HomeMy WebLinkAboutWQ0004972_Monitoring - 03-2023_20230427Monitoring Report Submittal
...................................................
Permit Number#* WQ0004972
Name of Facility:* Forest Lakes Preserve ELS
Month: * March Year: * 2023
Report Information
Type* Upload Document*
NDMR, NDAR-1, NDAR-2, NDMLR Forest Lakes —March 2023.pdf 3.1MB
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
Confirmation Email Address: * Jessica. Mize@pacelabs.com
Name of Submitter: * Jessica Mize
Signature:
Date of submittal: 4/27/2023
This will be filled in automatically
Initial Review
Reviewer: Wanda.Gerald
Is the project number correct?* WQ0004972
Is the monitoring report accepted?* Yes No
Regional Office* Winston-Salem
Reviewer: _anonymous
Review Date: 5/17/2023
Page 1 of 2
NON -DISCHARGE WASTE WATER MONITORING REPORT
PERMIT NUMBER: W00004972 MONTH: March YEAR: 2023
FACILITY NAME: Forest Lakes Preserve ELS COUNTY: Davie
Flow Monitoring Point: Effluent: I y I Influent: 1-1
Parameter Monitoring Point: Effluent: I Influent: I Surface Water S
SW Code/Name:
Was There Effluent Flow for this Month Generated At This Facili Yes: ht N
D
A
T
l:
Operator
Amval
Time
2400
Clock
Operator
Time on
Site
ORC
on
Site?
50050
00400
50060
00310
00610
00530
31616
00665
00625
00630
00600
00620
70300
00940
Daily Rate
(Flow) into
Treatment
S,Ytem
pH
Residua]
Chlorine
BOD-5
2(rc
NHJ•N
TSS
Fecal
Colirorm
(Gco-manic
Mean-)
Taal
Pl_
Total
Kieldha]
Nitrogen
NO2-NO3
Total
Namgm
Nitrate
NO3•N
Total
Di oked
Solids
Chloride
IIRS
L
M
HiOML
M
M
L
M
1
MGlL
M !Y
CentIRU0u5
CC
Onl a
onI V
onl }'
I
ml )'
ont )'
onl )'
on V
mrl Y
'Cat
'Car
0910 .
zis•4:25
'773
-=:7.3':,.
'<0.01
:_.
:s;•
., I
.'._,.'
'•-
;,
:-.; . ::
��_ ..
2
1635
0.25
B
158,859
7.3
<0.01
3
1150
0 . .
B i
11AW
7.3
<M01
4
10.251
6
1530
0.25
B
10,251
7.3
<0.01
1
!i:i1g20-
: ;..0123 .::
` $ `..`=
7J30'±
.7.3 ''
<0.01
-
a
1500
0.25
B
7,946
7.3
<0.01
9
73
;<0.01
10
1105
0.25
B
10,329
7.1
<0.01
11
10,815
W :.
12
10,815
;13
t,r 6 $a
MO
.•`46.4
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<&040
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14
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OSS6
0 25144.
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<O.o1
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16
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0.25
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: 0900.
o- .0.25.':
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7.1 ',
_<0.01
IS
12,285
19
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:.
20
1340
0.25
Y
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4125 r
`11
: 1 404`
- 7i4,:
<O.OI .
. . w- : ".'
22
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Y
11,141
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&25
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406
`73`
<&01
20
1020
0.25
B
11,058
7.3
<0.01
25
11058
26
11 058
27
0855.
'�"p".0.25 ,'
B.....
= `s-11058
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'&01
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0.25
B
5,501
7.0
<&01
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0855:=
.. 0.25
B7i1
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7.286
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3&4
at
0405=
-°025
B' `:.
-: 706
.71
4k01
i..'.
�;......"
,:
Average
14 676
C0.01
< .
--0.(140
Daily Maximum
158,859
7.4
<0.01
1.7
4 0
6.
717W
Daily Minimum
4,706
6.8
<0.01
46.4
44.7
11.7
2420
6.1
62.7
<0,040
62.7
<0.040
234
38.4
Monthly Limits (s)
4400
]
Composite Of Grab (G)
Operator in Responsible Charge (ORC): Glenn Price Grade: 11 Phone: 336-996-2841
Check Box if ORC Has Changed: ORC Certification Number: 987931/20771
Certified Laboratories (l): Pace Analytical Serivees (2);
Person(s) Collecting Samples: Glenn Price
Mail ORIGINAL and Two COPIES to:
ATTN: Non -Discharge Compliance Unit X \ _
DENR (SIGNATURE OF OPERATOR RONSIBLECHARGE)
Division of Water Quality By this signature, I certify that this report is accurate and
1617 Mail Service Center complete to the best of my knowledge.
RALEIGH, NC 27699-1617
DENR Form NDAR-1 (5/2003)
NON DISCHARGE WASTEWATER MONITORING REPORT
FACILITY STATUS:
Please answer the following question: Compliant Y N)
/. Does all monitoring data and sampling frequencies meet permit requirements?
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance with its
permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach
additional sheets if necessary.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief true, accurate, and complete. 1 am aware that there are significant
penalties for submitting false information, ' eluding the possibility of fines and imprisonment for knowing violations."
XZ -7'13 Baron Neal McDuffie
(Sign ure of Permitee)* Date (Name of Signing Official -Please print or type)
Baron Neal McDuffie (Authdfized Agent) Field Services Director (Pace AnalZical Services
(Permittee-Please print or type) (Position or Title)
2N Riverside Plaza , Suite 800 3/31/21
Chicago, 11 60606 (Permit Exp. Date)
(Permittee Address)
01002 Arsenic
01022 Boron
00310 BOD5
01027 Cadmium
00916 Calcium
00940 Chloride
50060 Chlorine, Total
Residual
01034 Chromium
00340 COD
31504
Coliform, Total
00094
Conductivity
01042
Copper
00300
Dissolved Oxygen
31616
Fecal Coliform
01051
Lead
00927
Magnesium
71900
Mercury
00610
NH3 as N
01067
Nickel
00600 Nitro en, Total
00630 NO2 & NO3
00620 NO3
00556 Oil & Grease
WQ09 PAN (Plant Available)
00400 pH
32730 Phenols
00665 Phosphorus, Total
00937 Potassium
00545 Settleable Matter
00929
Sodium
00931
SAR
00745
Sulfide
00515
TDS
00010
Temperature
00625
TKN
00680
TOC
00530
TSS/TSR
00076
Turbid'
01092
Zinc
Parameter Code assistance may be obtained by calling the Water Quality Compliance/Enforcement Unit at (919) 733-5083, extension 529.
The monthly average for Fecal Coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data.
* If signed by other than the Permittee, delegation of signatory authority must be on file with the stale per 15A NCAC 213.0506 (b) (2) (D).
Page 2 of 2
NON -DISCHARGE APPLICATION REPORT
SPRAY IRRIGATION SITE(S)
THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED
PERMIT NUMBER: W00004972 MONTH: March YEAR: 2023
FACILITY NAME: Forest Lakes Preserve ELS. COUNTY: Davie
Formulas:
Daily Loading (inches) = (Volume Applied (gallons) x 0.1336 (cubic feet/gallon) x 12 (inchesffooq] I (Area Sprayed (acres) x 43,560 (square feet/acre) or
= [Volume Applied (gallons) / (Area Sprayed (acres) x 27,152 (gallons/acre-inch).
Maximum Hourly Loading (inches) = Daily Loading (inches) / [Time Irrigated (minutes) / 60 (minutes/hour)] Monthly Loading (Inches) =Sum of Daily Loading (inches)
12 Month Floating Total (inches) = Sum of this month's Monthly Loading (inches) and previous 11 month's Monthly Loadings (inches)
Average Weekly Loading (inches) = IMonthly Loading (inchestmonth) / Number of days in the month (days/month )I x 7 (days/week)
Did Irrigation Occur At This Facility.
Yes FYI No❑
Did Irrigation Occur On This Field:
Ye No ❑
Did Irrigation Occur On This Field.
Ye❑ No. ❑
Field Number
Field Number
Area Sprayed (acres):
60
Area Sprayed (acres)'.
Cover Crop
Cover Crop.
Permitted ou
y Rate (inches).
0 11
PermittedHourly Rate (inches)
D
A
I
WEATHER CONDITIONS
Storage
Lagoon
Permitted Yearly Rate (inches).
46.8
Permitted Yearly Rate (inches)-
Weather
Code'
Temperature
at
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Preapda
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2.17
2S.7S
0.d3
1 e:mrer ( odes: U-dear, M partly cloudy, CI -cloudy, R-rain, Sn-snow, SI-sleet
Spray Irrigation Operator in Responsible Charge (ORC): Glenn Price Phone: 336 996-2841
ORC Certification Number: 987931/20771 Check Box if ORC Has Changed:
Mail ORIGINAI, and -I'wo COPIES to: I
A'I"TN: Non -Discharge Compliance Unit X �� � � � s�\
DENR (SIGNA'FURE OP OPERATOR IN RESPONS ARGF,)
Division of Water Quality By this signature, I certify that this report is accurate and
1617 Mail Service ('enter complete to the best of my knowledge.
RALEIGH, NC 27699-1617
DENR Form NDAR-1 (5/2003)
NON -DISCHARGE APPLICATION REPORT
SPRAY IRRIGATION SITE(S)
FACILITY STATUS:
Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been compliant
with the following permit requirements: (Note: If a requirement does not apply to your facility put (NA) in the
compliant box.)
1. The application rate(s) did not exceed the limit(s) specified in the permit.
Compliant (Y,N)
Z Adequate measures were taken to prevent wastewater runoff from the site(s).
3. 'A suitable vegetative cover was maintained on the site(s) in accordance with the permit.
4. All buffer zones as specified in the permit were maintained during each application.
S. The freeboard in the treatment and/or storage lagoon(s) was not less than the
limit(s) specified in the permit.
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance with its
permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach
additional sheets if necessary.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including t e possibility of fines and imprisonment for knowing violations."
7.) 3Baron Neal McDuffie
(Signature of Permiee)* to (Name of Signing Official -Please print or type)
Baron Neal McDuffie (Authorized Aaent)
(Permittee-Please print or type)
2N. Riverside Plaza, Suite 800
Chicago, Il 60606
(Permittee Address)
Field Services Director (Pace Analytical Services)
(Position or Title)
3 /31 /2021
(Pen -nit Exp. Date)
* If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506 (b) (2) (D).
laceAnalyfical'i
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
March 23, 2023
Tracy Overdurf
Forest Lake
192 Thousand Trails Dr.
Advance, NC 27006
RE: Project: Forest Lake
Pace Project No.: 92656585
Dear Tracy Overdurf:
Enclosed are the analytical results for sample(s) received by the laboratory on March 13, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Eden
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Stephanie Knott
stephanie.knoft@pacelabs.com
704-977-0981
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 16
a-Mnalytical
www.pacelhbs.ccm
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Project: Forest Lake
Pace Project No.: 92656585
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
VrginiaNELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
VirginiaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, L.L.C. Page 2 of 16
aceAnalj cal
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Project: Forest Lake
Pace Project No.: 92656585
Lab ID Sample ID
92656585001 Effluent
PASI-A = Pace Analytical Services - Asheville
PASI-E = Pace Analytical Services - Eden
SAMPLE ANALYTE COUNT
Method Analysts
SM 254OD-2015
VLG
EPA 353.2 Rev 2.0 1993
SRS
SM 521OB-2016
SRS
Colilert-18
VLG
TKN+NO3+NO2 Calculation
MA132
EPA 350.1 Rev 2.0 1993
ARJ
EPA 351.2 Rev 2.01993
MFO
EPA 365.1 Rev 2.01993
Zip
REPORT OF LABORATORY ANALYSIS
Analytes
Reported Laboratory
1
PASI-E
2
PASI-E
1
PASI-E
1
PASI-E
1
PASI-A
1
PASI-A
1
PASI-A
1
PASI-A
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 16
aceAnalytical
www.pacelabs.ccm
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
ANALYTICAL RESULTS
Project: Forest Lake
Pace Project No.: 92656585
Sample: Effluent
Parameters
Lab ID: 92656585001 Collected: 03/13/23 14:35
Results Units Report Limit DF
Received: 03/13/23 16:00 Matrix: Water
Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 254OD-2015
Pace Analytical Services - Eden
Total Suspended Solids
11.7 mg/L 6.7 1
03/14/23 14:31
353.2 NO2/NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, NO2 plus NO3
ND mg/L 0.040 1
03/14/23 17:13
Nitrogen, Nitrate
ND mg/L 0.040 1
03/14/23 17:13 14797-55-8
5210B BOD, 5 day EDN
Analytical Method: SM 521OB-2016 Preparation Method:
SM 521OB-2016
Pace Analytical Services - Eden
BOD, 5 day
46.4 mg/L 2.0 1
03/14/23 10:01 03/19/23 12:05 81,B3,
L1
Colllert-18 Fecal Coliform EDN
Analytical Method: Colilert-18 Preparation Method: Colilert-18
Pace Analytical Services - Eden
Fecal Coliforms
2420 MPN/100mL 1.0 1 03/13/23 18:05 03/14/23 12:52
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Pace Analytical Services - Asheville
Total Nitrogen
62.7 mg/L 0.040 1 03/21/23 14:18
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
44.7 mg/L 1.0 10 03/22/23 11:37 7664-41-7
351.2 Total KJeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Kjeldahl, Total
62.7 mg/L 2.5 5 03/17/23 16:40 03/18/23 05:16 7727-37-9
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Phosphorus
6.1 mg/L 0.10 2 03/23/2311:39 03/23/2315:23 7723-14-0
Date: 03/23/2023 05:26 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, I.I.C.
El
Page 4 of 16
duuftlytical
www.pacclabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Forest Lake
Pace Project No.: 92656585
QC Batch: 761195
Analysis Method:
SM 254OD-2015
QC Batch Method: SM 254OD-2015
Analysis Description:
2540D Total Suspended Solids
Laboratory:
Pace Analytical Services - Eden
Associated Lab Samples: 92656585001
METHOD BLANK: 3953720
Matrix: Water
Associated Lab Samples: 92656585001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
ND
2.5 03/14/23 14:27
LABORATORY CONTROL SAMPLE: 3953721
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Total Suspended Solids
mg/L
250 256
102 90-110
SAMPLE DUPLICATE: 3953722
92656412001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
ND
ND
SAMPLE DUPLICATE: 3953723
92656585001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
11.7
11.5 2
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/23/2023 05:26 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 16
aceAnalytical
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i
Project: Forest Lake
Pace Project No.: 92656585
QC Batch: 761304
QC Batch Method: EPA 353.2 Rev 2.0 1993
Associated Lab Samples: 92656585001
METHOD BLANK: 3954405
Associated Lab Samples: 92656585001
Parameter Units
Nitrogen, Nitrate mg/L
Nitrogen, NO2 plus NO3 mg/L
QUALITY CONTROL DATA
Analysis Method:
Analysis Description
Laboratory:
Matrix: Water
EPA 353.2 Rev 2.0 1993
353.2 Nitrate + Nitrite, Unpres. EDN
Pace Analytical Services - Eden
Blank Reporting
Result Limit Analyzed
ND 0.040 03/14/2317:06
ND 0.040 03/14/2317:06
Qualifiers
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
LABORATORY CONTROL SAMPLE:
3954406
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
Nitrogen, Nitrate
mg/L
1.5
1.5 100 90-110
Nitrogen, NO2 plus NO3
mg/L
2.5
2.4 98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3954407
3954408
MS
MSD
92656494001 Spike
Spike
MS
MSD MS MSD
% Rec
Parameter Units
Result Conc.
Conc.
Result
Result % Rec % Rec
Limits RPD Qual
Nitrogen, Nitrate mg/L
ND 1.5
1.5
1.6
1.5 108 102
90-110 5
Nitrogen, NO2 plus NO3 mg/L
0.62 2.5
2.5
3.3
3.2 108 104
90-110 3
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/23/2023 05:26 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 16
('�4,eAnalyficalo
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QUALITY CONTROL DATA
Project: Forest Lake
Pace Project No.: 92656585
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
QC Batch: 761186
Analysis Method:
SM 521OB-2016
QC Batch Method: SM 521OB-2016
Analysis Description:
5210E BOD, 5 day Final EDN
Laboratory:
Pace Analytical Services - Eden
Associated Lab Samples: 92656585001
METHOD BLANK: 3953687
Matrix: Water
Associated Lab Samples: 92656585001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
BOD, 5 day
mg/L
ND 2.0 03/19/23 11:47 B3
LABORATORY CONTROL SAMPLE: 3953688
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
BOD, 5 day
mg/L
198 302
153 84.6-115 B3, L1
SAMPLE DUPLICATE: 3953690
92656449001 Dup
Parameter
Units
Result Result
RPD Qualifiers
BOD, 5 day
mg/L
2120 2070 3 B3,L1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/23/2023 05:26 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 16
aceAnalyfical
www.pacefabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Forest Lake
Pace Project No.: 92656585
QC Batch: 761115 Analysis Method: Colilert-18
QC Batch Method: Colilert-18 Analysis Description: Colilert-18 Fecal Coliform EDN
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92656585001
SAMPLE DUPLICATE: 3953514
Parameter Units
Fecal Coliforms MPN/100mL
92656585001 Dup
Result Result
2420 2420
RPD Qualifiers
0 El
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/23/2023 05:26 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 16
aceAnalytical
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i
QUALITY CONTROL DATA
Project: Forest Lake
Pace Project No.: 92656585
Paco Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
QC Batch: 762607
Analysis Method: EPA 350.1 Rev 2.0 1993
QC Batch Method: EPA 350.1 Rev 2.0 1993
Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92656585001
METHOD BLANK: 3960479
Matrix: Water
Associated Lab Samples: 92656585001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Nitrogen, Ammonia mg/L
ND 0.10
03/22/23 10:56
LABORATORY CONTROL SAMPLE: 3960480
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Nitrogen, Ammonia mg/L
5 5.0
100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3960481 3960482
MS MSD
92657433001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qua]
Nitrogen, Ammonia mg/L 13.7
5 5 18.8
18.9 103 104
90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3960483 3960484
MS MSD
92657612001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qua[
Nitrogen, Ammonia mg/L ND
5 5 5.3
5.3 106 106
90-110 0
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/23/2023 05:26 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 16
aceAnalytical
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Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Forest Lake
Pace Project No.: 92656585
QC Batch: 762117 Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92656585001
METHOD BLANK: 3958575
Matrix: Water
Associated Lab Samples: 92656585001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Kjeldahl, Total
mg/L
ND 0.50
03/18/23 03:46
LABORATORY CONTROL SAMPLE:
3958576
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits
Qualifiers
Nitrogen, KJeldahl, Total
mg/L
10
10.6
106 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3958577
3958578
MS
MSD
92656582002
Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result
Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
Nitrogen, Kjeldahl, Total
mg/L 69.0
10
10 79.2
76.6 102
76
90-110 3 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3958579
3958580
MS
MSD
92656582003
Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result
Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
Nitrogen, Kjeldahl, Total
mg/L 58.3
10
10 68.9
69.7 106
114
90-110 1 M1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the resu1L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/23/2023 05:26 PM without the written consent of Pace Analytical Services, L.L.C.
Page 10 of 16
aceAnalytical
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Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Forest Lake
Pace Project No.: 92656585
QC Batch: 762990 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92656585001
METHOD BLANK: 3962417
Associated Lab Samples: 92656585001
Parameter Units
Phosphorus mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.050 03/2312315:15
LABORATORY CONTROL SAMPLE: 3962418
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Phosphorus mg/L 2.5 2.5 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3962419 3962420
MS MSD
92655582010 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/L 1.5 2.5 2.5 4.2 4.2 107 106 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3962421 3962422
MS MSD
92656551001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mglL 4.5 2.5 2.5 7.1 7.2 105 107 90-110 1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/23/2023 05:26 PM without the written consent of Pace Analytical Services, I.I.C.
Page 11 of 16
aceAnalytical o
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Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
QUALIFIERS
Project: Forest Lake
Pace Project No.: 92656585
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
B1 Less than 1.0 mg/L DO remained for all dilutions set. The reported value is an estimated greater than value and is
calculated for the dilution using the least amount of sample.
B3 The dissolved oxygen depletion of the dilution water blank exceeded 0.2 mg/L.
El Reported value should be considered a minimum estimate since it is the maximum reportable number for this method
based on the sample volume used. The true value is likely greater than the value reported.
L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte In associated
samples may be biased high.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/23/2023 05:26 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 16
aceAnalytical
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i
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Forest Lake
Pace Project No.: 92656585
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92656585001
Effluent
SM 254OD-2015
761195
92656585001
Effluent
EPA 353.2 Rev 2.0 1993
761304
92656585001
Effluent
SM 521OB-2016
761186
SM 521OB-2016
761462
92656585001
Effluent
Colilert-18
761115
Colilert-18
761116
92656585001
Effluent
TKN+NO3+NO2
762748
Calculation
92656585001
Effluent
EPA 350.1 Rev 2.0 1993
762607
92656585001
Effluent
EPA 351.2 Rev 2.0 1993
762117
EPA 351.2 Rev 2.0 1993
762266
92656585001
Effluent
EPA 365.1 Rev 2.0 1993
762990
EPA 365.1 Rev 2.0 1993
763338
Date: 03/23/2023 05:26 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, L.L.C.
Page 13 of 16
CHAIN -OF -CUSTODY / Analytical Request Document
ace The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Submitting a sample via this chain of custody constitutes acknowledgment and acceptance of the Pace Terms and Conditions found at htlps:trwft.pacelabs.com/hubfs/pas-standard-terms.
Rector A Section B Section C Wit • Q 2R5 w iR -%
Required CISan7 Information: Required Project Information: irtvoka IMormatian: 6C=7Ci) /`_) � 1
Pw-ny. Forest Lake eport To Tracy Ovordwi - - - -ff _ - — - - ! - -
ess 192 Thousand Trails Dr To: y Nama:
to.NC 27006 ddress:
II-
pye�urf s letom rcflase Order# Quofe:
NONE Fax, rgect Name. Forest Lake Monthly Protect Manager: wepharucAnc 92655585sted
r
Due Date' rolect M: ace Pmfils M 13254 �..
Fllfered
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SAMPLE ID oSL
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sample Ids must be unique r.c+++ rs
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-...:. ADI)MMALCOMMENTS RELINCtaSN=BYIAFFILIATION -
DATE
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SAMPLE CONDITIONS
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PLER NAME: AND S"ATu
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PRINT Name of
SIGNATURE of SAMPLER:
DATE Signed:
� DC#_Title: ENV-FRM-HUN1-0084 v01_Tech Spec Sample Condition
Pace Upon Receipt
1 ,. Effective Date: 05/12/2022
Laboratory receiving samples:
Asheville ❑ Eden ❑ Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑ Atlanta❑ Kernersville[I
Client Name.
Project q:
____�
Courier: Fed Ex ❑UPS ❑USPS ❑Client
❑ Commercial HPace ❑Other:__^
Carrier Tracking Number:
Custody Seal Present? ❑Yes gNo Seals Intact? ❑Yes ❑No Date/Initials Person Examining Contents:
Packing Material: ❑Bubble Wrap ❑Bubble Bags JfJNone ❑ Other Biological Tissue Frozen?
[]Yes ❑No [:]N/AThermometer: ❑ IR Gun ID: " T d C Z Type of Ice: ICJ Wet ❑ Blue ❑ None
Cooler Temp ('C ): 3 '-/ Correction Factor: Add / Subtract ('C) _�
- - Temp should be above freezing to 6'C
Corrected Cooler Temp t' C D []Samples out of temp criteria. Samples on ice, cooling process
)' has begun
USDA Regulated Soil ( (g N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? D d samples prig nate from a foreign source (internationally,
❑Yes No including Hawaii and Puerto Rico)? ❑Yes []No
Comments/Discrepancy:
Chain of Custody Present?
Yes
No
N/A
1.
Samples Arrived within Hold Time?
Yes
ONo
N/A
2.
Short Hold Time Analysis (<72 hr.)?
eYes
❑No
[]NIA
3.
Rush Turn Around Time Requested?
❑Yes
[TNo
❑N/A
4.
Sufficient Volume?
ZYes
QNo
N/A
S.
Correct Containers Used?
Pace Containers Used?
[rf Yes
[5Yes
[]No
❑No
❑N/A
❑N/A
6.
Containers Intact?
Clryes
ONo
N/A
7.
Dissolved analysis: Samples Field Filtered?
[]Yes
❑No
CIA/A
B.
Sample Labels Match COC?
Includes Date/Time/ID/Analysis Matrix:
y'tlYes
•v "
[]No
[]N/A
9.
Headspace in VOA Vials (>5-6mm)?
❑Yes
[]No
jfN/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
[]Yes
QYes
❑No
ONo
[ZN/A
QN/A
11.
COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes [:]No
Temp Log: Temp must be maintained
at <6 C during login, record temp
every 2t) minutes.
Time opened: I 0 p Temp:
Time: j i! 10 put in cooler
Time: Temp:
Person Contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Qualtrax Document ID: 70677
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Date/Time:
Date:
Date:
Pagel of 2
Page 15 of 16
f�
'�'�1Ce
. w'.Cu lia.vr
DC#_Title: ENV-FRM-HUN1.0084 v01_Tech Spec Sample Condition
Upon Receipt
Effective Date: 05112/2022
*Check mark top half of box if pH and/or dechlorination Project #
is verified and within the acceptance range for
preservation samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DROJ8015 (water) DOC, LLHg i
**Bottom half of box is to list number of bottles
***Check all unpreserved Nitrates for chlorine
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pH Adjustment Log for Preserved Samples
Sample IV
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot #
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers)
Qualtrax Document ID: 70677 Page 2 of 2
Page 16 of 16
aceAnalj cal
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
April 11, 2023
Tracy Overdurf
Forest Lake
192 Thousand Trails Dr.
Advance, NC 27006
RE: Project: Forest Lake - MW's
Pace Project No.: 92659645
Dear Tracy Overdurf:
Enclosed are the analytical results for sample(s) received by the laboratory on March 30, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Eden
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Stephanie Knott
stephanie.knott@pacelabs.com
704-977-0981
Project Manager
Enclosures
l pCCRF�I�
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 21
Pace Analytical Services, LLC
® 1377 South Park Drive
aceAnalytical Kemersville, NC 27284
www.paeelabs.com
(704)977-0981
CERTIFICATIONS
Project: Forest Lake - MW's
Pace Project No.: 92659645
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
VrginiaNELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
VrginiaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 21
aceAnalytical
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Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
SAMPLE ANALYTE COUNT
Project: Forest Lake - MW s
Pace Project No.: 92659645
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92659645001
MW-1
SM 2540C-2015
LRB
1
PASI-E
EPA 353.2 Rev 2.0 1993
SRS
1
PASI-E
SM 9222D-2015
MWF
1
PASI-E
EPA 300.0 Rev 2.1 1993
JCM
1
PASI-A
EPA 350.1 Rev 2.0 1993
ARJ
1
PASI-A
EPA 365.1 Rev 2.0 1993
Zip
1
PASI-A
SM 531OB-2014
MJP
1
PASI-A
92659645002
MW-2
SM 254OC-2015
LRB
1
PASI-E
EPA 353.2 Rev 2.0 1993
SRS
1
PASI-E
SM 9222D-2015
MWF
1
PASI-E
EPA 300.0 Rev 2.1 1993
JCM
1
PASI-A
EPA 350.1 Rev 2.0 1993
ARJ
1
PASI-A
EPA 365.1 Rev 2.0 1993
Zip
1
PASI-A
SM 531OB-2014
MJP
1
PASI-A
92659645003
MW-3
SM 254OC-2015
LRB
1
PASI-E
EPA 353.2 Rev 2.0 1993
SRS
1
PASI-E
SM 9222D-2015
MWF
1
PASI-E
EPA 300.0 Rev 2.1 1993
JCM
1
PASI-A
EPA 350.1 Rev 2.0 1993
ARJ
1
PASI-A
EPA 365.1 Rev 2.0 1993
Zip
1
PASI-A
SM 531OB-2014
MJP
1
PASI-A
92659645004
MW-4
SM 2540C-2015
LRB
1
PASI-E
EPA 353.2 Rev 2.0 1993
SRS
1
PASI-E
SM 9222D-2015
MWF
1
PASI-E
EPA 300.0 Rev 2.1 1993
JCM
1
PASI-A
EPA 350.1 Rev 2.0 1993
ARJ
1
PASI-A
EPA 365.1 Rev 2.0 1993
Zip
1
PASI-A
SM 531OB-2014
MJP
1
PASI-A
92659645005
Effluent
SM 254OC-2015
LRB
1
PASI-E
EPA 300.0 Rev 2.1 1993
JCM
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-E = Pace Analytical Services - Eden
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC, Page 3 of 21
aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
ANALYTICAL RESULTS
Project: Forest Lake - MW s
Pace Project No.: 92659645
Sample: MW4
Parameters
Lab ID: 92659645001 Collected: 03/30123 10:12
Results Units Report Limit DF
Received: 03/30/23 11:50 Matrix: Water
Prepared Analyzed CAS No. Qual
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2015
Pace Analytical Services - Eden
Total Dissolved Solids
66.0 mg/L 25.0
1
03/31/23 10:53
353.2 NO2/NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, Nitrate
0.22 mg/L 0.040
1
03/31/2310:03 14797-55-8
MBIO 9222D Fecal Coliform EDN
Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Eden
Fecal Coliforms
ND CFU/100 mL 1.0
1
03/30/23 16:04 03/31/23 15:44
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
Chloride
1.6 mg/L 1.0
1
04/01/2317:17 16887-00-6
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
04/07/2311:37 7664-41-7
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.01993 Preparation Method: EPA 366.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
ND mg/L 0.050
1
04/06/2315:33 04/07/2310:58 7723-14-0
5310B TOC
Analytical Method: SM 531 OB-2014
Pace Analytical Services - Asheville
Total Organic Carbon
2.3 mg/L 1.0
1
04/06/23 19:56 7440-44-0
Date: 04/11/202310:26 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 21
aceAnalytical e
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I
ANALYTICAL RESULTS
Project: Forest Lake - MW's
Pace Project No.: 92659645
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Sample: MW-2
Lab ID: 92659645002 Collected: 03/30/23 10:49
Received: 03/30/23 11:50 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2015
Pace Analytical Services - Eden
Total Dissolved Solids
48.0 mg/L 25.0
1
03/31/23 10:53
353.2 NO2IN03 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, Nitrate
0.47 mg/L 0.040
1
03/31/23 10:11
14797-55-8
MBIO 9222D Fecal Coliform EDN
Analytical Method: SM 9222D-2015 Preparation
Method: SM 9222D-2015
Pace Analytical Services - Eden
Fecal Coliforms
ND CFU/100 mL 1.0
1
03/30/23 16:30 03/31/23 15:44
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
Chloride
2.8 mg/L 1.0
1
04/01/2317:32
16887-00-6
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
04/07/23 11:38
7664-41-7
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
0.069 mg/L 0.050
1
04/0612315:33 04/07/2310:59
7723-14-0
5310E TOC
Analytical Method: SM 531 OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
ND mg/L 1.0
1
04/06/23 20:50
7440-44-0
Date: 04/11 /202310:26 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 21
aceAnalytical
www.pacslsbs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
ANALYTICAL RESULTS
Project: Forest Lake - MW's
Pace Project No.: 92659645
Sample: MW-3
Parameters
Lab ID: 92659645003 Collected: 03/30/23 10:22
Results Units Report Limit DF
Received: 03/30/23 11:50 Matrix: Water
Prepared Analyzed CAS No. Qual
2540C Total Dissolved Solids
Analytical Method: SM 2WC-2015
Pace Analytical Services - Eden
Total Dissolved Solids
131 mg/L 25.0
1
03/31/23 10:53
353.2 NO2IN03 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, Nitrate
11.5 mg/L 0.20
5
03/31/23 10:21
14797-55-8
MBIO 9222D Fecal Coliform EDN
Analytical Method: SM 9222D-2015 Preparation
Method: SM 922213-2015
Pace Analytical Services - Eden
Fecal Coliforms
ND CFU/100 mL 1.0
1
03/30/23 16:04 03/31/23 15:44
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Chloride
24.5 mg1L 1.0
1
04/01/2317:48
16887-00-6
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
04/07/2311:40
7664-41-7
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
ND mg1L 0.050
1
04/06/2315:33 04/07/2311:09
7723-14-0
5310B TOC
Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
ND mg1L 1.0
1
04/06/23 21:43
7440-44-0
REPORT OF LABORATORY ANALYSIS
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Date: 04/11/2023 10:26 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 21
aceAnalytical
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Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
ANALYTICAL RESULTS
Project: Forest Lake - MW's
Pace Project No.: 92659645
Sample: MW-4
Parameters
Lab ID: 92659645004 Collected: 03/30/23 10:38
Results Units Report Limit DF
Received: 03/30/23 11:50 Matrix: Water
Prepared Analyzed CAS No. Qua[
2640C Total Dissolved Solids
Analytical Method: SM 254OC-2015
Pace Analytical Services - Eden
Total Dissolved Solids
72.0 mg/L 25.0 1
03/31/23 10:53
353.2 NO2/NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.01993
Pace Analytical Services - Eden
Nitrogen, Nitrate
3.4 mg/L 0.040 1
03/31/23 10:22 14797-55-8
MBIO 9222D Fecal Coliform EDN
Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Eden
Fecal Coliforms
ND CFU/100 mL 1.0 1
03/30/23 16:30 03/31/23 15-44
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
Chloride
6.7 mg/L 1.0
1 04/01/2318:03 16887-00-6
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1 04/07/23 11:41 7664-41-7
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
ND mg/L 0.050
1 04/06/2315:33 04/07/2311:13 7723-14-0
5310B TOC
Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
ND mg/L 1.0
1 04/06/23 21:58 7440-44-0
Date: 04/11/2023 10:26 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 21
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ANALYTICAL RESULTS
Project Forest Lake - MW's
Pace Project No.: 92659645
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Sample: Effluent Lab ID: 92659645005 Collected: 03/30/23 10:46 Received: 03/30/23 11:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540C Total Dissolved Solids Analytical Method: SM 2540C-2015
Pace Analytical Services - Eden
Total Dissolved Solids 234 mg/L 50.0 1 03/31/23 10:53
300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
Chloride 38.4 mg/L 1.0 1 04/01/2318:19 16887-00-6
REPORT OF LABORATORY ANALYSIS
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Date: 04/11/2023 10:26 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 21
aceAnalytical
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Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Forest Lake - MW s
Pace Project No.: 92659645
QC Batch: 765155 Analysis Method: SM 254OC-2015
QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92659645001, 92659645002, 92659645003, 92659645004, 92659645005
METHOD BLANK: 3972996 Matrix: Water
Associated Lab Samples: 92659645001, 92659645002, 92659645003, 92659645004, 92659645005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Dissolved Solids mg/L ND 25.0 03/31/23 10:52
LABORATORY CONTROL SAMPLE: 3972997
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Dissolved Solids mg/L 250 256 102 90-110
SAMPLE DUPLICATE: 3972998
92659063003 Dup
Parameter Units Result Result RPD Qualifiers
Total Dissolved Solids mg/L 173 176 2
SAMPLE DUPLICATE: 3972999
92659063001 Dup
Parameter Units Result Result RPD Qualifiers
Total Dissolved Solids mg/L 266 269 1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 04/11 /202310:26 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 21
aceAnalytical
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f
QUALITY CONTROL DATA
Project: Forest Lake - MW's
Pace Project No.: 92659645
QC Batch: 765096 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. EDN
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92659645001, 92659645002, 92659645003, 92659645004
METHOD BLANK: 3972758 Matrix: Water
Associated Lab Samples: 92659645001, 92659645002, 92659645003, 92659645004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Nitrate mg/L ND 0.040 03/31/23 09:53
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
LABORATORY CONTROL SAMPLE: 3972759
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/L 1.5 1.5 97 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3972760 3972761
MS MSD
92659656004 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Nitrate mg/L ND 1.5 1.5 1.5 1.5 102 100 90-110 2
Results presented on this page are In the units Indicated by the "Units" column except whore an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/11 /2023 10:26 AM without the written consent of Pace Analytical Services, LLC.
Page 10 of 21
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I
QUALITY CONTROL DATA
Project: Forest Lake - MW's
Pace Project No.: 92659645
QC Batch: 765005 Analysis Method: SM 9222D-2015
QC Batch Method: SM 922213-2015 Analysis Description: 9222D Fecal Coliform(MF)-EDN
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92659645002, 92659645004
METHOD BLANK: 3972404 Matrix: Water
Associated Lab Samples: 92659645002, 92659645004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms CFU/100 mL ND 1.0 03/31/23 15:44
METHOD BLANK: 3972406 Matrix: Water
Associated Lab Samples: 92659645002, 92659645004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms CFU/100 mL ND 1.0 03/31/23 15:44
SAMPLE DUPLICATE: 3972405
92659645004 Dup
Parameter Units Result Result RPD Qualifiers
Fecal Coliforms CFU/100 mL ND ND
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Results presented on this page are In the units Indicated by the 'Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 04/11/2023 10:26 AM without the written consent of Pace Analytical Services, LLC.
Page 11 of 21
aceAnalyfical
www.pacalitbs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Project: Forest Lake - MW's
Pace Project No.: 92659645
QC Batch: 765045
QC Batch Method: SM 9222D-2015
Associated Lab Samples: 92659645001. 92659645003
METHOD BLANK: 3972588
Associated Lab Samples: 92659645001, 92659645003
Parameter Units
Fecal Coliforms CFU/100 mL
QUALITY CONTROL DATA
Analysis Method: SM 9222D-2015
Analysis Description: 9222D Fecal Coliform( MF}-EDN
Laboratory: Pace Analytical Services - Eden
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO 1.0 03131/2315:44
METHOD BLANK: 3972590 Matrix: Water
Associated Lab Samples: 92659645001, 92659645003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms CFU/100 mL ND 1.0 03/31/23 15:44
SAMPLE DUPLICATE: 3972589
92659645003 Dup
Parameter Units Result Result RPD Qualifiers
Fecal Coliforms CFU/100 mL ND 1.0
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 04/11/2023 10:26 AM without the written consent of Pace Analytical Services, LLC.
Page 12 of 21
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I
QUALITY CONTROL DATA
Project: Forest Lake - MW's
Pace Project No.: 92659645
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QC Batch: 765354 Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92659645001, 92659645002, 92659645003, 92659645004, 92659645005
METHOD BLANK: 3974002 Matrix: Water
Associated Lab Samples: 92659645001, 92659645002, 92659645003, 92659645004, 92659645005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chloride mg/L ND 1.0 04/0112314:27
LABORATORY CONTROL SAMPLE: 3974003
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Chloride mg/L 50 47.5 95 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3974004 3974005
MS MSD
92659920001 Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec
Limits RPD Qual
Chloride mg/L 2.2 50 50 %6 53.6 97 103
90-110 6
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3974006 3974007
MS MSD
92659873001 Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec
Limits RPD Qual
Chloride mg/L 2700 50 50 53.4 54.4 101 103
90-110 2
ug/L
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 041111202310:26 AM without the written consent of Pace Analytical Services, LLC.
Page 13 of 21
aceAnalytical
www.pacolabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Forest Lake - MW's
Pace Project No.: 92659645
QC Batch: 766332 Analysis Method: EPA 350.1 Rev 2.0 1993
QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92659645001, 92659645002, 92659645003, 92659645004
METHOD BLANK: 3979033
Matrix: Water
Associated Lab Samples: 92659645001,
92659645002, 92659645003, 92659645004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Ammonia
mg/L
ND 0.10
04/07/23 11:13
LABORATORY CONTROL SAMPLE:
3979034
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits
Qualifiers
Nitrogen, Ammonia
mg/L
5
5.1
102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3979035
3979036
MS
MSD
92659503001
Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result
Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
Nitrogen, Ammonia
mg/L 29.8
5
5 34.5
34.5 92
93
90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3979037
3979038
MS
MSD
92659506001
Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result
Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
Nitrogen, Ammonia
mg/L 37.9
5
5 43.1
43.0 104
103
90-110 0
Results presented on this page are In the units Indicated by the "Units" column except where an attemato unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 04/11 /2023 10:26 AM without the written consent of Pace Analytical Services, LLC.
Page 14 of 21
(�AlceAnalyficalo
www.pacelabs.cem
QUALITY CONTROL DATA
Project: Forest Lake - MW's
Pace Project No.: 92659645
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
QC Batch: 766228
Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993
Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92659645001. 92659645002
METHOD BLANK: 3978659
Matrix: Water
Associated Lab Samples: 92659645001, 92659645002
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Phosphorus mg/L
ND 0.050 04/07/2310:49
LABORATORY CONTROL SAMPLE: 3978660
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Phosphorus mg/L
2.5 2.5 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3978661
3978662
MS MSD
92659506001
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD Qua]
Phosphorus mg/L 2.6
2.5 2.5 5.2 5.6 106 121
90-110 7 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3978663 3978664
MS MSD
92659599001
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD Qual
Phosphorus mg/L 1.2
2.5 2.5 3.7 3.8 99 101
90-110 1
Results presented on thls page are In the units Indicated by the "Units" column except whom an altemato unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/11/2023 10:26 AM without the written consent of Pace Analytical Services, LLC.
Page 15 of 21
aceAnalytical
www.pacclabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Forest Lake - MW's
Pace Project No.: 92659645
QC Batch: 766230 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92659645003, 92659645004
METHOD BLANK: 3978668 Matrix: Water
Associated Lab Samples: 92659645003, 92659645004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mg/L ND 0.050 04/07/2311:08
LABORATORY CONTROL SAMPLE: 3978669
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Phosphorus mg/L 2.5 2.6 103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3978670 3978671
MS MSD
92659645003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/L ND 2.5 2.5 2.6 2.6 104 104 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3978672 3978673
MS MSD
92659645004 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[
Phosphorus mg/L ND 2.5 2.5 2.6 2.6 105 104 90-110 1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 04/11/2023 10:26 AM without the written consent of Pace Analytical Services, LLC.
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aceAnalXical
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Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Forest Lake - MW s
Pace Project No.: 92659645
QC Batch: 766460
Analysis Method: SM 531OB-2014
QC Batch Method: SM 531OB-2014
Analysis Description: 5310E TOC
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92659645001, 92659645002,
92659645003, 92659645004
METHOD BLANK: 3979774
Matrix: Water
Associated Lab Samples: 92659645001, 92659645002,
92659645003, 92659645004
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Total Organic Carbon mg/L
ND 1.0
04/06/23 13:55
LABORATORY CONTROL SAMPLE: 3979775
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Total Organic Carbon mg/L
25 24.1
96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3979776 3979777
MS MSD
92660161001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Total Organic Carbon mg/L ND
25 25 23.6
23.4 93 92
90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3979778 3979779
MS MSD
92659645001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Total Organic Carbon mg/L 2.3
25 25 25.5
25.7 92 93
90-110 1
Results presented on this page are In the unite Indicated by the "Units" column except where an alternate unit is presentod to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 04/11/2023 10:26 AM without the written consent of Pace Analytical Services, LLC.
Page 17 of 21
aceAnalyfical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
QUALIFIERS
Project: Forest Lake - MW's
Pace Project No.: 92659645
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 04/11 /2023 10:26 AM without the written consent of Pace Analytical Services, LLC. Page 18 of 21
aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Forest Lake - MWs
Pace Project No.: 92659645
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92659645001
MW-1
SM 2540C-2015
765155
92659645002
MW-2
SM 2540C-2015
765155
92659645003
MW-3
SM 2540C-2015
765155
92659645004
MW-4
SM 2540C-2015
765155
92659645005
Effluent
SM 2540C-2015
765155
92659645001
MW-1
EPA 353.2 Rev 2.0 1993
765096
92659645002
MW-2
EPA 353.2 Rev 2.0 1993
765096
92659645003
MW-3
EPA 353.2 Rev 2.0 1993
765096
92659645004
MW-4
EPA 353.2 Rev 2.0 1993
765096
92659645001
MW-1
SM 922213-2015
765045
SM 922213-2015
92659645002
MW-2
SM 9222D-2015
765005
SM 922213-2015
92659645003
MW-3
SM 9222D-2015
765045
SM 922213-2015
92659645004
MW-4
SM 9222D-2015
765005
SM 922213-2015
92659645001
MW-1
EPA 300.0 Rev 2.1 1993
765354
92659645002
MW-2
EPA 300.0 Rev 2.1 1993
765354
92659645003
MW-3
EPA 300.0 Rev 2.1 1993
765354
92659645004
MW-4
EPA 300.0 Rev 2.1 1993
765354
92659645005
Effluent
EPA 300.0 Rev 2.1 1993
765354
92659645001
MW-1
EPA 350.1 Rev 2.0 1993
766332
92659645002
MW-2
EPA 350.1 Rev 2.0 1993
766332
92659645003
MW-3
EPA 350.1 Rev 2.0 1993
766332
92659645004
MW-4
EPA 350.1 Rev 2.0 1993
766332
92659645001
MW-1
EPA 365.1 Rev 2.0 1993
766228
EPA 365.1 Rev 2.0 1993
92659645002
MW-2
EPA 365.1 Rev 2.0 1993
766228
EPA 365.1 Rev 2.0 1993
92659645003
MW-3
EPA 365.1 Rev 2.0 1993
766230
EPA 365.1 Rev 2.0 1993
92659645004
MW-4
EPA 365.1 Rev 2.0 1993
766230
EPA 365.1 Rev 2.0 1993
92659645001
MW-1
SM 5310B-2014
766460
92659645002
MW-2
SM 5310B-2014
766460
92659645003
MW-3
SM 5310B-2014
766460
92659645004
MW-4
SM 5310B-2014
766460
Date: 04/11 /2023 10:26 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
765046
765006
765046
765006
766539
766539
766540
766540
Page 19 of 21
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Pace Upon Receipt
1-VII:rtI Effective Date: 0511212022
*Check mark top half of box if pH and/or dechlorination
is verified and within the acceptance range for
preservation samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DROf8015 (water) DOC, LLHe
**Bottom half of box is to list number of bottles
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pill upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot it
Note: wnenever ineie is a oiscrepancy anecting Nortn "ronna compliance samples, a copy of this form wdl ac sent to the No•th Carolina DEHNR Certification Ol(ice (i.e.
Out of hold, incorrect p(eservative, out of temp, incorrect containers)
Qualtrax Document ID: 70677
Page 2 of 2
Page 21 of 21