WQ0005555_Monitoring - 03-2023_20230418

Monitoring Report Submittal
...................................................
Permit Number#* WQ0005555
Name of Facility:* Weyerhaeuser Company
Month: * March Year: * 2023
Report Information
Type* Upload Document*
NDMR, NDAR-1, NDAR-2, NDMLR 3 2023 Mar NDAR & NDMR.pdf 1.84MB
PDF Only
GW-59 MARCH 2O23 GW-59.pdf 4.26MB
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
Confirmation Email Address: * [e-mail]
Name of Submitter: * Dennis R Atkinson
Signature:
a�i� rr«t ��t. �:►�Jow
Date of submittal: 4/18/2023
This will be filled in automatically
Initial Review

Reviewer: Wanda.Gerald
Is the project number correct?* WQ0005555
Is the monitoring report accepted?* Yes No
Regional Office* Winston-Salem
Reviewer: _anonymous
Review Date: 6/13/2023

FORM: NDMR 05-16 NON -DISCHARGE MONITORING REPORT (NDMR) Page _1_ of_3_
Permit No.: WQ0005555
Facility Name: Weyerhaeuser - Elkin OSB Mill WWTF
County: Surry
Month: March
Year: 2023
PPI: 001
Flow Measuring Point: ❑� Influent ❑ Effluent ❑ No How generated
Parameter Monitoring Point: ❑ Influent ❑� Effluent E]Groundwater Lowering Surface water
Parameter Code -o.
50050
00310
00916
00680
00940
01034
31616
71880
00927
71900
00610
00625
00620
00600
00340
00400
�a
m
Q E
lx~
O
c
O
�,
iA
O
;93
o
O
m
E
9
V
Cr
ccc
ar o
O
C �%
ro
C
V
E
'-
c
w
m
V. (Oi
,� °'
U.
w
c
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p
E
Q
c
m CD
Y«
r Z
F-
A
«
Z
c
c rn
0
Z
G
v
=
a
24-hr
hrs
GPD
mg/L
mg/L
mg/L
mg/L
mg/L
#1100 mL
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
su
1
08:00
8
0
2
08:00
8
0
3
08:00
4
0
4
0
5
0
6
08:00
4
2,525
8.42
7
08:00
8
0
8
08:00
4
0
9
08:00
8
0
10
08:00
4
0
11
0
12
0
13
08:00
4
0
8.36
14
08:00
8
0
15
08:00
8
0
16
08:00
8
0
17
08:00
4
0
18
0
19
0
20
08:00
4
0
8.66
211
08:00
8
0
22
08:00
4
25,076
1170
28.5
1200
135
<0.0500
<2.0
0.507
27.1
<0.00020
<1.00
41.1
<20.0
41.1
5880
23
08:00
8
0
24
08:00
4
0
25
0
26
0
271
08:00
5
0
8.76
28
07:30
8
0
29
07:30
10
0
30
07:30
8
0
31
0
Average:
890
1,170.00
28.50
1,200.00
135.00
0.00
1.00
0.51
27.10
0.00
0.00
41.10
0.00
41.10
5,880.00
Daily Maximum:
25,076
1,170.00
28.50
1,200.00
135.00
0.05
2.00
0.51
27.10
0.00
1.00
41.10
20.00
41.10
5,880.00
8.76
Daily Minimum:
0
1,170.00
28.50
1,200.00
135.00
0.05
2.00
0.51
27.10
0.00
1.00
41.10
20.00
41.10
5,880.00
8.36
Sampling Type:
Recorder
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Monthly Limit:
Daily Limit:
28,800
Sample Frequency:
Continuous
3 X Year
3 X Year
3 X Year
3 X Year
3 X Year
3 X Year
3 X Year
3 X Year
3 X Year
3 X Year
3 X Year
3 X Year
3 X Year
3 X Year
Per Event

FORM: NDMR 05-16 NON -DISCHARGE MONITORING REPORT (NDMR) Page _2_of_3_
Permit No.: WQ0005555
Facility Name: Weyerhaeuser - Elkin OSB Mill WWTF
County: Surry
Month: March
1 1
'Flow Measuring Point: Influent Effluent No flow generated
•
•
MET:
1 1
----------------
®
1: 11
®
1: 11----------------

FORM: NDMR 05-16 NON -DISCHARGE MONITORING REPORT (NDMR) Page _3_ of _3-
Sampling Person(s) 11 Certified Laboratories
Name: Scott Miller Name: WayPoint Anaylical - Cert. No. 402
Name: Brody Edwards Name: PACE - Cert No. 40 & 633
Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? E compliant L Non -compliant
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective
action(s) taken Attach additional sheets if necessary.
Operator in Responsible Charge (ORC) Certification
Permittee Certification
ORC:
Dennis R. Atkinson
Permittee: Weyerhaeuser Co.
Certification No.: 15574
Signing Official: Steve Kobelak
Grade:
SI Phone Number: 336-526-6437
Signing Official's Title: Mill Manger
Has the ORC changed since the previous NDMR? E yes 2] No
Phone Number: 336-526-6456 Permit Expiration: 8/31/2025
L
r cif
.�,'l js_�2__ 3
Signature Date
Signature Date
By this signature, I certify that this report is accurrate and complete to the best of my knowledge.
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision �r
accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information
submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for
gathering the information, the information submitted is to the best of my knowledge and belief true accurate, and complete. I am
aware that there are significant penalties for submitting false information including the possibility of fines and imprisonment for
knowing violations
Mail Original and Two Copies to:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617

FORM: NDAR-1 08-11 N[]N-n1CC41oRr.F APPI IrATIAN RFPART fNnAR_11 Page 1 of
Permit No.: W00005555
Facility Name: Weyerhaeuser - Elkin, NC
County: Surry
Month: March
Year: 2023
Did irrigation occur
at this facility?
YES No
Field Name:
01
Field Name:
02
Field Name:
03
Field Name:
04
Area (acres):
2.17
Area (acres):
2.17
Area (acres):
2.17
Area (acres):
2.17
Cover Crop:Ha
Y
Cover Crop:
P:
Ha Y
Cover Crop:
P�
Ha Y
Cover Crop:
P�
Ha Y
Hourly Rate (in):
0.25
Hourly Rate (in):
0.25
Hourly Rate (in):
0.25
Hourly Rate (in):
0.25
Annual Rate (in):
20
Annual Rate (in):
20
Annual Rate (in):
20
Annual Rate (in):
20
Weather
Freeboard
Field Irrigated?
❑ YES ❑ NO
Field Irrigated?
❑✓ YES '- NO
Field Irrigated?
E] YES ❑ NO
Field Irrigated?
0 YES ❑ NO
T
o
0
c
a
°
o
aE
u
LR
m
m3 oa
oa
Q
m
E 9
0
g.e
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c
oo
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%4
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�
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v
=
J
o'a
a
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a
°ao
E 'o
c
ooa
x
JE
°F
in
ft
ft
gal
min
In
In
gal
min
in
in
gal
min
in
In
gal
min
in
in
1
0
2.27
2
0.37
2.22
3
0.14
1.96
4
1.12
2
5
C
66
0
2
6,419
30
0.11
0.11
8,293
30
0.14
0.14
4,113
15
0.07
0.07
61
1
0
2.29
7
0
2.05
8
0
2.06
9
C
65
0
2.07
7,971
30
0.14
0.14
10
0.11
2.38
11
0
2.39
121
1
0.16
2.37
13
0.04
2.36
14
0
2.36
15
0
2.38
16
0
2.39
17
0
2.39
18
0.04
2.39
19
C
36
0
2.4
7,896
30
0.13
0.13
20
0
2.33
21
0
2.34
22
0
2.35
231
C
1 74
0.14
2.35
6,714
30
0.11
0.11
7,090
30
0.12
0.12
24
0
2.37
25
0.35
2.34
26
0.05
2.35
27
0
2.36
28
0
2.37
29
1
0.23
2.35
30
1
0
2.37
31
072.38
Monthly Loading:
12 Month Floating Total (in):
13,133
0.22
15.84
7,090
1
0.12
1
8,293
It --
0.14
5.83
19,980
0.34
16.14
13.20

FORM• Nr1AR_1 nR-11 A1f1w1_n1Q1'UA01--C ADDI Ir`ATInK] D=0r1DT fidnAD_11 Paqe 3 of
Permit No.: W00005555
Facility Name: Weyerhaeuser - Elkin, NC
County: Surry
Month: March
Year: 2023
Did irrigation occur
at this facility?
[�] YES NO
Field Name:
A
Field Name:
B
Field Name:
CN
Field Name:
CS
Area (acres):
2.8
Area (acres):
2.56
Area (acres):
1.96
Area (acres):
1.24
Cover Crop:Ha
Y
Cover Crop:
P:
Ha Y
Cover Crop:
P�
Ha Y
Cover Crop:
P�
Ha Y
Hourly Rate (in):
0.25
Hourly Rate (in):
0.25
Hourly Rate (in):
0.25
Hourly Rate (in):
0.25
Annual Rate (in):
31.8
Annual Rate (in):
31.8
Annual Rate (in):
31.8
Annual Rate (in):
31.8
Weather
Freeboard
Field Irrigated?
YES ❑ NO
Field Irrigated?
❑ YES FZI No
Field Irrigated?
0 YES ❑ NO
Field Irrigated?
0 YES ❑ NO
o
t
m
?
l0
E
°
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a
a
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Im
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ar °i
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END
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=
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AV
0 0
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E aI
7` C
Ewa
A= 0
J
3
°F
in
It
It
gal
min
in
in
gal
min
in
in
gal
min
In
in
gal
I min
in
in
1
0
2.27
2
0.37
2.22
3
0.14
1.96
4
1.12
2
5
C
62
0
2
15,800
60
0.21
0.21
1
8,481
30
0.16
0.16
7,331
30
0.22
0.22
6
0
2.29
7
0
2.05
8
0
2.06
9
C
60
0
2.07
8,392
30
0.16
0.16
7,283
30
0.22
0.22
10
0.11
1 2.38
ill
1
0
2.39
12
0.16
2.37
13
0.04
2.36
14
0
2.36
15
0
2.38
16
0
1 2.39
17
0
2.39
18
0.04
2.39
19
C
45
0
2.4
8,420
30
0.16
0.16
7,288
30
0.22
0.22
20
0
2.33
21
0
2.34
221
1
0
2.35
23
PC
57
0.14
2.35
16,457
60
0.22
0.22
8,296
30
0.16
0.16
7,288
30
0.22
0.22
24
0
2.37
25
0.35
2.34
26
0.05
2.35
27
0
2.36
28
0
2.37
29
0.23
2.35
30
0
2.37
31
0
2.38
Monthly Loading:
32,257
-
0.42
0
0.00
33,589
29,190
0.87�__
,
12 Month Floating Total (in):
2.58
0.83
E2.O
_

FORM: NDAR-1 08-11 N[)N_r i-grWARC;F APPI IrATIPIN RFP()RT (IJDAR_11 Page 2 of 4
Permit No.: W00005555
Facility Name: Weyerhaeuser - Elkin, NC
County: Surry
Month: March
Year: 2023
Did irrigation occur
at this facility?
�] YES ❑ NO
Field Name:
05
Field Name:
06
Field Name:
07
Field Name:
08
Area (acres):
2.29
Area (acres):
1.3
Area (acres):
2.01
Area (acres):
2.08
Cover Crop:Ha
Y
Cover Crop:
P:
Ha Y
Cover Crop:
P�
Ha Y
Cover Crop:
P:
Ha Y
Hourly Rate (in):
0.25
Hourly Rate (in):
0.25
Hourly Rate (in):
0.25
Hourly Rate (in):
0.25
Annual Rate (in):
20
Annual Rate (in):
20
Annual Rate (in):
20
Annual Rate (in):
20
Weather
Freeboard
Field Irrigated?
❑ YES ❑ NO
Field Irrigated?
❑ YES ❑ NO
Field Irrigated?
❑ YES ❑ NO
Field Irrigated?
❑ YES ❑ NO
0
a
a`
a m
.2
M a
o A
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a
_Q
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to 0
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7JQ
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r=2
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xpoa
Ed
p
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I=�
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0�
=1C0
o
Js
°F
In
ft
ft
gal
min
in
in
gal
min
in
in
gal
min
In
in
gal
min
in
in
1
0
2.27
2
0.37
2.22
3
0.14
1.96
4
1.12
2
5
C
66
0
2
61
1
0
2.29
7
0
2.05
8
0
2.06
9
C
65
0
2.07
10
0.111
2.38
11
0
2.39
121
1
0.16
2.37
13
0.04
2.36
14
0
2.36
15
0
2.38
16
0
2.39
17
0
2.39
181
1
0.04
2.39
19
C
36
0
2.4
20
0
2.33
21
0
2.34
22
0
2.35
23
C
74
0.14
2.35
241
1
0
2.37
25
0.35
2.34
26
0.05
2.35
27
0
2.36
28
0
2.37
29
0.23
2.35
301
1
0
2.37
311
1
1 0
1 2.38
Monthly
Loading:
0
0.00
0
0.00
0
0.00
0
0.00
12 Month Floating Total (in):
999
12.42
11.09
8.80

FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page 4 of 4
Did the application rates exceed the limits in Attachment B of your permit?
Were adequate measures taken to prevent effluent ponding in or runoff from the sites?
Was a suitable vegetative cover maintained on all sites as specified in your permit?
Were all setbacks listed in your permit maintained for every application to each permitted site?
Were all freeboards maintained in accordance with the specified freeboard heights in your permit?
❑ Compliant
❑ Non -Compliant
0 Compliant
❑ Non -Compliant
Q Compliant
❑ Non -Compliant
❑� Compliant
❑ Non -Compliant
[] Compliant
❑ Non -Compliant
If the facility is non -compliant please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the correct vt
action(s) taken. Attach additional sheets if necessary.
Operator in Responsible Charge (ORC) Certification
Permittee Certification
ORC: Dennis R. Atkinson
Permittee:
Weyerhaeuser Company
Certification No.: 15574
Signing Official: Steve Kobelak
Grade: SI Phone Number: 336-526-6437
Signing Official's Title: Mill Manager
Has the ORC changed since the previous NDAR-1? yes No
Phone Number: 336-526-6456 Permit Exp.: 8/31/25
40
Signature Dat
Signature Date
By this signature, I certify that this report is accurrate and complete to the best of my knowledge.
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision In accordance
with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted Based on my
inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information the
information submitted is, to the best of my knowledge and belief true accurate and complete I am aware that there are significant
penalties for submitting false information including the possibility of fines and imprisonment for knowing violations
Mail Original and Two Copies to:
Division of Water Quality
Information Processing Unit
1617 Mail Service Center

Waypoeinto
ANALYTICAL
4/4/2023
Weyerhaeuser Corporation
Dennis Atkinson
524 Pride Way
Elkin, NC, 28621
Ref: Analytical Testing
Lab Report Number: 23-081-0028
Client Project Description: Wastewater EFF
Dear Dennis Atkinson:
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Waypoint Analytical, LLC (Charlotte) received sample(s) on 3/22/2023 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Terri W Cole
Laboratory Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 12

Waypoint
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytica I.tom
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State
Program
Lab ID
Expiration Date
North Carolina
State Program
37735
07/31/2023
North Carolina
State Program
402
12/31/2023
South Carolina
State Program
99012
07/31/2023
South Carolina
State Program
99012
12/31/2022
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2023
Florida
State Program - NELAP
E871157
06/30/2023
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2023
Illinois
State Program
- NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2023
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2023
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
11/14/2025
Texas
State Program
- NELAP
T104704180
09/30/2023
Virginia
State Program
00106
06/30/2023
Virginia
State Program
- NELAP
460181
09/14/2023
Page 1 of 1 00016/23-081-0028
Page 2 of 12

waypoint (D 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-081-0028
Client Project Description: Wastewater EFF
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
91901
EFF
Aqueous
03/22/2023
10:40
03/22/2023
13:10
91901
EFF
Aqueous
03/22/2023
10:40
03/22/2023
13:10
365.4
WP
MTN
91901
EFF
Aqueous
03/22/2023
10:40
03/22/2023
13:10
4500NORGD-2011
WP
MTN
91901
EFF
Aqueous
03/22/2023
10:40
03/22/2023
13:10
531OC-2011
WP
MTN
91901
EFF
Aqueous
03/22/2023
10:40
03/22/2023
13:10
8315A
WP
MTN
91901
EFF
Aqueous
03/22/2023
10:40
03/22/2023
13:10
245.1
WP
MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 12

Waypointo
ANALYTICAL
Client: Weyerhaeuser Corporation
Project: Wastewater
Lab Report Number: 23-081-0028
Date: 4/3/2023
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Total Metals Method EPA-200.7
Sample 92311 (Influent)
Analyte: Calcium
QC Batch No: V31375/V31270
LRB failed high. Result 10x concentration. Result not affected.
Analyte: Chromium
QC Batch No: V31375/V31270
LCS failed high. Sample concentration BRL. Result not affected.
CASE NARRATIVE
Sample 92311 (Influent)
Analyte: Sodium
QC Batch No: V31375/V31270
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the
system was in control, but the reported result could be affected by matrix interference.
Metals Digestion Method EPA-200.7 (PREP)
Sample 91901 (EFF)
QC Batch No: V31270/V31270
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Anions by Ion Chromatography Method 300.0
Sample 91901 (EFF)
QC Batch No: V31176/V31161
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Ammonia Method 4500-NH3G-2011
Sample 91901 (EFF)
QC Batch No: V31183/V31132
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Biochemical Oxygen Demand (BOD) Method 5210B-2015
Sample 91901 (EFF)
QC Batch No: V31224
Dilutions did not meet RPD criteria.
Total Organic Carbon Method 5310C-2014
Sample 59397 (JT-3.6)
Analyte: TOC
QC Batch No: 1-673553/1-673552
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Sample 91901 (EFF)
Analyte: TOC
QC Batch No: L673553/L673552
Page 4 of 12

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Page 5 of 12

wavDointe
ANALYTICAL
00052
Weyerhaeuser Corporation
Dennis Atkinson
524 Pride Way
Elkin , NC 28621
Report Number : 23-081-0028
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Project Wastewater EFF
Information :
REPORT OF ANAL YSIS
Report Date : 04/04/2023
Received : 03/22/2023
Lab No : 91901 Matrix: Aqueous
Sample ID : EFF Sampled: 3/22/2023 10:40
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
Fecal Coliform MPN/g
<2.0
MPN/100ml-
Sodium Absorption Ratio
1.55
Ratio
Conductivity
4360
pmhos/cm
Plant Available Nitrogen
12.3
mg/L
Ammonia Nitrogen
<1.00
mg/L
Biochemical Oxygen Demand (5-day)
1170
mg/L
Chloride
135
mg/L
COD (Chemical Oxygen Demand)
5880
mg/L
Nitrate (NO3-N)
<20.0
mg/L
Nitrite (NO2-N)
<10.0
mg/L
Nitrate+Nitrite-N
<10.0
mg/L
pH
8.7
S.U.
Total Dissolved Solids
6820
mg/L
Total Suspended Solids
484
mg/L
Total Kjeldahl Nitrogen
41.1
mg/L
Total Nitrogen
41.1
mg/L
Phosphorus
6.32
mg/L
TOC
1200
mg/L
Temperature
10.2
C
Calcium
28.5
mg/L
Chromium
<0.0500
mg/L
Magnesium
27.1
mg/L
Mercury (Total)
<0.00020
mg/L
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
2.0
1
03/22/23 13:43
SMW
9221E-2011
0.100
1
03/29/23 20:12
CALCULATION
1
1
03/22/23 10:40
FLD
FIELD
1.00
1
03/22/23 15:53
CALCULATION
1.00
10
03/24/23 11:17
CM]
4500-NH3G-2011
2.0
1
03/22/23 09:58
SLO
521OB-2015
100
100
03/22/23 15:53
CM]
300.0
90
1
03/27/23 10:57
SMW
5220D-2011
20.0
100
03/22/23 15:53
CM]
300.0
10.0
100
03/22/23 15:53
CMJ
300.0
10.0
100
03/22/23 15:53
300.0
1
03/22/23 10:40
FLD
FIELD
55
1
03/23/23 16:05
CM]
2540C-2015
50.0
1
03/24/23 12:09
EKF
2540D-2015
3.42 5.00
1
03/27/23 16:06
ANH
4500NORGD-2011
5.00
1
03/22/23 15:53
ELK
CALCULATION
2.12 5.00
1
03/27/2315:57
ANH
365.4
500
500
03/30/23 06:35
CJD
531OC-2011
0.1
1
03/22/23 10:40
FLD
FIELD
1.00
1
03/29/23 20:12
MMR
EPA-200.7
0.0500
1
03/29/23 20:12
MMR
EPA-200.7
1.00
1
03/29/23 20:12
MMR
EPA-200.7
0.00020
1
03/29/23 11:08
FDS
245.1
J Estimated value
Page 6 of 12

Waypointo.
ANALYTICAL
00052
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypoi nta na lytica Isom
Weyerhaeuser Corporation Project Wastewater EFF
Dennis Atkinson
524 Pride Way Information
Elkin , NC 28621
Report Date : 04/04/2023
Received : 03/22/2023
Report Number : 23-081-0028 REPOR T OF A NA L YSIS
Lab No : 91901 Matrix: Aqueous
Sample ID : EFF Sampled: 3/22/2023 10:40
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
Sodium 1520 m9/L 7.00 1 03/29/23 20:12 MMR EPA-200.7
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
J Estimated value
Page 7 of 12

Waypointo.
ANALYTICAL
00052
Weyerhaeuser Corporation Project
Dennis Atkinson
524 Pride Way Information
Elkin , NC 28621
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypoi nta na lytica Isom
Wastewater EFF
Report Date : 04/04/2023
Received : 03/22/2023
Report Number : 23-081-0028
REPOR T OF A NA L YSIS
Lab No : 91901
Matrix: Aqueous
Sample ID : EFF
Sampled: 3/22/2023
10:40
Analytical Method: 625.1
Prep Batch(es):
V31337 03/29/23 15:16
Prep Method: 625.1 (Prep)
Test
Results
Units
MDL MQL DF
Date / Time By
Analytical
Analyzed
Batch
Phenol
<0.005
mg/L
0.005 1
03/31/2314:03 3MV
V31521
Surrogate: Phenol-d5
26.4
Limits: 10-63%
1 03/31/23 14:03 3MV
625.1
Surrogate:2-Fluorophenol
39.9
Limits:22-84%
1 03/31/2314:03 3MV
V31521
Surrogate: 2,4,6-Tribromophenol
69.2
Limits:31-144%
1 03/31/2314:03 3MV
V31521
Analytical Method: 8315A
Prep Batch(es):
L671944 03/24/23 10:43
Prep Method: 8315A
Test
Results
Units
MDL MQL DF
Date / Time By
Analytical
Analyzed
Batch
Formaldehyde
507
Ng/L
500 1
03/24/23 22:15 KDL
L671968
Qualifiers/ DF Dilution Factor J Estimated value
Definitions MQL Method Quantitation Limit
Page 8 of 12

(2)
WayPAo0nt..
NALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 00052
Customer Name: Weyerhaeuser Corporation
Report Number: 23-081-0028
Shipping Method
0 Fed Ex 0 US Postal U Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
IRT-15 3.1C
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample Iabel(s)?
U Yes
0 No
COC properly completed
U Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
0 N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: Paula Blakeborough Date & Time: 03/22/2023 16:15:23
Page 9 of 12

• 0
Waypoint.
ANALYTICAL
449 Springbrook Road • Charlotte, INC 28217
Phone [phone] • Fax: [phone]
Client Company Name:
�kXgI�
Report TolContact Name:
Reporting Address:
Phone: Fax (Yes)(No):
Email Address:
EDD Type: PDF_ Excel Other
Site Location Name:
Site Location Physical Address:
CLIENT DATE
SAMPLE DESCRIPTION COLLECTED
�__1 J�-247_ r
TIME MATRIX
COLLECTED (SOIL,
MILITARY WATER, OR
HOURS SLUDGE)
N
0�240 38
Weverhaeuser Corporation 151451
Wastewater
CHAIN OF CUSTODY RECORD
PAGE I OF 2 OUOTE 8 TOENSURE PROPER BILLING: _
Project Name:
Short Hold Analysis (Yes) (No) UST Project: (Yes) (No)
'Please ATTACH any project specific reporting (OC LEVEL 1 II III IV)
provisions and/or QC Requirements
Invoice To:
Address:
Purchase Order NoJBilling Reference
Requested Due Date U 1 Day J 2 Days J 3 Days J 4 Days J 5 Days
"Working Days" ❑ 6-9 Days J Standard 10 days J Rush Work Must Be
Pre Approved
Samples received after 15:00 will be processed next business day.
Turnaround time is based on business days, excluding weekends and holidays -
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY WAYPOINT ANALYTICAL, LLC TO CLIENT)
SAMPLE CONTAINER I __
'TYPE
SEE BELOW
NO.
SIZE
PR - TIVIES
71vES
LJ
c;
3
yO
Sampler's Signature Sampled By {Pant Name} �'/ C�rJC/S Affiliation
Upon relinquishing, this Chain of Cilstody is your authorization for Waypoint Analytical to proceed with the analyses as requested above. A
submitted in writing to the Waypoint Analytical Project Manager, There will be charges for any changes after analyses have been initialized.
Rehl quis _1 B (Si- -I i Received By. (Signatureii Data
By
YES NO NIA
Samples INTACT upon arrival? V
Received IN ICE? V
PROPER PRESERVATIVES indicated? V" _
Received WITHIN HOLDING TIMES?� _
CUSTODY SEALS INTACT?
VOLATILES rec'd WIOUT HEADSPACE?
PROPER CONTAINERS used?
,=�li
�f
TEMP; Therm ID:_ 9bserved 3. °C /Corr.I _ C
TO BE FILLEDIN BY CL NTISAMPLING RSONNEL
Certification: I SC
Other NIA
Water Chlorinated: YES NO
Samples Iced Upon Collection. YES_ NO
SREQUESTED
REMARKS ID NO.
changes must be
312 3S
Method of Shipment NOTE, ALL SAMPLE COOLERS SHOULD BE TAPE SH ITH CUSTODY S LS FOR TRANSPORTATION TO THE LABORATORY. COC Group No
SAMPLES ARE NO AC EPTED AND VERIFIED AG T COC UNTIL RECEIVED AT THE LABORATORY.
J Fed Ex G UPS J Hand delnrored A point Analyti.l Field Service J Other
NPDES: UST: GRCIDWATER: DRINKING WATER: SOLID WASTE: RCRA: BRWNFLD LANDFILL OTHER:
❑NCJSC I JNC ❑SC JN JSC JNC JSC JNC JSC JNC JSC _I NC JSC _J NC JSC JNC JSC
O U J ❑ ❑ J ❑ J
`CONTAINER TYPE CODES: A = Amber C = Clear G- Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organi"Iyffo (Z9ro1K9ad Space)
Additional Comments_
Sly Arrival Time:
Site Departure Time:
Field Tech Fee:
Mileage:
ORIGINAL

0
Waypoint
ANALYTICAL
449 Springbrook Road • Charlotte, NC 28217
Phone [phone] • Fax: [phone]
Client Company Name:\�1941_��
Report To/Contact Name:
Reporting Address:
Phone: _ Fax (Yes)(No):
Email Address:
EDD Type: PDF Excel Other
Site Location Name:
Site Location Physical Address:
CHAIN OF CUSTODY RECORD
PAGE 2 of _ QUOTE M TOENSURE PROPER BILLING: YES NO NIA
Samples INTACT upon arrival?
Project Name:
Received IN ICE? d
Short Hold Analysis (Yes) (No) UST Project: (Yes) (No)
PROPER PRESERVATIVES Indicated? y
'Please ATTACH any project specific reporting (OC LEVEL 1 II III IV)
Received WITHIN HOLDING TIMES? +
provisions andlor OC Requirements
CUSTODY SEALS INTACT?
Invoice To:
VOLATILES reed W/OUT HEADSPACE? I/
Address:
PROPER CONTAINERS used? 'v
TEMP: Therm ID: - t_� Observed �-C /Corr.
Purchase Order No./Billing Reference
TO BE FILLED IN BY CL T/MAMPLING PERM
Requested Due Date 0 1 Day J 2 Days J 3 Days J 4 Days J 5 Days
Certification: NC Sc
"Working Days" ❑ 6-9 Days J Standard 10 days J RuP esh AW orkov dust Be
Samples received after 15 D0 will be processed next business day
Other NIA
Turnaround time is based on business days, excluding weekends and holidays-
(SEE REVERSE FOR TERMS 6 CONDITIONS REGARDING SERVICES
Water Chlorinated: YES NO
RENDERED BY WAYPOINT ANALYTICAL, LLC TO CLIENT)
Samples teed Upon Collection: YES NO
ONNEL
TIME MATRIX
SAMPLE CONTAINER
ANALYSIS REQUESTED \`
7
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
COLLECTED (SOIL,
MILITARY WATER, OR
_
-TYPE
PRESERVA-
TIVES
�' REMARKS
ID NO.
HOURS SLUDGE)
SEE BELOW NO. SIZE
�` r �L
11111 I' ►�{Il1 h 111 11i1 11I 0�2 2�8
Weyerhaeuser Corporation 16:14:51
Wastewater
Sampler's Signature Sampled By (Print Name)pl V y .� Affiliation +Z •
Upon relinquishing, this Chain of Cu Itody is your authorization for Waypoint Analytical to proceed with the analyses as requested above. A changes must be Sloe Arrival Time:
submitted in writing to the Waypoint Analytical Project Manager. There will be charges for any changes after analyses have been initialized.
nit
8y re Received
eived By: {Signature i Date MilitaryMourS Additional Comments:
s Site Departure Tirn•:
i �.�•�
Date
wii
:)3
NOTE_ ALL SAMPLE COOLERS SHOULD BETA
SAMPLES ARE NOT ACCEPTED AND VERIFIED
'WITH CUSTVQLSF.AkSFOR TRANSPORTATION
CDC UNTIL RECEIVED AT THE LABORATORY.
J F,-d E, J UPS J Nand-deilvered ` !fAaypoint Analytical Field Service J Other
NPDES: UST: GR�IYtVDWATER: DRINKING WATER: SOLID WASTE: RCRA: BRWNFLO LANDFILL OTHER:
J NC J Sc J NC J SC U C J SC J NC J SC J NC J SC I NC SG I JJ NC J SC JJ NC U SC I J NC J SC
J J J J
'CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA= Volatile OrganiipttApalytlieFarci�ead Space)
Field Tech Fee:
Mileage:
ORIGINAL

FIELD INFORMATION LOG (continued)
SAMPLING INFORMATION:
Method of Sampling: HAND BAILER
Water Level @ Sampling, Feet:
Sample Point ID: 'ET-V
Dedicated: Y / N
Well Collection Sequence Number:
Parameters: Annual ( ) Semi -Annual ( ) Quarterly ( ) Monthly ( ) Other (X)3X YEAR
SAMPLING DATA:
Date/ Time
Sample Rate:
Temp
pH
Conduct.
Turb.
Other
('C)
(std. units)
(µmhos/cm)
(NTU)
_T,22-Z
VOA
/0, 2
T17
q, U v
v
Other
INSTRUMENT CHECK DATA:
Turbidity Serial:
pH Serial #:
Conductivity Serial#:
NTU s d. = NTU
4.0 std.: = 7.0 std.: =
GENERAL INFORMATION:
Weather Conditions @ time of sampling:
r_'�_ _
Sample Characterisitics:
µmhos/cm =
NTU std. = NTU
10 std.. =
µmhos/cm =
ANALTYE COLLECTION ORDER, CONTAINERS, PRESERVATIVES AND TESTS PERFORMED:
COMMENTS AND OBSERVATIONS:
I certify that smapling procedures were in accordance with all applicable EPA, State and Client
protocols.
Date: /� / 23 By: Company:
S:\Field Services\WAYPOINT Field Information Log 2
Page 12 of 12