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HomeMy WebLinkAboutNCG030721_2022 DMR_20230110 NCDEQ Division of Energy, Mineral and Land Resources Stormwater Discharge Monitoring Report(DMR) Form for NCG030000 Metal Fabrication Click here for instructions Complete,sign,scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report(DMR) Upload form within 30 days of receiving sampling results. Mail the original,signed hard copy of the DMR to the appropriate DEMLR Regional Office. Certificate of Coverage No. NCGO3 0721 Person Collecting Samples:Dan Freitas Facility Name:Southwire Company Laboratory Name:Enthalpy Analytical Facility County:Franklin County Laboratory Cert. No.:495 Discharge during this period:El Yes ❑No (if no,skip to signature and date) Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances?Q Yes Q No If so,which Tier(I, II,or Ill)? A copy of this DMR has been uploaded electronically via https://edocs.deq.nc.gov/Forms/SW-DMR ❑� Yes 0 No Date Uploaded: 1/10/2023 Analytical Monitoring Requirements for Outfalls with Industrial Activities—Benchmarks in(Red) Parameter Parameter Outfall 001 Outfall Outfall Outfall Outfall Code N/A Receiving Stream Class Intermittent Stream N/A Date Sample Collected MM/DD/YYYY 12/22/2022 46529 24-Hour Rainfall in inches 0.96 C0530 TSS in mg/L(100 or 50*) 00400 pH in standard units(6.0—9.0 FW, 7.95 6.8-8.5 SW) Copper,total recoverable in mg/L 01119 <0.01 (0.010 FW,0.0058 SW) Lead,total recoverable in mg/L 01051 <0.01 (0.075 FW,0.22 SW) 01094 Zinc,total recoverable in mg/L(0.126 FW,0.095 SW) 0.0384 00340 Chemical Oxygen Demand(COD)in mg/L(120) 00552 Non-Polar Oil&Grease in mg/L(15) * Outfalls to Outstanding Resource Waters(ORW),High Quality Waters(HQW),Trout Waters(Tr)and Primary Nursery Areas(PNA) have a benchmark TSS limit of 50 mg/L.All other water classifications have a benchmark of 100 mg/L FW(Freshwater)SW(Saltwater) Notes(optional):Metals only evaluation to conclude the Monthly benchmark requried sampling.Per Tier II.No longer in Tier Reponse. "I certify by my signature below,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who manage the system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,accurate,and complete.I am aware that there are significant penalties for submitting false infor tion,inclu " the possibility of fines and imprisonment for knowing violations." 1.10.2023 Si ature of rmittee or Delegated Authorized Individual Date Kenneth.playford@soutwire.com 470.230.9903 Email Address Phone Number Kenneth Playford From: Daniel Freitas <dafreitas@montrose-env.com> Sent: Tuesday, January 3, 2023 9:10 AM To: Kenneth Playford Cc: Josh Perry; Robert Powell; Gilbert Brooks;Jan Dobinsky Subject: [EXTERNALMAIL]Re: [EXTERNALMAIL]December Metals Sampling Attachments: image001.png; 22L1330_2 EA_Level2 12 30 2022 1507.pdf Follow Up Flag: Follow up Flag Status: Flagged Categories: Compliance Reports, Site Support This email originated from outside the organization. Do not click links or open attachments unless you have verified this email is legitimate. Good morning, I hope you all had a wonderful holiday!The December metals sampling went very smoothly before the Christmas break and attached you will find the results. Below are my field notes and observations: Sampled on 22 December 2022 Rainfall:0.96 inches Outfall pH 7.95 at 8.8 deg C Roof drain pH 6.15 at 8.4 deg C All runoff was clear of sediment,odor free,and had no suds or oil sheen. If you have any questions please let me know. Regards, Dan Freitas Project Scientist X -_ 8048 Market St. Suite D, Wilmington, NC 28411 Mobile 530.559.2463 I Fax 407. 629.7595 dafreitasmontrose-env.com 1 This is a confidential communication.The information contained in this e-mail message is intended only for the use of the individual or entity to which it is addressed. Information contained herein may be protected from further dissemination or disclosure under applicable laws. If the reader of this transmission is not the intended recipient or the employee or agent responsible for delivering the transmission to the intended recipient,you are hereby notified that any dissemination, distribution,copying or use of this transmission or its contents is strictly prohibited. If you have received this transmission in error, please notify the e-mail sender. On Tue, Dec 27,2022 at 10:07 AM Kenneth Playford<Kenneth.Playford@southwire.com>wrote: Hi Daniel, Thank you for the heads up. Hopefully your sampling went well. ••• Kenneth Playford •.. 00 Environmental Manager I Corporate Phone 770-832-5547 Mobile 470-230-9903 Web www.southwire.com Email Kenneth.playford@southwire.com One Southwire Dr.,Carrollton Ga,30119 From: Daniel Freitas<dafreitas@montrose-env.com> Sent:Wednesday, December 21, 2022 3:41 PM To: Kenneth Playford<Kenneth.Playford@southwire.com>;Josh Perry<Josh.Perry@southwire.com>; Robert Powell <Robert.Powell@southwire.com>;Gilbert Brooks<Gilbert.Brooks@southwire.com>;Jan Dobinsky <jdobinsky@montrose-env.com> Subject: [EXTERNALMAIL]December Metals Sampling This email originated from outside the organization. Do not click links or open attachments unless you have verified this email is legitimate. Good afternoon, 2 I wanted to inform you that I will be onsite tomorrow morning to collect the December monthly metals samples for the Youngsville Southwire facility. I will keep an eye on the storm tonight to determine when I arrive but it will be very close to opening hours. If you have any questions please give me a call on my cell phone listed below. Respectfully, Dan Freitas Project Scientist 8048 Market St. Suite D, Wilmington, NC 28411 Mobile 530.559.2463 I Fax 407. 629.7595 dafreitas(a)montrose-env.com This is a confidential communication.The information contained in this e-mail message is intended only for the use of the individual or entity to which it is addressed. Information contained herein may be protected from further dissemination or disclosure under applicable laws. If the reader of this transmission is not the intended recipient or the employee or agent responsible for delivering the transmission to the intended recipient,you are hereby notified that any dissemination, distribution,copying or use of this transmission or its contents is strictly prohibited. If you have received this transmission in error, please notify the e-mail sender. CONFIDENTIALITY NOTICE:The contents of this email message and any attachments are intended solely for the addressee(s) and may contain confidential, proprietary and/or privileged information and may be legally protected from disclosure. If you are not the intended recipient of this message or their agent, or if this message has been addressed to you in error, please immediately alert the sender by reply email and then delete this message and any attachments and the reply from your system. If you are not the intended recipient, you are hereby notified that any disclosure, use, dissemination, copying, or storage of this message or its attachments is strictly prohibited. CONFIDENTIALITY NOTICE:The contents of this email message and any attachments are intended solely for the addressee(s) and may contain confidential, proprietary and/or privileged information and may be legally protected from disclosure. If you are not the intended recipient of this message or their agent, or if this message has been addressed to you in error, please immediately alert the sender by reply email and then delete this message and any attachments and the reply from your system. If you are not the intended recipient, you are hereby notified that any disclosure, use, dissemination, copying, or storage of this message or its attachments is strictly prohibited. 3 I wanted to inform you that I will be onsite tomorrow morning to collect the December monthly metals samples for the Youngsville Southwire facility. I will keep an eye on the storm tonight to determine when I arrive but it will be very close to opening hours. If you have any questions please give me a call on my cell phone listed below. Respectfully, Dan Freitas Project Scientist 8048 Market St. Suite D, Wilmington, NC 28411 Mobile 530.559.2463 Fax 407. 629.7595 dafreitas(a�montrose-env.com This is a confidential communication.The information contained in this e-mail message is intended only for the use of the individual or entity to which it is addressed. Information contained herein may be protected from further dissemination or disclosure under applicable laws. If the reader of this transmission is not the intended recipient or the employee or agent responsible for delivering the transmission to the intended recipient,you are hereby notified that any dissemination, distribution,copying or use of this transmission or its contents is strictly prohibited. If you have received this transmission in error, please notify the e-mail sender. CONFIDENTIALITY NOTICE: The contents of this email message and any attachments are intended solely for the addressee(s) and may contain confidential, proprietary and/or privileged information and may be legally protected from disclosure. If you are not the intended recipient of this message or their agent, or if this message has been addressed to you in error, please immediately alert the sender by reply email and then delete this message and any attachments and the reply from your system. If you are not the intended recipient, you are hereby notified that any disclosure, use, dissemination, copying, or storage of this message or its attachments is strictly prohibited. CONFIDENTIALITY NOTICE: The contents of this email message and any attachments are intended solely for the addressee(s) and may contain confidential, proprietary and/or privileged information and may be legally protected from disclosure. If you are not the intended recipient of this message or their agent, or if this message has been addressed to you in error, please immediately alert the sender by reply email and then delete this message and any attachments and the reply from your system. If you are not the intended recipient, you are hereby notified that any disclosure, use, dissemination, copying, or storage of this message or its attachments is strictly prohibited. 3 .01174 ENTHALPY �� ANALYTICAL 1941 Reymet Road • Richmond,Virginia 23237 •Tel:(804)-358-8295 Fax:(804)-358-8297 Certificate of Analysis Final Report Laboratory Order ID 22L1330 Client Name: MSE Group, LLC -Wilmington, NC Date Received: December 27, 2022 15:00 8048 Market Street Date Issued: December 30, 2022 15:07 Wilmington, NC 28411 Project Number: 20224360 Submitted To: Dan Freitas Purchase Order: Client Site I.D.: DCN Cables Enclosed are the results of analyses for samples received by the laboratory on 12/27/2022 15:00. If you have any questions concerning this report, please feel free to contact the laboratory. Sincerely, ,s Ted Soyars Technical Director End Notes: The test results listed in this report relate only to the samples submitted to the laboratory and as received by the Laboratory. Unless otherwise noted, the test results for solid materials are calculated on a wet weight basis. Analyses for pH, dissolved oxygen, temperature, residual chlorine and sulfite that are performed in the laboratory do not meet NELAC requirements due to extremely short holding times. These analyses should be performed in the field. The results of field analyses performed by the Sampler included in the Certificate of Analysis are done so at the client's request and are not included in the laboratory's fields of certification nor have they been audited for adherence to a reference method or procedure. The signature on the final report certifies that these results conform to all applicable NELAC standards unless otherwise specified. For a complete list of the Laboratory's NELAC certified parameters please contact customer service. This report shall not be reproduced except in full without the expressed and written approval of an authorized representative of Enthalpy Analytical. J°p TNI Accredited VELAP ID 460021 Page 1 of 11 ENTHALPY � ANALYTICAL 1941 Reymet Road *Richmond,Virginia 23230 *Tel:(804)-358-8295 Fax:(804)-358-8297 Certificate of Analysis Final Report Client Name: MSE Group, LLC-Wilmington, NC Date Issued: December 30, 2022 15:07 8048 Market Street Project Number: 20224360 Purchase Order: Wilmington NC, 28411 Submitted To: Dan Freitas Client Site I.D.: DCN Cables ANALYTICAL REPORT FOR SAMPLES Laboratory Order ID 22L1330 Sample ID Laboratory ID Matrix Date Sampled Date Received Outfall December 22L1330-01 Waste Water 12/22/2022 10:10 12/27/2022 15:00 Roof Drain December 22L1330-02 Waste Water 12/22/2022 10:20 12/27/2022 15:00 Page 2 of 11 ENTHALPY 9 ANALYTICAL 1941 Reymet Road•Richmond,Virginia 23230 •Tel:(804)-358-8295 Fax:(804)-358-8297 Certificate of Analysis Final Report Client Name: MSE Group, LLC-Wilmington, NC Date Issued: December 30, 2022 15:07 8048 Market Street Project Number: 20224360 Purchase Order: Wilmington NC,28411 Submitted To: Dan Freitas Client Site I.D.: DCN Cables Laboratory Order ID:22L1330 Analytical Results Sample I.D. Outfall December Laboratory Sample ID: 22L1330-01 Grab Date/Time: 12/22/2022 10:10 Field Residual CI: Field pH: Reporting Sample Prep Analysis Parameter Samp ID Method Result Qual Limit D.F. Date/Tme Date/me Analyst Metals(Total)by EPA 200 Series Methods Copper 01 EPA200.7 Rev 4.4 <0.0100 mg/L 0.0100 1 12/28/22 13:15 12/29/22 14:32 AB Lead 01 EPA200.7 Rev 4.4 <0.0100 mg/L 0.0100 1 12/28/22 13:15 12/29/22 14:32 AB Zinc 01 EPA200.7 Rev 4.4 0.0384 mg/L 0.0100 1 12/28/22 13:15 12/29/22 14:32 AB Page 3 of 11 ag'.J o ENTHALPY irt ANALYTICAL 1941 Reymet Road•Richmond,Virginia 23230 •Tel:(804)-358-8295 Fax:(804)-358-8297 Certificate of Analysis Final Report Client Name: MSE Group, LLC-Wilmington, NC Date Issued: December 30,2022 15:07 8048 Market Street Project Number: 20224360 Purchase Order: Wilmington NC, 28411 Submitted To: Dan Freitas Client Site I.D.: DCN Cables Laboratory Order ID:22L1330 Analytical Results Sample I.D. Roof Drain December Laboratory Sample ID: 22L1330-02 Grab Date/Time: 12/22/2022 10:20 Field Residual CI: Field pH: Reporting Sample Prep Analysis Parameter Samp ID Method Result Qual Limit D.F. Date/Time Date/Time Analyst Metals(Total)by EPA 200 Series Methods Copper 02 EPA200.7 Rev 4.4 <0.0100 mg/L 0.0100 1 12/28/22 13:15 12/29/22 14:37 AB Lead 02 EPA200.7 Rev 4.4 <0.0100 mg/L 0.0100 1 12/28/22 13:15 12/29/22 14:37 AB Zinc 02 EPA200.7 Rev 4.4 0.0390 mg/L 0.0100 1 12/28/22 13:15 12/29/22 14:37 AB Analytical Summary Administrative Preparation Method: Preparation Factors Sample ID Initial/Final Method Batch ID Sequence ID Calibration ID Metals(Total)by EPA 200 Series Methods Preparation Method: EPA200.2/R2.8 22L1330-01 50.0 mL/50.0 mL EPA200.7 Rev 4.4 BFL1032 SFL1027 AL20169 22L1330-02 50.0 mL/50.0 mL EPA200.7 Rev 4.4 BFL1032 SFL1027 AL20169 Page 4 of 11 ip411119 ENTHALPY _Z 4. 1, ANALYTICAL 1941 Reymet Road•Richmond,Virginia 23230 •Tel:(804)-358-8295 Fax:(804)-358-8297 Certificate of Analysis Final Report Client Name: MSE Group, LLC-Wilmington, NC Date Issued: December 30, 2022 15:07 8048 Market Street Project Number: 20224360 Purchase Order: Wilmington NC,28411 Submitted To: Dan Freitas Client Site I.D.: DCN Cables - QC Analytical Summary Preparation Factors Sample ID initial/Final Method Batch ID Sequence ID Calibration ID Metals(Total)by EPA 200 Series Methods Preparation Method: EPA200.2/R2.8 BFL1032-BLK1 50.0 mL/50.0 mL EPA200.7 Rev 4.4 BFL1032 SFL1027 AL20169 BFL1032-BS1 50.0 mL/50.0 mL EPA200.7 Rev 4.4 BFL1032 SFL1027 AL20169 BFL1032-MS1 50.0 mL/50.0 mL EPA200.7 Rev 4.4 BFL1032 SFL1027 AL20169 BFL1032-MSD1 50.0 mL/50.0 mL EPA200.7 Rev 4.4 BFL1032 SFL1027 AL20169 Page 5 of 11 I0,6C if � ENTHALPY _ ANALYTICAL 1941 Reymet Road•Richmond,Virginia 23230 •Tel:(804)-358-8295 Fax:(804)-358-8297 Certificate of Analysis Final Report Client Name: MSE Group, LLC-Wilmington, NC Date Issued: December 30, 2022 15:07 8048 Market Street Project Number: 20224360 Purchase Order: Wilmington NC, 28411 Submitted To: Dan Freitas Client Site I.D.: DCN Cables Metals(Total) by EPA 200 Series Methods-Quality Control Enthalpy Analytical Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Qual Batch BFL1032-EPA200.2/R2.8 Blank(BFL1032-BLK1) Prepared: 12/28/2022 Analyzed: 12/29/2022 Copper <0.0100 mg/L 0.0100 mg/L Lead <0.0100 mg/L 0.0100 mg/L Zinc <0.0100 mg/L 0.0100 mg/L LCS(BFL1032-BS1) Prepared: 12/28/2022 Analyzed: 12/29/2022 Copper 0.516 mg/L 0.0100 mg/L 0.500 mg/L 103 85-115 Lead 0.503 mg/L 0.0100 mg/L 0.500 mg/L 101 85-115 Zinc 0.511 mg/L 0.0100 mg/L 0.500 mg/L 102 85-115 Matrix Spike(BFL1032-MS1) Source:22L1329-01 Prepared: 12/28/2022 Analyzed: 12/29/2022 Copper 0.525 mg/L 0.0100 mg/L 0.500 <0.0100 mg/L 105 75-125 Lead 0.507 mg/L 0.0100 mg/L 0.500 <0.0100 mg/L 101 75-125 Zinc 9.71 mg/L 0.0100 mg/L 0.500 9.06 mg/L 130 75-125 M Matrix Spike Dup(BFL1032-MSD1) Source:22L1329-01 Prepared: 12/28/2022 Analyzed: 12/29/2022 Copper 0.518 mg/L 0.0100 mg/L 0.500 <0.0100 mg/L 104 75-125 1.47 20 Lead 0.497 mg/L 0.0100 mg/L 0.500 <0.0100 mg/L 99.4 75-125 2.06 20 Zinc 9.52 mg/L 0.0100 mg/L 0.500 9.06 mg/L 92.1 75-125 1.98 20 Page 6 of 11 I66,0U,o teel ENTHALPY � ANALYTICAL 1941 Reymet Road•Richmond,Virginia 23230 •Tel:(804)-358-8295 Fax:(804)-358-8297 Certificate of Analysis Final Report Client Name: MSE Group, LLC-Wilmington, NC Date Issued: December 30, 2022 15:07 8048 Market Street Project Number: 20224360 Purchase Order: Wilmington NC,28411 Submitted To: Dan Freitas Client Site I.D.: DCN Cables Certified Analyses included in this Report Analyte Certifications EPA200.7 Rev 4.4 In Non-Potable Water Copper VELAP,NCDEQ,WVDEP Lead VELAP,NCDEQ,WVDEP Zinc VELAP,NCDEQ,WVDEP Code Description Laboratory ID Expires MdDOE Maryland DE Drinking Water 341 12/31/2023 NC North Carolina DENR 495 07/31/2023 NCDEQ North Carolina DEQ 495 07/31/2023 NCDOH North Carolina Department of Health 51714 07/31/2023 NYDOH New York DOH Drinking Water 12096 04/01/2023 PADEP NELAP-Pennsylvania Certificate#008 68-03503 10/31/2023 VELAP NELAP-Virginia Certificate#12157 460021 06/14/2023 WVDEP West Virginia DEP 350 11/30/2023 Page 7 of 11 ag,,ono ENTHALPY 0. 1 ANALYTICAL 1941 Reymet Road w Richmond,Virginia 23230 a Tel:(804)-358-8295 Fax:(804)-358-8297 Certificate of Analysis Final Report Client Name: MSE Group, LLC-Wilmington, NC Date Issued: December 30, 2022 15:07 8048 Market Street Project Number: 20224360 Purchase Order: Wilmington NC, 28411 Submitted To: Dan Freitas Client Site I.D.: DCN Cables Summary of Data Qualifiers M Matrix spike recovery is outside established acceptance limits RPD Relative Percent Difference Qual Qualifers -RE Denotes sample was re-analyzed D.F. Dilution Factor. Please also see the Preparation Factor in the Analysis Summary section. TIC Tentatively Identified Compounds are compounds that are identified by comparing the analyte mass spectral pattern with the NIST spectral library.A TIC spectral match is reported when the pattern is at least 75%consistent with the published pattern. Compound concentrations are estimated and are calculated using an internal standard response factor of 1. PCBs,Total Total PCBs are defined as the sum of detected Aroclors 1016,1221,1232.1248,1254,1260,1262,and 1268. Page 8 of 11 1941 REYMET ROAD Chain of Custody107., RICHMOND, 58-829VIRGINIA 23237 Effective:Mar 10,2021 E N -1^ H A I (804)358-8295 PHONE ._ A ( ', f `!' i ! ( I (804)358-8297 FAX CHAIN OF CUSTODY PAGE 1 OF 1 COMPANY NAME:Montrose Environmental Group INVOICE TO:Jan Dobinsky PROJECT NAME/Quote#2022 NPDES SW Sampling CONTACT: Dan Freitas INVOICE CONTACT: ldobinsky@montrose-env.com SITE NAME: DCN Cables ADDRESS: 8048 Market St.Suite D.Wilmington.NC teat INVOICE ADDRESS West Chester, P Suite 0 PROJECT NUMBER: 20224360 PHONE#:530-559-2463 INVOICE PHONE#: 610-840-9136 P.O #: FAX#: EMAIL: dafreitas@montrose-env.com Pretreatment Program: Is sample for compliance reporting? ®NO Regulatory State: NC Is sample from a chlorinated supply? YES NO) PWS I.D. #. SAMPLER NAME (PRINT): Dan Freitas SAMPLER SIGNATURE: ) ,_,—X Turn Around Time. Circle 10 Days or_Day(s) Matrix Codes: WW=Waste Water/Storm Water GW=Ground Water DW=Drinking Water S=Soil!Solids OR=Organic A=Air WP=Wipe OT=Other COMMENTS Preservative Codes N=Nunc Aca -115 0. ANALYSIS/(PRESERVATIVE) C=HydrocnloncAce S=Suituric A;la O H=Sodium Hydroxide A=Ascorbic 2 0) Acid Z=Zinc Acetate T=Sodium -0 (L) . Thiosultate M=Methanol cD 7 N O W O N o Ti E n a) Q o CLIENT SAMPLE I.D. in o r a E -n „ m w x cfi U c a �I mi o a� o a (/) CO p (/) O U C)) r;• o CV a) N a) N a) 0) LO N '.0. 8 q E N (n o iLT_ I-- (1. N C a W 0 _O 0 0 O E @ PUMP PLEASE NOTE PRESERVAtIVi INTERFERENCE CHECKS or PUM O U U- 0 U 0 0 0 F- F- 2 Z RATE(Linn) 1) Outfall December X 1L./'zL 1010 WW 1 X HNO3 2) Roof Drain December X -2( 2z/n.Jo'1', WW 1 X HNO3 6) 7) 8) 9) 10) R QUISHED DATE// TIME RE IVER DATE ! TIME QC Data Package LAB USE ONLY Therm ID: 1-1 COOLER TEMP 13 •i6 ^°�C [ -DI Freitas t i hOL 11;tZ ./t I t/ 1,(i2 i/ZZ ll � O.7 i, .'ice t Custody Seals used and intact?(Y Received on i Y Iry i R 2QUISHED 7DAT/E / TIME RECEIVED / v DATE / ITIME Level III LI �/ _a-�-,,� ,Z/4Z/14- iy Y- i212111/2 103 MSE Group, LLC - 22L1330 R 0 QUISHED " DATE / TIME RECEIVED DATE / TIME Level IV . : 2022 NPDES SW Sampling — VQ A 14. C - Reed: 12/27/2022 Due: 01/04/2023 v130325002 Sample Preservation Log Form#.F1301 Rev#12.0 Effective:Feb 17,2022 EITHALPY Page 1 of 1 63111. 41-.1 A Nf A r VTICA L. Sample Preservation Log Order ID 22L1330 Date Performed: i2/2BJ22- Analyst Performing Check: C5 6 Pesticide Pest/PCB Metals Cyanide Sulfide Ammonia TICK Phos,Tot NO3+NO2 DRO (8081/808/508) SVOC CrVi • •• (508)I Q 9 PCB DW only (tilelDz7ttle2� SVOC(525) pH as PH as pH as pH to PH as pH m pH as PFI as Racelvd Rsealwd y pH as PH as PH as Received I. Raeatved u Received Received n Ranetv.d I. ReuaMd_ Received v Received =n Fos.CI final Rae.CI final Td Received $ Received n Received I. +or- +or• 1 <i Other •12 Other >8 Olhar `` <2 Other s2 Other <2 Other <2 Other <2 Other + + <2 Other r` Other Other 0I A / 02 A / . . . . - • 1aOH ID: HNO3 ID: CrVi preserved date/time: Analyst Initials: •pH must be attested sted between 9.3-A7 12SO4 ID: Na2S203 ID: Buffer Sorn ID: ICt.ID: Na2SO3 ID: 1N NaOH ID: 5N NaOH: 1J 0) ca m 0 0 THIS DOCUMENT IS UNCONTROLLED WHEN PRINTED V.\ 1 h,cedillas DISS CrVI and not T CM as an approved analyte under40CFR138 for waste water. F1301 Sample Preservation Log 12_0 ENTHALPY I ANALYTICAL 1941 Reymet Road * Richmond,Virginia 23230 •Tel:(804)-358-8295 Fax:(804)-358-8297 Certificate of Analysis Final Report Client Name: MSE Group, LLC -Wilmington, NC Date Issued: December 30, 2022 15:07 8048 Market Street Project Number: 20224360 Purchase Order: Wilmington NC, 28411 Submitted To: Dan Freitas Client Site I.D.: DCN Cables Sample Conditions Checklist Samples Received at. 13.80°C How were samples received? FedEx Express Were Custody Seals used? If so,were they received intact? No Are the custody papers filled out completely and correctly? Yes Do all bottle labels agree with custody papers? Yes Is the temperature blank or representative sample within acceptable limits or received on ice,and recently taken? Yes Are all samples within holding time for requested laboratory tests? Yes Is a sufficient amount of sample provided to perform the tests included? Yes Are all samples in appropriate containers for the analyses requested? Yes Were volatile organic containers received? No Are all volatile organic and TOX containers free of headspace" NA Is a trip blank provided for each VOC sample set? VOC sample sets include EPA8011,EPA504,EPA8260,EPA624, NA EPA8015 GRO,EPA8021,EPA524,and RSK-175. Are all samples received appropriately preserved? Note that metals containers do not require field preservation but lab Yes preservation may delay analysis. Page 11 of 11