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NC0025135_Permit Issuance_20160408
PAT MCCRORY Water Resources ENVIRONMENTAL QUALITY April 8, 2016 Mr. Lee Huffman, Manager Huffman Finishing Company P.O. Box 170 Granite Falls, North Carolina 28630 Govemor DONALD R. VAN DER VAART Secretary S. JAY ZIMMERMAN Director' Subject: Issuance of NPDES Permit Renewal Permit No. NCO025135 Huffman Finishing Company Caldwell County Facility Class 11 Dear Mr. Huffman: Division personnel have reviewed and approved your application for renewal of the subject permit. Accordingly, we are forwarding the attached NPDES discharge permit. This permit is issued pursuant to the requirements of North Carolina General Statute 143-215.1 and Memorandum of Agreement between North Carolina and the U.S. Environmental Protection Agency dated October 15, 2007 (or as subsequently amended). Through further review, several changes were made to the draft permit sent to you on February 10, 2016: • Electronic Discharge Monitoring Report (eDMR) requirements have been updated. Four main revisions include: 1) Electronic reporting of DMR data is required effective December 21, 2016;.2) Electronic reporting requirements of compliance monitoring data and reports have been added; 3) A section has,been added that requires permittees to identify the initial recipient of their electronic submissions; 4) A section has been added on how to request an electronic reporting waiver. A footnote was added under Section.A. (L) to state "No later than December 21, 2016, begin submitting discharge monitoring reports electronically using NC DWR's eDMR application system" and Special Condition A. (3.) was updated to reflect the eDMR reporting deadline of December 21, 2016. As identified previously, the renewal permit contains the following significant changes from your current permit: • Starting December 21, 2016, federal regulations require electronic submittal of all discharge monitoring reports (DMRs) and specify that, if a state does not establish a system to receive such submittals, then permittees must submit DMRs electronically to the Environmental Protection Agency (EPA). The fmal NPDES Electronic Reporting Rule was adopted .and became effective on December 21, 2015. State of North Carolina I Environmental Quality I Water Resources 1617 Mail service Center I Raleigh, North Carolina 27699-1617 919 707 9000 Page 2 of 3 w The requirement to begin reporting discharge monitoring data electronically using the NC DWR's Electronic Discharge Monitoring Report (eDMR) internet application has been added to your final NPDES permit. [See Special Condition A. (3.)] For information on eDMR, registering for eDMR and obtaining an eDMR user account, please visit the following web page: http://deq.ne.gov/about/divisions/water-resources/edmr. For more information on EPA's final NPDES Electronic Reporting Rule, please visit the following web site: http://www2.epa.gov/compliance/final-national-pollutant-discharge-elimination-s stem-npdes- electronic-reporting rule. © Effluent limitations for BODs, TSS, COD, total chromium, sulfide, and total phenol have been updated based on production data for the last five years. • Sampling type for effluent TSS has been changed to composite. See Section A. (i.). e Monitoring requirements for BODs, TSS, COD, fecal colifonn, pH and temperature have been reduced to 2/week. Monitoring requirements for total nitrogen and total phosphorus have been reduced to quarterly. See Section A. (1.). o Effluent samples for silver showed 44 samples < 5 ug/L and 1 sample < 50 ug/L. The Huffman Finishing WWTP's chronic allowable allocation for silver is 6.25 ug/L. In accordance with NC Administrative Code Section 15A NCAC 02B .0500, all test procedures must produce detection and reporting levels that are below the permit discharge requirements and all data generated must be reported to the approved detection level or lower reporting level of the procedure. DWR's Water Sciences Section has determined that the Practical Quantitation Limit (PQL) for silver is 1 ug/L. Please see that the certified laboratory performing the facility's metals analysis can measure to the approved detection level or lower reporting level. A list of PQL's determined by the Division can be found at the following website: http://deg.ne.gov/about/divisions/water-resources/water-resources-data/water- sciences-home-page/microbiolo y -inorganics-branch/methods-pgls-qa. The monitoring requirement for silver is maintained in the permit renewal with a reduced monitoring frequency of quarterly. Effluent samples for total phenolic compounds, nickel, and antimony showed no potential to violate water quality standards and the maximum predicted concentrations were all less than 50% of the allowable allocations. Limitations and monitoring requirements for nickel and antimony have been removed from the permit. Limitations for total phenols are based on EPA technology based effluent limits (TBEL) for Textile Mills, 40 CFR 410.52 and must be maintained in the permit. Some of the wording has changed in Special Condition A. (2), Chronic Toxicity Permit Limit, please review each paragraph carefully. DWR would also encourage the facility to fix the outfall pipeline cracks and consider extending the discharge pipeline in order to have better effluent mix. However, prior to performing any work on the outfall pipe, the pernittee shall contact the Asheville Regional Office for assistance and to obtain any necessary permits. If any parts, measurement frequencies or sampling requirements contained in this permit are unacceptable to you, you have the right to an adjudicatory hearing upon written request within thirty (30) days following receipt of this letter. This request must be in the form of a written petition, conforming to Chapter 150B of the North Carolina General Statutes, and filed with the Office of Administrative Hearings (6714 Mail Service Center, Raleigh, North Carolina 27699-6714). Unless such demand is made, this decision shall be final and binding. Please note that this permit is not transferable except after notice to the Division. The Division may require modification or revocation and reissuance of the pen -nit. This pen -nit does not affect the legal Page 3 of 3 requirements to obtain other permits which may be required by the Division of Water Resources or any other Federal, State, or Local government permits that may be required. If you have questions concerning this permit, please contact Yang Song by e-mail (yang.song@ncdenr.gov) or phone at (919) 807-6479. Sincerely, &torill /iS V/mle:�' ivision of Water Resources Enclosure: NPDES Permit NC0025135 cc: NPDES Unit Central Files Asheville Regional Office / Water Quality Program e-copy: EPA Region IV Susan Meadows, Aquatic Toxicity Branch Shuford Wise, Huffman Finishing Company ORC Permit NCO025135 i STATE- OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES PERMIT TO DISCHARGE WASTEWATER UNDER THE . NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, Huffman Finishing, Company, Inc. is hereby authorized to discharge wastewater from a facility located at 4919 Hickory Boulevard southeast of Granite Falls Caldwell County to receiving waters designated as the Catawba River (Lake Hickory) in the Catawba River Basin in accordance with effluent limitations, monitoring requirements, and other applicable conditions set forth in Parts I, II, Ill and IV hereof. This permit shall become effective May 1, 2016. This permit and authorization to discharge shall expire at midnight on January 31, 2020: Signed this day April 8, 2016. AxIL 9 SH y Zimmerm~ , P. . D' ector, Division of Water Resources By Authority of the Environmental Management Commission Page 1 of 6 Permit NCO025135 SUPPLEMENT TO PERMIT COVER SHEET All previous NPDES Permits issued to this facility, whether for operation or discharge are hereby revoked. As of this permit issuance, any previously issued permit bearing this number is no longer effective. Therefore, the exclusive authority to operate and discharge from this facility arises under the permit conditions, requirements, terms, and provisions included herein. Huffman Finishing Company, Inc. is hereby authorized to: 1. Continue to operate an existing 0.250 MGD wastewater treatment facility consisting of the following components: ➢ Vibrate screen ➢ Flow equalization basin with four floating aerators ➢ Lift pumps ➢ Oxidation ditch ➢ Circular clarifier ➢ Sludge recirculation pumps ➢ Chlorine contact tank Ultrasonic flow measurement ➢ Chemical dechlorination ➢ Cascade post aeration ➢ Aerobic sludge digester ➢ Sludge holding lagoon ➢ Sludge drying beds ➢ Auxiliary power The facility is located at Huffman Finishing Company Wastewater Treatment Plant, at 4919 Hickory Boulevard, southeast of Granite Falls, Caldwell County. 2. Discharge from said treatment works at the location specified on the attached map into the Catawba River (Lake Hickory), which are classified WS-IV, B; CA waters in the Catawba River Basin. Page 2 of 6 Permit NCO025135 PART I A. (1) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS [15A NCAC 02B .0400 et seq., 02B .0500 et seq.] During the period beginning upon the effective date of the pen -nit and lasting until expiration, the Permittee is authorized to discharge treated wastewater from outfa11001. Such discharges shall be limited and monitored' by the Permittee as specified below: X,k', lYIET9R' ` ,` _..Location_ _._ .-- LI1YiITS: _ _ _ .... -1ViONITQRIIVG REQUIREMENTS Monthly Average .Daily Naximum Measurement . Sample ganiple - - Flow ' 0.250 MGD' Continuous Recorder Influent or Effluent BOD, 5 day, 20°C 67.6 pounds/day 135.1 pounds/day 2 /Week Composite Effluent ' Total Suspended Solids 294.6 pounds/day 589.2 pounds/day 2 /Week Composite Effluent COD 810.8 pounds/day 1621.6 pounds/day 2 /Week Composite Effluent Fecal Coliform (geometric mean) 200/100 mL 400/100mL 2 /Week Grab Effluent pH > 6.0 and < 9.0 standard units 2 /Week Grab Effluent Temperature 2 /Week Grab Effluent Total Chromium 1.4 pounds/day 2.7 pounds/day Weekly Composite Effluent Sulfides 2.7 pounds/day 5.4 pounds/day Weekly Grab Effluent Phenols 1.4 pounds/day 2.7 pounds/day Weekly Grab Effluent Total Residual Chlorine 2 28 µg/L Weekly Grab Effluent Total Silver Quarterly Composite Effluent NH3 as N Monthly Composite Effluent Total Nitrogen (NO2 + NO3 + TKN) Quarterly Composite Effluent Total Phosphorus Quarterly Composite Effluent Chronic Toxicity 3 Quarterly Composite Effluent Notes 1. No later than December 21, 2016, begin submitting discharge monitoring reports electronically using NC DWR's eDMR application system. See Special Condition A.(3.). 2. The TRC limit and monitoring requirements apply only if chlorine is used for disinfection. The facility shall report all effluent TRC values reported by a NC certified laboratory including field certified. However, effluent values below 50 µg/L will be treated as zero for compliance purposes. 3. Chronic toxicity (Ceriodaphnia) P/F@ 0.96%; March, June, September, and December. See Special Conditions A (2) of the Supplement to Effluent Limitations. There shall be no discharge of floating solids or foam in other than trace amounts. Part I, Page 3 of 6 Permit NCO025135 A (2). CHRONIC TOXICITY PERMIT LIMIT (QUARTERLY) [15A NCAC 02B .0200 et seq.] The effluent discharge shall at no time exhibit observable inhibition of reproduction or significant mortality to Ceriodaphnia duhia at an effluent concentration of 0.96 %. The permit holder shall perform at a minimum,quarter lX monitoring using test procedures outlined in the "North Carolina Ceriodaphnia Chronic Effluent Bioassay Procedure," Revised December 2010, or subsequent versions or "North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure" (Revised- December 2010) or subsequent versions. The tests will be performed during the months of March, June, September and December. These months signify the first month of each three-month toxicity testing quarter assigned to the facility. Effluent sampling for this testing must be obtained during representative effluent discharge and shall be performed at the NPDES permitted final effluent discharge below all treatment processes. If the test procedure performed as the first test of any single quarter results in a failure or ChV below the permit limit, then multiple -concentration testing shall be performed at a minimum, in each of the two following months as described in "North Carolina Phase H Chronic Whole Effluent Toxicity Test Procedure" (Revised -December 2010) or subsequent versions. All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge Monitoring Form (MR-1) for the months in which tests were performed, using the parameter code TGP3B for the pass/fail results and THP313 for the Chronic Value. Additionally, DWR Form AT-3 (original) is to be sent to the following address: Attention: North Carolina Division of Water Resources Water Sciences Section/Aquatic Toxicology Branch 1623 Mail Service Center Raleigh, NC 27699-1623 Completed Aquatic Toxicity Test Forms shall be filed with the Water Sciences Section no later than 30 days after the end of the reporting period for which the report is made. Test data shall be complete, accurate, include all supporting chemical/physical measurements and all concentration/response data, and be certified by laboratory supervisor and ORC or approved designate signature. Total residual chlorine of the effluent toxicity sample must be measured and reported if chlorine is employed for disinfection of the waste stream. Should there be no discharge of flow from the facility during a month in which toxicity monitoring is required, the permittee will complete the information located at the top of the aquatic toxicity (AT) test form indicating the facility name, pen -nit number, pipe number, county, and the month/year of the report with the notation of "No Flow" in the comment area of the form. The report shall be submitted to the Water Sciences Section at the address cited above. Should the permittee fail to monitor during a month in which toxicity monitoring is required, monitoring will be required during the following month. Assessment of toxicity compliance is based on the toxicity testing quarter, which is the three month time interval that begins on the first day of the month in which toxicity testing is required by this permit and continues until the final day of the third month. Should any test data from this monitoring requirement or tests performed by the North Carolina Division of Water Resources indicate potential impacts to the receiving.stream, this permit may be re -opened and modified to include alternate monitoring requirements or limits. NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control organism survival, minimum control organism reproduction, and appropriate environmental controls, shall constitute an invalid test and will require immediate follow-up testing to be completed no later than the last day of the month following the month of the initial monitoring. Part I, Page 4 of 6 Permit NC0025135 A (3) EILECTRONIC REPORTING OF DDISCHARGE MONITORING REPORTS [G. S. 143-215.1(b)] Federal regulations require electronic submittal of all discharge monitoring reports (DMRs) and program reports and specify that, if a state does not establish a system to receive such submittals, then permittees must submit monitoring data and reports electronically to the Environmental Protection Agency (EPA). The final NPDES Electronic Reporting Rule was adopted and became effective on December 21, 2015. NOTE: This special condition supplements or supersedes the following sections within Part II of this permit (Standard Conditions for NPDES Permits): • Section B. (11.) • Section D. (2.) • Section D. (6.) • Section E. (5.) Signatory Requirements Reporting Records Retention Monitoring Reports I. Reportint4 Requirements [Supersedes Section D. (2.) and Section E (5) (a)1 Effective December, 21, 2016, the permittee shall report discharge monitoring data electronically using the NC DWR's Electronic Discharge Monitoring Report (eDMR) internet application. Monitoring results obtained'during the previous month(s) shall be summarized for each month and submitted electronically using eDMR. The eDMR system allows permitted facilities to enter monitoring data and submit DMRs electronically using the internet. Until such time that the state's eDMR application is compliant with EPA's Cross -Media Electronic Reporting Regulation (CROMERR), permittees will be required to submit all discharge monitoring data to the state electronically using eDMR and will be required to complete the eDMR submission by printing, signing, and submitting one signed original and a copy of the computer printed eDMR to the following address: NC DENR / Division of Water Resources / Water Quality Permitting Section ATTENTION: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 If a permittee is unable to use the eDMR system due to a demonstrated hardship or due to the facility being physically located in an area where less than 10 percent of the households have broadband access, then a temporary waiver from the NPDES electronic reporting requirements may be granted and discharge monitoring data may be submitted on paper DMR forms (MR 1, 1.1, 2, 3) or alternative forms approved by the Director. Duplicate signed copies shall be submitted to the mailing address above. See "How to Request a Waiver from Electronic Reporting" section below. Regardless of the submission method, the first DMR is due on the last day of the month following the issuance of the permit or in the case of a new facility, on the last day of the month following the commencement of discharge. Starting on December 21, 2020, the permittee must electronically report the following compliance monitoring data and reports, when applicable: Sewer Overflow/Bypass Event Reports; Pretreatment Program Annual Reports; and Clean Water Act (CWA) Section 316(b) Annual Reports. The permittee may seek an electronic reporting waiver from the Division (see "How to Request a Waiver from Electronic Reporting" section below). Part I, Page 5 of 6 Permit NCO025135 2. Electronic Submissions In accordance with 40 CFR 122.41(1)(9), the permittee must identify the initial recipient at the time of each electronic submission. The permittee should use the EPA's website resources to identify the initial recipient for the electronic submission. Initial recipient of electronic NPDES information fi-om NPDES-regulated facilities means the entity (EPA or the state authorized by EPA to implement the NPDES program) that is the designated entity for receiving electronic NPDES data [see 40 CFR 127.2(b)]. EPA plans to establish a website that will also link to the appropriate electronic reporting tool for each type of electronic submission and for each state. Instructions on how to access and use the appropriate electronic reporting tool will be available as well. Information on EPA's NPDES Electronic Reporting Rule is found at: http://www2.epa.gov/compliance/final-national-pollutant-discharge-elimination-s stem-npdes-electronic-reporting- rule. Electronic submissions must start by the dates listed in the "Reporting Requirements" section above. 3. How to Request a Waiver from Electronic Reporting The permittee may seek a temporary electronic reporting waiver from the Division. To obtain an electronic reporting waiver, a penmittee must first submit an electronic reporting waiver request to the Division. Requests for temporary electronic reporting waivers must be submitted in writing to the Division for written approval at least sixty (60) days prior to the date the facility would be required under this permit to begin submitting monitoring data and reports. The duration of a temporary waiver shall not exceed 5 years and shall thereupon expire. At such time, monitoring data and reports shall be submitted electronically to the Division unless the permittee re -applies for and is granted a new temporary electronic reporting waiver by the Division. Approved electronic reporting waivers. are not transferrable. Only 'permittees with an approved reporting waiver request may submit monitoring data and reports on paper to the Division for the period that the approved reporting waiver request is effective. Information on eDMR and the application for a temporary electronic reporting waiver are found on the following web page: http:Hdeq.ne.gov/about/divisions/water-resources/edmr 4. Signatory Requirements [Supplements Section B. (I1.) (b) and Supersedes Section B. (11.) (d)1 All eDMRs submitted to the permit issuing authority shall be signed by a person described in Part II, Section B. (11.)(a) or by a duly authorized representative of that person as described in Part If, Section B. (11.)(b). A person, and not a position, must be delegated signatory authority for eDMR reporting purposes. For eDMR submissions, the person signing and submitting the DMR must obtain an eDMR user account and login credentials to access the eDMR system. For more information on North Carolina's eDMR system, registering for eDMR and obtaining an eDMR user account, please visit the following web page: http://deq.ne.gov/about/divisions/water-resources/edmr Certification. Any person submitting an electronic DMR using the state's eDMR system shall make the following certification [40 CFR 122.22]. NO OTHER STATEMENTS OF CERTIFICATION WILL BE ACCEPTED: 7 certify, under penalty of law, that this document and all attachments were prepared under nay direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. " 5. Records Retention [Supplements Section D. (6.)] The permittee shall retain records of all Discharge Monitoring Reports, including eDMR submissions. These records or copies shall be maintained for a period of at least 3 years from the date of the report. This period may be extended by request of the Director at any time [40 CFR 122.41]. Part I, Page 6 of 6 M [it 'Z 7 # vh' C— NJ 41 V I owe Discharge location Q 1� V, -Y V I HIM' W red, aV S f J it �Ifc -D&L 11 isers o 3 Huffman Finishing - NCO025135 F fifi0 V, i - 7r2oi [W LU WMI W11 It R Facility Location North Not to SCALE I I NCDEQ/DWR FACT SHEET FOR NPDES PERMIT DEVELOPMENT Huffman Finishing Company, Inc. NCO025135 Facility Information Applicant/ Facility Name: Huffman Finishing Company, Inc./ Huffinan Finishing Company WWTP Applicant Address: P.O. Box 170, Granite Falls, NC 28630 Facility Address: 4919 Hickory Boulevard, Granite Falls, NC 28630 Permitted Flow 0.25 MGD to Catawba River Type of Waste: 95% Industrial, 5% Domestic Facility/ Permit Status: Grade II, Major/ Renewal County: Caldwell Miscellaneous Receiving Stream: Catawba River Regional Office: Asheville Stream Classification: WS-IV, B, CA 8-digit HUC: 03050101 303(d) Listed?: NO Permit Writer: Yang Song Subbasin/ Stream Index: 03-08-32/ 11-(53) Date: March 29, 2016 Drainage Area (mil): 1090 Lat. 350 45' 34" N Long. 81' 23' 48"W Summer 7Q 10 (cfs) 40 (min. inst. release) Winter 7Q 10 (cfs): N/A Average Flow (cfs): N/A IWC (%) @ 9.0 MGD: 0.96 % Primary SIC Code: 2252 Background Huffinan Finishing, Inc. is a textile plant that manufactures hosiery and has requested renewal of their existing NPDES permit. The application for permit renewal (EPA Form 1, Form 2C) was received on July 14, 2014. The permit expired on January 31, 2015 and has been administratively continued. The applicable effluent guidelines are 40 CFR 410.52 (Textile Mills, Subpart E, Knit Fabric). The facility has a designed flow of 0.25 MGD and its wastewater is 95% textile dyeing and bleaching process wastewater and 5% domestic wastewater. Huffman Finishing Company WWTP utilizes activated sludge to treat wastewater. Treatment consists of the following components: vibrating screen, flow equalization basin with four floating aerators, lift pumps, oxidation ditch, circular clarifier, sludge recirculation pumps, chlorine contact tank, ultrasonic flow measurement, chemical dechlorination, cascade post aeration, aerobic sludge digester, sludge holding lagoon, sludge drying beds, auxiliary power system. The plant is located in Subbasin 03-08-32 and discharges to the Catawba River (Lake Hickory) approximately 2.5 miles below Rhodhiss Dam. This segment of the Catawba River is a class WS-IV, B; CA waterbody. The receiving stream is not listed on the 2014 303(d) list as impaired. The outfall is approximately one mile upstream from the water supply intake for the City of Hickory. NPDES Permit Fact Sheet — 03/29/ 16 Page 2 Huffman Finishing NCO025135 Current Effluent Characteristics The Huffman Finishing Company WWTP's average flow was 0.035 MGD during the calendar year of 2014, which represents 14% of permitted flow. In 2014, the monthly average flows ranged from 0.029 MGD to 0.044 MGD. Table 1. Lists average and maximum effluent. data collected from 1/2012 through 9/2015. Parameter Flow BOD5 COD Total Suspended Solids Ammonia Nitrogen Total Nitrogen Total Phosphorus (MGD) (lbs/day) (lbs/day) (lbs/day) (mg/L) (mg/L) (mg/L) average 0.043 1.39 27.90 36.47 0.27 21.75 2.61 maximum 0.164 8.68 227.2 238.7 1.64 94.6 5.64 Limit (MA) T 0.25 1 65.9 790.9 1 287.4 Table 1 continued Parameter Total Chromium Sulfides Total Nickel Total Silver Total Antimony Fecal Coliform (lbs/day) (lbs/day) (µg/L) (µg/L) (µg/L) (#/100ml) Average 0.25 0.023 5.34 6 25.93 2.55 maximum 3.97 0.4 9 50 40 95 Limit (MA) 1 1.3 2.6 200/100 ml MA: Monthly Average Evaluation of Compliance Data Discharge Monitoring Reports (DMRs) have been reviewed for the period of January 2010 through September 2015. During that time only one pen -nit limit violation was reported: one chromium daily maximum limit violation (08/13/2012), which proceeded to a NOV. The most recent inspection was conducted on January 7, 2016. Linda Wiggs of ARO with staff from the NPDES Complex Permitting Unit inspected the treatment plant as well as the discharge outfall. Inspectors were informed that the EQ Basin float would not automatically trigger level control; instead, the level control is designed with manual operation. A properly certified back-up ORC was also reported to the ARO as required in the 2014 inspection report. At the discharge point, blue/purple color could be seen around the Outfall but appeared to mix with the river 2 feet away from the discharge point. Two inspections performed in 2014 and 2012 showed the facility was in compliance with the permit. The 2010 inspection found that wastewater was leaking from the clarifier prior to entering the chlorine contact tank. This issue was not reported in 2012 inspection. Toxicity Testing. Since January 2010 the facility has passed 20 of 20 chronic toxicity tests (Ceriodaphnia @ 0.96%). Evaluation of Instream Data Instream monitoring is not required for this discharge. Development of Effluent Guidelines Applicable effluent guidelines are listed in 40 CFR 410.52 Textile Mills Subpart E, Knit Fabric. Huffman Finishing Company was able to provide five years of yearly average product production (in lbs/day). The averages were: 27,027 lbs/day in 2011, 25,833 lbs/day in 2012, 25,112 lbs/day in 2013, 25,904 lbs/day in 2014, and 26,009 lbs/day in 2015. Since the highest yearly average (27,027 lbs/day) was determined not to be an outlier (greater than 20% of long term average), that value was used to NPDP-S Permit Fact Sheet — 03/29/ 16 Page 3 Huffman Finishing NCO025135 calculate the Technology Based Effluent Limitations (TBELs). Table 2 summarizes the proposed limit development based on the federal effluent guidelines. For example, the BOD5 daily maximum limits in lbs per day = 5.0 (pounds per 1000 pounds of product) * 27,027 (lbs/day) / 1000 = 135.1 lbs/day. Table 2: Technology Based Effluent Limitations Calculation Highest yearly average production 4 27,027 lbs/day Pollutant BPT limitations (pounds per 1000 pounds ofproduct) Calculated Limits (lbs/da Daily Maximum Monthly Average Daily Max Monthly Average BOD5 5.0 2.5 135.1 67.6 COD 60.0 30.0 1621.6 810.8 TSS 21.8 10.9 589.2 294.6 Sulfide 0.20 0.10 5.4 2.7 Phenols 0.10 0.05 2.7 1.4 Total Chromium 0.10 0.05 2.7 1.4 H 6.0 - 9.0 s.u. Huffman Finishing Company also has 5% sanitary wastewater which could allow for extra allocations for BOD and TSS; however, these additions were minor and were not added in this permit renewal. Reasonable Potential (RP) Analysis The Division conducted EPA recommended analyses to determine the reasonable potential for toxicants to be discharged by this facility, based on DMR data from January 2012 through September 2015 and EPA 2C Form submitted with the permit renewal application. No limit or Monitoring: The following parameters will not receive a limit or monitoring, since they did not demonstrate reasonable potential to exceed applicable water quality standards/criteria and the maximum predicted concentration was < 50% of the allowable concentration: copper, cyanide, nickel, zinc, and antimony. Note the data sets analyzed for copper, cyanide, and zinc were limited (< 8 samples). Monitoring Only: Effluent samples for silver showed 44 samples < 5 ug/L and 1 sample < 50 ug/L. The Huffman Finishing WWTP's chronic allowable allocation for silver is 6.25 ug/L. In accordance with NC Administrative Code Section 15A NCAC 02B .0500, all test procedures must produce detection and reporting levels that are below the permit discharge requirements and all data generated must be reported to the approved detection level or lower reporting level of the procedure. DWR's Water Sciences Section has determined that the Practical Quantitation Limit (PQL) for silver is 1 ug/L. The Permittee will be notified in the permit cover letter to confirm that the certified laboratory performing the facility's metals analysis can measure to the approved detection level or lower reporting level and that a list of PQL's determined by the Division can be found at the following website: http://portal.ncdenr.ora/web/wq/lab/ops/inorg. The monitoring requirement for silver is maintained in the permit renewal with a reduced monitoring frequency of quarterly. NPDES Permit Fact Sheet — 03/29/ 16 Page 4 Huffman Finishing NCO025135 • Effluent Limit with Monitoring: Effluent samples for total phenolic compounds showed no potential to violate water quality standards and the maximum predicted concentrations were all less than 50% of the allowable allocations. Limitations for total phenols are based on EPA technology based effluent limits (TBEL) for Textile Mills, 40 CFR 410.52 as discussed above and must be maintained in the permit. In addition, effluent samples for chlorinated phenols were also analyzed since the receiving stream is classified as WS-IV and the state has a Water Supply total chlorinated phenolic compounds water quality standard of 1 ug/L. Chlorinated phenolic compounds reported included: 2-chlorophenol, 2,4— dichlorophenol, 2,4,6-trichlorophenol, 4-chloro-3-methylphenol, and pentachlorophenol which were all below detection limits. Therefore, it was not necessary to limit chlorinated phenolic compounds in the permit. Comparison of TBEL and WQBEL A comparison table of proposed technology based effluent limits (TBELs) and water quality based effluent limits (WQBELs) is showed in Table 3. For parameters subject to both TBELs and WQBELs, the more stringent limit shall be applied. In order to compare both effluent limits, the concentration based limits (water quality limits) have been converted to the mass based limits using a permitted flow of 0.25 MGD. As shown in the Table 3, bolded parameter limits are more stringent limits and they will be applied in the permit renewal. Table 3: Comparison of TBEL and QWBEL TBEL (lbs/da) WQBEL m /L WQBEL lbs/da ) Parameter Daily Maximum Monthly Average Daily Maximum . Monthly Average Daily Maximum Monthly Average BOD5 135.1 67.6 - - - - COD 1621.6 810.8 - - - - TSS 589.2 294.6 - - - - Sulfide 5.4 2.7 - - - - Phenols 2.7 1.4 - 31.3 - 65.3 Total Chromium 2.7 1.4 87.7 5.21 182.8 10.9 , Fecal Colifonn - - 400# /100 mL 200# /100 mL - - TRC - - 28 u /L - - - pH 6.0 - 9.0 s.u. Mercury TMDL Evaluation As required, the Permittee performed a low level effluent mercury test on 4/3/2014 for submittal with the permit renewal application. In accordance with the 2012 Mercury TMDL NPDES Guidance the permittee needs to show annual mean effluent concentrations below both the Water Quality Based Effluent Limitation (WQBEL) of 1250 ng/L and the Technology Based Effluent Limitation (TBEL) of 47 ng/L. The effluent sample (19 ng/L) was below both the WQBEL and the TBEL, therefore, no NPDkS Permit Fact Sheet — 03/29/ 16 age 5 Huffman Finishing NCO025135 mercury limitation is required. Guidance for industrial wastewater treatment facilities does not require a Mercury Minimization Plan if no limitation is needed. The permittee will be required to continue monitoring mercury as part of its permit renewal, using EPA method 1631 E. Basis for Permit Effluent Limits PARAMETER LIMITS RATIONALE FOR LIMITATION Monthly Average Daily Maximum Flow 0.250 MGD 15A NCAC 02B .0400 et seq., 02B .0500 et seq. BOD, 5 day, 20°C 67.6 pounds/day 135.1 pounds/day 40 CFR 410.52; Production Amount* Total Suspended Solids 294.6 pounds/day 589.2 pounds/day 40 CFR 410.52; Production Amount* COD - 810.8 pounds/day 1621.6 pounds/day 40 CFR 410.52; Production Amount* Fecal Coliform (geometric mean) 200/100 mL 400/100mL Administrative Code 15A NCAC 02B .0211 pH > 6.0 and < 9.0 standard units — — 40 CFR 410.52; Administrative Code 15A NCAC 02B .0211 Temperature Administrative Code 15A NCAC 02B .0508 Total Chromium 1.4 pounds/day 2.7 pounds/day 40 CFR 410.52; Production Amount* Sulfides 2.7 pounds/day 5.4 pounds/day 40 CFR 410.52; Production Amount* Phenols 1.4 pounds/day 2.7 pounds/day 40 CFR 410.52; Production Amount* Total Residual Chlorine 28 µg/L Administrative Code 15A NCAC 02B .0211 Total Silver Administrative Code 15ANCAC 02B :0211; BPJ NH3 as N Administrative Code 15A NCAC 02B .0508; BPJ Total Nitrogen (NO2 + NO3 + TKN) Administrative Code 15A NCAC 02B .0508 Total Phosphorus Administrative Code 15A NCAC 02B .0508 Chronic Toxicity Administrative Code 15A NCAC 02B .0200 et seq. *Production Amount — 27,027 lbs/day Summary of Proposed Changes The following permit changes are proposed for this permit renewal: 1. Addition of electronic DMR requirement. 2. Update effluent limitations requirements for BOD5, TSS, COD, total chromium, sulfide, and phenol based on updated production amount. 3. Changed sampling type for effluent TSS as composite. 4. Reduced monitoring requirements for BOD5, TSS, COD, fecal coliform, pH, and temperature to 2/week. NPDES Permit Fact Sheet - 03/29/ 16 Huffman Finishing Page 6 NCO025135 5. Removal of limitations and monitoring requirements for nickel and antimony. 6. Reduced monitoring requirements for silver to quarterly. 7. Reduced monitoring requirements for total nitrogen and total phosphorus to quarterly. 8. Addition of revised Toxicity testing language. Proposed Schedule of Permit Issuance Draft Permit to Public Notice: Feb 10, 2016 (estimate) Permit Scheduled to Issue: April 4, 2016 (estimate) NPDES Division Contact If you have questions regarding any of the above information or on the attached permit, please contact Yang Song at (919) 807-6479 or by email at yang song_amcdenr. og_v. NAME: DATE: Comments No comments were received from EPA Region IV or the Asheville Regional Office - Water Quality Program. Song, Yang From: Heim, Tim Sent: Monday, February 29, 2016 10:46 AM To: Song, Yang Subject: FW: Draft Permit Renewal for the Huffman Finishing Company WWTP - NCO025135 Yang, I can't remember if I send this already, but it's good to go. Tim Heim, P.E. Environmental Engineer —Asheville Regional Office Water Quality Regional Operations Section NCDEQ — Division of Water Resources 828 296 4500 office email: tim.heim(cbncdenr.gov 2090 U.S. Hwy. 70 Swannanoa, N.C. 28778 Nothing Compares_-.,.. t -. Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. From: Wiggs, Linda Sent: Tuesday, February 16, 2016 6:14 PM To: Heim, Tim <Tim.Heim@ncdenr.gov> Subject: RE: Draft Permit Renewal for the Huffman Finishing Company WWTP - NCO025135 I have been working with Raleigh on this one for over a year. We also did a joint inspection. They have taken into account all of my comments. Yang did a great job on this one. ARO recommends issuance as drafted. zm& GOrvg Environmental Senior Specialist — Asheville Regional Office Water Quality Regional Operations Section NCDEQ — Division of Water Resources 828 296 4500 office 828 299 7043 fax Email: linda.wigygs(q-)_ncdenr.gov 2090 U.S. Hwy. 70 Swannanoa, N.C. 28778 N-C. Nothing Compares,, Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. From: Heim, Tim Sent: Monday, February 15, 2016 1:04 PM To: Wiggs, Linda <linda.wiggs@ncdenr.gov> Subject: FW: Draft Permit Renewal for the Huffman Finishing Company WWTP - NC0025135 Sent Excelsior when I meant to send this one. Tim Heim, P.E. Environmental Engineer —Asheville Regional Office Water Quality Regional Operations Section NCDEQ — Division of Water Resources 828 296 4500 office email: tim.heim(o)ncdenr.gov 2090 U.S. Hwy. 70 Swannanoa, N.C. 28778 he. Nothing Compares Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. From: Song, Yang Sent: Wednesday, February 10, 2016 6:38 PM To: Heim, Tim <Tim.Heim@ncdenr.gov> Subject: Draft Permit Renewal for the Huffman Finishing Company WWTP - NC0025135 Hello Tim, Enclosed please find the draft permit with the cover letter and factsheet for the Huffman Finishing Company WWTP (NC0025135) for your review. Let me know if you have any questions. Please note the public notice ends on March 18, 2016. Thank you! Yang Song Engineer, NPDES Complex Permitting Unit NCDWR/Water Quality Programs 919-807-6479 512 N. Salisbury Street, Archdale Bldg #925Z, Raleigh, NC 27604 1617 Mail Service Center, Raleigh, NC 27699-1617 Water Resources ENVIRONMENTAL QUALITY February 10, 2016 MEMORANDUM To: Randy Hintz NC DEQ / DWR / Regional Engineer Asheville Regional Office From: Yang Song 919-807-6479 NPDES Unit Subject: Review of Draft NPDES Permit NCO025135 Huffman Finishing Company WWTP Caldwell County PAT MCCRORY Governor DONALD R. VAN DER VAART tiecreiary S. JAY ZIMMERMAN Director Please indicate below your agency's position or viewpoint on the draft permit and return this form by March 18, 2016. If you have any questions on the draft permit, please feel free to contact me at the telephone number shown above. RESPONSE: (Check one) FRIConcur with the issuance of this permit provided the facility is operated and maintained properly, the stated effluent limits are met prior to discharge, and the discharge does not contravene the designated water quality standards. F-1 Concurs with issuance of the above permit, provided the following conditions are met: ❑ Opposes the issuance of the above permit, based on reasons stated below, or attached: Signed a-14a '�'- for Randy Hintz Date: Feb. 26, 2016 State of North Carolina I Environmental Quality I Water Resources 1617 Mail service Center I Raleigh, North Carolina 27699-1617 919 707 9000 Public Noticg North Carolina Environmental Management Commission/NPDES Unit' 1617 Mail Service Center Raleigh, NC 27699-1617 Notice of Intent to Issue a' NPDES Wastewater Permit' The North Carolina Environ- mental Management Commis- sion proposes to issue a NP- DES wastewater discharge permit to the person(s) listed below. Written comments re- garding the proposed permit will be accepted until 30 days after the publish date of this notice. The Director of the NC Division of Water Resources (DWR) may hold a public hear- ing should there be a signific- ant degree of public interest. Please mail comments and/or information requests to DWEI at the above address. Inter- ested persons may visit the DWR at 512 N. Salisbury Street, Raleigh, NC to review information on file. Additional information on NPDES per- mits and this notice may be found on our websita: http.Hportal.nedenr.org/web/wq /swp/ps/npdes/calendar, or by calling (919) 807-6304. Huffman Finishing, Inc. re= quested renewal of permit NC0025135 for Huffman Fin- ishing Company in Caldwell County; this permitted dis- charge is treated industrial wastewater to the Catawba River, in the Catawba River Basin. Feb. 14, 2016 NORTH CAROLINA, CALDWELL COUNTY, AFFIDAVIT OF PUBLICATION Before the undersigned, a Notary Public of said County and State, duly commissioned, qualified, and authorized by law to administer oaths, personally appeared Terese Almquist who being first duly sworn, deposes and says: that she is Publisher of Lenoir Newspapers, Inc., engaged in the publication of a newspaper known as Lenoir News -Topic, published, issued, and entered as second class mail in the City of Lenoir, in said County and State; that she is authorized to make this affidavit and sworn statement; that the notice or other legal advertisement, a true copy of which is attached hereto, was published in Lenoir News - Topic on the following dates FEB. 14 and that the said newspaper in which such notice, paper. document, or legal advertisement was published was, at the time of each and every publication, a newspaper meeting all of the requirements and qualifications of Section 1-597 of the General Statutes of North Carolina and was a qualified newspaper within the meaning of Section 1-597 of the General Statutes of North Carolina. This 14th y of Febru a-��6 U//1, ................................................................................ Sworn to and subscri ed befor me, this 14 day of Feb 2 6. e �aF F N.Pt}idTA:.�Y w. �f%%•%. ..Z7 My Commission SdacptrQs: ............ ....-.........-,e�� Av30 G Huffman Finishing Company WWTP NCO025135 2015 Freshwater RPA - 95% Probability/95% Confidence MAXIMUM DATA POINTS = 58 Qw(MGD)= 0.25 WWTP/WTPCIass. Class II 1Q10S (cfs)= 32.86 IWC% @ IQ10S = 1.165501166 7QIOS (cfs) = 40.00 IWC% @ 7Q10S = 0.95945528 7Q10W (cfs) = NO 7Q10w DATA IWC% @ 7Q10W = N/A 30Q2 (cfs) = 40.00 IWC% @ 30Q2 = 0.95945528 Avg. Stream Flow, QA (cfs) = 40.00 IWC% @ QA = 0.95945528 Receiving Stream: Catawba River (Hickory Lake) Stream Class: WS-IV, B, CA Outfal1 001 Qw = 0.25 MGD PARAMETER STANDARDS & CRITERIA (2) REASONABLE POTENTIAL RESULTS RECOMMENDED ACTION TYPE (1) NC WQS / Applied /z FAV n # Det. Max Pred Cw Allowable Cw Chronic Standard Acute Acute: NO WQS Total Phenolic Compounds NC 300 A(30Q2) u�_I. 38 1 S 22.0 _ _ Chronic: 31,267.7 No RP, Predicted Max < 50% of Allowable Cw - No value> Allowable Cw Monitoring continue with EPA 2C Form requirements Acute: 87,687.6 Chromium NC 50 FW(7QIOs) 1022 uU/L 0 N/A _ _ _ Chronic: 5,211.3 Refer to EPA Textile Effluent Guideline Acute: 626.3 Copper (AL) NC 7 FW(7QIOs) 7.3 a ;l. I 1 69.0 Note: n <_ 9 Default C.V. Chronic: 729.E No RP, Predicted Max <50 % of Allowable Cw - Limited data sc, No value> Allowable Cw Monitoring continue with EPA 2C Form reuirements Acute: 1,887.6 Cyanide NC 5 FW(7QIOs) 22 10 ug/L 1 1 5.0 ___ _ _ _ _ _ _ _ _ Note: n <_ 9 Default C.V. Chronic: 521.1 _ _ _ _ _ _ _ _ No RP, Predicted Max < 50% of Allowable Cw - Limited data set No value > Allowable Cw Monitoring continue with EPA 2C Form reuiqrements Acute: 22,393.8 Nickel NC 25 WS(7Q10s) 261 ug/L 45 12 9.5 ______ ____________ Chronic: 2,605.6 _______ No RP, Predicted Max < 50% of Allowable Cw No value > Allowable Cw Monitoring continue with EPA 2C Form requirements Acute: 105.534 Silver (AL) NC 0.06 FW(7QIOs) 1.23 a<_'). 15 0 NO DETECTS _ _ Chronic: 6.254 No detections. No Monitoring required. Max MDL = 50 Acute: 5,748.6 Zinc (AL) NC 50 FW(7Q10s) 67 ug/L l 1 98.0 _ _ _ -_ _ __ _-_-_-_-_-___-_-___ _ Note: n < 9 Default C.V. Chronic: 5,211.3 No RP; Predicted Max < 50% of Allowable Cw - Limitcd data set No value> Allowable Cw Monitoring continue with EPA 2C Form requirements Acute: NO WQS Antimony NC 5.6 WS(7Q10s) u_rl. 3 58.80000 _ _ _ _ _ _ _ Chronic: 583.66452 _ _ _ _ _ _ _ _ No RP; Predicted Max <50% of Allowable Cw No value> Allowable Cw Monitoring continue with EPA 2C Form requirements Copy of 9595 FRESHWATER RPA2015_4, rpa Page 1 of 1 1/26/2016 REASONABLE POTENTIAL ANALYSIS 7 Total Phenolic Compounds Date Data BDL=1/2DL Results 1 8/1112014 7 7 Std Dev. 2 8/18/2014 17 17 Mean 3 8/25/2014 < 5 2.5 C.V. 4 9/2/2014 < 5 2.5 n 5 9/8/2014 19 19 6 9/15/2014 < 5 2.5 Mult Factor = 7 9/22/2014 12 12 Max. Value 8 9/29/2014 14 14 Max. Pred Cw 9 10/6/2014 < 5 2.5 10 10/13/2014 < 5 2.5 11 10/20/2014 < 5 2.5 12 10/28/2014 9 9 13 11/3/2014 < 5 2.5 14 11/10/2014 < 5 2.5 15 11/17/2014 < 5 2.5 16 11/24/2014 10 10 17 12/1/2014 22 22 18 12/8/2014 19 19 19 12/15/2014 < 5 2.5 20 12/29/2014 < 5 2.5 21 1/5/2015 8 8 22 1/12/2015 < 5 2.5 23 1/19/2015 < 5 2.5 24 1/26/2015 6 6 25 2/2/2015 < 5 2.5 26 2/9/2015 < 5 2.5 27 2/16/2015 12 12 28 2/23/2015 6 6 29 3/2/2015 12 12 30 3/9/2015 < 5 2.5 31 3/16/2015 < 5 2.5 32 3/23/2015 < 5 2.5 33 3/30/2015 < 5 2.5 34 4/6/2015 6 6 35 4/13/2015 < 5 2.5 36 4/20/2015 < 5 2.5 37 4/27/2015 < 5 2.5 38 5/4/2015 < 5 2.5 39 5/11/2015 < 5 2.5 40 5/18/2015 < 5 2.5 41 5/26/2015 < 5, 2.5 42 6/1/2015 < 5 2.5 43 6/8/2015 < 5 2.5 44 6/15/2015 < 5 2.5 45 6/22/2015 < 5 2.5 46 6/29/2015 < 5 2.5 47 7/13/2015 < 5 2.5 48 7/20/2015 < 5 2.5 49 7/27/2015 7 7 50 8/3/2015 < 5 2.5 51 8/10/2015 10 10 52 8/17/2015 < 5 2.5 53 8/24/2015 < 5 2.5 54 9/l/2015 < 5 2.5 55 9/8/2015 < 5 2.5 56 9/14/2015 5 5 57 9/22/2015 < 5 2.5 58 9/28/2015 < 5 2.5 Use"PASTE SPECIAL Values" then "COP . Maximum data.: points = 58 . 4.9327 5.1897 0.9505 58 1.00 22.0 ug/L 22.0 ug/L 8 Date Data 1 6 7 8 9 10 11 12 13- 14 15 16 17 18 19 20 21 22 23 24 25' 26 27 28 29 30 31 32 33 . 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 Chromium BDL=1/2DL Results Std Dev Mean C.V. n Mult Factor = Max. Value Max. Fred Cw Use"PASTE SPECIAL Values" then "COPY" . Maximum data points = 58 NO DATA NO DATA NO DATA 0 N/A N/A ug/L N/A ug/L Copy of 9595 FRESHWATER RPA2015_4, data 2 - 1/26/2016 REASONABLE POTENTIAL ANALYSIS 9 Copper (AL) Us. PASTE SPEC[ /1 Values" then "COPY" 10 Cyanide . Maximum data _ points = 58` Date Data BDL=1/2DL Results Date Data BDL=1/2DL Results 1 4/3/2014 69 69 Std Dev. N/A 1 413/2014 5 5 Std Dev. 2 - Mean 69.0000 2 Mean 3 C.V. 0.0000 3 C.V. 4 n 1 4 IT 5 5 6 Mult Factor = 1.00 6 Mult Factor = 7 Max. Value 69.0 ug/L 7 Max. Value 8 Max. Fred Cw 69.0 ug/L 8 Max. Pred Cw 9 9 10 10 11 11 12 12 13 13 14 14 15 15 16 16 17 17 18 18 19 19 20 20 21 21 22 22 23 23 24 ' 24 25 25 26 26 27 27 28 28 29 29 30 - 30 31 31 32 32 33 33 34 34 35 35 36 36 37 37 38 38 39 39 40 40 41 41 42 42 43 43 44 - 44 45 45 46 46 47 47 48 48 49 49 50 50 51 51 52 52 53 53 54 54 55 55 56 56 57 57 58 58 Use"PASTE SPECIAL Values" then "COPY" . Maximum data points.= 58 - 5.00 0.0000 1 1.00 5.0 ug/L 5.0 ug/L Copy of 9595 FRESHWATER RPA2015_4, data -3- 1/26/2016 REASONABLE POTENTIAL ANALYSIS 15 Use "PASTE SPECI Values" then "COP .. 17 Silver (AL) Use "PASTE SPECIAL Values" then "COPY" Nickel ..:,Maximum data . Maximum data points = 58 points = 58 Date Data BDL=1/2DL Results Date Data BDL=1/2DL Results 1 1/2/2012 < 5 2.5 Std Dev. 1.8600 1 1/2/2012 < 5 2.5 Std Dev. 3.3541 2 2/l/2012 < 5 2.5 Mean 3.5313 2 2/l/2012 < 5 2.5 Mean 3.0000 3 3/6/2012 < 5 2.5 C.V. 0.5267 3 3/6/2012 < 5 2.5 C.V. 1.1180 4 4/4/2012 < 5 2.5 n 45 4 4/4/2012 < 5 2.5 n 45 5 5/1/2012 < 5 2.5 5 5/l/2012 < 5 2.5 6 6/5/2012 < 5 2.5 Mult Factor = 1.06 6 6/5/2012 < 5 2.5 Mult Factor = 1.12 7 7/10/2012 < 5 2.5 Max. Value 9.0 ug/L 7 7/10/2012 < 5 2.5 Max. Value 25.000 ug/L 8 8/1/2012 < 5 2.5 Max. Fred Cw 9.5 ug/L 8 8/1/2012 < 5 2.5 Max. Pred Cw O DETECTS ug/L 9 9/4/2012 8 8 9 9/4/2012 < 5 2.5 10 10/2/2012 5 5 10 10/2/2012 < 5 2.5 11 11/12/2012 6 6 11 11/12/2012 < 5 2.5 12 12/3/2012 < 5 2.5 12 12/3/2012 < 5 2.5 13 1 /2/2013 < 5 2.5 13 1 /212013 < 5 2.5 14 2/4/2013 < 5 2.5 14 2/4/2013 < 5 2.5 15 3/4/2013 < 5 2.5 15 3/4/2013 < 5 2.5 16 4/1/2013 < 5 2.5 16 4/1/2013 < 5 2.5 17 5/7/2013 5 5 17 5/7/2013 < 5 2.5 18 6/3/2013 < 5 2.5 18 6/3/2013 < 5 2.5 19 7/1/2013 < 5 2.5 19 7/l/2013 < 5 2.5 20 8/5/2013 5 5 20 8/5/2013 < 5 2.5 21 9/3/2013 < 5 2.5 21 9/3/2013 < 5 2.5 22 10/1/2013 < 5 2.5 22 10/1/2013 < 5 2.5 23 11/4/2013 < 5 2.5 23 11/4/2013 < 5 2.5 24 12/2/2013 < 5 2.5 24 12/2/2013 < 5 2.5 25 1 /2/2014 < 5 2.5 25 1 /2/2014 < 5 2.5 26 2/3/2014 < 5 2.5 26 2/3/2014 < 5 2.5 27 3/3/2014 < 5 2.5 27 3/3/2014 < 5 2.5 28 4/2/2014 < 5 2.5 28 4/2/2014 < 5 2.5 29 5/5/2014 < 5 2.5 29 5l5/2014 < 5 2.5 30 6/2/2014 < 5 2.5 30 6/2/2014 < 5 2.5 31 7/7/2014 5 5 31 7/7/2014 < 5 2.5 32 8/4/2014 6 6 32 8/4/2014 < 5 2.5 33 9/2/2014 9 9 33 9/2/2014 < 5. 2.5 34 10/6/2014 7 7 34 10/6/2014 < 5 2.5 35 11 /3/2014 7 7 35 11 /3/2014 < 5 2.5 36 12/1/2014 < 5 2.5 36 12/1/2014 < 5 2.5 37 1 /5/2015 < 5 2.5 37 1 /5/2015 < 5 2.5 38 2/2/2015 5.7 5.65 38 2/2/2015 < 5 2.5 39 3/2/2015 7.8 7.76 39 3/2/2015 < 5 2.5 40 4/6/2015 < 5 2.5 40 4/6/2015 < 5 2.5 41 5/4/2015 < 5 2.5 41 5/4/2015 < 50 25 42 6/1/2015 < 5 2.5 42 6/1/2015 < 5 2.5 43 7/l/2015 < 5 2.5 43 7/1/2015 < 5 2.5 44 8/3/2015 < 5 2.5 44 8/3/2015 < 5 2.5 45 9/1/2015 < 5 2.5 45 9/1/2015 < 5 2.5 46 46 47, 47 48 48 49 49 50 50 51 51 52 52 53 53 54 54 55 55 56 56 57 57 58 58 Copy of 9595 FRESHWATER RPA2015_4, data 4- 1 /26/2016 REASONABLE POTENTIAL ANALYSIS 18 Zinc (AL) Date Data BDL=1/2DL Results 1 4/3/2014 98 98 Std Dev. 2 Mean 3 C.V. 4 n 5 6 Mult Factor = 7 Max. Value 8 Max. Pred Cw 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51_ 52 53 54 55 56 57 58 "PASTE SPECIAL jes" then "COPY" Maximum data points = 58 98.0000 0.0000 1 1.00 98.0 ug/L 98.0 ug/L 19 [Use -PASTE SPECIAL Antimony Values" then "COPY" . Maximus, data points = 58 Date Data BDL=1/2DL Results IL 1 3/6/2012 < 25 12.5 Std Dev. 8.9918 2 6/5/2012 < 25 12.5 Mean 15.9333 3 9/4/2012 36 36 C.V. 0.5643 412/3/2012 < 25 12.5 n 15 5 3/4/2013 < 25 12.5 6 6/3/2013 < 25 12.5 Mult Factor= 1.47 7 9/3/2013 < 25 12.5 Max. Value 40.000000 pg/L 8 12/2/2013 < 25 12.5 Max. Pred Cw 58.800000 pg/L 9 3/3/2014 < 25 12.5 10 6/2/2014 < 25 12.5 11 9/2/2014 40 40 1212/1/2014 < 25 12.5 13 3/2/2015 < 25 12.5 14 6/1/2015 < 25 12.5 15 9/1 /2015 13 13 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 Copy of 9595 FRESHWATER RPA2015_4, data -5- 1 /26/2016 IWC Calculations Facility: Rockingham NC0020427 Prepared By: Yang Song Enter Design Flow (MGD): =40 Enter s7Q10 (cfs): Enter w7Q10 (cfs): Total Residual Chlorine (TRC) Daily Maximum Limit (ug/1) Ammonia (Summer) Monthly Average Limit (mg NH3-N/1) s7Q10 (CFS) 40 s7Q10 (CFS) 40 DESIGN FLOW (MGD) 0.25 DESIGN FLOW (MGD) 0.25 DESIGN FLOW (CFS) 0.3875 DESIGN FLOW (CFS) 0.3875 STREAM STD (UG/L) 17.0 STREAM STD (MG/L) 1.0 Upstream Bkgd (ug/1) 0 Upstream Bkgd (mg/1) 0.22 IWC (%) 0.96 IWC (%) 0.96 Allowable Conc. (ug/1) 1772 Allowable Conc. (mg/1) 81.5 Ammonia (Winter) Monthly Average Limit (mg NH3-N/1) Fecal Coliform w7Q10 (CFS) 40 Monthly Average Limit; 2001100ml DESIGN FLOW (MGD) 0.25 (If DF >331; Monitor) DESIGN FLOW (CFS) 0.3875 (If DF<331; Limit) STREAM STD (MG/L) 1.8 Dilution Factor (DF) 104.23 Upstream Bkgd (mg/1) 0.22 IWC (%) 0.96 Allowable Conc. (mg/1) 164.9 Total Residual Chlorine 1. Cap Daily Max limit at 28 ug/I to protect for acute toxicity Ammonia (as NH3-N) 1. If Allowable Conc > 35 mg/l, Monitor Only 2. Monthly Avg limit x 3 = Weekly Avg limit (Municipals); capped at 35 mg/I 3. Monthly Avg limit x 5 = Daily Max limit (Non-Munis); capped at 35 mg/I 4. BAT for Minor Domestics: 2 mg/I (summer) and 4 mg/I (winter) 5. BAT for Major Municipals: 1 mg/I (year-round) Fecal Coliform 1. Monthly Avg limit x 2 = 400/100 ml = Weekly Avg limit (Municipals) = Daily Max limit (Non -Muni) NPDES Server/Current VersionsfWLA; TB 1/16/2009 Pt. 122, App. E F), and Paperboard from Waste Paper (sub- part E); testing and reporting for the vola- tile, base/neutral and pesticide fractions in the following subcategories: BCT Bleached Kraft (subpart H), Semi -Chemical (subparts B and C), and Nonintegrated -Fine Papers (subpart R); and testing and reporting for the acid, base/neutral, and pesticide fractions in the following subcategories: Fine Bleached Kraft (subpart 1), Dissolving Sulfite Pulp (subpart K), Groundwood-Fine Papers (sub- part O), Market Bleached Kraft (subpart G), Tissue from Wastepaper (subpart T), and Nonintegrated -Tissue Papers (subpart S). 5. Testing and reporting for the base/neu- tral fraction in the Once -Through Cooling Water, Fly Ash and Bottom Ash Transport Water process wastestreams of the Steam Electric Power Plant industrial category. This revision continues these suspensions.]" For the duration of the suspensions, there- fore, Table I effectively reads: TABLE [-TESTING REQUIREMENTS FOR OR- GANIC TOXIC POLLUTANTS BY INDUSTRY CAT- EGORY Industry category GCIMS fraction Vola- Acid Neu- Pes- tile Val ticide Adhesives and sealants .... Aluminum fomring ............. Auto and other laundries ... Battery manufacturing ....... Coal mining ....................... Coil coating ........................ Copper forming .................. Electric and electronic compounds .................... Electroplating ..................... Explosives manufacturing (') V) Foundries ........................... Gum and wood (all sub- parts except D and F) Subpart D--tall oil rosin .... (+) (+) (+) Subpart F--rosin-based derivatives ...................... Inorganic chemicals manu- facturing ......................... Iron and steel manufac- luring.............................. Leather tanning and fin- ishing.............................. Mechanical products man- ufacturing ....................... (') (') (') Nonferrous metals manu- facturing ......................... (') (') (') (') Ore mining (applies to the base and precious met- aWSubpart B) ................ (+) Organic chemicals manu- facturing ......................... Paint and ink formulation Pesticides .......................... Petroleum refining ............. (1) 40 CFR Ch. 1 (7-1-00 Edition) TABLE I —TESTING REQUIREMENTS FOR OR- GANIC TOXIC POLLUTANTS BY INDUSTRY CAT- EGORY —Continued Industry category GC/MS fraction 2 Vola- Acid Neu- Pes- tile tral ticide Phannaceuticalprepara- tions............................... Photographic equipment and supplies ................... Plastic and synthetic mate- rials manufacturing Plastic processing ............. (+) Porcelain enameling .......... Printing and publishing ...... Pulp and paperboard mills —see footnote ...... Rubber processing ............ Soap and detergent manu- facturing ......................... Steam electric power plants............................. Textile mills (Subpart C— Greige Mills are exempt from this table) ............... Timber products proc- essing ............................. +Testing required. 2The pollutants in each fraction are listed in Item V- C. 3 Pulp and Paperboard Mills: .Subpart 3 GS/MS fractions Base/ Pes- VOA Acid neu- ticides tral A......................... 2 (') 2 (') B ........ .... .........."' 2 (1) 2 2 C .:........ ............... 2 (1) 2 2 D......................... 2 (1) 2 2 E ......................... (') (') 2 (') F ......... .......:........ (') (') 2 2 G ......................... (,) (1) 2 2 H ......................... (+) (1) 2 2 .I ...................... ..... (1) (1) 2 2 i .......................... (') (') (') 2 K......................... (1) (1) 2 2 L .......................... (7) (1) 2 2 M......................... (,) (,) 2 2 N......................... (1) (1) 2 2 O ......................... (1) • (1) 2 2 (') (1) 2 2 Q .........................(') (') 2 (') R......................... 2 (1) 2 2 S ......................... (') (') 2 (') T ......................... (') (') 2 (') U ......................... (') (') (') 2 + Must test. 2 Do not test unless "reason to believe" it is discharged. 3 Subparts are defined in 40 CFR Part 430. [48 FR 14153,' Apr. i; 1983, as amended at 49 FR 38050, Sept. 26, 1984; 50 FR 6940, Feb. 19, 19851 - `Editorial Note: The words "This revision" refer to the document published at 48 FR 14153, Apr. 1, 1983. 976 permit Information — ❑ X 1'� Permit Information Send to Notice NO Reset j Owner Information Permit Number NC0025135 Owner Huffman Finishing, Inc. Mailling Address Line 1 P.O. Box 170 Mailing Address Line 2 City Granite Falls State NC Zip 28630 Notice Language - Paper Huffman Finishing, Inc. requested renewal of permit NC0025135 foi is treated industrial wastewater to the Catawba River, in the Catawl Permit Writer Yang.Song Facility Information Facility Huffman Finishing Company County Caldwell Facility Type Industrial Process & Commercial Permitted Flow 250000 Receiving Stream CATAWBA RIVER (Lake Hickory) Subbasin 30832 Region Office Asheville Huffman Finishing -a River Basin. Find Permit in Caldwell County; this permitted discharge Notice Language - Website Huffman Finishing, Inc.( P.O. Box 170 Granite Falls, NC 28630] has requested renewal of permit NC0025135 for its wTP in Caldwell county. This permitted facility discharges treated inductrial wastewater to the Catawba River in the Catawba River Basin. Currently, some parameters are water quality limited. This discharge may affect future allocations in this segment of the Catawba River. Record: 11 4 201 of 1616 ► ► ► Uniiftered 1. 1.1 APPENDIX A TO PART 136 METHODS FOR ORGANIC CHEMICAL ANALYSIS OF MUNICIPAL AND INDUSTRIAL WASTEWATER METHOD 624—PURGEABLES Scope and Application This method covers the determination of a number of purgeable organics. The following parameters may be determined by this method: Parameter STORET No. CAS No. / V Benzene ...................................... 34030 71-43-2 \/$romodichloromethane .......................... 32101 75-27-4 \f Bromoform................................... 32104 75-25-2 r,/'Bromomethane................................ 34413 74-83-9 /Carbon tetrachloride ............................ 32102 56-23-5 �,. Chlorobenzene................................ 34301 108-90-7 Chloroethane.................................. 34311 75-00-3 \./2-Chloroethylvinyl ether ......................... 34576 110-75-8 ✓l,hloroform ................................... 32106 67-66-3 Chloromethane ........ • • • . • • ....... • • • ... • .. 34418 74-87-3 Dibromochloromethane .......................... 32105 124-48-1 1,2-Dichlorobenzene ............................ 34536 95-50-1 1,3-Dichlorobenzene ............................ 34566 541-73-1 1,4-Dichlorobenzene ............................ 34571 106-46-7 V 1,1-Dichloroethane .............................. 34496 -, 75-34-3 1,2-Dichloroethane .............................. 34531 107-06-2 1,1-Dichloroetha?j. ......................... 34501 75-35-4 V trans-1,2-Dichloroethene ......................... 34546 156-60-5 1,2-Dichloropropane ............................ 34541 78-87-5 cis-1,3-Dichloropropene .......................... 34704 10061-01-5 trans-1,3-Dichloropropene ........................ 34699 10061-02-6 \,/'Ethyl benzene ................................. 34371 100-41-4 \AAethylene chloride ............................. 34423 75-09-2 1,1,2,2-Tetrachloroethane ......................... 34516 79-34-5 Tetrachloroethene .............................. 34475 127-18-4 Toluene ...................................... 34010 108-98-3 1,1,1-Trichloroethene ............................ 34506 71-55-6 �/1,1,2-Trichloroethene ............................ 34511 79-00-5 Trichloroethane................................ 39180 79-01-6 .�" Trichlorofluoromethane .......................... 34488 75-69-4 Vinyl chloride ................................. 39175 75-01-4 1.2 The method may be extended to screen samples for acrolein (STORET No. 34210, CAS No. 107-02-8) and acrylonitrile (STORET No. 34215, CAS No. 107-13-1), however, the preferred method for these two compounds is Method 603. 6, S Mee el f 11. McNair, N.M. and Bonelli, E.J. "Basic Chromatography," Consolidated Printing, Berkeley, California, p. 52, 1969. 12. Burke, J.A. "Gas Chromatography for Pesticide Residue Analysis; Some Practical Aspects," Journal of the Association of Official Analytical Chemists, 48, 1037 (1965). 13. Olynyk, P., Budde, W.L. and Eichelberger, J.W. "Method Detection Limit for Methods 624 and 625," Unpublished report, May 14, 1980. 14. "EPA Method Study 30, Method 625, Base/Neutrals, Acids, and Pesticides," EPA 600/4-84-053, National Technical Information Service, P1384-206572, Springfield, Virginia 22161, June 1984. Table 1—Base/Neutral Extractables Parameter I STORET No. I CAS No. cenap t ene...................................... \,/ Acenaphthylene.................................... \,/Anthracene........................................ Aldrin............................................ � / Benzo(a)anthracene.................................. �'/Benzo(b)fluoranthene................................ `,,,/Benzo(k)fluoranthene................................ Benzo(a)pyrene..................................... �I Benzo(ghi)perylene.................................. �Aenzyl butyl phthalate ............................... R-BHC............................................ S-BHC............................................ \✓Bis(2-chloroethyl)ether ................................ V Bis (2-chloroethoxy) methane ............................ �Bis(2-ethylhexyl)phthalate ............................. Bis(2-chloroisopropyl)ethera ............................ �/4-13romophenyl phenyl ethers .......................... Chlordane ......................................... V 2-Chloronaphthalele................................. `, - 4-Chlorophenyl phenyl ether .......................... . \_/Chrysene.......................................... 4,4'-DDD.......................................... 4,4'-DDE.......................................... 4,4'-DDT........................................ Dibenzo(a,h)anthracene ............................... \./Di-n-butylphthalate.................................. \,/1,3-Dichlorobenzene................................. V1,2-Dichlorobenzene................................. ,:,./1,4-Dichlorobenzene......................... .... I... I, * 3,3'-Dichlorobenzidine ................................ Dieldrin........................................... . Diethyl phthalate .................................... VDimethyl phthalate ............................... I . . \,A,4-Dinitrotoluene................................... 34GU5 83-3G-9 34200 208-96-8 34220 120-12-7 39330 309-00-2 34526 56-55-3 34230 205-99-2 34242 207-08-9 34247 50-32-8 _ 34521 191-24-2 34292 85-68-7 39338 319-85-7 34259 319-86-8 34273 111-44-4 34278 111-91-1 39100 117-81-7 34283 108-60-1 34636 101-55-3 39350 57-74-9 34581 91-58-7 34641 7005-72-3 34320 218-01-9 39310 72-54-8 39320 72-55-9 39300 50-29-3 34556 53-70-3 39110 84-74-2 34566 541-73-1 34536 95-50-1 34571 106-46-7 34631 91-94-1 39380 60-57-1 34336 84-66-2 34341 131-11-3 34611 121-14-2 Table 1—Base/Neutral Extractables Parameter STORET No. CAS No. - initroto uene ................. 34626 6 -2 -2 Di-n-octylphthalate.................................. 34596 117-84-0 Endosulfan sulfate ................................... 34351 1031-07-8 Endrin aldehyde .................................... 34366 7421-93-4 Fluoranthene ........................................ 34376 206-44-0 Fluorene.......................................... 34381 86-73-7 Heptachlor ........................................ 39410 76-44-8 Heptchlor epoxide ................................... 39420 1024-57-3 Hexachlorobenzene.................................. 39700 118-7.4-1- Hexachlorobutadiene................................. 34391 - 87-68-3 Hexachloroethane................................... 34396 67-72-1 ndeno(1,2,3-cd)pyrene ............................... 34403 193-39-5 'Isophorone........................................ 34408 78-59-1 \_/Naphthalene ....................................... 34696 91-20-3 \,/*Nitrobenzene ....................................... 34447 98-95-3 \,^-Nitrosodi-n-propylamine ............................ 34428 621-64-7 PCB-1016.......................................... 34671 12674-11-2 PCB-1221.......................................... 39488 11104-28-2 PCB-1232.......................................... 39492 11141-16-5 PCB-1242.......................................... 39496 53469-21-9 PCB-1248.......................................... 39500 12672-29-6 PCB-1254.......................................... 39504 11097-69-1 PCB-1260.......................................... 39508 11096-82-5 Phenanthrene...................................... 34461 85-01-8 /Pyrene............................................ 34469 129-00-0 Toxaphene.......................................... 39400 8001-35-2 1,2,4-Trichlorobenzene................................ 34551 120-82-1 aThe proper chemical name is 2,2'-oxybis(1-chloropropane). Table 2--Acid Extractables Parameter STORET No. CAS No. 4-Chloro-3-methylphenol ............................. 34452 59-50-7 U°2-Chlorophenol..................................... 34586 95-57-8 � /- 2,4-Dichlorophenol................................. 34601 120-83-2 \L,4-Dimethylphenol................................. 34606 34616 105-67-9 51-28-5 \_/2,4-Dinitrophenol.................................. 2-Methyl-4,6-dinitrophenol ........................... 34657 534-52-1 2-Nitrophenol..................................... 34591 88-75-5 4-Nitrophenol..................................... 34646 100-02-7 ,:/Pentachlorophenol.................................. 39032 87-86-5 Phenol ........................................... 34694 108-95-2 ` ,,2,4,6-Trichlorophenol................................ 34621 88-06-2 M. Table 3—Additional Extractable Parameters' Parameter STORET No. CAS No. Method IBenzidine................................... 39120 92-87-5 605 R-BHC...................................... 39337 319-84-6 608 S-BHC...................................... 39340 58-89-8 608 Endosulfan I ................................. 34361 959-98-8 608 Endosulfan II ................................ 34356 33213-65-9 608 Endrin ........ ............................... 39390 72-20-8 608 Hexachlorocylopentadiene ....................... 34386 77-47-4 612 N-Nitrosodimethylamine ........................ 34438 6Z-75=9 607 ' J-Nitrosodiphenylamine ........................ 34433 86-30-6 607 'See Section 1.2. Table 4—Chromatographic Conditions, Method Detection Limits, and Characteristic Masses for Base/Neutral Extractables` Reten- ethod Charactesti masses ` Parameter tion detec- deter- tion Electronirnpact Chemical ionization ti (min)()lg limit ) /L.. Primaryar e'con -Second- ethane Methane ethane �"" Y ar Y 1,3-Dichlorobenzene 7.4 01111'9J ,,, 148 113 M 1 1,4-Dichlorobenzene 7,8 4.4 146 148 113 146 148 150 Hexachloroethane .... 8.4 1.6 117 201 199 199 201 203 Bis(2-chloroethyl) ,,.��° ether' ...... rim'.... 8.4 5.7 93 63 95 63 107 109 1,2-Dichlorobdnzene 8.4 1.9 146 148 1,1i3 146 148 150 Bis (2-chloroisopropyl) ether' .............. 9.3 5.7 45 77 79 77 135 137 N-Nitrosodi-n- propylamine ........ .... .... 130 42 101 .... .... I Grayb, Julie From: Belnick, Tom Sent: Tuesday, October 20, 2015 6:33 PM To: Belnick, Tom; Berry, Ron; Chernikov, Sergei; Davis, Timothy B; Grzyb, Julie; Rodriguez, Teresa; Song, Yang Subject: Fact Sheet/RPA Results I'm offering the following verbage as one way to write up RPA results in a Fact Sheet in a clear/concise manner. Based on the EPA audit recommendations, we will need to upgrade our Fact Sheet template down the road, and have a., consistent approach by all permit writers. Reasonable Potential Analysis/Toxicants A reasonable potential analysis was conducted on effluent toxicant data collected between Month 20xx and Month 20xx. Based on this analysis, the following permitting actions are proposed for this permit: • Effluent Limit with Monitoring. The following parameters will receive a water quality -based effluent limit (WQBEL) since they demonstrated a reasonable potential to exceed applicable water quality standards/criteria: Toxicant A, Toxicant B, etc • Monitoring Only. The following parameters will receive a monitor -only requirement since they did not demonstrate reasonable potential to exceed applicable water quality standards/criteria, but the maximum predicted concentration was >50% of the allowable concentration: Toxicant A, Toxicant B, etc. • No Limit or Monitoring: The following parameters will not receive a limit or monitoring, since they did not demonstrate reasonable potential to exceed applicable water quality standards/criteria and the maximum predicted concentration was <50% of the allowable concentration: Toxicant A, Toxicant B, etc. - A spreadsheet of the RPA results is attached to this Fact Sheet. Tom Belnick Supervisor, NPDES Complex Permitting Unit NCDWR/Water Quality Programs 919-807-6390 E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and may be disclosed to third parties Chernikov, Sergei From: Wiggs, Linda Sent: Tuesday, March 24, 2015 4:27 PM To: Chernikov, Sergei Subject: RE: Huffman NC0025135 The TSS is listed in the current permit as a grab sample but should be listed as a composite sample. Thanks Linda Wiggs Linda.Wiggs@ncdenr.gov Environmental Senior Specialist North Carolina Dept. of Environment and Natural Resources Asheville Regional Office Division of Water Resources - Water Quality Regional Operations 2090 U.S. 70 Highway Swannanoa, NC 28778 Tel: 828-296-4500 Fax: 828-299-7043 Link to Division of Water Resources Home Page http://portal.ncdenr.org/web/wq Notice: E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and therefore may be disclosed to third parties. -----Original Message ----- From: Chernikov, Sergei Sent: Tuesday, March 24, 2015 4:25 PM To: Wiggs, Linda Subject: RE: Huffman NC0025135 Linda, What do you mean by TSS grab error? Thank you! Sergei From: Wiggs, Linda Sent: Tuesday, March 24, 2015 2:33 PM To: Chernikov, Sergei Subject: RE: Huffman NC0025135 When you do get to this permit: Please fix the TSS Grab error. Remove manual trash screen. I Add mechanical lint screen. Linda Wiggs Linda.Wiggs@ncdenr.gov Environmental Senior Specialist North Carolina Dept. of Environment and Natural Resources Asheville Regional Office Division of Water Resources - Water Quality Regional Operations 2090 U.S. 70 Highway Swannanoa, NC 28778 Tel: 828-296-4500 Fax: 828-299-7043 Link to Division of Water Resources Home Page http://portal.ncdenr.org/web/wq Notice: E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and therefore may be disclosed to third parties. -----Original Message ----- From: Chernikov, Sergei Sent: Monday, October 20, 2014 4:51 PM To: Wiggs, Linda Subject: RE: Huffman NC0025135 Linda, I have not looked at that permit yet. We are too busy with the coal ash. Thank you! Sergei From: Wiggs, Linda Sent: Monday, October 20, 2014 4:06 PM To: Chernikov, Sergei Subject: Huffman NC0025135 I have not received a request for staff report for the Huffman renewal yet. But I am going out there tomorrow (Tuesday 10/21) for an inspection. I guess the day before at 4:00 is too late to ask you if there is anything you want me to look at ... but I am asking? If there is, reply to this email first thing and I will check my emails before heading out there. Linda Wiggs Linda.Wiggs@ncdenr.gov<mailto:Linda.Wiggs@ncdenr.Bov> Environmental Senior Specialist North Carolina Dept. of Environment and Natural Resources Asheville Regional Office Division of Water Resources - Water Quality Regional Operations 2090 U.S. 70 Highway - 2 04affman dkaAm ifompaV ®at ffive ox 770 tanite Cfaf, Cffotfli Iffatoftna 28630 10, 2074 N.C. DENR/DWQ NPDES Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: Renewal of NPDES Permit NCO025135 Huffman Finishing Company WWTP Granite Falls, Caldwell County RECEIVEDIDENRIDWR JUL 14 2014 Water Quality Permitting Section Attached please find the following items for your review and consideration in renewal of the Subject NPDES Permit number NC0025135. 1. One signed original and two copies of Completed EPA Form 3510-1. 2. One Signed original and two copies of completed EPA application Form 3510-2C. 3. Three (3) copies of the Priority Pollutant Analysis by R&A Laboratories. 4. Three (3) copies of Mercury Analysis by GEL Laboratories LLC. 5. A corrected facility location map. (The map in the current NPDES Permit is incorrect) 6. A narrative description of the Sludge Management Plan. 7. A schematic of water supply and wastewater (Process and Sanitary) flows for Huffman Finishing Company. 8. A flow schematic of the Huffman Finishing Company Wastewater Treatment Plant. If you require additional information to process this permit application or if I can be of any further assistance please let me know. My telephone number is (828) 396-1741, Fax number (828) 396-4235, and email address huffhoslth@aol.com Sincerely,—1 4g-v�' u� Lee T. Huffman Manager Enclosures: ` Pleay. Arint or type in the unshaded areas only /fill-in nrPn.e arP snar.Prl fnrPIMP tvne- i-e-- 12 rhararter.qfinch) For Approved. OMB No. 2040-0086. Approval expires 5-31-92 FORM U.S. ENVIRONMENTAL PROTECTION AGENCY 1. EPA I.D. NUMBER GENERAL INFORMATION. T/A CD F `�%. '�� Consolidated Permits Program ' .1 2 13 1415 GENERAL Read the "General Instructions"before;startin LABEL ITEMS GENERAL INSTRUCTIONS If a preprinted has .been provided, I. EPA I.D. NUMBER .label affix it in the designated space. Review the -information carefully; . if' any of it is Huffman Finishing. Company III. FACILITY NAME ;no ecte . cross through it and enter the correct data in the appropriate fill-in area Post Office Box 'I70.. below. Also, if any of the preprinted data is absent. (the area. to the left.of the label V. FACILITY Granite Falls North Carolina 28630' � space. lists the information itin a that should appear) -please provide it in the proper fill- MAILING LIST 4919 Hickory Boulevard C:ounty):. in.arears) below. If the, label .is co Ipmete. and correct you need. not. complete Items 1 Ili, V, and VI(except VPB which must be . ,Southeast.of Granite. FaIIS; NC completed regardless). Complete all items VI. FACILITY if no label has been proved., Refer to -the LOCATION instruction& for.:idetailed item descriptions and .for he.legal authorization under which this data is collected. -- II. POLLUTANT CHARACTERISTICS. INSTRUCTIONS:. Complete.A through J to determine whether -you, need to submit any permit application. rms to -the EPA. If you.:answer."yes" to any - questions, you must submit this form and the.supplemental,from listed in the parenthesis following the question..Mark "Xin.the.box in the third .column if the supplemental: form is attached. If you. answer "no" to each :question, .you'need not submit- any of these forms; You may: answer "no" if your activity is, excluded from; ermit re uirements` see Section rC of the instructions. See:also-Section D of:the. instructions for definitions ofbold-faced terms. . MARK "X MARK "X" . SPECIFIC QUESTIONS SPECIFIC'QUESTIONS YES . NO FORM YES NO � FORM ATTACHED ATTACHED A. Is this facility a publicly owned treatment works which results in a discharge to waters of the ❑ ® ❑ B. Does: or will. this. facility (either existing or proposed) • .include.. a concentrated, animal ❑ U.S.? (FORM-2A) feeding operation.:, or aquatic animal production facility. which results -in a Aischarge to waters of the U.S.? (FORM 2B) - 16 17 18, 19 20 ' 21 C. Is . this . facility which. rcurrently ; results in ® ❑ ® D. 1s this proposal. facility (other Man those described . ❑ ® El. discharges to waters of. the. U.S. other than in A, or above) which' will result in a discharge 22 23 24 25 zs 27 - those described: in A or B above? FORM 2C ' to waters of the U:S.? FORM 2D E. Does or will this facility'treat, store, or dispose of hazardous wastes? (FORM 3) . ❑ ® ❑ F. Do you or will you inject at this facility industrial or municipal. effluent below. the lowermost.. stratum ❑ ® ❑ containing, within one quarter. mile of the . well bore, underground .sources- of -drinking .water? 28 29 30 31 32 33 FORM 4) G. Do you or will you inject at this facility any H. .Do you orwill you inject at this facility Fluids for d produced water other fluids which ,are brought to the surface in connection with conventional oil or ❑ ® ElFrasch special processes such as mining of sulfer by the process solution mining of minerals, in ❑ ® ❑ natural gas production, inject fluids used for situ combustionof fossil fuel, or recovery of enhanced recovery of oil or natural gas, or inject . geothermal energy? (FORM 4) fluids for storage of. liquid. hydrocarbons? 34 35 36 37 1 38 1 39 FORM 4 I. Is this facility 'a. proposed stationary.. source J:.. Is this - facility a proposed stationary source. which is one of the 28 industrial categories- listed ❑ which .is NOT, one of.'the:28 industrial categories ® ❑ .which ❑ Z ❑ in the' instructions. and. which will potentially emit listed in the,instruetions and will. potentially 100 tons per year of any air pollutant regulated. emit 250 .tons per year. of any-.. air. pollutant under the Clean Air Act and may affect or be. regulated under the.Clean.AirAct;and may.affect located in an attainment area?' FORM 5 40 41 42 or be Iodated,.inanattainment are? FORM 5 43'- 44 45 III. NAME OF FACILITY ' SKIP Huffman Finishing Company WWTP 4 15 16-29 30 _ _. ' 69 . IV. FACILITY' CONTACT. A. NAME & TITLE last first, & title): - .B. PHONE area code & no. . c Lee Huffman, Manager ' 828 396 1741 46' 48 49 - 51-1 1 52 55'' 2 15 .16 45 V.' FACILITY MAILING ADDRESS' A. STREET OR P.O. BOX . ... D. ZIP CODE 28630 ' Post Office Box 170 3 15 16 45 B. CITY OR TOWN C. STATE a Granite Falls NC 15 16 40 41 42 47 51 ., V1. FACILITY LOCATION -A. STREET, ROUTE NO. OR:OTHER SPECIFIC IDENTIFIER' c 4919 Hickory Boulevard, Southeast of Granite Falls, NC 5 15 1 16 45 B.,000NTY •NAME Caldwell 46 70 C. CITY OR TOWN D. STATE E: ZIP CODE. F. COUNTY CODE c Granite Falls NC 28630 s 15 1 16 40 41 42 47 - 51 52 54' EPA FORM 3510-1 (8-90) CONTINUED ON REVERSE L CONAUFD FROM THE FRONT VII. SIC CODES 4-di it,.in orderofpriority) . A. FIRST B. SECOND e 2390 (specify) Textile (specify) 5 16 17 5 16 19 . C: THIRD. D. FOURTH 7 (specify) —:_ _, (specify) 5 16 17 15 1. 16 19 Vill. OPERATOWINFORMATION - A. NAME B. Is the name listed in Item c M. Shuford Wise VIII-A also the owner? El YES' ®NO. 8 18 . 19 55 C:`STATUS OF OPERATOR' (Enter the appropriate letterinto the answerbox; if "Other," seci D. PHONE area code & no. F = FEDERAL M = PUBLIC (other than federal or state) P (specify) c 828 396 1741 A 'S = STATE O = OTHER (specify) 56 16 18 19 21 22 25 P =-PRIVATE 15 1. E. STREET OR PO BOX' ' Post Office Box 170 26 56' F. CITY OR TOWN G. STATE H. ZIP CODE IX. INDIAN LAND ' c Granite Falls NC 28630 Is.the facility.located:on Indianlands? 42 42 47 ... 51 E..YES .. :® NO: B 15 16 40... X. EXISTING ENVIRONMENTAL-. PERMITS D. PS D. Air Emissions from Proposed Sources 9 T 8., �15 16 1 17 1 18 30 ' A. NPDES. Dischar es to Surface•Water T I NCO025135 9 15 16 1 17 1 18 30 B. UIC (Underground Injection of Fluids E. OTHER (specify) (Specify) 9 U I9'. 15 16 1 17 1 18 30 15 16 17 18 30 C: RCRA Hazardous Wastes E. OTHER s eci (Specify) C T .I o I .T . 8 , 9 R 9'. . 15 1 16 17 18 . 30j 15J 16. 17 1.18 30 XI. MAP, Attach to tt is. application a.topographic.map of,the area extending to.at least:.one mile beyond.property boundaries.. The map must show the .outline of•.the facility, the location of each'of.its existing and proposed intake:.and. discharge structures; each of its hazardous: waste.freatment, storage,. or. disposal facilities, and each well.where,it, injects fluids -.underground.. Include:all,springs, rivers and; other surface water bodies in the map area. See instructions,for precise re uirements; . . XII. NATURE, OF: BUSINESS (rovide a brief descri tion Bleaching of Cotton and cotton/synthetic socks. Dyeing of cotton and cotton/synthetic socks XIII.-CERTIFICATION see instructions certify underpena/ty:oflaw that / have 'persona//y:examined and,am`familiar;with the:informationsubmitted.in;this application and all attachments and that, based on my. inquiry of those persons immediately.re.sponsible'for obtaining the. i nformation. contained in: the application; 'I believe that information is true; accurate- and.: complete. I am awang that there are significant penalties for submittin false information, including the possibft of firne and imprisonment A. NAME & OFFICIAL TITLE (type or print) B. C. DATE SIGNED FSINATUR Lee T. Huffman, Manager 0711012014 COMMENTS FOR OFFICIAL USE ONLY c 15 16 55 EPA FORM 3510-1 (8-90) 4 1 4- Please orint or tvoe in the unshaded areas only. EPA I.D. NUMBER (copyfrom Item I ofFornt l) Form Approved. OMB No.2040-0086. Approval expires 3-31-98. FORM 2C NPDES U.S. ENVIRONMENTAL PROTECTION AGENCY APPLICATION FOR PERMIT TO DISCHARGE WASTEWATER 4,8/EPA EXISTING MANUFACTURING, COMMERCIAL, MINING AND SILVICULTURE OPERATIONS Consolidated Permits Program I. OUTFALL LOCATION For each ouffall, list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water. A. OUTFALL NUMBER (list) B. LATITUDE C. LONGITUDE D. RECEIVING WATER (name) 1. DEG. 2. MIN. 3. SEC. 1. DEG. 2. MIN. 3. SEC. 001 35.00 45.00 34.00 81.00 23.00 48.00 Catawba River (lake Hickory) Il. FLOWS, SOURCES OF POLLUTION, AND TREATMENT TECHNOLOGIES A. Attach a line drawing showing the water flow through the facility. Indicate sources of intake water, operations contributing wastewater to the effluent, and treatment units labeled to correspond to the more detailed descriptions in Item B. Construct a water balance on the line drawing by showing average flows between intakes, operations, treatment units, and outfalls. If a water balance cannot be determined (e.g., for certain mining activities), provide a pictorial description of the nature and amount of any sources of water and any collection or treatment measures. B. For each outfall, provide a description of: (1) All operations contributing wastewater to the effluent, including process wastewater, sanitary wastewater, cooling water, and storm water runoff; (2) The average flow contributed by each operation; and (3) The treatment received by the wastewater. Continue on additional sheets if necessary. 1. OUT- 2. OPERATION(S) CONTRIBUTING FLOW 3. TREATMENT FALL NO. (list) a. OPERATION (list) b. AVERAGE FLOW (include units) a. DESCRIPTION b. LIST CODES FROM TABLE 2C-1 001 955 Textile Dying .and Finishing 0.250 MGD Scrrening 1-T 55 Domestic Aerated Equalization Tank ' Activated Sludge 3-A Sedimentaion Clarification Chlorine Disinfection 2-F . Dechlorinarion 2-E Cascade Post Aeration Discharge To Surface Water 4-A Aerobic Sludge Digestion 5-A Sludge Holding Lagoon , 5-T Sludge Drying Beds . 5-H OFFICIAL USE ONLY (effluent guidelines sub-calegories) EPA Form 3510-2C (8-90) PAGE 1 of 4 CONTINUE ON REVERSE CONTINUED FROM THE FRONT C. Except for storm runoff, leaks, or spills, are any of the discharges described in Items II -A or B intermittent or seasonal? [:]YES (complete the following lable) .. ® NO (go to:Section 111) 3. FREQUENCY 4. FLOW a. DAYS PER B. TOTAL VOLUME 2. OPERATION(s) WEEK b. MONTHS a. FLOW RATE (in mgd) (speclfvwnh units) 1, LONG TERM 2. MAXIMUM 1. LONG TERM 2. MAXIMUM 1. OUTFALL CONTRIBUTING FLOW (specify PER YEAR C.. DURATION NUMBER(list) (fist) average) (specfivaverage) AVERAGE DAILY AVERAGE DAILY (inda¢i) III. PRODUCTION A. Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Act apply to your facility? © YES (complete Item Ill-B) ❑ NO (go w Section lk) B. Are the limitations in the applicable effluent guideline expressed in terms of production (or other measure of operation)? © YES (complete Item III-C) ❑ NO (go to Section 10 C. If you answered "yes' to Item III-B, list the quantity which represents an actual measurement of your level of production, expressed in the terms and units used in the applicable effluent guideline, and indicate the affected outfalls. 1. AVERAGE DAILY PRODUCTION 2. AFFECTED OUTFACES (list outJall numbers) a. QUANTITY PER DAY b. UNITS OF MEASURE c . OPERATION, PRODUCT, MATERIAL, ETC. (specify) 22,680 1000 lb. Bleaching of cotton/synthetic socks and dyeing of 001 cotton/synthetic socks. IV. IMPROVEMENTS A. Are you now required by any Federal, State or local authority to meet any implementation schedule for the construction, upgrading or operations of wastewater treatment equipment or practices or any other environmental programs which may affect the discharges described in this application? This includes, but is not limited to, permit conditions, administrative or enforcement orders, enforcement compliance schedule letters, stipulations, court orders, and grant or loan conditions. ❑ YES (crnnpleie the fidlowing table) © NO (goa1o71em IV-B) 1. IDENTIFICATION OF CONDITION, 2. AFFECTED OUTFALLS 3. BRIEF DESCRIPTION OF PROJECT 4. FINAL COMPLIANCE DATE AGREEMENT, ETC. a. NO. b. SOURCE OF DISCHARGE a. REQUIRED b. PROJECTED B. OPTIONAL: You may attach additional sheets describing any additional water pollution control programs (or other environmental projects which may affect your discharges) you now have underway or which you plan. Indicate whether each program is now underway or planned, and indicate your actual or planned schedules for construction. ❑ MARK"X" IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED EPA Form 3510-2C (8-90) PAGE 2 of 4 CONTINUE ON PAGE 3 CONTINUED FROM PAGE 2 EPA I.D.r D. NUMBER (convom Item I of(lorm !) V. INTAKE AND EFFLUENT CHARACTERISTICS A, B, & C: See instructions before proceeding —Complete one set of tables for each outfall —Annotate the outfall number in the space provided. NOTE: Tables V-A, V-B, and V-C are included on separate sheets numbered V-1 through V-9. D. Use the space below to list any of the pollutants listed in Table 2c-3 of the instructions, which you know or have reason to believe is discharged or may be discharged from any outfall. For every pollutant you list, briefly describe the reasons you believe it to be present and report any analytical data in your possession. 1. POLLUTANT 2. SOURCE I.POLLUTANT 2. SOURCE VI. POTENTIAL DISCHARGES NOT COVERED BY ANALYSIS or a component of a substance which you below) currently use or manufacture as an intermediate NO (go it) Rem VI-H) or final product or byproduct? Is any pollutant listed in Item V-C a substance El YES (list all such pollulants EPA Form 3510-2C (8-90) PAGE 3 of 4 CONTINUE ON REVERSE CONTINUED FROM THE FRONT VII. BIOLOGICAL TOXICITY TESTING DATA Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in relation to your discharge within the last 3 years? © YES (identify the )estfe) and describe their purposes below) ❑ NO (go io Section VIM Chronic toxicity (ceriodephnia) P/F @ 0.96e, March, June, September, and December for observable inhibition of reproduction or significant mortality to ceriodaphnia dubia at an effluent concentration of 0.96%. Vill. CONTRACT ANALYSIS INFORMATION Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm? YES (list the name, address, and telephone number of,' and pollutants analyzed by, ❑ NO (go to Section IJQ each such laboratory or firm below) A. NAME B.ADDRESS C.TELEPHONE D.POLLUTANTS ANALYZED (area code & no.) (list) 1. Water -Tech Laboratories 5 Pinewood Plaza (828) 396-4444 Total Residual Chlorine, Post Office Box 1056 BOD, COD, Ammonia Nitrogen, Granite Falls, North Carolina 28630 Total Suspended Residue, Fecal Coliform, Total Nitrogen, Total Phosphorus 2. Reearch & Analytical 107 Short Street (336) 996-2841 Total Sulfides, Laboratories Post Office Box 476 Total Phenolics, Kernsville, North Carolina 27284 Total Chromium, Total Nickel, Total Silver, 3. Gel Laboratories 2040 Savage Road (843) 556-8171 Low level Mercury Charleston, South Carolina 29407 ' IX. CERTIFICATION 1 certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. A. NAME & OFFICIAL TITLE (type or print) B. PHONE NO. (area code & no.) Lee T. Huffman Manager (828) 396-1741 C. SIGNATUFj D. DATE SIGNED yd.(, t q4n14__ 07/10/2014 EPA Form 3510-2C (8-90) v V PAGE 4 of 4 PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of this information EPA I.D. NUMBER (copyfrom Item I of Form 1) on separate sheets (use the same format) instead of completing these pages. SEE INSTRUCTIONS. O )TFALL NO. ooi V. INTAKE AND EFFLUENT CHARACTERISTICS (continued from page 3 of Form 2-C)I M PART A -You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details. 3. UNITS 4. INTAKE 2. EFFLUENT (specifyiJ'blank) (optlonal) b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. VALUE a. LONG TERM a. MAXIMUM DAILY VALUE (ifavailable) (ifavailable) AVERAGE VALUE d. NO. OF a. CONCEN- b. NO. OF 1 1 1. POLLUTANT CONCENTRATION (2) MASS CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION (2) MASS ANALYSES a. Biochemical Oxygen 10.2 8.68 2.33 3.99 0.42 1.61 290 MG/L LBS Demand (BOD) b. Chemical Oxygen 175.9 209.9 130.8 76.4 90.6 34.8 290 MG/L LBS Demand (COD) c. Total Organic Carbon (TOC) d. Total Suspended Solids(TSS) 179.5 238.7 173.8 86.9 100.0 38.4 290 MG/L LBS e. Ammonia (asN) 0.62 0.160 0.62 0.160 0.27 0.104 28 MG/L VALUE VALUE VALUE VALUE f.Flow .164 .073 .046 362 MGD g. Temperature VALUE VALUE, VALUE °C VALUE (winter) 17.0 13.9 9.7 138 h. Temperature VALUE VALUE VALUE °C VALUE (summer) 28.6 26.9 21.3 152 MINIMUM MAXIMUM MINIMUM MAXIMUM i• pH 6.1 8.3 6. 1 8. 3 + 290 STANDARD UNITS PART B - Mark "X" in column 2-a for each pollutant you know or have reason to believe is present. Mark "X" in column 2-b for each pollutant you believe to be absent. If you mark column 2a for any pollutant which is limited either directly, or indirectly but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide quantitative data or an explanation of their presence in your discharge. Complete one table for each outfall. See the instructions for additional details and requirements. 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optionaI) 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. VALUE a. LONG TERM AVERAGE AND a b. a. MAXIMUM DAILY VALUE (ifavailable) (ifavailable) VALUE CAS NO. BELIEVED BELIEVED d. NO. OF a. CONCEN- b. NO. OF (1) (1) (1) (1) (ifavailable) PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION (2) MASS ANALYSES a. Bromide (24959-67-9) b. Chlorine, Total �/ <20 <20 <20 115 UG/L Residual /� c. Color X d. Fecal Coliform X 95 17 <1.7 290 #/100ML e. Fluoride \/ X (16984-48-8) f. Nitrate -Nitrite \/ (as M X EPA Form 3510-2C (8-90) PAGE V-1 CONTINUE ON REVERSE ITEM V-B CONTINUED FROM FRONT 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c. LONGTERM AVRG. VALUE a. LONG TERM AND a b a. MAXIMUM DAILY VALUE (ijaeailable) (ijarailable) AVERAGE VALUE CAS NO. BELIEVED BELIEVED d. NO. OF a. CONCEN- b. NO. OF (1) (1) (1) (1) (ifarailable) PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION (2) MASS ANALYSES g. Nitrogen, Total Organic (as 94.60 24.46 94.60 24.46 27.3 10.47 28 MG/L LBS N) h. Oil Grease and Gre Greas <5.6 <5 . 6 <5 .6 1 MG/1 I. Phosphorus \ / (as P),Total X 5.64 1.46 5.64 1.46 2.67 1.02 28 MG/L LBS (7723-14-0) j. Radioactivity (1) Alpha, Total X (2) Beta, Total (3) Radium, Total (4) Radium 226, \/ Total X\ k. Sulfate (as S0,) u (14808-79-8) 1. Sulfide (as S) <0.05 <0.07 <0.06 <0.03 <0.06 <0.02 115 MG/L LBS m. Sulfite (asSO1) (14265A5-3) n. Surfactants X o. Aluminum, Total (7429-90-5) p. Barium, Total (7440-39-3) q. Boron, Total \� (7440-42-8) x r. Cobalt, Total �/ x (7440-48-4) s. Iron, Total �/ x (7439-89.6) t. Magnesium, Total x (7439-95-4) u. Molybdenum, Total (7439-98-7) v. Manganese, Total X (7439-96-5) w. Tin, Total \/ (7440-31-5) X\ x. Titanium, Total (7440-32-6) EPA Form 3510-2C (8-90) PAGE V-2 CONTINUE ON PAGE V-3 I EPA I.D. NUMBER (copyfromitem 1 of Form 1) OUTFALL NUMBER CONTINUED FROM PAGE 3 OF FORM 2-C I 1 001 PART C - If you are a primary industry and this outfall contains process wastewater, refer to Table 2o-2 in the instructions to determine which of the GC/MS fractions you must test for. Mark "X" in column 2-a for all such GC/MS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary industries, nonprocess wastewater outfalls, and nonrequired GC/MS fractions), mark "X" in column 2-b for each pollutant you know or have reason to believe is present. Mark "X" in column 2-c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be discharged in concentrations of 10'ppb or greater. If you mark column 2b for acrolein, acrylonitrile, 2,4 dinitrophenol, or 2-methyl-4, 6 dinitrophenol, you must provide the results of at least one analysis for each of these pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part; please review each carefully. Complete one table (all 7 pages) for each outfall. See instructions for additional details and requirements. 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (option!) 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. a. LONGTERM AND a. b. C. a. MAXIMUM DAILY VALUE (ifavailable) VALUE (tfavailable) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED d. NO. OF a. CONCEN- b. NO. OF (1) (1) (1) (1) r available (f ) REQUIRED PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION (2) MASS ANALYSES METALS, CYANIDE, AND TOTAL PHENOLS 1M.Antimony, Total 36 <25 <25 28 UG/L (7440-36-0) 2M. Arsenic, Total (7440-38-2) 3M. Beryllium, Total (7440-41-7) 4M. Cadmium, Total (7440-43-9) SMal(744Chromium,47- Total (7440-47-3) / ` X 2.840 33.790 1.120 2.776 .634 .243 110 MG/L LBS 6M. Copper, Total (7440-50-8) u 0.069 0.069 0.069 1 MG/L 7M. Lead, Total (7439-92-1) 8M. Mercury, Total 19.0 1 NG/L (7439-97-6) 9M. Nickel, Total 8.0 <5 . 0 <5 . 0 - 28 UG/L (7440-02-0) 10M. Selenium, Total (7782-49-2) 11M. Silver, Total u <5 .0 <5 . 0 <5 . 0 28 UG/L (7440-22-4) 12M. Thallium, Total (7440-28-0) 13M. Zinc, Total 1 MG/L (7440-66-6) .098 14M. Cyanide, X 005 1 MG/1 Total(57-12-5) 15M. Phenols, Total X 16.0 10.8 1.43 115 UG/L DIOXIN 2,3,7,8-Tetra- DESCRIBE RESULTS chlorodibenzo-P- FX I Dioxin (1764-01-6) EPA Form 3510-2C (8-90) PAGE V-3 CONTINUE ON REVERSE CONTINUED FROM THE FRONT 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. a. LONG TERM AND a. b. C. a. MAXIMUM DAILY VALUE (ifavadable) VALUE (ifavailable) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED d. NO. OF a. CONCEN- b. NO. OF (1) (1) (1j (1) available if ) REQUIRED PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION (2) MASS ANALYSES GCIMS FRACTION — VOLATILE COMPOUNDS 1V. Accrolein (107-02-8) 2V. Acrylonitrile v (107-13-1) 3V. Benzene v (71-43-2) t (Chl \ mel med0yn Ether (542-88-1) /X\ 5V. Bromoform (75-25-2) Carbon Tetrachloride Tetrachloride ' X (56-23-5) 7V. Chlorobenzene (108-90-7) bromomethane (124A8-1) /X\ 9V. Chloroethane v (75-00-3) 1 OV. 2-Chloro- ethylvinyl Ether (110-75-8) 11 V. Chloroform (67-66-3) 12V. Dichloro- bromomethane X (75-27-4) 13V. Dichloro- difluoromethane X (75-71-8) 14V. 1,1-Dichloro- ethane (75-34-3) 15V. 1,2-Dichloro- v ethane (107-06-2) 16V. 1,1-Dichloro- �/ x ethylene (75-35.4) 17V. 1,2-Dichloro- propane (78-87-5) 3-Dichloro- ` propylene propyl X (542-75-6) 19V. Ethylbenzene �/ (100-41-4) 20V. Methyl v Bromide (74-83-9) 21 V. Methyl Chloride (74-87-3) EPA Form 3510-2C (8-90) PAGE V-4 CONTINUE ON PAGE V-5 CONTINUED FROM PAGE V-4 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. a. LONG TERM AND a. b. C. a. MAXIMUM DAILY VALUE (ijarailable) VALUE (ijarailable) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED d. NO. OF a. CONCEN- b. NO. OF (1) (1) (1) (ijarailable) REQUIRED PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION (2) MASS ANALYSES GC/MS FRACTION — VOLATILE COMPOUNDS (continued) 22V. Methylene �/ Chloride (75-09-2) Tetrachloroethane 79-34-5 /�(\ 24V. Tetrachloro- ethylene (127-18-4) 25V. Toluene (108-88-.3) 26V. 1,2-Trans- Dichloroethylene ` , X 156-60-5 27V. 1,1,1-Trichloro- v ethane (71-55-6) 28V. 1,1,2-Trichloro- �/ x ethane (79-00-5) 29V Trichloro- �/ x ethylene (79-01-6) 30V. Trichloro- ` Fluoromelhane 75-69-4 /X` 31 V. Vinyl Chloride (75-01-4) GC/MS FRACTION — ACID COMPOUNDS 1A.2-Chlorophenol �/ x (95-57-8) 2A. 2,4-Dichloro- x phenol(120-83-2) 3A. 2,4-Dimethyl- phenol(105-67-9) 4A. 4,6-Dinitro-0- Cresol (534-52-1) 5A. 2,4-Dinitro- �/ phenol (51-28-5) 6A. 2-Nitrophenol (88-75-5) 7A. 4-Nitrophenol �/ x (100-02-7) 8A. P-Chloro-M- Cresol (59-50-7) 9A. Pentachloro- �/ x phenol(87-86-5) 10A. Phenol �/ (108-95-2) 11A. 2,4,6-Trichloro- phenol(88-05-2) EPA Form 3510-2C (8-90) PAGE V-5 CONTINUE ON REVERSE 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (oplionan 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. a. LONG TERM AND b. c. a. MAXIMUM DAILY VALUE (ifarailobleJ I VALUE (ifava/lable) AVERAGE VALUE CAS NUMBER a. TESTING BELIEVED BELIEVED d. NO. OF a. CONCEN- b. NO. OF (1) (1) (1) (1) (ifavailable) REQUIRED PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION (2) MASS ANALYSES GC1MS FRACTION — BASE/NEUTRAL COMPOUNDS 1B. Acenaphthene �/ x (B3-32-9) 28. Acenaphtylene �/ x (208-96-8) 3B. Anthracene �/ x (120-12-7) 4B. Benzidine �/ x (92-87-5) 5B. Benzo (a) Anthracene (56-55-3) 6B. Benzo (a) �/ x Pyrene (50-32-8) 7B. 3,4-Benzo- fluoranthene (205-99-2) 8B. Benzo (ghi) Perylene (191-24-2) 9B. Benzo (k) Fluoranthene X (207-08-9) 10B. Bis (2-Chloro- erhoxy) Methane (111-91-1) 11B. Bis (2-Chloro- erhyo Ether �/ x (111-44-4) 128, Bis (2- Chloroisopropyn Ether (102-80-1) 13B. Bis (2-Erhyl- hexyn Phthalate (117-81-7) 14B. 4-Bromophenyl Phenyl Ether (101-55-3) 158. Butyl Benzyl �/ x Phthalate (85-68-7) 16B. 2-Chloro- naphthalene (91-58-7) 17B. 4-Chloro- phenyl Phenyl Ether (7005-72-3) 18B. Chrysene �/ x (218-01-9) 19B. Dibenzo (a,h) Anthracene X (53-70-3) 20B. 1,2-Dichloro- �/ x benzene (95-50-1) 21 B. 1,3-Di-Chloro- x benzene (541-73-1) /� EPA Form 3510-2C (8-90) PAGE V-6 UUN I INUt UN VAUt: V-1 CONTINUED FROM PAGE V-6 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (opriona� 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c. LONGTERM AVRG. a. LONGTERM AND a. b. c. a. MAXIMUM DAILY VALUE (ifaval/able) VALUE (ifarailable) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED d. NO. OF a. CONCEN- b. NO. OF (1) (1) (1) (1) (rfavailable) REQUIRED PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION (2) MASS ANALYSES GCIMS FRACTION — BASE/NEUTRAL COMPOUNDS (continued) 22B. 1,4-Dichloro- \/ benzene (106-46-7) x 23B. 3,3-Dichloro- benzidine (91-94-1) 24B. Diethyl Phthalate (84-66-2) 25B. Dimelhyl Phthalate (131 -11-3) 26B. Di-N-Butyl Phthalate (84-74-2) 27B. 2,4-Dinilro- toluene (121-14-2) 28B. 2,6-Dinitro- �/ toluene (606-20-2) x 29B. Di-N-Octyl Phthalate (117-84-0) 30B. hydrazine (as Azo- hydr zine(asAzo- benzene)(122-66-7) 31B. Fluoranlhene (206-44-0) 32B. Fluorene (86-73-7) 33B. Hexachloro- �/ benzene(118-74-1) 34B. Hexachloro- v butadiene (87-68-3) 35B. Hexachloro- cyclopentadiene (77-47-4) 36B Hexachloro- ethane (67-72-1) 37B.Indeno (1,2,3-cd) Pyrene (193-39-5) 38B.Isophorone (78-59-1) 39B. Naphthalene (91-20-3) 40B. Nitrobenzene (98-95-3) 41 B. N-Nitro- sodimethylamine (62-75-9) 42B. N-Nitrosodi- N-Propylamine (621-64-7) EPA Form 3510-2C (8-90) PAGE V-7 CONTINUE ON REVERSE G CONTINUED FROM THE FRONT 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optionao 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. a. LONGTERM AND a, b. C. a. MAXIMUM DAILY VALUE (ifavailable) VALUE (ifavailable) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED Q. NO. OF a. GONCEN- b. NO. OF (1) (1) (1) (1) r available rf ) REQUIRED PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION (2) MASS ANALYSES GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (continued) 43B. N-Nitro- sodiphenylamine X (86-30-6) - 44B. Phenanthrene �/ (85-01-8) 45B. Pyrene (129-00-0) 46B. 1,2,4-Tri- chlorobenzene x (120-82-1) /� GC/MS FRACTION — PESTICIDES 1P. Aldrin �/ (309-00-2) 2P. a-BHC (319-84-6) 3P. [l-BHC �/ (319-85-7) x 4P. y-BHC (58-89-9) 5P. 8-BHC �/ (319-86-8) x 6P. Chlordane (57-74-9) 7P. 4,4'-DDT �/ (50-29-3) 8P. 4,4'-DDE (72-55-9) 9P. 4,4'-DDD (72-54-8) 10P. Dieldrin (60-57-1) 11P. a-Enosulfan �/ (115-29-7) /� 12P. a-Endosulfan (115-29-7) 13P. Endosulfan Sulfate (1031-07-8) 14P. Endrin �/ (72-20-8) 15P.Endrin Aldehyde (7421-93-4) 16P. Heptachlor �/ (76-44-8) EPA Form 3510-2C (8-90) PAGE V-8 CONTINUE ON PAGE V-9 EPA I.D. NUMBER (copy from /rem I of Form I) OUTFALL NUMBER CONTINUED FROM PAGE V-8 I 1 001 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. a. LONG TERM AND a. b. C. a. MAXIMUM DAILY VALUE (ifavailable) VALUE (ifarailable) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED d. NO. OF a. CONCEN- b. NO. OF (1) (1) (1) (1) (ifavailable) REQUIRED PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION (2) MASS ANALYSES GC/MS FRACTION — PESTICIDES (continued) 17P. Heptachlor Epoxide (1024-57-3) 18P. PCB-1242 \/ x (53469-21-9) 19P. PCB-1254 \/ (11097-69-1) x 20P. PCB-1221 (11104-28-2) 21 P. PCB-1232 �/ (11141-16-5) x 22P. PCB-1248 v (12672-29-6) 23P. PCB-1260 (11096-82-5) 24P. PCB-1016 (12674-11-2) n 25P.Toxaphene (8001-35-2) EPA Form 3510-2C (8-90) PAGE V-9 wivrKR6TEcH LRDS-Inc. POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. • GRANITE FALLS, NORTH CAROLINA 28630 (828)396-4444 SAMPLE: Huffman Finishing COLLECTION DATE: 4/3/2014 PERMIT #. NCO025135 COLLECTION TIME: 10:00 ADDRESS: Huffman Finishing RECEIVED DATE: 4/3/2014 P.O. Box 170 RECEIVED TIME: 11:20 Granite Falls, NC 28630 REPORTED: 4/25/2014 ANAL:YSI S. ` ANALYSIS EFFLUENT _. UNITS DATE' ANALYST. ppa scan see attached Mercury (low level) see attached NH3 <0.2 mg/L 4/9/14 jrg TDS 3,594 mg/L 4/4/14 lag Oil & Grease <5.6 mg/L 4/14/14 jdg NO2+NO3 8.80 mg/L 4/24/14 jdg TKN 9.52 mg/L 4/24/14 jdg T. Nitrogen 18.32 mg/L 4/24/14 jdg T. Phosphorus 3.10 mg/L 4/24/14 jdg LOG ID: 1404-114 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor i 6, 6 WATER TECH LABORATORIES, ®T®RIES® NCB 5 Pinewood Plaza DR. P.O. Box 1056 Granite Falls, N.C. 28630 (828) 396-4444 CHAIN OF CUSTODY CLIENT: Huffman Finishing Company Wastewater Treatment Plant P.O. Box 170 Granite Falls, N.C. 28630 NPDES# NCO025135 PHONE: (828) 396-1741 TYPE SAMPLE: Wastewater NO. LOCATIONS: 1 SAMPLER NAME: S. Wise Sample Location Facility Name Sample Collection Date Time Temp °C Sample Type Grab/Composite Containers No. Plastic/Glass Analysis Required Effluent 04/03/14 060 3° Composite 4 P PPA Scan Effluent 04/03/14 9 ° Grab 2 P PPA Scan Effluent 04/03/14 13. O Grab 9 G PPA Scan Relinq i he '; Date: 04/03/2014 Time: Receiv` Date_ Time: C[ Relinquished By: Date: Time: ceived 77 Date: Time: Preservation: [X] Cool 4°C-[BOD,TSS] . Conductivity, MBAS, Color Alkalinity Vi,Turbidity [X] Cool 40C - pH<2 w/H2SO4- NH3, NO2-NO3, TKN, Oil & Grease, TOC,[COD], Hardness, Total Phosphorus, Total Phenolics bt] Cool 4°C, pH<2 w/ HNO3 - Metals except Cr, VI [ ] None - Chloride, pH, Fluoride Other: [X] Cool 4°C, Na2S203 - [Coliform, Bacteria] Cool 4°C, pH>12 w/NaOH, 0.6 gm. Ascorbic acid - Cyanide [ ] Cool 4°C, pH>9 w/ NaOH, ZnOAc- Sulfide [� Per Analyzing Lab — Organics Sample Temperature at Lab (°C ) 1' (-.> 130 RESEARCh&ANAtyTICAt :O�tvar e�fQLAbORATORiES, INC. Z� Nc 6 Analytical/Process Consultations l`°�.Yl� g �'1 Chemical Analysis for Selected Parameters and Water Sample Identified as Huffman Finish-PPA Scan (A Water Tech Labs, Inc. Project, collected 03 April 2014) 1. Volatile Organics Quantitation Huffman Finish j]j, Semi -volatile Organics Quantitation Huffman Finish EPA Method 624 Limit PPA Scan Method 625 Limit PPA Scan Parameter (mp/L) (me/L) Parameter (me/L) (ingLL1 �i Metbylene Chloride 0.010 BQL 4-Chloro-3-methylphenol 0.010 BQL Trichlorofluoromethane 0.010 BQL 2-Chlorophenol 0.010 BQL ✓1,1-Dichloroetbene 0.010 BQL 2,4-Dichlorophenol 0.010 BQL ,,/ 1,1-Dichloroethane 0.010 BQL 2,4-Dimethylphenol 0.010 BQL /'Chloroform 0.010 BQL 2,4-Dinitrophenol 0.050 BQL J Carbon Tetrachloride 0.010 BQL 2-MethylA,64initrophenol 0.050 BQL ✓ 1,2-Dichloropropane 0,010 BQL 2-Nitrophenol 0.010 BQL Tnchloroethene 0.010 BQL 4-Nitrophenol 0.050 BQL Dibromochloromethane 0.010 BQL Pentachlorophenol 0.050 BQL v 1,1,2.Tnchioroethane 0.010 BQL Phenol 0.010 SQL \/Tetrachloroethene 0.010 BQL 2,4,6-Trichlorophenol 0.010 BQL v' Cblorobm=c 0.010 BQL Acenaphtbene 0.010 BQL J Trans-l2-Dichlomethene 0.010 BQL Acenaphthylene 0.010 BQL v 1,2-Dichloroethane 0.010 BQL Anthm=e 0.010 BQL v' 1,1,1-Trichloroethane 0.010 BQL Benzidine 0.050 BQL V Bromodichlommethane 0.010 BQL Benzo(a)anduacme 0.010 BQL Cis-1,3-Dichloropropene 0.010 BQL Benzo(a)pyrene 0.010 BQL Benzene 0.010 BQL Benzo(b)fluoranthene 0.010 BQL JTrans-1,3-Dichloropropene 0.010 BQL Benzo(ghi)perylene 0.010 BQL Bromoform 0.010 BQL Benzo(k)fluoranthene 0.010 BQL �1,122-Tarachloroethane 0.010 BQL Bcnzyl butyl phthalate 0.010 BQL Toluene 0.010 BQL Bis(2-chloroethoxy)methane 0.010 BQL Ethyl Benzerre 0.010 BQL Bis(2-chlomethyl)ether 0.010 BQL "Chloromethane M of t y C4,p Olp ; 0( a BQL Bis(2-chlcroisopropyl)ether 0.010 BQL \/Bromomethane M tP-t F j 'Vinyl Chloride 0.010 ,, J �Il" �l BQL BQL Bis(2 ethyl-hexyl)phthalate 4-Bromophenyl phenyl ether 0.010 0,010 BQL 13QL Chloroethane 0.010 BQL 2-Chloronaphthalene 0.010 BQL Total Xylenes 0.010 BQL 4-Chlorophenyl phenyl ether 0.010 BQL Acrolein 0.100 BQL Chrysene 0.010 BQL Acrylonitrile 0.100 BQL Drbenzo(a h)anthracene 0,010 BQL 2-Chloroethyl vinyl ether 0.010 BQL 12-Dichlorobenzene 0.010 BQL 1,3-Dichlorobenzene 0.010 BQL Dilution Factor 1 1,4-Dichlorobenzene 0.010 BQL 3,3-Dichlorobenzidine 0.020 BQL Ouantitation Huffman Finish M-N-Butyl phthalate 0.010 BQL Miscellaneous Limit PPA Scan 24-Dinitrotoluene 0.010 BQL lI. Parameters (rrngJL) m /L 2,6-Dinitrotoluene 0.010 BQL Di-N-Octyl phthalate 0.010 BQL Antimony, Total 0.025 BQL Fluoranthene 0.010 BQL Arsenic, Total 0.005 BQL Hexachloroben=e 0,010 BQL Beryllium, Total 0.001 BQL Hexachlorobutadiene 0.010 BQL Cadmium, Total 0.002 BQL Hexachlorocyclopentadiene 0.010 BQL Chromium, Total O.CO5 0.419 Hexachloroetbane 0.010 BQL Copper, Total 0.005 0.069 Indeno(1,2,3-cd) pyrene 0.010 SQL Lead, Total 0.005 BQL Lsophoroce 0.010 BQL Nickel, Total 0.005 BQL Naphthalene 0.010 BQL Selenium, Total 0.005 BQL Nitrobenzene 0.010 BQL Silver, Total 0.005 BQL N-Nitrosodimethylamine 0.010 BQL Thallium, Total 0.005 BQL N-nitrosodi-n-propylamine 0.010 BQL Zinc, Total 0.010 0.098 N-Nitrosodiphenylamine 0.010 BQL Cyanide 0.005 0.005 Phenanthrene 0.010 BQL Phenols 0.005 BQL Pyrene 0.010 BQL Hardness,Tot 1.00 49.9 1,2,4-Tnchlorobenzene 0.010 BQL Diethyl phthalate 0.010 BQL Dimethyl phthalate 0.010 BQL Fluorene 0.010 BQL Sample Number 782400 12-diphenylhydrazine 0.050 BQL Sample Date 04/03/14 Sample Time (hrs) 1000 Dilution Factor I Sample Number 782400 Sample Date 04/03/14 Sample Time (hrs) 1000 SQL - Below Quantitahon Limits mg/L - milligrams per Liter - parts per million (ppm) GEL LABORATORIES LLC m 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Water Tech Laboratories Address : P.O. Box 1056 Granite Falls, North Carolina 28630 Contact: Mr. Tony Gregg Project: Low Level Hg Client Sample ID: Huffman Finishing Company Sample ID: 347088001 Matrix: Water Collect Date: 03-APR-14 10:40 Receive Date: 15-APR-14 Collector: Client Report Date: April 29, 2014 Project: WATR00101 Client ID: WATR001 Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method Mercury Analysis-CVAA EPA 1631 Low Level Mercury Analysis "As Received" Mercury 19.0 0.200 0.500 ng/L 1 BCDI 04/28/14 1344 1381664 1 The following Analytical Methods were performed: Method Description Analyst Comments I EPA 1631 E Notes: Page 3 of 10 J Mt GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Water Tech Laboratories Address : P.O. Box 1056 Granite Falls, North Carolina 28630 Contact: Mr. Tony Gregg Project: Low Level Hg Client Sample ID: Huffman Blank Sample ID: 347088002 Matrix: BLANK Collect Date: 03-APR-14 10:40 Receive Date: 15-APR-14 Collector: Client Report Date: April 29, 2014 Project: WATR00101 Client ID: WATR001 Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method Mercury Analysis-CVAA EPA 1631 Low Level Mercury Analysis "As Received" Mercury J 0.35 0.200 0.500 ng/L I BCD] 04/28/14 1318 1381664 1 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 1631 E Notes: Page 4 of 10 f H GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Resort Date: April 29, 2014 Water Tech Laboratories P.O. Box 1056 Granite Falls, North Carolina Contact: Mr. Tony Gregg Workorder: 347088 Page 1 of 2 Parmname NOM Sample Qual QC Units RPD% RUC% Range Anlst Date Time Metals Analysis -Mercury Batch 1381664 QC 1203072232 LCS Mercury 5.00 4.56 ng/L 91.3 (77%-123%) BCD1 04/28/1413:05 QC1203072225 MB Mercury U <0.2 ng/L 04/28/1412:58 QC1203072226 347087001 MS Mercury 15.0 5.73 19.6 ng/L 92.7 (71%-125%) 04/28/1414:09 QC1203072229 347087001 MSD Mercury 15.0 5.73 20.2 ng/L 2.57 96.1 (0%-24%) 04/28/1414:15 Notes The Qualifiers in this report are defined as follows: < Result is less than value reported > Result is greater than value reported E %difference of sample and SD is >10%. Sample concentration must meet Flagging criteria FB Mercury was found present at quantifiable concentrations in field blanks received with these samples. Data associated with the blank are deemed invalid for reporting to regulatory agencies H Analytical holding time was exceeded J Value is estimated N Metals --The Matrix spike sample recovery is not within specified control limits N/A RPD or %Recovery limits do not apply. NI See case narrative ND Analyte concentration is not detected above the detection limit NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Q One or more quality control criteria have not been met. Refer to the applicable narrative or DER. R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD. X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y Other specific qualifiers were required to properly define the results. Consult case narrative. ^ RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. h Preparation or preservation holding time was exceeded Page 5 of 10 �f GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 347088 Page 2 of 2 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone, by a factor of 4 or more. ^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater tlian five times (5X) the contract required detection limit (RL). In cases where either the sample, or duplicate value is less than 5X the RL, a control limit of+/- the RL is used to evaluate the DUP result. * Indicates that a Quality Control parameter was not within specifications. For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. Page 6 of 10 Sludge Management Plan Wastewater Treatment System Improvements Huffman Finishing Company Granite Falls, North Carolina NPDES Permit No. NCO025135 The Huffman Finishing Company operates the 0.25 mgd extended aeration (Oxidation Ditch) type activated sludge plant which discharges its effluent into Catawba River (Lake Hickory) in accordance with the requirements set forth in the NPDES Permit NC0025135. The plant includes screening, flow equalization, extended aeration type activated sludge system, chlorine disinfection, pre and post dechlorination, post aeration, influent and effluent flow metering and sampling facilities, aerobic sludge stabilization/storage facilities, and disposal of stabilized sludge by land application in accordance with the requirements set forth in the land application of residuals (Non-503) Permit No. WQ002431. The settled sludge from the clarifier is periodically wasted to two (2) aerobic stabilization/storage basins for stabilization, settling and supernatant withdrawal operations. The supernatant withdrawn is recycled back at the headwork for reprocessing. The process of sludge wasting, stabilization, settling, and supernatant withdrawal is repeated and the stabilized sludge is disposed of once a year by land application at agronomic rates. The estimated waste activated sludge quantity of 325 lbs/day (4,775 gallons/day at specific gravity of 1.02 and 0.8 percent solids), at design conditions, will be aerobically stabilized to comply with the Class B pathogen reduction requirement, included in item no I.7 of the land application of residual solids Permit No. WQ002431. The Permit does not require Vector Attraction Reduction requirements. However, the existing aerobic sludge stabilization/storage facilities are adequately designed to comply with the Vector Attraction Reduction requirements. The 227 lbs/day (890 gallons/day at specific gravity of 1.02 and 3.0 percent solids) aerobically stabilized sludge will be disposed of by land application at agronomic rates on the permitted sites, using a private contractor engaged in sludge or residual disposal service. For disposal of the stabilized sludge by land application, the Huffinan Finishing Company will comply with the pathogen reduction requirement and vector attraction reduction requirement as follows: Class B Pathogen Reduction: Compliance with the Class B pathogen reduction will be achieved by using one of the following alternatives: Alternative 1: Monitoring of Fecal Coliform (EPA 503.32 (b) (2)). Alternative 2: Use of PSRP Aerobic Digestion and Lime Stabilization (EPA 503.32 (b) (3)) Vector Attraction Reduction: Compliance with the vector attraction reduction will be achieved by using one of the following options: Option 1: Reduction of volatile solids content (EPA 503.33 (b) (1)) WATER SUPPLY 0.25 MGD 0.0125 MGD 1 0.1425 MGD 1 0.095 MGD SANITARY SOCKS SOCKS FACT LI TI ES BLEACH] NG DYEI NG OPERATIONS OPERATIONS 0.0125 MGD T 0.1425 MGD T 0.095 MGD 0.25 MGD WASTEWATER TREATMENT PLANT EFFLUENT OUTFALL 001 wl 0.25 MGD THE WOOTEN WATER AND WASTEWATER FLOWS SCHEMATIC' COMPANY HUFFMAN FINISHING COMPANY ENGINEERING PLANNING GRANITE FALLS, NC ARCHITECTURE J DECHLORINATI ON FACI LI TI ES -------- -------------------------- , I _ T I SCREEN INFLUENT EQUALIZATION o.zs MGD TANK 0.25 MGD DECANT i- 0.0041 MGD AERATION TANK (OXIDATION DITCH) 0.25 MGO 0.25 MGD CHLORINE CLARIFIER CONTACT TANK I SLUDGE RECIRCULATION SLUDGE RECIRCULATION/ - - - WASTE PUMP STATION 0.25 MGD 'WASTE SLUDGE 0.005 MGD ALTERNATE SLUDGE HANDLING AEROBIC SLUDGE DI GESTI ON FACILITIES AEROBI C SLUDGE DI GESTI ON FACILITIES CASCADE EFFLUENT POST AERATION 0.25 MGD STABI LI ZED SLUDGE TO - LAND APPLICATION SI TES 0.0009 MGD HUFFMAN FINISHING COMPANY WVVFP PROCESS SCHEMATIC CASCADE O AERATOR 0.25 MGD EFFLUENT 0.25 MGD- LAKE HICKORY- THE WOOTEN COMPANY ENGINEERING PLANNING ARCHITECTURE