NC0021407_Effluent Pollutant Scan_20230215

Action History (UTC-05:00) Eastern Time (US & Canada)
Submit by Anonymous User 2/15/2023 9:35:51 AM (Supplemental Submittal)
Submit by bradley.bennett 6/27/2023 2:09:36 PM (Supplemental Info Submittal)
• The task was assigned to Wren.Thedford, bradley.bennett 2/15/2023 9:35:55 AM
• bradley.bennett assigned the task to bradley.bennett 6/27/2023 9:33:23 AM

Initial Review Information
......... ......... .......................................................................................................................................................................................................................
Updated ID#: * IMPORTANT: REVIEWER SHOULD VERIFY and revise here if necessary.
NCO021407
How should this project be handled?
File Discard
Information Submitted on 2/15/2023
Submitter Information
Name: Mark Teague
Who is submitting the information?
Email Address:* [e-mail]
Submittal Information
The Division of Water Resources (DWR) is providing this site to allow for the upload of required supplemental information
associated with discharge monitoring reports (DMR). All DMR data is required to be submitted electronically through
the eDMR system and should not be submitted here. Division staff will review all uploaded documents and will only
maintain required information. Documents such as laboratory reports are not required to be submitted and will not be
maintained in the system.
Project Information:
Please supply the permit number for this project.
...............................................................................................................................
Existing ID#* Permit Number
NCO021407
Examples: NCxxxxxxx or NCGxxxxxx
Facility Name: * Town of Highlands WWTP
County: Macon
Please upload all files that need to be submited. *
Click the upload button or drag and drop files here to attach document
Town of Highlands Pollutant Scan.pdf 1.89MB
Only pdf files are accepted.
Please provide descriptive comments about the attached information.
Annual pollutant scan
* By checking the box and signing box below, I certify that:
o I have given true, accurate, and complete information on this form;

• I agree that submission of this Supplemental Information form is a "transaction" subject to Chapter 66, Article 40 of the
NC General Statutes (the "Uniform Electronic Transactions Act')
• I agree to conduct this transaction by electronic means pursuant to Chapter 66, Article 40 of the NC General Statutes
(the "Uniform Electronic Transactions Act');
• I understand that an electronic signature has the same legal effect and can be enforced in the same way as a written
signature; AND
• I intend to electronically sign and submit the Supplemental Information form."
Full Name: Mark Teague
Signature:
�tl& 9�rlw
Date Submitted: 02/15/2023

Pace Analytical Services, LLC
2225 Riverside Dr.
1"!;8clemalXical' Asheville. NC 28804
[phone]
ANALYTICAL RESULTS
Project: Town of Highlands WWTP
Pace Project No,: 92593587
Sample: HIGHLANDS WWTP. EFF Lab ID: 92593687001 Collected: 03/15/22 12:05 Received: 03/15/22 16:50 Matrix AAI�f.
Parameters
Results Units Report Limit
I
DF Prepared Analyzed CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Antimony
ND ug/L 5-0
1 03/17/22 03:10 03/17/22 09:38 7440-36-0
Arsenic
ND ug/L 10.0
1 03/17/22 03:10 03/17/22 09:38 7440-38-2
Beryllium
ND ug/L 1.0
1 03/17/22 03:10 03/17/22 09:38 7440-41-7
Cadmium
ND ug/L 1.0
1 03/17/22 03:10 03/17/22 09:38 7440-43-9
Chromium
ND ug/L 5.0
1 03/17/22 03:10 03/17/22 09:38 7440-47-3
Copper
ND Ug/L 5.0
1 03/17/22 03:10 03/17/22 09:38 7440-50-8
Lead
Nickel
ND ug/L. 5.0
1 03/17/22 03:10 03/17/22 09:38 7439-92-1
Selenium
ND ug/L 5,0
1 03117/22 03:10 03/17/22 09:38 7440-02-0
Silver
ND ug/L 10.0
1 03/17/22 03:10 03/17/22 09:38 7782-49-2
Thallium
ND ug/L 5,0
1 03/17/22 0110 03/17/22 09:38 7440-22-4
Hardness, Total(SM 234013)
ND ug/L 10.0
20900 ug/L 662
1 03/17/22 03:10 03/17/22 09:38 7440-28-0
Zinc
1 03/17/22 03:10 03/17/22 09:38
78.4 ug/L 10.0
1 03/17/22 03:10 03/17/22 09:38 7440-66-6 BC
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2015
Pace Analytical Services - Asheville
Total Dissolved Solids
162 mg/L 25.0
1 03/19/22 1119
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2,0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
0.37 rng/L 0A0
1 03/28/22 16:26 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev
Pace Analytical Services - Asheville
2.0 1993
Nitrogen, Kjeldahl, Total
1.8 mg/L 0.50
1 03/24/22 1647 03/25/22 03:14 7727-37-9
353.2 Nitrogen, NO2/NO3 pres.
Analytical Method: EPA 353,2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, NO2 plus NO3
1.1 mg/L 0.040
1 03/25/22 10:26
365.1 Phosphorus, Total
Analytical Method: EPA 365,1 Rev 2,0 1993 Preparation
Method: EPA 365.1 Rev
Pace Analytical Services - Asheville
2.0 1993
Phosphorus
3.1 mg/L 0,050
1 03/24/22 23:01 03/25/22 17:05 7723-14-0
Sample: HIGHLANDS WWTP, Lab ID: 92593587003 Collected: 03/15/22 11:06 Received: 03115/22 16:50 Matrix: Water
UPSTREAM
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200,7 Rev 4A 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
Hardness, Total(SM 234013) 6620 ug/L 662 1 03/17/22 03:10 03/17/22 09:41
Date: 04/27/2022 11:43 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
Page 5 of 38

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Town of Highlands WVVTP
Pace Project No.,: 92593587
Sample: HIGHLANDS WWTR EFF
Lab ID: 92693687004 Collected:
03/15122 12:10
Received; 03/15/22 16:50 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared Analyzed
CAS No. Qua]
626 RVE
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/L.
4.5
1
03/21/22 09:48 03/21/22 19:54
83-32-9
Acenaphthylene
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
208-96-8
Anthracene
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
120-12-7
Benzo(a)anthracene
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
56-55-3
Benzo(a)pyrene
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
50-32-8
Benzo(b)fluoranthene
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
191-24-2
Benzo(k)fluoranthene
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
4.5
1
03/21122 09:48 03/21/22 19:54
101-55-3
Butylbenzylphtha late
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
85-68-7
4-C hioro-3-methyl phenol
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
9.1
1
03/21/22 09:48 03/21/22 19:54
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
111-44-4
2-Chloronaphthalene
ND
ug/L
4.5
1
03/21/22 0948 03/21/22 19:54
91-58-7 L2
2-Chlorophenol
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
7005-72-3
Chrysene
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
218-01-9
Dibenz(a,h)anthraGene
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
9.1
1
03/21/22 09A8 03/21/22 19:54
91-94-1
2,4-Dichlorophenol
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
120-83-2
Di ethylphtha late
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
84-66-2
2A-D irnethyl phenol
ND
ug/L
9.1
1
03/21/22 09:48 03/21/22 19:54
105-67-9
Dimethylphthalate
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
131-11-3
Di-n-butylphthalate
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
84-74-2
4,6-Dinitro-2-methylphenol
ND
uq/L
9.1
1
03/21/22 09:48 03/21/22 19:54
534-52-1
2,4-Dinitrophenof
ND
ug/L
45,5
1
03/21/22 09:48 03/21/22 19:54
51-28-5
2,4-Dinitrotoluene
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
121-14-2
2,6-Dinitrotoluelie
ND
Ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
606-20-2
Di -n-octylphtha late
ND
ug/L
4,5
1
03/21/22 09:48 03/21/22 19:54
117-84-0
bis (2- Ethyl hexyl) phtha late
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
117-81-7
Fluoranthene
ND
ug/L.
4.5
1
03/21/22 09:48 03/21/22 19:54
206-44-0
Fluorene
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
87-68-3
Hexachlorobenzene
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
118-74-1
Hex achl orocyclopentadiene
ND
Ug/L
9.1
1
03/21/22 09:48 03/21/22 19:54
77-47-4
Hexachloroethane
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
67-72-1 L2
Indeno(1,2,3-cd)pyrene
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
193-39-5
Isophorone
ND
ug/L
9.1
1
03/21/22 09:48 03/21/22 19:54
78-59-1
Naphthalene
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
91-20-3
Nitrobenzene
ND
ug/L
4.5
1
03/21/22 09A8 03/21/22 19:54
98-95-3
2-Nitrophenol
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
88-75-5
4-Nitrophenol
ND
ug/L
9A
1
03/21/22 09:48 03/21/22 19:54
100-02-7
N-Nitrosodimethylamine
ND
ug/L
4.5
1
03/21/2209:48 03/21/22 19:54
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
621-64-7
N-Nitrosocliphenylamine
ND
ug/L
9.1
1
03121/22 09:48 03/21/22 19:54
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
Ug/L
4.5
1
03/21/2209:48 03/21/22 19:54
108-60-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/27/2022 11:43 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 38

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Town of Highlands WWTP
Pace Project No.: 92593587
Sample: HIGHLANDS WWTR EFF
Lab ID: 92693587004 Collected:
03/15/22 12:10
Received: 03/15/22 16:50 Matrix: Water
Parameters
Results
Units Report
Limit
DF
Prepared Analyzed
CAS No. Qual
625 RVE
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical
Services - Charlotte
Pentachlorophenol
ND
ug/L
9.1
1
03/21/22 09:48 03/21/22 19:54
87-86-5
Phenanthrene
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
85-01-8
Phenol
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
108-95-2
Pyrene
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
4.5
1
03/21/22 09:48 03/21/22 19:54
120-82-1 L2
2,4,6-Trichlorophenol
ND
ug/L
9.1
1
03/21/22 09:48 03/21/22 19:54
88-06-2
Surrogates
Nitrobenzene-d5 (S)
50
%
10-120
1
03/21/22 09:48 03/21/22 19:54
4165-60-0
2-Fluorobiphenyl (S)
42
%
15-120
1
03/21/22 09:48 03/21/22 19:54
321-60-8
Terphenyl-id14 (S)
84
%
11-131
1
03/21/22 09:48 03/21/22 19:54
1718-51-0
Phenol-d6(S)
23
%
10-120
1
03/21/22 09:48 03121/22 19:54
13127-88-3
2-Fluorophenol (S)
16
%
10-120
1
03/21/22 09:48 03/21/22 19:54
367-12-4
2,4,6-Tribromophenol (S)
37
%
10-137
1
03/21/22 09A8 03/21/22 19:54
118-79-6
624 Volatile Organics
Analytical Method:
EPA 624.1
Pace Analytical
Services - Charlotte
Benzene
ND
ug/L
11.0
1
03/17/22 13:54
71-43-2
Bromodichloromethane
ND
ug/L
ZO
1
03/17/22 13:54
75-27-4
Bromoform
ND
ug/L
2.0
1
03/17/22 13:54
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/17/22 13:54
74-83-9
Carbon tetrachloride
ND
ug/L
2.0
1
03/17/22 13:54
56-23-5
Chlorobenzene
ND
ug/L
2.0
1
03/17/22 13:54
108-90-7
Chloroethane
ND
ug/L
ZO
1
03/17/22 13:54
75-00-3
Chloroform
ND
ug/L
2,0
1
03/17/22 13:54
67-66-3
Chloromethane
ND
ug1L
ZO
1
03/17/22 13:54
74-87-3
Dibromochloromethane
ND
ug/L
2.0
1
03/17/22 13:54
124-48-1
1,2-Dichlorobenzene
ND
ug/L
2,0
1
03/17/22 13:54
95-50-1
1,3-Dichlorobenzene
ND
ug/L
2.0
1
03/17/22 13:54
541-73-1
1,4-Dichlorobenzene
ND
ug/L
ZO
1
03/17/22 13:54
106-46-7
1, 1 -Diehl orcrethane
ND
ug/L
2.0
1
03/17/22 13:54
75-34-3
1,2-DiGhloroethane
ND
ug/L
2.0
1
03/17/22 13:54
107-06-2
1,1-Dichloroethene
ND
ug/L
2.0
1
03/17122 13:54
75-35-4
cis- 1,2-Dichloroethene
ND
ug/L
ZO
1
03/17/22 13:54
156-59-2
trans- 1,2-Dichl oroethene
ND
ug/L
2,0
1
03/17/22 13:54
156-60-5
1,2-Dichloropropane
ND
ug/L
ZO
1
03/17/22 13:54
78-87-5
cis- 1, 3-Dichloropropene
ND
ug/L
ZO
1
03/17/22 13:54
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
2,0
1
03/17/22 13:54
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/17/22 13:54
100-41-4
Methylene Chloride
ND
ug/L
2,0
1
03/17/22 13:54
75-09-2
1, 1,2,2-Tetrachloroethane
ND
ug/L
2.0
1
03/17/22 13:54
79-34-5
Tetrachloroethene
ND
ug/L
ZO
1
03/17/22 13:64
127-18-4
Toluene
3.3
ug/L
1.0
1
03/17/22 13:54
108-88-3
1, 1, 1 -Trichloroethane
ND
ug/L
ZO
1
03/17/22 13:54
71-55-6
1, 1,2-Trichloroethane
ND
ug/L
2.0
1
03/17/22 13:54
79-00-5
Trichloroethene
ND
ug/L
ZO
1
03/17/22 13:54
79-01-6
Trichlorcifluoromethane
ND
ug/L
2.0
1
03/17/22 13:54
75-69-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/27/2022 11:43 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 38

ANALYTICAL RESULTS
Project: Town of Highlands WWTP
Pace Project No.: 92593587
Pace Analytical Services, LLC
2225 Riverside Dr
Asheville NC 28804
[phone]
Sample: HIGHLANDS WWTR EFF Lab ID: 92593587004 Collected: 03/15J22 12:10 Received: 03/15/22 16:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
624 Volatile Organics
Vinyl chloride
Surrogates
4-Bromofl uo to benzene (S)
Toluene-d8 (S)
1,2-Dichloroethane-d4 (S)
420.4 Phenolics, Total
Phenolics, Total Recoverable
460OCNE Cyanide, Total
Cyanide
Date: 04127/2022 11:43 AM
Analytical Method: EPA 624.1
Pace Analytical Services - Charlotte
ND ug/L
2.0 1
03/17/22 13:54
75-01-4
99 %
70-130 1
03/17/22 13:54
460-00-4
107 %
70-130 1
03/17/22 13:54
2037-26-5
86 %
70-130 1
03/17/22 13:54
17060-07-0
Analytical Method: EPA420.4 Rev 1.0
1993 Preparation Method: EPA 420.4 Rev 1.0 1993
Pace Analytical Services - Asheville
0.021 mg/L
0.020 1
03/23/22 10:55 03/23/22 15:04
64743-03-9
Analytical Method: SM 4500-CN-E-2016 Preparation
Method: SM 4500-CN-E-2016
Pace Analytical Services - Asheville
ND mg/L
0,0080 1
03/22122 18:10 03/23/22 01:44
57-12-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC
Page 8 of 38