NCG030669_2022 DMR_20230124

NCDEQ Division of Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report(DMR) Form for NCG030000
Metal Fabrication
Click here for instructions
Complete,sign,scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report(DMR) Upload form within
30 days of receiving sampling results. Mail the original,signed hard copy of the DMR to the appropriate DEMLR Regional Office.
Certificate of Coverage No. NCGO3 t , 6 9 Person Collecting Samples: R066 R T 11E/(,/5 L E y
Facility Name: MPS /VJ F G L L, C Laboratory Name: PACE ANA L Y T /C 4 I-.
Facility County: /?O IN4 N Laboratory Cert. No.: wW 37 I
70� A 20/2 NC3f1/
W /2 N
Discharge during this period:El Yes El No (if no,skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances?®Yes ®No
If so,which Tier(I, II,or III)?
A copy of this DMR has been uploaded electronically via https://edocs.deci.nc.gov/Forms/SW-DMR El Yes 0 No
Date Uploaded:
Analytical Monitoring Requirements for Outfalls with Industrial Activities—Benchmarks in(Red)
Parameter Parameter Outfall Outfall f 3 Outfall Outfall Outfall
e
N/A Receiving Stream Class G C
N/A Date Sample Collected MM/DD/YYYY /2//5/?Q22 /2/5/2621
46529 24-Hour Rainfall in inches /. 'f- // /• 4 '/
C0530 TSS in mg/L(100 or 50*) < z,5 rN. 2,5 "',.
00400 pH in standard units(6.0-9.0 FW, �J d
6.8-8.5 SW) / •Z0 7� r
01119 Copper,total recoverable in mg/L C3„v05//nj a oo5/
(0.010 FW,0.0058 SW) /�
01051 Lead,total recoverable in mg/L �Oo/D�.� 00/0 /
(0.075 FW,0.22 SW) /4
Zinc,total recoverable in mg/L(0.126 /!1
01094 FW,0.095SW) ��d/d/ L O.,vlD/ L
00340 Chemical Oxygen Demand(COD)in <25<0 /n L <�5-o rn
g/ ( )
00552 Non-Polar Oil&Grease in mg/L(15) < 4,$/"m C-1 J'n',YA
*Outfalls to Outstanding Resource Waters(ORW),High Quality Waters(HOW),Trout Waters(Tr)and Primary Nursery Areas(PNA)
have a benchmark TSS limit of 50 mg/L.All other water classifications have a benchmark of 100 mg/L
FW(Freshwater)SW(Saltwater)
Notes(optional):
"I certify by my signature below,under penalty of law,that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information,the information
submitted is,to the best of my knowledge and belief,true,accurate,and complete.I am aware that there are significant penalties for submitting
false inf rmation,includin the possibility of fines and imprisonment for knowing violations."
1 ( I (8 ) 2v2,3
ign of Permittee or Dele ted Authorized Individual Date
Kb'e.mA-. r aNDy ihe)c Ago n A9i ( cow .10 I 210 35 12—
Email Address Phone Number

Pace Analytical Services,LLC
® 9800 Kincey Ave. Suite 100
aceAnalytical Huntersville,NC 28078
www.psalsbs.com [phone]
January 10, 2023
Robert Hensley
Agility Fuel Systems
1010 Corporate Center Drive
Salisbury, NC 28146
RE: Project: STORMWATER 4TH QUARTER
Pace Project No.: 92642647
Dear Robert Hensley:
Enclosed are the analytical results for sample(s) received by the laboratory on December 16, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services-Asheville
• Pace Analytical Services-Charlotte
• Pace Analytical Services-Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
, /, REPORT OF LABORATORY ANALYSIS
', 4 This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 1 of 18

Pace Analytical Services,LLC
® 9800 Kincey Ave. Suite 100
aceAnalytical Huntersville,NC 28078
www.pacelabs.cam [phone]
CERTIFICATIONS
Project: STORMWATER 4TH QUARTER
Pace Project No.: 92642647
Pace Analytical Services Charlotte
South Carolina Laboratory ID:99006 South Carolina Certification#:99006001
9800 Kincey Ave.Ste 100,Huntersville,NC 28078 South Carolina Drinking Water Cert.#:99006003
North Carolina Drinking Water Certification#:37706 Florida/NELAP Certification#:E87627
North Carolina Field Services Certification#:5342 Kentucky UST Certification#:84
North Carolina Wastewater Certification#:12 Louisiana DoH Drinking Water#:LA029
South Carolina Laboratory ID:99006 VirginiaNELAP Certification#:460221
Pace Analytical Services Asheville
2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030
Florida/NELAP Certification#:E87648 South Carolina Certification#:99030001
North Carolina Drinking Water Certification#:37712 VrginiaNELAP Certification#:460222
North Carolina Wastewater Certification#:40
Pace Analytical Services Peachtree Corners
110 Technology Pkwy,Peachtree Corners,GA 30092 North Carolina Certification#:381
Florida DOH Certification#:E87315 South Carolina Certification#:98011001
Georgia DW Inorganics Certification#:812
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC, Page 2 of 18

Pace Analytical Services,LLC
aceAnalytical® 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
www.pacelabs.cora [phone]
SAMPLE ANALYTE COUNT
Project: STORMWATER 4TH QUARTER
Pace Project No.: 92642647
•
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92642647001 OUTFALL 2 GRAB EPA 1664B REL 1 PASI-C
EPA 200.8 CW1 3 PASI-GA
SM 2540D-2015 JMH1 1 PASI-A
SM 5220D-2011 JMH1 1 PASI-A
92642647002 OUTFALL 1B GRAB EPA 1664B REL 1 PASI-C
EPA 200.8 CW1 3 PASI-GA
SM 2540D-2015 JMH1 1 PASI-A
SM 5220D-2011 JMH1 1 PASI-A
PASI-A=Pace Analytical Services-Asheville
PASI-C=Pace Analytical Services-Charlotte
PASI-GA=Pace Analytical Services-Peachtree Corners,GA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 3 of 18

Pace Analytical Services,LLC
® 9800 Kincey Ave. Suite 100
aceAnalytical Huntersville,NC 28078
www,pacelabs.com
[phone]
SUMMARY OF DETECTION
Project: STORMWATER 4TH QUARTER
Pace Project No.: 92642647
Lab Sample ID Client Sample ID
Method Parameters Result Units Report Limit Analyzed Qualifiers
92642647001 OUTFALL 2 GRAB
EPA 200.8 Copper 5.1 ug/L 5.0 01/09/23 23:09
EPA 200.8 Zinc 10.1 uglL 10.0 01/09/23 23:09
92642647002 OUTFALL 1B GRAB
EPA 200.8 Copper 5.1 ug/L 5.0 01/09/23 23:33
EPA 200.8 Zinc 10.1 uglL 10.0 01/09/23 23:33
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 4 of 18

Pace Analytical Services,LLC
aceAnalytical ffi 9800 Kincey Ave. Suite 700
Huntersville,NC 2807B
www.pacetabs.com
[phone]
ANALYTICAL RESULTS
Project: STORMWATER 4TH QUARTER
Pace Project No.: 92642647
Sample: OUTFALL 2 GRAB Lab ID: 92642647001 Collected: 12/15/22 06:45 Received: 12/16/22 12:15 Matrix: Water
Parameters Results Units Report Limit DE Prepared Analyzed CAS No. Qual
1664 SGT-HEM,TPH Analytical Method:EPA 1664E
Pace Analytical Services-Charlotte
Total Petroleum Hydrocarbons ND mg/L 4.8 1 12/23/22 00:30
200.8 ATL ICPMS,NC Analytical Method:EPA 200.8 Preparation Method:EPA 200.8
Pace Analytical Services-Peachtree Corners,GA
Copper 5.1 ug/L 5.0 1 01/09/23 11:48 01/09/23 23:09 7440-50-8
Lead ND ug/L 1.0 1 01/09/23 11:48 01/09/23 23:09 7439-92-1
Zinc 10.1 ug/L 10.0 1 01/09/23 11:48 01/09/23 23:09 7440-66-6
2540D Total Suspended Solids Analytical Method:SM 2540D-2015
Pace Analytical Services-Asheville
Total Suspended Solids ND mg/L 2.5 1 12/21/22 14:13
5220D COD Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011
Pace Analytical Services-Asheville
Chemical Oxygen Demand ND mg/L 25.0 1 12/17/22 12:52 12/17/22 19:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:01/10/2023 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 18

Pace Analytical Services,LLC
aceAnalytical® 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
www.pacelaha.cam {704)875.9092
ANALYTICAL RESULTS
Project: STORMWATER 4TH QUARTER
Pace Project No.: 92642647
Sample: OUTFALL 1 B GRAB Lab ID: 92642647002 Collected: 12/15/22 07:50 Received: 12/16/22 12:15 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM,TPH Analytical Method:EPA 1664B
Pace Analytical Services-Charlotte
Total Petroleum Hydrocarbons ND mg/L 4.8 1 12/23/22 00:30
200.8 ATL ICPMS,NC Analytical Method:EPA 200.8 Preparation Method:EPA 200.8
Pace Analytical Services-Peachtree Corners,GA
Copper 5.1 ug/L 5.0 1 01/09/23 11:48 01/09/23 23:33 7440-50-8
Lead ND ug/L 1.0 1 01/09/23 11:48 01/09/23 23:33 7439-92-1
Zinc 10.1 ug/L 10.0 1 01/09/23 11:48 01/09/23 23:33 7440-66-6
2540D Total Suspended Solids Analytical Method:SM 2540D-2015
Pace Analytical Services-Asheville
Total Suspended Solids ND mg/L 2.5 1 12/21/22 14:20
5220D COD Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011
Pace Analytical Services-Asheville
Chemical Oxygen Demand NO mg/L 25.0 1 12/17/22 12:52 12/17/22 18:47
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:01/10/2023 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 18

Pace Analytical Services,LLC
aceAnalytical® 9800 Kincey Ave. Suite 100
Fiuntersville,NC 28978
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: STORMWATER 4TH QUARTER
Pace Project No.: 92642647
QC Batch: 745392 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM,TPH
Laboratory: Pace Analytical Services-Charlotte
Associated Lab Samples: 92642647001,92642647002
METHOD BLANK: 3877653 Matrix: Water
Associated Lab Samples: 92642647001,92642647002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Petroleum Hydrocarbons mg/L ND 5.0 12/23/22 00:30
LABORATORY CONTROL SAMPLE: 3877654
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Petroleum Hydrocarbons mg/L 20 16.2 81 64-132
MATRIX SPIKE SAMPLE: 3877655
35766750001 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Total Petroleum Hydrocarbons mg/L 4.9U 19.4 14.3 65 64-132
SAMPLE DUPLICATE: 3877656
35767365001 Dup
Parameter Units Result Result RPD Qualifiers
Total Petroleum Hydrocarbons mg/L 4.9U ND
Results presented on this page are In the units Indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:01/10/2023 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 18

Pace Analytical Services,LLC
® 9800 Kincey Ave. Suite 100
aceAnalytical Huntersville,NC 28078
www.paceIabs.com [phone]
QUALITY CONTROL DATA
Project: STORMWATER 4TH QUARTER
Pace Project No.: 92642647
QC Batch: 748154 Analysis Method: EPA 200.8
QC Batch Method: EPA 200.8 Analysis Description: 200.8 ATL
Laboratory: Pace Analytical Services-Peachtree Corners,GA
Associated Lab Samples: 92642647001,92642647002
METHOD BLANK: 3889289 Matrix: Water
Associated Lab Samples: 92642647001,92642647002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Copper ug/L ND 5.0 01/09/23 22:57
Lead ug/L ND 1.0 01/09/23 22:57
Zinc ug/L ND 10.0 01/09/23 22:57
LABORATORY CONTROL SAMPLE: 3889290
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Copper ug/L 100 99.6 100 85-115
Lead ug/L 100 103 103 85-115
Zinc ug/L 100 101 101 85-115
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3889291 3889292
MS MSD
92642647001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Copper ug/L 5.1 100 100 104 102 99 97 70-130 2
Lead ug/L ND 100 100 101 100 101 100 70-130 0
Zinc ug/L 10.1 100 100 109 106 99 96 70-130 3
Results presented on this page are in the units indicated by the"Units"column except where an attemate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:01/10/2023 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 8 of 18

Pace Analytical Services,LLC
aceAnalytical® 9800 Kincey Ave. Suite 100
Huntersville,NC 2807878
www.pacelalts.cem [phone]
QUALITY CONTROL DATA
Project: STORMWATER 4TH QUARTER
Pace Project No.: 92642647
QC Batch: 744855 Analysis Method: SM 2540D-2015
QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92642647001
METHOD BLANK: 3875037 Matrix: Water
Associated Lab Samples: 92642647001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 12/21/22 14:07
LABORATORY CONTROL SAMPLE: 3875038
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Suspended Solids mg1L 250 240 96 90-110
SAMPLE DUPLICATE: 3875873
92642572002 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mglL 340 383 12
SAMPLE DUPLICATE: 3875874
92642579003 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 284 288 1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:01/10/2023 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 18

Pace Analytical Services,LLC
9800 Kincey Ave. Suite 100
aceAnalyfical Huntersville,NC 28078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: STORMWATER 4TH QUARTER
Pace Project No.: 92642647
QC Batch: 744971 Analysis Method: SM 2540D-2015
QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92642647002
METHOD BLANK: 3875620 Matrix: Water
Associated Lab Samples: 92642647002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L NO 2.5 12/21/22 14:20
LABORATORY CONTROL SAMPLE: 3875621
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Suspended Solids mg/L 250 248 99 90-110
SAMPLE DUPLICATE: 3875876
92642857005 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 235 229 3
SAMPLE DUPLICATE: 3875877
92642857006 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 1430 1460 2
Results presented on this page are In the units indicated by the"Units"column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:01/10/2023 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 10 of 18

Pace Analytical Services,LLC
aceAnalytical® 9800 Kincey Ave, Suite:
Huntersville,NC 28078
www.pacelabs.com
[phone]
QUALITY CONTROL DATA
Project: STORMWATER 4TH QUARTER
Pace Project No.: 92642647
QC Batch: 744152 Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92642647002
METHOD BLANK: 3871777 Matrix: Water
Associated Lab Samples: 92642647002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chemical Oxygen Demand mg/L ND 25.0 12/17/22 18:41
LABORATORY CONTROL SAMPLE: 3871778
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 754 100 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3871801 3871802
MS MSD
92642758001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 199 100 100 325 327 126 128 90-110 1 M1
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3871803 3871804
MS MSD
92642759001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 203 100 100 408 417 205 214 90-110 2 M1
Results presented on thit page are In the units Indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:01/10/2023 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 11 of 18

Pace Analytical Services,LLC
® 9800
aceAnalytical :intersv Suite lle,NC28078
www.pacelabs.cetn
[phone]
QUALITY CONTROL DATA
Project: STORMWATER 4TH QUARTER
Pace Project No.: 92642647
QC Batch: 744155 Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92642647001
METHOD BLANK: 3871795 Matrix: Water
Associated Lab Samples: 92642647001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chemical Oxygen Demand mg/L ND 25.0 12/17/22 19:05
LABORATORY CONTROL SAMPLE: 3871796
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 756 101 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3871797 3871798
MS MSD
92642470002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 5160 100 100 6230 6230 1070 1070 90-110 0 M1
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3871799 3871800
MS MSD
92642472001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 493 100 100 600 600 107 107 90-110 0
Results presented on this page are In the units Indicated by the"Units"column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:01/10/2023 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 12 of 18

Pace Analytical Services,LLC
i ® 9800 Kincey Ave. Suite:
aceAnalyteal
Huntersville,NC 28078
www.pacelabs.com
[phone]
QUALIFIERS
Project: STORMWATER 4TH QUARTER
Pace Project No.: 92642647
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
TNTC-Too Numerous To Count
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyt ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as
"Total"may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TNI-The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:01/10/2023 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 13 of 18

Pace Analytical Services,LLC
e 9800 Kincey Ave. Suite 100
aceAnalytical Huntersviile,NC 28078
www.pacelabs.com [phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: STORMWATER 4TH QUARTER
Pace Project No.: 92642647
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92642647001 OUTFALL 2 GRAB EPA 1664B 745392
92642647002 OUTFALL 1B GRAB EPA 1664B 745392
92642647001 OUTFALL 2 GRAB EPA 200.8 748154 EPA 200.8 748221
92642647002 OUTFALL 1 B GRAB EPA 200.8 748154 EPA 200.8 748221
92642647001 OUTFALL 2 GRAB SM 2540D-2015 744855
92642647002 OUTFALL 1 B GRAB SM 2540D-2015 744971
92642647001 OUTFALL 2 GRAB SM 5220D-2011 744155 SM 5220D-2011 744186
92642647002 OUTFALL 18 GRAB SM 5220D-2011 744152 SM 5220D-2011 744183
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:01/10/2023 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 14 of 18

� L)Cit Title: ENV-FRM-HUN1-0083 v01 Sample Condition Upon Receipt
lace
Effective Date: 05/121202205/12/2022
Laboratory receiving samples:
Asheville❑ Eden(? Greenwood E Huntersville(4 Raleigh Mechanicsville❑ Atlanta❑ Kernersville❑
SartteCnp an` Client Name: 1
lpaft Receipt / :WO#
fi 1 (?`� (met �C it e7tH: t
Courier: Fed Ex / ❑UPS (; S
❑LISPS �lient If 11111
❑Commercial Pace ['Other:
11111
III
I I III
92642347
Custody Seal Present? ❑Yes ]No Seals Intact? ❑Yes FijNo r'
Date/Initials Person Examining Contents://!`,TIU f la fi�/iL
Packing Material: ❑Bubble Wrap 1Bubble Bags ['None El Other Biological Tissue Frozen?
Thermometer: Oyes DNo J1N/A
[ejIR Gun ID: c2')7:rt-i b
Type of ice: ]Wet ❑Blue Duane
2 6 Correction Factor:
Cooler Temp: Add/Subtract(DC) ".O• ( Temp should be above freezing to 6°C
['Samples out of temp criteria.Samples on ice,cooling process
Cooler Temp Corrected(°C}: S has begun
USDA Regulated Soil([ICJ N/A,water sample)
Did samples originate in a quarantine zone within the United States:CA,NY,or SC Did samples originate from a foreign source(internationally,
(check maps)?Oyes juo including Hawaii and Puerto Rico)?Dyes ENO
Comments/Discrepancy:
Chain of Custody Present? I Yes ONo ON/A 1,
Samples Arrived within Hold Time? ❑Yes ❑No ON/A 2.
Short Hold Time Analysis(<72 hr.)? ❑Yes Duo (IN/A 3.
Rush Turn Around Time Requested? @Yes ❑Na ON/A 4.
Sufficient Volume? jYes Duo ON/A 5.
Correct Containers Used? ( Yes [No ON/A 6.
-Pace Containers Used? ®Yes Ohio ON/A
Containers Intact? IT/�Yes ❑No ON/A 7.
Dissolved analysis:Samples Field Filtered? ❑Yes Duo (IN/A 8,
Sample Labels Match COC? WIYes Quo ON/A s.
-Includes Date/Time/ID/Analysis Matrix: w
Headspace in VOA Vials(>5.6mm)? ❑Yes Duo VA N/A 1D.
Trip Blank Present? Oyes ❑No lffN/A 11.
Trip Blank Custody Seals Present? ❑Yes ❑No N/A
COMMENTS/SAMPLE DISCREPANCY Field Date Required? ['Yes Duo
Lot ID of splitcontainers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/Time:
Project Manager SCURF Review: Date:
_f'rOjett Manager SRE Review:__.. .__.._—
Qualtrax ID:69614 Page 1 of 2 Page 15 of 18

�/ UL#F_Title: ENV-FRNi-HUN1-0083 v01_Sample Condition Upon Receipt
i ace
Effective Date:05/121202205/12/2022
*Check mark top half of box if pH and/or dechlorination is verified and Project# 92642647
within the acceptance range for preservation samples. PM: TIH Due Date: 12/23/22
Exceptions:VOA,Coliform,TOC,Oil and Grease,OR0/8015{water}DOC,LLlig CLIENT: 92—Ag i 1 i ty F
**Bottom half of box is to list number of bottles l
***Check all unpreserved Nitrates for chlorine
.d. u O 22. V. ¢ _ IA
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N a. N J.
Q Z ea N f.l
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RI N OJ V y A N N y = Q .Y Q Q 4 z N
m 4/ m 2 - 0. a f° Z v a a n Z m ` d fa Z a v ' m
m • _ �
ai v v vim, a m u = Y1 N x m v D U ¢ m ,s Z z v ,3 y
a O 10 v a a. N a „ O ,„ z r;� O.
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2 u O _.,.. _-u u u . v-. T U n c m N.. -M a.: ii .ts 0.) •ni a.
- �, as w .a 2 7 2 :ac v a ... .0 = a
ll; 2 r, 1 m 1�° n E c .a • E n E £ Q < Q < Q ,- u '-. g ' E c E
.L `.. a Q E Q Q Q 1 J O > O O O a vt tel 1 0 Q
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N O — N sn N N O U1 u7 O O O O O 5 N a ° O O O
H N L11 .i .:1 N r1 .-1 'i .^r N .•i 1V N Y sr q i tl .s .i N r;el a-, N 1.
>t a O ' 3 h Z N m 2 7 = O V! N 4 2 Y. D > Yl Y $� h` K 6 O 7
E et m N .-1 a m a a. (g ,.1 .1 to f/1 Q. T M CA OY 01 0 Ill N PI O 0 cn
v a a a a a tt a a ( a co C) is 8 `? w t l7 U' a a a 0 w 0
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Adjustment Log for Preserved Samples
Sample 1D Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Lot ft
adjusted added
Note:-WheneVer there is a dik epancy affecting North Carolina compliance samples,a copy of this form will be sent to the NorthrY I— —Carolina 0£NR Certification Office(i.e.
Out of hold,incorrect preservative,out of temp,incorrect containers.
Qualtrax ID:69614 Page 2 of 2 Page 16 of 18

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ET 0
N.• "V A'. �J`� 1JT Q.) EOFCO)ITAMIERS . a�i.. _0...3 ? e n �,a C
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S^ Oilier o D W
Analyses Test Y/N 8
,a m
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Received On(CO - C) o'
(YIN) t ` 33D l
Custody Seated
a
Cooler a- ( � ` ,(-.- 0
(YIN) F.
Samples Intact ('
(YIN) -,1.
I
Page 17 of 18

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1 SAMPLE TEMP AT COLLECTION} g
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NOFeserve CONTAINERS b y v g p T R 2.
' a 3 0 ,moo, �c 'CA
Unpre$eNod .00
o a v O m N V•
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a' Melhnnaf I
^ Z
l Other Q D C'3
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Custody Sealed ?! t
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(YIN) $ O
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(Y/N) 2
b
Page 18 of 18