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HomeMy WebLinkAboutHISTORICALBarber, Jim From: Hardee, Ed Sent: Monday, November 02, 2009 9:36 AM To: Barber, Jim Cc: stolson@cheraw.com Subject: RE: FW: WQ0014248 Jim, Payment was received 10-27-09 from the Town of Cheraw, check number 4598. Ed Hardee Aquifer Protection Section Land Application Unit 1636 Mail Service Center Raleigh, NC 27699-1636 Phone (919) 715-6189 Fax (919) 715-0588 DISCLAIMER: Per Executive Order No. 150, all e=mails sent�to and from this'account are subject to the North Carolina Public Records Law and ;may be disclosed to third parties. From: Barber, Jim Sent: Monday, November 02, 2009 8:53 AM To: Hardee, Ed Subject: FW FW: WQ0014248 Ed; Here's the reply from the Town of Cheraw relative to my email about their annual permit fee being late. Can you help Ms. Tolson? . Thanks Jim Barber From: stolson@cheraw.com [mailto:stolson@cheraw.com] Sent: Thursday, October 29., 2009.10:03 AM To: Barber, Jim Subject: RE: FW: WQ0014248 Hi Jim, I spoke with our clerk after our conversation yesterday. A check was sent with the original invoice. The check was'dated 8/25/2009. When we were sent. the second notice, we found out that check had not yet cleared. A second check, dated 10/20/2009 has been sent. Do you think we should wait 30'days to see what happens? Thanks for your help, Sherry --------- Original Message -------- Subject: FW: WQ0014248 From: "Barber; Jim" <jim.barber(d)ncdenr.aov> Date:, Wed, October 28, 2009 2:20 pm 1 #To: "stolson(a)cheraw.com" <stolson(abcheraw.com> Ms. Tolson; Thanks for the information provided during our phone call this.afternoon concerning the Town of Cheraw Class "A" residuals program. As discussed, the above attachments are provided. The last document, page 3, is the panel from DWQ's database that indicates the annual permit administration fee is late. Once you have the opportunity to see if the town has received notice (cancelled check or notification from NC DWQ by receipt) that the bill has been resolved, please email me. If you have any questions relating to this issue, don't hesitate to call me at 910-433-3340 or Mr. Ed Hardee in our Raleigh Central office at 919-715-6189. Thanks again Jim Barber DWQ-Fayetteville Regional Office E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and may be disclosed to third parties. 2 N Barber, Jim From: Bernard, Jane Sent: Thursday, October 15, 2009 3:12 PM To: Barber, Jim Subject: W00014248 Jim, I've got an annual report that shows distribution of Biosolids in a field located on -the Scotland/Roberson line Allan Baucom Site. Matt Fleahman suggested I to pass this to you. The file is here but there is very little in it. You may get more information from central files if you need it. Jane (note: new e-mail address - iane.bernard(@ncdenr.gov ) Jane R. Bernard Environmental Specialist ------------------------------------ -- Aquifer Protection Section, DWQ Phone 919-791-4200 Fax 919-571-4718 - E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law.and may be disclosed to third parties- 1 rM CHERAW I Mr. Daryl Merritt DENR/DWQ/Water Quality Section 1617 Mail Service Center Raleigh, NC 27699-1617 Dear Mr. Merfitt: Enclosed. is the annual Biosolids marketing and distribution report. Please contact me if you'have any questions or comments. Sin cerely�/2 /� 3 S� SheTolson Industrial. Pretreatment Coordinator QA/QC Director /110 fz Q) (-C— � 2 Uk- flr-:--- S-, C Cheraw Public Utility Department Post Office Box 219, Cheraw, South Carolina 29520 843.537.8440, Fax 843.537.8442 www.chera-,v.com, zz MV 9 LG 7'A" I . NI- OFFICE �10N Jnit ANNUAL LAND APPLICATION CERTIFICATION FORM Permit#: W40014248 County: Chesterfield ,- = Yey ark'„ 2008 Facility Name (as shown on permit):. Town of Cheraw Land Application Operator: Phone: (843)537-8440 Land application of residual solids as allowed by the permit occurred during the past calender year? ® Yes ❑ No If No; skip Part A, and Part B and proceed to -the certification. Also, if residuals were generated but not land ,applied, please attach an explanation on how the residuals were handled. Part A: Total number of application fields in permit: Total number of fields land application occurred during the year: _ 1 Total amount of dry tons applied during the year for all application sites: 92 Total number of acres land application occurred during the ear:1 100 Part B: Facility was compliant during calendar year 2008 with all conditions of the land application permit (including but not limited -to items 1-12 below) issued by the Division of Water Quality. ® Yes 0 No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis were.performed on each site, receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed. any of the Pollutant Concentration Limits in Table 1, of 40 CFR Part 503.13 or the Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated, facilities). 7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All operations and maintenance requirements in the. permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed in accordance with the crop management plan. 11. No. runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 12. All buffer requirements as. specified on the permit were maintained during ti f residuals. "I certify, under penalty of law, that the above information is, to the best oIm nowe nd belief, true, accurate, and complete. I am aware that there are significant penalties for flti��ffige information, including the possibility of fines and imprisonment for knowing violat' nsY�R.ctuHLHr Jac rioN Information Processing unit q Ricky Ingram/Public Utility Director Permittee Name and Title (type or print) Sig re of larmittee Date Signature of Preparer* Date Signiture, of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) Preparer is defined in 40 CFR Part 503.9 (r) Author Daryl D. Merritt DENR FORM ACF 17/9nn91 TOWN OF CHERAW WASTEWATER TREATMENT FACILITY BIOSOLIDS REPORT 2008 PRESS DRY CAKE TONS LIME % TOTAL LIME $/ POLY $/ ;LBS. POLY/ LBS. POLY MONTH HOURS SOLIDS T. USED LIME DRY PROD. TON PROD. TON CAKE TON CAKE USED JAN 189.30 85.77 99.26 53.65 185.03 73.45 , 8.62 4.66 400.00 FEB 137.70 77.18 71.77 48.18 148.95 65.89 10.91 5.51 425.00 MAR 145.10 83.94 55.27 39.70 139.21 59.41 12.38 6.25 525.00 APR 118.50 73.92 ' 30.56 - 29.25 104.48 40.35 5.37 2.71 200.00 MAY 168.30 77.54 99.75 56.26 177.29 77.55 11.48 5.80 450.00 JUN 165.00 74.21 77.96 '51.23 152.17 73.63 13.35' 6.74 500.00 JUL 181.90 93.60 73.26 43.91 166.86 65.73 11.64 5.88 550.00 AUG - 155.00 88.72 65.46 42.46 154.18 63.71 11.72 5.92 525.00 SEP 102.50 53.87 36.87 45.67 80.74. _ 49.25 10.10 5.10 275.00 OCT 116.80 57.42 33.86 37.09 91.28 .54.70 14.65 7.40 425.00 NOV 4.10 2.13 2.28 51.70 4.41 76.24 26.86 11.73 25.00 DEC 27.90 14.31 15.08 51.31 29.39 75.67 16.01 6.99 100.00 TO 1512.10 782.61' 661.38 1,443.99 775.58 153.09 74.69 4,400.00- AVG 126.01 65.22 55.12' 45.87 120.33 64.63 12.76 10.71 366.67 MIN 4.10 2.131 2.28 29.25 4.41 40.35. .5.37 2.71 25.00 MAX 189.30 93.601 99.75 56.261 185.03 77.55 26.86 11.73 550.00 ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM PERMIT #: W00014248 FACILITY NAME: Town of Cheraw PHONE: (843) 537-8440 COUNTY:' Chesterfield -OPERATOR: .FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) ® Distribution and Marketing (complete Parts A, B, and C) Was the facility in operation during the past calendar year? ® - Yes-- ❑No No If No skip parts A; B, C and certify -form below _ Part A*: Part B*: Month - Sources s (include NPDES # if applicable) Volume (dry tons) Admendment/ Bulking Agent Residual In Product Out Recipient Information Name(s) Volume (dry tons) Intended use(s _. January SC0020249 99.26 85.77 185.03 Allan Baucom 92 so beans February SCO020249 71.77 77.18 148.95 March SCO020249 55.27 83.94 139.21 April SCO020249 30.56 73.9.2 104.48 May -SC0020249 99.75 '77.54 177.29 June SC0020249, 77:96 74.21 152.17 July SCO020249 73.26 93.60 166.86 August SCO020249 65.46 88.72 154.18.- September S00020249 36.87 53.87 80.74 October SCO020249 33.86 .57.42 91.28 November SCO020249 2.28 2.13 4.41 December SCO020249 15.08 14.31 29.39 Totals: Annual (dry tpns)-.T 661.38 782.61 1443'.99 ` Admendment(s) used: I Lime Bulking Agent s) used: *If more space than given is. required, please attach additional information sheet(s). ❑ Check box if additional sheet(s) are attached Part C: Facility was compliant during calendar year 2007 with all conditions of the permit (including but not limited to items 1-3 below) issued by the Division of Water Quality. ® Yes [INo If No, please provide a written description why the facility was not compliant. 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization'was received from the Division of Watei Quality. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware th the a are si ificant penalties for submitting false, informaiton, including the possibility of fines and imprisonment for knowing violations." 2 /.0- d 9 Sig a of Pe ee Date Signature of Preparer** Date (if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r) Author Daryl D. Merritt DENR FORM DMSDF (7/2002) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report Please note that your permit may contain additional parameters. to be analyzed than those required to be summarized on this form. Permit Number: WQ0014248 Facility Name: Town of ' Cheraw NPDES # or WQ#: SCO020249 WWTP Name: Town of Cheraw wwTP Residual Analysis Data Laboratory: 1) Davis & Brown 2) .Clemson University. 3) 4) 5) , Sample or Composite Date 1/16/08 1./1.6/08 8/09/08 3/19/08 5/21 /08 5/21 /08 7/15/08 7/15/08 9/17/08 9/17/08 11 /19/0 11 /19/0 Percent Solids 47.00 46.32- 55.94 58.00 52.10 54.02 46.10- 48.25 70.90 72.90 52.00 52.98 Arsenic 1.30 .1.11 2.19 1.14 2.04 0.959 Cadmium 0.212 1.11 0.219 1.14 2.04 0.9 Chromium 14.9 97.6 16.1 .13.9 125.0 ' 41.6 23.2 Copper 28.6 -48.0 30.1 15.4 42.7_ Lead 1.80 1.64 2.02 1.14 2.04 0.959 Mercury 0.049 ' 0.091 0.099 0.039 0.115 0.190 Molybdenum 1.40 1.46 10.1 4.58 2.52 3.84 Nickel 11.7 29.0 12.9 15.3 25.7 18.2 Selenium 1.30 1:1.1 2.19 1.14 .2.04 0.959 Zinc 81.7 170.0 97.7 62.7 128.0 78.3 TKN 1.7973 2.1049 - 1.6429 2.2218 1.1159 1.2269 Ammonia -Nitro a 0.6477 0.1251 0.0370 0.1036 0.2058 0.0566 Nitrate and Nitrite Total Phosphorus 0.0.381 1 .213_j 3. 0.0604 1 .1682 0.0037 1.1218 D.0016. 1.0767 0.0001 0.8471 0.0098 0.9390 661 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to'assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant en dfl s for submitting false information, including the possibility of fines and imprisonment for knowing violations. Signatur Prepa Date Author Daryl D. Merritt DENR FORM RSSF (7/2002) CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES BIOSOLIDS SAMPLE DATE-.WWn y 1e :20Q8 Biosolids Maximum Maximum Maximum Maximum Metal Allowable Allowable, Application Application Content, Metal App. Rate, Rate, Rate.. METALS ow Content Dom r1/Acre/Yr. OT/Acre/Yr. WT/AcrdYr. Arsenic, Total 1.38 • 41.00 1A0 325.38 660.77 Cadmium, Total 0.23 ` 39.00 1.70 1884.43 3768.87 Chromium, Total 15.85 1200.00 134.00 2113:42 4226.85 Copper, Total 30.43 1500.00 67.00 550.52 1101.05 Lead, Total ' 1.91 300.00 13.00 1697.22 3394.44 Mercury,`Totel 0.05 17.00 0.75 3596.94 7193.88 Molybdenum, Total 1.49 18.00 0.60 134.29 268.57 , Nickel, Total 12.45 420.00 18.70 375.60 751.20 Selenium, Total 1.38 36.00 . 4.50 813.46 1626.92 Zinc, Total 88.91 1525.00 ' 125.00 359.65 719.09 PCB 0.70 1.60 ' Actual metal content less than amount indicated.- Biosolids Biosolids Maximum Maximum Nutrient Nutrient Crop/Soil Application Application Content, Content, Requirement, Rate, Rate, oom % INAcre •' DT/Acre/Yr. WT/Acre/Yr. Ammonium Nitrogen 323.83 0.03 Organic Nitrogen 8662.58 . 0.87 Incorporated Available Nitrogen 5758.85 0.58 120:00 5.21 10A2 Surface Available Nitrogen 5601.70 0.67 120.00 5.30 10.60 Phosphorus as P205 6088.49. 0.61 80.06 3.30 6.59 Potassium as K20 .723.23 0.07 - 50.00 17.28 34.57 Calcium, Total 144257.34 14.43 Calcium as CaO, 201960.28 20.20 Calcium as CaCO3 (CCE) 359515.33 35.95 2000.00 1.39 2.78 Magnesium, Total 2450.35 0.25 Manganese 75.56 0.01 Sulfur 1300.13 0.13 Percent Masture 50.00 • These are typical values, and must be adjusted based upon specific site conditions - DT is Dry Tons of Biosolids. - WT is Wet Tons of Biosolids. CERTIFICATION: This blosoiid product has been produced by the Tam of CheraWs Wastewater . Treatment Plant by a beab. ant process that pasteurized plant residual solids using high temperature and lime (calcium oxide). The Town of Cheraw certifies that this biosolid complies with the Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A product and has a metal and nutrient content as presented above. DIRECTIONS FOR USE This bioaolid is intneded to be used as a soil amendment The blosolid land application race shall not exceed the most restrictive Maximum Application Rate as indicated in. the table above. The application rate for nitrogen, phosphorus, potassium, and calcium is dependent upon the crop gram and site soil characteristics. The user should contact the Clemson Extension Service (843-623-2134) and/or the Sal Conservation Service (843.823-2187) for aasistanoe in determining the proper application rate for each crop and site. In no case shall the land application rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension Service Circular N478 titled "Lime and Fertilizer Recommendations." THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY. AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES. THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS BIOSOLID PRODUCT. Mr. Ricky D. Ingram, Public Utlllty Director P. 0. Box 219; Cheraw, SC 29520 Telephone: 843-537-8440 FAX: 843-537-8442 Davis & Brown PO Box 15038 Quin6y, SC 29506 (843) 665-6746 FAX: (843) 629-1444 Certificate of Analysis Client: CHERAW, TOWN OF South Carolina Certification Number: 21117 P.O. BOX 219 CHERAW, SC 29520 Client #: 168 Receipt Date: 17-Jan-08 Contact: SHERRY TOLSON • Report Date: 31-Jan-08 Sample Date: 16-Jan-08 , SDG.#: SDG-058820 Approved By:�_,ir A.;. Van Ward Lab Director Reporting Parameter Result Limit Unit 'Method Flag Date Time Analyst LSID-130336 1iu-5 ,o8= 00 Acid Digestion (Solids) YES EPA 200.2 1/18/2008 9:30 DH pH (Waste) 12 S.U. EPA�90451) S16 1/22/2008 9:45 RBS TCLP PASS P/F SW-846 ' 1/30/2.008 WSF Ignitability >170 Deg. F. SW846 1010 S16 1/25/2008 10:30 KPB Percent Moisture 53.0 0.1 wt% SW846 3540 1/15/2008 17:15 BW Aluminum, Total 5060 0.425 mg/kg SW846 6010A 1/23/2008 16:29 DH Arsenic, Total <1.30 1.3 mg/kg SW846 6010A 1/24/2008 0:00 JR Cadmium, Total' <0.212 0.212 mg/kg SW846 601OA 1/22/2008 12:16 DH Chromium, Total 14.9 0.212 mg/kg SW846 6010A 1/22/2008 12:16 DH Copper, Total 28.6 0.212 mg/kg SW846 6010A 1/22/2008 12:16 DH Lead, Total 1.80 1.1 mg/kg SW846 6010A 1/21/2008' 15:18 DH Molybdenum, Total 1.40 0.85 mg/kg SW846 601OA 1/23/2008 16:29 DH Nickel, Total 11.7 0.212 mg/kg SW846 6010A 1/22/2008 12:16 DH Zinc, Total 81.7 0.212 mg/kg SW846 601OA 1/22/2008 12:16 DH Mercury, Total <0.049 0.049 mg/kg SW846 7470A 1/18/2008 13:28 DH Selenium, Total <1.30 1.3 mg/kg SW846 7741A 1/29/2008 13:11 JR PCB 0.66 mg/kg SW846 8080 S16 1/20/2008 22:20 CSU Reactivity, Cyanide <0.125 0.125 mg/kg SW846 9010 S16 1/24/2008 12:34 LEM Reactivity, Sulfide <25 25 mg/kg SW846 9030 S16 1/24/2008 10:15 LJN . Paint Filter PASS P/F SW8469095 S16 1/24/2008 7:00 KPB Page 1 12065 Lebanon Rd. 0 Mt. Juliet, TN 37122 ENVIRONMENTAL i-800 767-5859 SCIENCE CORP. Fax (615) 756-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Mr. Scott Fields January 29,2008 Davis 6 Brown P.O. Box 15038 Quinby, SC 29506 ESC Sample # L328165-02 Date Received January 18, 2008 Description Site ID Sample ID 130336 Project # Collected By Collection Date 01/16/08 14:30 Parameter Result Det. Limit Units Method Date/Time Analyst Dil. Ignitability See Footnote Deg. F - D93 01/25/08 1030 KPB 1` pH 12. su 9045D 01/22/08 0945 RBS 1 Paint Filter Test See Footnote 9095B 01/24/080700 KPB 1 Reactive.CN (SW846 7.3.3.2) BDL 0.125 mg/kg 9012B 01/24/08 1234 LEM 1 Reactive 'Sulf.(SW846'7.3.4.1) BDL 25. mg/kg 9034/9030 01/24/08 1015 KPB 1 TCLP Extraction - 1311 01/21/08 1015 LJN 1 Mercury BDL 0.0010 mg/1 7470A 01/22/08 1907 KBW 1 Arsenic BDL 0.050 mg/1 6010B 01/21/08 1658 LRL 1 Barium 0.31 0.050 mg/1 6010B 01/21/08 1658 LRL 1 Cadmium BDL 0.050 mg/1 6010B 01/21/08 1658 LRL 1 Chromium BDL 0.050 mg/1 6010B �01/21/08 1656 LRL 1 Lead BDL 0.050 mg/1 6010E 01/21/08 1658 LRL 1 Selenium 0.092 0.050 mg/1 6010B 01/21/08 1658 LRL 1 Silver BDL 0.050 mg/1 6010B 01/21/08 1658 LRL 1 TCLP ZHE Extraction - 1311 01/19/08 1113 MVE 1 TCLP Volatiles Benzene BDL 0.050 mg/1 8260B 01/22/08 0325 BRW 1 Carbon tetrachloride BDL 0.050 mg/1 8260B 01/22/08 0325 BRW 1 Chlorobenzene BDL 0.050 mg/1 8260B 01/22/08 0325 BRW 1 Chloroform BDL 0.25 mg/1 8260B 01/22/08 0325 BRW 1 1,2-Dichloroethane BDL 0.050 mg/1 8260B 01/22/08 0325 BRW- 1 1,1-Dichloroethene BDL 0.050 mg/1 8260B 01/22/08 0325 BRW 1 2-Butanone (MEK) BDL 0.50 mg/1 8260B 01/22/06 0325 BRW 1 Tetrachloroethene BDL 0.050 mg/1 8260B 01/22/08 0325 BRW 1 Trichloroethene BDL 0.050 mg/l 8260B 01/22/08 0325 BRW I Vinyl chloride BDL 0.050 mg/l 8260B 01/22/08 0325 BRW 1 Surrogate Recovery Dibromofluoromethane ill. 9 Rec. 8260B 01/22/08 0325 BRW 1 Toluene-d8 108. 9 Rec. 8260E 01/22/08 0325 BRW 1 4-Bromofluorobenzene 102. 8 Rec. 8260E 01/22/08 0325 BRW 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) . Notes: The reported analytical results relate only to the sample submitted This report shall not be reproduced, except in full, without the written approval from ESC. L328165-02 (IGNITABILITY)'- Did Not Ignite @ 170 L328165-02 (PAINT) - Contains No Free Liquid Page 3 of 6 0 ENVIRONMENTAL SCIENCE CORP. REPORT OF ANALYSIS Mr. Scott Fields Davis 6 Brown P.O. Box 15030 Quinby, SC 29506 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-761-5859 Fax (615) 758-5859 Tax I.D. 62-0814-189 Est. 1970 January 29,2008 ESC Sample # L328165-02 Date Received January 18, 2008 Description Site ID Sample ID 130336 Project # Collected By Collection Date 01/16/08 14:30 Parameter Result Det. Limit Units Method Date/Time Analyst Dil. TCLP Pesticides Chlordane BDL 0.0050 mg/l 8081A 01/24/08_2130 CSU 1 Endrin BDL 0.0050 mg/l 8081A 01/24/08 2130 CSU 1 Heptachlor BDL 0.0050 mg/1 8081A 01/24/08 2130 CSU 1 Lindane BDL 0.0050 mg/1 8081A 01/14/08 2130 CSU 1 Methoxychlor BDL 0.0050 mg/l 8081A O1/24/08 2130 CSU 1 Toxaphene BDL 0.010 mg/l 8081A 01/24/08 2130 CSU 1 Surrogate Recovery Decachlorobiphenyl 67.6 % Rec. 6081A 01/24/08 2130 CSU 1 Tetrachloro-m-xylene 61.8 % Rec. 8081A 01/24/08 2130 CSU 1 TCLP Herbicides 2,4,5-TP (Silvex) BDL 0.020 mg/1 8151A 01/28/OB 1351 JSW 10 2,4-D BDL 0.020 mg/l 8151A 01/28/08 1351 JSW 10 Surrogate Recovery 2,4-Dichlorophenyl Acetic Acid 156. % Red. 8151A 01/28/08 1351 JSW 10 TCLP Semi-Volatiles 1,4-Dichlorobenzene BDL 0.10 mg/l 8270C 01/23/08 1629 CMJ 1 2,4-Dinitrotoluene BDL 0.10 mg/l 8270C 01/23/08 1629 CMJ 1 Hexachlorobenzene BDL 0.10 mg/1 8270C 01/23/08 1629 CMJ 1 Hexachloro-1,3-butadiene BDL 0.10 mg/l 8270C 01/23/OB 1629 CMJ 1 Hexachloroethane BDL 0.10 mg/l 8270C 01/23/08 1629 CMJ 1 Nitrobenzene BDL 0.10 mg/l 8270C 01/23/08 1629 CMJ 1 Pyridine BDL 0.10 mg/l 82,70C 01/23/08 1629 CMJ 1 m&p-Cresol BDL 0.10 mg/1 8270C 01/23/08 1629 CMJ 1 o-Cresol BDL 0.10 mg/l 8270C 01/23/00 1629 CMJ 1 . Pentachlorophenol BDL 0.10 mg/1 9270C 01/23/08 1629 CMJ 1 2,4,5-Trichlorophenol BDL 0.10 mg/l 8270C 01/23/08 1629 CMJ 1 2,4,6-Trichlorophenol BDL 0.10 mg/l 8270C 01/23/08 1629 CMJ 1 Surrogate Recovery Nitrobenzene-d5 58.3 % Rec. 8270C 01/23/08 1629 CMJ 1 2-Fluorobiphenyl 53.1 % Rec. 8270C 01/23/08 1629 CMJ 1 p-Terphenyl-dl4 72.3 % Rec. 8270C 01/23/08 1629 CMJ 1 Phenol-d5 35.8 % Rec. 8270C 01/23/09 1629 CMJ 1 2-Fluorophenol 45.1 % Rec." 8270C 01/23/08 1629 CMJ 1 2,4,6-Tribromophenol 97.4 % Rec. 8270C 01/23/08 1629 CMJ 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Notes: The reported analytical results relate only to the sample submitted This report shall not be reproduced, except in full, without the written approval from ESC. All samples analyzed in adcordance with 40 CFR, Part 136.3 Reported: 01/29/08 14:06 Printed: 01/29/08 15:00 L328165-02 (IGNITABILITY) - Did Not Ignite @ 170 L328165-02, (PAINT) - Contains No Free Liquid Page 4 of 6 Attachment A List of Analytes with QC'Qualifiers Sample # Analyte Qualifier L328165-02 2,4,5-TP (Silvex) 0 2,4-D OJ5 2,4-Dichlorophenyl Acetic Acid J1 Methoxychlor J3 Page 5 of 6 Attachment B Explanation of QC Qualifier Codes Qualifier Meaning J1 Surrogate recovery limits have been exceeded; values are outside,upper control limits J3 The associated batch QC was outside the established quality control range for precision. O (ESC) Sample diluted due to matrix interferences that impaired the ability to make an accurate analytical determination. The detection limit is elevated in order to reflect the necessary dilution. J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high Qualifier Report Information ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical results. Each qualifier is designated in the qualifier explanation as either EPA or ESC. Data qualifiers are intended to provide the ESC client with more detailed information concerning the potential bias of reported data. Because of the wide range of constituents and variety of matrices incorporated by most EPA methods,it is common for some compounds to fall outside of established ranges. These exceptions are evaluated and all reported data is valid and useable unless qualified as 'R' (Rejected). Definitions Accuracy - The relationship of the observed value of a known sample to the true value of a known sample. Represented by percent recovery and relevant to samples such as: control samples, matrix spike recoveries, surrogate recoveries, etc. Precision - The agreement between a set of samples or between duplicate samples. Relates to how close together the results are and is represented by Relative Percent Differrence. Surrogate - Organic compounds that are similar in chemical composition, extraction, and chromotography to analytes of interest. The surrogates are used to determine the probable response of the group of analytes that are chem- ically related to the surrogate compound. Surrogates are added to the sample and carried through all stages of preparation and analyses. TIC - Tentatively Identified Compound: Compounds detected in samples that are not target compounds, internal standards, system monitoring compounds, or surrogates. Page 6 of 6 DAVIS & BROWN Data Qualifiers Within the attached report, some analytical data may be reported as "Qualified Data" .as indicated by a "Data Qualifier" or "flag" next to the result. The.data qualifier "S" indicates that the analysis was performed by another SC certified Lab. This table summarizes the South Carolina Lab Certification Numbers for those laboratories. S South Carolina Lab Certification Number: 99040001 S1 South Carolina Lab Certification Number: 96031 S2 South Carolina Lab Certification Number: 23105 S3 South Carolina Lab Certification Number: 10120 ". S4 South Carolina Lab Certification Number: 84002 S5 South Carolina Lab Certification Number: 3211.7 S6 Agricultural Service Laboratory Clemson University S7 South Carolina Lab Certification Number: 36001 S8 ********** S9 South Carolina Lab Certification Number: 94014001; 94014002 S 10 South Carolina Lab Certification Number: 84009 S 11 South Carolina Lab Certification Number: 96023; 96026; 96031; 9800 1;73006 S12 AASHTO R18 Certified S 13 South Carolina Lab Certification Number: 96012 S 14 South Carolina Lab Certification Number: 89002 - S15 ********** S16 South Carolinalab Certification Number: 84004 S 17 South Carolina Lab Certification Number: 96037001 S 18 South Carolina Lab Certification Number: 95005 S 19 South Carolina Lab Certification Number: 23104 S20 South Carolina Lab Certification Number: 96027001 S21 South Carolina Lab Certification Number: 21005 S22 South Carolina Lab Certification Number: 24110 S23 South Carolina Lab Certification Number: 84001001 S24 South Carolina Lab Certification Number: 82014001 S25 Sam levas analyzed by Microsee s, Inc Laboratory S26 North Carolina Lab Certification Number: 21 Wilson Division NC00120) S27 South Carolina Lab Certification Number: 40569 I i' Revision 06/05 Dataqual (SubLabs) .wpd CHAIN Page of __L__ OF CUSTODY RECORD DAVIS & BROWN Post Office an Ism 124 West McIver Road Ouift South CamMa 29506 Florence. South Carotins 2M1 Telephone (843) 665-6746 5'8a2D Use Codes in the boxes to indicate whether sample was filtered or preserved. �mmiiiilllllllllll Neill I I low M,.gm-.M- Inn M.- I Mfj, ���Lq "*its R MINE I NA/ "-'J- WOW • Program Area: D - Drinking Water / G - Grouodwator / S - Solid / W - Waste Water / N - NPDES / O - Other A N I M A L W A S T E A N A L Y S I S R E P O R T Agricultural Service Laboratory LAB No. 10110 Clemson University TOLSON, SHERRY ACCOUNT COCHSFL PO BOX 219 DATE 02-01-2008 CHERAW SC 29520 CHERAWTO.WNOF656@BELLSOUTH.NET SAMPLE NO. 0116085:OMANURE: OTHER STORAGE: UNCOVERED -----------------RESULTS REPORTED ON AN AS -SAMPLED BASIS---------------------- lbs/ton Ammonium Nitrogen 0.03 % 0.60 Organic Nitrogen .0.80 % 16.05 Nitrate Nitrogen 176.49 ppm 0.35 ---------------------------------------------------------------' INCORPORATED AVAILABLE NITROGEN ESTIMATE 10.67 SURFACE AVAILABLE NITROGEN ESTIMATE 10.49 --------------------------------------------------------------- Phosphorus as P205 0.56 % 11.24 Potassium as K20 0.07 % 1.34 Calcium 13.36 % 267.28 Magnesium 0.23 % 4.54 Sulfur 0.12 % 2.41 Zinc 100.52 ppm 0.20 Copper 33.35 ppm 0.07 Manganese 70.87 ppm 0.14 Sodium '123.68 ppm 0.25 Moisture 53.68 % Calcium Carbonate Equivalency 33.31 % 666.11 ------------------------------------------------------------------------------ INCORPORATED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of organic-N, and 100% of.nitrate-N (if determined). Assumes the manure will be incorporated into the soil within hours of application. Assumes some loss of ammonium-N during application and prior to incorporation. SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be left on the surface of the soil with no incorporation by plowing or irrigation. Available nitrogen calculations are estimates and if nitrate-N was not re- quested the amount of available nitrogen may be slightly more than reported. Also, the actual amount may be more or less than the estimate depending on the composition of the manure, soil type, and environmental conditions. All of the potash in the animal waste should be plant available in the first year of application. Although not all of the phosphorous is available in the. first year, its availability should be comparable to that in commercial fertilizers. The rate of animal waste to apply for crop production is dependent on the nutrient content of the waste, method of application and incorporation, soil test, crop to be grown, and previous manure applications. In most cases, the plant available nitrogen content of the waste is used to determine the rate of application. The Agricultural Service Laboratory is a public service of Clemson University, an affirmative action and equal opportunity educational institution.- http://www.clemson.edu/aglabresultsICOCHSFLTOLSON,%20SHERRY0802011538451.htm 2/4/08 % moisture % solids lbs. solids/ton lbs. solids/500 tons 53.68 46.32 926.4 463200 % ppm lbs/ton % ppm Ibsfton as -sampled as-dampled as -sampled dry ton dry ton dry Ammonium Nitrogen 0.03 300 0.6 0.064767 647.6684 1.295337 Organic Nitrogen 0.8025 8025 16.05 1.732513 17325.13 34.65026 Nitrate Nitrogen 0.017649 176.49 0.35298 0.038102 381,0233 0.762047 Incorporated Available Nitrogen Estimate 0.5335 5335 10.67 1.15177 11517.7 23.03541 Surface Available Nitrogen Estimate 0.5245 5245 10.49 1.13234, 11323.4 22.6468 Phosphorus as P205 0.562 5620 11.24 1,213299 12132.99 24.26596 Potassium as K20 0.067 670 1.34 0.144646 1446.459 2.892919 Calcium 13.364 133640 267.28 28.85147 288514.7 577.0294 Magnesium 0.227 2270 4.54 0.490069 4900.691 9.801382 Sulfur 0.1205 1205 2.41 0.260147 2601.468 5.202936 Zinc 0.010052 100.52 0.20104 0.021701 217.0121 0.434024 Copper 0.003335 33.35 0.0667 .0.0072 71.99914 0.143998 Manganese 0.007087 70.81 0.14174 0.0153 153.0009 0.306002 Sodium 0.012368 123.68 0.24736 0.026701 267.0121 0.534024 Calcium Carbonate Equivalency 33.3055 333055 666.11 71.90307 719030.7 1438.061 CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES BIOSOLIDS SAMPLE DATEr,! _arc 9; 2008 Biosolids Maximum Maximum Maximum Maximum. Metal Allowable Allowable Application Application Content, Metal App. Rate, Rate, Rate, METALS ppm Content, ppm WAcre/Yr. DT/AcrefYr. WT/Acre/Yr. Arsenic, Total 0.96 • 41.00 1.80 470.27 940.54 Cadmium, Total 0.96 • 39.00 1.70 444.14 888.29 Chromium, Total 84.14 1200.00 134.00 398.16 796.31 Copper, Total 41.38 1500.00 67.00 404.79 809.58 Lead, Total 1.41 300.00 , 13.00 2298.78 4597.56 Mercury, Total 0.08 17.06 0.75 2390.11 4780.22 Molybdenum, Total 1.26 18.00 0.80 158.90 317.81 Nickel, Total 25.00 420.00 18.70 167.00 374.00 Selenium, Total 0.96 36.00" 4.50 1175.68 2351.35 Zinc, Total 146.55 1525.00 - 125.00 213.24 426.47 PCB BDL 1.60 • Actual metal content less than amount Indicated. Biosdids Nutrient Content, ppm Biosdids Nutrient Content, % Crop/Soil Requirement, #/Acre •• Maximum Application Rate, DT/Acre/Yr. Maximum Application Rate, WT/Acre/Yr. Ammonium Nitrogen 625.67 , 0.06 Organic Nitrogen 9899.00 0.99 Incorporated Available Nitrogen 6922.60 0.69 120.00 4633 8.67 Surface Available Nitrogen 6734.89 0.67 120.00 4.45 8.91 Phosphorus as P205 5841.08 0.58 80.00 3.42 6.85 Potassium as K20 1264.75 0.13 " 50.00 9.88 19.77 Calcium, Total 131051.13 13.11 Calcium as C20 183471.58 18.35. Calcium as CaCO3 (CCE) 337705.58 33.77 2000.00 1.48 2.96 Magnesium, Total 2301.57 0.23 Manganese 67.04 0.01 Sulfur 1202.18 0.12 Percent Moisture 50.00 •• These are typical values and must be adjusted based upon specific site conditions DT is Dry Tons of Blosdids. WT is Wet Tons of Blosdids. CERTIFICATION: This biosdid product has been produced by the Town of Cho w's Wastewater Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature and lime (calcium oxide). The Town of Cheraw certifies that this biosdid complies with the Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has a metal and nutrient content as presented above. DIRECTIONS FOR USE: This biosdid is intneded to be used as a sail amendment. The biosdid land application rate shalt not exceed the most restrictive Maximum Application Rate as indicated in the table above. The application rate for nitrogen, phosphorus, potassium, and calcium is dependent upon the prop grown and site soil characteristics. The user should contact the Clemson Extension Service (843-623-2134) and/or the Soil Conservation Service (843-623-2187) for assistance in determining the proper application rate for each crop and site. in no case shall the land application rate exceed the agronomic rate for the crop grown. •User should also refer to the Clemson Extension Service Circular #476 titled "Lime and Fertilizer Recommendations." THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY. .. AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES. THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING"OF THIS BIOSOLID PRODUCT. Mr. Ricky D. Ingram, Public Utility Director P. O. Box 219; Cheraw, SC 29520 Telephone: 843-537-8440 FAX: 843-537-8442 Davis & Brown PO Box 15038 Quinby, SC 29506 (843) 665-6746 FAX: (843) 629-1444 Certificate of Analysis Client: CHERAW, TOWN OF P.O. BOX 219 CHERAW, SC 29520 Client #: 168 Contact: SHERRY TOLSON South Carolina Certification Number: 21117 Receipt Date: 20-Mar-08 Report Date: 15-Apr-08 Sample Date: 19-Mar-08 v SDC #: SDG-059817 Approved By: f 'A- IZ/ �_.._. Lab Sample ID: LSID-132469 Van Ward Sample ID: B107S01,IDS_03=.F9'-08-500' Lab Director Parameter Result Reporting Limit Unit Method Flag Date Time Analyst Acid Digestion (Solids) YES EPA 200.2, 3/20/2008 10:50 DH Percent Moisture 42.0 0.1 wt% SW846 3540 3/24/2008 16:30 BW Aluminum, Total 7040 0.558 mg/kg SW846 6010B 4/7/2008 16: I8 DH Arsenic, Total <1.11 1.1 1 mg/kg SW846 6010B 3/28/2008 12:03 DH Cadmium, Total <1.11 1.11 mg/kg SW846 6010B 3/27/2008 16:01 DH Chromium, Total 97.6 1.11 mg/kg SW846 6010B N27/2008 16:.01 DH Copper, Total 48.0 1.11 mg/kg SW846 6010B 3/27/2008 16:01 DH Lead, Total 1.64 1.11 mg/kg SW846 6010B 3/27/2008 16:01 DH Molybdenum, Total 1.46 1.12 mg/kg SW846 6010B 4/7/2008 16:18 DH Nickel, Total 29.0 I. i l mg/kg SW846 6010B 3/27/2008 16:01 DH Zinc, Total 170 0.14 mg/kg SW846 6010B 4/10/2008 1 1:44 DH Mercury; Total . 0.091 0,037 mg/kg SW846 7470A 4/10/2008 9:24 DH Selenium, Total <l.l 1 1.1 1 mg/kg SW846 7741A 3/28/2008 12:03 DH PCB BDL mg/kg SW846 8080 S16 3/28/2008 16:13 CSU Page 3 1'2065 Lebanori Rd. 0 Mt. Juliet, TN 37122 ENVIRONMENTAL (61'.) 758-5 - 1-800-767-S858 59 SCIENCE CORP. Fax (615) 758-5659 Tar. I.D. 62-0814289 ' Est. 1970 REPORT OF ANALYSIS Mr. Scott Fields March 31,2008 Davis 6 Brown P.O. Box 15038 Quinby, SC 29506 # ESC Sample L337765-01 Date Received March 25, 2008 Description 132469 Site ID Sample ID 132469 Project # Collected By Collection Date 03/19/08 13:20 Parameter Dry Result Det. Limit Units Method Date Analyst Total Solids 47.5 8 254OG 03/29/08 1513 JDW Polychlorinated Biphenyls PCB 1016 BDL 0.18 mg/kg 8082 03/28/08 1613 CSU PCB 1221 BDL 0.18 mg/kg 8082 03/28/08 1613 CSU PCB 1232 BDL 0.18 mg/kg 8082 03/28/08 1613 CSU PCB 1242 BDL 0.18 mg/kg 8082 03/28/OB 1613 CSU PCB 1248 BDL 0.18 mg/kg 8082 03/28/08 1613 CSU PCB 1254 BDL 0.18 mg/kg 8082 03/28/08 1613 CSU PCB 1260 BDL 0.18 mg/kg 8082 03/28/08 1613 CSU Results listed are dry weight basis. BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TNO02, WI - 998093910 Note: This report shall not be reproduced, except in full, without the written approval .from ESC. The reported analytical results relate only to the sample submitted Reported: 03/31/08 13:44 Printed: 03/31/08 13:45 Page 2 of 2 - —b— a va a A N I M A L W A S T E A N A L Y S I S R E P O R T Agricultural Service Laboratory LAB No. 30593 Clemson *University TOLSON, SHERRY ACCOUNT COCHSFL PO BOX 219 DATE 04-01-2008 CHERAW SC 29520 CHERAWTOWNOF656@BELLSOUTH.NET SAMPLE N0.�03;0=9085.Q MANURE: OTHER STORAGE: UNCOVERED -----------------RESULTS REPORTED ON AN AS -SAMPLED BASIS--------------- lbs/ton Ammonium Nitrogen 0.07 % 1.40 Organic Nitrogen 1.11 % 22.15 Nitrate Nitrogen --------------------------------------------------------------- 337.88 ppm 0.68 INCORPORATED AVAILABLE NITROGEN ESTIMATE 15.49 SURFACE AVAILABLE --------------------------------------------------------------- NITROGEN ESTIMATE 15.07 Phosphorus'as P205 0.65 % 13.07 Potassium as K20 0.14 % 2.83 Calcium 14.66 % 293.24 Magnesium 0.26 % 5.15 Sulfur 0.13 % 2,69 Zinc 109.64 ppm 0.22 Copper 36.92 ppm 0.07 Manganese 72.72 ppm 0.15 Sodium 190.20 ppm 0.38 Moisture 44.06 % Calcium Carbonate Equivalency 37.78 % 755.65 ------------------------------------------------------------------------------ INCORPORATED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be incorporated into the soil within hours of application. Assumes some loss of ammonium-N during application and prior to incorporation. SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be left on the surface of the soil with no incorporation by plowing or irrigation. Available nitrogen calculations are estimates and if nitrate-N was not re- quested the amount of available nitrogen may be slightly more than reported. Also, the actual amount may be more or less than the estimate depending on the composition of the manure, soil type, and environmental conditions. All of the potash in the animal waste should be plant available in the first year of application. Although not all of the phosphorous is available in the first year, its availability should be comparable to that in commercial fertilizers. The rate of animal waste to apply for crop production is dependent on the nutrient content of the waste, method of application and incorporation, soil test, crop to be grown, and previous manure applications. In most cases, the plant available nitrogen content of the waste is used to determine the rate of application. The Agricultural Service Laboratory is a public service of Clemson University, an affirmative action and equal opportunity educational institution. ** http://www.clemson.edu/agsrvlb ** http://www. clemson. edu/aglabresults/C OCHSFLT'OLSON,%20SHERRY0804010925 5 93 .h... 4/2/200R % moisture _ % solids lbs. solids/ton lbs. solids/500 tons 44.06 55.94 1118.8 559400 % ppm , . lbstton. % ppm Ibstton - as -sampled as -sampled is -sampled dry ton dry ton dry Ammonium Nitrogen, 0.07 ' 700 1.4 .0.125134 1251.341 2.502681 Organic Nitrogen 1.1075 11075 22.15 1.9798 19798 - 39.596 Nitrate Nitrogen 0.033788 337.88 0.67576 0.0604 604.0043 1.208009 Incorporated Available Nitrogen Estimate 07745 7745 15.49 1.384519 13846.19 27.69038 Surface Available Nitrogen Estimate 0.7635 7535 15.07 1.346970 13469.79 26.93958 Phosphorus as P205 0.6535 6535 13.07 1.168216 11682.16 23.36432 Potassium as K20 0.1415 1415 - 2.83 0.25295 2529.496 5.058992 Calcium 14.662 146620 293.24 26.21023 262102.3 524.2045 Magnesium 0.2575 2575 5.15 0.460315 4603.146 9.206292 Sulfur 0.1345 1345 2.69 0.240436 2404.362.4.808724. Zinc 0.010964 109.64 0.21928 0.0196 195.9957 0.391991 Copper 0.003692 36.92 0.07384 0.0066 65.99928 0.131999 Manganese 0.007272 72.72 0.14544 0.013 129.9964 0.259993 Sodium 0.01902 190.2 0.3804 0.034001 340.0072 0.680014 Calcium Carbonate Equivalency 37.7825 377825 755.65 67.54112 675411.2. 1350.822 �March2008 CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES BIOSOLIDS SAMPLE DATE^Mav: 12 2008� Biosolids Maximum ' Maximum Maximum Maximum Metal Allowable Allowable Application Application Content, Metal App. Rate, ' Rate, ` Rate, METALS ppm Content, ppm #/Acre/Yr. DT/Acre/Yr. WT/Acre/Yr. Arsenic, Total 2.10 ' 41.00 1.80 214.11 428.22 Cadmium, Total 6.21 • 39.00 1.70 2022.15 4644.29 Chromium, Total 15.45 1200.00 134.00 2168.14 4336.27 Copper, Total 28.89 1500.00 67.00 579.85 1159.70 Lead, Total 1.94 300.00 13.00 1676A9 -3352.97 Mercury, Total 0.10 17.00 0.75 1973.48 3946.97 Molybdenum, Total 9.69 18.00 0.80 20.63 41•.27 Nickel, Total 12.38 420.00 18.70 377.62 755.25 Selenium, Total 2.10 36.00 4.50 535.27 1070.55 Zinc, Tote) 93.78 1525.00 125.00 333.29 666.58 PCB BDL 1.60 "Actual metal content less than amount Indicated. Biosolids Biosolids Maximum Maximum Nutrient Nutrient Crop/Soil Application Application Content, Content, Requirement, Rate, Rate, ppm % IWAcre" DT/Acre/Yr. WT/Acre/Yr. . Ammonium Nitrogen Organic Nitrogen Incorporated Available Nitrogen Surface Available Nitrogen Phosphorus as P205 Potassium as K20 Calcium, Total 185.12 0.02 8029.43 0.80 4998.15 0.50 120.00 4942.61 0.49 120.00 5609.03 0.56 80.00 1082.93 0.11 50.00 144400.22 14.44 6.100 12.00 6.07 12.14 3.57 7.13 11.54 23.09 Calcium as Ca0 202160.31 20.22 Calcium as CaCO3 (CCE) 354452.05 35.45 2000.00 1.41 2.82 Magnesium, Total 2448.17 .0.24 Manganese 83.30 0.01 Sulfur 1147.72 0.11 Percent Moisture 50.00 These are typical values and must be adjusted based upon specific site conditions DT is Dry Tons of Blosdids. ; WT is Wet Tons of Biosdids: CERTIFICATION: This biosolid product has been produced by the Town of Cheraw's Wastewater Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature and lime (calcium oxide). The Town of Cheraw certifies that this biosolid compiles with the Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has a metal and nutrient content as presented above. DIRECTIONS FOR USE: This biosclid is intneded to be used as a soil amendment. The biosdid land application rate shall not exceed the most restrictive Maximum Application Rate as indicated in the table above. The application rate for nitrogen, phosphorus, potassium, and calcium is dependent upon the crop grown and site soil characteristics. The user should contact the Clemson Extension Service (843-623-2134) and/or the Sal Conservation Service (843- i23-2187) for assistance in determining the proper application rate for each crop and site. In no case shall the land application rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension Service Circular #476 titled "Lime and Fertilizer Recommendations." THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY. AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES. THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS BIOSOLID PRODUCT. Mr. Ricky D. Ingram, Public Utility Director P.O. Box 219; Cheraw, SC 29520 Telephone: 843-53741440 FAX: 843-537-8442 PRODUCT USER NAME: Davis & Brown PO Box 15038 Quinby; SC 29506 (843) 665-6746 FAX: (843) 629-1444 Certificate of Analysis Client: CHERAW, TOWN OF South Carolina Certification Number: 21117 P.O. BOX 219 CHERAW, SC 29520 Client #: 168 Receipt Date: 22-May-08 Contact: SHERRY TOLSON Report Date: • 13-.tun-08 Sample. Date: 21-May-08 SDG #: SDG-06081 1 Approved By: Lab Sample ID: LSID-134706 Van Ward a Lab Director r'(1 MQ Sample ID: W 20,- BL0 SOLIDS - Parameter Result Reporting Limit Unit Method Flag Date Time Analyst Acid Digestion (Solids) YES EPA 200.2 5/28/2008. 9:30 DH Percent Moisture 47.9 0.1 wt% SW846 3540 5/27/2008 16:40 BW AILInllnunl, Total 4'180 438 mg/kg SW846 601 OB 5/29/2008 1 1:30 DH Arsenic, Total <2.19 2.19 nlg/kg SW846 601 OB 5/30/2008 1 1:20 DH CadnliLim, Total <0.2.19 0.219 nlg/kg SW846 6010B 6/3/2008 13:51 DH Chromium. Total 16.1 0.219 nlg/kg SW846 601OB 6/3/2008 13:51 DH Copper, Total 30.1 _ 0.219 nlg/kg SW846 601 OB 6/3/2008 13:51 DH Lead. Total 2.02 1.3 mg/kg SW846 601 OB 6/5/2008 14:23 DH Molybdenum, Total <10.1 10.1 mg/kg SW846 6010E 6/10/2008 . 9:53 DH Nickel, Total 12.9 0.219 mg/kg SW846 601 OB 6/3/2008 13:51 DH Zinc, Total 97.7 0.219 mg/kg SW846 601 OB 6/3/2008 13:51 DH Mercury, Total 0:099 0.014 nlg/kg SW846 7470A 6/6/2008 10:27. DH Selenium, Total <.2.19 2.19 mg/kg SW846 7741A 5/30/2008 1 1:20 DH PCB BDL nlg/kg SW8468080 S16 5/29/2008 22:58 LSB Page 1 0 1 ENVIRONMENTAL SCIENCE CORP. REPORT OF ANALYSIS [Ar. '."co-t Fields Dac'is & Brown F.U. Box 15038 Quinby, SC 29506 .nilie[, TIJ t?I. T.I:: I.h. A--'1F14 Eot . I.1-71, June 02,2008 ESC Sample # L347131-01 Date Received May 23, 2008. Description Site ID Sample ID 134706 Project # Collected By. Collection Date 05/21/08 10:00 Parameter Dry Result Det. Limit Units Method Date Analyst Total Solids 48.2 •. 2540C 05,130/08 1001 JDW Polychlorinated Biphenyls PCB 1016 BDL 0.18 mg/l:g 8082 05/29/08 2258 LSB FCB 1221 BDL 0.18 mg/kg 8082 05/29/08 2258 LSB PCB 1232 BDL 0.18 mg/kg 8082 05/29/OB 2258 LSB PCB 1243 BDL 0.18 mg/kg 8082 05/29/08 22258 LSB PCB 1248 BDL 0.18 mg/l:g 8082 05/29/08 2258 LSB PCB 1254 BDL 0.18 mg/kg 8082 05/29/08 2=58 LSB PCE 1260 BDL 0.18 mg/kg 808Z 05/29/08 2258 LSB Re:;ults listed are dry weight basis. BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 17Y - 90010, 1:YUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TNO02, WI - 998093910 Nnte: This report shall not be reproduced, except in full, without the written approval from ESC. The reported analytical results relate only to the sample submitted P.eporr.ed: 061 02/OS 09:38 Printed: 06/02/08 09:38 Page 2 of 2 DAVIS & BROWN Data Qualifiers Within the attached report, some analytical data may be reported as "Qualified Data" as indicated by a "Data Qualifier" or "flag" next to the result. The data qualifier "S" indicates that the analysis was performed by another SC certified Lab. This table summarizes the South Carolina Lab Certification Numbers for those laboratories. S South Carolina Lab Certification Number: 23101 S 1 South Carolina Lab Certification Number: 93013 S2 South Carolina Lab Certification Number: 23105 S3 South Carolina Lab Certification Number: 10120 S4 South Carolina Lab Certification Number: 84002 S5 South Carolina Lab Certification Number: 32117 S6 Agricultural Service Laboratory Clemson University S7 South Carolina Lab Certification Number: 36001 S8 ********** S9 South Carolina Lab Certification Number: 94014001; 94014002 S 1 O South Carolina Lab Certification Number: 84009 S1 1 South Carolina Lab Certification Number: 96023; 96026; 96031; 98001, 73006 S 12 AASHTO R18 Certified S 13 South Carolina Lab Certification Number: 96012 S 14 South Carolina Lab Certification Number: 89002 S15 ********* S 16 South Carolina Lab Certification Number: 84004 S 17 South Carolina Lab Certification Number: 96037001 S 18 South Carolina Lab Certification Number: 95005 S 19 South Carolina Lab Certification Number: 23104 S20 South Carolina Lab Certification Number: 96027001 S21 South Carolina Lab Certification Number: 21005 S22 South Carolina Lab Certification Number: 24110 S23 South Carolina Lab Certification Number: 84001001 S24 South Carolina Lab Certification Number: 82014001 S25 Sample was analyzed by Microsee s, Inc Laboratory S26 North Carolina Lab Certification Number: 21 (Wilson Division NC00120) S27 South Carolina Lab Certification Number: 40569 RC%iswn (K)A)? 1XIMLI of (SUTA1111R) .wpd CHAIN OF CUSTODY RECORD Nge_L of _L DAVIS & BROWN Post Office Boot 15M 124 WON Mckw Road OWnby. S011M Carolina WM mle ". scum cam= moll Tammnm gak.6"'m L-11-1 NAM/ Facility Nam TOWAI Of SAMEANALYSIS REQUIRED (z)—m temttka Dirt to specify tpeube compounds ar tegbods, Use Codes in the boxes to indicate I 011mv1 whether sample was filtered or preserued. Code. HNO3 w A H2SO4 = D AMA 5 JS EE € HCLol L& A&,., Ff NAOH.0 ZINCACETATE G SAMPLE ID DATE TE W REMARKS LAB ID 0, fill Rd' NATW)- Date Time Rdinquisbed by (SiGNKIURl:�• DaceRdWW�by (S�IGNATUREI- TIM Recci IS NATURE? Due Tuve by (SIGNATURE . raw Rccd%vd by (SIMM—URE)e ICED Lk:o 746S MID t 6 a4m commen s elf (;� C3 NO a N= Redalamry • Pr mm Am2. A. A N I M A L W A S T E A N A L Y S I S R E P O R T Agricultural Service Laboratory LAB No. 50992 Clemson University TOLSON, SHERRY ACCOUNT COCHSFL PO BOX 219 DATE 06-04-2008 CHERAW SC 29520 CHERAWTOWNOF656@BELLSOUTH.NET SAMPLE NO'y Qr521V8'S,0 MANURE: OTHER STORAGE: UNCOVERED -----------------RESULTS REPORTED ON AN AS -SAMPLED BASIS---------------------- lbs/ton Ammonium Nitrogen 0.02 % 0.40 Organic Nitrogen 0.87 % 17.35 Nitrate Nitrogen -----------------------------------------=--------------------- 19.99 ppm 0.04 INCORPORATED AVAILABLE NITROGEN ESTIMATE 10.80 SURFACE AVAILABLE --------------------------------------------------------------- NITROGEN ESTIMATE 10.68 Phosphorus as P205 0.61 % 12.12 Potassium as K20 0.12 % 2.34 Calcium 15.60 % 312.02 Magnesium 0.26 % 5.29 Sulfur 0.12 % 2.48 Zinc 102.64 ppm 0.21 Copper 55.64 ppm 0.11 Manganese 89.67 ppm 0.18 Sodium 231.21 ppm 0.46 Moisture 45.98 % Calcium Carbonate Equivalency 38.30 % 765.90 ------------------------------------------------------------------------------ INCORPORATED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be incorporated into the soil within hours of application. Assumes some loss of ammonium-N during application and prior to incorporation. SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of organic-N, and 100% of nitrate-N'(if determined). Assumes the manure will be left on the surface of the soil with no incorporation by plowing or irrigation. Available nitrogen calculations are estimates and if nitrate-N was not re- quested the amount of available nitrogen may be slightly more than reported. Also, the actual amount may be more or less than the estimate depending on the composition of the manure, soil type, and environmental conditions. All of the potash in the animal waste should be plant available in the first year of application. Although not all of the phosphorous is available in the first year, its availability should be comparable to that in commercial fertilizers. The rate of animal waste to apply for crop production is dependent on the nutrient content of the waste, method of application and incorporation, soil test, crop to be grown, and previous manure applications. In most cases, the plant available nitrogen content of the waste is used to determine the rate of application. The Agricultural Service Laboratory is a public service of Clemson University, an affirmative action and equal opportunity educational institution. http://www.clemson.edu/aglabresults/COCHSFLTOLSON,%20SHERRY0806041.638041.htm 6/6/08 % moisture % solids lbs. solids/ton lbs. solids/500 tons 45.98 54.02 1080.4 540200 % ppm lbs/ton % . ppm lbs/ton as -sampled as -sampled - as -sampled d ton d ton dry Ammonium Nitrogen 0.02 200 0.4 0.037023 370.2332 0.740466 Organic Nitrogen 0.8675 8675 17.35 1.605881 16058.87 32.11773 Nitrate Nitrogen 0.001999 19.99 0.03998 0:0037 37.00481 0.07401 Incorporated Available Nitrogen Estimate 0.54 5400 10.8 0.99963 9996.298 19.9926 Surface Available Nitrogen Estimate 0.534 5340 10.68 0.988523 9885.228 19.77046' Phosphorus as P205 . 0.606 6060 12.12 1.121807 11218.07 22.43613 Potassium as K20 0.117 1170 2.34 0.216586 2165.864 4.331729 Calcium 15.601 156010 •312.02 28.88004 288800.4 577.6009 Magnesium 0.2645 2645• 5.29 0.489633 4896.335 9.792669 Sulfur 0.124 1240 2.48 0.229545 2295.446 4.590892 Zinc 0.010264 102.64 0.20528 0.019 190.0037 0.380007 Copper 0.005564 55.64 0.11128 • 6.0103 102.9989 0.205998 Manganese 0.008967 89.67 0.17934 0.016599 165.9941 0.331988 Sodium 0.023121 231.21 0.46242 0.042801 428.0081 0.856016 Calcium Carbonate Equivalency 38.295 382950 .765.9 70.89041 708904.1 1417.808 Mayw200 CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES BIOSOLIDS SAMPLE DATE,•. y 15 200 Biosolids Maximum Maximum Maximum Maximum Metal Allowable Allowable Application Application Content, Metal App. Rate, Rate, Rate, METALS ppm Content, ppm #/Acre/Yr. DT/Acre/Yr. WT/Acre/Yr. Arsenic, Total 1.24 ' 41.00 1.80 363.95 727.89 Cadmium, Total 1.24 ' 39.00 1.70 343.73 687.46 Chromium, Total 15.08 1200.00 134.00 2222.09 4444.17 Copper, Total 16.70 1500.00 67.00 1002.82 2005.65 Lead, Total 1.24 ' 300.00 13.00 2628.51 5257.02 Mercury, Total 0.04 ' 17.00 0.75 4432.69 8865.38 Molybdenum, Total 4.97 ' 18.00 0.80 40.26 80.52 Nickel, Total 16.59 420.00 18.70 281.72 563.44 Selenium, Total 1.24 ' 36.00 4.50 909.87 1819.74 Zinc, Total 68.00 1525.00 125.00 459.53 919.06 PCB BDL 1.60 ' Actual metal content less than amount indicated. Biosolids Biosolids Maximum Maximum Nutrient Nutrient Crop/Soil Application Application Content, Content, Requirement, Rate, Rate, ppm % #/Acre " DT/Acre/Yr. WT/Acre/Yr. Ammonium Nitrogen 518.13 0.05 Organic Nitrogen 10590.67 1.06 Incorporated Available Nitrogen 6782.38 0.68 120.00 4.42 8.85 Surface Available Nitrogen 6626.94 0.66 120.00) 4.53 9.05 Phosphorus as P205 5383.42 0.54 80.00 ' 3.72 7.43 Potassium as K20 1989.64, 0.20 50.00 6.28 12.57 Calcium, Total 126005.18 12.60 Calcium as CaO 176407.25 17.64 Calcium as CaCO3 (CCE) 279067.36 27.91 2000.00 1.79 3.58 Magnesium, Total 2202.07 0.22 Manganese 129.53 0.01 Sulfur 1150.26 0.12 Percent Moisture .50.00 " These are typical values and must be adjusted based upon specific site conditions DT is Dry Tons of Biosolids. WT is Wet Tons of Biosolids. CERTIFICATION: This biosolid product has been produced by the Town of Cheraw's Wastewater Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature and lime (calcium oxide). The Town of Cheraw certifies that this biosolid complies with the Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has a metal and nutrient content as presented above. DIRECTIONS FOR USE: This biosolid is intneded to be used as a soil amendment. The biosolid land application rate shall not exceed the most restrictive Maximum Application Rate as indicated in the table above. The application rate for nitrogen, phosphorus, potassium, and calcium is dependent upon the crop grown and site soil characteristics. The user should contact the Clemson Extension Service (843-623-2134) and/or the Soil Conservation Service (843-623-2187) for.assistance in determining the proper application rate for each crop and site. In no case shall the land application rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension Service Circular #476 titled "Lime and Fertilizer Recommendations." THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY. AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES. THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS BIOSOLID PRODUCT. Mr. Ricky D. Ingram, Public Utility Director P. O. Box 219; Cheraw, SC 29520 Telephone: 843-537-8440 FAX: 843-537-8442 PRODUCT USER NAME: ADDRESS: INTENDED USE: LOCATION OF USE: QUANTITY RECEIVED: RECEIVED BY: .Davis & Brown PO Box 15038 Quiuby, SC 29506 (843) 665-6746 FAX: (843) 629-1444 Certificate of Analysis Client: ('FIERA W. TOWN OF South Carolina Certification Number: 21117 1'.0.B0X 219 C'HRRA W. SC29520 Client #: 168 Contact: SHERRY TOLSON Sample Date: SDC #: SDG-06171 1 Receipt Date: 17-.ILII-08 Report Date: 04-Aug-08 Approval By: Van Ward Lab Director Reporting Parameter Result Limit Unit 'Method Flag Date Time Analyst LSID-136477 1001-F fluoride- IC 3.09 0.2 mg/L EPA 300.0 S 1 1 7/23/2008 15:25 JEM LSID-136478 1001-C Acid Di-estion ( Liquids) YES EPA 200.2 7/22/2008 10:00 DH Chromium. TOtal -c0,005 0.005 m­/L EPA 200.7 W25/2005 17:18 DH Copper. "I'utal 0.045 0.005 mg/L EPA 200.7 7/25/2008 17:1 S DH Mun-ancse, 'total 0.026 0.005 nig/L EPA 200.7 7/25!2008 17: I S DH Zinc, Tot:ll 0.041 0.005 mg!L EPA 200.7 7/25/2008 17:1 S DH LSID-136479 E F F. 7-15-08-001 lcid Digestion (Liquids) YES EPA 200.2 7/2212008 10:00 DH Silver. Total =•0.005 0.005 mg/L EPA 200.7 7/29/2008 12:16 DH LSID-136480 IOUSOR I US-67=15=08=50 Acid Dicc,; ion (Solids) YES EPA 200.2 7/22/2008 10:00 DH PUCCnt N1101Snu-c 53.9 0.1 wt'%I SW8403540 7/15,12008 16:45 BW Aluminum. Total 2750 4.0 mg/k;, SW840 601 OB 7/23/2008 1 1:56 DH Arsenic. Total •.-.1.14 1.14 mg/kg SW840 601 OB 7/25/200S 14:00 DH Page 2 Davis & Brown PO Box 15038 Quimby, SC 29506 (843) 665-6746 FAX: (843) 629-1444 Certificate of Analysis Client: CHERAW, TOWN OF South Carolina Certification Number: 21117 P.0.130X 219 t CH ERA W. SC 29520 Client #: 16\ Receipt Date: 17-.1u1-08 Contact: SHERRY TOLSON Report Date: 04-Aag-08 Sample Date: 15-Jul-08 ' SDC #: SD(.;-()6 171 I Approved By: N1:1II .Ward Lab Director Reporting Parameter Result Limit Unit Method Flag Date Time Analyst C'admiunt, focal •--,1.14 1.14 mg/kg SWS46601013 7/25/2008 17:I8 DH C'hrontiunt. "Total 13.9 1.14 mg/kg SW846 601OB 7/25/2008 17: I S DH {'olthcr.'fnlal. 15.4 1.14 mg/kg SW840601OB 7/25/2008 17:I8 DH Lead. "total •c1.14 1:14 ntg/kg ' SW840 GOIOB 7/251'2008 17:I8 DH Mo IVIIdcnunt. Tol:tl Z#ice 4s,10 4.6 mg!kg. SWS46 601013 7/23/2008 11:56 DH Nickel. Total 15.3 1.14 mg/kg SW8406010B 7/25/2008 17:I8 DH Zinc. Toml 62.7 1.14 mg/kg SW846 601 OB 7/25/2008 17:1 S DH Mercury.] owl :0.039 0.039 mill/kg SWS46 7470A 7/22/2008 14:10 DH Selenium, Tidal =1.14 1.14 ma 11(g SW846 7741A 7/25/2008 14:00 DH PCC13 BDL mg/kg SWS46 SOSO S16 7/24/2008 0:45 LSB Page 3 12,11.�. L.�t,.ot ,i r:•I. ENVIRONMENTAL SCIENCE CORP. REPORT OF ANALYSIS Hi.. Scott Fields July 24,2008 Davis L Brown P.O. Lax 15038 Qllinby, SC :Ci506 ESC ample # L.355817-01 P,:te Received July 18, 2008 Description Site ID ,:ample ID 13t;480 Project # . Collected By Coll,>r_tion Date 07/15/08 13:40 Pai.Imeter Dry Result Det..Limit Units Method Date Analyst Total solid:: 43.9 254OG 07/23/08 2101 JDW Pol_hlor_aated Eiphenyls F'Cc 101r; BDL 0.39 mg/kg 8010-- 07/24/08 0045 LSB FCc 1221 EDL 0.39 mg/kg 8082 07/-24/08 0045 LSE PCB 1232 BDL 0.39 mg/kg 8082 07/24/08 0045 LSE PCE6 1214:' EDL 0.39 mg/kg 8062 07/_-'/08 004S LSP. PCL 11--40 BDL 0.39 mg/kg 8082 07,124/08 0045 L:E PCF.. 1254 EDL 0.39 mg/kg 808, 07/24/08 9045 L_'B BDL 0.39 mg/kg 8082 07/24/03 0045 LSE P.e!'uLts listed are dry weight basis. BDL Blow Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 E'' - 90010, EYOST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 blote: AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - !)98093910 This: Leport shall not be reproduced, except in full, without the written approval from ESC. Thy Lehorted analytical results relate only to the sample submitted F-pnrt�[I: 07/24/08 17:28 Printed: 07/2--4/08 17:29 L�S5817-01 rPCBSt - IS/SUP.R failed on lower dilution. Page of 4 Attachment A List of Anal yt es with QC Qualifiers Analyte Qualifier. PCB 1016 PCB 12 2 1 PCB 1232 C) PCB 1242 0 PCB 1248 0 PCB 12154 0 PCB 1260 0 9 P,ige 3 of 4 Attachment ! Explanation of QC Qualifier Codes I uilrfier Meaning (ESC) Sample diluted due to matrix; interferences that impaired the ability to make an accurate analytical determination. The detection limit is ele•rated in order to reflect the necessary dilution. Qualifier Report Information ' utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and .i.,: required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted Yr, ESC:, we have implemented ESC qualifiers to provide more information pertaining to our analytical re>ult::. Each Qualifier is designated in the qualifier explanation as either EPA or ESC. Mitzi qualifiers, are intended to provide the ESC client with more detailed information concerning. the pr.tential bias of reported data. Because of the wide range of constituents and variety of matrices'incorporated by most EPA methods,it is common for some compounds to fall outside of established ranges. These exceptions are evaluated and all reported data is valid and useable unlss qualified as 'R' (Rejected). Definitions c'::irric,, - The :e_sitionr,hip of the observed value of a known example to the tree value of a known sample. Represented by percent recovery and _+>levant to samples such as: control samples, matrix spike recoveries, .,Arrogate recoveries, etc. PsFcie,_or. - The agreement between a set of samples or between duplicate samples. Relates to how close together the results are and is represented by Felatcve Percent Differrence. ._eog.,%e - organic compounds that are similar ,n chemical compos_t;.on, extract --on., ond.chromotography to analytes of interest. The surrogates are u:,ed to d,�term,ne the probable response of the group of analytes that are Chem- ically related to the surrogate compound. Surrogates are added to the jatiple and Carried through all stages of preparation and analyzes. i - Te:•:tatively Ident-,fied Compound: Compounds detected it. ,--ample:, that are not'target compounds, infernal standards, system monitoring co:rpo.:ndz;, Page 4 of 4 DAVIS & BROWN r Data Qualifiers Within the attached report, some analytical data may be reported as "Qualified Data" as' indicated by "Data Qualifier" or "flag" next to the result: The. data. qualifier "S" indicates that the analysis was performed by another -SC certified Lab. This table summarizes the South Carolina_ Lab Certification Numbers for those laboratories. S South Carolina Lab Certification Number: 23101 S 1 South Carolina Lab Certification Number: 93013 S2 South Carolina Lab Certification Number: 23105 S3 SoUth Carolina Lab Certi ficati on'Number: 10120 . S4 South Carolina Lab Certification Nurriber: 84002 S5 South Carolina Lab Certification Number: 32117 96, Agricultural Service Laboratory Clemson Uhiversit ST South Carolina Lab, Certificatioh' Number: _ 36001 S8 S9 South Carolina Lab Certification Number: 94014001; 94014002 S 10 South Carolina Lab Certification Number: 84009 S I 1 South Carolina Lab.Certif cation :Number: 96023; 96026; 96031; 98001: 73006 S 12 AASHTO R 18 Certified S 13 SOL th Carolina Lab Certification Number: 96012 S 14 South Carolina Lab Certification Number: 89002. S15 ******** S 16 South Carolina Lab Certification:Niunber: 84004 . S 17 South Carolina Lab Certification Number: 96037001 S18 South Carolina Lab Certification Number: 95005 S 19 South Carolina Lab Certification Number: 23104 S20 `South Carolina Lab Certification Number:. 96027001 S21 South Carolina Lab Certification Number: 2100.5 - S22 South Carolina.Lab Certification Number: 24110 S23 South Carolina Lab Certification Number: 840.01001 S24 South Carolina Lab Certification Number: 82014001 -S25 Sam le was analyzed by _Microsee s, Inc Labora'tory S26 North Carolina Lab Certifi.cation.Number: 21 (Wilson Division NC001"20) S27 South Carolina Lab Certification Number: 40569 Revision tNv'05 Dataguul ISuhLabsl .wpd CHAIN OF CUSTODY RECORD Page__L__ of I DAVIS & BROWN Pose Olf1w Box 15M 124 West McIver Road t wft South CamkM 2V" Flm m*. South Cmulkm 2tl I Taleph= (M) 60.6748 _ CQ lit 1 Em� �_ MII M� Use Codes in the boxes to indicate "Mr' dtered or preserved. PO M�W MORM M-11i� "°�� wd-f ilk - Program Area: D - Drinking Wata / G - Groundwater / S - Solid / W - Waste Water / N - NPDES / O - Other Page 1 of 1 A N I M A L W A S T E A N A L Y S I S R E P O R T Agricultural Service Laboratory LAB No. 71184 Clemson University TOLSON, SHERRY ACCOUNT c COCHSFL PO BOX 219 DATE 07-29-2008 CHERAW SC 29520 CHERAWTOWNOF656@BELLSOUTH.NET SAMPLE NO.07fi.5Q 58 MANURE: OTHER STORAGE: UNCOVERED --RESULTS REPORTED ON AN AS -SAMPLED BASIS---------------------- lbs/ton Ammonium Nitrogen 0.05 % 1.00 Organic Nitrogen 1;02 % 20.44 Nitrate Nitrogen --------------------------------------------------------------- 7.72 ppm 0.02 INCORPORATED AVAILABLE NITROGEN ESTIMATE 13.09 SURFACE AVAILABLE NITROGEN ESTIMATE .12.79 --------------------------------------------------------------- Phosphorus as P205 0.52 % 10.39 Potassium as K20 0.19 % 3.84 Calcium 12.16 % 243.19 Magnesium 0.21 % 4.25 Sulfur 0.11 % 2.22 Zinc 75.27 ppm 0.15 Copper 30.40 ppm 0.06 Manganese 125.46 ppm 0.25 Sodium 185.29 ppm 0.37 Moisture 51.75 % Calcium Carbonate Equivalency 26.93 % 538.60 ------------------------------------------------------------------------------ INCORPORATED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of organic-N, and 100% of nitrate-N (if determined)., Assumes the manure will be incorporated into the soil within hours of application. Assumes some loss of ammonium-N during application and prior to incorporation. SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be left on the surface of the soil with no incorporation by plowing or irrigation. Available nitrogen calculations are estimates and if nitrate-N was not re- quested the amount of available nitrogen may be slightly more than reported. Also, the actual amount may be more or less than the estimate depending on the composition of the manure, soil type, and environmental conditions. All of the potash in the animal waste should be plant available in the first - year of application . Although not all of the phosphorous is available in the first year, its availability should be comparable to that in commercial fertilizers. The rate of animal waste to apply for crop production is dependent on the nutrient content of the waste, method of application and incorporation, soil test, crop to be grown, and previous manure applications. In most cases, the plant available nitrogen content of the waste is used to determine the rate of application. The Agricultural Service Laboratory is a public service of Clemson University, an affirmative action and equal opportunity educational institution. ** http://www.clemson.edu/agsrvlb ** I'AA . //, .....,ao.....,,.., mnT cnt,r ,A, .,�,..�..�..., % moisture • solids lbs. solids/ton lbs. solids/500 tons' 51.75 48.25 965 482500 % ppm lbs/ton % ppm Ibs/ton as -sampled as -sampled as -sampled dry ton dry ton dry Ammonium Nitrogen 0.05 500 1 0.103627 1036.269 2.072539 Organic Nitrogen 1.022 10220 20.44 2.118135 21181.35 42.36269 Nitrate Nitrogen 0.000772 7.72 0.01544 0.0016 16 0.032 Incorporated Available Nitrogen Estimate 0.6545 .6545 13.09 1.356477 13564.77 27.12953 Surface Available Nitrogen Estimate 0.6395 6395 12.79 1.325389 13253.89 26:50777 Phosphorus as-P205 0.5195 5195 10.39 1.076684 10766.84 21.53368 Potassium as K20 0.192. 1920 3.84 0.397927 3979.275 7.958549 Calcium 12.1595 121595 243.19 25.20104 252010.4 504.0207 Magnesium 0.2125 2125 14.25 0.440415 4404.145 8.80829 Sulfur 0.111 1110 2.22 0.230052 2300.518 4.601036 Zinc 0.007527 75.27 0.15054 0.0156 156 0.312 Copper 0.00304 30.4 .0.0608 0.006301 63.00518 0.12601 Manganese 0.012546 125.46 0.25092 0.026002 260.0207 0.520041 Sodium 0.018529 • 185.29 0.37058 0.038402 384.0207 0.768041 Calcium Carbonate Equivalency 26.93 269300 538.6 55.81347 558134.7 1116.269 V- ,luly 2008=: CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES BIOSOLIDS SAMPLE DATE,$eptenitier;l.7;2008 Biosolids Maximum Maximum Maximum Maximum Metal Allowable Allowable Application • Application Content, Metal App. Rate, Rate, Rate, METALS ppm Content, ram N/AcrelYr. DT/Acre/Yr. WT/Acre/Yr. Arsenic, Total 1.44 " 41.00 1:86 312.79 625.59 Cadmium, Total 1.44 • 39.00 1.70 295.42 590.83 Chromium, Total 88.15 . 1200.00 134.00 380.02 760.05 Copper, Total 30.11 1500.00 67.00 556.24 1112.48 Lead, Total 1.44 • 300.00 13.00 2259.07 4518.14 Mercury, Total • 0.08 • 17.00 0.75 2311.96 4623.91 Molybdenum, Total 1.78 18.00 0.80 112.54 225.08 Nickel, Total 18.12 420.00 18.70 257.94 515.89 Selenium, Total 1.44 _ 38.00 4.50 781.99 1563.97 ,.Zinc, Total 90.27 1525.00 125.00 346.19 692.38 PCB BDL 1.60 Actual metal content less than amount Indicated. Biosolids Biosollds Maximum, Maximum Nutrient Nutrient Crop/Soil Application 'Application Content, Content, Requirement, Rate, Rate, aam % #/Acre " DT/Acre/Yr. WT/Acn31Yr. Ammonium Nitrogen 1028.81 0.10 Organic Nitrogen 4550.75 " 0.46 Incorporated Available Nitrogen 3552.61 0.36 120.00 8.44 '16.89 Surface Available Nitrogen 3244.17 0.32 _ 120.00 9.25 18.49 Phosphorus as P205 4235.25 0.42 80.00 4.72 9.44 Potassium as K20 723.59 0.07 50.00 17.27 34.55 Calcium, Total 119694.79 11.97 Calcium as COO 167572.70 16.76 Calcium as CaCO3 (CCE) 304187.24 30.42 2000.00 1.64 3.26 Magnesium, Total 1899.86 0.19 Manganese 78.88 0.01 Sulfur 896.49 0.09 Percent Moisture 50.00 These are typical values and must be adjusted based upon specific site conditions DT is Dry Tans of Biosolids. WT is Wet Tons of Biosoiids. CERTIFICATION: This biosolid product has been produced by the Town of Cheraw's Wastewater Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature and lime (calcium o)dde). The Town of Cheraw certifies that this blosolld complles.with the Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has a metal and nutrient content as presented above. DIRECTIONS FOR USE: This blosoiid Is intneded to be used as a soil amendment. The biosoild land application rate shall not exceed the most restrictive Maximum Application Rate as indicated in the table above. The application rate far nitrogen, phosphorus, potassium, and calcium is dependent upon the crop grown and site soil characteristics. The user should contact the Clemson Extension Service (843-623-2134) and/or the Soil Conservation Service (843-623-2187) for assistance In determining the proper application rate for each crop and site. In no case shall the land application rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension Service Circular #476 titled "Lime and Fertilizer Recommendations." THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY. AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES. THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS BIOSOLID PRODUCT. Mr. Ricky D. Ingram, Public Utility Director P. 0. Bar 219; Cheraw, SC 29520 Telephone: 843-537-8440 FAX: 843-5374442 Davis & Brown PO Box 15038 Quiuby, SC 29506 (843) 665-6746 FAX: (843) 629-1444 Certificate of Analysis Client: CHERAW, TOWN OF South Carolina Certification Number: 21117 P.O.130X 219 CHERAW. SC 29520 Client #: 168 Receipt Date: 18-Sep-08 Contact: SHERRY TOLSON Report Date: 08-Oct-08 Sample Date: I 71--sep-08 Approved By: Lab tiamplc ID: I.SID-135704 Van Ward 'Sample II): f)'tiUL D ?)f7=G)S� -5 0 ~ Lab Director Reporting Parameter Result Limit Unit Method Flag Date Time Analyst \cnl I)i_x:unn !S ,lids! YES EPA 200.2 9/22/2008 1 1:00 DH I',rccn! \•Ini:aurc 29.1 (l.l ��t:„ SW8403540 9/23/2008 17:00 13\V 0310 164 mg/kg SWS466010B 9!29!-?()OS I0:47 DH Al-scn!c. fatal 2.04 2.04 mg/kg SW846 601OB 9/22/2008 16:44 DH ('aLlmium. total -:2.04 2.04 mg/kg SW846 601OB 9/23/2008 10:45 DFI ('11f„mltttt). •f,,lal 125 2.04 mpg/kg SWS46 601 OB 9/23/2008 10:45 DH ('opper.'I'olal 42.7 2.04 mg/kg SW846601OB 9/23/2008 10:45 DH I.cail. Total 2.04 2.04 mgikg SW846 601OB 9/23/2008 10:45 DH mt,d),hdcnum. Total 2.52 1.64 mg/kg SW846 601013 9/29/2008 16:47 DH N''icku•I.'I'n!al 25.7 2.04 mg/kg SW846601OB 9/23/2008 10:45 DFI zinc. Towl 128 .1.04 mg/kg SWS46 601OB 9/23:'2008 10:45 DH VIcrcurN. Total �0.1 15 0.1 15 mg/kg SW846 7470A 10/1/2008 14:23 DH S, Irninm. I'ntal �.04 �.04 mg/kg SWS46 7741A 9'22/2008 16:44 DFI 1'('[1 C3DL mg/kg SW846 8080 S16 9/27/2008 5:12 AD1= Page 2 ENVIRONMENTAL SCIENCE CORP. REPORT OF ANALYSIS September 30,2008 ESC Sample 4 : L366100-01 September 19, 2008 Site ID ::a111J.A- JD 136704 Project # By 09/17/08 12:45 Dry Result Det. Limit Units Method Date Analyst 73.0 09/25/08 1141 TRR BDL 2.3 mg/l:g 8082 09/27/08 0512 ADF BDL 2.3 mg/kg 8082 09/27/08 0512 ADF BDL - mg/kq 01082 09/27/08 0512 ADF BDL 2.3 mg/kg 3002 09/27/08 0512 ADF BDL 2.3 mg/kg 30`2 '09/27/05 0 1. 12 ?LIF BDL 2.31 rrig/l-.g 8082 09/27/08 05121 ADF BDL 2 -.3 mg/hg E082 0 9 /21 7 /;1 "" 0512 T. DF i,;t-d are dry weight basis. Limit -,iwi.r. Preict)-,--al Quantitation Limit(PQL) Laboratory Certification Numbers: :%iH'-. - 1007bcJ, AL - 40660, CA - 1-2327, CT- PH-0197, FL E87487,_ GA - �42-i, 10 C-TN-01 FY115T - (1016, MC 7 ENV375,DW21704, ND R-140,SC- 84004, TN 2006, VA 00109, WV 233 AZ -0612, MN - 047.-999-395, HY 11742, NJ TN002-j WI 998093910 Thi-.; :;h,ill not be reproduced, except in full, without the written approval from ESC-. analvtical results 'relate only to the sample submitted ol,/21-1/08 -11:14 Revised: 09/30/08 12:00 1, t--10( -0i Dilution due to matri-.. Page 2 of 4 Attachment A List of Anal7tes with QC Qualifiers 1 If Anal_ r.e Qualifier PCB 1016 PCB 1221 0 PCB 12-32 0 PCB 1242 a PCB 12.38 C) PCE, 1254 P�---B 1260 Pa (I F. 3 .) f 4 E! E_-:planatic-n of Code_-, tESC) Sample diluted due to matxix, interferences O-iat ijnl:;;iired thr. ability t,., mal:e an- accurate analytical determination. The detection limit is e1,:,7ated in,order to reflect the necessary dilution. _ Qualifier Report Information :111d result qualifiers as set forth by the EPA Contract Laboratory Program and h-v most i.:&rtifying' bodies including NELAC. In addition to the EPA qualifiers adopted implemented ESC qualifiers to provide more information' pertaining to our analytical E-:ich qualifier is designated in the qualifier e_xplanation as either. -EPA or ESC. tiel.-S are intended to provide the ESC client with more detailed information concerning bias of reported data. because of the wide range of constituents and variety of by most -EPA methods, it is common for some compounds t---, fall out-ni-le of 1-111ries. These e%-ceptions are evaluated and all reported data it, valid and useable I'ILI,;Iifilaa .,s IR' (Rejected) Definitions The, relationship of the observed Salue of a ):nown sample to, the i:Lle value of a known sample. Repre.sented by .percent recovery and -levant to samples such as: control .5antl5les, inatri-.: spike recoveries, etc. between ci set of samples or between duplicate sa.mplL-­ -o how close together the results are and is represented by Percent Differrence. compounds that are similar in chemical ..!.,Ci .-:i:z-)wOtoCriphy to cine-Ilytes of int-rest. The surroaate.s al-e "Ised to r - thfF p_,ob.=.b.Le responre of -Le group of analyre!, .,he�.t c*hem- --ed to tsurrogatehe icomi:o.ind. S,irroc1 ates circ added co r:!- arid al -cages o_prepira.-on and- - identified Compound: detected in :!.:r rompo"zr. cis, internal standard:.,, system moni-..orin.7 1 1: f C g;, t e - 4 of 4. ENVIRONMENTAL C-1 L)CIENCE CORP. Report Summary Tuesday September 30, 2008 Report Number: L366100 Samples Received: 09/19/08 Client Project: Description: T..:. 1, . D. - —, . il �,; 0, in this report based upon ini,**. rnAFlf - -1 01, pp1ied i, Vhe -:J-Jent, and are for your exclusive use. r-garding this data package, please do Entire Report Reviewed By: T. Alan harviii, Eou Rep CeftifiClqdO17 M1117bei-s -ALJ(-,1-01, AIHA - 09227, AL -'40660, CA - 1-2327, CT - EIII-0197'FL - E87487 IN - C.-TN-01, KY - 90010, KYUST - 0016, NC - ENV375,DW-'?1704, ND R-140 THJf'0,', :-7',C' 84004, TN - 2006,.VA - 00109, WV - 233 12 [IN 047-999-39 5,'NY 11742, WI 998093910 I L I - u, Ei i .,j -i an E 1 . 1 f, V i DAVIS & BROWN Data Qualifiers Within the attached report, some analytical data may be reported as "Qualified Data" as indicated by a "Data Qualifier" or "flag" next to the result. The data qualifier "S" indicates that the analysis was performed by another SC certified Lab. This table summarizes the South Carolina Lab Certification Numbers for those laboratories. S South Carolina Lab Certification Number: 23101 S 1 South Carolina Lab Certification Number: 93013 S2 South Carolina Lab Certification Number: 23 105- S3 South Carolina Lab Certification Number: 10120 S4 South Carolina Lab Certification Number: 84002 S5 South Carolina Lab Certification Number: 32117 S6 Agricultural Service Laboratory Clemson University S7 South Carolina Lab Certification Number: 36001 S8 **** S9 South Carolina Lab Certification Number: 94014001; 94014002 S10 South Carolina Lab Certification Number: 84009 S11 South Carolina Lab Certification Number: 96023; 96026; 96031; 98001; 73006 S 12 AASHTO R18 Certified S 13 South Carolina Lab Certification Number: 96012 S 14 South Carolina Lab Certification Number: 89002 S 15***** S 16 South Carolina Lab Certification Number: 84004 S17 South Carolina Lab Certification Number: 96037001 S 18 South Carolina Lab Certification Number: 95005 S 19 South Carolina Lab Certification Number: 23104 S20 South Carolina Lab Certification Number: 96027001 S21 South Carolina Lab Certification Number: 21005 S22 South Carolina Lab Certification Number: 24110 S23 South Carolina Lab Certification Number: 84001001 S24 South Carolina Lab Certification Number: 82014001 S25 Sam le was analyzed by Microsee s, Inc Laboratory S26 North Carolina Lab Certification Number: 21 (Wilson Division NC00120) S 2 7 South Carolina Lab Certification Number: 40569 Revision (X)-05 Da[ayual ISuKabsl .wpd CHAIN OF CUSTODY RECORD Page____ of DAVIS & BROWN Post Office Box 15038 124 West McIver Road Quinby, South Carolina 29506 Florence, South Carolina 29501 Telephone (m3) 665.6746 f "" Use Codes in the boxes to indicate A ether sample was filtered or preserved. o „ter In� Him F, , r 14,� jjjjjjjj, iNONNI! n eiiiiieii loii� o•-••• - - . .wng u - c,rounawater / 3 - Solid / W - Wade Water / N - NPDES / 0 - Other A N I M A L W A S T E A N A L Y S I S R E P O R T Agricultural Service Laboratory LAB No. 91496 Clemson University TOLSON, SHERRY ACCOUNT COCHSFL PO BOX 219 DATE 09/26/2008 CHERAW SC 29520 CHERAWTOWNOF656@BELLSOUTH.NET SAMPLE NO. VP170:&5;_O_-jMANURE : OTHER STORAGE: UNCOVERED -----------------RESULTS REPORTED ON AN AS -SAMPLED BASIS---------------------- lbs/ton Ammonium Nitrogen 0.15 % 3.00 Organic Nitrogen 0.66 % 13.27 Nitrate Nitrogen --------------------------------------------------------------- 0.73 ppm 0.00 INCORPORATED AVAILABLE NITROGEN ESTIMATE 10.36 SURFACE AVAILABLE NITROGEN ESTIMATE --------------------------------------------------------------- 9.46 Phosphorus as P205 0.62 % 12.35 Potassium as K20 0.11 % 2.11 Calcium 17.45 % 349.03 Magnesium 0.28 % 5.54 Sulfur 0.13 % 2.62 Zinc 159.64 ppm 0.32 Copper 42.28 ppm 0.08 Manganese 117.36 ppm 0.23 Sodium 885.70 ppm 1.77 Moisture 27.10 % Calcium Carbonate Equivalency 44.35 % 887.01 ------------------------------------------------------------------------------ INCORPORATED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be incorporated into the soil within hours of application. Assumes some loss of ammonium-N during application and prior to incorporation. SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50%of ammonium-N, 60% of organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be left on the surface of the soil with no incorporation by plowing or irrigation. Available nitrogen calculations are estimates and if nitrate-N was not re- quested the amount of available nitrogen may be slightly more than reported. Also, the actual amount may be more or less than the estimate depending on the composition of the manure, soil type, and environmental conditions. All of the potash in the animal waste should be plant available in the first year of application. Although not all of the phosphorous is available in the first year, its availability should be comparable to that in commercial fertilizers. The rate of animal waste to apply for crop production is dependent on the nutrient content of the waste, method of application and incorporation, soil test, crop to be grown, and previous manure applications. In most cases, the plant available nitrogen content of the waste is used to determine the rate of application. The Agricultural Service Laboratory is a public service of Clemson University, an affirmative action and equal opportunity educational institution. http://www.clemson.edu/aglabresults/COCHSFLTOLSON,%20SHERRY0810201153231.htm 2/9/09 % moisture % solids lbs. solidstton lbs. solidsJ500 tons 27.1 72.9 1458 729000 % ppm Ibstton % ppm Ibstton as -sampled as -sampled as -sampled dry ton dry ton d Ammonium Nitrogen 0.15 1500 3 0.205761 2057.613 4.115226 Organic Nitrogen 0.6635 6636 13.27 0.910151 9101.509 18.20302 Nitrate Nitrogen 7.3E-05 0.73 0.00146 0.0001 1.001372 0.002003 Incorporated Available Nitrogen Estimate 0.518 5180 10.36 0.710562 7105.624 14.21125 Surface Available Nitrogen Estimate 0.473 4730 9.46 0.648834 6488.34 12.97668 Phosphorus as P205 0.6175 6175 12.35 0.847051 8470.508 16.94102 Potassium as K20 0.1055 1055 2.11 0.144719 1447.188 2.894376 Calcium 17.4515 174515 349.03 23.93896 239389.6 478.7791 Magnesium 0.277 2770 5.54 0.379973 3799.726 7.599451 Sulfur 0.131 1310 2.62 0.179698 1796.982 3.593964 Zinc 0.015964 159.64 0.31928 0.021898 218.9849 0.43797 Copper 0.004228 42.28 0.08456 0.0058 57.99726 0.115995 Manganese 0.011736 117.36 0.23472 0.016099 160.9877 0.321975 Sodium 0.08857 885.7 1.7714 0.121495 1214.952 2.429904 Calcium Carbonate Equivalency 44.3505 443505 887.01 60.83745 608374.5 1216.749 �"September>208 CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES_ BIOSOLIDS SAMPLE DATE:14q,v mi5er19 20Q8 Biosolids Maximum Maximum Maximum Maximum Metal Allowable Allowable Application Application Content, Metal App. Rate, Rate, Rate, METALS ppm Content, ppm #/Acre/Yr. DT/Acre/Yr. WT/Acre/Yr. Arsenic, Total 0.92 ' 41.00 1.80 488.01 976:02 Cadmium, Total 0.92 • 39.00 1.70 460.90 921.79 Chromium, Total 40.00 1200:00 134.00 837.50 1675.00 Copper, Total 22.31 1500.00 67.00 750.86 1501.72 Lead,'Total 0.92 ` 300.00 13.00 3524.50 7049.01 Mercury, Total 0.18 17,00 0.76 1026.32 2052.63 Molybdenum, Total 3.69 18.00 ' 0.80 54.17 108.33 Nickel, Total 17.50 420.00 18.70 267.14 534.29 Selenium, Total 0.92 36.00 4.50 1220.02 2440.04 Zinc, Total - 75.29 1525.00 125.00 415.07 830.14 PCB BDL 1.60 Actual metal content less than amount indicated. Biosolids Biosolids Maximum Maximum Nutrient Nutrient Crop/Soil Application Application Content, Content, Requirement, Rate, Rate, ppm % #/Acre" DT/Acre/Yr. WT/Acre/Yr. Ammonium Nitrogen 283.13 0.03 Organic Nitrogen 5861.26 0.59 Incorporated Available Nitrogen 3817.48 - 0.38 120.00 7.86 15.72 Surface Available Nitrogen 3732.54 0.37 120.00 8.04 16.07 Phosphorus as P205 4695.17 0.47 80.00 4.26 8.52 Potassium as K20 721.97 0.07 50.00 17.31 34.63 Calcium, Total 154147.79- 15.41 Calcium as CaO 215806.91 21.58 Calcium as CaCO3 (CCE) 441586.45 44.16 2000.00 1.13 2.26 Magnesium, Total 2850.13 0.29 Manganese. 84.94 0.01 ,Sulfur 948.47 ' 0.09 Percent Moisture 50.00 " These are typical values and must be adjusted based upon specific site conditions DT is Dry Tons of Biosolids. WT is Wet Tons of Biosolids. CERTIFICATION: This biosolid product has been produced by the Town of Cheraw's Wastewater Treatment Plant by a treatment process that pasteurized plant residual•solids using high temperature and lime (calcium oxide). The Town of Cheraw certifies that this biosolid complies with the Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has meta_ I .and nutrient content as presented above. DIRECTIONS FOR USE: This biosolid is intneded to be used as a soil amendment. The biosolid land application rate shall not exceed the most restrictive Maximum Application Rate as indicated in the table above. The application rate fix nitrogen, phosphorus, potassium, and calcium is dependent upon the crop grown and site soil characteristics. The user should contact the Clemson Extension Service (843-623-2134) and/or the Soil Conservation Service (843-6234187) for assistance in determining the proper application rate for each crop and site. In no case shall the land application rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension Service Circular #476 titled "Lime and Fertilizer Recommendations." THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY. AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES. THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS BIOSOLID PRODUCT. Mr. Ricky D. Ingram, Public Utility Director P. 0. Box 219; Cheraw, SC 29520 Telephone: 843-537-Wo FAX: 843-537-8442 PRODUCT USER NAME: Davis & Brown PO Box 15038 Quinby, SC 29506 (843) 665-6746 FAX: (843) 629-1444 Certificate of Analysis Client: CHERAW, TOWN OF, P.O.BOX 219 CHERAW, SC 29520 Client #: 168 Contact: SHERRY TOLSON - Sample Date: 19-Nov-08 SDG #: SDG-063870 Lab Sample ID: LSID-141 193 Sample ID: B10` D9 1-1:-19-08-50 South Carolina Certification Number: 21117 Receipt Date: 21-Nov-08 Report Date: 05-Dec-08 Approved By: F •� _ a: !f Van Ward Lab Director Reporting Parameter Result Limit Unit Method Flag Date Time Analyst Acid Digestion (Solids) YES EPA 200.2 11/24/2008 8:00 DH Percent Moisture 48.0 0.1 wt% SW846 3540 11/20/2008 16:30 BW Aluminum. Total 3640 38.4 mg/kg SW846 6010B 12/l/2008 15:37 DH Arsenic, Total <0.959 0.959 mg/kg SW846 601013 12/2/2008 10:51 DH Cadmium, Total <0.959 0.959 mg/kg SW846 6010B 11/25/2008 10:00 DH Chromium. Total 41.6 0.959 mg/kg SW846 6010E 11/25/2008 10:00 DH Copper, Total 23.2 0.959 mg/kg SW846 6010E 11/25/2008 10:00 DH Lead, Total _<0.959 0.959 mg/kg SW846 6010B 11/25/2008 10:00 DH Molybdenum, Total <3.84 3.84 mg/kg SW846 6010B 11/25/2008 14:38 DH Nickel, Total 18.2 0.959 mg/kg SW846 6010B 11/25/2008 10:00 DH Zinc, Total 78.3 0.959 mg/kg SW846 601013 11/25/2008 10:00 DH Mercury, Total <0.190 0.19 mg/kg SW846 7470A . 11/25/2008 14:53 DH Selenium, Total <0.959 0.959 mg/kg SW846 7741A 12/2/2008 10:51 DH PCB BDL mg/kg SW846 8080 S16 11/28/2008 13:52 ADF Page 1 ENVIRONMENTAL SCIENCE CORP. Mr. Scott Fields Davis & Brown P.O. Box 15038 Quinby, SC 29506 REPORT OF ANALYSIS IIt. .Tali=-, T14 I - , i GI 75t:-S','',ti 7-Y;nfi-7n.7-S Ta': I.D. r._-iiIli 14_r',9 E::t . 197U December,03,2008 ESC Sample # L376626-01 Date Received November 25, 2008 Description Site ID Sample ID 141193 Project # Collected By , Collection Date 11/19/08 13:00 Parameter Dry Result Det. Limit Units Method Date Analyst Total Solids "• 51.3 2540G 12/03/08 1016 JDW Polychlorinated Biphenyls PCB 1016 BDL 0.033 mg/kg 8082 11/28/08 1352 ADF PCB 1221 BDL 0.033 mg./kg 8082 11/28/08 1352 ADF PCB 1232 BDL `0.033 mg/kg 8082 11/28/08 1352 ADF PCB 1242 BDL 0.033 mg/kg 8082 11/28/08 1352 ADF PCB 1248 BDL 0.033 mg/kg 8082- 11/28/08 1352 ADF PCB 1254 BDL 0.033 mg/kg 8082 11/28/08 1352 ADF PCB 1260 BDL 0.033 mg/kg 8082 11/28/08 1352 ADF Results listed are dry weight basis. BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0'197, FL - E87487, GA - 923, IN - C-TN-01 F-Y - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Note: AZ -0612, MN - 047-999-395, NY - 11742, NJ - TNO02, WI - 998093910 This report shall not be reproduced, except in full, without the written approval from ESC. The reported analytical results relate only to the sample submitted Reported: 12/03/08 14:14 Printed: 12/03/08 14:14 Page 2 of 2 DAVIS & BROWN Data ,Qualifiers Within the attached report, some analytical data may be reported as "Qualified Data" as indicated by a "Data Qualifier" or "flag" next to the result. The data qualifier "S" indicates that the analysis was performed by another SC certified Lab. This table summarizes the South Carolina Lab Certification Numbers for those laboratories. S South Carolina Lab Certification Number: 23101 S 1 South Carolina Lab Certification Number: 93013 S2 South Carolina Lab Certification Number: 23105 S3 South Carolina Lab Certification Number: 10120 S4 South Carolina Lab Certification Number: 84002 S5 South Carolina Lab Certification Number: 32117 S6 Agricultural Service Laboratory Clemson University S7 South Carolina Lab Certification Number: 36001 S8 ********** S9 South Carolina Lab Certification Number: 94014001; 94014002 S 10 South Carolina Lab Certification Number: 84009 S11 South Carolina Lab Certification Number: 96023; 96026; 96031; 98001; 73006 S12 AASHTO R1.8 Certified S 13 South Carolina Lab Certification Number: 96012 S 14 South Carolina Lab Certification Number: 89002 S15 ********** S 16 South Carolina Lab Certification Number: 84004 S17 South Carolina Lab Certification Number: 96037001 S 18 South Carolina Lab Certification Number: 950.05 S 19 South Carolina Lab Certification Number: 23104 S20. South Carolina Lab Certification Number: 96027001 S21 South Carolina Lab Certification Number: 21005 S22 South Carolina Lab Certification Number: 24110 S23 South Carolina Lab Certification Number: 84001001 S24 South Carolina Lab Certification Number: 82014001 S25 Sample was analyzed by Microsee s, Inc Laboratory S26 North Carolina Lab Certification Number: 21 Wilson Division NC00120 S27 South Carolina Lab Certification Number: 40.569 Revision 06/05 Dataqual (SubLabs) .wpd CHAIN OF CUSTODY RECORD #1 Page of DAVIS & BROWN PM OEM Box i s= 124 wea4 Mckw Reed OWnW. South CMMa 2=6 %rem. South C Mm 2MI TONAMe (M) 665$746 Bee���e�III� Ba�B��ee f�l�f��Yi � fe37�i� i��lYi - o i - aue aw / N - NPDESO-Odier Salmm Bu�lnesa sDaIn Me= form No. 811• 156 2104 1g1-W A N I M A L W A S T E A N A L Y S I S R E P 0 R T Agricultural Service Laboratory LAB No. 121916 Clemson University TOLSON, SHERRY ACCOUNT COCHSFL PO BOX 219 DATE 12/09/2008 CHERAW SC 29520 CHERAWTOWNOF656@BELLSOUTH.NET SAMPLE NO. 1`'1=1;9Q:85z0 MANURE: OTHER STORAGE: UNCOVERED -----------------RESULTS REPORTED ON AN AS -SAMPLED BASIS---------------------- lbs/ton Ammonium Nitrogen 0.03 % 0.60 Organic Nitrogen 0.62 % 12.40 Nitrate Nitrogen --------------------------------------------------------------- 51.92 ppm 0.10 INCORPORATED AVAILABLE NITROGEN ESTIMATE 8.09 SURFACE AVAILABLE NITROGEN ESTIMATE -------------------------------- 7.91 Phosphorus as P205 ------------------------------- 0.50 % 9.95 Potassium as K20 0.08 % 1.53 Calcium 16.33 % 326.67 Magnesium, 0.30 % 6.04 Sulfur 0.10 % 2.01 Zinc 81.59 ppm 0.16 Copper 31.26 ppm 0.06 Manganese 87.94 ppm 0.18 Sodium 113.90 ppm 0.23 Moisture 47.G2 % Calcium Carbonate Equivalency 46.79 % 935.81 INCORPORATED PLANT,AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be incorporated into the soil within hours of application.' Assumes some loss of ammonium-N during application and prior to incorporation. SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be left on the surface of the soil with no incorporation by plowing or irrigation. Available nitrogen calculations are estimates and if nitrate-N was not re- quested the amount of available nitrogen may be slightly more than reported. Also, the actual amount may -be more or less than the estimate depending on the composition of the manure, soil type, '.and environmental conditions. All of the potash in the animal waste should be plant available in the first year of application. Although not all of.the phosphorous is available in the first year, its availability should be comparable to that in commercial fertilizers. The rate of animal waste to apply for.crop production is dependent on the nutrient content of the waste, method of application and, incorporation, soil test, crop to be grown, and previous manure applications. In most cases, the plant available nitrogen content of the waste is used to determine the rate of application, The Agricultural Service Laboratory is a public service of Clemson University, an affirmative action and equal opportunity educational institution. ** http://www.clemson.edu/agsrvlb ** http://www.clemson.edu/aglabresults/COCHSFLTOLSON,%20SHERRY081209085435... 12/11 /2008 % moisture ---- % solids lbs. solidsiton lbs. solids/500 tons - 47.02 52.98 1059.6 529800 % ppm lbs/ton % PI)m Ibs/ton as -sampled as -sampled as -sampled dry ton dry ton d Ammonium Nitrogen 0.03 300 0.6 0.056625 566.2514 1.132503 Organic Nitrogen 0.62 6200 12.4 1.170253 11702.53 23.40506 Nitrate Nitrogen 0.005192 51.92 0.10384 0.0098 97.99924 0.195998 Incorporated Available Nitrogen Estimate 0.4045 4045 8.09 0.763496 7634.957 15.26991 Surface Available Nitrogen Estimate . 0.3955 3955 7.91 0.746508 7465.081 14.93016 Phosphorus as P205 0.4975 4975 9.95 0.939034 9390336 18.78067 Potassium as K20 0.0765 765 1.53 0 .144394 1443.941 2:887882 Calcium 16.3335 .163335 326.67 30.82956 308295.6 616.5912 Magnesium 0.302 3020, 6.04 0.570026 5700.264 11.40053 Sulfur 0.1005 1005 2.01 0.189694 1896.942 3.799884 Zinc 0.008159 81.59 - 0.16318 0.0154 154.0015 0.308003 Copper 0.003126 31.26 0.06252 0.0059 59.0034 0.118007 Manganese 0.008794 87.94 0.17588 0.016599 165.9872 0.331974 Sodium 0.01139 113.9 0.2278 0.021499 214.9868 0.429974 Calcium Carbonate Equivalency .46.7905 467905 935.81 88.31729 883172.9 1766.346 November,2008� ' Davis & Brown PO Box 15638 Quinby, SC 29506 (843) 665-6746 FAX: (843) 429-1444 Certificate` of Analysis Client: CHERAW, TOWN, OF South Carolina Certification Number: 21117 P.O. BOX 219 CHERAW, SC 29520 Client #: 168 Receipt Date: 17-Jan-08• Contact: SHERRY TOLSON Report Date: 31-Jan-08 Sample Date: 16-Jan-08 By: VIxI+_.�,•c.-: SDG #: SD6-058820 Approved Van Ward Lab Director Reporting Parameter Result 'Limit Unit Method Flag Date Time Analyst LSID-130336 "_--I6' 5080 01 Acid Digestion (Solids) YES EPA 200.2 1/18/2008 9:30 DH pH (Waste) 12 S.U. EPA 9045D S16' 1/22/2008 9:45 RBS 11*9TINPPWA iP sSA 'P/F` SW-846 1/30/2008 WSF Ignitability . >170 Deg. F; SW846 1010 S16 1/25/2008 10:30 KPB Percent Moisture 53.0 0.1 Wt% SW846 3540 l/15/2008 17:15 BW , Aluminum, Total 5060 0.425 mg/kg SW846 6010A 1/23/2008 16:29 DH Arsenic, Total <1.30 1.3 mg/kg, SW846.6010A 1/24/2008, '. 0:00 JR Cadmium, Total <0.212 0.212 mg/kg SW846 60110A 1/22/2008 12:16 ,, DH' Chromium, Total 14.9 0.212 mg/kg SW846 6010A 1/22/2008 •12:16 DH Copper, Total 28.6 0.212 mg/kg. SW846 6010A 1/22/2008 12:16 DH Lead, Total- 1.80 • 1.1 mg/kg SW846 6010A 1/21/2008 15:18 DH Molybdenum, Total 1.40 0.85 _ mg/kg SW846 6010A , 1/23/2008 16:29 DH Nickel, Total 11.7 0.212 mg/kg SW846 6010A 1/22/2008 1.2:16 DH Zinc, Total 817 0.212 mg/kg SW846 6010A 1/22/2008 12:16 DH. Mercury, Total <0.649 0.049 mg/kg SW846 7470A 1/18/2008 13:28. DH Selenium, Total'. <1.30 1.3 mg/kg SW846 7741A 1/29/2008 13:11 JR PCB 0.66 mg/kg 9W846 8080 S16 1/20/2008 22:20 CSU Reactivity, Cyanide <0.125 0.125 mg/kg SW846 9010 S16 1/24/2008 12:34 LEM Reactivity, Sulfide <25 25 mg/kg SW846 9030 S16 1/24/2008 10:15 LJN Paint Filter PASS P/F SW846.9095 S16;' 1/24/2008 . 7:00 KPB -Page 1 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: Town of Cheraw Permit Number: WWTP Name: Town of Cheraw WWI'P NPDES Number: Monitoring Period: From 01 /01 /08 To 12/31 /08 WQ0014248 SCO020249 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 40 T Alternative 5 El I Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization IM Class B: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Level in Pathogen Density g y Number o Excee- encts Frequency of Analysis Sample Type Analytical Tech-niqu inimu Geo. Mean aximu Units Fecal Coliform 2 x 10 et6th power MPN per gram of total solids or 2 x 10 to the 6th power CFU per gram of 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 ❑ Option 2 ❑ Option 3 ❑ Option 4 ❑ Option 5 ❑ Option 6 ® Option 7 ❑ Option 8 ❑ Option 9 ❑ Option 10 ❑ No vector attraction reduction options were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) ® "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector .attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "1 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Ricky'Ingram/Public Utility Director Preparer Name nd Title (type or print) Land Applier Name and Title (if applicable)(type or print) 2 a,7 Signade of PlWarer Date Signature of Land Applier (if applicable) Date Author Daryl D. Merritt DENR FORM RF (7/2002) FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS A-1 Medium Double Strength Single Strength 10 ' dilution/ 10 ml sample l 0-' dilution i 1.0 ml sample Single Strength 10-2 dilution ! 1.0 ml sample Single Strength 10` dilution / 0.1 ml sample Date.'T•ime Test Set -Up: - - Q8' ,?,'30 ,,r... Date! Time Test Read: -1708 Time Placed in Incubator: 3. AO,o,,r, , Incubator Te rnp: 3 �D Time Transferred to Water Bath: A A'00, -2 Water Bath Temp: sG Operator Media Lot # : Q % Solids Sample # :I i DQ MPN Fecal Coliform = lox MPN Index i 100 atl Per Gram Total Solids Largest Volume'x' % Dry Solids NOTE + indicates positive results ; - indicates negative results FORMULA: Where: CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE % Total Solids = (A - B) x 100 C-B A = Weight of dried residue + dish (mg) B = Weight of empty dish (mg) C = Weight of wet sample + dish (mg) Sample # : %—/e - 6 ff Saa Weight of dried residue + dish: , Duplicate weight of dried residue .+ dish: Weight of empty dish Weight of wet sample + dish' ; % Total Solids a a. 39 9P2 a,a�io .aGI f�X /DD a6x14.06 $;. 67 0 FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS A-1 Medium Double Strength Single Strength , l 0-' dilution i' 1,0 nil sample 10-' dilution i 1.0 ml sample Single Strength "- Single Strength 10-2 dilution',, 1.0 ml sample, I V, dilution / 0.1 ml sample Date:Time Test SetooT : oZ�.ZO /, • Date:' Time Test Read: Time Placed in Incubator: Incubator- Temp: . Jr. L C- Time Transferred to Water Bath: /'-`/ ° Water Bath Temp: TT Operator Media Lot # % Solids —a. Sample # -otD- 08- ,41616 MPN Fecal Coliforrn 10 x MEN Index i 160 ml Per Gram Total Solids Largest Voltime `x % Dry Solids NOTE: + indicates..positive results`; - indicates negative results CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE FORMULA: % Total Solids _ (A-B)xI00 C-B A = Weight of dried residue + dish (mg) B = Weight of empty dish (mg) C = Weight of wet sample + dish (mg) Sample # : ? - 20 - a F- S,46 Weight of dried residue + dish: Duplicate weight of dried residue + dish : Weight of empty dish Weight of wet sample + dish : % Total Solids = �. 0? / 1 {/ 4-! 7,D 39.1513 FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS A- l Medium Date "Time Test Set-LTp; - d $ : 3Q date.' Time Test Read: Time Placed in Incubator: L.s o,,� Incubator Temp: Time Transferred to Water Bath: ° . i'►'►. Water Bath Temp: Operator r� JAI Media Lot # . • % Solids. 7D Sample # MPN Fecal Coliform = 10 x' MPN Index / 100 ml = Q per Gram"Total Solids Largest Volume x % Dry Solids NOTE: + indicates positive results ; - indicates negative results CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE FORMULA: % Total Solids . (A - B) x 100 C-B Where: A = Weight of dried residue + dish (mg) B = Weight of empty dish (mg) C = Weight of wet sample + dish -(mg) Sample # : 3 ' % - Q $ Oro D Weight of dried residue + dish: 016 • S 3 /Q Duplicate weight of dried residue + dish: aZ U 0 3 Weight of empty dish *I . Q 3 / oZ Weight of wet sample + dish % Total Solids = 7 p, .7 = D.g003-X-039'� XlOD I qm, 44 FECAL COLIFORM FOR MUNICIPAL, BIOSOLIDS A-1 Medium Double Strength Single Strength 10-' dilution / 10 ml sample 10-' dilution / 1.0 ml sample t— Single Strength Single Strength 10'2 dilution ' 1.0 ml sample. 10-2 dilution 10A ml sample Date.rI'ime Test Set-LTp: d0 Date. Time Test Read — _ Q 8 • Time Placed in Incubator:3��,� , Incubator Temp: Time Transferred to Water Bath: : 30 Water Bath Te nix Operator f �[A i' Media Lot _ 3 3 ? Solids 'S, Sample # 4 r AA MPN Fecal Coliform = 10 x MPN In / l00 ml per Gram Total Solids.' Largest Volume x % D r} Solids NOTE: + indicates positive results ; - indicates negative results FORMULA: Where: CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE % Total Solids = (A - B) x 100 C-B A = Weight of dried residue + dish (mg) B = Weight of empty dish (mg) C = Weight of wet sample + dish (mg) Sample #: 5�-Jl -h9-5100 Weigi. ,f dned residue + dish: Duplicate weight of dried residue + dish Weight ,ji empty dish Weight of wet sample + dish %-Total Solids ,23r 3 9 r S a3.39.!W a 3. 3q�o—a.oGo� 1C Sao J a133.�6 �F 9�9G 0 r FECAL'COLIFORM FOR MUNICIPAL BIO SOLIDS ` A=1 Medium . Double Strength 107' dilution i 10 ml sample Single Strength 10-' dilution / 1.0 ml sample Single Strength l 0-' dilution / 1.0 ml sample Single Strength 10` dilution / 0.1 ml sample Date."Time Test Set -Up: a-Vate.' Time Test Read: - D8 Time Placed in Incubator: Incubator Temp: Sd G Time Transferred to Water Bath: .3� .r• Water Bath Temp: Operator Media Lot # 3 3 fir % Solids . 3 D Sample. # S MPN Fecal Coliform = 10 x MPN Index / 100 ml = Per Gram Total Solids Largest Volume x % Dry Solids NOTE: + indicates positive results ; - indicates negative results FORMULA: Where: CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE % Total Solids (A-B)x 100 C-B A = Weight of dried residue + dish (mg) B = Weight of empty dish (mg) C = Weight of wet sample + dish (mg) Sample # : �— a f — Q ?- �o Weight of dried residue + dish: Duplicate weight of dried residue + dish: Weight of empty dish Weight of wet sample + dish : % Total Solids = L 3. 3 A a.DS. 4 5?, SS3D? c2 3 0 - � 43. 3 5/. qq.ST FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS A-1 Medium Single Strength 10-2 dilution! 1.0 ml sample Single Strength 10-: dilution / 0.1 ml sample Date,!Time Test Set-LTp: A; Date.! Time Test Read: !p - —Q • •3,$ • Time Placed in Incubator: �3•S /►'` • Incubator Temp: Time Transferred to Water Bath: ; .3 S� Water Bath Temp: C Operator Media Lot # 73 3 / p b % Solids T o Sample # MPN Fecal Coliform = 10 x MPN Index / 100 ml = Q per Gram Total Solids Largest Volume x % Dry Solids NOTE: + indicates positive results; - indicates negative results FORMULA: Where: CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE % Total. Solids = (A - B) x 100 C-B A = Weight of dried residue + dish (mg) B = Weight of empty dish (mg) C = Weight of wet sample + dish (mg) Sample # : �o - i ff— o S _ Soo Weight of dried residue + dish: Duplicate weight of dried residue + dish: Weight of empty. dish Weight of wet sample + dish : % Total Solids 53.1/G�—a•aGGo 30 S/. osaa FECAL COLIFORM FOR MUNICIPAL:BIOSOLIDS A-1 Medium.'. Single Strength 10-2 dilution 1.0 ml sample Single Strength 10-: dilution ! 0.1 ml sample Date,rrime Test Set -Up: - Q 8 %' 14okpate! Time Test Read: 10 Time Placed in Incubator: ; Q Incubator Temp: 3 ,5, Q Time Transferred to Water Bath: Water Bath Temp: Operator Media Lot #. % 1 3 R % Solids ��s Sample # — Q MPN Fecal .Coliform 10 x MPN Index/ 100 ml Per Gram Total Solids Largest Volume x % Dry Solids - NOTE: + indicates positive results ; - indicates negative results FORMnA: Where: CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE % Total Solids = (A B) x 100 C-B A = Weight of dried residue + dish (mg) B = Weight of empty dish (mg) C = Weight of wet sample + dish (mg) Sample#: Weight of dried residue + dish: Duplicate weight of dried residue + dish: Weight of empty dish Weight of wet sample + dish % Total Solids 70/0 /07C x MO ------------ w N FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS A-1 Medium Double Strength 10'' dilution / 10 ml sample Single Strength 10 2 dilution / 1.0 ml sample Single Strength 10-' dilution / 1.0 ml sample Single Strength 10-= dilution / 0.1 mi sample r , Date. 'rime Test Set -Lip: �[� C7 R' Date. Time Test Read: Time Placed in Incubator:'; Incubator Temp: 0 a ' C Time Transferred to Water Bath. o Water Bath Temp: Operator Media Lot Solids : �'��j Sample # MPN Fecal Coliform = 10 x MPN In i 100 ml = V Per Gram Total Solids Largest Volume x- % Dry Solids NOTE: + indicates positive results ; = indicates negative results CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE FORMULA: % Total Solids (A-B)x100 C-B A = Weight of dried residue + dish (mg) B = Weight of empty dish (mg) C = Weight of wet sample + dish (mg) Sample # : g-- 01;6-0 2- C a 6 Weight of dried residue + dish: Duplicate weight of dried residue + dish : Weight of empty dish Weight of wet sample + dish % Total Solids = 0 09 O'C' o Sg� �S�� FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS A-1 Medium Double Strength Single Strength- 10-1 dilution /, 10 ml sample l 0` dilution / 1.0 ml sample Single Strength Single Strength 10'' dilution / 1.0 ml sample 10-2 dilution / 0.1 ml sample Date.rFime Test Set -Up: 7 - i / " Q • 41- Date! Time Test Read: L9-d • Time Placed in Incubator: . 3Q Incubator. Te Time Transferred to Water Bath: PW Water Bath Temp: Operator Media Lot 3, D % Solids Sam le # p MFN Fecal Coliform ' 10 x MPN Index/* 100 ml = Per Gram Total Solids Largest Volume x %DrySolids NOTE: + indicates positive results ; - indicates negative results FORMULA: Where: CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE % Total Solids = (A - B) x 100 C-B A = Weight of dried residue + dish (mg) B = Weight of empty dish (mg) , C = Weight of wet sample + dish (mg) Sample # Weight of dried residue + dish: Duplicate weight of dried residue .+ dish: Weight of empty dish Weight of wet sample + dish : % Total Solids = �' 3 • �� a�a q I a 91x �aa 3 q.584 9 �s FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS A- I Medium Double Strength 10` dilution / 10 ml sample Single Strength 10`2 dilution / 1.0 ml sample Single Strength 10-1 dilution / 1.0 nil sample Single Strength 10-: dilution / 0.1 nil sample Date:rTime Test Set -Up: Time Test Read: —/ - wh� ��•+•� Time Placed in Incubator: �: ,,� , C Incubator. Temp: SQ Time Transferred to Water at: . BhQ �'"• Water Bath Temp: Operator p Media Lot # _7 3 3 9 �O % Solids �, / /O Sample # p _/D-/S•-D -SDD MPN Fecal Coliforin = 10 x MPN Index / 100 m[ _ Per Gram Total Solids Largest 1Jolume x % Dry Solids NOTE: + indicates positive results ; -indicates negative results FORMULA: Where: CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE % Total Solids (A-B)x100 C-B A = Weight of dried residue + dish (mg) B = Weight of empty dish (mg) C =. Weight of wet sample + dish (mg) Sample # Weight of dried residue + dish: Duplicate weight of dried residue + dish Weight of empty dish Weight of wet sample + dish % Total Solids oz Fl �CIDa s3. �970 FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS . A-1 Medium Double Strength Single Strength _ 1,0'' dilution / 1 O.ml sample 10-' dilution / l .0 ml sample Single Strength Single Strength 10'' dilution / 1.0 ml sample 10' dilution ! 0.1 ml sample Date/Time Test Set -Up: �V ; QQ , Date! Time Test Read: -,26 — 4? Time Placed in Incubator: %.'3D�0,� Incubator Temp:, Time Transferred to Water Bath: .'30 Water Bath Temp: S O Operator ' I Al Media Lot #.3 q 8 Solids 49 4—. Sample # MPN Fecal Coliform. = 10 x MPN Index / 100 nil = Q Per Gram Total Solids Largest Volume x % Dry Solids ' NOTE: + indicates positive results ; - indicates negative results FORMULA: Where: CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE % Total Solids = (A - B) x 100 C-B A = Weight of dried residue + dish (mg) B = Weight of empty dish (mg) C = Weight of wet sample + dish (mg) Sample # : Weight of dried residue + dish: Duplicate weight of dried residue + dish: Weight of empty dish . Weight of wet sample + dish 33.19 S.� 33,67 9f % Total Solids = . 33.-07 3r00.so_iq.5°fo 4a.s76 / FECAL COLIFORM FOR MUNICIPAL BIOSOLDS A-1 Medium Date/Time Test Set -Up: — Q ; A Date! Time Test Read: M Time Placed in Incubator: • • � Incubator Temp: Time Transferred to Water Bath: 0 Water Bath Temp: S I. Operator Media Lot ## Q S % Solids r%. �p Sample # IJ — — A0 MPN Fecal Coliform — 10 x MPN Index 1100 ml. _ Q per Gram Total Solids Largest Volume x % Dry Solids NOTE: + indicates positive results ; - indicates negative results FORMULA: Where: CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS-SAMPLE % Total Solids _ (A-B)x100 C -B A = Weight of dried residue + dish (mg) -B = Weight of empty dish (mg) C = Weight of wet sample + dish (mg) Sample # : 162-1 % - b V — soo Weight of dried residue + dish: Duplicate weight of dried residue + dish: Weight of empty dish Weight of wet sample + .dish % Total Solids �.0L Sl, 8 80 H4. 93.3 1 Pasteurization vessel operates on a constant speed with an in/out time duration of 30 minutes. - MINIMUM MINIMUM DATE 2 HOUR pH 24 HOUR pH TEMP IN TEMP OUT 01 /02/08 12.34 12.24 159 164 01/03/08 12.57' 12.31 157 178 01 /07/08 12.38' 12.19 160 163 01 /08/08 12.27 12.11 163 168 01 /09/08 12.21 12.08 159 164 01/10/08 12.35 12.15 166 160 01/11/08 12.22 , 12.09 166 163 01 / 14/08 12: 39 12.20 161 164 01/15/08 12.46 12.22 - 160 161 01 /16/08 12.28 12.12 160 158 01 / 17/08 12.39 12.22 159 171 01 /18/08 12.39 12.19 158 158 01 /22/08 12.41 12.22 159 160 01 /23/08 12.34 12.13 159 166 01 /24/08 12.17 12.03 161 166 01 /28/08 12.23 12.09 159 ," 176 01 /29/08 12.37 12.18 158 168 . 01 /30/08 12.22 12.08 159 161 01 /31 /08 12.29 12.13 159 169 02/01 /08 12.26 12.09 161 172 02/04/08 12.21 12.13 164 156 02/06/08 12.28 12,12 159 164 02/06/08 12.34 . 12.18 160 170 02/07/08 12.22 12.12 159 164 02/08/08 , 12.28 12.14 163 174 02/11 /08 12.23 12.09 164 171 02/ 12/08 12.24 12.18 163 178 02/ 13/08 12.26 12.14 161 172 02/20/08 .12.29 12.04 159 172 02/21 /08 12.15 12.05 159 158 02/25/08 12.25 12.14 163 167 02/26/08 12.27 12.16. 164 169 02/28/08 12.25 12.16 159 160 02/29/08 - 12.24 " 12.07 160 166 03/03/08 12.18 12.11 161 157 03/04/08 12.32 12.18 164 170 03/05/08 12.20 12.13 160 168 03/06/08 12.33 12.17 159 157 03/07/08 12.31 12.13 160 168 ' 03/ 10/08 12.24 12.12 159 164 03/11 /08 12.06 . 11.87 159 . 161 03/ 12/08 12.08 12.01 160 158 03/13/08 1-2.31 12.18 160 158 03/14/08 12.05 11.96 '158 167 03/ 17/08. 12.17 12.06 161. 164 03/ 18/08 12.31 12.16 165 '168 03/ 19/08 12.24 12.01 161 169 03/20/08 12.22 12.13 165 159 03/21 /08 12.26 12.17 159 162 03/25/08 12.21 12.04 160 169 03/26/08 12.23 12.11 159, 161 03/27/08 12.24 12.07 160 167 03/28/08 12.08, 12.01 160 169 Pasteurization vessel operates on a constant speed with an, in/out time duration of 30. minutes. MINIMUM MINIMUM DATE 2 HOUR pH 24 HOUR pH TEMP IN TEMP OUT 04/01 M 12.21 12.06 155 162 04/02/08 12.21 12.07 159 160 04/03/08 12.19 12.04 159 158 04/04/08 12.20 12.06 159 162 04/07/08 12.22. 12.09 159 158 04/08/08 12.27 12.12 159 162 04/09/08 12.23 12.09 162 168 04/10/08 12.16 12.08 161 160 04/11 /08 12.24 12.13 158 164 04/14/08 12.18 12.01 158 163 04/15/08 12.21 12.03 157 160 04/16/08 .12.08 12.04 157 162 04/25/08 12.23 12.17 161 167 04/28/08 12.17 12.04- 161 -160 04/29/08 12.22 12.04 159 158 04/30/08 12.23 12.08 159 163 05/01 /08 12.24 12.09 161 .166 05/02/08 12.31 12.17 161 158 ' 05/05/08 . 12.28 12.09 162 160 05/06/08 12.24 12.09 159 167, 05/07/08 12.15 12.08 159 165 05/08/08 12.16 12.09 159 162 05/09/08 12.11 12.01 164 162 05/12/08 12.20 12.08 159 167 05/13/08 12.18 12.04 159 164 05/14/08 12.30 12.20 '159 166 05/15/08 12.22 12.14 160, 169 05/16/08 ' 12.27 12.13 160 158 05/19/08' 12.20 12.06 160 160 05/20/08 12.23 12.09 159 162 05/21/08 12.37 1.2.19 -159 162 05/22/08 12.30 12.23 160 170 05/23/08 12.31 12.09 159 '1'60 05/27/08 12.29 12.07 159 168 05/28/08 12.09 12.04 161 159 05/29/08 12.19 12.10 159 167 - 05/30/08 12.26 12.13 163 171 06/02/08 12.08 11.92 159 167 06/03/08 12.14 12.06 160 166 06/04/08 12.13 12.00 159 164 06/05/08 12.10 , 11.96 165 160 06/06/08 12.17 12.03 159 1.59 06/09/08 12.09 11.94 161 164 06/10/08 12.21 12.07 159 159 06/11 /08 12.25 12.08 159 162 06/12/08 12.20 12.03 159 160 06/13/08 12.18 12.00 160 160 06/16/08 12.20 12.05 162 170 06/17/08 12.31 12.25 157 158 06/18/08 12.27 12.12 167 169 06/ 19/08 12.07.. 11.96 159 156 06/20/08 12.11 12.01 159 155 06/23/08 12:27 12.06 166 167 06/24/08 12.25 12.18. 159 161 06/25/08 12.23 12.13 163 160 06/26/08 12.21 12.03 159 161 06/27/08 12.26 12.06 159 159 06/30/08 12.27 12.08 162 159 Pasteurization vessel operates on a constant speed with an in/out time duration of 30 minutes. DATE 2 HOUR pH 24 HOUR pH MINIMUM TEMP IN MINIMUM TEMP OUT 07/01 /08 12.27 12.08 160 162 07/02/08 12.18 12.11 159 164 07/03/08 12.21 12.13 159 169 07/07/08 12.23 12.09 161 167 07/08/08 12.26 12.11 162 158 07/09/08 12.17 12.05 161 161 07/10/08 12.19 12.08 161 161 07/11 /08 12.28 12.17 159 159 07/14/08 12.24 12.12 159 1.60 07/15/08 12.19 12.06 164 167 07/16/08 12.18 12.10 160 173 07/17/08 12.25 12.13 159 162 07/18/08 12.21 12.11 1.60 164 07/21 /08 12.11 12.02 163 168 07/22/08 12.30 12.04 159 162 07/24/08 12.27 12.06 167 161 07/25/08 12.23 12.09 159 160 07/28/08 12.09 12.04 163 165 07/29/08 12.25 12.12 160 163 07/30/08 12.27 12.14 160 168 07/31 /08 12.24 12.08 160 163 08/01/08 12.12 12.01 159 161 08/04/08 12.28 12.09 159 164 08/05/08 12.17 12.09 164 165 O8/06/08 12.24 12.06 164 161 08/07/08 12.08 12.04 160 172 08/08/08 12.26 12.13 161 168 08111 /08 12.19 12.09 164 172 08/12/08 12.25 12.10 160 170 08/ 13/08 12.20 12.03 159 159 08/ 14/08 12.21 12.08 162 159 08/ 15/08 12.26 12.11 161 159 08/ 19/08 12.18 12.09 159 180 08/20/08 12.28 12.03 166 162 08/21 /08 12.29 12.12 160 170 08/22/08 12.23 12.14 170 181 08/25/08 12.20 12.12 165 168 08/26/08 12.23 12.03 171 181 08/28/08 12.27 12.16 161 160 08/29/08 12.06 12.01 160 170 09/02/08 12.20 12.09 162 170 09/03/08 12.24 12.21 161 174 09/05/08 12.30 12.19 159 160 09/08/08 12.18 12.07 165 168 09/09/08 12.23 12.03 160 181 09/ 10/08 12.27 12.13 161 186 09/ 12/08 12.23 12.09 161 186 09/ 15/08 12.21 12.11 .16 5 174 09/16/08 12.19 12.07 162 175 09/ 17/08 12.31 12.12 160 172 09/18/08 12.25 12.12 160 170 09/19/08 12.28 12.09 170 182 09/22/08 12.33 12.18 160 160 09/24/08 12.30 12.16 161 155 09/26/08 12.28 12.06 169 159 Pasteurization vessel operates on a constant.speed with an in/out time duration of 30 minutes. DATE 2 HOUR pH 24 HOUR pH MINIMUM TEMP IN MINIMUM TEMP OUT 10/02/08 12.19 12.05 158 160 10/07/08 12.17 12.07 160 168 10/08/08 12.27 12.08 159' 172 10/09/08 12.21 12.18 157 174 10/ 10/08 12.34 12.23 161 163 10/ 13/08 12.21 12.09 159 177 10/ 14/08 12.31 12.16 150 172 10/ 15/08 12.29 12.20 159 162 10/16/08 12.33 ' 12.14 168 176 10/17/08 12.18 12.07 161 163 10/20/08 12.22 12.11 161 174 10/21 /08 12.29 .12.13 164 162 10/22/08 12.21 12.15 172 172 10/23/08 12.19 12.08 159 162 11 / 17/08 12.18. 12.08 169 179 12/ 18/08 12.08 12.01 181 183 12/19/08 12.09 12.03 160 159 12/30/08 12.22 12.07 160 160 12/31 /08 12.13 12.03 160 159 Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Town of Cheraw Total Dry Tons Applied (Annual): 92 WQ0014248 Cation Exchange Capacity (non 503 only): Allan Baucom Owner: Allan Baucom 100 'Acres Permitted: Site #: 106 Field #: Residual, Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Total Phos- _phorusEMENEEMENEEN Annual Heavy Metal Field Loadings (Calculated in lbs/acre): ' t Me Phos- phorusTotal "I certify, under penalty of law, that this -document was prepared under my- direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware'that there are significant penalties for submitting false information, including the possibility of fines and imprison or knowing violations". Z o 0 Signature o Lan Applier Date " Author Daryl D. Merritt DENR FORM"MFLSF (7/2002) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. 1 'PLACE A- "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. .Facility Name: Town of Cheraw Permit #: WQ0014248 Annual Dry Tons Applied: Owner: Allan Baucan Operator: Allan Baucom ' Cation Exchange Capacity (non 503): Site #: 106 Field #: Acres Utilized:, 100 Acres Permitted: � Q SGalf Totals Per Acre Solids As Deci- Dry Tons Per Acre Residual Sou �rces (Summarize) site Cond. Dry, Wet, Inches Preci Past 24 Hrs. Appli- cation Meth- od** Voli- tila- zation Rate* Miner- ala- zatiop' n. Rate TKN Ammo nia- Ni- trogen Ni- trate- Ni- trogen PAN 1 PAN 2 Must Select Cro 1 or Cro p P 2 Cu.Yd. Report Totals in Gal.Moist Crop 1 Crop 2 April- N/A - ' N A 0.509 0.92 S 0.5 17973 648 381 10776 X TOTALSt ' As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Ap lied Annuallbs/acre .0047 .0008 .0539 .1034 .0065 .0002 .0051 .0423 .0047 .2953 43.86 38.95.1 Date .lbs/ac Current Cumulative lbs/acre .0111, .0042 .2002 .3428- .0270 .001.2 1.0216 .1793' .0095 .8156 - 0064 .0034 1.1463 1.2394 1.0205 .0010 .0165 .1370 .0048 1.5203 Prior Years Cumulative lbs/acre Permitted C., P. L. R. *-* Permit PAN Limit 1 st/2nd Crop ..1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that -there are, - significant penalties fo r.sabmitting false information, including the possibility of fines and imprisonment for knowing violations." too *Application Method: S - Surface, IN - Injection, INC - Incorporation, Signature of Land Applier Date **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 ***C.P.L.R.:.Cumulative Pollutant Loading.Rate Author Daryl D. Merritt DENR FORM FSF (7/2002) 74 _ _2V - - - . ] Ah- Iles �' -►•- :. - ,��� _ � : � -_ Matt - • .. f �'� n � .� raw Allan Baucom site „ 106 N34043.110 ' - 100 acres ..., :`: _'�% � •' _J ,,� •yew ._ :..:< oI� W79°22.764' 101 .0 (Nt •` � \ _,—� � •� * =J� .. �� ..�, mom, l� i , ",.` - .�,� 1107) N3442- 3-D lapoquub Copprigh! 0 1999 DeLom,e Tareoath, 1R 0096 Sonya Data: USGS 900 ft Scale: 1 : 22,100 Detail: 13-2 Daum: MSSI ANNUAL LAND APPLICATION CERTIFICATION FORM Permit#: WQ0014248 Couvty: Facility Name (as shown on permit): Land Application Operator: Chesterfield Year: 2006 Town of Cheraw Land application of residual solids afi allowed by the permit occurred during the past calender year? � ® Yes ❑ No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A: Total number of application fields in permit: Total number of fields land application occurred during the year: 4 Total amount of dry tons applied during the year for all application sites: 1510 Total number of acres land application occurred during the year: 1265 Part B: Facility was compliant during calendar year 2006 with all conditions of the land application permit (including but not limited to items 1-12 below) issued by the Division of Water Quality. M Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permi 2. Soil pH was adjusted as specified in the permit and lime was app i least 6.0 or the limit specified in the permit. 3. Annual soils analysis were performed on each site receiving residl ` (3) copies of laboratory results are attached. 4. Annual TCLP analysis was performed and three (3) copies of certi 5. All other monitoring was performed in accordance with the permit) and three (3) copies of certified laboratory results are attached. , V 6. The facility did not exceed any of the Pollutant Concentration Lim Pollutant Loading Rates- in Table 2 of 40 CFR part 503.13 (applica 7.- All general requirements in 40 CFR Part 503.12 and management I - complied with (applicable to 40 CFR Part 503 regulated facilities). / �rr✓1 ��� P.. 8. All operations and maintenance requirements in the permit were c prior authorization was received from the Division of Water Qualit� - J 9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed in accordance with the crop management plan. 11. No runoff of residuals from the application sites .onto adjacent property or nearby surface waters has occurred. 12. All buffer requirements as specified on the permit were maintained during each application of residuals. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there -are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." -----, � Ricky Ingram/Public Utility Director fr W"4- o Permittee Name. and Title (type or print) FEB Z 3 2007 Signature of l4rrnittee Date I [DEhIn-FAMTE,4) I P RCPrno.fAI Signature of Preparer* Date _-Signiture of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) Author Daryl D. Merritt DENR FORM ACF (7/2002) ANNUAL DISTRIBUTION AND MARKETING/ SURFACE. DISPOSAL CERTIFICATION AND SUMMARY FORM. PERMIT #: WQ0014248 FACILITY NAME.: Town of Cheraw PHONE: (843) 537-8440 COUNTY: Chesterfield OPERATOR• FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) ® Distribution and Marketing (complete Parts A, B, and C) Was the facility in operation during the past calendar _year? ® Yes ❑No No If No ckin nnrtc -A R V and t,nrtwv, f.., _ hpi_' Part A*: _ t B*: Par -. Month Sources s O (include<NPDES-# if applicable) Volume (dry tons) Recipient Information Admendment/ Bulking Agent Residual In Product Out Names) Volume (dry tons) Intended use s O , January February. March SCO020249 SC0020249 SCO020249 27.54 88.76 113.31 38.43 68.47 101.31 65.97 157.23 214.62 Allan'Bauccm Allan Baucom 71717 948 crop fert. crop fert. April. SCO020249 89.62 97:98. 187..60 May SCO020249 64:00 68.1-5 131.90_ June SCO020249 6 00 6.82 12'.82 July SCO020249 54 55 45.60 100.15 August SC0020249 _ . - . 110.77 .81.. 43 192..20 September SC0020249 28.18., 24.32 52.50 r October SCO020249' — 101.46 ' 61.11 -- 162. 57 - November Sd0020249.74,09.74. 09 148.18 ` December SC0020249 75 64 86.07, 161.71 Totals:, Annual (dry: tons): 753 78 .1587 45' Admendment(s) used: Lime Bulking Agents) used: 1 none * If more space than given is required, please attach additional information sheet(s). [3 Check box if additional sheets) are attached .- Part C: Facility, was compliant during -,calendar year . 2006 .:with all conditions of the permit (including but -not limited to items 1-3 below), issued. by the Division of Water Quality. ® Yes ❑ No If No, please provide a written description' why the facility was not compliant, 1. All monitoring was done, in' accordance with the permit and.reported for the year as'required and three (3) copies of certified laboratory results are attached 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the -Division of Water Quality. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law; that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that here are significant penalties for submitting false informaiton,,including the possibility.of fines and imprisonment for knowing violations." Signatur of P ttee' Date Signature of Preparer** Date (if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r) Author Darvl D. Merritt DFNR FnRm nm.gnF (7/9nroi TOWN OF CHERAW WASTEWATER TREATMENT FACILITY BIOSIOLIDS REPORT' MONTH PRESS HOURS DRY CAKE SOLIDS T. TONS LIME USED % LIME TOTAL DRY PROD. LIME $/ TON PROD. POLY $/ TON CAKE LBS. POLY/ TON CAKE LBS. POLY USED JAN 06 85.80 38.43 27.54 41.75 65.97 50.37" 28.11 13.99 537.50 FEB 152.50 68.47 88.76 56.45 157.23 68.21 16.15 8.15 550.00 MAR 192.50 101.31 113.31 52.80 214.62 63.82 15.38 7.65 775.00 APR 181.50 97.98 89.62 47.77 187.60 57.80 13.33 6.63 650.00, MAY _ 143.50 , .68.15 64 .48.33 _ 131.90 58.64 15.48 7.70 525.00 JUN 15.50 6.82 6.00 46.80 12.82 56.78 14.74 7.33 50.00 JUL 97.50 45.60 54.65 54.47 100.15 66.53 15.43 7.68 350.00 AUG 212.00 81.43 110.77 57.63 192.20 70.40 20.36 10.13 825.00 SEP- 73.50 24.32 28.18 53.68 --52.50 65.74 '20.66 10.28 250.00 OCT 171.50 61.11 101.46 62.41 ' '162.57 76.44 16.45 8.18 ' 500.00 NOV. 159.00 74.09 74.09 ' 50.00 148.18 60.52 , 5:43 2.70 200.00 DEC 173.50 86.07 75.64 ' 46.78 161.71 56.59 8.17 4.07 350.00 TOT 1,658.30 753.78 833.67 1,587.45 751.84 189.69 94.49 5,562.50 AVG 138.19 62.82 3.00 51.57 132.29 62.65 15.81 7.87 463.54 MIN 15.50 6.82 .6.00 41.75, 12.82 50.37 5.43. 2.70 50.00 MAX 212.00 101.31 113.31 62.41 214.62 76.44 28.11 13.99 825.00 ANNUAL,.RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report' Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ001'4248 Laboratory: 1) Davis &Brown , Facility Name: Town of Cheraw 2) Clemson University - . NPDES # or 3) WQ#: SCO020249 4) .WWTP Name: Town of Cheraw WWTP, 5) Residual Analvciic Data Sample or Composite Date . 1 /05/06 1 /05/06 3/09/06 3/09/06 5/04/06 5/01/06 7/13/06 7/13/06 9/07/06 9/67/06 11 /6/06 11 /6/06 Percent Solids 42.80 -44.98 44..30 47.04 53.40 .45.30 .40.50 - 51 .84 34.00 - 29.51 54.00 47.18 Arsenic .230, _ .446 .1 .48 :230 ' 1-.05 1 .35 Cadmium . 292 : 307 4.295 _ : 410, : . 210 4.269 . Chromium 13.2. , 13.7 20. 9 ' 24:7 15.8` 22.4 Copper 21.. 8 22.9 25. 2 - 36. 2 � 40.0 48.6 Lead 1'.92 2.34 1:84 2.20 2.22. 3.43 A Mercury .156 .021 .150 .084 .044 .182 `1Vlolybdenum 1:62 1.35 , 1..40 . 2.54 _ 1 77 <.885 Nickel., 9.45 6.5E 9.07 10.E 18.E 20.0 77. Selenium .131 :125 <1.48 .205 1.05 1.35 Zinc 40.2 44:7 64- :.3 67.1 64.4 91.1 ._.... TKN 14550'.9 22193.9 21578.4 16425.5 - 34378.2 16553.6 Ammonia-Nitroge 1333. 9; 1062..9 441.5 771.E 3727.5 847.8 _Nitrate and Nitrite 187.0 363.0j 459:0 845._0 958.1 1200.1 FTotal Phosphorus 6869..7 10533.E 11445.9` 11217.2 19241.1 12823.2 "I certify', under penalty of law; that ;this document was prepared under my direction or supervision in accordance With a system designed .to assure that qualified personnel,properly gathered and evaluated the in submitted: I, am aware that there are significant. penalties for submitting false information, including the_possibility of fines and imprisonment for knowing violations." Signatu of P eparer Date Author Darvl D. Merritt. nFniR FnPKA Rcc;: MOWWN ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: Town of Cheraw, Permit Number: - WQ0014248 WWTP Name: Town "of Cheraw WWTP, NPDES Number: SCO020249 Monitoring Period: _ From 01 /01 /06 To ' 12/31 /06 _ Pathogen .Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: ' Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4❑ , . ,Altemadve 5 ®F -(� Alternative 6 _ ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ 71 Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ 'Pasteurization Class B: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ If applicable .to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization -; ❑ Air Drying ❑ ' Coinposting erobic Digestion ❑ Anaerobic Digestion❑ If applicable to alternative performed (Class A or Class -B) complete the'following monitoring data: Parameter ' - Level in Pathogen Density - g Y um er o -Excee- _ deuces Frequency of Analysis .Sarriple 'Type " Analytical Tech-nique' MinimumGeo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power MPN per gratn.of total solids or 2 x 1'0 to the 6th power CFU per grain, of 1000 mpn per gram of total solid (dry, weight) 0 0 !, 0 MPN 0 Monthly Grab multi - tube Salmonella bacteria (in lieu of fecal coliform) ' 3 MPN per 4 grams total solid (dryweight) Vector Attraction Reduction (40- CFR 50333) - Please indicate option performed: Option 1- 1.0ption 2 [11 Option 3, 10ption 4 ❑ Option 5 ❑ Option 6 El Option T ElOption 8 ❑. Option 9 ❑ Option 10 ❑ ,PNo vector attraction reduction options were performed - E3. ERTIFICATION STATEMENT (please check the appropriate statement) ; ® "I certify, under penalty of law; that the pathogen requirements. in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have. been met." ❑ `;, "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector, attraction reduction requirement in 40 CFR. 503.33 have not been met." (Please note if you check this statement attach an explanation why, you have not met one or •both of the requirements.) "This. determination has been made under my direction and supervision in accordance with the • '-system designed to ensure "that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met: I am aware that there are significant penalties for -false -certification including fine. and imprisonment." Ricky Ingram/Public Utility Director Preparer Name and Title (type or print) Land. Applier Naive and Title (if applicable)(type or print) Signs a of P parer Date* .'Signature of Land Applier (if applicable) Date Author Daryl D. Merritt DENR FORM. RF (7/2002) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Town of Cheraw Owner: Allan . Baucom Site #: 104 Field #: Permit #: WQ0014248 Annual Dry Tons Applied: * 400 Operator: Allan Baucom Cation Exchange Capacity (non 503): Acres Utilized: 330 Acres Permitted: A S'Galf Totals Per Acre Solids As Deci- 1 Dry Tons ' Per Acre Residual Sources (Summarize) Site Cond. C Dry, Wet, ois Inches Preci Past 24 Hrs. Appli- cation Meth- od** Voli- tila- zation Rate* Miner- ala- zation Rate TKN Ammp' nia- Ni- trogen Ni- trate- Ni- trogen PAN 1 PAN 2 Must Select Crop P 1 or Crop 2 Cu.Yd. Report Totals . in Gal. Crop 1 Crop 2 Jan. N/A N/A .4389 13.21 S 0.5 114551 1334 187 8117 g TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Ap lied Annual lbs/acre 0.0013 0.0016 0.0728 0.1202 0.0106 0.0009 0.0089 0.0521 0 0007 0,2217 37,8781 44 755 Date lbs/ac Current Cumulative lbs/acre 0.0096 0.0033 0.1467 0.3160 0.0223 0.0012 0.0138 0.1116 0.0073 0.4323 0.0083 0.0017 0. 0739 0.1958 0. 0117 0:1.0003 0,0049 0.0595 0.0066 0.2106 Prior Years Cumulative lbs/acre Permitted C. P. L. R.*** Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and, evaluated the information submitted. I am aware that there are significa gnial 'es bmitting false information, including the possibility of fines and imprisonment for knowing violations." 2 Q *Application Method: S - Surface, IN - Injection, INC - Incorporation ignature of Land Applier Date **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate Author Daryl D. Merritt DENR FORM FSF (7/2002) ------- ----- 1'Vl\L1• Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Town of Cheraw Total Dry Tons Applied (Annual): W00014248 Cation Exchange Capacity (non 503 only): Allan Baucom Owner: Allan Baucom 330 Acres Permitted: Site #: 104 Field #: 400 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg. % Solids use Raiv PPrrant ttl. .. • .:. • .. Annual Heavy Metal Field Loadings (Calculated in lbs/acre): • e e . __�_®____®_ Elms were e • eee • "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, includin he possibilit fines and imprisonment for knowing violations" 2 lZ o 7 Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) .s✓ "' �• —'`� aJ: •.fit, :N�.. 120 �'• '_ �•. � ,.. � it 4. ,..: . h r'�• Allan Baucom site104 - • �� r _ ,, �.•. ; N34046.580' 330 acres , =.\ .- '�� r_-_,• 1 W79025.690' 441 dlnt Lincoln .. l+r� It ; t '_I •'ir - o ' - f •2 ' y. '�. ••l=� J -- ��'. • �.. o• .t, :.:._.:�.�c; a r-F �� f M n 4 l41 • . ast L 4H t _F.r ,{ a • 74. •. s • b Ir N y t B 200 � \ •�• �•�nb _ m - r'-:.Zr-- _�'.:' ..:+tip , � ��� ��__c�:-1 =3�v III .. 7 ;2--. u� j - N .. \\ `\ �+.� yy Ott � t: t`��1� �p ..I' ..l \\ ��x S2 Lw•' �\\ d� � i \1 \ '2U '\.`, ,` � ��t 1 !' � / ^+•^��/ 1 � f/) \�1 -_\\ 44yq ,,• �r .�1 fJ�.i� Y'•!J" :��� 3-D RopoNads Copyright 0 1999 DeUrme Yarmouth, W 04096 Source Data: DSCS i --I900 ft Scale: 1 : 22,400 Detail: 13-2 Datum: UGS94 ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM .TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Town of Cheraw Owner: Allan Baucom Site #: 105 Field #: Operator: Permit #: WQ0014248 Allan Baucom Acres Utilized:- 210 Annual Dry Tons Applied: 250 Cation Exchange Capacity (non 503): Acres Permitted: " A Specify Totals Per Acre Solids As Deci- D Dry Tons Per Acre Residual Sources (Summarize) Site Cond. Dry, Wet, Moist Inches Preci p' Past 24 Hrs. pp .- A li cation - Meth- od** Voli- tila- zation Rate* Miner- ala- zation Rate TK1V Ammo nia- Ni- trogen Ni- trate- Ni- trogen PAN 1 PAN 2 Must Select Crop 1 or Cro P F 2 f Cu.Yd. Report Totals in Gal.mal Crop 1 Crop 2 Jan. N/A N/A . .4389 1.19 S 0.5 14551 1334 187 8117 X TOTALS: As Cd Cr Cu Pb HR Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre .0012 .0016 .07116 J182 .01-04 .0008 .0088 .0512 .0007 .2180 37..252 44.02 Date lbs/ac Current Cumulative lbs/acre .0092 .0034 .1525 .3326 .0231 .0011 .0140 .1157 .0070 .4452 .0080 .0018 .0809 .2144 .0127 :0003 .0052 .0645 .0063 :2272 Prior Years Cumulative lbs/acre Permitted C. P. L. R. * * * Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated,the information submitted. I am aware that there are signrtt enalties for submitting false information, including the possibility of fines and' imprisonment for knowing violations." 2 l?r o 7 *Application Method: S - Surface, IN - Injection, INC - Incorporation Signature of Land Applier bate **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.6 ***C.P.L.R.: Cumulative Pollutant Loading Rate Author Daryl D. Merritt . DENR FORM FSF (7/2002) l al • 1 . V AL 1.11� 1 ALV 1' a1:/LJl L V ALll \ l7 U lJ lTlITJLt&1\ 1 l %-J JLNl\'1 Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Town of Cheraw Total Dry Tons Applied (Annual): 250 Permit #: WQ0014248 Cation Exchange Capacity {non 503 only): Operator: Allan Baucom Owner: Allan Baucom Acres Used: 210 Acres Permitted: Site #: 105 - Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use m % Solids use Raw Total Phos- .. .:. • Annual Heavy Metal Field Loadings (Calculated in lbs/acre): tal Phos- phorusIMENEEMENEEMEN "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, includi the possibility of fines and imprisonment for knowing violations" ztzo� Signs re of and Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) f {+v .� _ .. --�' `` / •'N • � .. -•_. ':i• •.�-_ Cat x ` ` 5P j1 :i11. — ,�\j� /+� r J l'!' ••/\jJ `fN�,`Y� '�� ..'— .���. �•l t!� _—.�.._ �5` _ �.. , .. , ," f194 ly N34',44: \' ,\ ��`�'� ; ✓`' f`=%' Z� _ Gj 5tewartsville`\`: �\l !97 �\\ � 1$14. � •- eY�l ` '� � ` _ � it � — `,- .. • � � •` : � 160I Y' •2' � � it �. - /• �\i s _ f E [may' 1�Nt• 8 i., ar Ili IS NK ._t._ 11 �{ W C `l _�-= l ` .�`• -- `c, ydl/r 2. + � Allan Baucom site #105 ? N34o43.286' 210 acres .✓'� _-�� "I�� - , � ' W79°886' 276 dmt W��' JInk 7. 3-D Topoquads Copyright ® 1999 DeLorme Yarmouth, HE 04096 Source Data: DSGS i 900 ft Scale: I : 22,400 Detail: 13-2 Datum: WGS84 ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Town of Cheraw Owner: Allan Baucom Site #: 106 Field #: Permit #: WQ0014248 Operator: Allan Baucom Acres Utilized: 306 Annual Dry Tons Applied: • 360 Cation Exchange Capacity (non 503): Acres Permitted: A S'Galf Totals Per Acre Solids As Deci- mal Dry Tons Per Acre Residual Sources (Summarize) Site Cond. Dry, Wet, Moist Inches Preci p' Past 24 Hrs. Appli- cation Meth- od** Voli- tila- zation Rate* Miner- ala- zation Rate TKN Ammo nia- Ni- trogen Ni- trate- Ni- trogen PAN 1 PAN 2 Must Select Crop 1 p or Cro 1 2 Cu.Yd. Report Totals in Gal. Crop 1 Crop Feb. N/A N/A .41-89 1.18 S 0.5 14551 11334 187 8117 g TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Ap lied Annuallbs/acre .0012 .0016 .0710 .1172 .0,1103 .0008 .0087 .0508 .0007 .2162 36.939 43.646 Date lbs/ac Current Cumulative Ibs/acre .0041 .0029 .1226 .2136 .0171 .0009 .0152 .1140 .0025 .4464 .0029 .0013 .0516 1.0964 .0068 1 .0001 .0065 .0632 .0018 .2302 Prior Years Cumulative lbs/acre Permitted C. P. L. R. * * * Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are signi cant penalties forsubmitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation Signature of Land Applier Date **Volitilization Rate: Surface - 0.5, Injection/Incorporation 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate Author Daryl D. Merritt DENR FORM FSF (7/2002) Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Town of Cheraw Total Dry Tons Applied (Annual): 360 Permit #: WQ0014248 Cation Exchange Capacity (non 503 only): Operator: Allan Baucom Owner: Allan Baucom Acres Used: 305 Acres Permitted: Site #: . Residual Analvsis Data (Heavv Metals and Total Phncnhnrnc i,qP mo/ko 106 Field #: % gr%HrIL nen 1Do—r D^ ...4 al\_ Total Phos- phorusEWEEMENEEMEN Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Mr. M. NMI Total . os- "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations" vrzo7 f6atuof Lan Applier Date Author Daryl D. Merritt DENR FORM, MFLSF (7/2002) W;ta 1?1� I'l-, i. At I ; . t 41. 1 It 4" NTIA At., u NA C• it- ' � • }`4Cr�,CC-. ``\ , i /,`i) 1• I'�11-�I r't � ���il I =_,,.i.-'i �1.�''� �fi �I �� �_ 1 J / �-�\ 1/ / o . � ��� I.I.il, i t it 9V Ot 4:: it IN I jiAl 1,0 En W,791,23 4 Ln r- —1 m % % ro ro:: ®r pq I J re) C14 101 rt z it 0 4r, I-' 24 n ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Town of Cheraw Owner: Allan Baucom Operator: Allan Site #: 113 Field #: Permit #: W00014248 Annual Dry Tons Applied: * 500 Baucom Cation Exchange Capacity (non 503): Acres Utilized: 420 Acres Permitted: Q S�Galf Totals Per Acre Solids As Deci- mal Dry Tons Per Acre Residual Sources (Summarize) Site Cond. Dry, Wet, Moist Inches Preci p' Past 24 Hrs. Appli- cation Meth- od** Voli- tila- zation Rate* Miner- ala- zation Rate TKN Ammo nia- Ni- trogen Ni- trate- Ni- trogen � PAN 1 PAN 2 Must Select Crop 1 or Cro P F 2 Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 Feb. N/A N/A .43891 500 S 1 0.5 14551 1334 187 81177 X L TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Ap lied Annuallbs/acre .0012 .0016 .0716 .1182 .0104 .0008 .0088 .0512 .0007 1.2180 37.25 44.02 Date lbs/ac Current Cumulative lbs/acre .0051 .0034 .2152 .3237 .0222 .0011 .0221 .1657 .0016 .6504 .0039 .0018 .1436 1.2055 .0118 .0003 .0133 .1145 .0009 .4324 Prior Years Cumulative lbs/acre Permitted C. P. L. R. * * Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant enalties fors mitting false information, including the possibility of fines and imprisonment for knowing violations." 4e4d►z(b7 *Application Method: S - Surface, IN - Injection, INC - Incorporation Signature of Land Applier Date **Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate Author Daryl D. Merritt DENR FORM FSF (7/2002) Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Owner: Allan Baucom Acres Used: 420 Acres Permitted: Site #: 113 Field #: Residual Analysis Data (Heavy Metals and Total Phosnhnrnc nce mofk4_ a/,� Cnlirlc ncn RQ.0 po,., _+ 4N. Town of Cheraw WQ0014248 Allan Baucom 500 Sample - ---- - -- ----- ••. or Com- 1 /5/ 1 /5/ 06 06 posite Date % Solids 42.80 44.98 Arsenic 0.23 Cadmium 0.292 Chromium 13.2 Copper 21.8 Lead 1.92 Mercury 0.156 Molyb- 1.62 denum Nickel 9.45 Selenium 0.131 Zinc 40.2 Total Phos- 6869.7 horus Annual Heavy Metal Field Loadings (Calculated in lhs/acre): y� y 3 a y s� Arsenic .0012 .0012 Cadmium .0016 .0016 hromiu .0716 .0716 Copper .1182 .1182 Lead .0104 , .010404 Mercury .0008 .0008 Molyb- , 0088 denum .0088 Nickel .0512 .0512 Selenium .0007 .0007 Zinc .2180 .2180 Total 37.25 Phos- 37.252 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, includine,the possibility of fines and imprisonment for knowing violations" f2 ni ignature o La Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) 3-D TopoQoads Copyright ® 1999 DeLome Yarmouth, NE 04096 Source Data: DSGS f-- �900 ft Scale: 1 : 22,400 Detail: 13-2 Datum: AGS84 CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES BIOSOLIDS SAMPLE DATEJ'Jaituary 542006 Biosolids Maximum Maximum Maximum Maximum Metal Allowable Allowable Application Application Content, Metal App. Rate, Rate, Rate, METALS ppm Content, ppm #/Acre/Yr. DT/Acre/Yr. WT/AcrelYr, Arsenic, Total 0.27 41.00 1.80 1674.78 3349.57 Cadmium, Total 0.34 ' 39.00 1.70 1245.89 2491.78 Chromium, Total 15.42 1200.00 134.00 2172.42 4344.85 Copper, Total 25.47 1500.00 67.00 657.71 1315.41 Lead, Total 2.24 300.00 13.00 1448.96 2897.92 Mercury, Total. 0.18 17.00 0.75 1028.85 2057.69 Molybdenum, Total 1.89 18.00 0.80 105.68 211.36 Nickel, Total 11.04 420.00 18.70 423.47 846.94 Selenium, Total 0.15 36.00 4.50 7351.15 14702.29 Zinc, Total 46.96 1625.00 125.00 665.42 1330.85 PCB BDL 1.60 ' Actual metal content less than amount indicated. Blosolids Biosolids Maximum Maximum Nutrient Nutrient Crop/Soil Application Application Content, Content, Requirement, Rate, Rate, ppm % #/Acre" DT/Acre/Yr. WT/Acre/Yr. Ammonium Nitrogen 666.96 0.07 Organic Nitrogen 6608.49 0.66 Incorporated Available Nitrogen 4646.51 0.46 120.00 6.46 12.91 Surface Available Nitrogen 4446.42 0.44 120.00 6.75 13.49 Phosphorus as P205 3434.86 0.34 80.00 5.82 11.65 Potassium as K20 844.82 0.08 50.00 14.80 29.59 Calcium, Total 152767.90 15.28 Calcium as CaO 213875.06 21.39 Calcium as CaCO3 (CCE) 219972.77 22.00 2000.00 2.27 4.55 Magnesium, Total 2751.22 0.28 Manganese 77.81 0.01 Sulfur 1000.44 0.10 Percent Moisture 50.00 '* These are typical values and must be adjusted based upon spec site conditions DT is Dry Tons of Biosolids. WT is Wet Tons of Biosolids. CERTIFICATION: This biosolid product has been produced by the Town of Cheraw's Wastewater Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature and lime (calcium oxide). The Town of Cheraw certifies that this biosolid complies with the Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has a metal and nutrient content as presented above. DIRECTIONS FOR USE: This biosolid is intneded to be used as a soil amendment. The biosolid land application rate shall not exceed the most restrictive Maximum Application Rate as indicated in the table above. The application rate for nitrogen, phosphorus, potassium, and calcium is dependent. upon the crop grown and site soil characteristics. The user should contact the Clemson Extension Service (843-623-2134) and/or the Soil Conservation Service (843-623-2187) for assistance in determining the proper application rate for each crop and site. In no case shall the land application rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension Service Circular #476 titled "Lime and Fertilizer Recommendations." THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY. AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES. THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS BIOSOLID PRODUCT. Mr. Ricky D. Ingram, Public Utility Director P.O. Box 219; Cheraw, SC 29520 Telephone: 843-537-8440 FAX: 843-537-8442 QUANTITY RECEIVED: RECEIVED BY: Davis & Brown PO Box 15038 Quinby, SC 29506 (843) 665-6746 .FAX: (843) 629-1444 Certificate of Analysis Client: CHERAW, TOWN OF South Carolina Certification Number: 21117 P.O.BOX 219 North Carolina Certification Number: 612 CHERAW, SC 29520 Client #: 168 Receipt Date: 06-Jan-.06 Contact: SHERRY TOLSON Report Date: 27-Jan-06' Sample Date: 05-Jan-06 SDG #: - SDG-046340 Parameter Lead, Total Nickel, Total Zinc, Total Reporting Result Limit Unit <0.656 0.05 mg/L 0.037 0.01 mg/L 0.468 0..01 mg/L, Approved By: Van Ward Lab Director Method Flag Date Time Analyst EPA 200.7 1/11/2006 10:45 DH EPA 200.7 1/9/2006 17:38 DH EPA 200.7 1/9/2006 17:38 DH LSID-104212 1001-X Cyanide <0.005 0.005 mg/L EPA 335.2 1/10/2006 8:00 MLL LSID-104213 1002-X Cyanide <0.005 0.005 mg/L. EPA 335.2 1/10/2006 8:00 MLL LSID-104214 Be IO:&O.LIDS is0&201 Acid Digestion (Solids) YES EPA 200.2 1/9/2006 10:00 DH TCLP PASS P/F SW-846 S16 1/13/2006 WSF Ignitability >170 Deg. F. SW846 1010 'S16 1/9/2006 10:00 _ CWP Percent Moisture 57.2 0.1 Wt% SW846 3540 1/10/2006 12:30 JR Aluminum, Total 3840 0.584 mg/kg SW846 6010A 1/12/2006 14:46 DH Arsenic; Total 0.230 0.131 mg/kg SW846-6010A 1/25/2006 16:40 JR Cadmium, Total . <0.292 0.292 mg/kg SW846 6010A 1/9/2006 17:38 DH Chromium, Total 13.2 0.292 rng/kg SW846 6010A 1/9/2006 17:38 DH Copper, Total 2.1.8 0.292 mg/kg SW846 6010A 1/9/2006 17:38 DH Lead, Total 1.92 1.46 mg/kg SW846 6010A 1/11/2006 10:45 DH- Page 2 Davis & Brown PO Box 15038 Quinby, SC 29506 (843) 665-6746 FAX: (843) 629-1444 Certificate of Analysis Client:. CHERAW, TOWN. OF 'South Carolina Certification Number: 21117 P.O.BOX 219 _ North Carolina Certification Number: 612 CHERAW, SC 29520 Client #: 168 Receipt Date: . 06-Jan-06 Contact: SHERRY. TOLSON Report Date: 27-Jan-06 Sample Date: 05-Jan-06 SDG #: SDG-046340 Approved By: VanVard Lab Director Reporting Parameter Result Limit Unit Method Flag Date Time . Analyst' Molybdenum, Total 1.62 1.2 mg/kg SW846 6010A 1/12/2006 ' 14:51 DH Nickel,- Total 9.45 0.292 mg/kg SW846 6010A 1/9/2006 17:38 DH Zinc, Total 40.2 0.292- mg/kg SW846 6010A:. 1./9/2006 .17:38. DH Mercury, Total 0.156, 0.053' mg/kg. SW846 7470A 1%12%2006 15:26 DH Selenium, Total <0.131 0.131 mg/kg SW846 7741A 1/17/2006 12:04 . JR PCB BDL 1.4 mg/kg SW846 8080. S16 1/10/2006 S:23 JSW Reactivity, Cyanide <0.12 0.12 mg/kg SW846 9610 S16 1/11/2006 11:45 DJS Reactivity, Sulfide 29 25 mg/kg SW846 9030 1/9/2006 15:00 CWP pH (Solids) 10.6' S.U. SW846 9045 : 1/16/2006 14:40 LM Paint Filter PASS P/F SW8469095 S16 1/9/2006 11:30 CWP LSID-104215 1-5-06-102 Acid Digestion (Liquids) Aluminum, Total YES 0.040 0.02 mg/L EPA 200.2 'EPA-200.7 1/9/2006 1/12/2006 1:00 14:46 DH DH LSID-104216 1001-0 Total Toxic Organics 0.154 0.01 mg/L 8260/8270. S11 1/10/2006 15:11 VMW LSID-104217 1002-0 Total Toxic Organics 0.209 0.01 mg/L 8260/8270 Sl l 1/11/2006 17:08 JCK 0 Page 3 ANIMALWAS TEANALYSISREPO RT Page l of A N I M A L W A S T E A N A L Y S I S R E P O R T Agricultural -Service Laboratory LAB No. 10092 'Clemson.University- TOLSON, SHERRY ACCOUNT COCHSFL PO BOX 219 DATE 01-30-2006 CHERAW SC 29520 CHERAWTOWNOF656@BELLSOUTH..NET SAMPLE NO. 012,5952:0_ MANURE : OTHER STORAGE: UNCOVERED -----------------RESULTS REPORTED ON AN AS-SAMPLED-BASIS---------------------- lbs/ton Ammonium Nitrogen 0.06 % 1.20 Organic Nitrogen 0.59 % 11.89 Nitrate Nitrogen --------------------------------------------------------------- 84.12 ppm 0.17• INCORPORATED AVAILABLENITROGEN ESTIMATE 8.36 SURFACE AVAILABLE NITROGEN ESTIMATE 8.00 --------------------------------------------------------------- Phosphorus as P205 0.31 % 6.18 Potassium as K20• 0.08 % 1.52 Calcium 13.74 % 274.86 Magnesium 0.25 % 4.95 Sulfur 0.09 % 1.80 Zinc 43.64 ppm 0.09 Copper 21.59 ppm 0.04 Manganese 68.83 ppm 0.14 Sodium 161.95 ppm 0.32 Moisture 55.02 Calcium Carbonate Equivalency 39.58 % 791.55 -------------------------------------- 7--------------------------------------- INCORPORATED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of organic-N, and 100% of nitrate-N (if determined). Assumes the manure, will be incorporated into the soil within'hours of application. Assumes some loss of ammonium-N during application and prior to incorporation., SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of organic-N, and 100% of•nitrate-N (if determined). Assumes the manure will be left on the surface•of the soil with no incorporation by plowing or irrigation. Available nitrogen calculations are estimates and if nitrate-N was not re- quested the amount of .available nitrogen may be slightly more than reported. Also, the actual amount may be more or less than the estimate depending on the composition of the manure, soil type, and environmental conditions. All of the potash in the animal waste should be plant available in the first year of application. Although not all of.the phosphorous is available in the first year, its availability should -be comparable to that in commercial fertilizers. The rate of animal.waste to apply for crop production is dependent on the nutrient content of the waste, method of application and incorporation,•soil, test, crop to be grown, and previous manure applications. In most cases, the plant available nitrogen content of the waste is used to determine the rate of application. The Agricultural Service Laboratory is a public service of Clemson University, an affirmative action and equal opportunity educational institution. ** http://www.clemson.edu/agsrvlb ** http://www.Clemson.edu/aglabresults/COCHSFLTOLSON,%20SHERRY0601300000001.... , 1/31/2006 %moisture % solids lbs. solids/ton lbs. solids/500 tons 44.98 899.E 449800 % ppm lbs/ton % ppm lbs/ton as -sampled as-sam led as -sampled- dry,ton dry ton d Ammonium Nitrogen 0.06 " 600 1, 2 0.133393 1333.926 2.667852 Organic Nitrogen 0.5945 " 5945 �u 11 $9 1.321699 13216.99, 26.43397 Nitrate Nitrogen 0.008412 84`1:2 0 16824. 0.018702 '.187.0165 0.374033 Incorporated.Available Nitrogen Estimate 0.418 4180 8 36: 0.929302 9293,01.9 18.58604 Surface Available Nitrogen Estimate 0.4 4000 '8; 0.889284 8892.841 17.78568 Phosphorus as P205 0.309 3090 6 18 0.686972 6869.72 13.73944 Potassium as K20 0.076 760 ^ 1 52 0.168964 1689.64 3.37928 Calcium . .13.743 , 137430 : ' x ` 274 86 30.55358 305535.8 611.0716 Magnesium 0.2475 2475 4:95 0.550245 5502.446 11.00489 Sulfur 0.09 900 0.200089 2000.889 4.001779. Zinc . 0.004364 43 64 0.08728 0.009702 97.0209 0.194042 Copper 0.002159 r ` , 21 59 0.04318 - 0.0048 47.99911 0.095998 Manganese 0.006883 ti 6&83 i 0.13766 0.015302 153.0236 0.306047 Sodium 0.016195 a 161 95, 0.3239 0:036005 360.0489, 0.720098. Calcium Carbonate Equivalency 39.5775 395776 k 1 791 55 87.98911 879891 A 1759.782� CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES BIOSOLIDS SAMPLE DATE:VOC- 2006P METALS Biosolids Metal Content, ppm Maximum Allowable Metal Content, ppm Maximum Allowable App. Rate, #/Acre/Yr. Maximum Application Rate, DT/Acre/Yr. Maximum Application Rate, WT/AcrelYr. 1 Arsenic, Total 0.50 41.00 1.80 893.95 17a7.89 Cadmium, Total 0.35 39.00 1.70 1226.55 2453.09 Chromium,.Total 15.46 1200.00 134.00 2166.50 4332.99 Copper, Total 25.85 1500.00 67.00 648.06 1296.11 Lead, Total 2.64 300.00 13.00 1230.56 2461.11 Mercury, Total 0.02 17.00 0.75 7910.71 15621.43 Molybdenum, Total 1.52 18.00 0.80 131.26 262.52 Nickel, Total 7.40 420.00 18.70 631.41 1262.82 Selenium, Total 0.14 . 36.00 4.50 7974.00 15948.00 Zinc, Total 50.45 1525.00 125.00 619.41 1238.81 PCB . BDL 1.60 ' Actual metal content less than amount indicated. Biosolids Nutrient Content, ppm Biosolids Nutrient Content, % Crop/Soil Requirement, #/Acre " Maximum Application Rate, DT/Acre/Yr. Maximum Application Rate, W'f/AcrelYr. Ammonium Nitrogen 531.46 0.05 Organic Nitrogen 10565,48 1.06 - Incorporated Available Nitrogen 7057.82 0.71 120.'00 4.25 8.50 Surface Available Nitrogen 6898.38 0.69 120.00 4.35 8.70 Phosphorus as P205 6266.79 0.63 80.00 3.80 7.59 Potassium as K20 1626.28 0.16 50.00 7.69 15.37 Calcium, Total 140896.05 14.09 , Calcium as CaO 197254.46 19.73 Calcium as CaCO3 (CCE) 176392.43 17.64 2000.00 2.83 5.67 Magnesium, Total 2800.81 0.28 Manganese 47.83 0.00, Sulfur 1349.91 0.13 Percent, Moisture 60.00 - `rhese are typical values and must be adjusted based upon specific site conditions DT is. Dry Tons of Biosolids. WT is Wet Tons of Biosolids.. CERTIFICATION: This biosolid product has been produced by the Town of Cheraw s Wastewater Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature and lime (calcium, oxide). The Town of Cheraw certifies that this biosolid complies with the Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has a metal and nutrient content as presented above. DIRECTIONS FOR USE: This biosolid is intneded to be used as a soil amendment. The biosolid land application rate shall not exceed the most restrictive Maximum Application Rate as indicated In the table above. The application rate for nitrogen, phosphorus, potassium, and calcium Is dependent upon the crop grown and site soil characteristics. The user should contact the Clemson Extension Service (843-623-2134) and/or the Soil Conservation Service (843-623-2187) for assistance in determining the proper application rate for each crop and site. In no case shall the land application rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension Service Circular #476 titled "Lime and Fertilizer Recommendations." THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY. AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES. THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS BIOSOLID. PRODUCT. Mr. Ricky D. Ingram, Public Utility Director P.O. Box 219; Cheraw, SC 29520 Telephone: 843-537-8440 FAX: 843-537-8442 PRODUCT USER 14AME: ADDRESS: UUhltl 11I I nr_l,M VCU: RECEIVED BY: Davis & . Brown PO Box 15038 Quinby, SC 29506 (843) 665-6746 FAX: (843) 629-1444 Certificate of Analysis Client: CHERAW, TOWN OF P.O.BOX 219 CHERAW., SC 29520 Client #: 168 Contact: SHERRY TOLSON Sample Date: 09-Mar-06 SDG #: SDG-047386 Reporting Parameter Result Limit Unit South Carolina Certification Number: 21117 North Carolina Certification Number: 612 Receipt Date: 10-Mar-06 Report Date: 30-Mar-06 Approved By: Van Ward Lab Director Method Flag Date Time Analyst LSID-106258 SLI SO IL DS 3 9 06=500 V Acid Digestion (Solids) YES EPA 200.2 3/14/2006 13:00 DH Percent Moisture 55.7 0.1 wt% SW846 3540 3/14/2006 16:30 JR Aluminum, Total 3800 0.5 mg/kg SW846 6010A_ 3/24/2006 11:37 `DH Arsenic, Total 0.446 0.125 mg/kg SW846 6010A 3/13/2006 18:14 JR Cadmium, Total <0.307 0.307 mg/kg SW846 6010A 3/13/2006 16:08 DH Chromium, Total 13.7 0.307 mg/kg SW846 6010A 3/1372006 16:08 DH Copper, Total 22.9 0.307 mg/kg SW846 6010A 3/13/2006 16:08 DH Lead, Total 2.34 1.5 r-ig/kg SW846 6010A 3/14/2006 16:10 DH Molybdenum, Total 1.35 1.2 mg/kg SW846 6010A 3/15/2006 17:21 DH Nickel, Total 6.56 ' 0.307 mg/kg SW846 6010A 3/13/2006 16:08 DH Zinc, Total 44.7 0.307 mg/kg SW846 6010A 3/13/2606 16:08 DH Mercury, Total <0.021 0.021 mg/kg SW846 7470A 3/21/2006 9:35 DH Selenium, Total <0.125 0.125 mg/kg SW846-7741A 3/14/2006 14:14 JR PCB BDL 6.273 mg/kg SW846 8080 S16 3/16/2006 11:47 TLW i Page 2 ANIMAL WAS TEANALYSISREPORT Page 1 of 2 A N:.I M A L W A S T E A N A L Y S I S R E P O R T Agricultural Service Laboratory LAB No. 30500 Clemson University TOLSON,, SHERRY ACCOUNT COCHSFL PO BOX 219 DATE 03-29=2006 CHERAW SC 29520 CHERAWTOWNOF@BELLSOUTH.NET SAMPLE NO.R0�3000-Q5. NURE: OTHER STORAGE: UNCOVERED -----------------RESULTS REPORTED ON AN AS -SAMPLED BASIS------------------=--- lbs/ton Ammonium Nitrogen 0.05 % 1.00 Organic Nitrogen 0.99 % 19.88 Nitrate Nitrogen ------------------------------------------------------------- 170.75 ppm 0.34 INCORPORATED AVAILABLE NITROGEN ESTIMATE 13.28 SURFACE AVAILABLE NITROGEN ESTIMATE ----------------------------------------------------- 12,98 Phosphorus as 'P205 0.50 % 7--------- 9.91 Potassium as K20 0.15 % 3.06 Calcium 13.26 % 265.11 Magnesium 0.26 % 5.27 Sulfur 0.13 % 2.54 Zinc 67.74 ppm 0.14 Copper 35.75 ppm 0.07 Manganese 45..16 ppm 0.09 Sodium 166.99 ppm 0.33 Moisture 52.96 % Calcium Carbonate Equivalency 33.19 % 663.80 ------------------------------ 7----------------------------------------------- INCORPORATED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be incorporated into the soil within hours of application. Assumes some loss of ammonium-N during application .and prior to incorporation. SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of organic-N, and 100%.of nitrate-N (if determined). Assumes the manure will be left on the surface of the soil with no incorporation by plowing or irrigation. Available nitrogen calculations are estimates and if nitrate-N was not re- quested the amount of available -nitrogen may be slightly more than reported. Also, the actual amount may be more or less than the estimate depending on the composition of the,manure, soil type, and environmental conditions. All of the potash in the animal waste should be plant available in the. first year of application. Although not all of the phosphorous is available in the first year, its availability should be comparable to that in commercial fertilizers. The rate of animal waste to apply for crop production is dependent on the nutrient content of the waste, method of application and incorporation, soil test, crop to be grown, and previous manure applications. In most cases, the plant available nitrogen content of the waste is used to determine the rate of application. The Agricultural Service Laboratory is a public service of Clemson University, an affirmative action and equal opportunity educational institution. ** http://www.clemson.edu/agsrvlb ** http://www.clemson.edu/aglabresults/COCHSFLTOLSON,%20SHERRY0603290000005.... 3/30/2006 % moisture % solids lbs. solids/ton lbs. solidst500 tons .-47.04 940.8 470400 % PPm lbs/ton %g ppm lbstton as-sam led as -sampled as -sampled dry, ton dry ton d - Ammonium Nitrogen 0.05 500 , 1:.0.106293 1062.925 2.12585 Organic Nitrogen 0.994 9940 19:88 2.113095 21.130.95 . 42.261,9 Nitrate. Nitrogen 0.017675 r 170 75,, 0.3415 0.036299. 362.9889 0.725978 Incorporated Available Nitrogen Estimate 0.664 6640 13 28 1.411565 141,15.65 28.23129 Surface Available Nitrogen Estimate : 0.649. 6490 1298 1.379677 13796.77 27.59354 Phosphorus as P205 0.4955 4%5 9 91'' 1.053359 10533.59 21.06718 Potassium as It20 0.1.53 1530 3:06. 0.325255 3252.551 6.505102 Calcium 13.2555 132555 265;1=1' 28.17921 281192.1 563.5842 Magnesium 0.2635 2635 ;- , 5z2i 0.660162 5601.616 11.20323 Sulfur 0.127 1270 2.54. 0.269983 2699.83 5.39966 Zinc 0:066774 67 74; 0.13548 .0.014401 144.0051 0.28801 Copper. 0.003575 35 75`-; , 0.0715 0.0076 75.99915 0.151998 Manganese 0.004516 ,' 4516+ . 0.09032 0.0096 96.0034 0.192007 Sodium 0.016699 166 99 ° 0.33398 0.0355 354.9957 0.709991 Calcium Carbonate E uivalenc,y 33.19 331900 - L 6638 '70.55697 705569.7 1411.139 CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES BIOSOLIDS SAMPLE DATE: May-1,-2006- Biosolids Maximum Maximum Maximum Maximum Metal Allowable Allowable Application Application Content, Metal App. Rate, Rate, Rate, METALS ppm Content, ppm #/AcrefYr. DT/Acre/Yr. WT/Acre/Yr. Arsenic, Total 1.39 41.00 1.80 324.73 649.46 Cadmium, Total 0.28 '. 39.00 1.70 1538.64 3077.29 Chromium, Total 19.57 1200.00 134.00 1711.87 3423.73 Copper, Total 23.60 1500.00 67.00 709.88 1419.76 Lead, Total 1.72 300.00 13.00 1886.41 3772.83 Mercury, Total, 0.14 17.00 0.75 1335.00 2670.00 Molybdenum, Total 1.31 18.00 0.80 152.57 305.14 Nickel, Total 8.49 420.00 18.70 550.49 1100.97 Selenium, Total 1.39 36.00 4.50 811.82 1623.65 Zinc, Total 60.21 1525:00 125.00 519.05 1038.10 PCB BDL 1.60 " Actual metal content less than amount indicated. Biosolids Biosolids Maximum Maximum, Nutrient Nutrient Crop/Soil Application 'Application Content, Content, Requirement, Rate, , Rate, ppm % #/Acre *° DT/Acre/Yr. WT/Acre/Yr. Ammonium Nitrogen 220.75 0'02 Organic Nitrogen 10568.43 1.06 Incorporated Available Nitrogen 6887.42 0.69 120.00 4.36 8.71 Surface Available Nitrogen 6821.19 0.68 120.00 4.40 8.80 Phosphorus as P205 5722.96 0.57 80.00 3.49 6.99 Potassium as K20 1385.21 0.14 ' 50.00 9.02 18.05 Calcium, Total 139034.22 13.90 Calcium as C60 194647.90 19.46 Calcium as CaCO3 (CCE) 183907.28 18.39 2000.00 2.72 5.44 Magnesium, Total 2500.00 0.25 Manganese 77.26 0.01 Sulfur 1302.43 0.13 Percent Moisture 50.00 These are typical values and must be adjusted based upon specific site conditions DT is Dry Tons of Biosolids. WT is Wet Tons of Biosolids. CERTIFICATION: This biosolid product has been produced by the Town of Cheraw s Wastewater Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature and lime (calcium oxide). The Town of Cheraw certifies that this biosolid complies with the Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has a metal and nutrient content as presented above. DIRECTIONS FOR USE: This biosolid is intneded to be used as a soil amendment. The biosolid land application rate shall not exceed the most restrictive Maximum Application Rate as indicated in the table above. The application rate for nitrogen, phosphorus, potassium, and calcium is dependent upon the crop grown and site soil characteristics. The user shouldcontact the Clemson Extension . Service (843-623-2134) and/or the Soil Con va sertion Service (843-623-2187) for assistance in determining the proper application rate for each crop and site. In no case shall the land application rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension . Service Circular #476 titled "Lime and Fertilizer Recommendations." THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY. AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES. THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS BIOSOLID PRODUCT. Mr. Ricky D. Ingram, Public Utility Director P. 0. Box219; Cheraw, SC 29520 Telephone: 843-537-8440 FAX: 843-537-8442 PRODUCT USER NAME: ADDRESS: INTENDED USE: LOCATION OF USE: QUANTITY RECEIVED: RECEIVED BY: Davis & Brown PO Box 15038 Quinby, SC 29506 (843) 665-6746 FAX: (843) 629-1444 Certificate of Analysis Client: CHERAW, TOWN OF South Carolina Certification Number: 21117 P.O.BOX 219 North Carolina Certification Number: 612 CHERAW, SC 29520 Client #: 168 Receipt Date: 05-May-06 Contact: SHERRY TOLSON L" ReportDate: 01-Jun-06 Sample Date: 26-Apr-06 SDG #: SDG-048280 Approved By: Van Ward, -Lab Director Reporting Parameter Result Limit Unit Method LSID-108152 5-4-06-F Flag Date Time Analyst Fluoride 0.96 0.2 mg/L SM 4500FC 5/16/2006 15:00 MLL LSID-108153 SOURCE 050406 Total Organic Carbon 2.9 .0.5, mg/L EPA 415.1 5/17/2006 9:30 SM LSID408154 FINISHED 050406 Total Organic Carbon <0.50 0.5 mg/L EPA 415.1 5/17/2006 9:30 SM LSID-108155 Xr5_B-4W0-e-50TJUW Acid Digestion (Solids) YES EPA 200,2 5/10/2006 9:00 DH Percent Moisture 46.6 0.1 Wt% SW846 3540 5/5/2006 15:30 JR Aluminum, Total 3340 0.59 mg/kg SW846 6010A -5/15/2006 12:06 DH Arsenic, Total <1.48 1.48 mg/kg SW846 6010A 5/15/2006 14:29 JR Cadmium, Total <0.295 0.295 mg/kg SW846 6010A 5/10/2006 14:07 DH Chromium, Total 20.9 0.295 mg/kg SW846 6010A 5/10/2006 14:07 DH Copper, Total 25.2 0.295 mg/kg SW846 6010A 5/10/2006 14:07 DH Lead, Total 1.84 1.5 mg/kg SW846 6010A 5/10/2006 16:38 DH Molybdenum, Total 1.40 0.981 mg/kg SW846 6010A 5/31/2006 10:09 DH Nickel, Total 9.07 0.295 mg/kg SW846 6010A 5/10/2006 14:07 DH Page 2 a Davis & Brown PO Box 15038 Quinby, SC 29506, (843) 665-6746 FAX: (843) 6294444 Certificate of, Analysis Client: CHERAW, TOWN OF South Carolina Certification Number:-21117 P.O.BOX 219 North Carolina Certification Number: 612 CHERAW, SC 29520 Client #: 168 Receipt Date:' 05-May-06 Contact: SHERRY TOLS'ON Report Date: 01-Jun-06 Sample Date: 04-May-06 SDG #: SDG-048280 Approved By: G , Van Ward Lab Director Reporting Parameter Result Limit Unit . Method Flag, Date Time Analyst Zinc, Total 64.3 0.295 mg/kg SW846 6010A 5/10/2006 14:07 DH Mercury, Total 0.150 6.053 mg/kg SW846 7470A 5/24/2006 14:18 DH Selenium, :Total <1.48 1.48 mg/kg SW846 7741A 5/16/2006 13:39 JR PCB BDL 1.6 mg/kg SW846 8080 S16 5/15/2006 9:42 JSW LSID-108156 5-4-06-001 Acid Digestion (Liquids) YES . EPA 2002 5/8/2006 1:00 DH Lead; Total <0.050 0.05 mg/L EPA200.7 5/10/2006 16:38 DH Arsenic, Total <0.005 0.005 mg/L SM 3113B 5/15/2006 14:29 JR Page 3 12065 Lebanon Rd. Mt. Juliet, TN 37122 ENVIRONMENTAL 1-800 767-5859 SCIENCE CORP. Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 -REPORT OF ANALYSIS Mr. Scott -Fields, May 15,2006 Davis & Brown P.O. Box 15038 Quinby, SC 29506 ' ESC Sample #.: L244348-02 Date Received May 69, 2006 Description Site ID Sample ID 108155 . Project # Collected By Collection Date :, 05/04/06 13:00 Parameter Dry Result Det. Limit Units Method Date Analyst Total Solids 44.9 % 25400- 05/13/.06 0834 MAS Polychlorinated Biphenyls PCB 1016 BDL 0.038 mg/kg 8082 05/15/06 0942 JSW PCB 1221 BDL,' 0.038 mg/kg 8082 05/15/06 0942 JSW PCB 1232 BDL 0.038 mg/kg 8082 05/15/06 0942 JSW PCB•1242 BDL 0.038 mg/kg 8082 05/15/06 0942 JSW- PCB 1248 BDL 0.038 mg/kg B082 05/15/06 0942 JSW PCB-1254 BDL 0.038 mg/kg 8082 05/15/06 0942 JSW PCB 1260 BDL 0.038 mg/kg 8082 05/15/06 0942 JSW Jeff Carr, ESC Representative Results listed are dry weight basis. BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) - Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923,. IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC-'84004, TN - 2006; VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ.- 81002, WI - 998093910 Note: This report shall not be reproduced, except in full, without the written approval from ESC. The reported analytical results relate only to the sample submitted Reported: 05/15/06 16:01 Printed- 05/15/06 16:01 Page 2 of 5 ' 0 ANIMAL WA91 LANAL Y J19KrFUK.1 rage 1 OIL A N I M A L' W A S T-E A N A L Y S I S R E P O R T Agricultural Service Laboratory LAB No. -50771 Clemson University TOLSON', SHERR ACCOUNT. COCHSFL PO BOX 219 DATE 05-08-2006 CHERAW SC 29520 CHERAWTOWNOF656@BELLSOUTH.NET SAMPLE N0. 5t0}]04� MANURE: OTHER STORAGE: UNCOVERED -= SULTS REPORTED ON AN•AS-SAMPLED BASIS -------------- lbs/ton Ammonium Nitrogen 0.02 % 0.40 Organic Nitrogen 0.96 . % 19.15 Nitrate Nitrogen 207.91 ppm 0.42 INCORPORATED AVAILABLE NITROGEN ESTIMATE 12.48 SURFACE AVAILABLE NITROGEN ESTIMATE 12.36 --------------------------------------------------------------- Phosphorus as P205 0.52 % 10.37 Potassium as K20 0.13 % 2.51 Calcium 12.60 % 251.93 Magnesium 0.23 % 4.53 Sulfur 0.12 % 2.36 Zinc 77.00 ppm 0.15 Copper 33.97 ppm 0.07 Manganese 72.47 ppm 0.14, Sodium 167.14 ppm 0.33 Moisture 54.70 % Calcium.Carbonate Equivalency 33.32 % 666.48 - - - - - - - - - - - - - - - - - - - - - 1- - - - - - - - - - - - - - - ----------------------------------------- INCORPORATED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be incorporated into the,soil within hours of application. Assumes some loss of ammonium7N during application and prior to incorporation. - SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be. .left on the surface of the soil with no incorporation by plowing or irrigation. Available nitrogen calculations are estimates and if nitrate-N was not re- quested the amount of available nitrogen may be slightly more than reported. Also, the actual amount may be more or less than the estimate depending on the composition of.the manure, soil type, and environmental conditions. All of the potash in the animal waste should be plant available in the first year of application. Although not all of the phosphorous is available in -the first year, its -availability shouldbe comparable to that in commercial fertilizers. The rate of animal waste to apply for crop,production is dependent on the nutrient content of the waste, method of•application and incorporation, soil test, crop to be grown, and previous manure applications. In most cases, the plant available nitrogen content of the waste is used to determine the rate of application. The Agricultural Service Laboratory is a public service of Clemson University, an affirmative action and equal opportunity educational institution. ** http://www.clemson.edu/agsrvlb ** http://www.clemson.edu/aglabresults/COCHSFLTOLSON,%2OSHERRO60508000000111tm • 5/9/2006 % moisture % solids lbs. solids/ton lbs. solids/500 tons 547. 45.3 906 453000 ppm lbs/ton % ppm lbs/ton . as -sampled as -sampled as=sam led , dry ton dry ton dry Ammonium Nitrogen 0.02 200 b 4: 0.04415 441.6011 0.883002 Organic'Nitrogen 0.9575 9575 rr 19 15 2.113687, 21136.87 42.27373 Nitrate Nitrogen 0.020791 `;20T91 041582 0.045896 .458.9625 -,0.917925 Incorporated Available Nitrogen Estimate 0.624 : 62401.377483 13774.83 27.54967 Surface Available Nitrogen Estimate 0:618 6180 < F ' 12:36 1.364238 13642.38 27.28477 Phosphorus as P205 0.5185 5185 10.37 1.144592 11445.92 -22.89183 Potassium as 1C20 A1255 1255 `" 2 51' 0.277042 ; 2770.419 5.540839 Calcium 12-.5965 125965 "; 25,1 s93 27.80684 278068.4 556.1369 Magnesium 0.2265 2265 A'53 ` 0.5 5000 10 Sulfur 0.'118. 1180 `' 2:36 0.260486 2604.857 5.209713 Zinc 0.007,7 77; 0.154 0.016998 169.9773 0.339956 Copper 0.003397 y 33 97 0.06794 0.0.07499 74.98896 0.149978. Manganese 0 007247, " . 72 0.14494 0.015998 159.9779 0.319956 Sodium 0.016714 -'`16714: .114 0.33428 0.036896 368.9625 0.737925 Calcium Carbonate Equivalency 33.324 333240 66648 73.56291 735629.1 1471.258 CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES BIOSOLIDS SAMPLE DATE:" 13, 2005'V Biosolids Maximum Maximum Maximum Maximum Metal Allowable Allowable Application Application Content, Metal App. Rate, Rate, Rate, METALS porn Content, ppm #/Acre/Yr. DT/Acre/Yr. WT/AcrefYr. Arsenic, Total 0.28 41.00 1.80 1584.78 3169.57 Cadmium, Total 0.51 39.00 1.70 839.63 1679.27 Chromium, Total 30.49 1200.00 134.00 1098.58 2197.17 Copper, Total 44.69 1500.00 67.00 374.19 749.59 Lead, Total 2.72 300.00 13.00 1196.59 2393.18 Mercury, Total 0:10 17.00 0.75 1808.04 3616.07 Molybdenum, Total 3.14 18.00 0.80 63.78 127.56 Nickel, Total 13.09 420.00 18.70 357.24 714.48 Selenium, Total 0.25 * " 36.00 4.50 4445.12 8890.24 Zinc, Total 82.84 1525.00 125.00 377.24 754.47 PCB BDL 1.60 * Actual metal content less than amount indicated. Biosolids Biosolids Maximum Maximum Nutrient Nutrient Crop/Soil Application Application Content,, Content, Requirement, .Rate, Rate, ppm % #/Acre'° DT/Acre/Yr. WT/Acrn1Yr. Ammonium Nitrogen 385.80 0.04 Organic Nitrogen 7826.97 0.78 Incorporated Available Nitrogen $680.94 0.57 120.00 5.28 10.56 Surface Available Nitrogen 6565.20 0.56 120.00 6.39 10.78 Phosphorus as P205 5608.60 0.56 80.00 3.57 7.13 Potassium as K20 781.25 0.08 50.00 16.00 32.00 Calcium, Total 139009.45 13.90 Calcium as Ca0 194613.23 19.46 Calcium as CaCO3 (CCE) 175583.53 17.56 2000.00 2.85 5.70 Magnesium, Total 2748.84 0.27 Manganese 101.27 0.01 Sulfur 1302.08 0.13 Percent Moisture 50.00 *° These are typical values and must be adjusted based upon specific site conditions DT is Dry Tons of Biosolids. WT is Wet Tons of Biosolids. CERTIFICATION: This biosolid product has been produced by the Town of Cheraw's Wastewater Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature and lime (calcium o)dde). The Town of Cheraw certifies that this biosolid complies with the Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has a metal and nutrient content as presented above. DIRECTIONS FOR USE This biosolid is intneded to be used as a soil amendment. The biosolid land application rate shall not exceed the most restrictive Maximum Application Rate as indicated in the table above. The application rate for nitrogen; phosphorus, potassium, and calcium is dependent upon the crop grown and site soil characteristics. The user should contact the Clemson Extension Service (843-623-2134) and/or the Soil Conservation Service (843-623-2187) for assistance in determining the proper application rate for each crop and site. In no case shall the land application rate exceed the agronomic rate for the crop grown. User should "also refer to the Clemson Extension Service Circular #476 titled "Lime and Fertilizer Recommendations." THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY. AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES. THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS BIOSOLID PRODUCT. Mr. Ricky D: Ingram, Public Utility Director P.O. Box 219; Cheraw, SC 29520 Telephone: 843-537-8440 FAX: 843-537-8442 QUANTITY RECEIVED: RECEIVED BY: -.. Davis - & Brown PO Box 15038 Quinby, SC 29506 (843) 665-6746 FAX: (843) 629-1444 Certificate of Analysis Client: CHERAW, TOWN OF South Carolina Certification Number: 21117 P.O.BOX 219 North Carolina Certification Number: 612 CHERAW, SC 29520 Client #: 168 Receipt Date: 14-Jul-06 Contact: SHERRY TOLSON Report Date: 03-Aug-06 Sample Date: 12-Jul-06 SDG #: SDG-049352 Parameter LSID-1'10454 Acid Digestion (Solids) Percent Solids Aluminum, Total Arsenic, Total Cadmium, Total Chromium, Total Copper, Total Lead, Total Molybdenum, Total Nickel, Total Zinc, Total Mercury, Total Selenium, Total PCB Approved By: Van Ward Lab Director Reporting Result Limit Unit Method Flag Date Time Analyst YES EPA 200.2 40.5 0.1 wt% SW846 3540 2990 75.1 mg/kg SW846 6010A 0.230 0.205 mg/kg SW846 6010A <0.410 0.41 mg/kg SW846 6010A 24.7 0.41 mg/kg SW846.6010A 36.2 0.41 mg/kg SW846 6010A 2.20 2.1 mg/kg SW846 6010A 2.54 1.5 mg/kg SW846 6010A 10.6 0.41 mg/kg SW846 6010A 67.1 0.41 mg/kg SW846 6010A 0.084 0.023 mg/kg SW846 7470A <0.205 0.205 mg/kg SW846 7741A BDL 1.5 mg/kg SW846 8080 7/18/2606 10:00 DH 7/20/2006 ' 17:30 JR 7/24/2006 17:49 DH 7/18/2006 14:28 JR 7/19/2006 9:17 DH 7/19/2006 9:17 DH 7/19/2006 9:17 DH 7/19/2006 15:46 DH 7/24/2006 17:54 DH 7/19/2006 9:17 DH . �7/19/2006 9:17 DH 7/24/2006 13:29 DH . 7/18/2006 20:06 JR S16 7/20/2006 21:56 TLW L9I13-110455 7-13-06-F Fluoride 1.08 0.2 mg/L SM 4500FC 7/24/2006 14:00 MLL LSID-110456 SOURCE H2O Page 2 J Lebanon R37 Mt. Juliet, TN 122 " ENVIRONMENTAL (615) 758-5858 1-800-767-58s9 -SCIENCE CORP. Fax (615) 7 e-se59 Tax I.D. 62-0814289 Est. 1970 . REPORT OF ANALYSIS Mr. Scott Fields July 24,2006 Davis & Brown P.O. Box 15038 Quinby, SC 29506 ESC Sample # L253316-01 Date Received July 19,: 2006 Description Site ID Sample ID 110454 Project .: #"_ Collected By Collection Date b7/13/0:6 00:00 Parameter Dry Result Det. Limit Units` Method Date Analyst Total: Solids 40.4 % 2540G 07/22/06 1214 LF Polychlorinated Biphenyls PCB 1016 BDL 0.21 mg/kg 8082 07/20/06 2156 TLW PCB 1221 BDL 0.2 mg/kg 8082 07/20/06 2156 TLW PCB 1232 BDL- 0.21 - mg/kg 8082 07/20/06 2156 TLW PCB 1242 BDL 0.21 .mg/kg 8082 07/20/06,2156 TLW PCB 1248 BDL 0.21 mg/kg 8082 07/20/06 2156 TLW PCB 1254 B6L 0.21 mg/kg 8082 07/20/06 2156 TLW PCB 1260 BDL 0.21 mg/kg 8082 07/20/06 2156 "TLW Results listed are dry weight basis. BDL- Below. Detection Limit Det,. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: ANIMAL WAN 1EANALYNINKEYUK1 Page Iot2 A N I M A L W A S T E A N A L Y S I S R E P O R T Agricultural Service Laboratory LAB No. 71013- Clemson University' TOL'SON, SHERRY ACCOUNT COCHSFL PO BOX 219 DATE 07-26-2006 CHERAW SC 29520 CHERAWTOWNOF656@BELLSOUTH.NET SAMPLE NO. 7'13`'6 'MANURE: OTHER STORAGE: UNCOVERED -----------------RESULTS REPORTED ON AN AS -SAMPLED BASIS ---------------------- lbs/ton Ammonium Nitrogen 0.04 % 0.80 Organic Nitrogen 0.81 % 16.23 Nitrate Nitrogen 438.07 ppm 0.88 INCORPORATED AVAILABLE NITROGEN ESTIMATE 11.78 SURFACE AVAILABLE NITROGEN ESTIMATE 11.54 -------•-------------------------------------------------------- Phosphorus as P205 0.58 % 11.63 Potassium as K20 0.08 % 1.62 Calcium 14.41 % 288.25 Magnesium 0:29 % 5.70 Sulfur 0.13 % 2.70 Zinc 81.91 ppm. 0.16 Copper 34.73 ppm 0.07 Manganese 106.80 ppm 0.21 Sodium 125.98 ppm 0.25 Moisture. 48:16 % Calcium Carbonate Equivalency 36.41 % 728.18 --------------------------------------------------------------------------'---- INCORPORATED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of organic-N, and 100% of nitrate-N (if determined). Assumes the manure,will be incorporated into the soil within hours of application. Assumes some loss of ammonium-N during application and prior to incorporation. SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be left on the surface of the soil with no incorporation by plowing or irrigation.' Available nitrogen calculations are estimates and if nitrate-N was not re- quested the amount of available nitrogen may slightly more than reported. Also, the actual amount may be more or less than the estimate depending on the composition of the manure, soil type, and environmental conditions. All of the potash in the animal waste should be plant available in the first year of application. Although not all of the phosphorous is available in the first year, its availability should be comparable to that,in commercial fertilizers. The rate of animal waste to apply for crop production is dependent on the nutrient content of the waste, method of application and incorporation, soil test, crop to be grown, and previous manure applications. In most cases, the plant available nitrogen content of the waste is used to determine ,the rate of application. The Agricultural Service Laboratory is a public service of Clemson University, an affirmative action and equal opportunity educational institution.- http://www.clemson.edu/agsrvlb http://www.clemson.edu/agsrvlb ** http://Www.clemson.edu/aglabresults/COCHSFLTOLSON%20SHERRY0607260000001.htm 7/27/06 % moisture % solids lbs. solidsiton lbs. solids1500 tons 4816 51.84 1036.8 518400 % ppm Ibstton ' % ppm ., : lbs/ton, as -sampled- as -sampled as-sam led dry ton dry ton - dry Ammonium Nitrogen 0.04 400 08 0.07716 771.6049 1.54321 Organic Nitrogen ' 0.8115 8115 18 23 ,1.565394: 15653.94 31.30787 Nitrate Nitrogen 0.043807 438 07 0.87614 0:084504 845.0424 1.'690085 Incorporated Available Nitrogen Estimate 0.589 5890 11 78 1136188 11361.88 22.72377 Surface Available Nitrogen Estimate 0.577 5770 t11 54: ,1;11304. 11130.4 2-2.2608 Phosphorus as P205 0.5815 5815 11'63; 1.121721 11217.21 22.43441 Potassium as K20 0:081 810 1'.fi2' 0.15625 1562.5 3.125 Calcium 14.4125 144125 288.25' 27.80189- 278018.9 556.0378 Magnesium 0:285 2850 5:7 0.549169 5497.685 10.99537 Sulfur 0.135 1350 ` g 27 0.260417 2604.167 5.208333 Zinc 0.008191 0.16382 0.015801 158.0054 0.316011 Copper 0/.003473 ', 34 73 0.06946 0.006699 66.9946 0.133989 Manganese 0.01068 j ,.,L ,106`8a 0.2136 0.020602 206.0185 0.412037 Sodium 0.012598 ° 1{2598 0 25196 0.024302' 243.017 0.486034 Calcium Carbonate E uivalenc 36.409 364090 " 7.28:-18 70.23341 702334.1 1404.668 CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES BIOSOLIDS SAMPLE DATE: %eptember 77.2006 Biosolids Maximum Maximum Maximum Maximum Metal Allowable Allowable. Application Application Content, Metal App. Rate, Rate, Rate, METALS pp m Content, ppm #/AcrelYr. DT/Acre/Yr. WT/Acre/Yr. Arsenic, Total 1.54 ' 41.00 1.80 291.43 582.86 Cadmium, Total 0.31' ' 39.00 1.70 1376.19 2752.38 Chromium, Total 23.24 1200.00 134.00 1441.77 2883.54 Copper, Total 58.82 1500.00 67.00 284.75 569.60 , Lead, Total 3.26 300.00 13.00 995.50 f 1990.99 Mercury, Total 0.06 17.00 0.75 2897.73 5795.45 Molybdenum, Total 2,60 18.00 0.80 76.84 153.67 Nickel, Total 27.35 420.00 18.70 170.91 341.83 Selenium, Total 1.54 36.00 4.50 728.57 1457.14 Zinc, Total 94.71 1525.00 125.00 329.97 659.94. PCB BDL 1.60 "Actual metal content less than amount indicated. Biosblids Biosolids Maximum Maximum Nutrient Nutrient Crop/Soil Application Application Content, Content, Requirement, Rate, Rate, aam % #/Acre" DT/Acre/Yr. WT/Acre/Yr. Ammonium Nitrogen 1863.77 0.19 Organic Nitrogen 15325.31 1.53 Incorporated Available Nitrogen 11453.74 1.15 120.00 2.62 5.24 Surface Available Nitrogen 10894.61 1.09 120.00 2.75 5.51 Phosphorus as P205 9623.86 0.96 80.00 2,08 4.16 Potassium as K20 1872.25 0.19 50.00 6.68 13.35 Calcium, Total 80167.74 8.02 Calcium as CaO 112234.84 11.22 Calcium as CaCO3 (CCE) 95967.47 9.60 2000.00 5.21 10.42 Magnesium, Total -1948.49 0.19 Manganese 203.32 0.02 Sulfur 1702.81 0.17 Percent Moisture 50.00 " These are typical values and must be adjusted based upon specific site conditions DT is Dry Tons of Biosolids. I WT is Wet Tons of Biosolids. CERTIFICATION: This biosolid product has been produced by the Town of Cheraw's Wastewater Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature and lime (calcium oxide). The Town of Cheraw certifies that this biosolid complies with the Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has a metal and nutrient content as presented above. DIRECTIONS FOR USE: This biosolid is intneded to be used as a soil amendment. The biosolld land application rate shall not exceed the most restrictive Maximum Application Rate as indicated in the table above. The application rate for nitrogen, phosphorus, potassium, and calcium is dependent upon the crop grown and site soil characteristics. The user should contact the Clemson Extension Service (843-623-2134) and/or the Soil Conservation Service (843-623-2187) for assistance in determining the proper application rate for each crop and site. In no case shall the land application rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension Service Circular #476 titled "Lime and Fertilizer Recommendations." THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY. AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES. THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS BIOSOLID PRODUCT. Mr. Ricky D. Ingram, Public Utility Director P.O. Box 219, Cheraw, SC 29520 Telephone: 843-537-8440 FAX: 843-537-8442 RECEIVED BY: Davis &'Brown PO Box 15038 Quinby, SC 29506 (843) 665-6746 FAX: (843) 629-1444 Certificate of Analysis Client: CHERAW, TOWN OF South Carolina Certification Number: 21117 P.O.BOX 219 North Carolina Certification Number: 612 CHERAW, SC 29520 Client #: 168 Receipt Date: 08-Sep-06 Contact: SHERRY TOLSON Report Date: 27-Sep-06 Sample Date: 06-S'ep-06 SDG #: SDG-050277 Approved By:��� Van Ward Lab Director Reporting Parameter Result 'Limit Unit Method Flag Date Time Analyst LSID-112411 1005-B Oil and Grease 57.2 5 mg/L EPA 413.1 9/13/2006 13:00 JR LSID-112412 1005-T Oil• & Grease, Hydrocarbon 6.0 5 mg/L SM 503E 9/13/2006 15:00 JR LSID-112413 1005-D Chemical Oxygen Demand 1900 100 J mg/L EPA 410.4 9/15/2006 9:30 DH LSID-112414 RIO'-``S"6LID 09-07-0' 00* Acid Digestion (Solids) YES EPA 200.2 9/12/2006 -10:00 DH Percent Moisture 66.0 0.1 wt% SW846 3540 9/8/2006 16:30 JR Aluminum, Total 4730 0.397 mg/kg SW846 6010A 9/22/2006 10:01 DH Arsenic, Total. <1.05 1.05 mg/kg SW846 6010A 9/13/2006 19:26 JR Cadmium, Total <0.210 0.21 mg/kg SW846 6010A 9113/2006 17:51 DH Chromium, Total 15.8 0.21 mg/kg SW846 6010A 9/14/2006 12:42 DH Copper, Total 40.0 0.21 mg/kg SW846 6010A 9/13/2006 17:51 DH Lead, Total 2.22 1.1 mg/kg SW846 6010A 9/15/20U6 9:23 DH Molybdenum, Total 1.77 0.794 mg/kg SW846 6010A 9/21/2006 9:48 'DH Nickel, Total 18.6 0.21 mg/kg SW846 6010A 9/13/2006 17:51 DH Zinc, Total 64.4 0.05 mg/kg SW846 6010A 9/13/2006 17:51 DH Page 1 Davis & Brown PO Box 15038 Quinby, SC 29506 (843) 665-6746 FAX: (843) 629-1444 Certificate of Analysis Client: CHERAW, TOWN OF South Carolina Certification Number: 21117 P.O.BOX 219North Carolina Certification Number: 612 CHERAW, SC 29520 Client #: 168 Receipt Date: 08-Sep-06 Contact: SHERRY TOLSON Report Date: 27-Sep-06 Sample Date: 07-Sep-06 SDG #: SDG-050277 Approved By: Van Ward Lab Director Reporting Parameter Result Limit Unit Method Flag Date Time Analyst Mercury, Total 0.044 0.019 mg/kg SW846 7470A- 9/19/2006 12:66 DH. Selenium, Total <1.05 1.05 mg/kg SW846 7741A 9/13/2006 16:59 JR PCB BDL 1.6 mg/kg SW846 8080 S16 9/1-4/2006 12:06 TLW LSID-112415 FINISHED WATER 9-7-06 Total'Organic Carbon 2.0 0.5 mg/L EPA 415.1 9/15/2006 9:30 SF LSID-112416 SOURCE WATER 9-7-06 Total Organic Carbon 4.5 0.5 mg/L EPA 415.1 9/15/2006 9:30 SF LSID-112417 .9-7-06-F Fluoride 0.90 0.2 mg/L SM 4500FC 9/13/2006 14:00 MLL- Page 2 12065 Lebanon Rd. Mt. 'Juliet, TN 7122 ENVIRONMENTAL-800-767-5859 Fax (615) 758-58,59 SCIENCE CORP . Tax B.D.62-0814289 Est. 1970 REPORT OF ANALYSIS Mr. 'Scott Fields September 19,2006 Davis &'Brown P.O' Box 15038 Quinby, SC 29506 ESC Sample # L260494-03 Date Received, September 12, 2006 Description Site ID Sample,ID 112414 Project # Collected By Collection Date 09/07/06 1j,:45 Parameter- Dry Result.Det. Limit Units Method: ;Date Analyst Total Solids 33.0' % 254OG 09/16/06 0850'.MAS Polychlorinated Biphenyls PCB�1016 BDL 0.26 mg/kg 8082 09/14/06 1206 TLW PCB 1221 BDL 0.26 mg/kg 8082 09/14/06 1206 TLW PCB 1232 BDL 0.26 mg/kg 8082 09/14/06 1206 TLW PCB 1242 BDL0.26 mg/kg 8082 09/14/06 1206 TLW PCB 1248 BDL 0.26 mg/kg 8082 09/14/0.6 1206 TLW', PCB 1254 BDL 0.26 mg/kg 8082 09/14/06 1206 TLW PCB'12'60 BDL 0.26 mg/kg 8082 09/14/06 1206 TLW Results listed are dry weight basis. BDL,- Below Detection Limit 'Det. Limit - Practical Quantitation Limit(PQL)• Laboratory Certification Numbers: AIHA - 100789, AL - 40660,'CA - I-2327," CT- PH-.0197, FL - E87487, GA - 923, IN - C-TN-01 KY'- 90010, KYUST-•0016, NC-'.ENV375,'DW21704, ND - R-1401- SC _ 84004, TN - 2006, VA'-.00109, WV - 233 A2 -0612, MN.- 047-999-395, NY - 11742, NJ - TN002, WI - 998093910.. Note: This report shall not be reproduced, except in full, without the written approval from ESC. The reported analytical results relate only to the sample submitted , Reported: 09/18/06 13:43 Revised: 09/19/06 07:55 Page 3 of 5, = A 114 1 lYl n, L YY 1-1 0 1 L 111 14 r-1 L i a 1 a 1C Z r V 1C 1 rage i of A N I M A L W A S T E A N A L Y S I S R`E P 0 R T Agricultural Service Laboratory LAB No. 91224 Clemson University TOLSON, SHERRY PO BOX 219 CHERAW.SC 29520 ACCOUNT COCHSFL DATE 10-02-2006 CHERAWTOWNOF656@BELLSOUTH.NET SAMPLE NO. &Oc7,0.65:Oj INURE: OTHER STORAGE: UNCOVERED --------- RESULTS REPORTED ON AN AS -SAMPLED BASIS ---------------------- lbs/ton Ammonium Nitrogen 0.11 % 2.20 Organic Nitrogen 0.90 % 18.09 Nitrate Nitrogen ----------------------------------------------- 282.75 ppm ---------------- •0.57 INCORPORATED AVAILABLE NITROGEN ESTIMATE 13:52 SURFACE AVAILABLE NITROGEN --------------------------------------------------------------- ESTIMATE 12.86 Phosphorus as P205 0.57 % 11.36 Potassium as K20 0.11 % 2.21 Calcium 4.73 % 94.63 Magnesium 0.12 % 2.30 Sulfur 0.10 % 2.01 Zinc 59.03 ppm 0.12 Copper 39.55 ppm 0.08 Manganese 119.83 ppm 0.24 Sodium 132.23 ppm 0.26 Moisture 70.49 % Calcium Carbonate Equivalency 11.33 % 226.56 ------------------------------------------------------------------------------ INCORPORATED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be incorporated into the soil within hours of application. Assumes some loss of ammonium-N during application and prior to�incorporation. SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be left on the surface of the soil with no incorporation by plowing or irrigation. Available nitrogen calculations are estimates and if nitrate-N was not re- quested the amount of available nitrogen may be slightly more than reported. Also, the actual amount may be more or less than the estimate depending on the composition of the manure, soil type, and environmental conditions. All of the potash in the animal waste should be plant available in the first year of application. Although not all of the phosphorous is available in the first year, its availability should be comparable to that in commercial fertilizers. The rate of animal waste to apply for crop production is dependent on the nutrient content of the waste, method of`application and incorporation, soil test, crop to be grown, and previous manure applications. In most cases, the plant available nitrogen content of the waste is used to determine the rate of application. The Agricultural Service Laboratory is a public service of Clemson University, an affirmative action and equal opportunity educational institution. ** http://www.clemson.edu/agsrvlb ** http://www.clemson.edu/aglabresults/COCHSFLTOLSON,%2OSBERRY0610020000006.htm 10/5/06 moisture % solids lbs. solidsiton lbs. solids/500 tons ::. . ',70:49 29"51 590.2 295100 ppm Ibs/ton % ppm. lbs/ton as-sam lets as -sampled as -sampled dry,ton d ton dry Ammonium Nitrogen 0.11 1100 .2:2 0.372755 3727.55 . 7.4551 Organic Nitrogen 0.9045 9045 1'8a09: 3.065063 30650:63 61.30125 Nitrate Nitrogen 0.028275 : 282 75' 0.5655 0.095815 958.1498 1.9163 Incorporated Available Nitrogen Estimate 0.676 6760 13:52 2290749 22907.49 45.81498 Surface Available Nitrogen. Estimate 0.643 6430 12 86 2.1789" 21789.22 43-57845 Phosphorus as P205_ 0.568 5680 11 36 1:924771 19247.71 38.49543 Potassium as K20 0.1105 1105 ' sF 2 2f 0.374449 3744.403 7.488987 Calcium 4.7315 47315 -, '04.63 16.03355 160335.5 320.671 Magnesium 0.115 t-, 11.50 2.3 0.389698.3896.984 7.793968 Sulfur 0.1005 1005 _` 2 01j 0.340563 3405.625 6.81125 Zinc 0.065903 59 R03 0.11806 0.020003 200.0339 0.400068 Copper 0.003955 r ; `39 55 " 0.0791 0.013402 134.0224 .0.268045 Manganese 0.011983 °' 119 83 0.23966 0.040607 406.0657 0.812131 Sodium 0.013223 ' 1.32 23 0 26446 0.044809 448.0854 0.896171 Calcium Carbonate E uivalen 11.328 . 115280 s 226:56 38.38699 383869.9. 767J397 CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES BIOSOLIDS SAMPLE DATE:'pc e-Mber-fi;,2006W' METALS Biosolids Metal Content, ppm Maximum Allowable Metal Content, ppm Maximum Maximum Allowable Application App. Rate, Rate, #/Acre/Yr. DT/AcreJYr. Maximum Application Rate, WT/AcrelYr. Arsenic, Total 1.25 ' 41.00 1.80 360.00' 720.00 Cadmium, Total 0.25 ` 39.00 1.70 1706.32 . 3412.64 Chromium; Total 20.74 1200.00 134.'00 1615.18 3230.36 Copper, Total 45.00 1500.00 67.00 372.22 744.44 Lead, Total 3.18 300.00 13'00 1023.32 2046.65 Mercury, Total 0.17 17.00 0.75 1112.64 2225.27 Molybdenum, Total 0.62 • .18.00 0.80 244.07 488.14 Nickel, Total . 18.52 420.00 18.70 252.45 504.90 Selenium, Total 1.25 ' 36.00 4.50 900.00 1800.00 Zinc, Total 84.35 1525.00 125.00 370.47 740.94 PCB BDL 1.60 ' Actual metal content less than amount indicated. - Biosolids Biosolids 1 Maximum Maximum Nutrient Nutrient Crop/Soil Application Application Content, Content, Requirement, Rate, Rate, ppm % #/Acre" DT/AcrelYr. WT/AcrafYr. Ammonium Nitrogen Organic Nitrogen Incorporated Available Nitrogen Su -dace Available Nitrogen Phosphorus as P205 Potassium as K20 Calcium, Total 423.91 0.04 7852.90 0.79 6008.90 0.60 120.00 5881.73 0.59 120.00 6411.62 0.64 80.00 1266.43 0.13 50.00 150365.62 15.04 4.99 9.99 5.10 10.20 3.12 6.24 9.87 19.74 Calcium as Cab 210511.87 21.05 Calcium as CaCO3 (CCE) 339683.13 33.97 2000.00 1.47 2.94 Magnesium, Total 2750.11 0.28 Manganese 185.46 0.02 Sulfur 1250.53 0.13 Percent Moisture 50.00 These are typical values and must be adjusted based upon specific site conditions DT is Dry Tons of Btosolids. WT is Wet Tons of Biosolids, CERTIFICATION: This biosolid product has been produced by the Town of Cheraw'iWastewater Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature and(lime (calcium oxide). The Town of Cheraw certifies that this biosolid complies with the Environmental Protection Agency regulations 40 CFR Part 503 for a "Class Al' product and has a metal and nutrient content as presented above. DIRECTIONS FOR USE: This biosolid is intneded to be used as a soil amendment.. The biosolid . land application rate shall not exceed the most restrictive Maximum Application Rate as indicated in the table above. The application rate for nitrogen, phosphorus, potassium, and calcium is dependent upon the crop grown and site soil characteristics. The user should contact the Clemson Extension Service (843-623-2134) and/or the Soil Conservation Service (843-623-2187) for assistance in determining the proper application rate for each crop and site. In no case shall the land application rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension Service Circular #476 titled "Lime and Fertilizer Recommendations." THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY. AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES. THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS BIOSOLID PRODUCT. Mr. Ricky D. Ingram, Public Utility Director P.O. Box 219; Cheraw, SC 29520 Telephone:' 843-537-8440 FAX: 843-537-8442 Davis & Brown PO Box 15038 Quinby, SC 29506 (843) 665-6746 FAX: (843) 629-1444 Certificate of Analysis Client: CHERAW, TOWN OF South Carolina Certification Number: 21117 P.O.BOX 219 CHERAW, SC 29520 Client #: 168 Receipt Date: 06-Nov-06 Contact: SHERRY TOLSON Report Date: 28-Nov-06 Sample Date: 06-Nov-06 SDG SDG-051175 #: Approved By: Van Ward Lab Director Reporting Parameter Result Limit Unit Method Flag, Date Time Analyst LSID-114251 $IOS"OLIDS'11 66=06=500 Acid Digestion (Solids) YES EPA 200.2 11/7/2006 10:00 DH Percent Moisture 46.0 0.1 wt% SW846 3540 11/8/2006 17:30 JR Aluminum, Total 6.32 0.445 mg/kg SW846 6010A 11/14/2006 10:57 DH Arsenic, Total <1.35 1.35 mg/kg SW846 6010A 11/14/2006 16:27 JR Cadmium, Total <0.269 0.269 mg/kg SW846 6010A 11/7/2006 15:56 DH Chromium, Total 22.4 0.269 xng/kg SW846 6010A 11/7/2006 15:56 DH Copper, Total 48.6 0.269 mg/kg SW846 6010A 11/7/2006' 15:56 DH Lead, Total 3.43 1.4 mg/kg SW846 6010A 1.1/8/2006 16:42 DH Molybdenum, Total <0.885 0.885 mg/kg SW846 6010A 11/27/2006 15:55_ DH Nickel, Total 20.0 0.269 mg/kg SW846 6010A 11/7/2006 15:56 DH- Zinc, Total 91.1 0.269 mg/kg SW846 6010A -11/7/2006 15:56 DH Mercury, Total 0.182 0.066 mg/kg SW846 7470A 11/20/2006 14:17 DH Selenium, Total <1.35 1.35 mg/kg SW846 7741A 11/15/2006 17:15 DH PCB BDL 1.6 ug/kg SW846 8080 S11 11/9/2006 18:09 KA LSID-114252 FINISHED WATER Chloride- IC 20.2 1 mg/L EPA 300.0 11/8/2006 11:02 SF LSID-114253 FINISHED WATER Page 1 AINIAlALWAalhANAL YJI�;.K_,YUKh Pagel oft A N I M A L W A S T E, A N A L Y S I S R E P O R T Agricultural Service.Laboratory LAB No. 111390 Clemson University TOLSON, SHERRY, ACCOUNT COCHSFL PO BOX 219 DATE 11-16-2006' CHERAW SC 29520 CHERAWTOWNOF656@BELLSOUTH.NET SAMPLE NO. 11060;6 0 URE: OTHER STORAGE: UNCOVERED ------------ RESULTS REPORTED ON AN AS -SAMPLED BASIS--- -------- ---=_------- lbs/ton Ammonium Nitrogen 0.04 % 0.80 Organic Nitrogen 0.74 % 14,82 Nitrate Nitrogen --------------------------------------------------------------- 566.21 ppm 1:13 INCORPORATED AVAILABLE NITROGEN ESTIMATE 11.34 SURFACE AVAILABLE NITROGEN ESTIMATE 11.10 Phosphorus as P205 0.61 % 12.10 Potassium as K26 0.12 % 2.39 Calcium 14.19 % 283.77 Magnesium 0.26 % 5.19 Sulfur 0.12 % 2.36 Zinc 64.64 ppm 0.13 Copper 34.44 ppm 0.07 Manganese 174.11 ppm 0.35 Sodium 203.84 ppm 0.41 Moisture 52.82 % Calcium Carbonate Equivalency 32.05 $ .641..05 ------------------------------------------------------------------------------ INCORPORATED PLANT AVAILABLE'NITROGEN ESTIMATE - 80% of ammonium-N, 60% of organic-N, and 100% of_nitrate-N (if determined). Assumes the manure will'be incorporated into the soil within hours of application. Assumes some loss of ammonium-N during application and prior to incorporation. SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 6'0% of organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be left.on the surface of the soil with no incorporation"by plowing or irrigation. Available nitrogen calculations are estimates and if nitrate-N was not re- quested the amount of'available nitrogen may be slightly more than reported. Also, the actual amount may be more or less than the estimate depending on the composition of the manure, soil type, and environmental conditions. All of the potash in the animal waste should be plant available in the first year of application. Although not all: of the phosphorous is available in the first year,.its availability should:be comparable to that in commercial fertilizers. The rate of animal waste to apply for crop production is dependent on the nutrient content of the waste, method of application and incorporation, soil test, crop to be grown, and previous manure applications. In most cases, -the plant available nitrogen'content of the waste is used to determine the rate of application. The Agricultural Service Laboratory is a public service of Clemson University, an affirmative action and equal opportunity educational institution. **-http://www.clemson.edu/agsrvlb ** hq://www.clemson.edu/aglabresults/COCHSFLTOLS ON,%20SHERRY0611160000001.h... 11 /17/06 % moisture % solids lbs. solids/ton lbs. solids/500 tons 47.18. "943.6 471800 % ppm Ibst.ton . % .;, ppm lbstton " as -sampled as -sampled as-sam" led ft ton 'dry tone dry Ammonium Nitrogen 0.04 400 , :'08 0.084782 847.8169 1.695634 Organic Nitrogen. . 0.741 7410 � - 14:82 1:570581 ` 15705:81 31.41162 Nitrate Nitrogen 0;056621 =566 21' 1.13242 0:120011 1200.106 2.400212 Incorporated Available Nitrogen Estimate 0.567 5670 ;. a 11 34. 1.20178 12017.8 24.03561 Surface Available Nitrogen Estimate 0.555 . 5550 . Ir>_, , ,1.1.1, 1.176346 11763:46 23.52692 Phosphorus as P205 0.605 ' 6050 , 12:1'_ 1.282323 12823.23 25.64646 Potassium as K20 0.1195 .. 1195 . , >y . , 2`39 0.253285 2532.853 5.065706 Calcium - 14.1885 141885 28347 '30.07312 3007312 601.4625 Magnesium 0.2595:. 2595 ;: 5:16 0.550021 5500.212 11.00042 Sulfur 0.118 1180 .... ,_, = . ,;2:36; 0.250106 2501.06 5.00212 Zinc 0.006464 :, 64 64, 0:.12928 0.013701 137'0072 .0.274014 Copper 0.003444 r. 3444 0.06888 0.0073 72.99703 .0.145994 _ Manganese 0.017411 t17411 034822 0.036903 '369.0335 0.738067 Sodium 0.020384 203 84 0.40768 0.043205 432.0475 0.864095 Calcium Carbonate E uivalenc 32.0525 320525 641 6 67.93663 679366.3 1358.733 Pasteurization vessel operates on a constant speed with an in/out time duration of 30°minutes. - MINIMUM 'MINIMUM DATE ' 2 HOUR pH 24 HOUR pH. TEMP IN TEMP OUT 01/09/06 12.38 12.26 °158 157 01/12/06 12.79 12V 152 162 01/13/06 12.16. 12.08 - -156 159" 01/23/06, 12.32 12.25 160 - 160 01 /24/06 . 12.33 12.17 158 157 01 /25/06 ' 12.24 ' 12.07 166 165 . 01 /26/06 12.36 12.19 - 157 :. '160 01/27/06 12.01 11.87- 158 159 01/30/06 12.19 11.97 158- 158 - 01 /31 /06 - 12.03 11.86 157 157 02/01/06 1236 . 12.18- 157 158 02/06106. 12.19 12.08 160 160 ' 02/07/06 12.16 12.62 169 158 02/08/06 .12.09. , 11.92 158 160. `02/09/06 12.17 12.10 159 160 , 02/ 10/06 12 -"47 12.31 160 167 02/13/06 12.07 .; " 12.01 157. 159 . 02/14/06 • . 12.32 12.10 160 164 , 02/15/06 12.29 12.08. 158 -150 -- 02/16/06 12.27:, 12.12 162 .162 02/17/06 1229 12.13 162 158, 02/20/06 12.27 12.02 ,'.160 148 02/21 %06 1 i 19 12.08 160 160 02/22/06 12.28 • ' 12.13 159 . .158 02/23/06 12.27 12.04 162 - 158 02/24/06, 12.33 12.13 , ' - ' 164 160 " 02/27/06 " 12.44 12:27 160 _ 162 02/28/06 12.38 12.10158 159 03/01 /06 12.27 12.07 158 163 . 03/02/06 - 12.22 12.03 -158 160 , 03/03/06 12.08 11.90 158 160' " 03/06/06 12.29 .. 12.0-1 163- 169 03/07/06 12.14 12.06 159 1.62" 03/06/06 12.26• 12.1.7 '161 164 03/09/06 12.32: -12.10 -160 159 03/10/06 12.33 12.25 158 -160.. 03/13/06 12.21 11.97 158 163 03/ 15/06 12.09 11.91 158 159 03/16/06 12.00 11.94 159' 164 03/17/06 12.21 " 12.03 164 160 03/20/06 12.02 ' 11.91 164 164 03/21/06 12.24 ' 11-88 169 162 03/22/06 12.08 11:90 160 158 - 03/23/06 12.22 12.08 . 165 ,-"169 03/24/06 12.36 " 12.15 161 '160 03/27/06 12.18 12.98 167 165, - 03/28/06 12.20 12.06 158 164. 03/29/06 12t.24. 11.97 162 . " 167 : 03/30/06 12.09 12.03 166 164 03/31 /06 112.14. 12.03 160 167 ' Pasteurization vessel operates on a.constant speed vAth an in/out time duration of 30 minutes. MINIMUM MINIMUM DATE .2 HOUR pH 24 HOUR pH TEMP IN TEMP OUT 04/03/06 12.16 12.08 169- 168 W04/06 12.20 12.01 166 160 04/05 06 12.16 . 12.03 .160 . 160 - 04/06/06 12.21 11.69 162 100 04/07/06 12.22 12.03 166' 165 ° 04/10/06 12.06 11.94 163" 166 04/11/06 - 12.02 11.89 160 164 04/12/06 12.08 .11.93 161 163 - 04/13/06 1.2.09 12.00 171 174 04/14/06 12.03 11.93 162 163 . 04/18/06 12.02 11.90 167 170 04/19/06 12.09 12.87 162 160 04/20/06 12:06 11.89 163 161 04/21 /06 12.11 11.96 162 163 04/24/06 12.04 12.59 162- 165 04/25/06 12.03 11.94 165 .166 04/26/06 12.07 11.93 161 - 160 04/27/06 12.24 11.91 158 159 04/28/06 12.09 1,1.93 164 164 05101 /06 1223 12.04 160 165 05102.106 12.22 11.98 159 160 05/03/06 12.10 11.77 - 165 163 05/05/06 12.21 11.99 165 160 05/08/06 .12.25 11.97 159 162 0 510 9/06 12.15 11.72 158 162 05/10/06 12.20 12.13 162 165 05/11 /06 12.31 12.10 163 161 05/12/06 12.26 12.03 158 159 65/15/06 . 12.16 12.03 158 163 05/16/06 12.18 12.05 162 158 05/17/06 12.17 12.04 160 158 05/18/06 12.24 . 11.93 162 159 - 05/19/06 12.21 11.99 160 158 . 05/22/06 12618 12.03 160 166 06/29/06 , • 12.15 11.97 163 158 06/30/06 12.17 12.00 162 160 138810 ..38811 38812 38813 38814 38817 38818 38810 38820 38821 38825 38826 38827 38828 38831 38832 38833 38834 38835 38838 38839 38840 38842 38845 38846 38847 38848 38849 38852 " . 38853 38854 38855 38856' 38859 38897 38898 'Pasteurization vessel operates on a constant speed with an in/out : time duration of 30 minutes. MINIMUM, MINIMUM DATE- 2 HOUR pH .24 HOUR pH TEMP:. IN TEMP OUT • 07/03/06 ' 12.23' - 11.97 162 158 07/05/06 12.14 11.09 158 159 07/06/06 12.26 12.08 161 160 : 07/07/06 12.17 12.03 162- .162 07/10/06 12.09 11.88 ; 163 •1" 07/11/06 ,... 12.19 11.98 167 168. 07/17/06 12.14 12:0.1 160 159 67/18/06 12.20 12,11 -163 163 07/19/06 ` 12.09 11.8T 102 137, 07/20/06 12.25 12.17 174 169. 07/31/06 1211, 12.03 160 -163 08/01 /06 12.08 11.92 165 166 08/02/06 12.14- 12.06: 1.64 1'62 " 08/03/06 12.13 ' 12.00 169 168 08/04/06 . , 12.10 12.03 •160 163 08/07/06 12:20 12.12 160 158 . 08/08/06 12.26 12.18 168 161 ; 08/09/06 1203 11.89 . 163 160 ' 08/10/06 12.12 1,1.97 160' 165 08/12/66" 12.17 11.86 166 165 08/14/061. 12.20 12.05 -162 167 08/15/06 ' 12.12 12.02 161 158 08/16/66 12.23 12.04 . 161 168 08/17/06 12.11 12.96 164 165, 08/18/06 12.04 11.90' 120 130 _ 08/21 /06 12.20 ` 12.06 160 165' 08/22/06 12.21 12.02 162 161 08/23/06 12. 22 12.03 161 166 08/24/06 ' 12.19 12.09 , 169 168 08/25/06 -12.20 - 11.94 159 _ '162 08/28/06 12.18 12.06 . 162'. 163 ` 08/29/06 12.24 12.06 163 169 08/30/06 12.18 .12: 06 162 164 08/31 /06 , 12.01 11.96 165 168 ' 09/05/06 12.21 11.97 158 159 09/06/06 12.08 11.86 159 158 - 09/07/06 - -12.10 12.01 160 145. 09/08/06 12:20 12.05 " 164 162 . 09/11/06 12.18 12.03 • 170 172 09/12/06 12.18 1106 162 166 09/13/06 .. 12.27 12.03 169 166 V10 �. q� 41�o�i �� J FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS A' l Medium Double Strength 10` dilution / 10 ml sample - Single Strength 10-'- dilution / 1.0 ml sample Single Strength 10'2 dilution / 1.0 nil sample Single Strength., 10-2dilution / 0.1 ml sample Date/Time Test Set -Up. A-_.30_.J.)!Datel Time Test Read: Time Placed in Incubator: �; �d ,o, �r, , Incubator Temp: % Time Transferred to Water Bath: Water Bath Temp: T Operator /D-rMedia Lot : _'�lc l 736 Solids 7/D Sample # INN Fecal Coliform = 10 x 1VIPN-Index / 100 ml .. _ per Guam Total Solids . Largest Volume x % Dry Solids NOTE: + indicates positive results ; - indicates negative results FORMULA: Where: r CALCULATION'FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE % Total Solids = (A - B) x 100 C-B A = Weight of dried residue + dish (mg) B = Weight of empty dish (mg) C = Weight.of wet sample + dish (mg) Sample # : f --/D -D - 340 Weight of dried residue + dish: Duplicate weight of dried residue + dish : Weight of empty dish Weight of wet sample + dish : % Total Solids = 02 3, 7 Q Q x l Q D � 1 ly q. 71 ;=7 q-a e ? /%0 FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS A-1 Medium Double Strength 10-' dilution / 10 in1 sample Single Strength 10-' dilution / 1.0 ml sample ............. � Single Strength 10 ^ dilution /.1.0 ml sample Single Strength 10-2 dilution / 0.1 ml sample Date/Time Test Set -Up: -A r , ;QQ wh , Date" Time Test Read: , 36 Time Placed in Incubator: .30 Incubator Temp: ,3 S. PC - Time Transferred to Water Bath: Q Water Bath Temp:'. G Operator Media Lot #*. Y S� % q 3 6- %Solids �. Sample # : 2- 9 D -D 6 3 66 MPN Fecal Coliform = 10: x 1v1PN Index / 100 ml per Gram Total Solids Largest Volume x % Dry Solids _ NOTE: + indicates positive results -: indicates negative results FORMULA: Where: CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE % Total Solids (A-B)x 100 C-B A = Weight of dried residue + dish (mg) B = Weight of empty dish (mg) C = Weight of wet sample + dish (mg) .gym. � / // Weight of dried residue + dish: Duplicate weight of dried residue:+ dish Weight of empty dish Weight of wet sample + dish /45, 7,3 Total Solids = �'3, �' rl 67. Z7Z- x M ------------ -33.Yle4—/7)ar /3 L, 3j-- 3a.o917 FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS A-1 Medium Double Strength 10-' dilution / 10 ml sample Single Strength 10_2 dilution / 1.0 ml sample Single Strength 10" dilution / 1.0 ml sample Single Strength 10' dilution / 0.1 ml sample - �' ;3D Date/ Time Test Read: Date/Time Test Set -Up: A. Time Placed in Incubator: .3 ; Qp, �+�: Incubator Tem p': Time Transferred to Water Ba (p•�Qp.rv.. Water Bath Temp: '�; C Operator Media Lot % Solids �' �. /0 Sample.# r MPN Fecal Coliform = 10 x MPN Index / 100 ml = Q per Gram Total Solids Largest Volume x % Dry, Solids NOTE: + indicates positive results ; - indicates negative results CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE HIM:?Tlil� % Total Solids (A-B)x100 C-B A = Weight of dried residue + dish (mg) B = Weight of empty dish (mg) C = Weight of wet sample + dish (mg) Sampie # :.39-t16 — `j O Weight of dried residue + dish: Duplicate weight of dried residue .+ dish Weight of empty dish Weight of wet sample + dish % Total Solids = T 1 7 1666. .R. ��o6 • �f13 aa, �300 TV 0 FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS A-1 Medium Double Strength Single Strength; 10-' dilution / 10 ml sample 10-.1 dilution / 1.0 ml sample Single Strength Single Strength 10-2 dilution 1.0 ml sample 10-1 dilution / 0.1 nil sample Date/Time Test Set-U`Ly - - ;36 ,.Date! Time Test Read: Time Placed in Incubator: ° 3 ' ®d g. Ih, Incubator Temp, 34 � C. Time Transferred to Water Bath: _ ; a0 sr , Water Bath Temp: 7 �— Operator A&I ,aMedia Lot g . S�o % Solids F-j . �a �6 Sample # MPN Fecal Coliform = 10 x MFN index / 100 ml = per Grant Total Solids Largest Volume x-% Dry Solids NOTE: + indicates positive results ; indicates negative results FORMULA: 1" - - CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE % Total Solids (A-B)x100 C-B A = Weight of dried residue + dish (mg) B = Weight of empty dish (mg) C = Weight of wet sample + dish (mg) Sample_# Weight of dried residue + dish: $Q q S Duplicate weight of dried residue+ dish: Weight of empty dish a, Q � I Weight of wet sample + dish Total Solids ='3, 6 P6 a64 3-:3—= 43.G%a FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS A-1 Medium Double Strength 10-' dilution / 10 ml sample Single Strength 10 dilution 1/.1.0 rn! sample Single Strength 10-' dilution / 1.0 rnl sample Single Strength 10-' dilution / 0.1 ml sample Dat:.e/Time Test Set -Up: 6--0 4 4:34404te' Time Test Read: Time Placed in Incubator: ��; D D A. r� • Incubator Temp: Tine Transferred to Water Bath: ; dQ ,�_ Water.Bath Temp: G Operator Media Lot # . 661173 O Solids-3 . Sample # WT'NT Fecal Coliform = 10 x lv N, Index / 100 ml = per Gram Total Solids Largest Volume x % Dry Solids V0 TE: + indicates positive results ; - indicates negative results FORMULA: Where: CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE % Total Solids = (A - B)x 100 C-B A = Weight of dried residue + dish (mg) B = Weight of empty dish (mg) C ; Weight of wet sample + dish (mg) Sample # : s5 - / -- Q6 — ,-d Q Weight of dried residue + dish: Duplicate weight of dried residue .+ dish: Weight of empty dish Weight of wet sample + dish Total Solids I,,66 - �.dS � X aaa9.�s _ 415�a FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS A-1 Medium Double Strength 10"1 dilution / 10 ml sample Single Strength 10 = dilution / 1.0 m1 sample Single Strength 10-1 dilution / 1.0 ml s Single Strength 10-1 dilution / 0.1 ml sample Dat:e!Time Test Set -Up: - : /d or Date! Time Test Read: Tune Placed in Incubator: : 3 , n., Incubator Te ' mp: Tune Transferred to Water Bath: Water Bath Temp: Dperator Media Lot #,SAP 73d Yo SolidsSample # D NDN Fecal Coliform = 10 x MPN-Index./ 100 nil = Q per Gram Total Solids Largest Volume x % Dry Solids 90-M: + indicates positive results z -indicates negative results FORMULA: Where: CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE % Total Solids = (A - B) x 100 C'B A = Weight of dried residue + dish (mg) B = Weight of empty dish (mg) C = Weight of wet sample + dish (mg) Sample#:�p—f Weight of dried residue + dish: Duplicate weight of dried. residue .+ dish: Weight of empty dish Weight of wet sample +dish : % Total Solids r2 4, 4 a 7v 4. 4Z A a. 0.2 -0 P—. 4 4 d.��3 FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS A-1 Medium \ Single Strength Single Strength 10'dilution / 1.0 ml sample 10-' dilution / 0'.1 ml sample Date Time Test Set -Up: I' 3"�� ��: QS Date! Time Test — • .fir,, F.ead: Time Placed in Incubator: d oZ J Incubator Temp: Time Transferred to Water Bath: 446. r Water'Bath Temp: Operator Media Lot:: % .Solids �" / . �0 Sample # JI MPN Fecal Coliform = `10 x WN Index / 100 fnl = per Ceram Total Solids Largest Volume x % D.ry Solids NOTE:' + indicates positive results; indicates negative resoles �• . Where: CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE % Total Solids = (A - B) x 100 C-B A = Weight of dried residue + dish (mg) B = Weight of empty dish (mg) C = Weight of wet sample + dish (mg) Sample # :. 7— 13 0lv Weight of dried residue + dish: Duplicate weight of dried residue .+ dish: Weight of empty dish Weight of wet sample + dish : % Total Solids = 9, /v 33. oo?( a. os� qs 073 3 3, LLA 6a.6y 7 � I FECAL COLIFORM-FOR MUNICIPAL BIOSOLIDS A-1 Medium Double Strength 10"' dilution / 10 ml sample Single Strength 1 0•'-, dilution / 1.0 ml sample Single Strength 10" dilution i 1.0 ml sample �o Single Strength 10-' dilution / 0.1 ml sample Date, Time Test Set -Up: - -Q '3Q ^ date/ Time Test Read: b Time Placed in Incubator: �; _�Q �o, A,. , Incubator Temp:. Time Transferred to Water Bath: ° ODD,,r, ; -Water Bath Temp: ��. S , C Operator Media Lot % o Solids !'p�. i sd Sample MPN Fecal Coliform = l0 x IvTN Index./ 100 ml per Cram Total Solids Largest Volume x % Dry Solids NOTE:. + indicates positive results ; - indicates negative results MM Where: CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE % Total Solids = (A - B) x 100 C-B A = Weight of dried residue + dish (mg) B = Weight of empty dish (mg) C = Weight of wet sample + dish (mg) Sample#: Weight of dried residue + dish: Duplicate weight of dried residue .+ dish: Weight of empty dish Weight of wet sample + dish : % Total Solids a3.3 � JO �3.3/18 S1.. S"9�,3 3.3118-�..o6�fS� S/. 59.s3 a1a4.73 �9.530$ FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS A-1 Medium Double Strength 10-' dilution / 10 ml sample Single Strength 10'- dilution / 1.0 ml sample Single Strength 10-1* dilution / 1.0 ml sample Single Strength 10-' dilution / 0.1 ml sample Date/Time Test Set-LTp: ''7- 66 o2'6d , vD'ate! Time Test Read: �- 8'� Q � o?.'3D �,, % Time PIaced in Incubator: _ dZ 364,A r., > Incubator. Temp:�'- Tune Transferred to Water Bath: Water Bath Temp:. . Sc Operator Media Lot# % Solids TJ • 7" /d Sample # MPN Fecal Coliform = 1.0 x MPN Index / 100 mI = per Gram Total Solids Largest Volume x .% Dry Solids NOTE: + indicates positive results; - indicates negative results CALCULATION FOR TOTAL SOLIDS IN BIOSOLID9 SAMPLE 'FORMULA: % Total Solids = '(A' B ) x 100 -C - B Where: A = Weight of dried residue + dish (mg) B Weight of empty dish (mg) C = Weight of wet sample + dish (mg) Sample # : Weight of dried residue +dish: Duplicate weight of dried residue •+ dish: Weight of empty. dish Weight of wet sample + dish 3► %Q .QQ - Total Solids 01�-� X 0 76 X �a6 3q /Dao—/d7D "FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS A-1 Medium Double Strength 10"' dilution / 10 ml sample Single Strength 10 dilution / 1.0 ml sample Single Strength 10-" dilution / 1.0 ml sample Single Strength 10-1 dilution / 0.1 nil sample Date!Time Test Set -Up: /Q - -Q� D •%,,,Date/Time Test Read: Time Placed in Incubator: Incubator Temp: : 3. Q Time Transferred to Water Bath: i►•+ : Water Bath Temp: T Li 1i Operator Media Lot 9 %'Solids17 Sample # a'L - , S" WN Fecal Coliform .. = 10 x MPN Index / 100 ml. = 0 per Gram Total Solids Largest Volunie x %,Dry Solids NOTE: +indicates positive results ; - indicates negative results . Where: CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE % Total Solids = (A - B)x 100 C-B A = Weight of dried residue + dish (mg) B = Weight of empty dish (mg) C = Weight of wet sample + dish (mg) Sample # :1 , %4 ` D t/O .�® Weight of dried residue + dish: Duplicate weight of dried residue -+ dish: Weight of empty dish Weight of wet sample + dish ��. 1 /C /ol. V 4 . 2 L �� Y 36. 6)R % Total Solids //I//,- x AM 36, I L�4,3. U, 33. % 6 6 FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS A-1 Medium -Double Strength 10' dilution / 10 ml sample Single Strength 10' dilution ! 1.0 ml sample Single Strength I07",dilution / 1.0 ml sample - Single Strength 10-2 dilution 7 0.1 ml sample Date/Time Test Set -Up: P Ob Date/ Time Test Read: Time PIaced in Incubator: - -3 Op.. , Incubator Temp: 3 5; L0 C_ Time Transferred to Water Bath: Water Bath Temp: Operator /�J� Media Lot # �� �f �j % 4 97 % Solids 3 8.6 /0 Sample # a " �o -' EQ a WN Fecal Coliform = 10 x MPi\? Index i' 100 ml = per Gram Total Solids Largest Volume x % Dry Solids NOTE: + indicates positive results ; - indicates negative results i FORMULA: Where: CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE % Total Solids = (A - B) x 100 C-B A = Weight of dried residue + dish (mg) B = Weight of empty dish (mg) C = Weight of wet sample + dish (mg) Weight of dried residue .+ dish: Duplicate weight of dried residue -+ dish: Weight of empty dish Weight of wet sample + dish : /a /, C2 7 % Total Solids = 3 ! , a Z 76 �3 �0��0 FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS A-1 Medium Double Strength 10' dilution / 10 ml sample Single Strength l 0-' dilution / 1.0 nit sample Single Strength 10-1' dilution / 1.0 ml sample Single Strength 10-' dilution / 0.1 ml sample Date/Time Test Set -Up: -- -� a,'Q�D,r�te!-Time Test Read: Time Placed in Incubator: - 30 Incubator Temp:°c- Time Transferred to Water Bath: `I/� ° D .n� Water Bath Temp: Tr Operator Media Lot # 44)31 % Solids g� Sample MPN Fecal Coliform = 10 x MPN Index / 100 ml = per Grans Total Solids Largest Volume x % Dry Solids NOTE: + indicates positive results ; . - ihdicates negative results FORMULA: Where: CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE % Total Solids (A-B)xl00 C-B A = Weight of dried residue + dish (mg) B = Weight of empty dish (mg) - C = Weight of wet sample + dish (mg) Sample # : A_ J* -d (o - pD Weight of dried residue + dish: o7 Ll. a 3 /D Duplicate weight of dried residue + dish Weight of empty dish : C/ Weight of wet sample + dish % Total Solids3Y 3 RECEIVED IDEN R1D\NQ AOUIFFR'PRQTFr FEB 21 'tub/ F WATF • OHO !QpG r Michael F. Easley, Governor y William G. Ross Jr., Secretary r✓ North Carolina Department of Environment and Natural Resources =1 Alan W. Klimek, P.E.,.Director —_ Division-of_W.ater Quality - _ August 26, 2005 - Mr. Ricky Ingram, Public Utility Director _Post Office Box 219 Cheraw, South Carolina 29520 --- - Subject: Permit No. WQ0014248 _ Town of Cheraw, South Carolina _- Town of Cheraw Residuals Distribution Program Distribution of Class A Wastewater Residuals - Central Office — Out of State Operation Dear Mr. Ingram: - In accordance with your application received on July 30, 2003 and additional information received on February 25, 2004, we are forwarding herewith Permit No. WQ0014248, dated August 26, ,2005, to the Town of Cheraw for the continued operation of a wastewater residuals facility for the distribution of Class A residuals. _ = This permit shall be effective from the date of issuance until July 31, 2010, shall void Permit No. WQ0014248 issued August 15,,199,7; andshall be subject to the conditions and limitations as specified therein. Please pay particular attention to the monitoring and reporting requirements contained in this permit. Failure to establish an adequate system for collecting and maintaining the required operational - information will.result in future compliance problems. _ -- If any parts, requirements, or limitations contained in this permit are unacceptable, you have the _ - right to request an adjudicatory hearing upon written request within thirty (30) days following receipt of _ this permit. This request must be in the form of a written petition; conforming to Chapter, 150B of North Carolina General Statutes, and filed with the'Office of Administrative Hearings, 6714 Mail Service Center, Raleigh, NC 27699-6714. Unless such demands are made this permit shall be final and binding. If you need additional information concerning this matter, ple e contact Duane Leith at (919) 715-6186 or email duane.leith@ncmail.net. Sincer y. V6Alan W. Klimek, P.E. cc: lNCDWQ Regional Offices,_ __ater_QuaTity Secti i Technical Assistance and Certification Unit Water Quality Central Files NDPU Files - - NDPU Residuals Program Coordinator_—_ Aquifer Protection Section 1636 Mail Service Center Raleigh Internet: http://h2o.enr.state.nc.us 2728 Capital Boulevard Raleigh An Equal Opportunity/Affirmative Action Employer— 50% Recycled/10% Pj ,C Ciha C) o 1 Tina lly . 0 NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES RALEIGH PERMIT FOR THE DISTRIBUTION OF CLASS A RESIDUALS In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, and other applicable Laws, Rules, and Regulations _ PERMISSION IS HEREBY GRANTED TO Town of Cheraw Chesterfield County, South Carolina FOR THE continued operation of a wastewater residuals facility for the distribution of Class A residuals consisting of -- the distribution of 1,800 dry tons per year of residuals from the sources listed in Condition 112, with no discharge of wastes to the surface waters, pursuant to the application received on July 30, 2003 and in conformity with the project plan, specifications, and other supporting data subsequently filed and approved by the Department of Environment and Natural Resources and considered a part of this permit. _ This permit shall be effective from the date of issuance until July 26, 2010, shall -void Permit No. . WQ0014248 issued August 15, 1997, and shall be subject to the following specified conditions and limitations: L. PERFORMANCE STANDARDS = _ 1. The distribution -of Class A residuals program shall be effectively maintained and operated as a non -discharge system to prevent the discharge of any wastes -resulting from the operation of this program. 2. This permit shall become voidable in the event of^failure of the residuals program to adequately protect the assigned water quality standards of the surface waters and groundwaters. 3. The issuance of this permit shall not relieve the Permittee of the responsibility for damages to - surface or groundwaters resulting from the operation of this program. 4. In the event that the residuals.program is-rio"t operated satisfactorily, including the creation of nuisance conditions, the Permittee shall take any immediate corrective actions as may be required by the Division of Waterquality,_(Division). 1 EIS 5. Diversion or. bypassing of the untreated residuals or leachate from the residual treatment fa"litiesis prohibited. 6. All leachate must be reused as a wetting agent for the processing of residuals or routed to the head of the treatment plant. 7. When wastewater residuals are sold or given away, one of the Class A pathogen requirements in 40 CFR Part 503.32(a) and one of vector attraction reduction requirements in 40 CFR Part 503.33 must be met. Additionally, an evaluation must be performed which demonstrates the residuals ability to comply with. this requirement. Upon request, a copy of this evaluation must be submitted including all test results and calculations. OPERATION AND MAINTENANCE REQUIREMENTS 1. The residuals treatment facilities shall be properly maintained and operated at all times. 2. No residuals other than.the following are hereby approved for distribution in accordance with this permit: Permit Volume Source County Number (Dry Tons/Year) Town of Cheraw Chesterfield, SC SCO020249 1,800 3. All residuals shall be adequately stored to prevent leachate runoff until treated., The finished product may be placed on a concrete pad, placed under shelter or covered until such time as it is distributed to the buyer. If an alternate storage site is to be used, approval must be obtained from the Division. 4. No other residuals other than those specified under Condition H 2 above may be distributed. The Permittee shall request and obtain a permit, amendment from the Division for each additional residual source prior to acceptance of that residual. 5. For a Class A residual to be sold or given'away in bags or other container for application to the land, the following must be satisfied: The Ceiling Concentrations (Dry Weight Basis) and the Pollutant Monthly Average Concentrations (Dry Weight Basis) must be maintained: Ceiling Monthly Average Concentrations Concentrations Parameters mg/kg mg/kg Arsenic 75 41 Cadmium 85 39 Copper 4,300 1,500 Lead 840 300 Mercury 57 17 Molybdenum 75 ---- Nickel 420 420 Selenium 100 100 Zinc 7,500 2,800 2 6. Upon classification of the facility by the Water Pollution Control System Operators Certification Commission (WPCSOCC), the Permittee shall employ a certified residuals operator to be in responsible charge (ORC) of the residuals program. The operator must hold a certificate of the type classification assigned to the residuals program by the WPCSOCC. The Permittee must also employ a certified back-up operator of the appropriate type to comply with the conditions of 15A NCAC 8G .0202. 7. Adequate provisions shall be taken to prevent wind erosion and surface runoff from conveying pollutants from -the residuals treatment area onto the adjacent.property or into any surface waters. A label shall be affixed to the bag or other container in which residuals that are sold or given away for application to the land, or an information sheet shall be provided to the person who receives the residuals sold or given away in an other container for application to the,land. The label or information sheet shall contain the following information: a. The name and address of the person who prepared the residuals that is sold or given away in a bag or other container for application to the land. b. A statement that application of the residuals to the land is prohibited except in accordance with the instructions on the label or information sheet. c. A statement which identifies that this material shall be prevented from entering any public or private water supply source (including wells) and any stream, lake, or river. d. Residuals shall not be applied to any site that is flooded, frozen or snow-covered. e Adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored residuals into any surface waters. III. MONITORING AND REPORTING REQUIREMENTS 1. Any monitoring (including groundwater, surface water, residuals, soil, or plant tissue analyses) deemed necessary by the Division to insure protection of the environment will be established and an acceptable sampling and reporting schedule shall be followed. 2. Proper records shall be maintained by the Permittee tracking all residual activities. These records shall include, but are not necessarily limited to the following information: a. source, volume and analysis of each residuals b. name of residuals' recipient, volume received, and intended use 3 3. A residual analysis shall be conducted annually from the date of permit issuance by the Permittee. The results of all analysis shall be maintained on file by the Permittee for a minimum of five years. The residuals analysis shall include the following parameters: Arsenic Cadmium. Copper Lead Mercury Molybdenum Nickel Selenium Zinc Aluminum Ammonia -Nitrogen Calcium , Magnesium Nitrate -Nitrite Nitrogen % Total Solids_ pH Phosphorus Potassium Sodium TKN Plant Available Nitrogen (by calculation) 4. The residuals generated by each residuals source -generating facility listed in condition 11.2. above shall be analyzed to demonstrate that they are non -hazardous under the Resource Conservation and Recovery Act (RCRA). A corrosivity, ignitability, and reactivity analysis as: well as a Toxicity Characteristics Leaching Procedure (TCLP) analysis shall be conducted on the residuals generated by each residual's source -generating facility listed in condition 11.2. above. The analyses shall be perfonned annually, and the results shall be maintained on file by. the Permittee for a minimum of five years. If the residuals generated by a. particular residuals source -generating facility are land applied at a frequency less than annually, the Analyses shall be required for each residuals land application event. The TCLP analysis shall 'include the following parameters (please note the regulatory level in mg/L in parentheses): Arsenic (5.0) Barium (100.0) Benzene (0.5) Cadmium (1.0) Carbon tetrachloride (0.5) Chlordane (0.03) Chlorobenzene (100.0) Chloroform (6.0) Chromium (5.0) o-Cresol (200.0) m-Cresol (200.0) p-Cresol (200.0) Cresol (200.0) 2;4-D (10.0) 1,4-Dichlorobenzene (7.5) 1,2-Dichloroethane (0.5) 1;1-Dichloroethylene (0.7) 2,4-Dinitrotoluene (0.13) Endrin (0:02) Heptachlor (and its hydroxide) (0.008) , Hexachlorobenzene ,(0.13) Hexachloro-1,3-butadiene (0.5) Hexachloroethane (3.0) Lead (5.0) Lindane (0.4) Mercury (0.2) Methoxychlor (10.0) Methyl ethyl ketone (200.0) Nitrobenzene (2.0) Pentachlorophenol (100.0) Pyridine (5.0) Selenium (1.0) Silver (5.0) Tetrachloroethylene (0.7) Toxaphene (0.5) Trichloroethylene (0.5) 2,4,5-Trichlorophenol (400.0) 2,4,6-Trichlorophenol (2.0) 2,4,5-TP (Silvex) (1.0) Vinyl chloride (0.2) After the residuals have been monitored annually for two years, the Permittee may submit a request to the Division for a permit modification to reduce the frequency of the TCLP analysis. In no case, however, shall the frequency of TCLP monitoring be ,less than once per permit cycle when residuals are sold or given away. 4 5. All residuals included in this permit must be monitored annually, from the date of permit issuance, for compliance with condition I.7. of this permit. Data to verify stabilization of the residuals must be maintained by the Pennittee. The required data is specific to the stabilization process utilized, but should be sufficient to clearly demonstrate compliance with the Class A pathogen requirements in 40 CFR Part 503.32(a) and the vector attraction reduction requirements in 40 CFR Part 503.33. In addition, the EPA certification statements concerning compliance with pathogen requirements, vector attraction reduction requirements and management practices must be completed annually by the proper authority or authorities if more than one is involved, either the person who generates the residuals or the person who prepares the residuals to be sold or given away. 6. Three copies of all required monitoring and reporting requirements as specified in conditions III 1, III 2, 111 3, I1I 4, and 1115 shall be submitted annually on or before March 1 of the following year to the following address. Division of Water Quality Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 7. Noncompliance Notification: The Permittee shall report by telephone to the appropriate DWQ Regional Office as soon as possible, but in no case more than 24 hours or on the next working day following the occurrence or first knowledge of the occurrence of any of the following: a. Any occurrence with the distribution program which results in the land application of significant amounts of wastes which are abnormal in quantity or characteristic. b. Any failure of the distribution program resulting in a release of material to receiving waters. c. Any time that self -monitoring information indicates that the facility has gone out of 'compliance with the conditions and limitations of this permit or the parameters on which the system was designed. d. Any process unit failure, due to known or unknown reasons, that render the facility incapable of adequate residual treatment. e. Any spillage or discharge from a vehicle or piping system during transportation of residuals. Persons reporting- such occurrences by telephone shall also file a written report in letter form within five (5) days following first knowledge of the occurrence. This report must outline the actions taken or proposed to be taken to ensure that the problem does not recur. IV. GROUNDWATER REQUIREMENTS Any groundwater quality monitoring, as deemed necessary by the'Division, shall be provided. 5 V. INSPECTIONS L . The Pern- ittee or his designee shall inspect the residuals storage, transport, and treatment facilities to prevent malfunctions and deterioration, operator errors and discharges which may cause or lead to the release of wastes to the environment, a threat to human health, or a nuisance. The Permittee shall maintain an inspection log or summary including at least the date and time of inspection, observations made, and any maintenance, repairs, or corrective actions taken by the Permittee. This log of inspections shall be maintained by the Permittee for a period of five years from the date of,the inspection and shall be. made available to the Division or other permitting authority, upon request. 2. Any duly authorized officer, employee, or -representative of the Division may, upon presentation of credentials, enter and inspect any property, premises or place on or related to the treatment site or facility at any reasonable time for the purpose of determining compliance with this permit; may inspect or copy any. records that must be kept under- the terms and conditions of this permit; and may obtain samples of groundwater, surface water, or leachate. VI. GENERAL CONDITIONS This permit shall become, voidable unless. the distribution activities are carried out in accordance with the conditions of this permit, the supporting materials, and in the manner approved by this Division. . 2. This permit is effective only with respect to the nature and volume of residuals described in the application and other supporting data. 3. This permit is not automatically transferable, In the event that there is a desire for the facilities to change ownership or a name change of the Permittee, a formal permit request must be submitted to the Division accompanied by an application fee, documentation from the parties involved, and other supporting materials as may be appropriate. The approval of this request will be considered on its merits and may or may not be approved. 4. Failure to abide by the conditions and limitations contained in this permit may subject the Permittee to an enforcement action by the Division in -accordance with North Carolina General Statute 143-215.6A to 143-215.6C. 5. The annual administering and compliance fee must be paid by the Permittee within thirty (30)- days after being billed by :the Division. , Failure to pay the fee accordingly may cause the Division to initiate action to revoke this permit as specified by 15 NCAC 2H .0205 (c)(4). 6. The issuance of this permit does not exempt the Permittee from complying with any and all, statutes, rules, regulations, or ordinances which may be imposed by other government agencies (local, state, and federal) which have jurisdiction, including but not limited to applicable river buffer rules in 15A NCAC 2B.0200, erosion and sedimentation control requirements in 15A NCAC Chapter 4 and under the Division's General Permit NCGO10000, and any requirements pertaining to wetlands under 15A NCAC 2B .0200 and 2H .0500. , . 6 7. The Permittee, at least six (6) months prior to the expiration of this permit, shall request its extension. Upon receipt of the request, the Commission will review the adequacy of the facilities described therein, and if warranted, will extend the permit for such period of time and under such conditions and limitations as it may deem appropriate. 8. This permit may be modified, or revoked and reissued to incorporate any conditions, limitations and monitoring requirements the Division deems necessary in order to adequately protect the environment and public health. Permit issued this the 26t"day of August, 2005. NORZCLINA ENVIRONMENTAL MANAGEMENT COMMISSION ✓LAlan W. Klimek, P.E., Director Division of Water Quality By Authority of the Environmental Management Commission Permit Number WQ0014248. 7 NON -DISCHARGE REGIONAL WATER.QUALITY " STAFF REPORT AND RECOMMENDATIONS Da` 'ie I78fiO4t County: Unknown,, To: on Dischar a Permittin "Unit m g Perittee: Town of Cheraw. SC NDPU Reviewer: Duane Leith . Application No:: W00014248 Regional Login Nos W00014248-Residuals Distribution GENERAL INFORMATION 1. -This application IS (check all that apply): ❑ New Z ;Renewal El MiriorMWifkation'❑ Major Modification ❑ Surface Irrigation [:]-Reuse ❑ Recycle ❑ High Rate Infiltration ❑,EvaporatioWMfiltration Lagoon ❑ Land Application of Residuals , ❑ Attachment B included as appropriate Z 503 regulated ❑ 503 exempt Z Distribution of Residuals ❑ Surface Disposal ,2.. Was a site visit conducted in order to prepare -this report? ❑ Yes or. [E No. a. Date of site visit: b. Person contacted'and contact information:. ; c. Site visit conducted by; d. Inspection Report Attached: ❑ Yes or Z,N6. 3. Is the following information entered into the BIMS°record for this application correct? ' Yes or No. " If h6;. please complete the following 'or indicate that it is correct on the current application. For Treatment Facilities: a, Location: Cheraw, .SC in Chesterfield'Co b. Driving -Directions: a USGS Quadrangle Map name and number: Wallace' d. Latitude: 34-41-24 Longitude: 79-52=10- e. Regulated Activities % Type of Wastes (e.g., subdivision, food processing, municipal wastewater): Municipal For Disposal Sites: into the document for each site, or attach additional- pages for each site) a. Location(s): b. Driving Direction's: c. USGS, Quadrangle, Map name and number: d. Latitude: Longitude: FORM; NDSRR 03/02 ' 1 v NON -DISCHARGE REGIONAL .WATER ,QUALITY STAFF REPORT AND RECOMMENDATIONS NEWAND MAJOR MODIFICATIONAPPLICATIONS (this_ section not needed for renewals or minor modirications, skin to next section) DESCRIPTION OF WASTES) AND FACILITIES 1. Please attach completed rating sheet. Facility Classification: 2. Are the new treatment facilities -adequate for the type of waste and disposal system? ❑ Yes ❑ No ❑ N/A. If no, please explain: 3.. Are the new site conditions (soils, topography, etc) consistent with what was reported by the soil scientist and/or Professional Engineer? ❑ Yes ❑ -No ❑ N/A. If no, please explain: 4. Is the proposed residuals management plan for the adequate and/or acceptable to the Division. ❑ Yes ❑ No ❑ N/A. If no, please explain: 5. Are the proposed application rates for new sites (hydraulic or nutrient) acceptable? ❑ Yes ❑ No ❑ N/A. If no, please explain: 6: Are the new treatment facilities or any new disposal sites located in a 109-year floodplain? ❑ Yes. ❑ No ❑ N/A. If yes, please attach a map showing areas of 100-year floodplain and please explain and recommend any mitigative measures/special conditions in Part IV: 7. Are there any buffer conflicts (new treatment facilities or new disposal sites)? ❑ Yes or ❑ No: If_ - yes, please attach a map showing conflict areas or attach any new maps, you have received from the applicant to be incorporated into the permit: FORM: NDSRR 03/02 2 NON -DISCHARGE REGIONAL WATER QUALITY STAFF REPORT AND RECOMMENDATIONS RENEWAL AND MODIFICATIONAPPLICATIONS (use previous section for new or maior modification systems) DESCRIPTION OF WASTE(S) AND FACILITIES 1. Are there an appropriately certified ORCs for the facilities? ❑ .Yes or ❑ No. Operator in Charge: Certificate #: Back- Operator in Charge: Certificate #: 2. Is the design, maintenance and operation (e.g. adequate aeration, sludge wasting, sludge storage, effluent storage, etc) of the treatment facilities, adequate for the -type of waste and disposal system? ® Yes or ❑ No. If no, please explain: Appears to be so. 3. Are the site conditions (soils, topography, etc) maintained appropriately and adequately assimilating thewaste? ❑ Yes or ❑ No: If no, please explain: 4. Is the residuals management plan for the facility adequate and/or acceptable to the Division? ❑ Yes or ❑ No. If no, please explain: 5. Are the existing application rates (hydraulic or nutrient) still acceptable? ❑ Yes or ❑ No. If no, please explain: 6. Are there any buffer conflicts (treatment facilities or disposal sites)? ❑ Yes or ❑ No. If yes, please attach a map showing conflict areas or -attach any new maps you have received from the applicant to be incorporated into the permit: 7. Is the type and/or volume of waste(s) as written in the existing permit correct? ❑ Yes. or ❑ No. If no, please explain:. _ 8. Is the description of the facilities as written in the existing permit correct? ❑ Yes or ❑ No. If no, please explain: 9. Has a review of all self monitoring data been conducted? ❑ Yes or ❑ No. Please summarize any findings resulting from this review: , 10. Check all that apply:. ❑ No compliance. issues; ❑ Notice(s) of viol ation.within the last permit cycle; ❑ Current enforcement action(s) ❑ Currently under SOC; El Currently under JOC; ❑ Currently. under moratorium. If any items, checked, please explain and attach any documents that may help clarify answer/comments (such as NOV, NOD etc): , 11. Have all compliance dates/conditions in the existing permit, SOC, JOC, etc. been complied with? ❑ Yes or ❑ No.. If no, please explain: 12. Are there any issues related to compliance/enforcement that should be resolved before issuing this permit? ❑ Yes or Z No. If yes, please explain: FORM: NDSRR 03/02 3 NON -DISCHARGE REGIONAL WATER QUALITY STAFF REPORT AND RECOMMENDATIONS E VAL UA TION AND RECOMMENDATIONS 1. Provide any additional narrative regarding your review of the application.: 2. List any items that you would like NDPU to obtain through an additional information request. Make sure that you provide a reason for each item: Item • Reason The sample product label advises users to contact the Clemson Extension Service and the Soil Conversation Service, that appears to be in SC. I will let Nondischarge Permitting decide whether more local contact information should be provided. 3. List specific Permit conditions that you recommend to be removed from the permit when issued. Make sure that you provide a reason for each condition: Condition Reason 4. List specific special conditions or compliance schedules that you recommend to be included in the permit when issued. Make sure that you provide a reason for each special condition: Condition Reason 5. Recommendation: ❑ Hold, pending receipt and review of additional information by regional office; ❑ Hold, pending review of draft permit by regional office; Z Issue; ❑ Deny. If deny, please state reasons:. Upon satisfactory review by Nondischarge Permitting. the WO RRO has no obiection to the issuance of the permit. 6. Signature of report preparers FORM: NDSRR 03/02 4 NON -DISCHARGE REGIONAL WATER -QUALITY STAFF REPORT AND 'nlECOMM NDATIONS' Signature of WAS re/lonal supervisor: Date: / M142 ADDITIONAL REGIONAL STAFF REVIEW ITEMS This request is for the renewal'of'a permit for the Distribution and'Marketing" of Residuals that oriainate and are produced in Cheraw, SC. The information submitted in the application package seems to be that information required for review and issuance of a renewed pemiit. FORM: NDSRR 03/02 5 NON -DISCHARGE APPLICATION REVIEW REQUEST FORM Dat st 18, 2003 To: ❑ Forrest Westall, ARO-WQS ❑ Paul Rawls, FRO-WQS Rex Gleason,_MRO-WQS = �❑ L H ,Ken Schuster, RRO-WQS., �^�___ ___.__v__ ❑ Jim Mulligan, WaRO-WQS ❑ Rick Shiver, WiRO-WQS ❑ Steve Mauney, WSRO-WQS From: Duane Leith, Non -Discharge Permitting Unit Telephone: (919) 733-5083 ext. 370 E-Mail. duane.leith@ncmail.net A. Permit Number: W00014248 B. Owner: Town of Cheraw (South Carolina) ❑ Debra Watts, COJS 2 rn- , Copies Sent to CO,-GWS Copies Sent to RO-WQS: 1 ❑ Distribute 0 Copies to RO-GWS Fax: (919) 715-6048 C. Facility/Operation: Town of Cheraw Residuals Distribution Program ❑ Proposed ®, Existing ❑ Facility : ® Operation D. Application: 1. Permit Type: ❑ CS (O&M) ❑ Surface Irrigation ❑ Reuse. ❑ H-R Infiltration ❑ Recycle ❑ I/E Lagoon ❑ GW Remediation (ND) For Residuals: ❑ Land App. ® D&M ❑ Surface Disposal ® 503 ❑ 503 Exempt ❑ Animal 2. Project Type: ❑ New ❑ Major Mod. ❑ Minor Mod. ® Renewal ❑ Renewal w/ Mod. E. Comments/Other Information: ❑ I would like to accompany you on a site visit. This is a new application. An earlier application was returned due to addinfo not being received. Attached, you will find all information submitted in support of the above -referenced application for your review, comment, and/or action. Within 30 calendar days, please take the following actions: For RO-WQS: ® Return a Completed Form NDSRR. ❑ Attach Attachment B for Certification by the NDPU. ❑ Issue an Attachment B Certification from the RO*. * Remember that you will be responsible for coordinating site visits, reviews, as well as additional information requests with other RO-WQS and RO-GWS representatives in order to prepare a complete Attachment B for certification. Refer to the RPP SOP for additional detail. For CO-GWS: ❑ Return a Memorandum with Permit Condition Recommendations. When you receive this request form, please write your name and dates in the spaces below, make a copy of this sheet, and return it to the appropriate Non- ischarge Permitting Unit contact person listed above. RO-WQS Reviewer: Date: 49 CO-GWS Reviewer: Date: FORM: NDARR 09/02 Page 1 of 1 Michael F. Easley, Governor William G. Ross Jr., Secretary North Carolina Department of Environment and Natural Resources Alan W. Klimek, P.E., Director Division of Water Quality August 5, 2003 Ricky Ingram Public Utility Director Town of Cheraw PO Box 219 Cheraw, SC 29520 Subject: Acknowledgement of Application No. WQ0014248 Town of Cheraw Distribution of Residual Solids Wake County Dear Mr. Ingram: The Non -Discharge Permitting Unit of the Division of Water Quality (Division) acknowledges receipt of your permit application and supporting materials on July 30, 2003. This application package has been assigned the number listed above and will be reviewed by Duane Leith. The reviewer will perform a detailed review and contact you with a request for additional information if necessary. To ensure the maximum efficiency in processing permit applications, the Division requests your assistance in providing a timely and complete response to any additional information requests. Please note at this time processing permit applications can take as long as 60 - 90 days after receipt of a complete application. If you have any questions, please contact Duane Leith at 919-733-5083, extension 370, or via e-mail at duane.leith@ncmail.net. If the reviewer is unavailable, you may leave a message, and they will respond promptly. PLEASE REFER TO THE ABOVE APPLICATION NUMBER IN CORRESPONDENCE AND WHEN MAKING INQUIRIES ON THIS PROJECT. To check the status of this permit application, go to http://h2o.onr.state.nc.us/bims/Reports/reportsPermits.htmi and check pending permits for the Non - Discharge program in the. pertinent region. Projects are listed (as facility) in alphabetical order. Sincerely, Kim H. Colson, P.E. Supervisor cc:. Raleigh=Regional=Gffice Water Q.uality�Section- Permit Application File WQ0014248 Non -Discharge Permitting Unit 1617 Mail Service Center, Raleigh, NC 27699-1617 DENR Customer Service Center An Equal Opportunity Action Employer Internet http://h2o.enr.state.nc.us/ndpu. NCDENR Telephone •(919) 733-5083 Fax (919) 715-6048 Telephone 1 800 623-7748 50% recycled/10% post -consumer paper Permit Number WQ0014248 Program Category Non -discharge Permit Type Distribution of Residual Solids (503) Primary Reviewer duane.leith Permitted Flow Facility Name Town of Cheraw Residuals Distribution Program Location Address Post Office Box 219 Cheraw Owner SC 29520 08/05/03 Permit Tracking Slip Status Project Type In review Renewal Version Permit Classification Individual Permit Contact Affiliation Major/Minor Region Minor Raleigh County Wake Facility Contact Affiliation Owner Name Owner Type Town of Cheraw Government - Municipal Owner Affiliation Ricky Ingram Post Office Box 219' Cheraw, SC 29520 Dates/Events Scheduled Orig Issue App Received Draft Initiated Issuance Public, Notice Issue Effective Expiration 08/15/97 07/30/03 Regulated Activities Requested/Received Events Wastewater treatment and disposal RO staff report received RO staff report requested Additional information requested Additional information received Groundwater -comments -requested ®V)%� r Grrouadwatemrnents-received ��� Outfall NULL ,,(/Waterbody Name Stream Index Number Current Class // Subbas-inn A/4 / e s 7zf 5r i't Ste./co.•: �%f��l cg J� o.�/ Su�iN'! � e J'�s� �/,'c%sj7`/t�ti. �..A J� �•-�1 r I t,. Department of Environment, Health and Natural Resources Division of Environmental Management. Non-Diisu'llaige Permit Application Form (THIS FORM MAY BE PHOTOCOPIED FOR USE AS AN ORIGINAL) DISTRIBUTION OF RESIDUAL SOLIDS This application is intended for facilities which are to be regulated under 40 CFR Part 503 I. GENERAL INFORMATION: 1. Applicant's name (please specify the name of the municipality, corporation, individual, etc.): - Town of Cheraw 2. Print owners or signing official's name and title (the person who is legally responsible for the facility and its compliance): Ricky Ingram — Public Utility Director 3. MailinQ address: P.O. Box 219 City: Cheraw State: SC Zip: 29520 Telephone Dumber: ( 843 ) 537-8440 4. Application Date: 07/23/03 , 5. Fee Submitted: S 400.00 [Tbe permit processing fee should be as specified in 15A NCAC 2H .0205(c)(5).] 6. Specify bow these residuals will be distributed: sold or giver. away in bags or other containers; lawn (bulk); home garden (bulk); X other; Given away in bulk quantities for pasture, land reclamation, forestry, etc. 7 If the alternative for residual disposal consists of "surface disposal" as dei:ned under 40 CFR Part 503, please complete the application titled "SURFACE DISPOSAL OF RESIDUAL SOLIDS. Please identify if there is any storage of residuals in a surface impoundment or disposal th.ru landfillins. Explain: 8. Is the residual process facility also the generator? X Yes; No 9. Latitude: 3404112411 Longitude: 79052' 10" of rCSidulp:oc:caa iauiiity 10. Specif; whether the process facility is owned by: federal; private; state; X local sovernment; 11. County where facility is located: Chesterfield II. PERMIT INFORMATION: I. Application No. (will be completed by DEM.): 2. Specify whether project is: new; X renewal"; modification For renewals, complete all sections included in the application. Engineering Signature and Seal not required. for renewals or if there is not any construction involved with the subject project. 3. If this application is being submitted as a result of a renewal or modification to an existing permit, list the existing permit number WQ0014248 and its issue date August 15, 1997 FORM: DRS 06/94 Page. 1 of 8 III. FACILITY INFORMATION (attach additional pages for additional sources of residuals): 1. Name r'f fa__': ; he:e residuals a.-e generated or prepamed: Town of Cheraw WWTp 2. Facility permit number: SCO020249 ; facility permit bolder: _ Town of Cheraw 3. Specify whether facility in Section IE.1 is owned by: federal; private; state; _X local government; 4. Specify facility design flow Type of residual storage: 4.0 mgd; facility average daily flow: 1.978 mgd; Concrete pad with shelter Volume of residual storage: 50,000 cubic feet Length of residuals storage at facility: 120 days (the Division requires a minimum 30 days storage in units that are separate from treatment system, i.e. not in clarifiers, aeration basins, etc.); Estimated volume of residuals: 1800 (dry tons/yr.); residual plus additives 5. If the residual process facility is not the same as the generator, please specify delivery frequency and quantity of residual to be processed: N/A 6. Facility contact (person familiar with residuals preparation): Ricky Ingram 7. Facility contact's telephone number: ( 843 537-8440 S. Location of treatment fatgity: South Carolina State; - Chesterfield County 9. Mailing address: P.O. Box 219 Cheraw SC 29520 P 10. Specify the source of the residuals: X treatment of domestic wastewater, X treatment of industrial wastewater; other (explain): Attach an explanation of either the treatment process, manufacturing process, or how the waste is generated. Provide full and complete details of the entire process. 11. Does the facility which generates the residuals have an approved pretreatment program? X Yes; No. This includes facilities wbicb are classified as -a "Class I" facility (any publicly owned treatment works required, under 40 CFR=03.8, to have an approved pretreatment program or any facility treating domestic sewage that is classified as "Class I" by the appropriate federal or State authority) IV. RESIDUALS INFORMATION (attach additional pages for additional sources of residuals): I. Information for Hazardous Waste (RCRA) Determination. The information requested or, the limitations snecifed belo:: pertain only to those residuals that are generated from a municipal wastewater treatment facility with industrial contribution or active pretreatment program and from any other treatment facility with wastewater sources that include industrial sources. a. Are any of the residuals covered by this application listed in 40 CFR 261.31-261.33? Yes: X No. If Yes, Iist the number(s): b. Do the residuals exhibit any of the four characteristics defined by 40 CFR 261.21-261.24? Yes; _X No. Attach laboratory results for the Toxicity Characteristic Leaching Procedure. Analyses, Reactivity, Ignitabdity, and Corrosivin• for each residual. FORM: DRS 06/94 Pate 2 of 8 Note: If -the following constituent levels (as determined by the Toxicity Characteristic Leaching'Procedure Analyses) are exceeded in the residuals ,or if the pH, of _the residual is. not within the range listed below, the residual is by - definition a Hazardous waste. Chemical analyses must be made to Minimum Detection Levels. - PENS REM .Arsenic 5.0 Barium 100.0 Benzene 0s Cadmium 1.0 Carbon tetrachloride 0.5 Chlordane - 0.03 Chlorobenzene 100.0 Chloroform 6.0 Chromium 5.0 o-Cresol 200.0 m-Cresol 200.0 p-Cresol- 200.0 Cresol 200.0 .. 2,4-D 10.0 1,4-Dichlorobenzene 7.5 1,2-Dichloroethane 0.5 - 1,1-Dichloroethylene 0.7 2,4-Dinitrotoluene 0.13 Endrin 0.02 Heptachlor (and its hydroxide) . 0.008 Hexachlorobenzene 0.13. Hexachloro-1,3-butadiene 0.5 Hexachloroethane 3.0 Lead 5.0 % 'Lindane 0.4 Mercury 0.2 Methoxychlor 10.0 Methyl ethyl ketone.,.- �' 200.0 Nitrobenzene 2.0 Pentachlorophenol 100.0 Pyridine 5.0 Selenium 1.0 Silver 5.0 Tetrachloroethylene .- 0.7 Toxaphene 0.5 Trcchooroethylene '. 0.5 . '2,4,5-Trichlorophenol 400.0 - 2,4,6-Trichlorophenol 2.0 2,4,5-TP -(Silvex) - 1.0 Vinyl chloride 0.2 pH (2:1 volJwt.): >2.0 s.u. - <12.5 s.u. i+ - NOTE: IF ANY OF THE RESIDUALS MEET THE DEFINITIONS- OF A HAZARDOUS WASTE, AS NOTED, IN EITHER "A" OR "B"- ABOVE; A. PERMIT CANNOT' BE -ISSUED :FOR THAT MATERIAL AND, IT SHOULD NOT .BE INCLUDED AS PART OF THIS APPLICATION. 2. For each residual, please attach a complete chemical analysis of the material. This analysis must be comprehensive enough to completely characterize the residual and must be based upon`a review of the process that generates the material. If the facility that will. generate the -residual is not yet in operation,, the characterization must be based on similar existing facilities and projection based on the type of facility. The analysis must include a minimum of the following parameters and any other known.and suspected contaminants that are tributary to the system. Arsenic Molybdenum Calcium Phosphorus Cadmium Nickel Magnesium Potassium Chromium Selenium Nitrate -Nitrite Nitrogen Sodium Copper Zinc % Total Solids TKN Lead Aluminum pH Mercury Ammonia -Nitrogen Plant Available Nitrogen (by calculation) FORM: DRS 06194 Page 3 of 8 3. Wastewater residuals can not be sold or given away if -the concentration of any pollutant in the residuals exceeds the ceiling concentrations specified in the table below. Specify the pollutant concentration of these residuals (attach lab analysis): Pollutant Pollutant Ceiling Concentration (mg/kg) Dry Weight Basis Pollutant.Concentration-(mg/kg) Dry Weight Basis Arsenic 75 < 2.73 Cadmium 85 0.549 Chromium 3000 15.2 Copper 4300 1 4 Lead 840 11.9 Mercury 57 0.310 Molybdenum 75 2.19 Nickel 420 Selenium 100 2.73 Zinc 7500 109 4. Provide, all applicable pilot studies and any bench scale tests performed on. each residual source and the results, including the approximate fertiliier equivalent. 5. Wastewater residuals can't be sold or Eiven away in bags or other containers for application to the land unless one of the following options is satisfied. A Specify either A .or B. Please be advised, if the residuals are to be sold or given away in bulk for application to lawn or home garden then Opdon A is the only option. A . The pollutant concentration of the residuals must be less than Pollutant Monthly Average Concentrations listed in the table below. Pollutant Monthly Average Concentrations Dry Weight Basis (mg/ke) Pollutant Concentration Dry Weight Basis (m ) . Arsenic 41 < '2.73 Cadmium - - 39 < 0,549 Chromium 1200 15.2 Copper 1500 61.4 Lead 300 111. 9 Mercury 17 0.310 Nickel 420 34.2 Selenium 36. < 2.73 Zinc 2800 109 B . The product of the concentration of each pollutant in the residual and the annual whole residual application rate for the residual shall not cause the Annual Pollutant Loading Rate to be exceeded. In order for the Annual «aole Residual Application Rate (AWRAR) to be calculated the Annual Pollutant Loading Rate (APLR) is divided by the pollutant concentration (PC) times 0.001 (a conversion factor) as follows: AWRAR = ARL& PC * 0.001 FORM: DRS 06/94 Pace 4 of 8 Pollutant Pollutant Concentration Dry Weight Basis (mJk) Annual Pollutant Loading Rates (APLR) kg/hectare - Annual Whole Residual Application Rate (AWRAR) kg/hectare Arsenic 2.0 Cadmium 1.9 Chromium 150 Copper 75 Lead 15 Mercury 0.85 Nickel 21 Selenium 5.0 ..Zinc 140 The AWRAR for -the residual is the lowest AWRAR calculated. This, is the maximum rate at which the subject residual can be applied (to convert kg/hectare to lbs/acre multiply by 0.8924). Please specify kg/hectare or lbs/acre: AWRAR = V . PATHOGEN AND VECTOR ATTRACTION REDUCTION INFORMATION .(attach additional pages for additional sources of residuals): I. In order for the residuals to be Class A, in accordance with the pathogen requirements in 40 CFR 503.32(a), tither Part a or Part b &rld one of the options in Part c must be completed (pleah submit all lab analysis, test results and calculations): X a.. A Fecal coliforin density less than 1000 Mosi.. Probable Number per gram of total dry solids, or b. A Salmonella sp. density less than 3 Most Probable Number per 4 grams of total dry solids. fig_ c. In addition to Part a or Part b being met. one of the following alternatives must also be completed. Please specify 1, 2, 3, 4, 5a, 5b, 5c, 5d, 5e, 5f, 5c or 6 below being met: 1. timeltemp rat it an increased residuals temperature should be maintained for a prescribed period of time, in accordance with the following guidelines. The results (D) shall be the amount of time, in days, that the residuals shall remain at the given temperature: Time anti Temr entire nnirieiinPc Total Solids Tem rature (t) Minimum Time Equation Notes No heating of small > or = 7% > or = 500 C > or = 20 minutes D=131,700,000 particles by warmed 100.14 t gases or immiscible liquid. > or = 7% > or = 500 C > or =15 seconds D = 131, 00,000 Small particles heated by 100.14 t warmed gases or - immiscible liquid. < 7% > or = 500 C > or =15 seconds D=131,700,000 to 100.14 t. < 30 minutes < 7% > or = 500 C >or = 30 minutes D = 50,070,000 . 100.14 t T.. FORM: DRS 06/94 Page-5 of 8 alkaline treatment - the pH of the residuals is raised to greater than 12 for at least 72 hours. During this lime, th, temperature of the residuals should be greater than 520 C for at least 12 hours. In addition, after the 72 hour period, the residuals are to be air dried to at least 50% total solids. 3. prior testing for Enteric VirucNiable Helmin h Ova - the residuals are analyzed for the presence of enteric viruses (Plaque -forming units) [pfu] and viable behninth ova. If the residuals are analyzed before the pathogen reduction process and found to have densities of enteric virus <1 pfu/4 grams of total solids and viable helminth ova <1/4g total solids, the residuals are Class A with respect to enteric virus and viable helminth ova until the next monitoring episode. If the residuals are analyzed before the pathogen reduction process and found to have densities of enteric virus > or = 1 pfu/4 g total solids or viable helminth ova > or = 1/4 g total solids, and tested again after processing and found to meet the enteric virus and viable helminth ova levels listed under "4" below, then the processed residuals will be Class A with respect to enteric viruses and viable helminth ova when the operating parameters for the pathogen reduction process are monitored and shown to be consistent with the values or ranges of values documented. 4. no prior testing for Enteric VintsNiable Helminth Ova - if the residuals are not analyzed before pathogen reduction processing for enteric viruses and viable helminth ova, the density of enteric viruses must be less than 1 pfu/4 g of total dry solids and the density of viable helminth ova must be less than 1/4 g of�total dry solids, -.or the residuals must be treated by a "Process to Further Reduce Pathogens" or a"'Process to Further Reduce Pathogens" equivalent process. 5. The "Processes to Further Reduce Pathogens" (PFRP) are described as follows: a. Com4sting - using either the within -vessel or static.aerated pile composting methods, the temperature of the residuals are raised to 550 C or higher for three days. ' Using the windrow composting method, the residuals are raised to 550 C or higher for fifteen days. During the high temperature period, there will be a minimum of five turnings of the windrow. b. Heat Drying - residuals are dried by direct or indirect contact with hot gases to reduce the moisture content of the residuals to 10% or lower. Either the temperature of the gas in contact with the residuals exceeds 800 C or the wet bulb temperature of the gas in contact with the residuals, when the residuals leave the dryer, exceeds 800 C. c. Heat Treatment - liquid residuals are heated to a temperature of 1800 C or higher for thirty minutes. d. Thermonhilic Aerobic Dices i n - liquid residuals are agitated with air or oxygen to maintain aerobic cond:dons at residence times of ten days at temperatures of 550 C to 600 C. e. Beta Rav Irradiation - residuals are irradiated with beta rays from an accelerator at dosages of at least 1.0 megarad at room temperature (ca. 200 Q. f. Gamma Rav Irradiation - residuals are irradiated with gamma rays from certain isotopes such as 60Co and 137Ce, at dosages of at least 1.0 megarad at room temperature (ca. 200 Q. g. Pa_tet�izad - the temperature of the residuals is maintained at 700 C or higher for at least thirty minutes. 6. The residuals shall be treated in a process that is equivalent to a "Processes to Further Reduce Pathogens" (PFRP), as determined by the permitting authority based on evaluations of the recommendations provided by the Pathogen Equivalency Committee. 2. When residuals are to be sold or given away, one of the following vector attraction reduction requirements (a, b, c, d, e, f, g, or h) described below must be met. f Specify the letter of the vector attraction reduction requirement that has been met (submit lab results, test results and calculations). Any variation of the below must be described in full detail and attached. a. Aerobic or Anaerobic Digestion - The mass of volatile solids are reduced by at least 38%. Volatile solids reduction is measured between the residuals, prior to stabilization, and the residuals ready for use or disposal. This criterion should be readily met by properly designed and operated anaerobic digestors, but not as readily met by aerobic digestors. Treatment facilities with aerobic digestors may need to meet the vector attraction reduction requirement through 19c or 19d. FORM: DRS 06194 Page 6 of 8 b. Anaerobic D;a scion - If 38% volatile solids reduction cannot be achieved, vector attraction reduction can be L r demonstrated by further digesting a portion of the previously digested residuals in a bench scale unit for an additional 40 days at 3U' C to 370 C. If, at the end of the 40 days, the volatile solids are reduced by less than 17%, vector attraction reduction is achieved. c. Aerobic Dig •ion - If 38% volatile solids reduction cannot be achieved, vector attraction reduction can be demonstrated by further digesting'a portion of -the previously digested residuals that have a solids content of 2% or less in a bench scale unit for an additional 30 days at 200 C. If, at the end of the 30 days, the volatile solids are reduced by less than 15%, vector artaction reduction is achieved. d. Aerobic Dig ; ion - The specific oxygen uptake rate (SOUR) shall be equal to or less than 1.5 milligrams of oxygen per hour per gram of total dry solids at 201 C. e. Aerobic Processes - The temperature of the residuals for at least 14 days shall be greater than 40' C. During this time, the average temperature shall be greater than 450 C. f. Alkaline Stabilization - The pH of the residuals is raised to 12 or higher by alkali addition and, without the addition of more alkali, remains at 12 or higher for 2 hours and then at 11.5 or higher for an additional 22 hours. g. DCvi g (stabili7ed solids) - The total solids of residuals that do not contain unstabilized solids, and which are generated in a primary wastewater treatment process, shall be equal to or greater than 75%. Blending with other materials is not allowed to acLeve the total solids percentage. h. ing (unstaaJiuLed solids) - The total solids of residuals that contains unstabilized solids, and which are generated in a primary wastewater treatment process, shall be equal to or greater than 90%. Blending with other materials is not allowed to acLeve the total solids percentage. VI. GENERAL INFORMATION: 1. Please provide a brief narrative concerning materials handling, including the following: �-T a. How will the materials will be handled and transported from where the residuals were produced to where it will be Al b. Where will the residuals be stored until processed? C. How will leach -ate collection be handled? t' d. What will be he duration of treatment? e. Where will the final product be stored? f. How long will the final product be stored before being distributed? a. How will the f:nal product be distributed (packaging)? Plegse attach a marketability statement detailing destinations and approximate amounts of the final product to be ibu distrted. 3. ,Please provide either a label which shall be affixed to the bagged processed residual or an information sheet which shall be provided to the person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following information: a. The name and :address of the person who prepared the residual that is sold or given away in a bag or other container for application to the land. b. A statement ths[ application of the residual to the land is prohibited except in accordance with the instructions on the label or information sheet. c. A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered. d A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored residuals into any surface waters. e. Information on ail applicable buffers including a 10 foot buffer between application site and any public or private water supply source (including wells) and any stream, lake, river, or natural drainage way. f. The Annual "A --hole Residual Application Rate (AWRAR) for the residual that does not cause any of the annual pollutant loadLr,, rates to be exceeded (if necessary). FORM: DRS 06,94 Page 7 of 8 Name and Complete Address of Engineering Firm: Haves, Seav, Mattern & Mattern, Inc, 181 E. Evans Street BTC 105 City: * Florence State: Sc Zip: 29506 Telephone Number: ( 843 ) 669-4491 Professional Engineer's Certification: I, attest that this application for has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed this material and have judged it to be consistent with the proposed design. North Carolina Professional Engineer's Seal, Signature, and Date: r Applicant's Certification: ii I, Ricky Ingram , attest that this application for Distribution of Residual Solids has been reviewed by me Ln_f is accurate and complete to the best of my knowledge. I understand that if all required parts of this application are not completed a, -id that if all required supporting information and attachments are not included, this application package will be retuned to kne_as incomplete+ Signature 646 � � Date THE CONIPLETED APPLICATION PACKAGE, INCLUDING ALL SUPPORTING INFOR, ATI0\ AND iIATERIALS, SHOULD BE SE\'T TO 'THL FOLLONi'IN° ; ADDRESS: NORTH CAROLINA DIVISION OF ENVIRONNIENTAL MANAGEMENT WATER QUALITY SECTION PERMITS AND ENGINEERING UNIT POST OFFICE BOX 29535 RALEIGH, NORTH CAROLINA 27626-0535 TELEPHONE NUMBER: (9I9) 733-5083. FORM: DRS 06194 Pace 8 of 8 Davis & Brown PO Bog 15038 Quinby, SC 29506 (843) 665-6746 FAX: (843) 629-1444 Certificate of Analysis Client: CHERAW, TOWN OF South Carolina Certification Number: 21117 P.O.BOX 219 North Carolina Certification Number: 612 CHERAW, SC 29520 Client"#: 168 Receipt Date: 31-Jan-03 Contact: SHERRY TOLSON Report Date: 27-Feb-03 Sample Date: 29-Jan-03 SDG #: SDG-028528 Approved By: Van Ward Lab Director Reporting Parameter Result Limit Unit Method Flag Date Time Analyst Silver, Total <0.010 0.01 mg/l EPA 200.7 02/13/03 15:51 DH Zinc, Total 0.089 0.01 mg/L EPA 200.7 02/10/03 10:21 DH LSED-064172 1-27-03-300 Acid Digestion (Solids) YES EPA 200.2 02/03/03. 16:00 DH TCLP PASS P/F SW-846 S16 02/10/03 8:13 KK Percent Moisture 52.1 0.1 Wt% SW846 3540 02/11/03 16:50 LM Aluminum, Total 9900 0.526 mg/kg SW846 6010A D 02/20/03 15:42 DH Arsenic, Total <2.73 2.73 mg/kg SW846 6010A D 02/03/03 14:51 DH Cadmium, Total <0.549 0.549 mg/kg SW846 6010A D " 02/10/03 10:21 DH Chromium, Total 15.2 0.263 mg/kg SW846 6010A D 02/10/03 10:21 DH. Copper, Total 61.4 0.263 mg/kg SW846 6010A D 02/10/03 10.-21 DH Lead, Total 11.9 1.31 mg/kg SW846 6010A D 02/10/03 14:58 DH Molybdenum, Total <2.19 2.19 mg/kg SW846 6010A - D 02/06/03 17:08 DH Nickel, Total 34.2 0.263 mg/kg SW846 6010A D 02/10/03 10:21 DH Zinc, Total 109 0.263 mg/kg 8W8461601OA D 02/10/03 10:21 DH Mercury, Total 0.310 0.014 mg/kg . SW846 7470A D . 02/20/03 8:42 DH Selenium, Total <2.73 2.73 mg/kg SW846 7741A D 02/19/03 10:46 DH PCB BDL 2.9 mg/kg SW846 8080 S16 02/07/03 13:38 KK Paint Filter PASS P/F SW846 9095 S16' 02/06/03 15:15 MNU Page 4, ENVIRONMENTAL SCIENCE CORP. REPORT OF ANALYSIS Mr. Scott Fields Davis & Brown P.O. Box 15038 Quinby, SC 29506 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 February 12, 2003 ESC Sample # : L103192-03 Date Received February 04, 2003 Description 2-3-2003 Site ID Sample ID 64172 Project # 2-3-2003 Collected By Collection Date 01/27/03 09:45 Parameter Dry Result Det. Limit Units Method Date Analyst Total Solids 47.3 % 254OG 02/04/03 1311 SA Polychlorinated Biphenyls PCB 1016 BDL 0.42 mg/kg 8082 02/07/03 1338 KK PCB 1221 BDL 0.42 mg/ka 8082 02/07/03 1338 KK PCB 1232 BDL 0.42 mg/kg 8082 02/07/03 1338 KK PCB 1242 BDL 0.42 mg/kg 8082 02/07/03 1338 KK PCB 1248 BDL 0.42 mg/kg 8082 02/07/03 1338 KK PCB 1254 BDL 0.42 mg/kg 8082 02/07/03 1338 KK PCB 1260 BDL 0.42 mg/kg 8082 02/07/03 1338 KK i Al 'en VUrilEerley, ESC Representative Results listed are dry weight basis. BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Note: This report shall not be reproduced, except in full, without the written approval from ESC. The reported analytical results relate only to the sample submitted Page 4 of 8 ENVIRONMENTAL SCIENCE CORP. REPORT OF ANALYSIS Mr. Scott Fields Davis & Brown P.O. Box 15038 Quinby, SC 29506 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax Z.D. 62-0814289 Est. 1970 February 12,2003 ESC Sample # : L103192-04 Date Received February 04, 2003 Description 2-3-2003 Site ID Sample ID 64172 Project # 2-3-2003 Collected By Collection Date 01/27/03 09:45 Parameter Result Det. Limit Units Method Date/Time Analvst Decachlorobiphenyl 92. % Rec. 8081A 02/07/03 1050 KK Tetrachloro-m-xylene 86. % Rec. 8081A 02/07/03 1050 KK TCLP Herbicides 2,4,5-TP (Silvex) BDL 0.0020 mg/1 8151A 02/10/03 0813 KK 2,4-D BDL 0.0020 mg/1 8151A 02/10/03 0813 iGC Surrogate Recovery 2,4-Dichlorophenyl Acetic Acid 98. % Rec. 8151A 02/10/03 0813 rK TCLP Semi-Vclatiles 1,4-Dichlorobenzene BDL 0.10 mg/l 8270C 02/07/03 1835 KSG 2,4-Dinitrotoluene BDL 0.10 mg/l 8270C 02/07/03 1835 KSG Hexachlorobenzene BDL 0.10 mg/l 8270C 02/07/03 1835 KSG Hexachlaro-1,3-butadiene BDL 0.10 mg/1 8270C 02/07/03 1835 KSG Hexachlorcethane BDL 0.10 mg/1 8270C 02/07/03 1835 KSG Nitrobenzene BDL 0.10 mg/l 8270C 02/07/03 1835 KSG Pyridine BDL 0.10 mg/l 8270C 02/07/03 1835 KSG m&p-Cresol BDL 0.10 mg/1 8270C 02/07/03 1835 KSG o-Cresol BDL 0.10 mg/l 8270C 02/07/03 1835 KSG Pentachlorophenol BDL 0.10 mg/l 8270C 02/07/03 1835 KSG 2,4,5.-Trichlorophenol BDL 0.10 mg/l 8270C 02/07/03 1835 KSG 2,4,6-Trichlorophenol BDL 0.10 mg/l 8270C 02/07/03 1835 KSG Surrogate Recovery Nitrobenzene-d5 53. % Rec. 8270C 02/07/03 1335 KSG 2-Fluorobiphenyl 48. % Rec. 8270C 02/07/03 1835 KSG p-Terphenyl-dl4 83. % Rec. 8270C 02/07/03 1835 KSG Phenol-d5 60. % Rec. 8270C 02/07/03 1835 KSG 2-Fluoromhenol 57. % Rec. 8270C 02/07/03 1835 KSG 2,4,6-Tribromophenol 78. % Rec. 8270C 02/07/03 :835 KSG AI'lenMinkerley, ESC Renresentative BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789 , AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST-0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Notes: The reported analytical results relate only to the sample submitted This report shall not be reproduced, except in full, without the written approval from ESC. All samples analyzed in accordance with 40 CFR, Part 136.3 L103192-04 (PAINT) - contains no free liquid Page 6 of 8 ENVIRONMENTAL SCIENCE CORP. 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Mr. Scott Fields February 12,2003 Davis & Brown P.O. Box 15038 Quinby, SC 29506 ESC Sample # : L103192-04 Date Received February 04, 2003 Description 2-3-2003 Site ID Sample ID 64172 Project # 2-3-2003 Collected By Collection Date 01/27/03 09:45 Parameter Result Det. Limit Units Method Date/Time Analyst Paint Filter Test See Footnote % 9095 02/06/03 1515 MNU TCLP Extraction - 1311 02/04/03 1506 TVH Mercury BDL 0.0010 mg/l 7470A 02/05/03 1751 RH Arsenic BDL 0.050 mg/l 60102 02/05/03 2339 CRF Barium 0.56 0.050 mg/l 6010B 02/05/03 2339 CRF Cadmium BDL 0.050 mg/•l 6010B 02/05/03 2339 CRF Chromium BDL 0.050 mg/l 6010B 02/05/03 2339 CRF Lead BDL 0.050 mg/l 6010B 02/05/03 2339 CRF Selenium 0.065 0.050 mg/1 6010B 02/05/03-2339 CRF Silver BDL 0.050 mg/1 6010B 02/05/03 2339 CRF TCLP ZHE Extraction - 1311 02/04/03 1507 TVH TCLP Volatiles Benzene BDL 0.050 mg/l 8260B 02/06/03 1743 CH Carbon tetrachloride BDL 0.050 mg/l 8260B 02/06/03 1743 CH Chlorcbenzene BDL 0.050 mg/l 8260B 02/06/03 1743 CH Chloroform BDL 0.050 mg/l 8260B 02/06/03 1743 CH 1,2-Dichloroethane BDL 0.050 mg/1 8260B 02/06/03 1743 CH 1,1-Dichloroethene BDL 0.050 mg/l 8260B 02/06/03 1743 CH 2-Butancne (MEK) BDL 2.5 mg/l 8260B 02/06/03 1743 CH Tetrachloroethene BDL 0.050 mg/l 8260B 02/06/03 1743 C4 Trichlcrcethene BDL 0.050 mg/l 8260B 02/06/03 1743 CH Vinyl chloride BDL 0.050 mg/l 8260B 02/06/03 1743 CH Surrogate Recovery Dibromofluoromethane 98- % Rec. 8260B 02/06/03 1743 CH Toluene-d8 100 % Rec. 8260B 02/06/03 1743 CH 4-Bromofluorobenzene 100 % Rec. 8260B 02/06/03 1743 CH TCLP Pesticides Chlordane BDL 0.030 mg/l 8081A 02/07/03 1050 KK Endrin BDL 0.0050 mg/l 8081A 02/07/03 1050 KK Heptachlor BDL 0.0050 mg/1 8081A 02/07/03 1050 KK Lindane BDL 0.0050 mg/l 8081A 02/07/03 1050 KK Methoxychlor BDL 0.0050 mg/l 8081A 02/07/03 1050 KK Toxanhene BDL 0.10 mg/l 8081A 02/07/03 1050 KK Surrogate Recovery BDL - Below Detection Limit' Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789 AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST-0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Notes: The reported analytical results relate only to the sample submitted This report shall not be reproduced, except in full, without the written approval from ESC. L103192-04 (PAINT) - contains no free liquid Page 5 of 8 A N I M A L W A S T E A N A L Y S I S R E P. O R T Agricultural Service Laboratory LAB No. 10119 . Clemson Extension 171 Old Cherry Rd, Clemson, SC 29634 http://www.clemson.edu/agsrvlb NAME TOLSON, SHERRY ACCOUNT COCHSFL ADDRESS P 0 BOX 219 DATE 02-04-2003 CITY CHERAW SC CHERAWUTILITY@MINDSPRING.COM ZIP CODE 29520 SAMPLE NO. 12703300 MANURE: OTHER STORAGE: COVERED -----------------RESULTS REPORTED ON AN AS -SAMPLED BASIS---------------------- lbs/ton Ammonium Nitrogen 0.03 % 0.60 Organic Nitrogen 0.74 % 14.83 Nitrate Nitrogen --------------------------------------------------------------- 60.79 ppm 0.12 INCORPORATED AVAILABLE NITROGEN ESTIMATE 9.58 SURFACE AVAILABLE --------------------------------------------------------------- NITROGEN ESTIMATE 9.40 Phosphorus as P205 0.39 % 7.73 Potassium as K20 0.15 % 2.91 Calcium 14.72 % 294.30 Magnesium 0.22 % 4.44 Sulfur 0.12 % 2.32 Zinc 67.06 ppm .0.13 Copper 37.15 ppm 0.07 Manganese 56.93 ppm 0.11 Sodium 184.78 ppm 0.37 Moisture 51.75 % Calcium Carbonate Equivalency 34.35'. % 686.93 ------------------------------------------------------------------------------ INCORPORP_TED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be incorporated into the soil within hours of application. Assumes some loss of ammonium-N during application and prior to incorporation. SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of organic-N, and 100.% of nitrate-N (if determined). Assumes the manure will .be left on the surface of the soil with no incorporation by plowing or irrigation. Available nitrogen calculations are estimates and if nitrate-N was not re- quested the amount of available nitrogen may be slightly more than reported. Also, the actual amount may be more or less than the estimate depending on the composition of the manure, soil type, and environmental conditions. All of the potash in the animal waste should be plant available in the first year of application. Although not all of the phosphorous is available in the first year, its availability should be comparable to that in commercial fertilizers. The rate of animal waste to apply for crop production is dependent on the nutrient content of the waste, method of application and i corpor tion, it test, crop to be grown, and previous manure applications m s ca the plant available nitrogen content of the waste is use rm n th r to of application. APPROVED BY Cooperative extension work in agriculture and home a onomics-state o SOUTH CAROLINA, CLEMSON UNIVERSITY, and the UNITED S3ATES DEPARTMENT of AGRICULTURE cooperating. 1 of 1 2/4/03 5:16 PM 1.0 1.1 1.2 1.3 2.0 WASTEWATER TREATMENT FACILITY .4 g TOWN OF CHERAW, SOUTH CAROLINA . � G O N FACILITY DESCRIPTION Treatment Process The Cheraw wastewater treatment plant is currently permitted for a capacity of 4.0 MGD. The plant treats wastewater utilizing the activated sludge process operating in the extended aeration mode. It includes the following treatment units: Bar screen, flow measurement,, grit chamber; aeration basins, clarifiers, and disinfection. Excess solids are removed from the treatment system pumped to a holding tank where the solids are mixed, aerated, and thickened. Solids are then dewatered utilizing a belt filter press and then further treated by the lime pasteurization process prior to a final disposal by land application. Current Operating Condition The current wastewater flow to the treatment plant averages approximately 1.54 MGD of which approximately 63 percent of this flow is from industrial users. The Town has an Industrial Pretreatment Program which controls the discharge of toxic pollutants. During the past year the influent and effluent BOD averaged 473 mg/1 and 12.4 mg/l respectively. Influent and effluent suspended solids have averaged 293 mg/1 and 12.8 mg/1 respectively. The plant's NPDES permit requires effluent BOD and TSS to be less than 30 mg/l. Solids Production The -quantity of solids produced by the plant is subject to many factors. During the past year, the plant staff removed from the treatment system approximately 1728 dry tons. Dewatered solids off the belt press are not sufficiently stabilized and must receive additional treatment in order to comply with EPA standards for land application. BIOSOLIDS TREATMENT AND DISPOSAL 2.1 Process Description Dewatered solids receive additional treatment by a process developed by the RDP Company call EnVessel pasteurization. This process utilizes quicklime and supplemental electrical heat to elevate the pH and temperature for the sludge to that level needed to destroy pathogens and meet vector attraction requirements. Amore detailed description of the process is presented below. As the sludge comes off the belt press it is conveyed to a storage hopper then on to a mixing chamber called a "thermoblender" where quicklime is added. The mixing chamber contains mixing rotors that blend the sludge and the quicklime. Within this chamber the sludge is heated to approximately 70°C (158°F) by reaction with the quicklime and by electrical heat tubes installed internal to the mixing rotors. The lime also elevates the sludge pH to 12. The heated sludge/lime mixture is then discharged to the pasteurization vessel where the entire mass of material is allowed to cook for approximately 30 minutes. This vessel is an enclosed, insulated environment, maintaining the proper temperature over time to destroy harmful pathogens. The vessel is equipped with heating elements to compensate for any heat losses during the processing period and to ensure that the sludge maintains the proper temperature throughout. After treatment the biosolids are conveyed from the pasteurization vessel to a concrete pad where they are windrowed to facilitate further dewatering after which the biosolids are moved into a covered storage area until land application. 2.2 Significant Process Technical Features 2.2.1 General: The process of sludge treatment by the addition of lime is not new and the technology is known and fully documented elsewhere. However, the process used in Cheraw has several unique technical features which improve the process of lime treatment and produces a biosolids product of superior quality. Some of those features are presented below. 2.2.2 Lime Dosage: the Cheraw biosolids treatment system utilizes a combination of lime and electrical heat to meet the temperature and pH requirements for pathogen destruction and reduction in vector attraction. A lime only treatment system would require approximately 1 pound of lime per pound of dry solids to create sufficient chemical hydration to raise the sludge temperature to 158°F. With the use of supplemental electrical heat, the Cheraw system has been able to reduce the lime requirement to approximately 0.43 pounds of lime per pound of dry solids. The reduction in requited lime dosage has several advantages to include the following. > Supplemental electrical heat allows the pH of the sludge to increase with less lime. > Ammonia gas is produced by the reaction of sludge and lime. With a lower lime dosage less ammonia gas is produced resulting in reduced process odors. It also results in preserving the nitrogen content of the final biosolids. > A lower lime dosage reduces the mass of biosolid product for final disposal. 2.2.3 Product Quality: The Cheraw system cures or cooks the sludge in an enclosed insulated treatment vessel. This method insures that the entire mass of sludge and lime mixture is maintained at the required temperature for complete pathogen destruction. As previously mentioned the vessel is equipped with electrical heating elements to compensate for any temperature loss during the treatment period. 2.2.4 Land Application R. In the Cheraw area most farmland requires the application of lime to make up the calcium that is absorbed by the crops. Lime is typically applied to the fields to maintain a pH of 6.5 to 7.0 generally at a rate of 2000 pounds per acre. The rate of land application of biosolids in the Cheraw area is typically limited by its lime content. Therefore, reducing the lime content as previously described allows a greater biosolids application rate per acre thereby decreasing the total amount of land required for biosolids disposal. For example, the land application rate for Cheraw's biosolids using a conventional lime only system would be 6.25 tons of biosolids per acre. With the lime and electrical heat system the application rate is increased to approximately 14.5 tons per acre. Therefore, the Cheraw system has reduced land requirement by approximately 57 percent. 2.3 Biosolids Product Quality In order to document compliance with the EPA 503 Regulation's Class A sludge pathogen reductions requirements and vector attraction requirements continuous measurements are made of sludge temperature and pH within the "thermoblender" and pasteurization vessel. The pH of the biosolids is also monitored at the end of the 24-hour treatment period to verify compliance with the EPA regulations. Since the process has been in operation, there has been no instance where temperature and pH requirements of EPA have not been met. Prior to hauling any biosolids off -site fecal coliform samples are taken. This sampling has indicated no evidence of fecal coliform regrowth even after several months of storage. 2.4 Biosolids Disposal The Town of Cheraw is currently marketing the biosolids to farmers and others. To date biosolids have been used for land reclamation, landfill top cover, and farmland. A research project has been, initiated by the State Forestry Commission and Clemson University to study the effect of Cheraw biosolids on pine tree growth at the Sandhills State Forest near Cheraw. Each recipient of biosolids is given a copy of a label as included. These labels describe the quality of the biosolids and provide assistance as to its proper use. . GENERAL INFORMATION DISTRIBUTION OF RESIDUAL SOLIDS TOWN OF CHERAW, SOUTH CAROLINA 1. Material Handling a. How will the residuals be handled and transported from where the residuals are produced to where they will be treated? Residuals are produced and treated at the same site. b. Where will the residuals be stored until processed? Residuals are stored in a holding tank until they are dewatered and pasteurized. c. How will leachate collection be handled? Leachate from the treatment system and storage facility are collected and returned to the head of the wastewater treatment plant. d. What will be the duration of treatment? Refer to attached biosolids treatment process description. e. Where will the final product be stored? After treatment biosolids are stored on a covered concrete pad. f. How long will the final product be stored before being distributed? The storage facility has the capacity to store product up to 120 days at current product rates. g. How will the final product be distributed? The biosolids are hauled by truck to land application sites in bulk. 2. Product Distribution Currently all product produced is being used by local farmers in South Carolina, North Carolina, and at the Sandhills State Forest. 3. Product Label Enclosed is a copy of the product label currently being used. This label is given to each recipient of product. �-� TOWN OF CHEQAW July 23, 2003 North Carolina Department of Environment and Natural Resources Division of Water Quality 1617 Mail Service Center Raleigh, N.C. 27699-1617 To Whom It May Concern: RE: NPDES PERMIT NO. SCO020249 TOWN OF CHERAW CHESTERFIELD, S.C. PART 11, B-6 SIGNATORY REQUIREMENTS The Town of Cheraw hereby authorizes the Town's Public Utility Director, currently Ricky Ingram, to sign and certify all applications, reports or documents containing information related to this permit that are submitted to the North Carolina Department of Environment and Natural Resources. This authorization shall remain in effect until this notice rescinds or changes this authorization and notifies. the North Carolina Department of Environment and Natural Resources in writing. Sincerely, J6 J. William Taylor Town Administrator JWT/em cc: , Andy Ingram, Mayor P.O. Box 219 • Cheraw, 6S.C. 29520 • (843) 537-8400 • FAX (843) , 537-8407 E-Mail: townofcheraw@mind,3prin8.com CHERAW-ALKALINE BIOSOLIDS SOIL AMENDMENT CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES BIOSOLIDS SAMPLE DATE: March 12, 2003 Biosolids Maximum Maximum Maximum Maximum Metal Allowable Allowable Application Application Content, Metal App. Rate, Rate, Rate, METALS ppm Content, ppm #/Acre/Yr. DT/Acre/Yr. WT/Acre/Yr. Arsenic, Total 3.25 41.00 1.80 127.55 277.04 Cadmium, Total 0.63 ' 39.00 1.70 623.64 1354.55 Chromium, Total 26.98 1200.00 134.00 1143.15 2482.94 Copper, Total 123.81 1500.00 67.00 124.57 270.58 Lead, Total 5.04 300.00 13.00 594.12 1290.44 Mercury, Total 0.08 17.00 0.75 2039.43 4429.69 Molybdenum, Total 4.51 18.00 0.80 40.85 88.73 Nickel, Total 36.40 420.00 18.70 118.26 256.85 Selenium, Total 3.13 36.00 4.50 330.72 718.33 Zinc, Total 223.28 1525.00 125.00 128.87 279.92 PCB BDL 10.00 `Actual metal content less than amount indicated. Biosolids Biosolids Maximum Maximum Nutrient Nutrient Crop/Soil Application Application Content, Content, Requirement, Rate, Rate, ppm % #/Acre" DT/Acre/Yr. WT/Acre/Yr. Nitrogen, Ammonia 608.17 0.06 Organic Nitrogen 6372.72 0.64 Plant Avail. Nitrogen (PAN) 108.60 0.01 120.00 254.36 552.48 Phosphorus as P205 3570.81 0.36 80.00 5.16 11.20 Potassium as K20 1494.35 0.15 50.60 7.70 16.73 Calcium, Total 118292.79 11.83 Calcium as CaO 165609.90. 16.56 Calcium as CaCO3 (CCE) 302432.67 30.24 2000.00 1.52 3.31 Magnesium, Total 1920.07 0.19 Manganese 39.10 0.00 Sulfur 1081.67 0.11 Percent Moisture 53.96 These are typical values and must be adjusted based upon specific site conditions DT is Dry Tons of Biosolids. WT is Wet Tons of Biosolids. CERTIFICATION: This biosolid product has been produced by the Town of Cheraw's Wastewater Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature and lime (calcium oxide). The Town of Cheraw certifies that this biosolid complies with the Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has a metal and nutrient content as presented above. DIRECTIONS FOR USE: This biosolid is intended to be used as a soil amendment. The biosolid land application rate shall not exceed the most restrictive Maximum Application Rate as indicated in the table above. The application rate for nitrogen, phosphorus, potassium, and calcium is dependent upon the crop grown and site soil characteristics. The user should contact the Clemson Extension Service (843-623-2134) and/or the Soil Conservation Service (843-623-2.187) for assistance in determining the proper application rate for each crop and site. In no case shall the land application rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension Service Circular #476 tilled "Lime and Fertilizer Recommendations." THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY. AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES. THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING. OF THIS BIOSOLID PRODUCT. Application of this residual is prohibited except in accordance with the instructions on this information sheet Residuals shall not be applied to any site that is flooded, frozen or snow-covered. The applier must provide adequate procedures to prevent surface run-off from carrying any disposed or stored residuals into any surface waters. A minimum buffer of 10 feet must be provided between the application site and any public or private water supply source (including wells) and any stream, lake, river or natural drainage way. Mr. Ricky D. Ingram, Public Utility Director P. 0. Box 111; Cheraw, SC 29520 Telephone: 843-537-8440 FAX: 843-537-8442 PP()nl IrT I BUM NAIIAP \O�OF W AT �RQG _ Michael F. Easley, Governor William G. Ross Jr., Secretary �y North Carolina Department of Environment and Natural Resources � r — I Alan W. Klimek, P.E., Director Division of Water Quality Apri] 28, 2003LIAPR 2 9 2003 RICKY D. INGRAM, PUBLIC UTILITY DIRECTOR TOWN OF CHERAW i POST OFFICE BOX 219 - - CHERAW, SOUTH CAROLINA, 29520 Subject: Application No. WQ0014248 Additional Information Request Town of Cheraw Residuals Distribution Program Distribution of Residual solids (503) Chesterfield County, South Carolina Dear Mr. Ingram: The Non -Discharge Permitting Unit has conducted a preliminary review of the subject permit application package. Additional information is required before we may continue our review. Please address the following items no later than May 28, 200.3. 1: The application must be signed by an appropriate person in accordance with 15A NCAC 211 .0206. This regulation states that, for a corporation, it must be signed by a principal executive officer of at least the level of vice-president, or his duly authorized representative. Please sign the application following the above requirement. You may provide documentation the signer, or any employee holding the position of the signer, is a duly authorized representative through a letter of delegation. 2. The copy -of the information sheet intended to accompany--the-residuals-does--not--meet-the requirements specified in item H.6 in your existing permit and our current regulations. Please provide either a label which shall be affixed to the bagged processed residual or a revised information sheet which shall be provided to the person who receives the processed residual. The label or information sheet shall contain at a minimum, the following information: a. The name and address of the person who prepared the residual that is sold or given away in a bog or other container for application to the land. b. A statement that application of the residual to the land is prohibited except in accordance with the instructions on the label or information sheet. . c. A statement that the residuals shall not be applied to any site that is flooded, frozen or - snow-covered. d. A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored residuals into any surface waters. Non -Discharge Permitting Unit 1617 Mail Service Center, Raleigh, NC 27699-1617 DENR Customer Service Center An Equal Opportunity Action Employer - Internet http://h2o.enr.state.nc.us/ndpu Telephone (919) 733-5083 Fax (919) 715-6048 Telephone 1 800 623-7748 5017o recycled/10% post -consumer paper NCDENIR e. Information on all applicable buffers including a 10 foot buffer between the • application site and any public or private water supply source (including wells) and any stream, lake, river or natural drainage way. 3. Please clarify the estimated volume of residuals listed 'as 1128 dry tons per year. Is this the weight of residuals alone or the residuals with amendments? Please note that we need the volume reported as weight of residuals with amendments. Your existing permit is for 1800 dry tons per year. You may provide a reasonable estimate of the .dry tons/year anticipated over the next five years if that might be different from the actual production recorded in a past year. Note that you are not allowed to distribute more than the dry tons/year specified in your permit. Please be aware that you are responsible for meeting all requirements set forth in North Carolina rules and regulations. Any oversights that occurred in the review of the subject application package are still the responsibility of the applicant. In addition, any omissions made in responding to the above items may result in future requests for additional.infon-nation. Please reference the subject application number when providing the requested information. Two copies of all revised and/or additional documentation should be signed, sealed, dated, and submitted to my attention at the address above. Please note that failure to provide -this additional information on or before the above requested date may result in your application being. denied. If you have any questions regarding this request, please do not hesitate to contact me at duane.leith@ncmail.net or (919) 733-5083, extension 370. You may also check the future status of this project online at http://h2o.enr.state.nc.us/bims/RQorts/reportsPermits.html. Thank you for your cooperation. Sincerely, Duane Leith Non -Discharge Permitting Unit Cc: NCDWQ Regional Offices, Water Quality Section Permit Application File WQ0014248 NON NPDES FACILITY AND PERMIT DATA 07/28/9}9k"07:46:41 RETRIEVE OPTION q TRXID 60U KEYWQ.0014248 PERSONAL DATA FACILITY APPLYING FOR PERMIT APP/PERMIT FEE-$ 400.00 --REGION FACILITY NAME> CHERAW, TOWN -A SLUDGE FACILIT5 CO.UNT_Y_>. WAKE f 05 ADDRESS: MAILING (REQUIRED) • ENGINEER: HAYES SEAY MATTERN & MATT STREET: PO BOX 111 STREET: 181 E. E.VANS ST; BTC 105 CITY: CHERAW ST SC ZIP 29520 CITY:.FLORENCE ST SC ZIP 2952 TELEPHONE 843 537 8440 TELEPHONE: 803 669 4491 STATE CONTACT> ALLEN FACILITY CONTACT JAMES T. MORRIS- TYPE OF PROJECT> SLUDGE D&M 15 LAT: 3441240 LONG: 07952100 DATE APP RCVD 08/07/97 N=NEW,M=MODIFICATION,R=REISSUE> N' DATE ACKNOWLEDGED 08/08/97 DATE REVIEWED 08/12/97 RETURN DATE REG COMM REQS / / DATE DENIED / / NPDES #- REG COMM RCVD / / DATE RETURNED / / TRIB Q .0000 MG ADD INFO REQS / / OT AG COM REQS / / TRIB DATE- ADD INFO RCVD / / OT AG COM RCVD / END STAT APP P 11/05/97 DATE ISSUED 08/15/97 DATE EXPIRE 07/31/02 FEE CODE( 6 ) 1=,(>1MGD) , 2= (>10KGD) , 3= (>1KGD) ,'4= (<1KGD+SF) , 5= (S>300A) , 6= (S'<`=300A) 7=(SENDEL),8=(SEDEL),9=(CLREC),0=(NO FEE) DISC CODES 01 ASN/CHG PRM ENG CERT DATE 11/11/11 LAST NOV DATE, / / CONBILL( )' COMMENTS: 1,800 DT/YR. NOV STABILIZATION,TCLP&MONITORING �. MESSAGE: r FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS JUL Me 1999 .a 1 ii�l,ut•ion- /iR'10,i1�:,rsa gle 10-1 dilution 0l 'Sample auo , i.i L r R I t XX ,LACTOSE 24 hr. 48 hr. E C� 24 hr. 48 hr. 10_2 dilution / 1.0 ml. sample X LACTOSE I hr. 48 hr.. -FINAL FINAL X' LACTOSE 24 hr. 48 ' hr.- E C 24 hr. F48 hr. FINAL Batch Production Dates. Date Test Performed Time. Z: OO P P1 Operator' I.s o %.solids MPN of total solids = (� MPNI from table (8M 13...9-50) . 11 x % solids RECEIVED -.fill to logo WATER QUALITY SECTION . Non-DIschargo Compliance c-' FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS 10 1 dilution / 10 ■l sample. 10-1 dilution / 1.0 al sample I XX LACTOSE 24 hr. 48 hr. E C 24 hr. 48 hr. 10 — dilution / 1.0 ■1 sample FINAL. X LACTOSE £4 hr. 48 hr. 1— . 124E C . hr. 48 hr. Batch Production Dates: Dat T t P f d 2- f FINAL Ti■ Ope % S So MPN MPN r e es er orme ator of total solids = from table (SM n. 9-50) FINAL FECAL COLIFORM,FOR MUNICIPAL BIOSOLIDS _�l 1 dilution / 10-■1 sample 10-1 dilution / 1.0,ml .sample. XX -LACTOSE 24 Fir. 48 hr. r' r� X LACTOSE 4 hr. 48hr. E C 124 hr. 48 hr. FINAL . X LACTOSE 24 hr, E hr. ---------7 E C 24 hr'. 48 hr. FINAL -Date Test.Performed FINAL Time Operator % Solids -- MPN of total.solids MPN from table (SM p.--9-50) FECAL COLIFORM FOR'MUNICIPAL BIOSOLIDS 10-1 dilution % 10 ■1 sample 10-1.dilution 1 1.0 m'l sample 10-2 dilution.:./ 1.0 ■1 sample. Batch Production .Dates:.. Date Test Performed X LACT05E E C' FINAL ` -Tine 24 hr. 48 hr.- 24 hr. 48 hr. Operator.. % Solids MPN of total'. solids V r, MPN from table. -(SM P. 9=50) 11 X % solids FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS dilution / 10 ■l sample 10-1 dilution./ 1.0 ml sample I XX LACTOSE 24 hr. 48 hr. E C 24 hr. 48 hr. FINAL X LACTOSE 24 hr. 48 hr. -E C 24 hr. 48 hr. FINAL Date Test Performed FINAL Time Operator X Solids S MPN of total solids MPN from table (SM a 9-50) 11 u 'X snI irla . E C 24 hr. 48 hr. FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS 10 1 dilution / 10 ml sample 10-1 dilution I / 1.0.ml sample XX LACTOSE 24 hr. 48 hr. 10 2'dilution / 1.0 al sample Batch Production Dates: Date Test Performed X LACTOSE E C FINAL. Time 24 hr. 48 hr. 24 hr. 48 hr. Operator c,� a J % Solids � / /f FINAL. X LACTOSE '24 fir. 48 hr. E C 24 hr. 48 hr. MPN of total solids = MPN from table (SM p. 9-50) 11 x % solids- FECALCOLIFORM FOR MUNICIPAL BIOSOLIDS _d 1 dilution / 10 a1 sample.. 10-1 di.lutiom / 1.0.m1 sample 10 2 dilution / 1.0 ml sample, Batch Production Dates: FECAL.COLIFORM FOR.MUNICIPAL BIOSOLIDS is ;_I dilution / 10 al sample 10 1 dilution / .1.0 ml sample•' 10-2-dilut-ion / 1.0•■1 sample Batch Production Dates: .FINAL 10_Z dilution /." 1.0 ■.1 sample Batch Product,i`on Dates: FECAL,COLIFORM-FOR MUNICIPAL--BIOSOLIDS dilution./ .10 ml- sample I 10-1 dilution / 1,.0 ml' saimple FINAL 1 10_p dilution / 1.0 ■1,sample Batch Production Dates:' FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS*- ad-1.dilution / 10 ml sample 10-1 dilution / 1.0 m1 sample . I :FINAL 10-2 dilution /..1.0 ■l sample Batch Production Dates: •4 g 4 hr. E;•. hr. Date Test Performed. _ h .FINAL Time . �S Operator. Q X Solids rd MPN of total'_solids .MPN'from table (SM p..9-50) -11 u .ti en7;r1� FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS 10 1 dilution 110 ■1 sample 10. dilution '/ 1.0 1.sample FINAL , 10 2 dilution / 1A 41 .sample Batch Production Dates 1 n, -4- Ts.} Dn"fnJMMnd I L R Pasteuriztion vessel operates on a constant speed with an in/out time duration of 30 minutes. MINIMUM MINIMUM DATE 2 HOUR pH 24 HOUR pH TEMP IN TEMP OUT 07101 /98 12.40 12.32 145 144 07/02/98 12.34 12.26 152 155 07/06/98 12.33' 12.21 153 157 07/07/98 12.32 12.23 150 148 07/08/98 . 12.37 12.25 156 158 . 07/09/98 12.21 12.17 . 158 .148 07/10/98 12.38 12.32 151 157 . 07/13/98 12.31 12.25 151 153 . 07/14/98 12.41 12.37 .158 158 07/15/98 12.33 12.26 152 156 07/16/98 12.32 - 12.26 156 159 . 07/17/98 12.37 12.30 154 133 07/20/98 12.37 12.32 161 157 07/21 /98 12.14 12.11 160 156 07/23/98 12.20 12.14 160 165 07/24/98 12.22 12.18 157 157 08/07/98 12.27 12.22 166 161 08/08/98 12.30 12.26 162 167 .08/10/98 12.24 12.18 1,58 138 08/11 /98 12.38 12.33 158 158 08/12/98 . 12.41 12.32 159 160 08/13/98 12.30 12.21 160 172 08/14/98 12.26 12.18 172 173 08/17/98 12.28 12.22 158 157 08/18/98 12.34 12.28 158 134 08/19/98 12.36 12.31 158 154 08/20/98 . . 12. 32 12.29 160 150 08/21 /98 12.28 12.22 158 140 08131 /98 1.2.38 12.33 159 161 09101 /98 12.30 12.25 160 150 09/02/98 . 12.34 - 12.26 159 164 09/03/98 -. 12.29 . 12.19 164 165 09/04/98 12.31 12.24 .158 _ 159 09/08/98 .1.2.34 12.28 160 169 09/09/98 .12.37 12.30 158 148 09/10/98- 12.35- . 12.18- .159 143 09/11/98 12:20 12.11 159 161 : 09/14/98 .12.35 12.29 158. 160 09/15/98 12: 33 12.26 158 162 . 09/16/98 . 12.29 12.24 158 A60 09/17/98 - .1.2.34 - 12.30 158` 156 09/18/68 12.29 ".: 12:22 154 155 - 09/21 /98 12.33 12.28 , 09/22/98 . .: ;12.22 12.17 159 . 160 09/23/98 1.2.31... 12.27 158 . 151 .09/24/98. ' 12.28 . 12.22 16.1 152 09/25/98 - 12.19 12.12 159 150 09/28/98 12.18 12.12 160 152 -09/29198 12.08 12.05 158 160 - 09/30/98 12.34. 12.21 160 154 Pasteuriztion vessel -operates on a constant speed with an in/out time duration of 30 minutes. MINIMUM MINIMUM DATE 2 HOUR pH 24 HOUR pH TEMP IN TEMP OUT' " 04/01/98 12.18 12.10 161• 158 04/02/98 12.30 . 12.22 158 159 04/03/98 12.25 12.19 140 146 04/07/98 .12.68 .12. 02 158 158 04/08/98 12.07 12.03 158 160 04%09/98 12.12 12.09 -158 158 04/ 10/98 12.16 . 12.12 158 159 04/14/98 12.18 .12.13 158 159 04/15/98 > . 12.17 12.1-1 158. 158. 04/16/98 .12.20' 12.16 160, 157 04/17/98 12.11 - 12.08 158 159 04/20/98 12.18 12.12 158 ' 160-'. 04/21 /98 12.20 12.16 158 158 04/22/98 12.22 12.16 158 159 04/23/98 12.14 12.10 156 158 04/24/98 12.10 12.03 99 158 04/27/98 12.18 12.11 160. , 159 04/28/98 -12.22 12.17 158 158 04/29/98 12.18 12.13 .: 158 163 04/30/98 12.27 12.21 158; 142 05/01/98. 12.18 12.10 158'' 158 05/04/98 12:08 12.06 '160 158 05/05/98 12.22 12.18, 160 158 05/06/98 12.17- 12.14 160 158 05/08/98 . 12.26 12.20 158 158 05/11 /98 12.16 .12.10 158 158 05/12/98, 12.19 12.14 158, 158 05/13/98 12.28 12.19 153 148 05/14/98 12.21 12.16 152 .145 ' 05/15/98 12.27 ,. 12.20 145 150 05/18198 12.22 12.16 155 . 156 05/19/98 12.30 12.22 148 151 05/20/98 12.23 12.20' 144 121 05/21/98 12.19 12.12 163 151 05/22/98 12.28 12.21 156 155 05/25/98 .12.20 12.15 150 147 05/26/98 12.21 12.16 157, 147 05/27/98 12.18 12.14 146 '147 05/28/98 12.12 • 12.09 139 138 06/01/98 12.14 12.1.0 150 - 153 06/02/98 12.31 12.26 144 151. 06/03/98 1218 , 12.24 156 153 06/04/98 12.22 12.15 149 158 06/05/98 . 12.19 12.15 145 132 06/08/98 12.31 12.26 144 137 06/09/98 .. ' 12.29 12.23 149 : 149. . - 06/`t 0/98 12.27 12.23 145 151 06/ 11 /98 12.20 : 12.15 146'* 146 06/12/98 ~ 12.27 12.21 145 147 06/15/98 12.26 --.12.20 142 147 06/16/98 _ 12.42 . ' 12.34. 147 1.50 06/1.7/98 12.38 ' 12.31 142 145 06/18/98 `12.-29 `. 12.23 141 - 143 06/19/98 12.42 12.34 148 138 06/22198. 12.39 12.'36 ' 146 151 06/24/98 12.56 1.2. 49 157 153 06/25/98 12 A4 12.40 156 164 06/26/98 -12.38 - 12.29 157 156 06/29/98 .12.22 12.17 145 154 06/30/98 12;31 12.25 150. i 140. e Pasteuriztion vessel operates on a constant speed vvith an in/Out time duration �� of 30 minutes. INiINIIVIUldi i'viiia''MU 1 MATE; 2 HOUR pH 224 FOUR pH TEMP" IN I CIIAP OUT 01 /02/98 12.22 12.16 162 162 . 01, 05f 98 12. C6 12. 01 160 158 01 /06/98 12.15 2.10 158 i 58 01 /07f98 - 121.09 12.04 158 158 011A4,198 12.12 12.1 ^v 158 158 0414 5f98 12.07 12.03 158 161 011,16/98 12.09 12.0A 158 i 58 01/20/98 12.19' 1 12.12 153 158 01'21198 12.24 i 2.19 i 58 158 01 f22/98 12.16 12:10 158 158 G 1 /201 12.2 1 12.14 _ 158 .159 01f26/98 12.26 12.18 15S 161 01 /27/98 12.20 12.11 158 158 01 /28/98 12.18 12.12 1.58 160 G 1 /29/98 12: 14 12.12 1 O 158 01 /3C/98 12.18 12.11 158 153. 02/02198 12.25 12.18 158 158 02f03r,98 12.20 12.14 158 158 OZ'04f98 12.15; 12.10 158 15-8 02'05/98 12.1.1 12.08 159 159 GZ'06/98 12.15 12. G9 158 158 02109f98 12.26 111 158 458 02/10/98 12.28 12.19 158 158 OZf11f98 12.1 12.14 158 160 02/12/98 12.16 I L.10 158 158 02/13, . 12.24 12:16 158 158 G2/i.7/98 '12.14 12.09 158 158 0111 98 12:24 12.17 159 158 12. i 9 12.13 153 158 n02119198 ' 02/40/98 12.15 � 1.2.11 159 158 - G2I23/9p8 i2.2 i i2.15 158 158 G2/24198 12.27, 121.2G 4158 158 . 02/25/98 i2.I 12.G8 15^v 152 03102M 12.16 12.11 158 163 03/03/98 12.19 12.13 158 1001 03f04/98 12.22 12.18 163 158 03/05/98 i 2.26, 12.20 158 158 03,106,198 12.20 12.14 ... 158 158 03/09/98 12.1 c6 12.12 158 155 03/12/98 12:17 12.1.0, 158 158_ 03' 6/�$ 12.Go :. 12.0 i i6 i 16 i . C3f17f98" . 12.11 12.06 158 160' .. 03/18195 . 12:1 12.00 - 158 158 . 03f19/98 _ 12.07 12.04 158 158 03/23/98 .. 12.09 . 12.03 158 i 5S 03/24/58 12.20 12.12 .. 158. 158 03i25198. i2.1-5- 12.10 158 158 03/26198: : •12.09 12.06 158 159 03/27/98 12:03 12.OG 150 158 03/30198 12.20 12.14 158 158 03/3. i /98 12.28 12. 22 158 158 Pasteuriztion vessel. operates on a constant speed with an irdout time duration of 30 minutes. MINIMUM MINIMUM DATE 2 HOUR pH 24 HOUR pH TEMP IN TEMP OUT 10/06/98 12.26 12.17 158 155 10/07/98 12.22 12.18 160 157 10/08/98 12.27 12.21 159 121 10/09/98 12.31 12.22' 158 160 10/12/98 2.28 12.21 158 136 10/13/98 12.26 12.19 158' 132 10/14198 12.30 12.18 158 160 10/15/98 . 12.28 12.16 158 138 10/16/98 12.34 12.22 156 156 10/19/98 . 12.28 12.22 158 138 10/20/98 12.24 12.18 161 156 10/21 /98 12.24 12.20 158 123 10/22/98 12.16 12.12 158 90 . 10/23/98 .12.20 12.16 166 120 10/26/98 12.30 12.25 158 153 10/27/98 12.22 12.18 158 151 .10.128198 12.31 12.23 .160 151 10/29/98 12.18. 12.12 158 110 ' 11/02/98 12.34 12.29 158 158 11 /03%98 12.35 12.29 158 154 11 /04/98 12.26 12.19 158 153 11/05/98 12.29 '12.24 158 145 11 /06/98 12.32 12.22 161 150 11/09/98 :. 12.37 " 12.23 158 159 11 /10/98 12:25 12.19 158 158 11 /11 /98 12.23 12.20 158 142 11/12/98 12.21 12.22 158 156 11 /13/98 12.21 12.15 164 158 11 /16/98 12.25 12.19 158 . 157 11 /17/98 .12.28 12.22 158 164 11 /18198 12.30 12.24 145 135 11 /19/98 12.28 12.23 158 153 11 /20/98 12.29 12.21 158 167 11 /23/98 12.31 12.25 158 162 11/24/98 12.28 12.22 158 151 12l01 /98 12.21 12.17 1.47 147 12/02/98 12.22 12.17 143 144 12/03/98 12.28 12.1.9 150 112 12/04/98 . 12.22 12.18 161 .160 12/05/98 . 12:30 12.22 152 153 12/06/98 12.19 12.15 158 156 12/07/98 ;12.22. '12.18 158 148 12/08/98 . 12.17 12.15 158 152 12/09198 12.24 12.19 158 96 12/10/98 . 12.42 12.37 160 153 12/11 /98 12.30. 12.23 146 126 12/14/98 12.36 12.27 152 1.55 12/15/98 12.24 12.19 145 150 12/16/98 12.23 12.18 152 151 12/17/98.' 12.29 12.25 158 142 12/18/98 12.20 12.12 145 146 12/21 /98 ::12.12 : 12:09 161 145 12/22/98 12.20 12.09 158 100 12/29/98 12.31. .12.28 158 156 . 12/30/98 '12.28 12.22 158 155 12/31/98 12:27' '12.20 152 154 Davis & Brown PO Box 15038 Quinby, SC 29506 (803) 665-6746 FAX: (803) 629-1444 Certificate of Analysis Client: CHERAW, CITY OF South Carolina Certification Number: 21117 P.O.BOX I I I CHERAW, SC 29520 Client #: 168 Receipt Date: 11-Mar-99 Contact: SHERRY LEBEL Report Date: 12-Apr-99 Sample Date: 10-Mar-99 SDG #: SDG-009504 Approved By: Van Ward Lab Director Reporting Parameter Result Limit Unit Method Flag Date Time Analyst LSID-021475 1009-Z Cyanide <0.010 0.01 mg/L EPA 335.2 3/17/99 14:06 TL LSID-021476 1010-Z Cyanide <0.010 0.01 mg/L EPA 335.2 3/17/99 14:06 TL LSID-021477 1011-Z Cyanide <0.010 0.01 mg/L EPA 335.2 3/17/99 14:06 TL LSID-021478 3-5-99-204 Aluminum, Total 0.070 0.02 mg/1 EPA 202.2 3/19/99 11:30 DH Acid Digestion (Liquids) YES EPA 4.1.4 3/15/99 14:00 DH LSID-021479 ., ` 3-8-99-200 TCLP PASS P/F 3/26/99 11:23 SF Nitrogen, Nitrate- IC 635 48.5 mg/kg EPA 300.0 D 3/18/99 12:11 SM Nitrogen, Nitrite- IC <121 48.5 mg/kg EPA 300.0 D 3/18/99 12:11 SM Nitrogen, Ammonia 578 98 mg/kg EPA 350.3 D 4/8/99 14:30 NW Acid Digestion (Solids) YES SW846 3050A 3/22/99 9:00 DH Percent Moisture 60.0 0.1 wt% SW846 3540 3/23/99 17:00 LM Aluminum, Total 9550 0.397 mg/kg SW846 6010A D 4/6/99 12:00 DH Page 1 Davis & Brown PO Box 15038 Quinby, SC 29506 (803) 665-6746 FAX: (803) 629-1444 Certificate of Analysis Client: CHERAW, CITY OF South Carolina Certification Number: 21117 P.O.BOX 111 CHERAW, SC 29520 Client #: 168 Receipt Date: 11-Mar-99 Contact: SHERRY LEBEL Report Date: 12-Apr-99 Sample Date: 08-Mar-99 SDG #: SDG-009504 Approved By: Van Ward Lab Director Reporting Parameter Result Limit Unit Method Flag Date Time Analyst Arsenic, Total 5.18 0.1 mg/kg SW846 6010A D 3/23/99 15:00 DH Cadmium, Total <0.990 0.397 mg/kg SW846 6010A D 3/23/99 17:49 DH Chromium, Total 60.0 0.397 mg/kg SW846 6010A D 3/26/99 11:16 DH Copper, Total 95.0 0.993 mg/kg SW846 6010A .D 3/23/99 17:49 DH Lead, Total 5.93 0.1 mg/kg SW846 6010A D 3/23/99 9:30 DH Molybdenum, Total 3.18 0.497 mg/kg SW846 6010A D 4/1/99 10:41 DH Nickel, Total 29.5 0.993 mg/kg 'SW846 6010A D 3/23/99 17:49 DH Zinc, Total 88.8 0.993 mg/kg SW846 6010A D 3/23/99 17:49 DH Mercury, Total <0.25 0.1 mg/kg SW846 7470A D 3/17/99 14:10 ROBI Selenium, Total 0.15 0.04 mg/kg SW846 7741 D 3/31/99 15:00 DH PCB BDL 1.6 mg/kg SW846 8080 S10 3/18/99 20:23 KLEP Page 2 . CHAIN OF CUSTODY RECORD Page J__ of Client T Name / Facility Name. rn SAMPLE ANALYSIS REQUIRED (x) -use remarks area to specify specific compounds or methods m o la la z o c 0. o y c A a` m Col17ted By:, L � "y JAM SAMPLE ID DATE TIME 3bo 0 1 - z 3.716- 9 p it 3-4 = T,T _LL_ R7�sh y: Date Time Receiv by R/elinpplUl shed by. / Date Time o Re !Ived y lab by: r+' * Program Area: N - NPDES, H.- Haz. Waste, D - Drinking Water, G - Groundwater, O. - Other, W - Waste Water a . DAVIS & BROWN-A.C. P.O. Box 15038 Quinby, SC 29506 (803) 665-6746 2121 Black Creek Road Florence, SC 29501 Use For Pin the boxes to indicate whether sample wasfiltered and/orpreseraed. Remarks Lab ID o /i i r'LGI I U i6, t/�rltl/cf�rr r f -�l Lf' Relinquished by: Date Time Received by: Date Time Circle One ICED YES NO Remarks - State of North Carolina Department ,of Environment, Health and .Natural Resources Division of Water Quality James B. Hunt; Jr., Governor Wayne McDevitt; Secretary A. Preston Howard, Jr., P.E., Director James T. Morris; Public Utility Director Town of Cheraw Post Office Box 111 Cheraw, South,Carolina 29520 Dear Mr. Morns: August 15, 1997 1 AUG 2 0 1991 FAYETTEVILLE REQ. 0FRCE Subject: Permit No .WQ001=4248 To no f Chem., . Distribution offass AWastewater Residuals , f, - esterfreldyCoun South Carolina In accordance with,your application received on August, 7, 1997; we are forwarding herewith Permit No.,WQ0014248, dated August 15, 1997, to the Town of Cheraw for the distribution of Class A residuals in North Carolina. This permit shall be effective from'the date of issuance until July 31, 2002, and shall be subject to the conditions, and limitations as specified therein. Please pay particular attention to the monitoring and, reporting requirements contained in this permit.. Failure to establish an adequate: system for collecting, and maintaining the required operational information will result in future 'compliance problems. If any parts, requirements, or limitations contained in this permit are unacceptable, you. have the right to request an adjudicatory hearing upon written request within thirty (30) days following receipt of this permit. This request must be in the form of a written petition, conforming to Chapter 150B of North Carolina General Statutes, and filed with the Office of Administrative Hearings, P.O. Drawer 27447, Raleigh, NC 27611-7441. Unless such demands are made this permit shall be final and binding. - If you, need additional information concerning this mattes;, please contact Mr. Michael D. Allen at (919)' 733-5083 extension 547.' = Sincerell L �A. Preston Howard, ,Jr., P.E. cc: NCDWQ Regional Offices, Water Quality Section Facilities Assessment Unit P.O. Box, 29535, Raleigh-, North Carolina 2762&0535 • Telephone (919) 733-5083 FAX (919) 733-0719 An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES RALEIGH PERMIT FOR THE DISTRIBUTION OF CLASS A RESIDUALS In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, and other applicable Laws, Rules, and Regulations PERMISSION IS HEREBY GRANTED TO THE Town of Cheraw Chesterfield County, South Carolina FOR THE the distribution of up to 1,800 dry tons per year of Class A wastewater residuals in North Carolina from the sources listed in Condition II 1, with no discharge of wastes to the surface waters, pursuant to the application received on August 7, 1997, and in conformity with the project plan, specifications, and other supporting data subsequently filed and approved by the Department of Environment, Health and Natural Resources and considered a part of this permit. This permit shall be effective from the date of issuance until July 31, 2002, and shall be subject to the following specified conditions and limitations: I. PERFORMANCE STANDARDS 1. The distribution of Class A residuals program shall be effectively maintained and operated as a non -discharge system to prevent the discharge of any wastes resulting from the operation of this program. 2. This permit shall become voidable in the event of failure of the residuals program to adequately protect the assigned water quality standards of the surface waters and groundwaters. 3. The issuance of this permit shall not relieve the Permittee of the responsibility for damages to surface or groundwaters resulting from the operation of this program. 4. In the event that the residuals program is not operated satisfactorily, including the creation of nuisance conditions, the Permittee shall take any immediate corrective actions as may be required by the Division. 5. When wastewater residuals are sold or given away, one of the Class A pathogen requirements in 40 CFR Part 503.32(a) and one of vector attraction reduction requirements in 40 CFR Part 503.33 must be met. Additionally, an evaluation must be performed which demonstrates the residuals ability to comply with this requirement. Upon request, a copy of this evaluation must be submitted to the Assistant Chief, Technical Support Branch, Division of Water Quality, Post Office Box 29535, Raleigh, NC 27626-0535. II: OPERATION AND MAINTENANCE REQUIREMENTS 1. No residuals .other than the following are hereby approved for distribution in accordance with this permit: Permit Volume Source County Number (Dry Tons/Year) Town of Cheraw Chesterfield, SC SCO020249 1,800 2. The finished product shall not be stored at, the land application sites unless it is placed on a concrete pad, placed under shelter -or covered until such time as it is land applied. If an alternate storage site is to be used, approval must be obtained from the Division of Water Quality. 3. No other residuals other than those specified under Condition II 2 above may be distributed. The Permittee shall request and obtain a permit amendment from the Division of Water Quality for each additional residual source prior to acceptance of that residual. 4. For a Class A residual to be sold or given away in bags or other container for application to the land, the following must be satisfied: The Ceiling Concentrations (Dry Weight Basis) and the Pollutant Mon_ thly Average Concentrations (Dry Weight Basis) must .be maintained: Ceiling Monthly Average Concentrations Concentrations Parameters mg/kg mg/kg Arsenic 75 41 Cadmium 85 39 Copper 4,300 1,500 Lead 846 300 Mercury 57 17 Molybdenum 75 ---- Nickel 420 420 Selenium 100 100 Zinc 7,500 2,800 5. Adequate provisions shall be taken to prevent wind erosion and surface runoff from conveying pollutants from the residuals treatment area onto the adjacent property or into any surface waters. 6. A label shall be affixed to the bag or other container in which residuals that are sold or given away for application to the land, or an information sheet shall. be provided to the person who receives the residuals sold or given away in an other container for application to the land. The label or information sheet shall contain the following information: a. The name and address of the person who prepared the residuals that is sold or given away in a bag or other container for application .to the land. b. A statement -that application of the residuals to the land is. prohibited except in accordance with the instructions on the label or information sheet. C. A statement which identifies that this material shall be prevented from entering any public or private water supply source (including wells) and -any stream, lake, or river. d. Residuals shall not be applied to. any site that is flooded, frozen or snow-covered. K e Adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored residuals into any surface waters. MONITORING AND REPORTING REQUIREMENTS 1. Any monitoring (including groundwater, surface water, residuals, soil, or plant tissue analyses) deemed necessary by the Division of Water Quality to insure protection of the environment will be established and an acceptable sampling and reporting schedule shall be followed. 2. Proper records shall be maintained by the Permittee tracking all residual activities. These records shall include, but are not necessarily limited to the following information: a. source, volume and analysis of each residuals b. name of residuals' recipient, volume received, and intended use 3. A residual analysis shall be conducted annually from the date of permit issuance by the Permittee. The results of all analysis shall be maintained on file by the Permittee for a minimum of five years. The residuals analysis shall include the following parameters: Arsenic Molybdenum Cadmium Nickel Copper Selenium Lead Zinc Mercury Aluminum pH Ammonia -Nitrogen Phosphorus Calcium Plant Available Nitrogen (by calculation) Magnesium Potassium Nitrate -Nitrite Nitrogen Sodium % Total Solids TKN 4. A Toxicity Characteristics Leaching Procedure (TCLP) analysis shall be conducted by the Permittee annually. The TCLP analysis shall include the following parameters (please note the regulatory level in mg/L in parentheses): Arsenic (5.0) Benzene (0.5) Carbon tetrachloride (0.5) Chlorobenzene(100.0) Chromium (5.0) m-Cresol (200.0) Cresol (200.0) 1,4-Dichlorobenzene (7.5) 1,1-Dichloroethylene (0.7) Endrin (0.02) Hexachlorobenzene (0.13) Hexachloroethane (3.0) Lindane (0.4) Methoxychlor (10.0) Nitrobenzene (2.0) Pyridine (5.0) Silver (5.0) Toxaphene (0.5) 2,4,5-Trichlorophenol (400.0) 2,4,5-TP (Silvex) (1.0) Barium (100.0) Cadmium (1.0) Chlordane (0.03) Chloroform (6.0) o-Cresol (200.0) p-Cresol (200.0) 2,4-D (10.0) 1,2-Dichloroethane (0.5) 2,4-Dinitrotoluene (0.13) Heptachlor (and its hydroxide) (0.008) Hexachloro-1,3-butadiene (0.5) Lead (5.0) Mercury (0.2) Methyl ethyl ketone (200.0) Pentachlorophenol (100.0) Selenium (1.0) Tetrachloroethylene (0.7) Trichloroethylene (0.5) 2,4,6-Trichlorophenol (2.0) Vinyl chloride (0.2) 3 5. All residuals included in this permit must be monitored annually, from the date of permit issuance, for compliance with condition 19 of this permit. Data to verify stabilization of the residuals must be maintained by -.the Permittee. The required data is specific'to the stabilization process, utilized, but should be sufficient to clearly demonstrate compliance with the Class A pathogen requirements in 40 CFR Part 503.32(a) and the vector attraction reduction requirements in 40 CFR Part 503.33. In addition, -the EPA. certification statements concerning compliance with pathogen requirements, vector attraction reduction requirements and management practices must be completed annually by the proper authority or authorities if more than one is involved, either the person who generates the residuals or the person who prepares the residuals to be sold or given away. 6. Three copies, of all required monitoring and reporting requirements as'specified in conditions 1111, III 2,1113;11I 4, and III 5 shall be submitted annually on or before March 1 of the "following year to the following address: NC Division of Water Quality Water Quality Section , Facility Assessment Unit PO Box 29535 Raleigh, NC 27626-0535 7. Noncompliance Notification: The Permittee 'shall report by telephone to the appropriate DWQ Regional Office (as outlined in attachment 1) as soon -as possible, but in no case more than 24 hours or on the next working day following the occurrence or first knowledge of the occurrence of any of the following: a. Any occurrence with the distribution program which results -in the land application of significant amounts of wastes which are, abnormal in quantity, or characteristic. b. Any failure of the distribution program resulting in a release of material to receiving waters. c. Any time that self -monitoring information indicates that the facility has gone out of compliance with the conditions and limitations of this permit or the parameters on which the system was designed. d. Any process unit failure, due to known or unknown reasons, that render the facility incapable of adequate residual treatment. e. Any spillage or discharge from a vehicle or piping system during transportation of residuals. Persons reporting such occurrences by telephone shall also file''a written report in letter form within five (5) days following first knowledge of the'occurrence. This report must outline the actions taken or proposed to be taken to ensure that the problem does not recur. IV. INSPECTIONS 1. Any duly authorized officer, employee, or representative of the Division of Water Quality' may, upon presentation of credentials, enter and inspect any property, premises or place on or related to the treatment site or facility at any .reasonable time for the purpose of determining compliance with this permit; may inspector copy any records that must be kept under the" terms and conditions of this permit; and may obtain samples of groundwater, surface .water, or.leachate.' 4 2. The Permittee or his designee shall inspect the residuals storage, transport, and treatment facilities to prevent malfunctions and deterioration, operator errors and discharges which may cause or lead to the release of wastes to the environment, a threat to human health, or a nuisance. The Permittee shall maintain an inspection log or summary including at least the date and time of inspection, observations made, and any maintenance, repairs, or corrective actions taken by the Permittee. This log of inspections shall be maintained by the Permittee for a period of five years from the date of the inspection and shall be made available to the Division of Water Quality or other permitting authority, upon request. V . GENERAL CONDITIONS 1. This permit shall become voidable unless the distribution activities are carried out in accordance with the conditions of this permit, the supporting materials, and in the manner approved by this Division: 2. This permit is effective only with respect to the nature and volume of residuals described in the application and other supporting data. 3. This permit is not automatically transferable. In the event that there is a desire for the facilities to change ownership or a name change of the Permittee, a formal permit request must be submitted to the Division of Water Quality accompanied by an application fee, documentation from the parties involved, and other supporting materials as may be appropriate. The approval of this request will be considered on its merits and may or may not be approved. 4. Failure to abide by the conditions and limitations contained in this permit may subject the Permittee to an enforcement action by the Division of Water Quality in accordance with North Carolina General Statute 143-215.6(a) to 143-215.6(c). 5. The annual administering and compliance fee must be paid by the Permittee within thirty (30) days after being billed by the Division. Failure to pay the fee accordingly may cause the Division to initiate action to revoke this permit as specified by 15 NCAC 2H .0205 (c)(4). 6. The issuance of this permit does not preclude the Permittee from complying with any and all statutes, rules, regulations, or ordinances which may be imposed by other government agencies (local, state, and federal) which have jurisdiction. 7. The Permittee, at least six (6) months prior to the expiration of this permit, shall request its extension. Upon receipt of the request, the Commission will review the adequacy of the facilities described therein, and if warranted, will extend the permit for such period of time and under such conditions and limitations as it may deem appropriate. 8. This permit may be modified, or revoked and reissued to incorporate any conditions, limitations and monitoring requirements the Division of Water Quality deems necessary in order to adequately protect the environment and public health. Permit issued this the fifteenth day of August, 1997 NORTH C INA ENAOAL MANAGEMENT COMMISSION Preston Howard, Jr., P.E., Director Division of Water Quality By Authority of the Environmental Management Commission Permit Number WQ0014248 5 ATTACHMENT 1 DIVISION OF WATER QUALITY REGIONAL OFFICES Asheville Regional' WQ Supervisor 59'Woodfin Place Asheville, NC 28801 (704)25.1-6208 Fax (704) 251-6098 Avery Macon Buncombe Madison Burke McDowell Caldwell Mitchell Cherokee Polk Clay Rutherford Graham Swain Haywood Transylvania Henderson Yancy Jackson Fayetteville Regional WQ Supervisor Wachovia Building, Suite 714 Fayetteville, NC 28301 (910)486-1541 Fax (9,10) 486-0707 Anson Moore Bladen Robeson Cumberland Richmond Harnett Sampson Hoke Scotland Montgomery Winston-Salem Regional WQ Supervisor 585 Waughtown Street Winston-Salem, NC 27107 (910)771-4600 Fax (910)771-4631 Alamance Rockingham Alleghany Randolph Ashe Stokes Caswell Surry Davidson Watauga Davie Wilkes Forsyth Yadkin Guilford Washington Regional WQ Supervisor 943 Washington Square Mall Washington, NC 27889_ (919) 946-6481 Fax (919) 975-3716 Beaufort Jones Bertie Lenoir CamdenMartin Chowan Pamlico Craven Pasquotank Cumtuck Perquimans Dare . Pitt Gates Tyrell Greene Washington Hertford Wayne Hyde Mooresville Regional WQ Supervisor 919 North Main Street Mooresville, NC 28115 (704).663-1.699 Fax (704).663-6040 Alexander Lincoln Cabarrus Mecklenburg Catawba Rowan Cleveland Stanly Gaston Union Iredell- Raleigh Regional.WQ Supervisor Post Office Box 27687 Raleigh, NC 27611 (919) 571-4700 Fax (919) 571-4718 Chatham Nash Durham Northampton Edgecombe Orange Franklin Person Granville Vance Halifax Wake Johnston Warren Lee Wilson Wilmington Regional WQ Supervisor 127 Cardinal Drive Extension Wilmington, NC 2840.5-3845 (910) 395-3900 Fax (910)350-2004 Brunswick New Hanover Carteret Onslow Columbus Pender Duplin '. Electronic Code of Federal Regulations (e-CFR) (e-CFR Data is current as of March 20,,2007 J ... Title 40: Protection of Environment PART 503-STANDARDS FOR THE USE OR DISPOSAL OF SEWAGE SLUDGE Section Contents Subpart A-General'Provisions § 503.1 . Purpose and applicability. § 503.2 Compliance period. § 503.3 Permits and direct enforceability. § 503.4 .Relationship to other regulations. § 503; 5 Additional or more stringent requirements. § 503.6. Exclusions., § 503.7 Requirement for a person who prepares'sewage sludge. § 503.8 Sampling and analysis. § 503.9 General -definitions. Subpart B=Land Application § 503.10 Applicability,. § 503.11 Special definitions. § 503.12 General requirements-. § 503.13 Pollutant limits. § 503.14 Management practices. § 503.15 Operational standards -pathogens and vector, attraction reduction. § 503.16 Frequency of monitoring. § 503.17 Recordkeeping. § 503.18 Reporting. Subpart C=Surface Disposal § 503.20 Applicability. § 503.21 Special definitions. § 503.22 General requirements. § 503.23 Pollutant limits_ (other than domestic septage). § 503.24 Management practices. § 503.25 Operational standards -pathogens and vector attraction reduction. § 503.26 Frequency of monitoring. § 503.27 Recordkeeping. § 503.28 Reporting. Subpart D-Pathogens and Vector Attraction Reduction § 503.30 Scope'. § 503.31 Special definitions.' § 503.32 Pathogens. § 503.33 Vector attraction reduction. Subpart E-Incineration § 503.40 Applicability. § 503.41 Special definitions. § 50142 General requirements. § 503.43 Pollutant limits. § 503.44 Operational standard -total hydrocarbons. § 503,45 Management practices. § 503.46 Frequency of monitoring. § 503.47 Recordkeeping. § 503-48 Reporting. Appendix A to Part 503=Procedure To Determine the Annual Whole Sludge Application Rate for a Sewage Sludge Appendix B to Part 503-Pathogen Treatment Processes a V PART 503—STANDARDS FOR THE USE OR DISPOSAL OF SEWAGE SLUDGE Authority: Sections 405 (d) and (e) of the Clean Water Act, as amended by Pub. L. 95-217, sec. 54(d), 91 Stat. 1591 (33 U.S.C. 1345 (d) and (e)); and Pub. L. 100-4, title IV, sec. 406 (a), (b), 101 Stat., 71, 72 (33 U.S.C. 1251 et seq. ). Source: 58 FR 9387, Feb. 19, 1993, unless otherwise noted. Subpart A —General Provisions § 503.1 Purpose and applicability. (a) Purpose. (1) This part establishes standards, which consist of general requirements, pollutant limits, management practices, and operational standards, for the final use or disposal of sewage sludge generated during the treatment of domestic sewage in a treatment works. Standards are included in this part for sewage sludge applied to the land, placed on a surface disposal site, or fired in a sewage sludge incinerator. Also included in this part are pathogen and alternative vector attraction reduction requirements for sewage sludge applied to the land or placed on a surface disposal site. (2) In addition, the standards in this part include the frequency of monitoring and recordkeeping requirements when sewage sludge is applied to the land, placed on a surface disposal site, or fired in a sewage sludge incinerator. Also included in this part are reporting requirements for Class I sludge management facilities, publicly owned treatment works (POTWs) with a design flow rate equal to or greater than one million gallons per day, and POTWs that serve 10,000 people or more. (b) Applicability. (1) This part applies to any person who prepares sewage sludge, applies sewage sludge to the land, or fires sewage sludge in a sewage sludge incinerator and to the owner/operator of a surface disposal site. (2) This part applies to sewage sludge applied to the land, placed on a surface disposal site, or fired in a sewage sludge incinerator. (3) This part applies to the exit gas from a sewage sludge incinerator stack. (4) This part applies to land where sewage sludge is applied, to a surface disposal site, and to a sewage sludge incinerator. § 503.2 Compliance period. (a) Compliance with the standards in this part shall be achieved as expeditiously as practicable, but in no case later than February 19, 1994. When compliance with the standards requires construction of new pollution control facilities, compliance with the standards shall be achieved as expeditiously as practicable, but in no case later than February 19, 1995. (b) The requirements for frequency of monitoring, recordkeeping, and reporting in this part for total hydrocarbons in the exit gas from a sewage sludge incinerator are effective February 19, 1994 or, if compliance with the operational standard for total hydrocarbons in this part requires the construction of new pollution control facilities, February 19, 1995. (c) All other requirements for frequency of monitoring, recordkeeping, and reporting in this part are effective on July 20, 1993. (d) Unless otherwise specified in subpart E, compliance with the requirements in §503.41(c) through (r), 503.43(c), (d) and (e), 503.45(a)(1), (b) through (f), 503.46(a)(1), (a)(3), and (c), and 503.47(f) that were revised on September 3, 1999 shall be achieved as expeditiously as practicable, but in no case -later than -September 5, 2000. When new pollution control facilities must be constructed to comply with the revised requirements in subpart.E, compliance with the revised requirements shall be achieved as expeditiously as practicable but no later than September 4, 2001. ' [58 FR 9387, Feb. 19, 1993, as amended at 64 FR 42568, Aug. 4, 19991 § 503.3 Permits and direct enforceability. (a) Permits. The requirements in this part may be implemented through a permit: (1) Issued to a "treatment works treating domestic sewage", as defined in 40.CFR 122.2, in accordance with 40 CFR parts 122 and 124 by EPA or by a State that has a State sludge management program approved by EPA in accordance with 40 CFR part 123 or 40 CFR part 501 or (2) Issued under subtitle C of the Solid Waste Disposal Act; part C of the Safe Drinking Water Act; the Marine Protection, Research, and Sanctuaries Act of 1972; or the Clean Air Act. "Treatment works treating domestic sewage" shall submit a permit application in accordance with either 40 CFR 122.21 or an approved State program. (b) Direct. enforceability. No person -'shall use or dispose of sewage sludge through any practice for which requirements are established' in this part except in accordance with such requirements. § 503.4 Relationship to other regulations. Disposal of sewage sludge in a municipal solid waste landfill unit, as defined in 40 CFR 258.2, that complies with the requirements in 40 CFR part 258 constitutes compliance with section 405(d) of the CWA. Any person who prepares sewage, sludge that, is disposed in a municipal solid waste landfill unit shall ensure that the sewage sludge. meets the"requirements in 40 CFR part 258,concerning the quality of materials . disposed- in a municipal solid waste landfill- unit. § 503.5 Additional or more stringent requirements. (a) On a case -by -case basis, the permitting authority may impose requirements for the use or disposal.of sewage sludge in addition to or more stringent than the requirements ih.this part when necessary'to protect public health and the environment from any adverse effect of a pollutant in the sewage sludge. (b) Nothing in this part precludes a State or political subdivision thereof or interstate agency from imposing `requirements for the use or disposal of sewage sludge more stringent than the requirements in this part or from imposing additional requirement's for the use or disposal of sewage sludge. § 503.6 Exclusions. (a) Treatment processes. This part does not establish requirements for processes:used to treat domestic sewage or for processes used to treat sewage sludge prior to final use or disposal, except as provided "in, §503.32 and §503.33. (b) Selection of'a use or disposal practice. This part does not require the selection of a sewage sludge -,use or disposal practice. The determination of the manner in which sewage sludge is used or disposed is a local determination. (c) Co -firing of sewage sludge.'This part does not establish requirements for sewage,sludge co -fired in an incinerator with other wastes or for the incinerator in which sewage sludge and -other wastes are co -fired. Other wastes do not include auxiliary fuel, as defined in 40 CFR 503.41(b), fired in a sewage sludge incinerator. (d) Sludge generated at an industrial facility: This part does not establish requirements for the use or disposal of sludge generated at an industrial facility during the treatment of industrial wastewater, including sewage sludge generated during -the treatment of industrial wastewater combined with domestic sewage. (e) Hazardous sewage sludge. This part- does not establish requirements for the use or disposal of sewage sludge determined to be hazardous in accordance with 40 CFR'part 261. (f) Sewage sludge with high PCB concentration. This part does not establish requirements for the use or disposal of sewage sludge with a concentration of polychlorinated biphenyls (PCBs) equal to or greater than 50 milligrams per kilogram of total solids (dry weight basis). (g) Incinerator ash. This part does not establish requirements for the use or disposal of ash generated during the firing,of sewage sludge in a sewage sludge incinerator. (h) Grit and screenings. This part does not establish requirements for the use or disposal of grit (e.g., sand, gravel, cinders, or other materials with'a high specific gravity) or screenings (e.g., relatively large materials such as rags) generated during preliminary treatment of domestic sewage in a treatment works. (i) Drinking water"treatment sludge. This part does not establish requirements, for the use or disposal of sludge generated during the treatment'of either'surface water or ground water used for drinking water. 0) Commercial and industrial septage. This part does�not establish requirements forthe use or disposal of commercial septage, industrial septage, a mixture of domestic septage and commercial, septage, or a mixture of domestic septage and industrial septage. § 503.7 Requirement for a person who prepares sewage sludge.., Any person who prepares sewage sludge shall ensure that the applicable requirements in this.part are met when the sewage sludge is applied to the land, placed on a surface disposal site, or fired in a sewage sludge incinerator, § 503.8 Sampling and analysis. (a) Sampling. Representative samples of sewage sludge that is applied to the land, placed on a surface disposal site, or fired in a sewage sludge incinerator shall be collected and analyzed. (b) Methods. The materials listed below are incorporated by reference in this part.. These incorporations by reference were approved by the Director of the Federal Register in accordance with 5 U.S.C. 552(a) and 1 CFR part 51. The materials are incorporated as they exist on the date of approval, and notice of any change in these materials will be published in theFederal Register.They are available for inspection at the Office of Water Docket, room L-102, U.S. Environmental Protection Agency, 401 M St., SW., Washington, DC, and at the National Archives and Records Administration (NARA). For information on the availability of this material at NARA, call 202-741-6030, or go to: http://www.archives.gov/federal_register/code of federal_regulations/ibr locations.html. Copies may be obtained from the standard producer or publisher listed in the regulation. Methods in the materials listed below shall be used to analyze samples of sewage sludge. (1) Enteric viruses. ASTM Designation: D 4994-89, "Standard Practice for Recovery of Viruses From Wastewater Sludges", 1992 Annual Book of ASTM Standards: Section 11—Water and Environmental Technology, ASTM, 1916 Race Street, Philadelphia, PA 19103-1187. (2) Fecal coliform. Part 9221 E. or Part 9222 D., "Standard Methods for the Examination of Water and Wastewater", 18th Edition, 1992, American Public Health Association, 1015 15th Street, NW., Washington, DC 20005. (3) Helminth ova. Yanko, W.A., "Occurrence of Pathogens in Distribution and Marketing Municipal Sludges", EPA 600/1-87-014, 1987. National Technical Information Service, 5285 Port Royal Road, Springfield, Virginia 22161 (PB 88-154273/AS). (4) Inorganic pollutants. "Test Methods for Evaluating Solid Waste, Physical/Chemical Methods", EPA Publication SW-846, Second Edition (1982) with Updates I (April 1984) and II (April 1985) and Third Edition (November 1986) with Revision I (December 1987). Second Edition and Updates I and II are available from the National Technical Information Service, 5285 Port Royal Road, Springfield, Virginia 22161 (FB-87-120- 291). Third Edition and Revision I are available from Superintendent of Documents, Government Printing Office, 941 North Capitol Street,, NE., Washington, DC 20002 (Document Number 955-001-00000-1). (5) Salmonella sp. bacteria. Part 9260 D., "Standard Methods for the Examination of Water and Wastewater", 18th Edition, 1992, American Public Health Association, 1015 15th Street, NW., Washington, DC 20005; or Kenner, B.A. and H.P. Clark, "Detection and enumeration of Salmonella and Pseudomonas aeruginosa Journal of the Water Pollution Control Federation, Vol. 46, no. 9, September 1974, pp. 2163-2171. Water Environment Federation, 601 Wythe Street, Alexandria, Virginia 22314. (6) Specific oxygen uptake rate. Part 2710 B., "Standard Methods for the Examination of Water and Wastewater", 18th Edition, 1992, American Public Health Association, 1015 15th Street, NW., Washington, DC 20005. (7) Total, fixed, and volatile solids. Part 2540 G., "Standard Methods for the Examination of Water and Wastewater", 18th Edition, 1992, American Public Health Association, 1015 15th Street, NW., Washington, DC 20005. [58 FR 9387, Feb. 19, 1993, as amended at 69 FR 18803, Apr. 9, 2004] § 503.9 General definitions. (a) Apply sewage sludge or sewage sludge applied to the land means land application of sewage sludge. (b) Base flood is a flood that has a one percent chance of occurring in any given year ( i.e. , a flood with a magnitude equalled once in 100 years). (c) Class I sludge management facility is any publicly owned treatment works (POT", as defined in 40 CFR 501.2, required to have an approved pretreatment program under 40 CFR 403.8(a) (including any POTW located in a State that has elected to assume local program responsibilities pursuant to 40 CFR 403.10(e)) and any treatment works treating domestic sewage, as defined in-40 CFR 122.2, classified as a Class I sludge management facility by the EPA Regional Administrator, or, in the case of approved State programs, the Regional Administrator in conjunction with the State Director, because of the potential for its sewage sludge use or disposal practice to affect public health and the environment adversely. (d)Cover crop is a small grain crop, such as oats, wheat, or barley, not grown for harvest. (e) CWA means the Clean Water Act (formerly referred to as either the Federal Water Pollution Act or the Federal Water Pollution Control Act Amendments of 1972), Public Law 92-500, as amended by Public Law 95-217, Public Law 95-576, Public Law 96-483, Public Law 97-117, and Public Law 10d-4. (f) Domestic septage is either liquid or solid material removed from, a septic tank, cesspool, portable toilet, Type III marine sanitation device, or similar treatment works that receives only domestic sewage. Domestic septage does not include liquid or solid material removed from a septic tank, cesspool, or similar treatment works that receives either commercial wastewater or industrial wastewater and does not include grease removed .from a grease trap at a restaurant. (g) Domestic sewage is waste and wastewater from humans or household operations that is discharged to or otherwise enters a treatment works.' (h) Dry weight basis means calculated on the basis of having been dried at 105 degrees Celsius until'' reaching a constant mass ( i.e. , essentially 100 percent solids content). (i) EPA'means the United States Environmental Protection Agency. (j) Feed crops are crops produced primarily for consumption by animals. (k) Fiber crops are crops such as flax and cotton. (1) Food crops 'are crops consumed by humans. These include, but are not limited to, fruits, vegetables, and tobacco: (m) Ground water is water below the land surface in the saturated zone. (n)"Industrial.wa"stewater is wastewater generated in a commercial or industrial process. (o) Municipality means a city,, town; borough, county, parish, district, association, or other public body (including an, intermunicipal Agency of two or more of the foregoing entities) created by or under State law; an Indian tribe or an authorized Indian tribal organization having jurisdiction over sewage sludge management; or a designated and -approved management Agency under section 208 of the CWA, as amended, The definition includes a special district created.under State law,.such as a water district, sewer district, sanitary'district, utility district, drainage district, or similar entity, or an integrated waste management facility as defined in - section 201(e) of the CWA, as amended, that has as one of its principal responsibilities the treatment, transport, use,' or disposal of sewage sludge. (p) Permitting authority is either EPA or a State with an EPA -approved sludge management program. (q) Person is an individual, association, partnership, corporation, municipality, State or Federal agency, or an agent or employee thereof. (r) Person who prepares sewage sludge is either the person who, generates sewage sludge during the treatment of domestic sewage in a treatment works or -the person who derives a material from sewage sludge. (s) Place sewage sludge or sewage sludge placed means disposal of sewage sludge on a surface, disposal site-. (t) Pollutant is an organic substance, an inorganic substance, a combination of organic.and inorganic substances, or a pathogenic organism that, after discharge and upon exposure, ingestion, inhalation, or assimilation into an organism either directly from the environment or indirectly by' ingestion through the food chain, could, on the basis of information available to the Administrator of EPA, cause death, disease' . behavioral abnormalities, cancer, genetic mutations, physiologicalmalfunctions (including malfunction in reproduction),` or physical deformations in either organisms or,offspring of the organisms. (u) Pollutant limit is a numerical value,that describes the amount of a pollutant allowed per unit'amount of sewage sludge (e.g., milligrams. per kilogram of total solids); the amount of a pollutant that can be applied -to a unit area of land (e.g.; kilograms per hectare); or the volume of a material that can be applied to a unit area of land (e.g., gallons per acre). (v) Runoff is rainwater, leachate, or other liquid that drains overland on any part of a land surface and runs off of the land surface. (w) Sewage sludge is solid, semi -solid, or liquid residue generated during the treatment of domestic sewage in a treatment'works. Sewage, sludge includes, but is not limited to, domestic se, ptage; scum or solids removed in primary, secondary, or advanced wastewater treatment processes; and a material derived from sewage sludge. Sewage sludge does not include ash generated during the firing of sewage sludge-in.'a , . sewage sludge incinerator or grit and screenings generated during preliminary treatment of domestic` sewage in a treatment works. (x) State is one'of the United States of America, the District of Columbia, the Commonwealth of Puerto Rico, the Virgin Islands, Guam, American Samoa, the Trust Territory of the Pacific Islands', the Commonwealth of the Northern Mariana Islands, and an Indian Tribe eligible for treatment as a State: pursuant to regulations promulgated, under the authority of section 518(e) of the CWA. (y) Store or storage of sewage sludge is the placement of sewage sludge on land on which the sewage sludge remains for two years -or less. This does not include the placement of sewage sludge on land for treatment. (z) Treat or treatment of sewage sludge is the preparation of sewage sludge for final use or disposal. This includes, but is not limited to, thickening, stabilization, and dewatering of sewage sludge. This does -not include storage of sewage sludge. (aa) Treatment works is either a federally owned, publicly owned, or privately owned device or system used to treat (including recycle and reclaim) either domestic sewage or a combination of domestic sewage and industrial waste of a liquid nature. (bb) Wetlands means those areas that are inundated or saturated by surface water or ground water at'a frequency and duration to support, and that under normal circumstances do support, a prevalence bf vegetation typically adapted for life in saturated soil conditions. Wetlands generally include swamps, marshes, bogs, and similar areas. Subpart B-Land Application § 503.10 Applicability. (a) This subpart applies to any person who prepares sewage sludge that is applied to the land, to `any person who applies sewage sludge to the land, to sewage sludge applied to the land, and to the land on which sewage sludge is applied. (b)(1) Bulk sewage sludge. The general requirements in §503.12 and the management practices in §503.14 do not apply when bulk sewage sludge is applied to the land if the bulk sewage sludge meets the ceiling concentrations in Table 1 of §503.13 and the pollutant concentrations in Table 3 of §503.13; the Class A pathogen requirements in §503.32(a); and one of the vector attraction reduction requirements in §503.33(b)(1) through (b)(8). (2) The Regional Administrator of EPA or, in the case of a State with an approved sludge management program, the State Director, may apply any or all of the general requirements in §503.12 and the management practices in §503.14 to the bulk sewage sludge in §503.10(b)(1) on a case -by -case basis after determining that the general requirements or management practices are needed to protect public health and the environment from any reasonably anticipated adverse effect that may occur from any pollutant in the bulk sewage sludge. (c)(1) The general requirements in §503.12 and the management practices in §503.14 do not apply when a bulk material derived from sewage sludge is applied to the land if the derived bulk material meets the ceiling concentrations in Table 1 of §503.13 and the pollutant concentrations in Table 3 of §503.13; the Class A pathogen requirements in §503.32(a); and one of the vector attraction reduction requirements in §503.33(b)(1) through (b)(8). (2) The Regional Administrator of EPA or, in the case of a State with an approved sludge management program, the State Director, may apply any or all of the general requirements in §503.12 or the management practices in §503.14 to the bulk material in §503.10(c)(1) on a case -by -case basis after determining that the general requirements or management practices are needed to protect public health and the environment from any reasonably anticipated adverse effect that may occur from any pollutant in the bulk sewage sludge. (d) The requirements in this subpart do not apply when a bulk material derived from sewage sludge is applied to the land if the sewage sludge from which the bulk material is derived meets the ceiling concentrations in Table 1 of §503.13 and the pollutant concentrations in Table 3 of §503.13; the Class A pathogen requirements in §503.32(a); and one of the vector attraction reduction requirements in §503.33(b)(1) through (b)(8)• (e) Sewage sludge sold or given away in a bag or other container for application to the land. The general requirements in §503.12 and the management practices in §503.14 do not apply when sewage sludge is sold or given away in a bag or other container for application to the land if the sewage sludge sold or given away in a bag or other container for application to the land meets the ceiling concentrations in Table 1 of §503.13 and the pollutant concentrations in Table 3 of §503.13; the Class A pathogen requirements in §503.32(a); and one of the vector attraction reduction requirements in §503.33(b)(1) through (b)(8). (f) The general requirements in §503.12 and the management practices in §503.14 do not apply when a material derived from sewage sludge is sold or given away in a bag or other container for application to the land if the derived material meets the ceiling concentrations in Table 1 of §503.13 and the pollutant concentrations in Table 3 of §503.13; the Class A pathogen requirements in §503.32(a); and one of the vector attraction reduction requirements in §503.33(b)(1) through (b)(8). _ (g) The requirements in this subpart do not apply when a material derived from sewage sludge is sold or given away in a bag or other container for application to the land if the sewage sludge from which the material is derived meets the ceiling concentrations in Table 1 of §503.13 and the pollutant concentrations in Table 3 of §503.13; the Class A pathogen requirements in §503.32(a); and one of the vector attraction reduction requirements in §503.33 (b)(1) through (b)(8). [58 FR 9387, Feb. 19, 1993,. as amended at 64 FR 42568, Aug. 4, 1999] § 503.11 Special definitions. (a) Agricultural land is land on which a food crop, a feed crop, or a fiber crop is grown. This includes range land and land used as pasture. (b) Agronomic rate is the whole sludge application rate (dry weight basis) designed: (1) To provide the amount of nitrogen needed by the food crop, feed crop, fiber crop, cover crop, or vegetation grown on the land; and (2) To minimize the amount of nitrogen in the sewage sludge that passes below the root zone of the.crop or vegetation grown on the land to the. ground water. (c) Annual pollutant loading rate is the maximum amount of a pollutant that can be applied to a unit area of - land during a 365 day period. (d) Annual whole sludge application rate is the maximum amount of sewage sludge (dry weight basis): that can be applied to a unit area of land during a 365 day period. (e) Bulk sewage sludge is sewage sludge that is not sold or given away in a bag or other container:for'`' application to the land. (f) Cumulative pollutant loading rate is the maximum amount of an inorganic pollutant that can be applied to an area of land. (g) Forest is a tract of land thick with trees and underbrush. (h) Land application is the spraying or spreading of sewage sludge onto the land surface; the injection of sewage sludge.below the land surface; or the incorporation of sewage sludge into the soil so that the sewage sludge can either condition the soil or fertilize crops or vegetation grown in the soil. (i) Monthly average is the arithmetic mean of all measurements taken during the month. 0) Other container is either an open or closed receptacle. This includes, but is not limited to, a bucket; a box, a carton, and a vehicle or trailer with a load capacity of one metric ton or less. (k) Pasture is land on which animals feed directly on feed crops such as legumes, grasses, grain stubble,: or stover. (1) Public contact site is land with a high potential for'contact by the'public. This includes, but is not limited to, public parks, ball fields, cemeteries, plant nurseries, turf farms, and golf courses. (m) Range land is open land with indigenous vegetation. (n) Reclamation site is drastically disturbed land that is reclaimed using sewage sludge. This includes, but is not limited to, strip mines and construction sites. § 503.12 General requirements. . (a) No person shall apply sewage sludge to the land except in accordance with the requirements in this subpart. (b) No person shall apply bulk sewage sludge subject to the cumulative pollutant loading rates in §503.13(b)(2) to agricultural land, forest, a public contact site, or a reclamation site if any of the cumulative pollutant loading rates in §503.13(b)(2) has been reached. (c) No person shall apply domestic septage to agricultural land, forest, or a reclamationsite during a 365 day period if the annual application rate in §503.13(c) has been reached during that period. (d) The person who prepares bulk sewage sludge that is applied to agricultural land, forest, a public contact site, or a reclamation site shall provide the person who applies the bulk sewage sludge written notification of the concentration of total nitrogen (as N on a dry weight basis) in. the bulk sewage sludge. (e)(1) The person who applies sewage sludge to the land shall obtain information needed to comply with the requirements in this subpart. (2)(i) Before bulk sewage sludge subject to the cumulative pollutant loading rates,i,n §503.13(b)(2) is applied to -the land, the person who proposes to apply the bulk sewage sludge shall contact the permitting authority for the State in;which the bulk sewage sludge will be applied to determine whether bulk sewage sludge subject to the cumulative pollutant loading rates in §503.1.3(b)(2) has been applied to the site since July 20, 1993. (ii) If bulk sewage sludge subject to the cumulative pollutant loading rates in §503.13(b)(2) has not been applied to the site since July 20, 1993, the cumulative amount for each pollutant listed in Table 2 of §503.13 may be applied to the site in accordance with-§503.13(a)(2)(i). (iii) If bulk sewage sludge subject to'the cumulative pollutant loading rates in §503.13(b)(2) has been applied to the site since July'20, 1993, and the cumulative amount of each pollutant applied to the site in the bulk sewage' sludge since that .date .is known, the cumulative amount of each pollutant applied to the site shall be, used to determine the additional amount of each pollutant that can be applied to the site in accordance with §503.13(a)(2)(i). (iv) If bulk sewage sludge subject to. the cumulative pollutant loading rates in §503.13(b)(2) has been applied to the site since July 20, 1993, and the cumulative amount of each pollutant applied to the site in the bulk sewage sludge since that date is not known, an additional amount of each pollutant shall not be applied to the site in accordance with §503.1-3(a)(2)(i). (f) When a person who prepares bulk sewage sludge provides the bulk sewage sludge to a person who . applies the bulk sewage sludge to the land, the person who prepares the bulk sewage sludge shall provide the person who applies the sewage sludge notice and necessary information.to comply with the requirements in this subpart. (g) When a person who prepares sewage sludge provides -the sewage sludge to another person who prepares the sewage sludge, the person who provides the sewage sludge shall provide the person who receives the sewage sludge notice and necessary information to comply with the requirements in this subpart. (h) The person who applies bulk sewage sludge to the land shall provide the owner or lease holder of the land on which the bulk sewage sludge is applied notice and necessary information to comply with the requirements in this subpart. (i) Any person who prepares bulk sewage sludge that is applied to land in a State other than the State in which the bulk sewage sludge is prepared shall provide written notice, prior to the initial application of bulk sewage sludge to the land application site by the applier, to the permitting authority for the State in which the bulk sewage sludge is proposed to be applied. The notice shall include: (1) The location, by either.street address or latitude and longitude, of each land application site. (2) The approximate time period bulk sewage sludge will be applied to the site. (3) The name, address, telephone number, and National Pollutant Discharge Elimination System permit number (if appropriate) for the person who prepares the bulk sewage sludge. (4) The name, address, telephone number, and National Pollutant Discharge Elimination System permit number (if appropriate) for the person who will apply the bulk sewage sludge. 0) Any person who applies bulk sewage sludge subject to the cumulative pollutant loading rates in §503.13(b)(2) to the land shall provide written notice, prior to the initial application of bulk sewage sludge to a land application site by the applier, to the permitting authority for the State in which the bulk sewage sludge will be applied and the permitting authority shall retain and provide access to.the notice. The notice shall include: (1) The location, by either street address or latitude and longitude, of the land application site. (2) The name, address, telephone number, and National Pollutant Discharge Elimination System permit number (if appropriate) of the person who will apply the bulk sewage sludge. § 503.13 Pollutant limits. (a) Sewage sludge. (1) Bulk sewage sludge or sewage sludge sold or given away in a bag or other container shall not be applied to the land if the concentration of any pollutant in the sewage sludge exceeds the ceiling concentration for the pollutant in Table 1 of §503.13. (2) If bulk sewage sludge is applied to agricultural land, forest, a public contact site, or a reclamation site, either: (i) The cumulative loading rate for each pollutant shall not exceed the cumulative pollutant loading rate for the pollutant in Table 2 of §503.13; or (ii) The concentration of each pollutant in the sewage sludge shall not exceed the concentration for the pollutant in Table 3 of §503.13. (3) If bulk sewage sludge is applied to a lawn. or a home garden, the concentration of each pollutant in the sewage sludge shall not exceed the concentration for the pollutant in Table 3 of .§503.13. (4) If sewage sludge is sold or given away in a bag or other container for application to the land, either: (i) The concentration of each pollutant in the sewage sludge shall not exceed the concentration for the pollutant in Table 3 of 5503.13; or (ii) The product of the concentration of each pollutant in the sewage sludge and the annual whole sludge application rate for the sewage sludge shall not cause the annual pollutant loading rate for the pollutant in Table 4 of §503.13 to be exceeded. The procedure used to determine the annual whole sludge application rate is presented in appendix A of this part. (b) Pollutant concentrations and loading rates —sewage sludge. —(1) Ceiling concentrations. Table 1 of &503.13—Ceiling Concentrations Pollutant Ceiling concentration (milligrams per kilogram)1 Arsenic . 75 Cadmium 85 Copper 4300 Lead 840 Mercury 57 Molybdenum 175 Nickel. 420 Selenium 100 1 Dry weight basis. (2) Cumulative 'pollutant loading rates. Table 2 of 8503.13=Cumulative Pollutant I nnriinn Ratac Pollutant Cumulative pollutant loading rate (kilograms per hectare) Arsenic 41 Cadmium 39 Copper 1500 Lead 300 Mercury 17 Nickel 420 Selenium I 100 Zinc 2800 (s) roiiutant concentrations. Table 3 of &503-13—Pollutant Conr_entrations ' Pollutant . Monthly average concentration (milligrams per kilogram)1 Arsenic 41 Cadmium 39 Copper. 1500 Lead 300 Mercury 17 Nickel 420 Selenium 100 " Zinc 2800 1 Dry weight basis. (4) Annual pollutant loading rates. Table 4 of §503.13—Annual Pollutant Loading Rates Pollutant Annual pollutant loading rate (kilograms per hectare per 365 day period) Arsenic 2.0 Cadmium 1.9 Copper 75. Lead 15 Mercury 0.85 Nickel 21 Selenium 5.0 Zinc 140 (c) Domestic septage. The annual application rate for domestic septage applied to agricultural land, forest, or a reclamation site shall not exceed the -annual application rate calculated using equation (1). AAR = N Eq. (1) 0.0026 Where: , AAR=Annual application rate in gallons per acre per 365 day period. N=Amount of nitrogen in pounds per acre per 365 day period needed by the crop or vegetation grown on the land. [58 FIR 9387, Feb. 19, 1993, as amended at 58 FIR 9099, Feb. 25, 1994; 60 FIR 54769, Oct. 25, 1995] § 503.14 Management practices. (a) Bulk sewage sludge shall not be applied to the land if it is likely to adversely affect a threatened or endangered species listed under section 4 of the Endangered Species Act or its designated critical habitat. (b) Bulk sewage sludge shall not be applied to agricultural land, forest, a public contact site, or a reclamation site that is flooded, frozen, or snow-covered so that the bulk sewage sludge enters a wetland or other waters of the United States, as defined in 40 CFR 122.2, except as provided in a permit issued pursuant to section 402 or 404 of the CWA. (c) Bulk sewage sludge shall not be applied to agricultural land, forest, or a reclamation site that is 10 meters or less from waters of the United States, as defined in 40 CFR 122.2, unless otherwise specified by the permitting authority. (d) Bulk sewage sludge shall be applied to agricultural land, forest, a public contact site, or a reclamation site at a whole sludge application rate that is equal to or less than the agronomic rate for the bulk sewage sludge, unless, in the case of a reclamation site, otherwise specified by the permitting authority. (e) Either a label shall be affixed to the bag or other container in which sewage sludge that is sold or given away for application to the land, or an information sheet shall be provided to the person who receives sewage sludge sold or given away in an other container for application to the land. The -label or information sheet shall contain the following information: (1) The name and address of the person who prepared the sewage sludge that is sold or given away in a bag or other container for application to the land. (2) A statement that application of the sewage sludge to the land is prohibited except in accordance with the instructions on the label or information sheet. (3) The annual whole sludge application rate for the sewage sludge that does not cause any of the annual pollutant loading rates in Table 4 of §503.13 to be exceeded. § 503.15 Operational standards —pathogens and vector attraction reduction. (a) Pathogens —sewage sludge. (1) The Class A pathogen requirements in §503.32(a) or the Class B pathogen requirements and site restrictions in §503.32(b) shall be met when bulk sewage sludge is applied to agricultural land, forest, a public contact site, or a reclamation site. (2) The Class A pathogen requirements in §503.32(a) shall be met when bulk sewage sludge is applied to a lawn or a home garden. (3) The Class A pathogen requirements in §503.32(a) shall be met when sewage sludge is sold or given away in a bag or other container for application to the land. (b) Pathogens —domestic septage. The requirements in either §503.32 (c)(1) or (c)(2) shall be met when domestic septage is applied to agricultural land, forest, or a reclamation site. (c) Vector attraction reduction —sewage sludge. (1) One of the vector attraction reduction requirements in §503.33 (b)(1) through (b)(10) shall be met when bulk sewage sludge is applied to agricultural land, forest, a public contact site, or a reclamation site. (2) One of the vector attraction reduction requirements in §503.33 (b)(1) through (b)(8) shall be met when bulk sewage sludge is applied to a lawn or a home garden. - (3) One of the vector attraction reduction requirements in §503.33 (b)(1) through (b)(8) shall be met when sewage sludge is sold or given away in a bag or other container for application to the land. (d) Vector attraction reduction —domestic septage. The vector attraction reduction requirements in §503.33(b)(9), (b)(10), or (b)(1 2) shall be met when domestic septage is applied to agricultural land, forest, or a reclamation site. § 503.16 Frequency of monitoring. (a) Sewage sludge. (1) The frequency of monitoring for the pollutants listed in Table 1, Table 2, Table 3 and Table 4 of §503.13; the pathogen density requirements in §503.32(a) and §503.32(b)(2); and the vector attraction reduction requirements in §503.33 (b)(1) through (b)(4) and §503.33 (b)(7) through (b)(8) shall be the frequency in Table 1 of §503.16. Table 1 of §503.16—Frequency of Monitorinq—Land Application (Amount of sewaqe sludge1(metric tons per 365 day period) IFreauencv Greater than zero but less than 290 Once per year. Equal to or greater than 290 but less than 1,500 Once per quarter (four times per year). Equal to or greater than 1,500 but less than 15,000 Once per 60 days (six times per year). Equal to or greater than 15,000 Once per month (12 times per year). 1 Either the amount of bulk sewage sludge applied to the land or the amount of sewage sludge prepared for sale or give-away in a bag or other container for application to the land (dry weight basis). (2) After the sewage sludge has been monitored for two years at the frequency in Table 1 of §503.16; the, permitting authority may reduce the frequency of monitoring for pollutant concentrations and for the pathogen density requirements in §503.32(a)(5)(ii) and (a)(5)(iii). (b) Domestic septage. If either the pathogen requirements in §503.32(c)(2) or the vector attraction reduction requirements in,§503.33(b)(1.2) are met when domestic septage is applied to agricultural land, forest; or a reclamation site,•each container of domestic septage applied to the land shall be monitored for compliance with those requirements. (Approved by the Office of Management and Budget under control number 2040=0157) [58 FIR 9387, Feb. 19, 1993, as amended at 64 FIR 42569, Aug. 4, 1999] § 503.17 Recordkeeping. (a) Sewage sludge. (1) The person who prepares the sewage sludge in §503.10(b)(1) or (e) shall develop the following information and shall retain the information for five years: (i) The concentration of each pollutant listed in Table 3 of §503.13 in the sewage sludge. (ii) The following certification statement: I certify, under penalty of law, that the information that will be used to determine compliance with the Class A pathogen requirements in §503.32(a), and the vector attraction reduction requirement in [insert one of the vector attraction reduction requirements in §503.33(b)(1) through §503.33(b)(8)] was prepared under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate this information. I am aware that there are. significant penalties for false certification including the possibility of fine and imprisonment. (iii) A description of how the Class A pathogen requirements in §503.32(a) are met. (iv) A description of how one of the vector attraction reduction requirements in §503.33 (b)(1) through (b)(8) is met. - (2) The person -who derives the material in §503.10 (c)(1) or (f) shall develop the following information and shall retain the information for five years: (i) The concentration of each pollutant listed in Table 3 of §503.13 in the material. (ii) The following certification statement: I certify, under penalty of law, that the information that will be used to determine compliance with the Class A pathogen requirements in §503.32(a) and the vector attraction reduction requirement in (insert one:of the vector attraction reduction requirements in §503.33(b)(1) through (b)(8)) was prepared under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate this information. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. (iii) A description of how the Class A pathogen requirements in §503.32(a) are met. (iv) A description of how one of the vector attraction reduction requirements in §503.33 (b)(1) through (b)(8) is met. (3) If the pollutant concentrations in §503.13(b)(3), the Class A pathogen requirements in §503.32(a), -and the vector attraction reduction requirements in either §503.33 (b)(9) or (b)(10) are met when bulk sewage sludge is applied to agricultural land, forest, a public contact site, or a reclamation site: (i) The person who prepares the bulk, sewage sludge shall develop the following information and shall retain the information for five years. (A) The concentration of each pollutant listed in Table 3 of §503.13 in the bulk sewage sludge. (B) The following certification statement: I certify, under penalty of law, that the information that will be used to determine compliance with the Class A pathogen requirements in §503.32(a) was prepared under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather.and evaluate this information. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. (C) A description of how the pathogen requirements in §503.32(a) are met. (ii) The person who applies the•.bulk sewage sludge shall develop the following information and shall retain the information for five years. (A) The following certification statement: I certify, under penalty of law, that the information that will be used to determine compliance with the management practices in §503.14 and the vector attraction reduction requirement in (insert either §503.33(b)(9) or (b)(10)) was prepared under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate this information. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. (B) A description of how the management practices in §503.14 are met for each site on which bulk sewage sludge is applied. (C) A description of how the vector attraction reduction requirements in either §503.33(b)(9) or (b)(10) are met for each site on which bulk sewage sludge is applied. (4) If the pollutant concentrations in §503.13(b)(3) and the Class B pathogen requirements in §503.32(b) are met when bulk sewage sludge is applied to agricultural land, forest, a public contact site, or a reclamation site: (i) The person who prepares the bulk sewage sludge shall develop the following information and shall retain the information for five years: (A) The concentration of each pollutant. listed in Table 3 of §503.13 in the bulk sewage sludge. (B) The following certification statement: I certify, under penalty of law, that the information that will be used to determine compliance with the Class B pathogen requirements in §503.32(b) and the vector attraction reduction requirement in (insert one of the vector attraction reduction requirements in §503.33(b)(1) through (b)(8)if one of those requirements is met) was prepared under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate this information. I am aware that there are significant' penalties for false certification including the possibility of fine and imprisonment. ' (C) A description of how the Class B pathogen requirements in §503.32(b) are met. (D) When one of the vector attraction reduction requirements in §503.33 (b)(1) through (b)(8) is met, a description of how the vector attraction reduction requirement is met. (ii) The person who applies the bulk sewage sludge shall develop the following information and shall retain the information for five years. (A) The following certification statement: I certify, under penalty of law, that the information that will be used to determine compliance with the management practices in §503.14, the site restrictions in §503.32(b)(5), and the vector attraction reduction requirement in (insert either §503.33(b)(9) or (b)(10) if one of those requirements is met) was prepared for each site on which bulk sewage sludge is applied under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate this information. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. (B) A description of how the management practices in §503.14 are met for each site on which bulk sewage sludge is applied. (C) A description of how the site restrictions in §503.32(b)(5) are met for each.site on which bulk sewage sludge is applied. (D) When the vector attraction reduction requirement in either §503.33 (b)(9) or (b)(10) is met, a description of how the vector attraction reduction requirement is met. (E) The date bulk sewage sludge is applied to each site. (5) If the requirements in §503.13(a)(2)(i) are met when bulk sewage sludge is applied to agricultural land, forest, a public contact site, or a reclamation site: (i) The person who prepares the bulk sewage sludge shall develop the following information and shall retain the information for five years. (A) The concentration of each pollutant listed in Table 1 of §503.13 in the bulk sewage sludge. (B) The following certification statement: I certify, under penalty of law, that the information that will be used to determine compliance with the pathogen requirements in (insert either §503.32(a) or §503.32(b)) and the vector attraction reduction .requirement in (insert one of the vector attraction reduction requirements in §503.33(b)(1) through (b)(8) if one .of those requirements is met) was prepared under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate this information. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. (C) A description of how the pathogen requirements in either §503.32 (a) or (b) are met. (D) When one of the vector attraction requirements in §503.33 (b)(1) through (b)(8) is met, a description of how the vector attraction requirement is met. (ii) The person who applies the bulk sewage sludge shall develop the following information, retain the information in §503.17 (a)(5)(ii)(A) through (a)(5)(ii)(G) indefinitely, and retain the information in §503.17 (a)(5)(ii)(H) through (a)(5)(ii)(M) for five years. '(A) The location, by either street address or latitude and longitude, of each site on which:bulk sewage sludge is applied. (B) The number of hectares in each site on which bulk sewage sludge is applied. (C) The date bulk. sewage sludge is applied to each site. (D) The cumulative amount of each pollutant ( i.e. , kilograms) listed in Table 2 of §503.13 in the bulk sewage sludge applied to each site, including the amount in §503.12(e)(2)(iii). (E) The amount of sewage sludge ( i.e. , metric tons) applied to each site. (F) The following certification statement: I certify, under penalty of law, that the information that will be -used to determine compliance with the requirement to obtain information in §503.12(e)(2) was prepared for each site on which bulk sewage sludge was applied under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate this information. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. (G) A description.of how the requirements to obtain information in §503.12(e)(2) are met. (H) The following certification statement: I certify, under penalty of law,'that the information that will be used to determine compliance with the:: ` management practices in §503.1.4 was prepared for each site on which bulk sewage sludge was -applied... under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate this information. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. (1) A description- of how the management practices in §503.14 are met for each site on which bulk sewage sludge is applied. (J) The following certification statement when the bulk sewage sludge meets the Class B pathogen requirements in §503.32(b): I certify, under penalty of law, that the information that will be used to determine compliance with the site restrictions in §503.32(b)(5) for each site on which Class B sewage sludge was applied was prepared under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate this information. I am aware that there'are significant penalties for false certification including the possibility of fine and imprisonment. (K) A description of how the site restrictions in §503.32(b)(5) are met for each site on which Class B bulk sewage sludge is applied'. (L) The following certification statement when the vector attraction reduction requirement in either §503.33(b)(9) or (b)(10) is met: I certify, under penalty of law, that the information that will be used to determine compliance with the vector attraction reduction requirement in (insert either §503.33(b)(9) or §503.33(b)(10)) was prepared under my - direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate this information. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. (M) If the vector attraction reduction requirements in either §503.33 (b)(9) or (b)(10) are'met, a description of how the requirements are met. (6) If the requirements in §503.13(a)(4)(ii) are met when sewage sludge is sold or given away in a bag or other container for application to the land, the person who prepares the sewage sludge that is sold or given away in a bag or other container shall develop the following information and. shall retain the information for five years: (i) The annual whole sludge application rate for the sewage sludge that does not cause the annual pollutant loading rates in Table 4 of §503.13 to be exceeded. (ii) The concentration of each pollutant listed in Table 4 of §503.13 in the sewage sludge. (iii) The following certification statement: I certify, under penalty of law, that the information that will be used to determine compliance with the management practice in §503.14(e), the Class A pathogen requirement in §503.32(a), and the vector attraction reduction requirement in (insert one of the vector attraction reduction requirements in §503.33(b)(1) through §503.33(b)(8)) was prepared under my direction and supervision in accordance with the system designed to ensure that qualified'personnel properly gather and evaluate this_ information. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. (iv) A description of how the Class A pathogen requirements in §503.32(a) are met. (v) A description of how one of the vector attraction requirements in §503.33 (b)(1) through (b)(8) is met. (b) Domestic septage. When domestic septage is applied to agricultural land, forest, or a reclamation site, the person who applies the domestic septage shall develop the following information and shall retain the information for five years: (1) The location, by either street address or latitude and longitude, of each site on which domestic septage is applied. (2) The number of acres in each site on which domestic septage is applied. (3) The date domestic septage is applied to each site. (4) The nitrogen requirement for the crop or vegetation grown on each site during a 365 day period. (5) The rate, in gallons per acre per 365 day period, at which domestic septage is applied to each site. (6) The following certification statement: I certify, under penalty of law, that the information that will be used to determine compliance with the pathogen requirements (insert either §503.32(c)(1) or §503.32(c)(2)) and the vector attraction reduction requirement in [insert §503.33(b)(9), 503.33(b)(10), or §503.33(b)(12)] was prepared under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate this information. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. (7) A description of how the pathogen requirements in either §503.32(c)(1) or (c)(2) are met. (8) A description of how the vector attraction reduction requirements in §503.33 (b)(9), (b)(10), or (b)(12) are met. (Approved by the Office of Management and Budget under control number 2040-0157) [58 FR 9387, Feb. 19, 1993, as amended at 64 FR 42569, Aug. 4, 1999] § 503.18 Reporting. (a) Class I sludge management facilities, POTWs (as defined in 40 CFR 501.2) with a design flow rate equal to or greater than one million gallons per day, and POTWs that serve 10,000 people or more shall submit the following information to the permitting authority: (1) The information A §503.17(a), except the information in §503.17 (a)(3)(ii), (a)(4)(ii) and in (a)(5)(ii), for the appropriate requirements on February 19 of each year. (2) The information in §503.17(a)(5)(ii)(A) through (a)(5)(ii)(G) on February 19th of each year when 90 percent or more of any of the cumulative pollutant loading rates in Table 2 of §503.13 is reached at a land application site, i (Approved by the Office of Management and Budget under control number 2040-0157) [58 FR 9387, Feb. 19, 1993, as amended at 64 FR 42570, Aug. 4, 1999] Subpart C—Surface Disposal § 503.20 Applicability. (a) This subpart applies to any person who prepares sewage sludge that is placed on a surface disposal site, to the owner/operator of a surface disposal site, to sewage sludge placed on a surface disposal site, and to a surface disposal site. (b) This subpart does not apply to sewage sludge stored on the land or to the land on which sewage sludge is stored. It also does not apply to sewage sludge that remains on the land for longer than two years when the person who prepares the sewage sludge demonstrates that the land on which the sewage sludge•remains is not an active sewage sludge unit. The demonstration shall include the following information, which shall be retained by the person who prepares the sewage sludge for the period that the sewage sludge remains on the land: (1) The name and address of the person who prepares the sewage sludge.. (2) The name and address of the person who either owns the land or leases the land. (3) The location, by either street address or latitude and longitude, of the land. (4) An explanation of why sewage sludge needs to remain on the land for longer than two years prior to final use or disposal. (5) The approximate time period when the sewage sludge will be used or disposed. (c) This subpart does not apply to sewage sludge treated on the land or to the land on which sewage sludge is treated. § 503.21 Special definitions. (a) Active sewage sludge unit is a sewage sludge unit that has not closed. (b) Aquifer is a geologic formation, group of geologic formations, or a portion of a geologic formation capable of yielding ground water to wells or springs. (c)'Contaminate an aquifer means to introduce a substance that causes the maximum contaminant level for nitrate in 40 CFR 141.62(b) to be exceeded in the ground water or that causes the existing concentration of nitrate in ground water to increase when the existing concentration of nitrate in the ground water exceeds the maximum contaminant level for nitrate in 40 CFR 141.62(b). (d) Cover is soil or other material used to cover sewage sludge placed on an active sewage sludge unit. (e) Displacement is the relative movement of any two sides of a fault measured in any direction. (f) Fault is a fracture or zone of fractures in any materials along which strata on one side are displaced with respect to strata on the other side. (g) Final cover is the last layer of soil or other material placed on a sewage sludge unit at closure: (h) Holocene time is the most recent epoch of the Quaternary period, extending from the end of the Pleistocene epoch to the present. (i) Leachate collection system is a system or device installed immediately above a liner that is designed, constructed, maintained, and operated to collect and remove leachate from a sewage sludge unit. Q) Liner is soil or synthetic material that has a hydraulic conductivity of 1 X10-7centimeters per second 'or less. (k) Lower explosive limit for methane gas is the lowest percentage of methane gas. in air, by volume,. that propagates a flame at 25.degrees' Celsius and atmospheric pressure. (1) Qualified ground -water scientist is an individual with a baccalaureate or post -graduate degree in the natural sciences or engineering who has sufficient training and experience in ground -water hydrology and related fields, as may be demonstrated by State registration, professional certification, or completion of accredited university programs, to make sound professional judgments regarding ground -water monitoring, pollutant fate and transport, and corrective action. (m) Seismic impact zone is an area that has a 10 percent or greater probability that the horizontal ground level acceleration of the rock in the area exceeds 0.10 gravity once in 250 years. (n) Sewage'sludge unit island on which only sewage sludge is placed for final disposal. This does not include land on which sewage sludge is either stored or treated. Land does not include waters of the United States, as defined in 40 CFR 122.2. (o) Sewage sludge unit boundary is the outermost perimeter of an active sewage sludge unit. (p) Surface disposal site is an area of land that contains one or more active sewage sludge units. (q) Unstable area is land subject to natural or human -induced forces that may damagethe structural components of an active sewage sludge unit. This includes, but is not limited to, land on which the soils are subject to mass movement. [58 FIR 9387, Feb. 19, 1993, as amended at 64 FIR 42570, Aug. 4, 1999] § 503.22 General requirements. (a) No person shall place sewage sludge on an active sewage sludge unit unless the requirements in this subpart are met. (b) An active sewage sludge unit located within 60 meters of a fault that has displacement in Holocene time; located in an unstable area; or located in a wetland, except as provided in a permit issued pursuant to either section 402 or 404 of the CWA, shall close by March 22, 1994, unless, in the case of an active sewage sludge unit located within 60 meters of a fault that has displacement in Holocene time, otherwise specified by the permitting authority. (c) The owner/operator of an active sewage. sludge unit shall submit a written closure and post closure plan to the permitting authority 180 days prior to the date that the active sewage sludge unit closes. The plan shall describe how the sewage sludge unit will be closed and, at a minimum, shall include: (1) A discussion of how the leachate collection system will be operated and maintained for three'years after the sewage sludge unit closes if the sewage sludge unit has a liner and leachate collection system. (2) A description of the system used to monitor for methane gas in the air in any structures within the surface disposal site and in the air at the property line of the surface disposal site, as required in §503.240)(2). (3) A discussion of how public access to the surface disposal site will be restricted for three years after the last sewage sludge unit in the surface disposal site closes. (d) The owner of a surface disposal site shall provide written notification to the subsequent owner of the site that sewage sludge was placed on the land. [58 FIR 9387, Feb. 19, 1993, as amended at 64 FIR 42570, Aug. 4, 1999] § 503.23 Pollutant limits (other than domestic septage). (a) Active sewage sludge unit without a liner and leachate collection system. (1) Except as provided in §503.23 (a)(2) and (b), the concentration of each pollutant listed in Table 1 of §503.23 in sewage sludge placed on an active sewage sludge unit shall not exceed the concentration for the pollutant in Table 1 of §503.28. Table 1 of §503.23—Pollutant Concentrations —Active Sewage Sludge Unit Without a Liner and Leachate Collection (Pollutant lConcentration (milligrams per kilogramsl) Arsenic 73 Chromium 600 Nickel 420 1 Dry weight basis. (2) Except as provided in §503.23(b), the concentration of each pollutant listed in Table 1 of §503.23 in sewage sludge placed on an active sewage sludge unit whose boundary is less than 150 meters from the property line of the surface disposal site shall not exceed the concentration determined using the following procedure: (i) The actual distance from the active sewage sludge unit boundary to, the property line of the surface disposal site shall be determined. (ii) The concentration of each pollutant listed in Table 2 of §503.23 in the sewage sludge shall not exceed the concentration in Table 2 of §503.23 that corresponds to the actual distance in §503.23(a)(2)(i). Table 2 of §503.23—Pollutant Concentrations —Active Sewage Sludge Unit Without a Liner and Leachate Collection Svstem That Has a Unit Boundary to Property Line Distance Less Than 150 Meters Unit boundary to property line Pollutant concentration1 Distance (meters) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) 0 to less than 25 30 200 210 25 to less than 50 34 220- 240 50 to less than 75 39 260 270 75 to less than 100 46 300 320 100 to less than 125 53 360 390 125 to less than 150 62 450 420 1 Dry weight basis. (b) Active sewage sludge unit without a liner and leachate collection system —site -specific limits. (1) At the time of permit application, the owner/operator of a surface disposal site may request site -specific pollutant, limits in accordance with §503.23(b)(2) for an active sewage sludge unit without a liner and leachate collection system when the existing values for site parameters specified by the permitting authority are different from the values for those parameters used to develop the pollutant limits in Table 1 of §503.23 and when the permitting authority determines that site -specific pollutant limits are appropriate for the active sewage sludge unit. (2) The concentration of each pollutant listed in Table 1 of §503.23 in sewage sludge placed on an active sewage sludge unit without a liner and leachate collection system shall not exceed either the concentration for the pollutant determined during a site -specific assessment, as specified by the permitting authority, or the existing concentration of the pollutant in the sewage sludge, whichever is lower. § 503.24 Management practices. .(a) Sewage sludge shall not be placed on an active sewage sludge unit if it is likely to adversely affect a threatened or endangered species listed under section 4 of the Endangered Species Act or its designated critical habitat. (b) An active sewage sludge unit shall not restrict the flow of a base flood. -(c) When a surface disposal site is located in a seismic impact zone, an active sewage sludge unit shall be designed to withstand the maximum recorded horizontal ground level acceleration. (d) An -active sewage sludge unit shall be located 60 meters or more from a fault that has displacement in Holocene time, unless otherwise specified by the permitting authority. (e) An active sewage sludge unit shall not be located in an unstable area. (f) An active sewage sludge unit shall not be located in a wetland, except as provided in a permit issued pursuant to section 402 or 404 of the CWA. (g)(1) Run-off from an active sewage sludge unit shall be collected and shall be disposed in accordance with National Pollutant Discharge Elimination System permit requirements and any other applicable requirements. (2) The run-off collection system for an active sewage sludge unit shall have the capacity to handle run-off from a 24-hour, 25-year storm event. (h) The leachate collection system for an active sewage sludge unit that has a liner and leachate collection system shall be operated and maintained during the period the sewage sludge unit is active and for three years after the sewage sludge unit closes. (i) Leachate from- an active sewage sludge unit that has a liner and leachate collection system shall be collected and shall be disposed in accordance with the applicable requirements during the period the sewage sludge unit is active and for three years after the sewage sludge unit closes. 0)(1) When a cover is placed on an active sewage sludge unit, the concentration of methane gas in air in any structure within the surface disposal site sliall not exceed 25 percent of the lower explosive limit for methane gas during the period that the sewage sludge unit is active and the concentration of methane gas in.air at the property line of the surface disposal site shall not exceed the lower explosive limit for methane gas -during the period that the sewage sludge unit is active. (2) When a final cover is placed on a sewage sludge unit at closure, the concentration of methane gas in air in any structure within the surface disposal site shall not exceed 25 percent of the lower explosive limit for methane gas for three years after the sewage sludge unit closes and the concentration of methane gas in air at the property line of the surface disposal site shall not exceed the lower explosive limit for methane gas for three years after the sewage sludge unit closes, unless otherwise specified by the permitting authority. (k) A food crop, a feed crop, or a fiber crop shall not be grown-on,an active sewage sludge unit, unless the owner/operator of the surface disposal site demonstrates to the permitting authority that through management practices public.health and the environment are protected from any reasonably anticipated adyerse,effects of pollutants in sewage sludge when crops are grown. (1) Animals shall not be grazed on an' active sewage sludge unit, unless the owner/operator of the surface disposal site demonstrates to the permitting authority that through management practices public health and the environment are protected from any reasonably anticipated adverse effects of pollutants in sewage sludge when animals are grazed. (m) Public access to a surface disposal site shall be restricted for the period that the surface disposal site contains an active sewage sludge unit and for three years after the last active sewage sludge unit in the . surface disposal site closes. (n)(1) Sewage sludge placed on an active sewage sludge unit shall not contaminate an aquifer. (2) Results of a ground -water monitoring program developed by a qualified ground -water scientist or a certification by a qualified ground -water scientist shall be used to demonstrate that sewage sludge, placed on an active sewage sludge unit does not contaminate an aquifer. § 503.25 Operational standards —pathogens and vector attraction reduction. (a) Pathogens —sewage sludge (other than domestic septage). The Class A pathogens requirements in §503.32(a) or one of the Class B pathogen requirements in §503.32 (b)(2) through (b)(4) shall be met when - sewage sludge is placed on an active sewage sludge unit, unless the vector attraction reduction requirement in §503.33(b)(11) is met. (b) Vector attraction reduction —sewage sludge (other than domestic septage). One of the vector attraction reduction requirements in §503.33 (b)(1) through (b)(11) shall be met when sewage sludge is placed on an active sewage sludge unit. (c) Vector attraction reduction --domestic septage. One of the vector attraction reduction requirement in §503.33 (b)(9) through (b)(12) shall be met when domestic septage is placed on an active sewage sludge unit. § 503.26 Frequency of monitoring. (a) Sewage sludge (other than domestic septage). (1) The frequency of monitoring for the pollutants in Tables 1 and 2 of §503.23; the pathogen density requirements in §503.32(a) and in. §503.32(b)(2); and the vector attraction reduction requirements in §503.33(b)(1) through (b)(4) and §503.33(b)(7) through'(b)(8) for sewage sludge placed on an active sewage sludge unit shall be the frequency in Table 1 of §503.26. Table 1 of §503.26—Frequency of Monitoring —Surface Disposal Amount of sewage sludge1 (metric tons per 365 day period) Frequency Greater than zero but less than 290 Once per year. Equal to or greater than 290 but less than 1,500 Once per quarter (four times per year). Equal to or greater than 1,500 but less than 15,000 Once per 60 days (six times per year): Equal .to or greater than 15,000 Once per month (12 times per year). 1Amount of sewage sludge placed on an active sewage sludge unit (dry weight basis). (2) After the sewage sludge has been monitored for two years at the frequency in Table 1 of this section, the permitting authority may reduce the frequency of monitoring for pollutant concentrations and for the pathogen density requirements in §503.32(a)(5)(ii) and (a)(5)(iii). (b) Domestic septage. If the vector attraction reduction requirements in §503.33(b)(12) are met when domestic septage is placed on an active sewage sludge unit, each container of domestic septage shall be monitored for compliance with those requirements. (c) Air. Air in structures within a surface disposal site and at the property line of the surface disposal site shall be monitored continuously for methane gas during the period that the surface disposal site contains an active sewage sludge unit on which the sewage sludge is covered and for three years after a sewage sludge unit closes when a final cover is placed on the sewage sludge. (Approved by the Office of Management and Budget under control number 2040-0157) [58 FIR 9387, Feb. 19, 1993, as amended at 64 FIR 42570, Aug. 4, 1999] § 503.27 Recordkeeping. (a) When sewage sludge (other than domestic septage) is placed on an active sewage sludge unit: (1) The person who prepares the sewage sludge shall develop the following information and shall retain the information for five years. (i) The concentration of each pollutant listed in Table 1 of §503.23 in the sewage sludge when the pollutant concentrations in Table 1 of §503.23 are met. (ii) The following certification statement: I certify, under penalty of law, that the information that will be used to determine compliance with the pathogen requirements in (insert §503.32(a), §503.32(b)(2), §503.32(b)(3), or §503.32(b)(4) when one of those requirements is met) and the vector attraction reduction requirement in (insert one of the vector attraction reduction requirements in §503.33 (b)(1) through (b)(8) if one of those requirements is met) was prepared under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate this information. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. (iii) A description of how the pathogen requirements in §503.32 (a), (b)(2), (b)(3), or (b)(4) are met when one of those requirements is met. - - (iv) A description of how one of the vector attraction reduction requirements in §503.33 (b)(1) through (b)(8) is met when one of those requirements is met. (2) The owner/operator of the surface disposal site, shall develop the following information and shall retain that information for five years. (i) The concentration of each pollutant listed in Table 2 of §503.23 in the sewage sludge when the pollutant concentrations in Table 2 of §503.23 are met or when site -specific pollutant limits in §503.23(b) are met. (ii) The following certification statement: I certify, under penalty of law, that the information that will be used to determine compliance with the management practices in §503.24 and the vector attraction reduction requirement in (insert one of the requirements in §503.33(b)(9) through §503.33(b)(11) if one of those requirements is met) was prepared under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate this information. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. (iii) A description of how the management practices in §503.24 are met. (iv) A description of how the vector attraction reduction requirements in §503.33 (b)(9) through (b)(1 1) are met if one of those requirements is met. (b) When domestic septage is placed on a surface disposal site: (1) If the vector attraction reduction requirements in §503.33(b)(12) are met, the person who places the domestic septage on the surface disposal site shall develop the following information and shall retain the information for five years: (i) The following certification statement: I certify, under penalty of law, that the information that will be used to determine compliance with the vector attraction' reduction requirements in §503.33(b)(12) was prepared under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate this information. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. i . (ii) A description of how the vector attraction reduction requirements in §503.33(b)(12) are met. (2) The owner/operator of the surface disposal site shall develop the following information and shall retain that information for five years: (i) The following certification statement: I certify, under penalty of law, that the information that will be used to determine compliance with the.;:. management practices in §503:24 and the vector attraction reduction requirements in (insert §5.03.33(b)(9) through §503.33(b)(11) if one of those requirements is met) was prepared under my direction and`supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate this information. I am aware that there are significant penalties for false certification including the possibility of- fine or imprisonment. - (ii) A description of how the management practices in §503.24 are met. (iii) A description how the vector attraction reduction requirements in §503.33(b)(9) through §503.33(b)(11) are met if one of those requirements is met. (Approved by the Office of Management and Budget under control number 2040-0157) [58 FR 9387, Feb.,19, 1993, as amended at 64 FR 42571, Aug. 4, 1999] § 503.28 Reporting. Class I sludge management facilities, POTWs (as defined in 40 CFR 501.2) with a design flow rate equal to or greater than one million gallons per day, and POTWs that serve 10,000 people or more shall submit the information in §503.27(a) to the permitting authority on February 19 of each year. (Approved by the Office of Management and Budget under control number 2040-0157) Subpart D—Pathogens and Vector Attraction Reduction § 503.30 Scope. (a) This subpart contains the requirements for a sewage sludge to be classified either Class A or Class B with respect to pathogens. (b) This subpart contains the site restrictions for land on which a Class B sewage sludge is applied.-- (c) This subpart contains the pathogen requirements for domestic septage applied to agricultural land, forest, or a reclamation site. (d) This subpart contains alternative vector attraction reduction requirements for sewage sludge that is applied to the land or placed on a surface disposal site. § 503.31 Special definitions. (a) Aerobic digestion is the, biochemical decomposition of organic matter in sewage sludge into carbon dioxide and water by microorganisms in the presence of air. (b) Anaerobic digestion is the biochemical decomposition of organic matter in sewage sludge into methane gas and carbon dioxide by microorganisms in the absence of air. (c) Density of microorganisms is the number of microorganisms per unit mass of total solids (dry weight) in the sewage sludge. (d) Land with a high potential for public exposure is land that the public uses frequently. This includes, but is not limited to, a public contact site and a reclamation site located in a populated area (e.g, a construction site located in a city). (e) Land with a low potential for public exposure is land that the public uses infrequently. This includes; but is not limited to, agricultural land, forest, and a reclamation site located in an unpopulated area (e.g., a strip mine located in a rural area)... (f) Pathogenic organisms are disease -causing organisms. These include, but are not limited to, certain bacteria, protozoa, viruses, and viable helminth ova. (g) pH means the logarithm of the reciprocal of the hydrogen ion concentration measured at 25 *Centigrade or measured at another temperature and then converted to an equivalent value at 25 .°Centigrade. (h) Specific oxygen uptake rate (SOUR) is the mass of oxygen consumed per unit time per unit mass of total solids (dry weight basis) in the sewage sludge. (i) Total solids are the materials in sewage sludge that remain as residue when the sewage sludge is dried at 103 to 105 degrees Celsius. 0) Unstabilized solids are organic materials in sewage sludge that have not been treated in either an aerobic or anaerobic treatment process. (k) Vector attraction is the characteristic of sewage sludge that attracts rodents, flies, mosquitos, or other organisms capable of transporting infectious agents. (1) Volatile solids is the amount of the total solids in sewage sludge lost when the sewage sludge is combusted at 550 degrees Celsius in the presence of excess air. [58 FR 9387, Feb. 19,' 1993, as amended at 64 FR 42571, Aug. 4, 1999] § 503.32 Pathogens. (a) Sewage sludge —Class A. (1) The requirement in §503.32(a)(2) and the requirements in either §503.32(a)(3), (a)(4), (a)(5), (a)(6), (a)(7), or (a)(8) shall be met for a sewage sludge to be classified Class A with respect to pathogens. (2) The Class A pathogen requirements in §503.32 (a)(3) through (a)(8) shall be met either prior to meeting or at the same time the vector attraction reduction requirements in §503.33, except the vector attraction reduction requirements in §503.33 (b)(6) through (b)(8), are met. 1((3) Class A —Alternative 1. (i) Either the density of fecal coliform in the sewage sludge shall be less than 1000 Most Probable Number per gram of total solids (dry weight basis), or the density of Salmonella sp. bacteria in the sewage sludge shall be less than three Most Probable Number per four grams of total solids (dry weight basis) at the time the sewage sludge is used or disposed; at the time the sewage sludge is prepared for sale or give away in a bag or other container for application to the land; or at the time the sewage sludge or material derived from sewage sludge is prepared to meet the requirements in §503.10 (b), (c), (e), or (f). (ii) The temperature of the sewage sludge that is used or disposed shall be maintained at a specific value for a period of time. (A) When the percent solids of the sewage sludge is seven percent or higher, the temperature of the sewage sludge §hall be 50 degrees Celsius or higher; the time period shall be 20 minutes or longer; and the temperature and time period shall be determined using equation (2), except when small particles of sewage sludge are heated by either warmed gases or an immiscible liquid. __ 131,700, 000 100.1400r Eq. (2) Where, D=time in days. t=temperature in degrees Celsius. (B) When the percent solids of the sewage sludge is seven percent or higher and small particles of sewage sludge are heated by either warmed gases or an immiscible liquid, the temperature of the sewage sludge shall be 50 degrees Celsius or higher; the time period shall be 15 seconds or longer; and the temperature and time period shall be determined using equation (2). (C) When the percent solids of the sewage sludge is less than seven percent and the time period is at least 15 seconds, but less than 30 minutes, the temperature and time period shall be determined using equation (2) (D) When the percent solids of the sewage sludge is less than seven percent; the temperature of the sewage sludge is 50 degrees Celsius or higher; and the time period is 30 minutes or longer, the temperature and time period shall be determined using equation (3). 50, 070, 000 = 100.14001 Eq. (3 Where, D=time in days. t=temperature in degrees Celsius. (4) Class A Alternative 2. (i) Either the density of fecal coliform in the sewage sludge shall be less than 1000 Most Probable Number per gram of total solids (dry weight basis), or the density of Salmonella sp. bacteria in the sewage sludge shall be less than three Most Probable Number per four grams of total. solids (dry weight basis) at the time the sewage sludge is used or disposed; at the time the sewage sludge is prepared for sale or give away in a bag or other container for application to the land; or at the time the sewage sludge or material derived from sewage sludge is prepared to meet the requirements in §503.10 (b), (c), (e), or (f). (ii)(A) The pH of the sewage sludge that is used or disposed shall be raised to above 12 and shall remain above 12 for 72 hours. (B) The temperature of the sewage sludge shall be above 52 degrees Celsius for 12 hours or longer during the period that the pH of the sewage sludge is above 12. (C) At the end of the 72 hour period during which the pH of the sewage sludge is above 12, the sewage sludge shall be air dried to achieve a percent solids in the sewage sludge greater than 50.percent. (5) Class A —Alternative 3. (i) Either the density of fecal coliform in the sewage sludge shall be less than 1000 . Most,Probable Number per gram of total solids (dry weight basis), or the density of Salmonella sp. bacteria in sewage sludge shall be less than three Most Probable Number per four grams of total solids (dry weight basis) at the time the sewage sludge is used or disposed; at the time the sewage sludge is prepared for sale or give away in a bag or other container for application to the land; or at the time the sewage sludge or material derived from sewage sludge is prepared to meet the requirements in §503.10 (b), (c), (e), or (f). (ii)(A) The sewage sludge shall be analyzed prior to pathogen treatment to determine whether the, sewage sludge contains enteric viruses. (B) When the density of enteric viruses in the sewage sludge prior to pathogen treatment is less than one Plaque -forming Unit per four grams of total solids (dry weight basis), the sewage sludge is Class A with respect to enteric viruses until the next monitoring episode for the sewage sludge. (C) When the density of enteric viruses in the sewage sludge prior to pathogen treatment is equal to or greater than one Plaque -forming Unit per four grams of total solids (dry weight basis), the sewage slud9e.is Class A with respect to enteric viruses when the density of enteric viruses in the sewage sludge. after; pathogen treatment is less than one Plaque -forming Unit per four grams of total solids (dry weight basis) and.. when the values or ranges of values for the operating parameters for the pathogen treatment process that produces the sewage sludge that meets the enteric virus density requirement are documented. (D) After the enteric virus reduction in paragraph (a)(5)(ii)(C) of this section is demonstrated for the pathogen treatment. process, the sewage sludge continues to be Class A with respect to enteric viruses when,the "' values for the pathogen treatment process operating parameters are consistent with the values or ranges of values documented in paragraph (a)(5)(ii)(C) of this section. (iii)(A) The sewage sludge shall be analyzed prior to pathogen treatment to determine whether the sewage sludge contains viable helminth ova. (B) When the density of viable helminth ova in the sewage sludge prior to pathogen treatment..is,less than* one per four grams of total solids (dry weight basis), the sewage sludge is Class A with respect to viable helminth ova until the next monitoring episode for the sewage sludge. (C) When the density of viable helminth ova in the sewage sludge prior to pathogen treatment is equal to or greater than one per four grams of total solids (dry weight basis), the sewage sludge is Class A with respect to viable helminth ova when the density of viable helminth ova in the sewage sludge after pathogen treatment is less than one per four grams of total solids (dry weight basis) and when the values or ranges of values for the operating parameters for -the pathogen treatment process that produces the sewage sludge that meets the viable helminth ova density requirement are documented. (D) After the viable helminth ova reduction in paragraph (a)(5)(iii)(C) of this section is demonstrated for the pathogen treatment process, the sewage sludge continues to be Class A with respect to viable helminth ova when the values for the pathogen treatment process operating parameters are consistent with the values or ranges of values documented in paragraph (a)(5)(iii)(C) of this section. (6) Class A Alternative 4. (i)' Either the density of fecal coliform in the sewage sludge shall be less than 1000 Most Probable Number per gram of total solids (dry weight basis), or the density of Salmonella sp. bacteria in the sewage sludge shall be less than three Most Probable Number per four grams of total solids (dry weight basis) at the time the sewage sludge is used or disposed; at the time the sewage sludge is prepared for'sale or give away in a bag or other container for application to the land; or at'the time the sewage sludge or material derived from sewage sludge is prepared to meet the requirements in §503.10 (b), (c), (e), or (f). (ii) The density of enteric viruses in the sewage sludge shall be less than one Plaque -forming Unit per four grams of total solids (dry weight basis) at the time the sewage sludge is used or disposed; at the time -the sewage sludge is prepared for sale or give away in a bag or other container for application to the land; or at the time the sewage sludge or material derived from sewage sludge is prepared to meet the requirements in §503.10 (b), (c), (e), or (f), unless otherwise specified by the permitting authority. (iii) The density of viable helminth ova in the sewage sludge shall be less than one per four grams of total solids (dry weight basis) at the time the sewage sludge is used or disposed; at the time the sewage sludge is prepared for sale or give away in a bag or other container for application to the land; or at the time the sewage sludge or material derived from sewage sludge is prepared to meet the requirements in §503.10 (b), (c), (e), or (f), unless otherwise specified by the permitting authority. (7) Class A —Alternative 5. (i) Either the density of fecal coliform in the sewage sludge shall be less than 1000 Most Probable Number per gram of total solids (dry weight basis), or the density of Salmonella, sp'. bacteria in the sewage sludge shall be less than three Most Probable Number per four grams of total solids (dry weight basis) at the time the sewage sludge is used or disposed; at the time the sewage sludge is prepared for sale or given away in a bag or other container for application to the land; or at the time the sewage sludge or material derived from sewage sludge is prepared to meet the requirements in §503.10(b), (c), (e), or (f). (ii) Sewage sludge that is used or disposed shall be treated in one of the Processes to Further Reduce Pathogens described in appendix B of this part. k(8) Class A Alternative 6. (i) Either the density of fecal coliform in the sewage sludge shall be less than 1000 Most Probable Number per gram of total solids (dry weight basis), or the density of Salmonella, sp. bacteria in the sewage sludge shall be less than three Most Probable Number per four grams of total solids (dry weight basis) at the time the sewage sludge is used or disposed; at the time the sewage sludge is prepared for sale or given away in a bag or other container for application to the land; or at the time the sewage sludge or material derived from sewage sludge is prepared to meet the requirements in §503.10(b), (c), (e), or (f). (ii) Sewage sludge that is used or disposed shall be treated in a process that is equivalent to a Process to Further Reduce Pathogens, as determined by the permitting authority. (b) Sewage sludge —Class B. (1)(i) The requirements in either §503.32(b)(2), (b)(3), or (b)(4) shall be met for a sewage sludge to be classified Class B with respect to pathogens. (ii) The site restrictions in §503.32(b)(5) shall be met when sewage sludge that meets the Class B pathogen requirements in §503.32(b)(2), (b)(3), or (b)(4) is applied to the land. (2) Class B—Alternative 1. (i) Seven representative samples of the sewage sludge that is used or disposed shall be collected. (ii) The geometric mean of the density of fecal coliform in the samples collected in paragraph (b)(2)(i) of this section shall be less than either. 2,000,000 Most Probable Number per gram of total solids (dry weight basis) or 2,000,000 Colony Forming Units per gram of total solids (dry weight basis). (3) Class B—Alternative 2. Sewage sludge that is used or disposed shall be treated in one of the Processes to Significantly Reduce Pathogens described in appendix B of this part. X. (4) Class B—Alternative 3. Sewage sludge that is used or disposed shall be treated in a process that is equivalent to a Process to Significantly Reduce Pathogens, as determined by the permitting authority. (5) Site restrictions. (i) Food crops with harvested parts that touch the sewage sludge/soil mixture and are totally above the land surface shall not be harvested for 14 months after application of sewage sludge. (ii) Food crops with harvested parts below the surface of the land shall not be harvested for 20 months after application of sewage sludge when the sewage sludge remains on the land surface for four months or longer prior to incorporation into the soil. (iii) Food crops with harvested parts below the surface of the land shall not be harvested for 38 months after application of sewage sludge when the sewage sludge remains on the land surface for less than four months prior to incorporation into the soil. (iv) Food crops, feed crops, and fiber crops shall not be harvested for 30 days after application of sewage sludge. (v) Animals shall not be grazed on the land for 30 days after application of sewage sludge. (vi) Turf grown on land where sewage sludge is applied shall not be harvested for one year after application of the sewage sludge when the harvested.turf is placed on either land with a high potential for public exposure or a lawn, unless otherwise specified by the permitting authority. (vii) Public access to land with a high potential for public exposure shall be restricted for one year after application of sewage sludge. (viii) Public access to land with a low potential for public exposure shall be restricted for 30 days after -application of sewage sludge. (c) Domestic septage. (1) The site restrictions in §503.32(b)(5) shall be met when domestic septage is applied to agricultural land, forest, or a reclamation site; or (2) The pH of domestic septage applied to agricultural land, forest, or -a reclamation site shall be raised to 12 or higher by alkali addition and, without the addition of more alkali, shall remain at 12 or higher for 30 minutes and the site restrictions in §503.32 (b)(5)(i) through (b)(5)(iv) shall be met. [58 FR 9387, Feb. 19, 1993, as amended at 64 FR 42571, Aug. 4, 1999] k§ 503.33 Vector attraction reduction. 7� (a)(1) One of the vector attraction reduction requirements in §503.33 (b)(1) through (b)(10) shall be met when bulk sewage sludge is applied to agricultural land, forest, a public contact site, or a reclamation site. (2) One of the vector attraction reduction requirements in §503.33 (b)(1) through (b)(8) shall be met when bulk sewage sludge is applied to a lawn or a home garden. *3) One of the vector attraction reduction requirements in §503.33 (b)(1) through (b)(8) shall be met when sewage sludge is sold or given away in a bag or other container for application to the land. A(4) One of the vector attraction reduction requirements in §503.33 (b)(1) through (b)(1 1) shall be met when sewage sludge (other than domestic septage) is placed on an active sewage sludge unit. (5) One of'the vector attraction reduction requirements in §503.33 (b)(9), (b)(10), or (b)(12) shall be met when domestic septage is applied to agricultural land, forest, or a reclamation site and one of the vector attraction reduction requirements in §503.33 (b)(9) through (b)(12) shall be met when domestic septage is placed on an active sewage sludge unit. (b)(1) The mass of volatile solids in the sewage sludge shall be reduced by a minimum of 38 percent (see calculation procedures in "Environmental Regulations and Technology —Control of Pathogens and Vector Attraction in Sewage Sludge") EPA-625/R-92/013, 1992, U.S. Environmental Protection Agency, Cincinnati, Ohio 45268). (2) When the 38 percent volatile solids reduction requirement in §503.33(b)(1) cannot be met for an. anaerobically digested sewage sludge, vector attraction reduction can be demonstrated by digesting a portion of the previously digested sewage sludge anaerobically in the laboratory in a bench -scale unit for 40 additional days at a temperature between 30 and 37 degrees Celsius. When at the end of the 40 days, the volatile solids in the sewage sludge at the beginning of that period is reduced by less than 17 percent, vector attraction reduction is achieved. (3) When the 38 percent volatile solids reduction requirement in §503.33(b)(1) cannot be met for an aerobically digested sewage sludge, vector attraction reduction can be demonstrated by digesting a portion of the previously digested sewage sludge that has a percent solids of two percent or less, aerobically in the laboratory in a bench -scale unit for 30 additional days at 20 degrees Celsius. When afthe end of the 30 days, the volatile solids in the sewage sludge at the beginning of that period is reduced by less than 15 percent, vector attraction reduction is achieved. (4) The specific oxygen uptake rate (SOUR) for sewage sludge treated in an aerobic process shall be equal to or less than 1.5 milligrams of oxygen per hour per gram of total:solids (dry weight basis) at a temperature of 20 degrees Celsius. (5) Sewage sludge shall be treated in an aerobic process for 14 days or longer. During that time, the temperature of the sewage sludge shall be higher than 40 degrees Celsius and the average temperature of the sewage sludge shall be higher than 45 degrees Celsius. (6) The pH of sewage sludge shall be raised to 12 or higher by alkali addition and, without the addition of more alkali, shall remain at 12 or higher for two hours and then at 11.'5 or higher for an additional'22 hours. (7) The percent solids of sewage sludge that does not contain unstabilized solids generated in a primary wastewater treatment process shall be equal to or greater than 75 percent, based on the moisture content: and total solids prior to mixing with other materials. (8) The percent solids of sewage sludge that contains unstabilized solids generated in a primary wastewater treatment process shall be equal to or greater than 90 percent based on the moisture content and total solids prior to mixing with other materials. (9)(i) Sewage sludge shall be injected below the surface of the land. (ii) No significant amount of the sewage sludge shall be present' on the land surface within one hour after the sewage sludge is injected. (iii) When the sewage sludge that is injected below the surface of the land is Class A with respect to pathogens; the sewage sludge shall be injected below the land surface within eight hours after being discharged from the pathogen treatment process. (10)(i) Sewage sludge applied to the land surface or placed on an active sewage sludge unit shall be incorporated into the soil within six hours after application to or placement on the land, unless'otherwise specified by the permitting authority: (ii) When sewage sludge that is incorporated into. the soil is Class A with respect to pathogens, the sewage sludge shall be applied to or placed on the land within eight hours after being discharged from the pathogen treatment process. (11) Sewage sludge placed on an active sewage sludge unit shall be covered. with soil or other material at the end of each operating day. (12) The pH of domestic septage shall be raised to 12 or higher by alkali addition and, without the addition of more alkali, shall remain at 12 or higher -for 30 minutes. [58 FIR,9387, Feb. 19, 1993, as amended at 64 FIR 42571, Aug. 4, 1999] Subpart E—Incineration § 503.40 Applicability. (a) This subpart applies to a person who fires sewage sludge in a sewage sludge incinerator, to a sewage sludge' incinerator, and to sewage sludge fired in a sewage sludge incinerator. (b) This subpart applies to the exit gas from a sewage sludge incinerator stack. (c) The management practice in §503,:45(a), the frequency of monitoring requirement for total hydrocarbon concentration in §503.46(b) and the recordkeeping requirements for total hydrocarbon concentration in §503.47(c) and (n) do not apply if the following conditions are met: (1) The exit gas from a sewage sludge incinerator stack is monitored continuously for carbon monoxide. (2) The monthly average concentration of carbon monoxide in the exit gas from a sewage sludge incinerator stack, corrected for zero percent moisture and to seven percent oxygen, does not exceed 100 parts per million on a volumetric basis. (3) The person who fires sewage sludge in a sewage sludge incinerator retains the following information for five years: (i) The carbon monoxide concentrations in the exit gas; and (ii) A calibration and maintenance log for the instrument used to measure the carbon monoxide concentration. (4) Class I sludge management facilities, POTWs (as defined in 40 CFR 501.2) with a design flow rate equal to or greater than one million gallons per day, and POTWs that serve a population of 10,000 people or greater submit the monthly average carbon monoxide concentrations in the exit gas.to the permitting authority on February 19 of each year. [58 FR 9387, Feb. 19, 1993, as amended' at 59 FR 9099, Feb. 25, 1994] § 503.41 Special definitions. (a) Air pollution control device is one or more processes used to treat the exit gas from a sewage sludge incinerator stack. (b) Auxiliary fuel is fuel used to augment the fuel value of sewage sludge. This includes, but is not limited to, natural gas, fuel oil, coal, gas generated during anaerobic digestion of sewage sludge, and municipal solid waste (not to exceed 30 percent of the dry weight of sewage sludge and auxiliary fuel together). Hazardous wastes are not auxiliary fuel. (c) Average daily concentration is the arithmetic mean of the concentration of a pollutant in milligrams per kilogram of sewage sludge (dry weight basis) in the samples collected and analyzed in a month. (d) Control efficiency is the mass of a pollutant in the sewage sludge fed to an incinerator minus the mass of that pollutant in the exit gas from the incinerator stack divided by the mass of the pollutant in the sewage sludge fed to the incinerator. (e) Dispersion factor is the ratio of the increase in the ground level ambient air concentration for a pollutant at or beyond the property line of the site where the sewage sludge incinerator is located to the mass emission rate for the pollutant from the incinerator stack. (f) Fluidized bed incinerator is an enclosed device in which organic matter and inorganic matter in sewage sludge are combusted in a bed of particles suspended in the combustion chamber gas. . (g) Hourly average is the arithmetic mean of all measurements, taken during an hour. At least two measurements must be taken during the hour. (h) Incineration is the combustion bf organic matter and inorganic matter in sewage sludge by high temperatures in.an enclosed device. (i) Incinerator operating combustion temperature is the arithmetic mean of the temperature readings in the hottest zone of the furnace recorded in a day (24 hours) when the temperature is averaged and recorded at least hourly during the hours the incinerator operates in a day. Q) Monthly average is the arithmetic mean of the hourly averages for the hours a sewage sludge incinerator operates during the month. (k) Performance test combustion temperature is the arithmetic mean of the average combustion temperature in the hottest zone of the furnace for each of the runs in a performance test. (1) Risk specific concentration is the allowable increase in the average daily ground level ambient air concentration for a pollutant from the incineration of sewage sludge at or beyond the property line of the site where the sewage sludge incinerator is located. (m) Sewage sludge feed rate is either the average daily amount of sewage sludge fired in all sewage sludge incinerators within the property line of the site where the sewage sludge incinerators are located for the number of days in a 365 day period that each sewage sludge incinerator operates, or the average daily design capacity for all sewage sludge incinerators within the property line of the site where the sewage sludge incinerators are located. (n) Sewage sludge incinerator is an enclosed device in which only sewage sludge and auxiliary fuel are,fired. (o)Stack height is the difference between the elevation of the top of a sewage sludge incinerator stack and the elevation of the ground at the base of the stack when the difference is equal to or less than 65 meters. When'the difference is greater than 65 meters, stack height is the creditable stack height determined in accordance with 40 CFR 51.100 (ii). (p) Total hydrocarbons means the organic compounds in the exit gas from a sewage sludge incinerator stack measured using a flame ionization detection instrument referenced to propane. (q) Wet electrostatic precipitator is an air pollution control device that uses both electrical forces .and water to remove pollutants in the exit gas from a sewage sludge incinerator stack. (r) Wet scrubber is an air pollution control device that uses water to remove pollutants in the exit gas from a sewage sludge incinerator stack. [58 FR 9387, Feb. 19, 1993, as amended at 64 FR 42571, Aug. 4, 1999] § 503.42 General requirements. No person shall fire sewage sludge in a sewage sludge incinerator except in compliance With the requirements in this subpart. § 503.43 Pollutant limits. (a) Firing of sewage sludge in a sewage sludge incinerator shall not violate the requirements in the National Emission Standard for Beryllium in subpart C of 40 CFR part 61. (b) Firing of sewage sludge in a sewage sludge incinerator shall not violate the requirements in the National Emission Standard for Mercury in subpart E of 40 CFR part 61. (c) Pollutant limit -lead. (1) The average daily concentration for lead in sewage sludge fed to a sewage sludge incinerator shall not exceed the concentration calculated using Equation (4). 0.1xALAAQSx86,400 C= DFx(1.-CE)xSF Eq. (4) Where: C = Average daily concentration of lead in sewage "sludge. NAAQS = National Ambient Air Quality Standard for lead in micrograms per cubic meter. DF = Dispersion factor'in micrograms.per cubic meter per gram per second. CE = Sewage sludge incinerator control efficiency for lead in hundredths. SF = Sewage sludge feed rate in metric tons per day (dry weight basis). ' (2) The dispersion factor (DF) in equation (4) shall be determined from an air dispersion model in accordance with §503.43(e). (i) When the sewage sludge stack height is 65 meters or less, the actual sewage sludge incinerator stack height shall be used in the air dispersion model to determine the dispersion factor (DF) for equation (4). (ii) When the sewage sludge incinerator stack height exceeds 65 meters, the creditable stack height shall be determined in accordance with 40 CFR 51.100(ii) and the creditable stack height shall be used in the air dispersion model to determine the dispersion factor (DF) for equation (4). (3) The control efficiency (CE) for equation (4) shall be determined from a performance test of the sewage sludge incinerator in accordance with §503.43(e). (d) Pollutant limit —arsenic, cadmium, chromium, and nickel. (1) The average daily concentration for arsenic, cadmium, chromium, and nickel in sewage sludge fed to a sewage sludge incinerator each shall. -not exceed the concentration calculated using equation (5). C = RSCx86,400 E DFx(1— CE) xSF q. ( 5 ) Where: C = Average daily concentration of arsenic, cadmium, chromium, or nickel in sewage sludge.. CE = Sewage sludge incinerator control efficiency for arsenic, cadmium, chromium, or nickel in. hundredths. DF = Dispersion factor in micrograms per cubic meter per gram,per second. RSC = Risk specific concentration for arsenic, cadmium, chromium, or nickel in micrograms per cubic meter. SF = Sewage sludge feed rate in metric tons per day (dry weight basis). ' (2) The risk specific concentrations for arsenic, cadmium, and nickel used in equation (5) shall be obtained from Table 1 of §503.43. Table 1 of §503.43—Risk Specific Concentration -for Arsenic. Cadmium. and Nickel Pollutant Risk specific concentration (micrograms per cubic meter) Arsenic 0.023 Cadmium 0.057 Nickel 12.0 (3) The risk specific concentration for chromium used in equation (5) shall be obtained from Table 2 of §503.43 or shall be calculated using equation (6). Table 2 of 5. 03.43—Risk Specific Concentration For Chromium of Incinerator uidized bed with wet scrubber bed with wet scrubber and wet electrostatic with wet scrubber with wet scrubber and wet electrostatic Risk specific concentration (micrograms per cubic meter) 0.65 0.23 0.064 0.016 precipitator RSC = 0.0085 Eq (o) r Where: RSC=risk specific concentration for chromium in micrograms per cubic meter used in equation (5). r=decimal fraction of the hexavalent chromium concentration in the total chromium concentration measured in the exit gas from the sewage sludge incinerator stack in hundredths. (4) The dispersion factor (DF) in equation (5) shall be determined from an air dispersion model in accordance with §503.43(e). (i) When the sewage sludge incinerator stack height is equal to or less than 65 meters, the actual sewage sludge incinerator stack height shall be used in the air dispersion model to determine the dispersion factor (DF) for equation (5). (ii) When the sewage sludge incinerator stack height is greater than 65 meters, the creditable stack height shall be determined in accordance with 40 CFR 51.100(ii) and the creditable stack height shall be used in the air dispersion model to determine the dispersion factor (DF) for equation (5). (5) The control efficiency (CE) for equation (5) shall be determined from a performance test of the sewage sludge incinerator in accordance with §503.43(e). (e) Air dispersion modeling and performance testing. (1) The air dispersion model used to determine the dispersion factor in §503.43 (c)(2) and (d)(4) shall be appropriate for the geographical, physical, and population characteristics at the sewage sludge incinerator site. The performance test used to determine the control efficiencies in §503.43 (c)(3) and (d)(5) shall be appropriate for the type of sewage sludge incinerator. (2) For air dispersion modeling initiated after September 3, 1999, the modeling results shall be submitted to the permitting authority 30 days after completion of the modeling. In addition to the modeling results, the submission shall include a description of the air dispersion model and the values used for the model parameters. (3) The following procedures, at a minimum, shall apply in conducting performance tests to determine the control efficiencies in §503.43(c)(3) and (d)(5) after September 3, 1999: (i) The performance test shall be conducted under representative sewage sludge incinerator conditions at the highest expected sewage sludge feed rate within the design capacity of the sewage sludge incinerator. (ii) The permitting authority shall be notified at least 30 days prior to any performance test so the permitting authority may have the opportunity to observe the test. The notice shall include a test protocol with incinerator operating conditions and a list of test methods to be used. (iii) Each performance test shall consist of three separate runs using the applicable test method. The control efficiency for a pollutant shall be the arithmetic mean of the control efficiencies for the pollutant from the three runs. (4) The pollutant limits in §503.43 (c) and (d) of this section shall be submitted to the permitting authority no later than 30 days after completion of the air dispersion modeling and performance test. (5) Significant changes in geographic or physical characteristics at the incinerator site or in incinerator operating conditions require new air dispersion modeling or performance testing to determine a new dispersion factor or a new control efficiency that will be used to calculate revised pollutant limits. [58 FIR 9387, Feb. 19, 1993, as amended at 64 FIR 42572, Aug. 4, 1999] § 503.44 Operational standard —total hydrocarbons. (a) The total hydrocarbons concentration in the exit gas from a sewage sludge incinerator shall be corrected for zero percent moisture by multiplying the measured total hydrocarbons concentration by the correction factor calculated using equation (7). Correction factor 1 Eq. (7) (percent moisture) (I Where: X=decimal fraction of the percent moisture in the sewage sludge incinerator exit gas in hundredths. (b) The total hydrocarbons concentration in the exit gas from a sewage sludge incinerator shall be corrected to seven percent oxygen by multiplying the measured total hydrocarbons concentration by the correction factor calculated using equation (8).. Correction factor 14 _ (oxygen) (21— Y) (8) Where: Y=Percent oxygen concentration in the sewage sludge incinerator stack exit gas (dry volume/dry volume). 9' (c) The monthly -average concentration for total hydrocarbons in the exit gas from a sewage sludge incinerator stack, corrected for zero percent moisture using the correction factor from equation (7) and to seven percent oxygen Using the correction factor from equation (8), shall not exceed 100 parts per million on a volumetric basis when measured using the instrument required by §503.45(a). § 503.45 Management practices. (a)(1) An instrument that continuously measures and records the total hydrocarbons concentration in the sewage sludge incinerator stack exit gas shall be installed, calibrated, operated, and maintained for a sewage sludge incinerator: (2) The total hydrocarbons instrument shall employ a flame ionization detector; shall have a heated sampling line maintained at a temperature of 150 degrees Celsius or higher at all times, and shall be calibrated at least once every 24-hour operating period using propane. (b) An instrument that continuously measures and records the oxygen concentration in the sewage sludge incinerator stack exit gas shall be installed, calibrated, operated, and maintained for a sewage-aludge ,:, incinerator. (c) An instrument that continuously measures and records information used to determine the moisture content in the sewage sludge incinerator stack exit gas shall be installed;. calibrated, operated, and maintained for a sewage sludge incinerator. (d) An instrument that continuously measures and records combustion temperatures shall be installed, calibrated, operated, and maintained'for a sewage sludge incinerator. (e) Operation of a sewage sludge incinerator shall not cause the operating combustion temperature for the sewage sludge incinerator to exceed the performance test combustion temperature by more than 20 percent. (f) An air pollution control device shall be appropriate for the type of sewage sludge incinerator and the operating parameters for the air pollution control device shall be adequate to indicate proper performance of the air pollution control device: For sewage sludge incinerators subject to the requirements in subpart O of 40 CFR part 60, operation of the air pollution control device shall not violate the requirements for the air pollution control device in subpart O of 40 CFR part 60. For all other sewage sludge incinerators, operation of the air pollution control device'shall not cause a significant exceedance of the average value Ifor the air pollution control device operating parameters from the performance test required by §503.43 (c)(3) and (d)(5). (g) Sewage sludge shall not be fired in a sewage sludge incinerator if it is likely to adversely affect a threatened or endangered species listed under section 4 of the Endangered Species Act or its designated critical habitat. (h) The instruments required in §'503.45(a)-(d) shall be appropriate for the type of.sewage sludge incinerator. [58 FIR 9387, Feb. 19, 1993, as amended at 64 FIR 42573, Aug. 4, 1999] § 503.46 Frequency of monitoring. (a) Sewage sludge. (1) The frequency of monitoring for beryllium shall be as required in subpart C of 40 CFR part 61, and for mercury as required in subpart E of 40 CFR part 61. (2) The frequency of monitoring for arsenic, cadmium, chromium, lead, and nickel in sewage sludge fed to a sewage sludge incinerator shall be the frequency in Table 1 of §503.46. Table 1 of §503.46—Frequency of Monitorinq—Incineration Amount of sewage sludge1(metric tons per 365 day period) Frequency Greater than zero but less than 290 Once per year. Equal to or greater than 290 but less than 1,500 Once per quarter (four times per year). Equal to or greater than 1,500 but less than 15,000 Once per 60 days (six times per year). Equal to or greater than 15,000 Once per, month (12 times per year). 1Amount of sewage sludge fired in a sewage sludge incinerator (dry weight basis). (3) After the sewage sludge has been monitored for two years at the frequency in Table 1 of §503.46, the permitting authority may reduce the frequency of monitoring for arsenic, cadmium, chromium, lead; and nickel. (b) Total hydrocarbons, oxygen concentration, information to determine moisture content, and combustion temperatures. The total hydrocarbons concentration and oxygen concentration in the exit gas from a sewage sludge incinerator stack, the information used to measure moisture content in the exit gas, and the combustion temperatures for the sewage sludge incinerator shall be monitored continuously. (c) Air pollution control device operating parameters. For sewage sludge incinerators subject to the requirements in subpart 0 of 40 CFR part 60, the frequency of monitoring for the appropriate air pollution control device operating parameters shall be the frequency of monitoring in subpart O of 40 CFR part 60. For all other sewage sludge incinerators, the appropriate air pollution control device operating parameters shall be at least daily. (Approved by the Office of Management and Budget under control number 2040-0157) [58 FR 9387, Feb. 19, 19.93, as amended at 64 FR 42573, Aug. 4, 1999] - § 503.47 Recordkeeping. (a) The person who fires sewage sludge in a sewage sludge incinerator shall develop the information in §503.47(b) through §503.47(n) and shall retain that information for five years. (b) The concentration of lead, arsenic, cadmium, chromium, and nickel in the sewage sludge fed to the sewage sludge incinerator. (c) The total hydrocarbons concentrations in the exit gas from the sewage sludge incinerator stack. (d) Information that indicates the requirements in the National Emission Standard for beryllium in subpart C of 40 CFR part 61 are met. (e) Information that indicates the requirements in the National Emission Standard for mercury in subpart E of 40 CFR part 61 are met. (f) The operating combustion temperatures for the sewage sludge incinerator. (g) Values for the air pollution control device operating parameters. (h) The oxygen concentration and information used to measure moisture content in the exit gas from the sewage sludge incinerator stack. (i) The sewage sludge feed rate. 6) The stack height for the sewage sludge incinerator. (k) The dispersion factor for the site where the sewage sludge incinerator is located. (1) The control efficiency for lead, arsenic, cadmium, chromium, and nickel for each sewage sludge incinerator. (m) The risk specific concentration for chromium calculated using equation (6), if applicable. (n) A calibration and maintenance log for the instruments used to measure the total hydrocarbons concentration and oxygen concentration in the exit gas from the sewage sludge incinerator stack, the information needed to determine moisture content in the exit gas, and the combustion temperatures. (Approved by the Office of Management and Budget under control number 2040-0157) [58 FR 9387, Feb. 19, 1993, as amended at 64 FR 42573, Aug. 4, 1999] § 503.48 Reporting. Class I sludge management facilities, POTWs (as defined in 40 CFR 501.2) with a design flow rate equal to or greater than one million gallons per day, and POTWs that serve a population of 10,000 people or. greater shall submit the information in §503.47(b) through §503.47(h) to the permitting authority on February 19 of each year. (Approved by the Office of Management and Budget under control number 2040-0157) Appendix A to Part 503—Procedure To Determine the Annual Whole Sludge Application Rate for a Sewage Sludge Section 503.13(a)(4)(ii) requires that the product of the concentration for each pollutant listed in Table 4 of §503.13 in sewage sludge sold or given away in a bag or other container for application to the land and the annual whole sludge application rate (AWSAR) for the sewage sludge not cause the annual pollutant loading rate for the pollutant in Table 4 of §503.13 to be exceeded. This appendix contains the procedure used to determine the AWSAR for a sewage sludge that does not cause the annual pollutant loading rates in Table 4 of §503.13 to be exceeded. The relationship between the annual pollutant loading rate (APLR) for a pollutant and the annual whole sludge application rate (AWSAR) for 1a sewage sludge is shown in equation (1). APLR =.0 X A WEAR X 0.001 (1) Where: APLR=Annual pollutant loading -rate in -kilograms per hectare per 365 day period. C=Pollutant concentration in milligrams, per kilogram of total solids (dry weight basis). AWSAR=Annual whole sludge application rate in metric tons per hectare per 365 day period (dry weight basis). 0.001=A conversion factor. To determine the AWSAR, equation (1) is rearranged into equation (2): AWSAR = APLR (2) Cx0.001 The procedure.used to determine the AWSAR for a sewage sludge is presented below. Procedure: 1. Analyze a sample of the sewage sludge to determine the concentration for each of the pollutants listed in Table 4 of §503.13 in the sewage sludge. 2. Using the pollutant concentrations from. Step 1 and the APLRs from Table 4 of §503.13, calculate an-_.., AWSAR for each pollutant using equation (2) above. 3. The AWSAR for the sewage sludge is the lowest AWSAR calculated in Step 2. "Appendix .B to Part 503—Pathogen. Treatment Processes A. Processes To Significantly Reduce Pathogens (PSRP) 1. Aerobic digestion —Sewage sludge is agitated with air or oxygen to maintain aerobic conditions for a. specific mean cell residence. time -at a specific temperature. Values for the mean cell residence time and temperature shall be between 40 days at 20 degrees Celsius and 60 days at 15 degrees Celsius. 2. Air drying —Sewage sludge is dried on sand beds or on paved or unpaved"basins.'The sewage -sludge dries fora minimum of.three months. During two of the three months, the ambient average daily temperature . is above zero degrees Celsius. 3.'Anaerobic digestion "Sewage sludge, is treated in. the absence of air for a specific mean cell residence time at a specific temperature. Values for the mean cell residence time and temperature shall be between 15 days at 35 to 55 degrees Celsius and 60 days at 20 degrees Celsius. 4. Composting —Using either the within -vessel, static aerated pile, or windrow composting methods, the temperature of the sewage sludge is raised to 40 degrees Celsius or higher and.remains at 40 degrees Celsius or higher' for. five days. For four hours during the five days, the temperature in the compost pile _ exceeds 55 degrees Celsius. 5. Lime stabilization —Sufficient lime is added to the sewage sludge to raise the pH of the sewage sludge.to 12 after two hours of contact. B. Processes to Further Reduce Pathogens (PFRP) 1. Composting —Using either the within -vessel composting method or the static aerated pile composting method, the temperature of the sewage sludge is maintained at 55 degrees Celsius or higher for three days. Using,the windrow composting method, the temperature'of the sewage sludge is maintained at 55 degrees or higher for 15 days or longer. During the period when the compost is maintained at 55 degrees or. higher, there shall be a.minimum of five turnings of the windrow. 2. Heat drying —Sewage sludge is dried by direct or indirect contact with hot gases to, reduce the moisture content of the sewage sludge to 10 percent or lower. Either the temperature of the sewage sludge particles exceeds 80 degrees Celsius or the wet bulb temperature of the, 'gas- in contact with the sewage sludge as the sewage sludge leaves the dryer exceeds.80 degrees Celsius. 3. Heat tr"eatment—Liquid sewage sludge is heated to a temperature of 180 degrees Celsius or higher for 30 minutes. 4. Thermophilic aerobic digestion —Liquid sewage sludge is agitated with air or oxygen -to maintain aerobic conditions and the mean cell residence time of the sewage sludge is 10 days at 55 to 60 degrees Celsius. 5. Beta ray irradiation —Sewage sludge is irradiated With beta rays from an accelerator at dosages of at least 1.0 megarad at room temperature (ca: 20 degrees'Celsius). (6) Gamma ray irradiation= Sewage sludge is irradiated with gamma rays from certain isotopes, such as60 Cobalt and137 Cesium, at dosages of at least 1.0 megarad at room temperature (ca. 20 'Celsius). 7. Pasteurization=The temperature of the sewage sludge is maintained at 70-degrees Celsius or higher for 30 minutes or longer. [58 FR 9387, Feb. 19, 1993, as amended at 64 FR 42573, Aug. 4, 1999]