FR 42571, Aug. 4, 1999]
k§ 503.33 Vector attraction reduction.
7� (a)(1) One of the vector attraction reduction requirements in §503.33 (b)(1) through (b)(10) shall be met when
bulk sewage sludge is applied to agricultural land, forest, a public contact site, or a reclamation site.
(2) One of the vector attraction reduction requirements in §503.33 (b)(1) through (b)(8) shall be met when bulk
sewage sludge is applied to a lawn or a home garden.
*3) One of the vector attraction reduction requirements in §503.33 (b)(1) through (b)(8) shall be met when
sewage sludge is sold or given away in a bag or other container for application to the land.
A(4) One of the vector attraction reduction requirements in §503.33 (b)(1) through (b)(1 1) shall be met when
sewage sludge (other than domestic septage) is placed on an active sewage sludge unit.
(5) One of'the vector attraction reduction requirements in §503.33 (b)(9), (b)(10), or (b)(12) shall be met when
domestic septage is applied to agricultural land, forest, or a reclamation site and one of the vector attraction
reduction requirements in §503.33 (b)(9) through (b)(12) shall be met when domestic septage is placed on an
active sewage sludge unit.
(b)(1) The mass of volatile solids in the sewage sludge shall be reduced by a minimum of 38 percent (see
calculation procedures in "Environmental Regulations and Technology —Control of Pathogens and Vector
Attraction in Sewage Sludge") EPA-625/R-92/013, 1992, U.S. Environmental Protection Agency, Cincinnati,
Ohio 45268).
(2) When the 38 percent volatile solids reduction requirement in §503.33(b)(1) cannot be met for an.
anaerobically digested sewage sludge, vector attraction reduction can be demonstrated by digesting a portion
of the previously digested sewage sludge anaerobically in the laboratory in a bench -scale unit for 40
additional days at a temperature between 30 and 37 degrees Celsius. When at the end of the 40 days, the
volatile solids in the sewage sludge at the beginning of that period is reduced by less than 17 percent, vector
attraction reduction is achieved.
(3) When the 38 percent volatile solids reduction requirement in §503.33(b)(1) cannot be met for an
aerobically digested sewage sludge, vector attraction reduction can be demonstrated by digesting a portion of
the previously digested sewage sludge that has a percent solids of two percent or less, aerobically in the
laboratory in a bench -scale unit for 30 additional days at 20 degrees Celsius. When afthe end of the 30 days,
the volatile solids in the sewage sludge at the beginning of that period is reduced by less than 15 percent,
vector attraction reduction is achieved.
(4) The specific oxygen uptake rate (SOUR) for sewage sludge treated in an aerobic process shall be equal to
or less than 1.5 milligrams of oxygen per hour per gram of total:solids (dry weight basis) at a temperature of
20 degrees Celsius.
(5) Sewage sludge shall be treated in an aerobic process for 14 days or longer. During that time, the
temperature of the sewage sludge shall be higher than 40 degrees Celsius and the average temperature of
the sewage sludge shall be higher than 45 degrees Celsius.
(6) The pH of sewage sludge shall be raised to 12 or higher by alkali addition and, without the addition of
more alkali, shall remain at 12 or higher for two hours and then at 11.'5 or higher for an additional'22 hours.
(7) The percent solids of sewage sludge that does not contain unstabilized solids generated in a primary
wastewater treatment process shall be equal to or greater than 75 percent, based on the moisture content: and
total solids prior to mixing with other materials.
(8) The percent solids of sewage sludge that contains unstabilized solids generated in a primary wastewater
treatment process shall be equal to or greater than 90 percent based on the moisture content and total solids
prior to mixing with other materials.
(9)(i) Sewage sludge shall be injected below the surface of the land.
(ii) No significant amount of the sewage sludge shall be present' on the land surface within one hour after the
sewage sludge is injected.
(iii) When the sewage sludge that is injected below the surface of the land is Class A with respect to
pathogens; the sewage sludge shall be injected below the land surface within eight hours after being
discharged from the pathogen treatment process.
(10)(i) Sewage sludge applied to the land surface or placed on an active sewage sludge unit shall be
incorporated into the soil within six hours after application to or placement on the land, unless'otherwise
specified by the permitting authority:
(ii) When sewage sludge that is incorporated into. the soil is Class A with respect to pathogens, the sewage
sludge shall be applied to or placed on the land within eight hours after being discharged from the pathogen
treatment process.
(11) Sewage sludge placed on an active sewage sludge unit shall be covered. with soil or other material at the
end of each operating day.
(12) The pH of domestic septage shall be raised to 12 or higher by alkali addition and, without the addition of
more alkali, shall remain at 12 or higher -for 30 minutes.
[58 FIR,9387, Feb. 19, 1993, as amended at 64 FIR 42571, Aug. 4, 1999]
Subpart E—Incineration
§ 503.40 Applicability.
(a) This subpart applies to a person who fires sewage sludge in a sewage sludge incinerator, to a sewage
sludge' incinerator, and to sewage sludge fired in a sewage sludge incinerator.
(b) This subpart applies to the exit gas from a sewage sludge incinerator stack.
(c) The management practice in §503,:45(a), the frequency of monitoring requirement for total hydrocarbon
concentration in §503.46(b) and the recordkeeping requirements for total hydrocarbon concentration in
§503.47(c) and (n) do not apply if the following conditions are met:
(1) The exit gas from a sewage sludge incinerator stack is monitored continuously for carbon monoxide.
(2) The monthly average concentration of carbon monoxide in the exit gas from a sewage sludge incinerator
stack, corrected for zero percent moisture and to seven percent oxygen, does not exceed 100 parts per
million on a volumetric basis.
(3) The person who fires sewage sludge in a sewage sludge incinerator retains the following information for
five years:
(i) The carbon monoxide concentrations in the exit gas; and
(ii) A calibration and maintenance log for the instrument used to measure the carbon monoxide concentration.
(4) Class I sludge management facilities, POTWs (as defined in 40 CFR 501.2) with a design flow rate equal
to or greater than one million gallons per day, and POTWs that serve a population of 10,000 people or greater
submit the monthly average carbon monoxide concentrations in the exit gas.to the permitting authority on
February 19 of each year.
[58 FR 9387, Feb. 19, 1993, as amended' at 59 FR 9099, Feb. 25, 1994]
§ 503.41 Special definitions.
(a) Air pollution control device is one or more processes used to treat the exit gas from a sewage sludge
incinerator stack.
(b) Auxiliary fuel is fuel used to augment the fuel value of sewage sludge. This includes, but is not limited to,
natural gas, fuel oil, coal, gas generated during anaerobic digestion of sewage sludge, and municipal solid
waste (not to exceed 30 percent of the dry weight of sewage sludge and auxiliary fuel together). Hazardous
wastes are not auxiliary fuel.
(c) Average daily concentration is the arithmetic mean of the concentration of a pollutant in milligrams per
kilogram of sewage sludge (dry weight basis) in the samples collected and analyzed in a month.
(d) Control efficiency is the mass of a pollutant in the sewage sludge fed to an incinerator minus the mass of
that pollutant in the exit gas from the incinerator stack divided by the mass of the pollutant in the sewage
sludge fed to the incinerator.
(e) Dispersion factor is the ratio of the increase in the ground level ambient air concentration for a pollutant at
or beyond the property line of the site where the sewage sludge incinerator is located to the mass emission
rate for the pollutant from the incinerator stack.
(f) Fluidized bed incinerator is an enclosed device in which organic matter and inorganic matter in sewage
sludge are combusted in a bed of particles suspended in the combustion chamber gas. .
(g) Hourly average is the arithmetic mean of all measurements, taken during an hour. At least two
measurements must be taken during the hour.
(h) Incineration is the combustion bf organic matter and inorganic matter in sewage sludge by high
temperatures in.an enclosed device.
(i) Incinerator operating combustion temperature is the arithmetic mean of the temperature readings in the
hottest zone of the furnace recorded in a day (24 hours) when the temperature is averaged and recorded at
least hourly during the hours the incinerator operates in a day.
Q) Monthly average is the arithmetic mean of the hourly averages for the hours a sewage sludge incinerator
operates during the month.
(k) Performance test combustion temperature is the arithmetic mean of the average combustion temperature
in the hottest zone of the furnace for each of the runs in a performance test.
(1) Risk specific concentration is the allowable increase in the average daily ground level ambient air
concentration for a pollutant from the incineration of sewage sludge at or beyond the property line of the site
where the sewage sludge incinerator is located.
(m) Sewage sludge feed rate is either the average daily amount of sewage sludge fired in all sewage sludge
incinerators within the property line of the site where the sewage sludge incinerators are located for the
number of days in a 365 day period that each sewage sludge incinerator operates, or the average daily
design capacity for all sewage sludge incinerators within the property line of the site where the sewage sludge
incinerators are located.
(n) Sewage sludge incinerator is an enclosed device in which only sewage sludge and auxiliary fuel are,fired.
(o)Stack height is the difference between the elevation of the top of a sewage sludge incinerator stack and
the elevation of the ground at the base of the stack when the difference is equal to or less than 65 meters.
When'the difference is greater than 65 meters, stack height is the creditable stack height determined in
accordance with 40 CFR 51.100 (ii).
(p) Total hydrocarbons means the organic compounds in the exit gas from a sewage sludge incinerator stack
measured using a flame ionization detection instrument referenced to propane.
(q) Wet electrostatic precipitator is an air pollution control device that uses both electrical forces .and water to
remove pollutants in the exit gas from a sewage sludge incinerator stack.
(r) Wet scrubber is an air pollution control device that uses water to remove pollutants in the exit gas from a
sewage sludge incinerator stack.
[58 FR 9387, Feb. 19, 1993, as amended at 64 FR 42571, Aug. 4, 1999]
§ 503.42 General requirements.
No person shall fire sewage sludge in a sewage sludge incinerator except in compliance With the
requirements in this subpart.
§ 503.43 Pollutant limits.
(a) Firing of sewage sludge in a sewage sludge incinerator shall not violate the requirements in the National
Emission Standard for Beryllium in subpart C of 40 CFR part 61.
(b) Firing of sewage sludge in a sewage sludge incinerator shall not violate the requirements in the National
Emission Standard for Mercury in subpart E of 40 CFR part 61.
(c) Pollutant limit -lead. (1) The average daily concentration for lead in sewage sludge fed to a sewage
sludge incinerator shall not exceed the concentration calculated using Equation (4).
0.1xALAAQSx86,400
C= DFx(1.-CE)xSF Eq. (4)
Where:
C = Average daily concentration of lead in sewage "sludge.
NAAQS = National Ambient Air Quality Standard for lead in micrograms per cubic meter.
DF = Dispersion factor'in micrograms.per cubic meter per gram per second.
CE = Sewage sludge incinerator control efficiency for lead in hundredths.
SF = Sewage sludge feed rate in metric tons per day (dry weight basis). '
(2) The dispersion factor (DF) in equation (4) shall be determined from an air dispersion model in accordance
with §503.43(e).
(i) When the sewage sludge stack height is 65 meters or less, the actual sewage sludge incinerator stack
height shall be used in the air dispersion model to determine the dispersion factor (DF) for equation (4).
(ii) When the sewage sludge incinerator stack height exceeds 65 meters, the creditable stack height shall be
determined in accordance with 40 CFR 51.100(ii) and the creditable stack height shall be used in the air
dispersion model to determine the dispersion factor (DF) for equation (4).
(3) The control efficiency (CE) for equation (4) shall be determined from a performance test of the sewage
sludge incinerator in accordance with §503.43(e).
(d) Pollutant limit —arsenic, cadmium, chromium, and nickel. (1) The average daily concentration for arsenic,
cadmium, chromium, and nickel in sewage sludge fed to a sewage sludge incinerator each shall. -not exceed
the concentration calculated using equation (5).
C = RSCx86,400 E
DFx(1— CE) xSF q. ( 5
)
Where:
C = Average daily concentration of arsenic, cadmium, chromium, or nickel in sewage sludge..
CE = Sewage sludge incinerator control efficiency for arsenic, cadmium, chromium, or nickel in. hundredths.
DF = Dispersion factor in micrograms per cubic meter per gram,per second.
RSC = Risk specific concentration for arsenic, cadmium, chromium, or nickel in micrograms per cubic meter.
SF = Sewage sludge feed rate in metric tons per day (dry weight basis). '
(2) The risk specific concentrations for arsenic, cadmium, and nickel used in equation (5) shall be obtained
from Table 1 of §503.43.
Table 1 of §503.43—Risk Specific Concentration -for Arsenic. Cadmium. and Nickel
Pollutant
Risk specific concentration (micrograms per cubic meter)
Arsenic
0.023
Cadmium
0.057
Nickel
12.0
(3) The risk specific concentration for chromium used in equation (5) shall be obtained from Table 2 of
§503.43 or shall be calculated using equation (6).
Table 2 of 5. 03.43—Risk Specific Concentration For Chromium
of Incinerator
uidized bed with wet scrubber
bed with wet scrubber and wet electrostatic
with wet scrubber
with wet scrubber and wet electrostatic
Risk specific concentration (micrograms per cubic
meter)
0.65
0.23
0.064
0.016
precipitator
RSC = 0.0085 Eq (o)
r
Where:
RSC=risk specific concentration for chromium in micrograms per cubic meter used in equation (5).
r=decimal fraction of the hexavalent chromium concentration in the total chromium concentration measured in
the exit gas from the sewage sludge incinerator stack in hundredths.
(4) The dispersion factor (DF) in equation (5) shall be determined from an air dispersion model in accordance
with §503.43(e).
(i) When the sewage sludge incinerator stack height is equal to or less than 65 meters, the actual sewage
sludge incinerator stack height shall be used in the air dispersion model to determine the dispersion factor
(DF) for equation (5).
(ii) When the sewage sludge incinerator stack height is greater than 65 meters, the creditable stack height
shall be determined in accordance with 40 CFR 51.100(ii) and the creditable stack height shall be used in the
air dispersion model to determine the dispersion factor (DF) for equation (5).
(5) The control efficiency (CE) for equation (5) shall be determined from a performance test of the sewage
sludge incinerator in accordance with §503.43(e).
(e) Air dispersion modeling and performance testing. (1) The air dispersion model used to determine the
dispersion factor in §503.43 (c)(2) and (d)(4) shall be appropriate for the geographical, physical, and
population characteristics at the sewage sludge incinerator site. The performance test used to determine the
control efficiencies in §503.43 (c)(3) and (d)(5) shall be appropriate for the type of sewage sludge incinerator.
(2) For air dispersion modeling initiated after September 3, 1999, the modeling results shall be submitted to
the permitting authority 30 days after completion of the modeling. In addition to the modeling results, the
submission shall include a description of the air dispersion model and the values used for the model
parameters.
(3) The following procedures, at a minimum, shall apply in conducting performance tests to determine the
control efficiencies in §503.43(c)(3) and (d)(5) after September 3, 1999:
(i) The performance test shall be conducted under representative sewage sludge incinerator conditions at the
highest expected sewage sludge feed rate within the design capacity of the sewage sludge incinerator.
(ii) The permitting authority shall be notified at least 30 days prior to any performance test so the permitting
authority may have the opportunity to observe the test. The notice shall include a test protocol with incinerator
operating conditions and a list of test methods to be used.
(iii) Each performance test shall consist of three separate runs using the applicable test method. The control
efficiency for a pollutant shall be the arithmetic mean of the control efficiencies for the pollutant from the three
runs.
(4) The pollutant limits in §503.43 (c) and (d) of this section shall be submitted to the permitting authority no
later than 30 days after completion of the air dispersion modeling and performance test.
(5) Significant changes in geographic or physical characteristics at the incinerator site or in incinerator
operating conditions require new air dispersion modeling or performance testing to determine a new
dispersion factor or a new control efficiency that will be used to calculate revised pollutant limits.
[58 FIR 9387, Feb. 19, 1993, as amended at 64 FIR 42572, Aug. 4, 1999]
§ 503.44 Operational standard —total hydrocarbons.
(a) The total hydrocarbons concentration in the exit gas from a sewage sludge incinerator shall be corrected
for zero percent moisture by multiplying the measured total hydrocarbons concentration by the correction
factor calculated using equation (7).
Correction factor 1
Eq. (7)
(percent moisture) (I
Where:
X=decimal fraction of the percent moisture in the sewage sludge incinerator exit gas in hundredths.
(b) The total hydrocarbons concentration in the exit gas from a sewage sludge incinerator shall be corrected
to seven percent oxygen by multiplying the measured total hydrocarbons concentration by the correction
factor calculated using equation (8)..
Correction factor 14 _
(oxygen) (21— Y) (8)
Where:
Y=Percent oxygen concentration in the sewage sludge incinerator stack exit gas (dry volume/dry volume).
9'
(c) The monthly -average concentration for total hydrocarbons in the exit gas from a sewage sludge incinerator
stack, corrected for zero percent moisture using the correction factor from equation (7) and to seven percent
oxygen Using the correction factor from equation (8), shall not exceed 100 parts per million on a volumetric
basis when measured using the instrument required by §503.45(a).
§ 503.45 Management practices.
(a)(1) An instrument that continuously measures and records the total hydrocarbons concentration in the
sewage sludge incinerator stack exit gas shall be installed, calibrated, operated, and maintained for a sewage
sludge incinerator:
(2) The total hydrocarbons instrument shall employ a flame ionization detector; shall have a heated sampling
line maintained at a temperature of 150 degrees Celsius or higher at all times, and shall be calibrated at least
once every 24-hour operating period using propane.
(b) An instrument that continuously measures and records the oxygen concentration in the sewage sludge
incinerator stack exit gas shall be installed, calibrated, operated, and maintained for a sewage-aludge ,:,
incinerator.
(c) An instrument that continuously measures and records information used to determine the moisture content
in the sewage sludge incinerator stack exit gas shall be installed;. calibrated, operated, and maintained for a
sewage sludge incinerator.
(d) An instrument that continuously measures and records combustion temperatures shall be installed,
calibrated, operated, and maintained'for a sewage sludge incinerator.
(e) Operation of a sewage sludge incinerator shall not cause the operating combustion temperature for the
sewage sludge incinerator to exceed the performance test combustion temperature by more than 20 percent.
(f) An air pollution control device shall be appropriate for the type of sewage sludge incinerator and the
operating parameters for the air pollution control device shall be adequate to indicate proper performance of
the air pollution control device: For sewage sludge incinerators subject to the requirements in subpart O of 40
CFR part 60, operation of the air pollution control device shall not violate the requirements for the air pollution
control device in subpart O of 40 CFR part 60. For all other sewage sludge incinerators, operation of the air
pollution control device'shall not cause a significant exceedance of the average value Ifor the air pollution
control device operating parameters from the performance test required by §503.43 (c)(3) and (d)(5).
(g) Sewage sludge shall not be fired in a sewage sludge incinerator if it is likely to adversely affect a
threatened or endangered species listed under section 4 of the Endangered Species Act or its designated
critical habitat.
(h) The instruments required in §'503.45(a)-(d) shall be appropriate for the type of.sewage sludge incinerator.
[58 FIR 9387, Feb. 19, 1993, as amended at 64 FIR 42573, Aug. 4, 1999]
§ 503.46 Frequency of monitoring.
(a) Sewage sludge. (1) The frequency of monitoring for beryllium shall be as required in subpart C of 40 CFR
part 61, and for mercury as required in subpart E of 40 CFR part 61.
(2) The frequency of monitoring for arsenic, cadmium, chromium, lead, and nickel in sewage sludge fed to a
sewage sludge incinerator shall be the frequency in Table 1 of §503.46.
Table 1 of §503.46—Frequency of Monitorinq—Incineration
Amount of sewage sludge1(metric tons per 365 day period)
Frequency
Greater than zero but less than 290
Once per year.
Equal to or greater than 290 but less than 1,500
Once per quarter (four times per year).
Equal to or greater than 1,500 but less than 15,000
Once per 60 days (six times per year).
Equal to or greater than 15,000
Once per, month (12 times per year).
1Amount of sewage sludge fired in a sewage sludge incinerator (dry weight basis).
(3) After the sewage sludge has been monitored for two years at the frequency in Table 1 of §503.46, the
permitting authority may reduce the frequency of monitoring for arsenic, cadmium, chromium, lead; and
nickel.
(b) Total hydrocarbons, oxygen concentration, information to determine moisture content, and combustion
temperatures. The total hydrocarbons concentration and oxygen concentration in the exit gas from a sewage
sludge incinerator stack, the information used to measure moisture content in the exit gas, and the
combustion temperatures for the sewage sludge incinerator shall be monitored continuously.
(c) Air pollution control device operating parameters. For sewage sludge incinerators subject to the
requirements in subpart 0 of 40 CFR part 60, the frequency of monitoring for the appropriate air pollution
control device operating parameters shall be the frequency of monitoring in subpart O of 40 CFR part 60. For
all other sewage sludge incinerators, the appropriate air pollution control device operating parameters shall be
at least daily.
(Approved by the Office of Management and Budget under control number 2040-0157)
[58 FR 9387, Feb. 19, 19.93, as amended at 64 FR 42573, Aug. 4, 1999] -
§ 503.47 Recordkeeping.
(a) The person who fires sewage sludge in a sewage sludge incinerator shall develop the information in
§503.47(b) through §503.47(n) and shall retain that information for five years.
(b) The concentration of lead, arsenic, cadmium, chromium, and nickel in the sewage sludge fed to the
sewage sludge incinerator.
(c) The total hydrocarbons concentrations in the exit gas from the sewage sludge incinerator stack.
(d) Information that indicates the requirements in the National Emission Standard for beryllium in subpart C of
40 CFR part 61 are met.
(e) Information that indicates the requirements in the National Emission Standard for mercury in subpart E of
40 CFR part 61 are met.
(f) The operating combustion temperatures for the sewage sludge incinerator.
(g) Values for the air pollution control device operating parameters.
(h) The oxygen concentration and information used to measure moisture content in the exit gas from the
sewage sludge incinerator stack.
(i) The sewage sludge feed rate.
6) The stack height for the sewage sludge incinerator.
(k) The dispersion factor for the site where the sewage sludge incinerator is located.
(1) The control efficiency for lead, arsenic, cadmium, chromium, and nickel for each sewage sludge
incinerator.
(m) The risk specific concentration for chromium calculated using equation (6), if applicable.
(n) A calibration and maintenance log for the instruments used to measure the total hydrocarbons
concentration and oxygen concentration in the exit gas from the sewage sludge incinerator stack, the
information needed to determine moisture content in the exit gas, and the combustion temperatures.
(Approved by the Office of Management and Budget under control number 2040-0157)
[58 FR 9387, Feb. 19, 1993, as amended at 64 FR 42573, Aug. 4, 1999]
§ 503.48 Reporting.
Class I sludge management facilities, POTWs (as defined in 40 CFR 501.2) with a design flow rate equal to or
greater than one million gallons per day, and POTWs that serve a population of 10,000 people or. greater shall
submit the information in §503.47(b) through §503.47(h) to the permitting authority on February 19 of each
year.
(Approved by the Office of Management and Budget under control number 2040-0157)
Appendix A to Part 503—Procedure To Determine the Annual Whole Sludge Application Rate for a
Sewage Sludge
Section 503.13(a)(4)(ii) requires that the product of the concentration for each pollutant listed in Table 4 of
§503.13 in sewage sludge sold or given away in a bag or other container for application to the land and the
annual whole sludge application rate (AWSAR) for the sewage sludge not cause the annual pollutant loading
rate for the pollutant in Table 4 of §503.13 to be exceeded. This appendix contains the procedure used to
determine the AWSAR for a sewage sludge that does not cause the annual pollutant loading rates in Table 4
of §503.13 to be exceeded.
The relationship between the annual pollutant loading rate (APLR) for a pollutant and the annual whole sludge
application rate (AWSAR) for 1a sewage sludge is shown in equation (1).
APLR =.0 X A WEAR X 0.001 (1)
Where:
APLR=Annual pollutant loading -rate in -kilograms per hectare per 365 day period.
C=Pollutant concentration in milligrams, per kilogram of total solids (dry weight basis).
AWSAR=Annual whole sludge application rate in metric tons per hectare per 365 day period (dry weight
basis).
0.001=A conversion factor.
To determine the AWSAR, equation (1) is rearranged into equation (2):
AWSAR = APLR (2)
Cx0.001
The procedure.used to determine the AWSAR for a sewage sludge is presented below.
Procedure:
1. Analyze a sample of the sewage sludge to determine the concentration for each of the pollutants listed in
Table 4 of §503.13 in the sewage sludge.
2. Using the pollutant concentrations from. Step 1 and the APLRs from Table 4 of §503.13, calculate an-_..,
AWSAR for each pollutant using equation (2) above.
3. The AWSAR for the sewage sludge is the lowest AWSAR calculated in Step 2.
"Appendix .B to Part 503—Pathogen. Treatment Processes
A. Processes To Significantly Reduce Pathogens (PSRP)
1. Aerobic digestion —Sewage sludge is agitated with air or oxygen to maintain aerobic conditions for a.
specific mean cell residence. time -at a specific temperature. Values for the mean cell residence time and
temperature shall be between 40 days at 20 degrees Celsius and 60 days at 15 degrees Celsius.
2. Air drying —Sewage sludge is dried on sand beds or on paved or unpaved"basins.'The sewage -sludge
dries fora minimum of.three months. During two of the three months, the ambient average daily temperature .
is above zero degrees Celsius.
3.'Anaerobic digestion "Sewage sludge, is treated in. the absence of air for a specific mean cell residence
time at a specific temperature. Values for the mean cell residence time and temperature shall be between 15
days at 35 to 55 degrees Celsius and 60 days at 20 degrees Celsius.
4. Composting —Using either the within -vessel, static aerated pile, or windrow composting methods, the
temperature of the sewage sludge is raised to 40 degrees Celsius or higher and.remains at 40 degrees
Celsius or higher' for. five days. For four hours during the five days, the temperature in the compost pile _
exceeds 55 degrees Celsius.
5. Lime stabilization —Sufficient lime is added to the sewage sludge to raise the pH of the sewage sludge.to
12 after two hours of contact.
B. Processes to Further Reduce Pathogens (PFRP)
1. Composting —Using either the within -vessel composting method or the static aerated pile composting
method, the temperature of the sewage sludge is maintained at 55 degrees Celsius or higher for three days.
Using,the windrow composting method, the temperature'of the sewage sludge is maintained at 55 degrees or
higher for 15 days or longer. During the period when the compost is maintained at 55 degrees or. higher, there
shall be a.minimum of five turnings of the windrow.
2. Heat drying —Sewage sludge is dried by direct or indirect contact with hot gases to, reduce the moisture
content of the sewage sludge to 10 percent or lower. Either the temperature of the sewage sludge particles
exceeds 80 degrees Celsius or the wet bulb temperature of the, 'gas- in contact with the sewage sludge as the
sewage sludge leaves the dryer exceeds.80 degrees Celsius.
3. Heat tr"eatment—Liquid sewage sludge is heated to a temperature of 180 degrees Celsius or higher for 30
minutes.
4. Thermophilic aerobic digestion —Liquid sewage sludge is agitated with air or oxygen -to maintain aerobic
conditions and the mean cell residence time of the sewage sludge is 10 days at 55 to 60 degrees Celsius.
5. Beta ray irradiation —Sewage sludge is irradiated With beta rays from an accelerator at dosages of at least
1.0 megarad at room temperature (ca: 20 degrees'Celsius).
(6) Gamma ray irradiation= Sewage sludge is irradiated with gamma rays from certain isotopes, such as60
Cobalt and137 Cesium, at dosages of at least 1.0 megarad at room temperature (ca. 20 'Celsius).
7. Pasteurization=The temperature of the sewage sludge is maintained at 70-degrees Celsius or higher for
30 minutes or longer.
[58 FR 9387, Feb. 19, 1993, as amended at 64 FR 42573, Aug. 4, 1999]