WQ0002503_Monitoring - 03-2023_20230428

Monitoring Report Submittal
Permit Number#*
Name of Facility:*
Month: * March
Report Information
Type *
GW-59
WQ0002503
FRIT CAR, INC.
Confirmation Email Address: * [e-mail]
Name of Submitter: * Connie Pettis
Signature:
Year:* 2023
Upload Document*
GW59 MARCH.pdf
PDF Only
3.16MB
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
Date of submittal: 4/28/2023
This will be filled in automatically
Initial Review
Reviewer: Wanda.Gerald

Is the project number correct?* WQ0002503
Is the monitoring report accepted?* Yes No
Regional Office* Washington
Reviewer: _anonymous
Review Date: 6/1/2023

GW-59A COMPLIANCE REPORT FORM Permit # WQ0002503
(Submit one each monitoring period with G W-59forms.)
I
Enter date monitoring results were due. 4/30/2023 Will this monitoring report(GIN-59 and GW-59A
YES
NO
be submitted after the established due date?
X
2
Was any required information missing on the GW-59 report forms?
ES
NO
IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s)
and explain the problems encountered in obtaining the required information.
SfAMpLE RE5UL-fS WERE tJOT c3i'PtINFD FOR MW-1., -rlte'y
N ERE NOT S 6NT To Ttt C \,.J G 1 N FENRO(z.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc.)? If the answer is "Yes ", contact the Regional Office for guidance.
X
4
Are any monitored constituents equal to or above the established standards?
S
NO
If the answer to question 4 is "NO", skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below:
--, ►v1N-5, Mw - to, Mw-7 iRoN 010H5
MAN-1 TDfLILDISSaLvet> S0LlD5 -10300
5
For the constituents identified in question 4 above, have standards been exceeded previously for
YES
NO
the same constituent(s) in the same well(s) in the last two years?
y
If the answer to question 5 is "NO", skip to section 8.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE
REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be
improperly located, contact the Regional Office.
7
Is the permittee implementing previously approved actions required by the Division involving
YES
NO
this groundwater quality problem?
x
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility, Failure to do so may subject the permittee to a Notice of Violation
fines, and/or penalties.
NO EFFLUENT }{kS BEEN A,9P -11Ep TO THE rkE�Z SiNCC
�B. 201"1
g
The person completing this portion (GW-59A) of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby V.,tknowledge that the above information was evaluated, and the information submitted in
this rep Compliance Report GW-59A) is true and complete to the best of my knowledge.
I __— +) Za 123
Signa re of Pe horized Agent) Date
GW-59A 12/8/2003

SUBMIT FORM ON YELLOW PAPER ONLY
• .
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
• • •
•
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 2/28/2029
Facility Name: FRIT CAR, INC.
Non -Discharge UIC
Permit Name (if different): SAME AS ABOVE
NPDES WQ0002503 Other
Facility Address: 2012 HIGHWAY 17 NORTH
TYPE OF PERMITTED OPERATION BEING MONITORED
BRIDGETON "" NC 28519 CountyCRAVEN
El Lagoon El Remediation: Infiltration Gallery
(Zip)
❑■ Spray Field ❑ Remediation:
Contact Person: MICHAEL NEWBY
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: FRIT CAR SPRAYFIELD
No. of wells to be sampled: 4
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-1
Date sample collected: 3/29/2023
FIELD ANALYSES:
WAS
Well Depth: 15.65 ft.
Well Diameter: 2 in.
pH 00400: units Temp. 00010: 16 °C
DRY at
Depth to Water Level 82546: 8.23 ft. below measuring point Screened Interval: ft. to
ft.
Spec. Cond. 00094: µ Mhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 3.56
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: 0 YES
❑ NO and field acidified: 0 YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: PACE ANALYTICAL
Certification No. EnV375
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L
Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 mg/L
Al - Aluminum 01105
mg/L
Note: Well Sample was not submitted to the lab in error.
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 00680 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑■ Yes (1) ❑ No (0)
Specific Conductance 00095 FtMhos
K - Potassium 00937
mg/L
VOC 7873 method #
Total Ammonia 00610 mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
method #
TKN as N 00625 mg/L
Ni - Nickel 01067
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Michael Newby, Senior Vice President
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev.06-07-2018

SUBMIT FORM ON YELLOW PAPER ONLY
• .
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
• • •
•
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 2/28/2029
Facility Name: FRIT CAR, INC.
Non -Discharge UIC
Permit Name (if different): SAME AS ABOVE
NPDES WQ0002503 Other
Facility Address: 2012 HIGHWAY 17 NORTH
TYPE OF PERMITTED OPERATION BEING MONITORED
BRIDGETON "" NC 28519 CountyCRAVEN
El Lagoon El Remediation: Infiltration Gallery
(Zip)
❑■ Spray Field ❑ Remediation:
Contact Person: MICHAEL NEWBY
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: FRIT CAR SPRAYFIELD
No. of wells to be sampled: 4
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-5
Date sample collected: 3/29/2023
FIELD ANALYSES:
WAS
Well Depth: 15.25 ft.
Well Diameter: 2 in.
pH 00400: 4.77 units Temp. 00010: 18 °C
DRY at
Depth to Water Level 82546:4.3 ft. below measuring point Screened Interval: ft. to
ft.
Spec. Cond. 00094: µ Mhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: NONE
check
Volume of water pumped/bailed before sampling: 5.22
gallons
Appearance CLEAR
here:❑
Samples for metals were collected unfiltered: ❑ YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 4/4/2023
Laboratory Name: PACE ANALYTICAL
Certification No. EnV375
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L
Pb -Lead o1o51 <2.0 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620 <• 10
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665 <0•1
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 703oo 75 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 0068o 3.24 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 14.2 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034 <2.0
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042 <.005
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 513
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 19.3 mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑■ Yes (1) ❑ No (0)
Specific Conductance 00095 FtMhos
K - Potassium 00937
mg/L
VOC 7873 method #
Total Ammonia 00610 <.25 mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
method #
TKN as N 00625 mg/L
Ni - Nickel 01067 2.62
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Michael Newby, Senior Vice President
Permittee (or Authorized Aqent) Name and Title - Please print or type
Signaturle of Permittee (or Autho
4/28/2023
(Date)
GW-59 Rev.06-07-2018

SUBMIT FORM ON YELLOW PAPER ONLY
• .
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
• • •
•
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 2/28/2029
Facility Name: FRIT CAR, INC.
Non -Discharge UIC
Permit Name (if different): SAME AS ABOVE
NPDES WQ0002503 Other
Facility Address: 2012 HIGHWAY 17 NORTH
TYPE OF PERMITTED OPERATION BEING MONITORED
BRIDGETON "" NC 28519 CountyCRAVEN
El Lagoon ❑Remediation: Infiltration Gallery
(Zip)
❑■ Spray Field ❑ Remediation:
Contact Person: MICHAEL NEWBY
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: FRIT CAR SPRAYFIELD
No. of wells to be sampled: 4
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-6
Date sample collected: 3/29/2023
FIELD ANALYSES:
WAS
Well Depth: 19.68 ft.
Well Diameter: 2 in.
pH 00400: 4.7 units Temp. 00010: 15.8 °C
DRY at
Depth to Water Level 82546: 8.75 ft. below measuring point Screened Interval: ft. to
ft.
Spec. Cond. 00094: µ Mhos
time of
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: NONE
sampling,
check
Volume of water pumped/bailed before sampling: 4.44
gallons
Appearance CLEAR
here:❑
Samples for metals were collected unfiltered: ❑ YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 4/4/2023
Laboratory Name: PACE ANALYTICAL
Certification No. EnV375
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L
Pb -Lead o1o51 <2.0 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620 <• 10
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665 <• 10
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 703oo 54 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 00680 1.62 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 12.6 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034 <2.0
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042 <.005
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 381
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 8.98 mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑■ Yes (1) ❑ No (0)
Specific Conductance 00095 FtMhos
K - Potassium 00937
mg/L
VOC 7873 method #
Total Ammonia 00610 <.25 mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
method #
TKN as N 00625 mg/L
Ni - Nickel 01067 <2.0
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: i Effluent Total VOCs: mg/L VOC Removall%
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, anrj teat the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibili.y of fines and imprisonment for knowing violations.
I
— : 1
Newby,
Michael ••-
AuthorizedPermittee (or - . - . D.
GW-59 Rev.06-07-2018

SUBMIT FORM ON YELLOW PAPER ONLY
• .
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
• • •
•
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 2/28/2029
Facility Name: FRIT CAR, INC.
Non -Discharge UIC
Permit Name (if different): SAME AS ABOVE
NPDES WQ0002503 Other
Facility Address: 2012 HIGHWAY 17 NORTH
TYPE OF PERMITTED OPERATION BEING MONITORED
BRIDGETON "" NC 28519 CountyCRAVEN
El Lagoon El Remediation: Infiltration Gallery
(Zip)
❑■ Spray Field ❑ Remediation:
Contact Person: MICHAEL NEWBY
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: FRIT CAR SPRAYFIELD
No. of wells to be sampled: 4
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-7
Date sample collected: 3/29/2023
FIELD ANALYSES:
WAS
Well Depth: 16.18 ft.
Well Diameter: 2 in.
pH 00400: 4.0 units Temp. 00010: 16 °C
DRY at
Depth to Water Level 82546: 8.75 ft. below measuring point Screened Interval: ft. to
ft.
Spec. Cond. 00094: µ Mhos
time of
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: NONE
sampling,
check
Volume of water pumped/bailed before sampling: 5.16
gallons
Appearance CLEAR
here:❑
Samples for metals were collected unfiltered: ❑ YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 4/4/2023
Laboratory Name: PACE ANALYTICAL
Certification No. EnV375
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L
Pb -Lead o1o51 <2.0 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620 <0.1
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665 <0•1
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 1130 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 0068o 8.62 mg/L
Ca - Calcium 00916
mg/L
Chloride 0094o 86.6 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034 <2.0
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042 <.005
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 1660
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 63.1 mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑■ Yes (1) ❑ No (0)
Specific Conductance 00095 FtMhos
K - Potassium 00937
mg/L
VOC 7873 method #
Total Ammonia 00610 <.25 mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
method #
TKN as N 00625 mg/L
Ni - Nickel 01067 •00308
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L A Effluent Total VOCs: mg/L VOC Removal%
Michael Newby, Senior Vice President
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev.06-07-2018

PaceAnalytical
ANALYTICAL REPORT
April 11, 2023
F � e0000-
Frit Car Inc.
Sample Delivery Group: L1600164
Samples Received: 03/31/2023
Project Number:
Description:
Report To: Connie Pettis
2012 US Hwy 17N
New Bern, NC 28560
Entire Report Reviewed By: 4�41
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ,
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
11 r
i
I
M
FSS
Rn
Rr
FQc
E
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1600164 04/11/23 17:42 1 of 30

TABLE OF CONTENTS
Cp: Cover Page
1
FP1
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
FSS
WELL #7 L1600164-01
5
rqn
WELL #6 L1600164-02
8
WELL #5 L1600164-03
11
Fr]
Qc: Quality Control Summary
14
Gravimetric Analysis by Method 2540 C-2011
14
FQ Cl
Wet Chemistry by Method 350.1
15
GI
Wet Chemistry by Method 365.4
16
Wet Chemistry by Method 9056A
17
rAl
Wet Chemistry by Method 9060A
19
Metals (ICPMS) by Method 6020B
20
FC
Volatile Organic Compounds (GC/MS) by Method 8260D
24
GI: Glossary of Terms
28
Al: Accreditations & Locations
29
Sc: Sample Chain of Custody
30
ACCOUNT: PROJECT: SDG:
DATE/TIME:
PAGE:
Frit Car Inc. L1600164
04/11/23 17:42
2 of 30

WELL #7 L1600164-01 GW
Method
SAMPLE SUMMARY
Collected by
KAZDAN
Batch
Gravimetric Analysis by Method 2540 C-2011
WG2034730
Wet Chemistry by Method 350.1
WG2034193
Wet Chemistry by Method 365.4
WG2036422
Wet Chemistry by Method 9056A
WG2033523
Wet Chemistry by Method 9060A
WG2034273
Metals (ICPMS) by Method 6020B
WG2034072
Metals (ICPMS) by Method 6020B
WG2034085
Volatile Organic Compounds (GC/MS) by Method 8260D
WG2035064
WELL #6 L1600164-02 GW
Collected date/time Received date/time
03/30/2312:30 03/31/2310:00
Dilution Preparation
Analysis
Analyst
Location
date/time
date/time
1 04/04/23 09:26
04/04/2316:48
AS
Mt. Juliet, TN
1 04/02/23 00:39
04/02/23 00:39
AEC
Mt. Juliet, TN
1 04/04/23 08:31
04/05/2319:22
UNP
Mt. Juliet, TN
1 03/31/2317:31
03/31/2317:31
GEB
Mt. Juliet, TN
1 04/03/2318:07
04/03/2318:07
LOH
Mt. Juliet, TN
1 04/04/2310:33
04/04/2315:25
JPD
Mt. Juliet, TN
1 04/02/2312:10
04/03/2310:49
SJM
Mt. Juliet, TN
1 04/04/2311:40
04/04/2311:40
JCP
Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
KAZDAN
03/30/2313:50
03/31/2310:00
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
date/time
date/time
Gravimetric Analysis by Method 2540 C-2011
WG2034730
1 04/04/23 09:26
04/04/2316:48
AS
Mt. Juliet, TN
Wet Chemistry by Method 350.1
WG2034193
1 04/02/23 00:01
04/02/23 00:01
AEC
Mt. Juliet, TN
Wet Chemistry by Method 365.4
WG2036422
1 04/04/23 08:31
04/05/2319:24
UNP
Mt. Juliet, TN
Wet Chemistry by Method 9056A
WG2033523
1 03/31/2317:45
03/31/2317:45
GEB
Mt. Juliet, TN
Wet Chemistry by Method 9060A
WG2034273
1 04/03/2318:41
04/03/2318:41
LOH
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG2039132
1 04/10/2310:58
04/10/2313:51
SJM
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG2039135
1 04/10/2310:57
04/10/2314:11
SJM
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG2035064
1 04/04/2312:02
04/04/2312:02
JCP
Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
WELL #5 L1600164-03 GW
KAZDAN
03/30/2315:18
03/31/2310:00
Method
Batch
Dilution Preparation
date/time
Analysis
date/time
Analyst
Location
Gravimetric Analysis by Method 2540 C-2011
WG2034730
1 04/04/23 09:26
04/04/2316:48
AS
Mt. Juliet, TN
Wet Chemistry by Method 350.1
WG2034193
1 04/02/23 00:02
04/02/23 00:02
AEC
Mt. Juliet, TN
Wet Chemistry by Method 365.4
WG2036422
1 04/04/23 08:31
04/05/2319:25
UNP
Mt. Juliet, TN
Wet Chemistry by Method 9056A
WG2033523
1 03/3112318:25
03/31/2318:25
GEB
Mt. Juliet, TN
Wet Chemistry by Method 9060A
WG2034273
1 04/03/2318:59
04/03/2318:59
LOH
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG2034072
1 04/04/2310:33
04/04/2315:32
JPD
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG2034085
1 04/02/2312:10
04/03/2311:02
SJM
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG2035064
1 04/0412312:27
04/04/2312:27
JCP
Mt. Juliet, TN
FP1
FTC
M
Fqn
Fr]
PC]
I q,
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1600164 04/11/23 17:42 3 of 30

CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
Heather J Wagner
Project Manager
FP1
FTC
FSS
Fr]
1qC
I q,
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME:
Frit Car Inc. L1600164 04/11/23 17:42
PAGE:
4 of 30

gm
WELL #7 SAMPLE RESULTS - 01
Collected date/time: 03/30/23 12:30 L1600164
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier RDL
Analyte ug/I ug/I
Dissolved Solids 1130000 20000
Wet Chemistry by Method 350.1
Result Qualifier
RDL
Analyte ug/I
ug/I
Ammonia Nitrogen ND
250
Wet Chemistry by Method 365.4
Result Qualifier
RDL
Analyte ug/I
ug/I
Phosphorus,Total ND
100
Wet Chemistry by Method 9056A
Analyte
Result
ug/I
Chloride 86600
Nitrate as (N) ND
Sulfate 63100
Wet Chemistry by Method 9060A
Qualifier RDL
ug/I
1000
100
5000
Result Qualifier RDL
Analyte ug/I ug/I
TOC (Total Organic Carbon) 8620 1000
Metals (ICPMS) by Method 6020B
Dilution Analysis Batch
date / time
1 04/04/202316:48 WG2034730
Dilution Analysis Batch
date / time
1 04/02/2023 00:39 WG2034193
Dilution Analysis Batch
date / time
1 04/05/202319:22 WG2036422
Dilution Analysis
date / time
03/31/202317:31
03/31/202317:31
03/31/202317:31
Batch
WG2033523
WG2033523
WG2033523
Dilution Analysis Batch
date / time
1 04/03/202318:07 WG2034273
Result
Qualifier RDL Dilution
Analysis
Batch
Analyte
ug/I
ug/I
date / time
Chromium
ND
2.00 1
04/03/202310:49
WG2034085
Chromium,Dissolved
ND
2.00 1
04/04/202315:25
WG2034072
Copper
ND
5.00 1
04/03/202310:49
WG2034085
Copper,Dissolved
ND
5.00 1
04/04/202315:25
WG2034072
Iron
1660
100 1
04/03/202310:49
WG2034085
Iron,Dissolved
358
100 1
04/04/202315:25
WG2034072
Lead
ND
2.00 1
04/03/202310:49
WG2034085
Lead,Dissolved
ND
2.00 1
04/04/202315:25
WG2034072
Nickel
3.08
2.00 1
04/03/202310:49
WG2034085
Nickel,Dissolved
3.42
2.00 1
04/04/202315:25
WG2034072
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
date / time
Acetone
ND
50.0
1 04/04/202311:40
WG2035064
Acrolein
ND
C3
50.0
1 04/04/202311:40
WG2035064
Acrylonitrile
ND
10.0
1 04/04/202311:40
WG2035064
Benzene
ND
1.00
1 04/04/202311:40
WG2035064
Bromobenzene
ND
1.00
1 04/04/202311:40
WG2035064
Bromodichloromethane
ND
1.00
1 04/04/202311:40
WG2035064
Bromoform
ND
C3
1.00
1 04/04/202311:40
WG2035064
Bromomethane
ND
C3
5.00
1 04/04/202311:40
WG2035064
n-Butylbenzene
ND
1.00
1 04/04/202311:40
WG2035064
sec -Butyl benzene
ND
1.00
1 04/04/202311:40
WG2035064
ter[-Butylbenzene
ND
1.00
1 04/04/202311:40
WG2035064
Carbon tetrachloride
ND
1.00
1 04/04/202311:40
WG2035064
ACCOUNT:
PROJECT: SDG:
Frit Car Inc.
L1600164
FP1
FTc
FSS
rqn
N
Fqc
I ql
FAI
FSC
DATE/TIME: PAGE:
04/11/23 17:42 5 of 30

WELL #7 SAMPLE
Collected date/time: 03/30/23 12:30
Volatile Organic Compounds (GC/MS) by Method 8260D
RESULTS - 01
L1600164
Result
Qualifier
RDL Dilution Analysis
Batch
FP1
Analyte
ug/I
ug/I
date / time
Chlorobenzene
ND
1.00 1
04/04/202311:40
WG2035064
z
Tc
Chlorodibromomethane
ND
1.00 1
04/04/202311:40
WG2035064
Chloroethane
ND
5.00 1
04/04/202311:40
WG2035064
Chloroform
ND
5.00 1
04/04/202311:40
WG2035064
FSS
Chloromethane
ND
2.50 1
04/04/202311:40
WG2035064
2-Chlorotoluene
ND
1.00 1
04/04/202311:40
WG2035064
Fqn
4-Chlorotoluene
ND
1.00 1
04/04/202311:40
WG2035064
1,2-Dibromo-3-Chloropropane
ND
5.00 1
04/04/202311:40
WG2035064
1,2-Dibromoethane
ND
1.00 1
04/04/202311:40
WG2035064
Dibromomethane
ND
1.00 1
04/04/202311:40
WG2035064
1,2-Dichlorobenzene
ND
1.00 1
04/04/202311:40
WG2035064
6
QC
1,3-Dichlorobenzene
ND
1.00 1
04/04/202311:40
WG2035064
1,4-Dichlorobenzene
ND
1.00 1
04/04/202311:40
WG2035064
Dichlorodifluoromethane
ND
5.00 1
04/04/202311:40
WG2035064
GI
1,1-Dichloroethane
ND
1.00 1
04/04/202311:40
WG2035064
1,2-Dichloroethane
ND
1.00 1
04/04/202311:40
WG2035064
FAI
1,1-Dichloroethene
ND
1.00 1
04/04/202311:40
WG2035064
cis-1,2-Dichloroethene
ND
1.00 1
04/04/202311:40
WG2035064
trans-1,2-Dichloroethene
ND
1.00 1
04/04/202311:40
WG2035064
FSC
1,2-Dichloropropane
ND
1.00 1
04/04/202311:40
WG2035064
1,1-Dichloropropene
ND
1.00 1
04/04/202311:40
WG2035064
1,3-Dichloropropane
ND
1.00 1
04/04/202311:40
WG2035064
cis-1,3-Dichloropropene
ND
1.00 1
04/04/202311:40
WG2035064
trans-1,3-Dichloropropene
ND
1.00 1
04/04/202311:40
WG2035064
2,2-Dichloropropane
ND
1.00 1
04/04/202311:40
WG2035064
Di -isopropyl ether
ND
1.00 1
04/04/202311:40
WG2035064
Ethylbenzene
ND
1.00 1
04/04/202311:40
WG2035064
Hexachloro-1,3-butadiene
ND
1.00 1
04/04/202311:40
WG2035064
Isopropylbenzene
ND
1.00 1
04/04/202311:40
WG2035064
p-Isopropyltoluene
ND
1.00 1
04/04/202311:40
WG2035064
2-Butanone (MEK)
ND
10.0 1
04/04/202311:40
WG2035064
Methylene Chloride
ND
5.00 1
04/04/202311:40
WG2035064
4-Methyl-2-pentanone (MIBK)
ND
10.0 1
04/04/202311:40
WG2035064
Methyl tert-butyl ether
ND
1.00 1
04/04/202311:40
WG2035064
Naphthalene
ND
C3
5.00 1
04/04/202311:40
WG2035064
n-Propylbenzene
ND
1.00 1
04/04/202311:40
WG2035064
Styrene
ND
1.00 1
04/04/202311:40
WG2035064
1,1,1,2-Tetrachloroethane
ND
1.00 1
04/04/202311:40
WG2035064
1,1,2,2-Tetrachloroethane
ND
1.00 1
04/04/202311:40
WG2035064
1,1,2-Trichlorotrifluoroethane
ND
1.00 1
04/04/202311:40
WG2035064
Tetrachloroethene
ND
1.00 1
04/04/202311:40
WG2035064
Toluene
ND
1.00 1
04/04/202311:40
WG2035064
1,2,3-Trichlorobenzene
ND
1.00 1
04/04/202311:40
WG2035064
1,2,4-Trichlorobenzene
ND
C3
1.00 1
04/04/202311:40
WG2035064
1,1,1-Trichloroethane
ND
1.00 1
04/04/202311:40
WG2035064
1,1,2-Trichloroethane
ND
1.00 1
04/04/202311:40
WG2035064
Trichloroethene
ND
1.00 1
04/04/202311:40
WG2035064
Trichlorofluoromethane
ND
C3
5.00 1
04/04/202311:40
WG2035064
1,2,3-Trichloropropane
ND
2.50 1
04/04/202311:40
WG2035064
1,2,4-Trimethylbenzene
ND
1.00 1
04/04/202311:40
WG2035064
1,2,3-Trimethyl benzene
ND
1.00 1
04/04/202311:40
WG2035064
1,3,5-Trimethyl benzene
ND
1.00 1
04/04/202311:40
WG2035064
Vinyl chloride
ND
1.00 1
04/04/202311:40
WG2035064
Xylenes, Total
ND
3.00 1
04/04/202311:40
WG2035064
(S) Toluene-d8
106
80.0-120
041041202311.40
WG2035064
(S) 4-Bromof/uorobenzene
96.1
77.0-126
041041202311.40
WG2035064
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Frit Car Inc.
L1600164
04/11/23 17:42
6 of 30

WELL #7 SAMPLE RESULTS - 01
Collected date/time: 03/30/23 12:30 L1600164
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Analyte ug/I
(S 1,2-Dich/oroethane-d4 101
Qualifier RDL Dilution Analysis Batch
ug/I date / time
70.0-130 041041202311.40 WG2035064
FP1
FTc
FSS
Fqn
N
FC]
I ql
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1600164 04/11/23 17:42 7 of 30

WELL #6 SAMPLE RESULTS - 02
Collected date/time: 03/30/23 13:50 L1600164
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier RDL
Analyte ug/I ug/I
Dissolved Solids 54000 10000
Wet Chemistry by Method 350.1
Result Qualifier
RDL
Analyte ug/I
ug/I
Ammonia Nitrogen ND
250
Wet Chemistry by Method 365.4
Result Qualifier
RDL
Analyte ug/I
ug/I
Phosphorus,Total ND
100
Wet Chemistry by Method 9056A
Dilution Analysis Batch
date / time
1 04/04/202316:48 WG2034730
Dilution Analysis Batch
date / time
1 04/02/2023 00:01 WG2034193
Dilution Analysis Batch
date / time
1 04/05/202319:24 WG2036422
Result
Analyte _ ug/I
Chloride 12600
Nitrate as (N) ND
Sulfate 8980
Wet Chemistry by Method 9060A
Qualifier
RDL Dilution
ug/I
1000 1
100 1
5000 1
Analysis
date / time
03/31/202317:45
03/31/202317:45
03/31/202317:45
Batch
WG2033523
WG2033523
WG2033523
Result
Qualifier
RDL Dilution
Analysis
Batch
Analyte ug/I
ug/I
date / time
TOC (Total Organic Carbon) 1620
B
1000 1
04/03/202318:41
WG2034273
Metals (ICPMS) by Method 6020B
Result
Qualifier
RDL Dilution
Analysis
Batch
Analyte ug/I
ug/I
date / time
Chromium ND
2.00 1
04/10/202314:11
WG2039135
Chromium,Dissolved ND
2.00 1
04/10/202313:51
WG2039132
Copper ND
5.00 1
04/10/202314:11
WG2039135
Copper,Dissolved ND
5.00 1
04/10/202313:51
WG2039132
Iron 381
100 1
04/10/202314:11
WG2039135
Iron,Dissolved ND
100 1
04/10/202313:51
WG2039132
Lead ND
2.00 1
04/10/202314:11
WG2039135
Lead,Dissolved ND
2.00 1
04/10/202313:51
WG2039132
Nickel ND
2.00 1
04/10/202314:11
WG2039135
Nickel,Dissolved ND
2.00 1
04/10/202313:51
WG2039132
Volatile Organic Compounds (GC/MS) by Method 8260D
FP1
FTC]
FS—S
rqn
N
Fqc
I ql
rAl
FSC
Result
Qualifier
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
date / time
Acetone
ND
50.0
1 04/04/202312:02
WG2035064
Acrolein
ND
C3
50.0
1 04/04/202312:02
WG2035064
Acrylonitrile
ND
10.0
1 04/04/202312:02
WG2035064
Benzene
ND
1.00
1 04/04/202312:02
WG2035064
Bromobenzene
ND
1.00
1 04/04/202312:02
WG2035064
Bromodichloromethane
ND
1.00
1 04/04/202312:02
WG2035064
Bromoform
ND
C3
1.00
1 04/04/202312:02
WG2035064
Bromomethane
ND
C3
5.00
1 04/04/202312:02
WG2035064
n-Butylbenzene
ND
1.00
1 04/04/202312:02
WG2035064
sec -Butyl benzene
ND
1.00
1 04/04/202312:02
WG2035064
ter[-Butylbenzene
ND
1.00
1 04/04/202312:02
WG2035064
Carbon tetrachloride
ND
1.00
1 04/04/202312:02
WG2035064
ACCOUNT:
PROJECT: SDG:
DATE/TIME: PAGE:
Frit Car Inc.
L1600164
04/11/23 17:42 8 of 30

WELL #6
SAMPLE
RESULTS - 02
Collected date/time: 03/30/23 13:50
L1600164
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
RDL Dilution Analysis
Batch
FP1
Analyte
ug/I
ug/I
date / time
Chlorobenzene
ND
1.00 1
04/04/202312:02
WG2035064
z
Tc
Chlorodibromomethane
ND
1.00 1
04/04/202312:02
WG2035064
Chloroethane
ND
5.00 1
04/04/202312:02
WG2035064
Chloroform
ND
5.00 1
04/04/202312:02
WG2035064
F
Chloromethane
ND
2.50 1
04/04/202312:02
WG2035064
2-Chlorotoluene
ND
1.00 1
04/04/202312:02
WG2035064
Fqn
4-Chlorotoluene
ND
1.00 1
04/04/202312:02
WG2035064
1,2-Dibromo-3-Chloropropane
ND
5.00 1
04/04/202312:02
WG2035064
1,2-Dibromoethane
ND
1.00 1
04/04/202312:02
WG2035064
Dibromomethane
ND
1.00 1
04/04/202312:02
WG2035064
1,2-Dichlorobenzene
ND
1.00 1
04/04/202312:02
WG2035064
6
QC
1,3-Dichlorobenzene
ND
1.00 1
04/04/202312:02
WG2035064
1,4-Dichlorobenzene
ND
1.00 1
04/04/202312:02
WG2035064
Dichlorodifluoromethane
ND
5.00 1
04/04/202312:02
WG2035064
GI
1,1-Dichloroethane
ND
1.00 1
04/04/202312:02
WG2035064
1,2-Dichloroethane
ND
1.00 1
04/04/202312:02
WG2035064
FAI
1,1-Dichloroethene
ND
1.00 1
04/04/202312:02
WG2035064
cis-1,2-Dichloroethene
ND
1.00 1
04/04/202312:02
WG2035064
trans-1,2-Dichloroethene
ND
1.00 1
04/04/202312:02
WG2035064
FSC
1,2-Dichloropropane
ND
1.00 1
04/04/202312:02
WG2035064
1,1-Dichloropropene
ND
1.00 1
04/04/202312:02
WG2035064
1,3-Dichloropropane
ND
1.00 1
04/04/202312:02
WG2035064
cis-1,3-Dichloropropene
ND
1.00 1
04/04/202312:02
WG2035064
trans-1,3-Dichloropropene
ND
1.00 1
04/04/202312:02
WG2035064
2,2-Dichloropropane
ND
1.00 1
04/04/202312:02
WG2035064
Di -isopropyl ether
ND
1.00 1
04/04/202312:02
WG2035064
Ethylbenzene
ND
1.00 1
04/04/202312:02
WG2035064
Hexachloro-1,3-butadiene
ND
1.00 1
04/04/202312:02
WG2035064
Isopropylbenzene
ND
1.00 1
04/04/202312:02
WG2035064
p-Isopropyltoluene
ND
1.00 1
04/04/202312:02
WG2035064
2-Butanone (MEK)
ND
10.0 1
04/04/202312:02
WG2035064
Methylene Chloride
ND
5.00 1
04/04/202312:02
WG2035064
4-Methyl-2-pentanone (MIBK)
ND
10.0 1
04/04/202312:02
WG2035064
Methyl tert-butyl ether
ND
1.00 1
04/04/202312:02
WG2035064
Naphthalene
ND
C3
5.00 1
04/04/202312:02
WG2035064
n-Propylbenzene
ND
1.00 1
04/04/202312:02
WG2035064
Styrene
ND
1.00 1
04/04/202312:02
WG2035064
1,1,1,2-Tetrachloroethane
ND
1.00 1
04/04/202312:02
WG2035064
1,1,2,2-Tetrachloroethane
ND
1.00 1
04/04/202312:02
WG2035064
1,1,2-Trichlorotrifluoroethane
ND
1.00 1
04/04/202312:02
WG2035064
Tetrachloroethene
ND
1.00 1
04/04/202312:02
WG2035064
Toluene
ND
1.00 1
04/04/202312:02
WG2035064
1,2,3-Trichlorobenzene
ND
1.00 1
04/04/202312:02
WG2035064
1,2,4-Trichlorobenzene
ND
C3
1.00 1
04/04/202312:02
WG2035064
1,1,1-Trichloroethane
ND
1.00 1
04/04/202312:02
WG2035064
1,1,2-Trichloroethane
ND
1.00 1
04/04/202312:02
WG2035064
Trichloroethene
ND
1.00 1
04/04/202312:02
WG2035064
Trichlorofluoromethane
ND
C3
5.00 1
04/04/202312:02
WG2035064
1,2,3-Trichloropropane
ND
2.50 1
04/04/202312:02
WG2035064
1,2,4-Trimethylbenzene
ND
1.00 1
04/04/202312:02
WG2035064
1,2,3-Trimethyl benzene
ND
1.00 1
04/04/202312:02
WG2035064
1,3,5-Trimethyl benzene
ND
1.00 1
04/04/202312:02
WG2035064
Vinyl chloride
ND
1.00 1
04/04/202312:02
WG2035064
Xylenes, Total
ND
3.00 1
04/04/202312:02
WG2035064
(S) Toluene-d8
107
80.0-120
041041202312.02
WG2035064
(S) 4-Bromof/uorobenzene
98.3
77.0-126
041041202312.02
WG2035064
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Frit Car Inc.
L1600164
04/11/23 17:42
9 of 30

WELL #6 SAMPLE RESULTS - 02
Collected date/time: 03/30/23 13:50 L1600164
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Analyte ug/I
(S 1,2-Dich/oroethane-d4 101
Qualifier RDL Dilution Analysis Batch
ug/I date / time
70.0-130 041041202312.02 WG2035064
FP1
FTc
FSS
Fqn
N
FC]
I ql
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1600164 04/11/23 17:42 10 of 30

WELL #5 SAMPLE RESULTS - 03
Collected date/time: 03/30/23 15:18 L1600164
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier RDL
Analyte ug/I ug/I
Dissolved Solids 75000 10000
Wet Chemistry by Method 350.1
Result Qualifier
RDL
Analyte ug/I
ug/I
Ammonia Nitrogen ND
250
Wet Chemistry by Method 365.4
Result Qualifier
RDL
Analyte ug/I
ug/I
Phosphorus,Total ND
100
Wet Chemistry by Method 9056A
Dilution Analysis Batch
date / time
1 04/04/202316:48 WG2034730
Dilution Analysis Batch
date / time
1 04/02/2023 00:02 WG2034193
Dilution Analysis Batch
date / time
1 04/05/202319:25 WG2036422
Result Qualifier
RDL
Dilution Analysis
Batch
Analyte _ ug/I
ug/I
date / time
Chloride 14200
1000
1 03/31/202318:25
WG2033523
Nitrate as (N) ND
100
1 03/31/202318:25
WG2033523
Sulfate 19300
5000
1 03/31/202318:25
WG2033523
Wet Chemistry by Method 9060A
Result Qualifier
RDL
Dilution Analysis
Batch
Analyte ug/I
ug/I
date / time
TOC (Total Organic Carbon) 3240
1000
1 04/03/202318:59
WG2034273
Metals (ICPMS) by Method 6020B
Result
Qualifier RDL Dilution
Analysis
Batch
Analyte
ug/I
ug/I
date / time
Chromium
ND
2.00 1
04/03/202311:02
WG2034085
Chromium,Dissolved
ND
2.00 1
04/04/202315:32
WG2034072
Copper
ND
5.00 1
04/03/202311:02
WG2034085
Copper,Dissolved
ND
5.00 1
04/04/202315:32
WG2034072
Iron
513
100 1
04/03/202311:02
WG2034085
Iron,Dissolved
ND
100 1
04/04/202315:32
WG2034072
Lead
ND
2.00 1
04/03/202311:02
WG2034085
Lead,Dissolved
ND
2.00 1
04/04/202315:32
WG2034072
Nickel
2.62
2.00 1
04/03/202311:02
WG2034085
Nickel,Dissolved
2.79
2.00 1
04/04/202315:32
WG2034072
Volatile Organic Compounds (GC/MS) by Method 8260D
FP1
FTC]
FS—S
rqn
Fqc
I ql
rAl
FSC
Result
Qualifier
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
date / time
Acetone
ND
50.0
1 04/04/202312:27
WG2035064
Acrolein
ND
C3
50.0
1 04/04/202312:27
WG2035064
Acrylonitrile
ND
10.0
1 04/04/202312:27
WG2035064
Benzene
ND
1.00
1 04/04/202312:27
WG2035064
Bromobenzene
ND
1.00
1 04/04/202312:27
WG2035064
Bromodichloromethane
ND
1.00
1 04/04/202312:27
WG2035064
Bromoform
ND
C3
1.00
1 04/04/202312:27
WG2035064
Bromomethane
ND
C3
5.00
1 04/04/202312:27
WG2035064
n-Butylbenzene
ND
1.00
1 04/04/202312:27
WG2035064
sec -Butyl benzene
ND
1.00
1 04/04/202312:27
WG2035064
ter[-Butylbenzene
ND
1.00
1 04/04/202312:27
WG2035064
Carbon tetrachloride
ND
1.00
1 04/04/202312:27
WG2035064
ACCOUNT:
PROJECT: SDG:
DATE/TIME: PAGE:
Frit Car Inc.
L1600164
04/11/23 17:42 11 of 30

WELL #5 SAMPLE
Collected date/time: 03/30/23 15:18
Volatile Organic Compounds (GC/MS) by Method 8260D
RESULTS - 03
L1600164
Result
Qualifier
RDL Dilution Analysis
Batch
FP1
Analyte
ug/I
ug/I
date / time
Chlorobenzene
ND
1.00 1
04/04/202312:27
WG2035064
z
Tc
Chlorodibromomethane
ND
1.00 1
04/04/202312:27
WG2035064
Chloroethane
ND
5.00 1
04/04/202312:27
WG2035064
Chloroform
ND
5.00 1
04/04/202312:27
WG2035064
F
Chloromethane
ND
2.50 1
04/04/202312:27
WG2035064
2-Chlorotoluene
ND
1.00 1
04/04/202312:27
WG2035064
Fqn
4-Chlorotoluene
ND
1.00 1
04/04/202312:27
WG2035064
1,2-Dibromo-3-Chloropropane
ND
5.00 1
04/04/202312:27
WG2035064
1,2-Dibromoethane
ND
1.00 1
04/04/202312:27
WG2035064
Dibromomethane
ND
1.00 1
04/04/202312:27
WG2035064
1,2-Dichlorobenzene
ND
1.00 1
04/04/202312:27
WG2035064
6
QC
1,3-Dichlorobenzene
ND
1.00 1
04/04/202312:27
WG2035064
1,4-Dichlorobenzene
ND
1.00 1
04/04/202312:27
WG2035064
Dichlorodifluoromethane
ND
5.00 1
04/04/202312:27
WG2035064
GI
1,1-Dichloroethane
ND
1.00 1
04/04/202312:27
WG2035064
1,2-Dichloroethane
ND
1.00 1
04/04/202312:27
WG2035064
FAI
1,1-Dichloroethene
ND
1.00 1
04/04/202312:27
WG2035064
cis-1,2-Dichloroethene
ND
1.00 1
04/04/202312:27
WG2035064
trans-1,2-Dichloroethene
ND
1.00 1
04/04/202312:27
WG2035064
FSC
1,2-Dichloropropane
ND
1.00 1
04/04/202312:27
WG2035064
1,1-Dichloropropene
ND
1.00 1
04/04/202312:27
WG2035064
1,3-Dichloropropane
ND
1.00 1
04/04/202312:27
WG2035064
cis-1,3-Dichloropropene
ND
1.00 1
04/04/202312:27
WG2035064
trans-1,3-Dichloropropene
ND
1.00 1
04/04/202312:27
WG2035064
2,2-Dichloropropane
ND
1.00 1
04/04/202312:27
WG2035064
Di -isopropyl ether
ND
1.00 1
04/04/202312:27
WG2035064
Ethylbenzene
ND
1.00 1
04/04/202312:27
WG2035064
Hexachloro-1,3-butadiene
ND
1.00 1
04/04/202312:27
WG2035064
Isopropylbenzene
ND
1.00 1
04/04/202312:27
WG2035064
p-Isopropyltoluene
ND
1.00 1
04/04/202312:27
WG2035064
2-Butanone (MEK)
ND
10.0 1
04/04/202312:27
WG2035064
Methylene Chloride
ND
5.00 1
04/04/202312:27
WG2035064
4-Methyl-2-pentanone (MIBK)
ND
10.0 1
04/04/202312:27
WG2035064
Methyl tert-butyl ether
ND
1.00 1
04/04/202312:27
WG2035064
Naphthalene
ND
C3
5.00 1
04/04/202312:27
WG2035064
n-Propylbenzene
ND
1.00 1
04/04/202312:27
WG2035064
Styrene
ND
1.00 1
04/04/202312:27
WG2035064
1,1,1,2-Tetrachloroethane
ND
1.00 1
04/04/202312:27
WG2035064
1,1,2,2-Tetrachloroethane
ND
1.00 1
04/04/202312:27
WG2035064
1,1,2-Trichlorotrifluoroethane
ND
1.00 1
04/04/202312:27
WG2035064
Tetrachloroethene
ND
1.00 1
04/04/202312:27
WG2035064
Toluene
ND
1.00 1
04/04/202312:27
WG2035064
1,2,3-Trichlorobenzene
ND
1.00 1
04/04/202312:27
WG2035064
1,2,4-Trichlorobenzene
ND
C3
1.00 1
04/04/202312:27
WG2035064
1,1,1-Trichloroethane
ND
1.00 1
04/04/202312:27
WG2035064
1,1,2-Trichloroethane
ND
1.00 1
04/04/202312:27
WG2035064
Trichloroethene
ND
1.00 1
04/04/202312:27
WG2035064
Trichlorofluoromethane
ND
C3
5.00 1
04/04/202312:27
WG2035064
1,2,3-Trichloropropane
ND
2.50 1
04/04/202312:27
WG2035064
1,2,4-Trimethylbenzene
ND
1.00 1
04/04/202312:27
WG2035064
1,2,3-Trimethyl benzene
ND
1.00 1
04/04/202312:27
WG2035064
1,3,5-Trimethyl benzene
ND
1.00 1
04/04/202312:27
WG2035064
Vinyl chloride
ND
1.00 1
04/04/202312:27
WG2035064
Xylenes, Total
ND
3.00 1
04/04/202312:27
WG2035064
(S) Toluene-d8
108
80.0-120
041041202312.27
WG2035064
(S) 4-Bromof/uorobenzene
98.7
77.0-126
041041202312.27
WG2035064
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Frit Car Inc.
L1600164
04/11/23 17:42
12 of 30

WELL #5 SAMPLE RESULTS - 03
Collected date/time: 03/30/23 15:18 L1600164
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Analyte ug/I
(S 1,2-Dich/oroethone-d4 101
Qualifier RDL Dilution Analysis Batch
ug/I date / time
70.0-130 041041202312.27 WG2035064
FP1
FTc
FSS
Fqn
FC]
I ql
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1600164 04/11/23 17:42 13 of 30

WG2034730
Gravimetric Analysis by Method 2540 C-2011
Method Blank (MB)
(MB) R3910412-1 04/04/2316:48
MB Result
Analyte ug/I
Dissolved Solids U
MB Qualifier MB MDL MB RDL
ug/1 ug/I
10000 10000
L16O0164-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1600164-01 04/04/2316:48 • (DUP) R3910412-3 04/04/2316:48
Original Result DUP Result Dilution DUP RPD
Analyte ug/I ug/I %
Dissolved Solids 1130000 1120000 1 0.890
L1600187-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
1-1600164-01,02,03
DUP Qualifier DUP RPD
Limits
o�
5
(OS) L1600187-01 04/04/2316:48 • (DUP) R3910412-4 04/04/23 16:48
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/1 % %
Dissolved Solids 465000 467000 1 0.429 5
Laboratory Control Sample (LCS)
(LCS) R3910412-2 04/04/2316:48
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I % %
Dissolved Solids 8800000 8460000 96.1 77.3-123
— I
Cp
FTC]
FS—S
rqn
FSr
_ �GI
rAl
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1600164 04/11/23 17:42 14 of 30

WG2034193
Wet Chemistry by Method 350.1
Method Blank (MB)
(MB) R3908247-1 04/01/23 23:38
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/I ug/I ug/I
Ammonia Nitrogen U 117 250
L1599795-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
1-1600164-01,02,03
(OS) L1599795-01 04/01/23 23:43 • (DUP) R3908247-3 04/01/23 23:44
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I % %
Ammonia Nitrogen ND ND 1 10.5 10
L1600201-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1600201-01 04/02/23 00:07 • (DUP) R3908247-6 04/02/23 00:08
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I % %
Ammonia Nitrogen 2490 2530 1 1.48 10
Laboratory Control Sample (LCS)
(LCS) R3908247-2 04/01/23 23:40
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I % %
Ammonia Nitrogen 7500 7990 107 90.0-110
L1599795-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1599795-01 04/01/23 23:43 • (MS) R3908247-4 04/01/23 23:46 • (MSD) R3908247-5 04/01/23 23:47
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
Analyte ug/I ug/I ug/I ug/I % % % %
Ammonia Nitrogen 5000 ND 5140 5060 102 100 1 90.0-110 1.51
L16O0201-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1600201-01 04/02/23 00:07 • (MS) R3908247-7 04/02/23 00:10
Spike Amount Original Result MS Result MS Rec.
Analyte ug/I ug/I ug/I %
Ammonia Nitrogen 5000 2490 7410 98.4
Dilution Rec. Limits MS Qualifier
1 90.0-110
RPD Limits
10
— I
Cp
FTc
FSS
rqn
FSr
_ �GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1600164 04/11/23 17:42 15 of 30

WG2036422
Wet Chemistry by Method 365.4
Method Blank (MB)
(MB) R3909810-1 04/05/2319:18
MB Result MB Qualifier MB MDL
Analyte ug/I ug/I
Phosphorus,Total U 35.0
MB RDL
ug/I
100
L16O0393-02 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
1-1600164-01,02,03
(OS) L1600393-02 04/05/2319:35 • (DUP) R3909810-3 04/05/2319:36
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I % %
Phosphorus,Total 201 ND 1 125 P1 20
L1600393-03 Original Sample (OS) • Duplicate (DUP)
(OS) L1600393-03 04/05/2319:40 • (DUP) R3909810-6 04/05/23 19:41
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I % %
Phosphorus,Total ND ND 1 0.742 20
Laboratory Control Sample (LCS)
(LCS) R3909810-2 04/05/2319:20
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I % %
Phosphorus,Total 2470 2530 102 83.2-116
L1600393-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1600393-02 04/05/2319:35 • (MS) R3909810-4 04/05/2319:38 • (MSD) R3909810-5 04/05/23 19:39
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
Analyte ug/I ug/I ug/I ug/I % % % %
Phosphorus,Total 2500 201 2260 2290 82.4 83.6 1 90.0-110 1.32
Sample Narrative:
MS: Matrix spike failure due to matrix.
MSD: Matrix spike failure due to matrix.
RPD Limits
20
— I
Cp
FTc
FSS
rqn
FSr
_ �GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1600164 04/11/23 17:42 16 of 30

WG2033523
Wet Chemistry by Method 9056A
Method Blank (MB)
(MB) R3908585-1 03/31/2310:10
MB Result
Analyte ug/I
Chloride U
Nitrate U
Sulfate U
MB Qualifier MB MDL MB RDL
ug/1 ug/I
379 1000
48.0 100
594 5000
L1600164-02 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
1-1600164-01,02,03
(OS) L1600164-02 03/31/2317:45 • (DUP) R3908585-3 03/31/2317:58
Original Result
DUP Result
Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
Analyte
ug/I
ug/I
%
%
Chloride
12600
12700
1 0.796
15
Nitrate
ND
ND
1 0.595
15
Sulfate
8980
8980
1 0.0657
15
L1600216-07 Original Sample (OS) • Duplicate (DUP)
(OS) L1600216-07 03/31/23 23:17 • (DUP) R3908585-5 03/31/23 23:30
Original Result
DUP Result
Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
Analyte
ug/I
ug/1
%
%
Chloride
81800
83100
1 1.58
15
Nitrate
451
465
1 3.01
15
Sulfate
161000
161000
1 0.00879
15
Laboratory Control Sample (LCS)
(LCS) R3908585-2 03/31/2310:23
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte ug/I
ug/1
%
%
Chloride 40000
39500
98.7
80.0-120
Nitrate 8000
7790
97.3
80.0-120
Sulfate 40000
39500
98.6
80.0-120
FP1
FTc
FSS
rqn
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1600164 04/11/23 17:42 17 of 30

WG2033523 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9056A L1600164-01,02,03
L16OO164-02 Original Sample (OS) • Matrix Spike (MS)
(OS) L1600164-02 03/31/2317:45 • (MS) R3908585-4 03/31/2318:12
Spike Amount
Original Result
MS Result
MS Rec.
Analyte
ug/I
ug/1
ug/1
%
Chloride
50000
12600
62400
99.6
Nitrate
5000
ND
4850
96.0
Sulfate
50000
8980
59600
101
Dilution Rec. Limits MS Qualifier
1 80.0-120
1 80.0-120
1 80.0-120
L1600216-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1600216-07 03/31/23 23:17 • (MS) R3908585-7 03/31/23 23:54 • (MSD) R3908585-8 04/01/23 00:32
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
ug/I
ug/1
ug/1
ug/I
%
%
Chloride
50000
81800
128000
128000
91.7
92.4
Nitrate
5000
451
5600
5730
103
106
Sulfate
50000
161000
205000
205000
86.3
86.3
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
1 80.0-120 0.271
1 80.0-120 2.28
1 80.0-120 E E 0.0141
RPD Limits
15
15
15
FP1
FTc
FSS
rqn
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1600164 04/11/23 17:42 18 of 30

WG2034273
Wet Chemistry by Method 9060A
Method Blank (MB)
(MB) R3908827-2 04/03/23 12:47
MB Result
Analyte ug/I
TOC (Total Organic Carbon) 275
MB Qualifier MB MDL MB ROL
ug/I ug/I
J 102 1000
L1599969-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1599969-01 04/03/2314:23 • (DUP) R3908827-3 04/03/2314:37
Original Result DUP Result Dilution DUP RPD
Analyte ug/I ug/I %
TOC 1820 1810 1 0.441
L1600164-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1600164-01,02,03
DUP Qualifier DUP RPD
Limits
20
(OS) L1600164-01 04/03/2318:07 • (DUP) R3908827-8 04/03/2318:27
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I % %
TOC 8620 8650 1 0.324 20
Laboratory Control Sample (LCS)
(LCS) R3908827-1 04/03/2312:32
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I % %
TOC 75000 74100 98.8 85.0-115
L1600133-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1600133-02 04/03/2314:52 • (MS) R3908827-4 04/03/2315:18 • (MSD) R3908827-5 04/03/2315:40
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec.
Analyte ug/I ug/I ug/I ug/I % %
TOC 50000 ND 50800 50700 99.9 99.6
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
1 80.0-120 0.355
L1600155-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
RPD Limits
20
(OS) L1600155-04 04/03/2316:55 • (MS) R3908827-6 04/03/2317:21 • (MSD) R3908827-7 04/03/2317:48
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/I ug/I ug/I ug/I % % % % %
TOC 50000 1250 52600 53100 103 104 1 80.0-120 1.10 20
— I
Cp
FTc
FSS
rqn
FSr
_ �GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1600164 04/11/23 17:42 19 of 30

WG2034072
Metals (ICPMS) by Method 6020B
Method Blank (MB)
(MB) R3909169-1 04/04/2315:02
MB Result
Analyte
ug/I
Chromium,Dissolved
U
Copper,Dissolved
U
Iron,Dissolved
28.2
Lead,Dissolved
U
Nickel.Dissolved
U
MB Qualifier MB MDL
ug/I
1.24
1.51
J 28.1
0.849
0.816
Laboratory Control Sample (LCS)
(LCS) R3909169-2 04/04/2315:05
Spike Amount
LCS Result
Analyte
ug/I
ug/1
Chromium,Dissolved
50.0
52.2
Copper,Dissolved
50.0
46.2
Iron,Dissolved
5000
5090
Lead,Dissolved
50.0
51.5
Nickel,Dissolved
50.0
53.3
QUALITY CONTROL SUMMARY
1-1600164-01,03
MB RDL
ug/I
2.00
5.00
100
2.00
2.00
LCS Rec.
Rec. Limits LCS Qualifier
104
80.0-120
92.5
80.0-120
102
80.0-120
103
80.0-120
107
80.0-120
L1600512-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1600512-04 04/04/2315:08 • (MS) R3909169-4 04/04/2315:15 • (MSD) R3909169-5 04/04/2315:18
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
ug/I
ug/1
ug/1
ug/I
%
%
Chromium,Dissolved
50.0
ND
49.4
50.7
98.7
101
Copper,Dissolved
50.0
ND
45.0
44.7
89.9
89.5
Iron,Dissolved
5000
110
4910
5050
96.0
98.8
Lead,Dissolved
50.0
ND
48.4
49.5
96.8
99.0
Nickel,Dissolved
50.0
5.14
54.2
54.4
98.0
98.5
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
1 75.0-125
2.72
1 75.0-125
0.491
1 75.0-125
2.88
1 75.0-125
2.33
1 75.0-125
0.395
RPD Limits
20
20
20
20
20
FP1
FTc
FSS
rqn
FSr
�GI
FAI
FSC
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Frit Car Inc. L1600164 04/11/23 17:42 20 of 30

WG2034085
Metals (ICPMS) by Method 6020B
Method Blank (MB)
(MB) R3908607-1 04/03/2310:19
MB Result
Analyte
ug/I
Chromium
U
Copper
U
Iron
U
Lead
U
Nickel
U
MB Qualifier MB MDL
ug/I
1.24
1.51
28.1
0.849
0.816
Laboratory Control Sample (LCS)
(LCS) R3908607-2 04/03/2310:22
Spike Amount
LCS Result
Analyte
ug/I
ug/I
Chromium
50.0
53.1
Copper
50.0
50.2
Iron
5000
5150
Lead
50.0
49.3
Nickel
50.0
51.7
QUALITY CONTROL SUMMARY
L1600164-01,03
MB RDL
ug/I
2.00
5.00
100
2.00
2.00
LCS Rec.
Rec. Limits LCS Qualifier
106
80.0-120
100
80.0-120
103
80.0-120
98.5
80.0-120
103
80.0-120
L1598983-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1598983-01 04/03/2310:25 • (MS) R3908607-4 04/03/2310:36 • (MSD) R3908607-5 04/03/23 10:39
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
ug/I
ug/I
ug/I
ug/I
%
%
Chromium
50.0
ND
49.5
46.6
99.0
93.1
Copper
50.0
8.37
57.3
54.6
97.9
92.5
Iron
5000
2580
7940
7030
107
88.9
Lead
50.0
4.47
54.2
51.5
99.5
94.1
Nickel
50.0
ND
50.1
46.2
100
92.4
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
1 75.0-125
6.18
1 75.0-125
4.87
1 75.0-125
12.2
1 75.0-125
5.07
1 75.0-125
8.07
RPD Limits
20
20
20
20
20
FP1
FTC
FSS
rqn
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1600164 04/11/23 17:42 21 of 30

WG2039132
Metals (ICPMS) by Method 6020B
Method Blank (MB)
(MB) R3911413-1 04/10/2313:45
MB Result
Analyte
ug/I
Chromium,Dissolved
U
Copper,Dissolved
U
Iron,Dissolved
U
Lead,Dissolved
U
Nickel.Dissolved
U
MB Qualifier MB MDL
ug/I
1.24
1.51
28.1
0.849
0.816
Laboratory Control Sample (LCS)
(LCS) R3911413-2 04/10/2313:48
MB RDL
ug/I
2.00
5.00
100
2.00
2.00
QUALITY CONTROL SUMMARY
L1600164-02
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
ug/I
ug/I
%
%
Chromium,Dissolved
50.0
48.3
96.6
80.0-120
Copper,Dissolved
50.0
46.5
93.0
80.0-120
Iron,Dissolved
5000
5030
101
80.0-120
Lead,Dissolved
50.0
49.2
98.4
80.0-120
Nickel,Dissolved
50.0
49.3
98.6
80.0-120
L1600164-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1600164-02 04/10/2313:51 • (MS) R3911413-4 04/10/2313:58 • (MSD) R3911413-5 04/10/2314:01
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
ug/I
ug/1
ug/1
ug/I
%
%
Chromium,Dissolved
50.0
ND
48.7
49.3
97.4
98.6
Copper,Dissolved
50.0
ND
47.1
47.6
94.2
95.3
Iron,Dissolved
5000
ND
5040
5070
100
101
Lead,Dissolved
50.0
ND
47.7
49.9
95.4
99.9
Nickel,Dissolved
50.0
ND
50.1
50.4
100
101
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
1 75.0-125
1.24
1 75.0-125
1.17
1 75.0-125
0.664
1 75.0-125
4.63
1 75.0-125
0.415
RPD Limits
20
20
20
20
20
FP1
FTc
FSS
rqn
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1600164 04/11/23 17:42 22 of 30

WG2039135
Metals (ICPMS) by Method 6020B
Method Blank (MB)
(MB) R3911414-1 04/10/2314:05
MB Result
Analyte
ug/I
Chromium
U
Copper
U
Iron
U
Lead
U
Nickel
U
MB Qualifier MB MDL
ug/I
1.24
1.51
28.1
0.849
0.816
Laboratory Control Sample (LCS)
(LCS) R3911414-2 04/10/2314:08
Spike Amount
LCS Result
Analyte ug/I
ug/I
Chromium 50.0
49.3
Copper 50.0
53.7
Iron 5000
4990
Lead 50.0
49.3
Nickel 50.0
49.9
QUALITY CONTROL SUMMARY
L1600164-02
MB RDL
ug/I
2.00
5.00
100
2.00
2.00
LCS Rec.
Rec. Limits LCS Qualifier
98.5
80.0-120
107
80.0-120
99.7
80.0-120
98.5
80.0-120
99.7
80.0-120
L1600164-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1600164-02 04/10/2314:11 • (MS) R3911414-4 04/10/2314:24 • (MSD) R3911414-5 04/10/2314:27
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
ug/I
ug/I
ug/I
ug/I
%
%
Chromium
50.0
ND�
49.9
47.7
99.9
95.4
Copper
50.0
ND
48.2
56.2
96.3
112
Iron
5000
381
5280
5250
97.9
97.3
Lead
50.0
ND
48.7
47.6
97.3
95.2
Nickel
50.0
ND
50.3
48.7
101
97.5
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
1 75.0-125
4.62
1 75.0-125
15.4
1 75.0-125
0.582
1 75.0-125
2.28
1 75.0-125
3.18
RPD Limits
20
20
20
20
20
FP1
FTc
FSS
rqn
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1600164 04/11/23 17:42 23 of 30

WG2035064
Volatile Organic Compounds (GC/MS) by Method 8260D
QUALITY CONTROL SUMMARY
1-1600164-01,02,03
Method Blank (MB)
(MB) R3909782-2 04/04/23 05:26
MB Result
Analyte
ug/I
Acetone
U
Acrolein
U
Acrylonitrile
U
Benzene
U
Bromobenzene
U
Bromodichloromethane
U
Bromoform
U
Bromomethane
U
n-Butylbenzene
U
sec -Butyl benzene
U
tert-Butylbenzene
U
Carbon tetrachloride
U
Chlorobenzene
U
Chlorodibromomethane
U
Chloroethane
U
Chloroform
U
Chloromethane
U
2-Chlorotoluene
U
4-Chlorotoluene
U
1,2-Dibromo-3-Chloropropane
U
1,2-Dibromoethane
U
Dibromomethane
U
1,2-Dichlorobenzene
U
1,3-Dichlorobenzene
U
1,4-Dichlorobenzene
U
Dichlorodifluoromethane
U
1,1-Dichloroethane
U
1,2-Dichloroethane
U
1,1-Dichloroethene
U
cis-1,2-Dichloroethene
U
trans-1,2-Dichloroethene
U
1,2-Dichloropropane
U
1,1-Dichloropropene
U
1,3-Dichloropropane
U
cis-1,3-Dichloropropene
U
trans-1,3-Dichloropropene
U
2,2-Dichloropropane
U
Di -isopropyl ether
U
Ethylbenzene
U
Hexachloro-1,3-butadiene
U
MB Qualifier
MB MDL MB RDL
ug/I ug/I
11.3 50.0
2.54 50.0
0.671 10.0
0.0941 1.00
0.118 1.00
0.136 1.00
0.129 1.00
0.605 5.00
0.157 1.00
0.125 1.00
0.127 1.00
0.128 1.00
0.116 1.00
0.140 1.00
0.192 5.00
0.111 5.00
0.960 2.50
0.106 1.00
0.114 1.00
0.276 5.00
0.126 1.00
0.122 1.00
0.107 1.00
0.110 1.00
0.120 1.00
0.374 5.00
0.100 1.00
0.0819 1.00
0.188 1.00
0.126 1.00
0.149 1.00
0.149 1.00
0.142 1.00
0.110 1.00
0.111 1.00
0.118 1.00
0.161 1.00
0.105 1.00
0.137 1.00
0.337 1.00
FP1
FTC
FSS
rqn
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1600164 04/11/23 17:42 24 of 30

WG2035064
QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS)
by Method
8260D
1-1600164-01,02,03
Method Blank (MB)
FP1(MB)
R3909782-2 04/04/23 05:26
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte ug/I
ug/I
ug/I
z
TC
Isopropylbenzene U
0.105
1.00
p-Isopropyltoluene U
0.120
1.00
FSS
2-Butanone (MEK) U
1.19
10.0
Methylene Chloride U
0.430
5.00
4-Methyl-2-pentanone (MIBK) U
0.478
10.0
rqn
Methyl tert-butyl ether U
0.101
1.00
Naphthalene U
1.00
5.00
FSr
n-Propylbenzene U
0.0993
1.00
Styrene U
0.118
1.00
1,1,1,2-Tetrachloroethane U
0.147
1.00
�
1,1,2,2-Tetrachloroethane U
0.133
1.00
1,1,2-Trichlorotrifluoroethane U
0.180
1.00
q
Tetrachloroethene U
0.300
1.00
Toluene U
0.278
1.00
1,2,3-Trichlorobenzene U
0.230
1.00
FAI
1,2,4-Trichlorobenzene U
0.481
1.00
1,1,1-Trichloroethane U
0.149
1.00
FSC
1,1,2-Trichloroethane U
0.158
1.00
Trichloroethene U
0.190
1.00
Trichlorofluoromethane U
0.160
5.00
1,2,3-Trichloropropane U
0.237
2.50
1,2,4-Trimethylbenzene U
0.322
1.00
1,2,3-Trimethyl benzene U
0.104
1.00
1,3,5-Trimethyl benzene U
0.104
1.00
Vinyl chloride U
0.234
1.00
Xylenes, Total U
0.174
3.00
(S) Toluene-d8 107
80.0-120
(S) 4-Bromof/uorobenzene 94.8
77.0-126
(S)1,2-Dich/oroethane-d4 97.8
70.0-130
Laboratory Control Sample (LCS)
(LCS) R3909782-1 04/04/23 04:44
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte ug/I
ug/I
%
%
Acetone 25.0
32.6
130
19.0-160
Acrolein 25.0
10.4
41.6
10.0-160
Acrylonitrile 25.0
27.9
112
55.0-149
Benzene 5.00
5.14
103
70.0-123
ACCOUNT:
PROJECT: SDG: DATE/TIME:
PAGE:
Frit Car Inc.
L1600164 04/11/23 17:42
25 of 30

WG2035064 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D 1-1600164-01,02,03
Laboratory Control Sample (LCS)
(LCS) R3909782-1 04/04/23 04:44
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
ug/I
ug/I
%
%
Bromobenzene
5.00
4.65
93.0
73.0-121
Bromodichloromethane
5.00
4.54
90.8
75.0-120
Bromoform
5.00
3.97
79.4
68.0-132
Bromomethane
5.00
3.14
62.8
10.0-160
n-Butylbenzene
5.00
4.34
86.8
73.0-125
sec -Butyl benzene
5.00
4.48
89.6
75.0-125
tert-Butylbenzene
5.00
4.46
89.2
76.0-124
Carbon tetrachloride
5.00
4.98
99.6
68.0-126
Chlorobenzene
5.00
4.83
96.6
80.0-121
Chlorodibromomethane
5.00
4.67
93.4
77.0-125
Chloroethane
5.00
4.45
89.0
47.0-150
Chloroform
5.00
4.86
97.2
73.0-120
Chloromethane
5.00
6.80
136
41.0-142
2-Chlorotoluene
5.00
4.66
93.2
76.0-123
4-Chlorotoluene
5.00
4.42
88.4
75.0-122
1,2-Dibromo-3-Chloropropane
5.00
4.20
84.0
58.0-134
1,2-Dibromoethane
5.00
5.08
102
80.0-122
Dibromomethane
5.00
4.76
95.2
80.0-120
1,2-Dichlorobenzene
5.00
4.90
98.0
79.0-121
1,3-Dichlorobenzene
5.00
4.40
88.0
79.0-120
1,4-Dichlorobenzene
5.00
4.59
91.8
79.0-120
Dichlorodifluoromethane
5.00
5.11
102
51.0-149
1,1-Dichloroethane
5.00
5.27
105
70.0-126
1,2-Dichloroethane
5.00
4.98
99.6
70.0-128
1,1-Dichloroethene
5.00
5.15
103
71.0-124
cis-1,2-Dichloroethene
5.00
4.78
95.6
73.0-120
trans-1,2-Dichloroethene
5.00
4.74
94.8
73.0-120
1,2-Dichloropropane
5.00
5.02
100
77.0-125
1,1-Dichloropropene
5.00
5.07
101
74.0-126
1,3-Dichloropropane
5.00
4.88
97.6
80.0-120
cis-1,3-Dichloropropene
5.00
4.87
97.4
80.0-123
trans-1,3-Dichloropropene
5.00
4.45
89.0
78.0-124
2,2-Dichloropropane
5.00
4.06
81.2
58.0-130
Di -isopropyl ether
5.00
5.15
103
58.0-138
Ethylbenzene
5.00
4.56
91.2
79.0-123
Hexachloro-1,3-butadiene
5.00
5.45
109
54.0-138
Isopropylbenzene
5.00
4.48
89.6
76.0-127
p-Isopropyltoluene
5.00
4.61
92.2
76.0-125
2-Butanone (MEK)
25.0
31.7
127
44.0-160
Methylene Chloride
5.00
4.72
94.4
67.0-120
ACCOUNT:
PROJECT:
Frit Car Inc.
SDG: DATE/TIME: PAGE:
L1600164 04/11/23 17:42 26 of 30
FP1
FTC
FSS
rqn
FSr
�GI
FAI
FSC

WG2035064 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D 1-1600164-01,02,03
Laboratory Control Sample (LCS)
(LCS) R3909782-1 04/04/23 04:44
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
ug/I
ug/I
%
%
4-Methyl-2-pentanone (MIBK)
25.0
26.9
108
68.0-142
Methyl tert-butyl ether
5.00
4.39
87.8
68.0-125
Naphthalene
5.00
3.21
64.2
54.0-135
n-Propylbenzene
5.00
4.53
90.6
77.0-124
Styrene
5.00
4.36
87.2
73.0-130
1,1,1,2-Tetrachloroethane
5.00
4.99
99.8
75.0-125
1,1,2,2-Tetrachloroethane
5.00
4.27
85.4
65.0-130
1,1,2-Trichlorotrifluoroethane
5.00
5.06
101
69.0-132
Tetrachloroethene
5.00
4.81
96.2
72.0-132
Toluene
5.00
4.90
98.0
79.0-120
1,2,3-Trichlorobenzene
5.00
4.76
95.2
50.0-138
1,2,4-Trichlorobenzene
5.00
3.89
77.8
57.0-137
1,1,1-Trichloroethane
5.00
4.96
99.2
73.0-124
1,1,2-Trichloroethane
5.00
4.89
97.8
80.0-120
Trichloroethene
5.00
5.30
106
78.0-124
Trichlorofluoromethane
5.00
3.83
76.6
59.0-147
1,2,3-Trichloropropane
5.00
4.77
95.4
73.0-130
1,2,4-Trimethylbenzene
5.00
4.35
87.0
76.0-121
1,2,3-Trimethyl benzene
5.00
4.68
93.6
77.0-120
1,3,5-Trimethyl benzene
5.00
4.39
87.8
76.0-122
Vinyl chloride
5.00
5.17
103
67.0-131
Xylenes, Total
15.0
13.9
92.7
79.0-123
(S) Toluene-d8
105
80.0-120
(S) 4-Bromof/uorobenzene
102
77.0-126
(S)1,2-Dich/oroethane-d4
98.8
70.0-130
FP1
FTC
FSS
rqn
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1600164 04/11/23 17:42 27 of 30

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
B
The same analyte is found in the associated blank.
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C3 The reported concentration is an estimate. The continuing calibration standard associated with this data responded low.
Method sensitivity check is acceptable.
E The analyte concentration exceeds the upper limit of the calibration range of the instrument established by the initial
calibration (ICAL).
J The identification of the analyte is acceptable; the reported value is an estimate.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
P1 RPD value not applicable for sample concentrations less than 5 times the reporting limit.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1600164 04/11/23 17:42 28 of 30

ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
Nebraska
NE-OS-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TN002
California
2932
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolinas
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhodelsland
LA000356
Kentucky16
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee' °
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas'
LAB0152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TN003
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A21-A
A21-A — ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A21-A — ISO 17025 s
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks 'Aquatic Toxicity ° Chemical/Microbiological 'Mold 6 Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
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ACCOUNT: PROJECT: SDG: DATE/TIME:
Frit Car Inc. L1600164 04/11/23 17:42
PAGE:
29 of 30

Company Name/Address:
Billing Information:
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Frit Car Inc.
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PO Box 1340
2012 US Hwy 17N'
Brewton, AL 36427
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New Bern, NC 28560
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Report to:
Email To: [e-mail]
Connie Pettis
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Sample Receipt Checklist
e Matrix:Remarks:
SS - Soil AIR - Air F - Filter pH Temp
CDC Seal Present/Intact: —�
NP 7' N
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COC Signed/Accurate:
GW - Groundwater B - Bioassay
Flow Other
X N
Bottles arrive intact:N
WW - Wastewater
Correct bottles used:
DW - Drinking Water Samples returned via:
Sufficient volume sent: X N
OT - Other _ UPS FedEx Courier Tracking#
_ —
If Applicable
VOA Zero Headspace: Y N
Preservation Correct/Checked: --11-N
Trip Received: Yes
Relinquished by : (Signature) Date:
Time.
Received by: (Signature)
Blank o
RAD Screen <0.5 mR/hr: fYrN
3 0
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/ MeoH
HCLO/
TBR
TBR
Relinquished by : (Signature) Date:
Time:
Received by: (Signature)
TlIem/Ill Bottles Receive
If preservation required by Login: Date/Time
Relinquished by : (Signature)
Date:
Time:
Received for lab .14griature l
Date: Time:
)
Hold:
Condi on:
NCF OK
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