NCG060089_2022 DMR_20221212 (3)

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ti' . eurofins
Environment Testing
ANALYTICAL REPORT
1 Eurofins Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
.__
L•;
s-- Laboratory Job ID: 680-224611-1
„i Client Project/Site: CF05510
-il / For:
k °K- 4. Environmental Conservation Laboratories
—_"-, 102 Woodwinds Industrial Ct, Suite A
� y Cary, North Carolina 27511
,f4011/00)
... Attn: Stephanie Franz
K atik; irlslit40A...4
Authorized for release by:
11/14/2022 10:53:06 AM
Naomi Flanagan, Project Manager
[phone]
[e-mail]
Designee for
Sheila Hoffman, Project Manager II
[phone]
[e-mail]
LINKS
Review your project
results through
%''. E O L
\+ The test results in this report meet all 2003 NELAC,2009 TNI,and 2016 TNI
requirements for accredited parameters,exceptions are noted in this report.This
Have a Question? report may not be reproduced except in full,and with written approval from the
laboratory. For questions please contact the Project Manager at the e-mail address or
w 5 telephone number listed on this page.
u //Th a This report has been electronically signed and authorized by the signatory. Electronic
I 1 signature is intended to be the legally binding equivalent of a traditionally handwritten
Ex ert signature.
Results relate only to the items tested and the sample(s)as received by the laboratory.
CThe test results in this report relate only to the samples as received by the laboratory
Visit Us at: and will meet all requirements of the methodology,with any exceptions noted.This
www eurofinsus com/Env report shall not be reproduced except in full,without the express written approval of
the laboratory.All questions should be directed to the{0}Project Manager.

Sample Summary
Client: Environmental Conservation Laboratories Job ID: 680-224611-1
Project/Site: CF05510
Lab Sample ID Client Sample ID Matrix Collected Received
680-224611-1 Outfall 1 Water 11/01/22 06:15 11/04/22 08:20
680-224611-2 Outfall 2 Water 11/01/22 06:25 11/04/22 08:20
680-224611-3 Outfall 3 Water 11/01/22 06:32 11/04/22 08:20
Page 2 of 17 Eurofins 4 O 2

Method Summary
Client: Environmental Conservation Laboratories Job ID: 680-224611-1
Project/Site: CF05510
Method Method Description Protocol Laboratory
1664B HEM and SGT-HEM 1664B EET SAV
1664B HEM and SGT-HEM (Aqueous) 1664B EET SAV
Protocol References:
1664B=EPA-821-98-002
Laboratory References:
EET SAV=Eurofins Savannah,5102 LaRoche Avenue,Savannah,GA 31404,TEL[phone]
Eurofins Savannah
Page 3 of 17 11/14/2022

Definitions/Glossary
Client: Environmental Conservation Laboratories Job ID: 680-224611-1
Project/Site: CF05510 �.
Qualifiers
General Chemistry
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
Listed under the"D"column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio(normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit(DoD/DOE)
DL,RA,RE, IN Indicates a Dilution,Re-analysis,Re-extraction,or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration(Radiochemistry)
EDL Estimated Detection Limit(Dioxin)
LOD Limit of Detection(DoD/DOE)
LOQ Limit of Quantitation(DoD/DOE)
MCL EPA recommended"Maximum Contaminant Level"
MDA Minimum Detectable Activity(Radiochemistry)
MDC Minimum Detectable Concentration(Radiochemistry)
MDL Method Detection Limit
ML Minimum Level(Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit(or MDL or EDL if shown)
NEG Negative/Absent
POS Positive/Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio(Radiochemistry)
RL Reporting Limit or Requested Limit(Radiochemistry)
RPD Relative Percent Difference,a measure of the relative difference between two points
TEF Toxicity Equivalent Factor(Dioxin)
TEQ Toxicity Equivalent Quotient(Dioxin)
TNTC Too Numerous To Count
Eurofins Savannah
Page 4 of 17 11/14/2022

Case Narrative
Client: Environmental Conservation Laboratories Job ID: 680-224611-1
Project/Site: CF05510
Job ID: 680-224611-1
Laboratory: Eurofins Savannah
Narrative
Job Narrative
680-224611-1
Receipt
The samples were received on 11/4/2022 8:20 AM. Unless otherwise noted below,the samples arrived in good condition, and,where
required, properly preserved and on ice. The temperature of the cooler at receipt time was 4.8°C
General Chemistry
No additional analytical or quality issues were noted,other than those described above or in the Definitions/Glossary page.
Eurofins Savannah
Page 5 of 17 11/14/2022

Detection Summary
Client: Environmental Conservation Laboratories Job ID: 680-224611-1
Project/Site: CF05510
Client Sample ID: Outfall 1 Lab Sample ID: 680-224611-1
No Detections.
Client Sample ID: Outfall 2 Lab Sample ID: 680-224611-2 4
No Detections.
Client Sample ID: Outfall 3 Lab Sample ID: 680-224611-3
Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type
HEM(Oil&Grease) 3.5 J 12.4 3.5 mg/L 1 1664E Total/NA
This Detection Summary does not include radiochemical test results.
Eurofins Savannah
Page 6 of 17 11/14/2022

Client Sample Results
Client: Environmental Conservation Laboratories Job ID: 680-224611-1
Project/Site: CF05510
Client Sample ID: Outfall 1 Lab Sample ID: 680-224611-1
Date Collected: 11/01/22 06:15 Matrix: Water
Date Received: 11/04/22 08:20
General Chemistry
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
HEM(Oil&Grease)(1664B) <3.2 11.5 3.2 mg/L 11/11/22 07:25 11/11/22 09:18 1
Eurofins Savannah
Page 7 of 17 11/14/2022

Client Sample Results
Client: Environmental Conservation Laboratories Job ID: 680-224611-1
Project/Site: CF05510
Client Sample ID: Outfall 2 Lab Sample ID: 680-224611-2
Date Collected: 11/01/22 06:25 Matrix: Water
Date Received: 11/04/22 08:20
General Chemistry
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
HEM(Oil&Grease)(1664B) <3.0 10.6 3.0 mg/L 11/11/22 07:25 11/11/22 09:18 1
Eurofins Savannah
Page 8 of 17 11/14/2022

Client Sample Results
Client: Environmental Conservation Laboratories Job ID: 680-224611-1
Project/Site: CF05510
Client Sample ID: Outfall 3 Lab Sample ID: 680-224611-3
Date Collected: 11/01/22 06:32 Matrix: Water
Date Received: 11/04/22 08:20
General Chemistry
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
HEM(Oil&Grease)(1664B) 3.5 J 12.4 3.5 mg/L 11/11/22 07:25 11/11/22 09:18 1
Eurofins Savannah
Page 9 of 17 11/14/2022

QC Sample Results
Client: Environmental Conservation Laboratories Job ID: 680-224611-1
Project/Site: CF0551O
Method: 1664B - HEM and SGT-HEM
Lab Sample ID: MB 680-750099/1-A Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 750134 Prep Batch: 750099
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
HEM(Oil&Grease) <1.4 5.0 1.4 mg/L 11/11/22 07:25 11/11/22 09:18 1 6
Lab Sample ID: LCS 680-750099/2-A Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 750134 Prep Batch: 750099
Spike LCS LCS %Rec
Analyte Added Result Qualifier Unit D %Rec Limits
HEM(Oil&Grease) 40.0 31.40 mg/L 78 78-114
Lab Sample ID: LCSD 680-750099/3-A Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: Total/NA
Analysis Batch: 750134 Prep Batch: 750099
Spike LCSD LCSD %Rec RPD
Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit
HEM(Oil&Grease) 40.0 33.80 mg/L 85 78-114 7 18
Eurofins Savannah
Page 10 of 17 11/14/2022

QC Association Summary
Client: Environmental Conservation Laboratories Job ID: 680-224611-1
Project/Site: CF05510
General Chemistry
Prep Batch: 750099
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
680-224611-1 Outfall 1 Total/NA Water 1664B
680-224611-2 Outfall 2 Total/NA Water 1664B
680-224611-3 Outfall 3 Total/NA Water 1664B
MB 680-750099/1-A Method Blank Total/NA Water 1664B
LCS 680-750099/2-A Lab Control Sample Total/NA Water 1664B
LCSD 680-750099/3-A Lab Control Sample Dup Total/NA Water 1664B13
Analysis Batch: 750134
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
680-224611-1 Outfall 1 Total/NA Water 1664B 750099
680-224611-2 Outfall 2 Total/NA Water 1664B 750099
680-224611-3 Outfall 3 Total/NA Water 1664B 750099
MB 680-750099/1-A Method Blank Total/NA Water 1664B 750099
LCS 680-750099/2-A Lab Control Sample Total/NA Water 1664B 750099
LCSD 680-750099/3-A Lab Control Sample Dup Total/NA Water 1664B 750099
Eurofins Savannah
Page 11 of 17 11/14/2022

Lab Chronicle
Client: Environmental Conservation Laboratories Job ID: 680-224611-1
Project/Site: CF05510
Client Sample ID: Outfall 1 Lab Sample ID: 680-224611-1
Date Collected: 11/01/22 06:15 Matrix: Water
Date Received: 11/04/22 08:20
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Prep 1664B 218 mL 500 mL 750099 11/11/22 07:25 KD EET SAV
Total/NA Analysis 1664B 1 750134 11/11/22 09:18 KD EET SAV
Instrument ID: NoEquip
Client Sample ID: Outfall 2 Lab Sample ID: 680-224611-2
Date Collected: 11/01/22 06:25 Matrix: Water 8
Date Received: 11/04/22 08:20
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Prep 1664B 235 mL 500 mL 750099 11/11/22 07:25 KD EET SAV
Total/NA Analysis 1664B 1 750134 11/11/22 09:18 KD EET SAV
Instrument ID: NoEquip
Client Sample ID: Outfall 3 Lab Sample ID: 680-224611-3
Date Collected: 11/01/22 06:32 Matrix: Water
Date Received: 11/04/22 08:20
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Prep 1664B 202 mL 500 mL 750099 11/11/22 07:25 KD EET SAV
Total/NA Analysis 1664B 1 750134 11/11/22 09:18 KD EET SAV
Instrument ID: NoEquip
Laboratory References:
EET SAV=Eurofins Savannah,5102 LaRoche Avenue,Savannah,GA 31404,TEL[phone]
Eurofins Savannah
Page 12 of 17 11/14/2022

:11,
.---FALs proy_o4d-
•z SUBCONTRACT ORDER
• ENCO Cary p ,(`J`���y/-�e
680-224611 COC CF05510 I`-
SENDING LABORATORY: RECEIVING LABORATORY:
ENCO Cary Test America(GA)
102-A Woodwinds Industrial Court 5102 LaRoche Avenue
Cary,NC 27511 Savannah,GA 31404
Phone: [phone] Phone:[phone]
Fax: [phone] Fax: -0
Project Manager: Shahla Vakili Project State of Origin: North Carolina
Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments
Outfall 1 Water 01-Nov-22 06:15
Analysis Due Expires Analysis Comments 9
O&G 1664B 11-Nov-22 15:00 29-Nov-22 06:15 l !'
Containers Supplied:
250mLA+H2SO4(B) 250mLA+142SO4(C)
Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments
Outfall 2 Water 01-Nov-22 06:25
Analysis Due Expires: Analysis Comments
O&G 1664B 11-Nov-22 15:00 29-Nov-22 06:25
Containers Supplied:
250mLA+H2SO4(B) 250mLA+H2SO4(C)
Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments
Outfall 3 Water 01-Nov-22 06:32
Analysis Due Expires Analysis Comments
O&G 1664B I I-Nov-22 15:00 29-Nov-22 06:32
Containers Supplied:
250mLA+F12SO4(B) 250mLA+H2SO4(C)
I i/ --/ -0-- 1 o
AftuN'a-t-taf 0---6LI--e-L,
Released Date Ry
rved y Date
Released By Date Received B) , Date I
Page I of I
Page 13 of 17 11/14/2022

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Page 14 of 17 11/14/2022

JpPreservation 'eri Verification ;
4 , , � •
ENG() C,,ry t;
Work Order: CF05510 Project: Stormwater
Client: MOODY DUNBAR FOODS(M0008) Project#: Standard
Logged In: 02-Nov-22 15:19U Logged By: Samantha L Hy tt
Preservation Check Performed By: � Date/Time: 1 t 1 -1 . t 4._(( :[.
..; a
CF05510-01
Cant. T e rip*(pH) 7p1-1 Checked/ Date/Time
Ya? ptAdjustl Reagent UsICamments
Regiitt ment In Central Adjusted
B 25OmLA+H2SO4 <2 Y I N / A Y I N / A' ; 8
Ali i
C 250mLA+H2SO4 <2 YIN / NA YIN N
D 250mLP+H2SO4 <2 (IejN / NA Y (1:1)f NA
i
CF05510-02
Pies(pH) PH O ed/ Date/Time
Cott`Type , ,. Requirement 1n Ci�r tr'Qt_,, pH Adjust -.. Adjusted Reagent U ed/Cotnmenfs
B 250mLA+H2SO4 �Z YIN / NA ; Y / N / N
C 250mLA+H2SO4 r:2 ` / N / NA Y I N `I N
D 250mLP+H2SO4 2 Y N I NA Y /rN / NA 1
CF05510-03
Cent Type Prey(pH) :PH Ch.,.ecked/ , . e -1
R irrttent In ntre], pH A�tj( t Reagent Used/Comments
Aa c J
B 250mLA+H2SO4 <2 Y / N I (NA ` Y I N / NA
C 250mLA+H2SO4 <2 Y I N / A\S Y / N /
1
D 250mLP+H2SO4 <2 \Y I N / NA Y / N /)NA
Reagent Name ID Reagent Name ID Reagent Name ID
1 3 5 �
2 4 6 -
PH Strip ID: A
C;\EL.MNT1Print\wko_PreservationCheck.rpt Page i i,;
Page 15 of 17 11/14/2022

Login Sample Receipt Checklist
Client: Environmental Conservation Laboratories Job Number:680-224611-1
Login Number: 224611 List Source: Eurofins Savannah
List Number: 1
Creator: Yonish, Rachel
Question Answer Comment
Radioactivity wasn't checked or is</=background as measured by a survey N/A
meter.
The cooler's custody seal, if present, is intact. True
Sample custody seals, if present, are intact. True
The cooler or samples do not appear to have been compromised or True
tampered with.
Samples were received on ice. True
Cooler Temperature is acceptable. True 10
Cooler Temperature is recorded. True
COC is present. True
COC is filled out in ink and legible. True
COC is filled out with all pertinent information. True
Is the Field Sampler's name present on COC? True
There are no discrepancies between the containers received and the COC. True
Samples are received within Holding Time(excluding tests with immediate True
HTs)
Sample containers have legible labels. True
Containers are not broken or leaking. True
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. True
There is sufficient vol.for all requested analyses, incl. any requested True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is True
<6mm (1/4").
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. N/A
Eurofins Savannah
Page 16 of 17 11/14/2022

Accreditation/Certification Summary
Client: Environmental Conservation Laboratories Job ID: 680-224611-1
Project/Site: CF05510
Laboratory: Eurofins Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina(WW/SW) State 269 12-31-22
m
Eurofins Savannah
Page 17 of 17 11/14/2022