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Home My WebLink AboutWQ0000485_Monitoring - 03-2023_20230414Monitoring Report Submittal ..................................................... Permit Number#* WQ0000485 Name of Facility:* Month: * March Report Information Type * G W-59 Darling Ingredients - Rose Hill Confirmation Email Address: * Name of Submitter: * Signature: Date of submittal: Initial Review Year:* 2023 Upload Document* scan 2023-03 WQ0000485 GW-59 DIRH.pdf 3.83MB PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). corey.lanier@darlingii.com Corey Lanier c4��.1 je ' -'t Reviewer: Wanda.Gerald 4/14/2023 This will be filled in automatically Is the project number correct?* WQ0000485 Is the monitoring report accepted?* Yes No Regional Office* Wilmington Reviewer: _anonymous Review Date: 5/17/2023 DARLING Adb- INGREDIENTS April 6, 2023 Division of Water Resources Attn: Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: Ground Water Quality Monitoring Report (GWQMR) Darling Ingredients — Rose Hill Permit WQ0000485 To whom it may concern, Please find enclosed the Groundwater Quality Monitoring Compliance Report for Surface Irrigation for the month of March 2023 for our Rose Hill Division. Should you require any additional information or wish to discuss this matter, please feel free to contact me at 910.289.2083 x 25119. Sincerely, JTI"�4 4k Larry Holt General Manager cc: DI Regional Corporate Office GW-59A COMPLIANCE REPORT FORM Permit # W00000485 (Submit one each monitoring period with GW-59jorms.) ] Enter date monitoring results were due. (04130/2023) Will this monitoring report (GW-59 and GW-59A) be submitted after the established due date? No 2 Was any required information missing on the GW-59 report forms? No IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. MW-BA was damaged by farm equipment and is scheduled to be closed and replaced by Register Well Co, INC; moving the replacement well 10' due North perDEQ direction. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missingidentirication plate, area overgrown, etc.)? Ijlhe answer is "Yes ", contact the Regional Ofcefor pddance No 4 Are any monitored constituents equal to or above the established standards? YES If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below., SEE ATTACHED GROUNDWATER MONITORING WELL 2 YR EXCEEDANCE HISTORY REPORT 5 For the constituents identified in question 4 above, have standards been exceeded previously for the same constituent(s) In the same well(s) in the last two years? YES If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date toreach occurrence (tor the last two years). SEE ATTACHED GROUNDWATER MONITORING WELL 2 YR EXCEEDANCE HISTORY REPORT Are the monitoring wells listed In section 5 located at or beyond the review boundary? YES If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this groundwater quality problem? YES If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7Is "NO" contact the Re Iona! Ofrrce within 90 da • an evaluation may be required to determine the impao the waste disppsal system Is having at the review and core llance boundaries surrounding this fart . Failure to do so may subject the permiffee to a Notice of Wolatlon, fines, and/or allies. Additional monitoring was performed to identify constituents of TOC in MW No.9. The facility has been communicating with Mr. Geoff Kegley in the Wilmington Regional Office. g The person completing this portion (G W-59A) of the monitoring report should sign below and submit this form with G W-59 forms for required wells to the address provided at the top of the current G W-59 form. I hereby acknowledge that the above Information was evaluated and the information submitted in this report (Compliance Report GW-59A) is true and complete to the best of my knowledge. ju.L4 ]A �, 44,-Z62 Slgna tute of Pet Inea (or Authorized Agerro Date GW-59A 12/8/2003 Valley Proteins, Inc - Rose Hill (WQ0000485) Groundwater Monitoring Well 2 Year Exceedance History Report TDS 500 10A 11A 14A March-23 804 517 1310 November-22 833 583 944 July-22 772 510 1280 March-22 783 527 1100 November-21 801 722 1230 July-21 706 522 1010 March-21 684 866 pH 6.5-8.5 1 2 4 7A 8A 9 10A 11A 12B 13A March-23 6.40 6.30 6.30 3.86 4.50 6.70 4.10 4.50 4.20 4.80 November-22 5.60 6.30 3.86 4.20 6.00 3.67 4.10 3.70 4.40 July-22 6.40 6.40 6.3 5.1 5.3 6.4 4.2 4.6 4 5.1 March-22 6.40 5.9 4.7 4.6 4.6 4.4 4.2 4.7 November-21 5.50 4.30 4.50 6.30 4.00 4.30 4.20 4.20 July-21 5.00 6.10 5.60 4.90 4.60 5.90 4.70 4.60 5.40 March-21 6.40 5.70 4.90 4.70 5.30 5.00 5.10 5.90 TOC 10 9 March-23 33 November-22 27.6 July-22 45.1 March-22 34.9 November-21 26.4 July-21 25.9 March-21 32.9 Chloride 250 10A March-23 350 November-22 305 July-22 261 March-22 294 November-21 July-21 425 March-21 Sulfate 250 14A March-23 375 November-22 July-22 287 March-22 277 November-21 322 July-21 March-21 November-20 SUBMIT FORM ON YELLOW PAPER ONLY ■ DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM ■ ■ 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print ClearlyorType PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin (city) (Zip) X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: from PErmi[ SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-1 Date sample collected: 3/17/2023 FIELD ANALYSES: WAS Well Depth: 12.46 ft. Well Diameter: 2 in. pH4500HB 6.40 units Temp. 000lo: 16.6 oc DRY at Depth to Water Level 82546: 4.3 Screened Interval: 12.46 ft. to 2.46 ft, Spec. Cond. 00094: µMhos time of Measuring Point is 1.17 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear checy--I Samples for metals were collected unfiltered X YES p NO and field acidified: X YES M NO here: —! LABORATORY INFORMATION Date sample analyzed: 03/17/2023-04/03/2023 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 8 /100mL Nitrate (NO3) as N 00620 0.28 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.07 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 135.00 mg/L Al -Aluminum 01105 mg/L Sodium 6.33 mg/L pH (Lab) 00403 6.40 units Ba - Barium 01007 ug/L TOC 00680 1.2 mg/L Ca - Calcium 00916 mg/L Chloride 00940 8 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 69 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? E Yes (0) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732 method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Larry Holt - General Manager Permittee (or Authorized Aqent) Name and Title - Please print or type Siqnature Aqent) -(e •Z.0Z (Date) GW-59 Rev.8/2013 SUBMIT FORM ON YELLOW PAPER ONLY • • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery (city) (State) (zip) X Spray Field ❑ Remediation: Contact Person- Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-2 Date sample collected: 3/17/2023 FIELD ANALYSES: WAS Well Depth: 31.00 ft. Well Diameter: 2 in. pH4500HB 6.30 units Temp. 000lo 17.2 °C DRY at Depth to Water Level 82546: 13.6 ft. below measuring point Screened Interval_ 30.15 ft. to 20.15ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Tan Tint check here: Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 03/17/2023-04/03/2023 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: IMF Fecal 31616 <1.0 /100mL Nitrate (NO3) as N 00620 0.19 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.18 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids -.Total 70300 288.00 mg/L Al - Aluminum 01105 mg/L Sodium 11.8 mg/L pH (Lab) 00403 6.30 units Ba - Barium 01007 ug/L TOC 00680 1.2 mg/L Ca - Calcium 00916 mg/L Chloride 00940 11 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 33 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? = Yes (0) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732 method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen. NH3as N, Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 1.1 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Larry Holt - General Manag Permittee (or Authorized Anent) Name and Title - Please print or type Signature of Permittde (or Authorized Aqent) '2D (Date) CeFPd.�:� CZ�:lf�ly 63 SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3.!31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery (City) (State) (zip) X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-4 Date sample collected: 3/17/2023 FIELD ANALYSES: WAS Well Depth: 28.93 ft. Well Diameter: 2 in. pH45001113 6.30 units Temp. 000lo 16.3 °C DRY at Depth to Water Level 82546: 6.3 ft. below measuring point Screened Interval: 28.93 ft. to 18.93ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear check here: Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO LABORATORY INFORMATION Date sample analyzed. 03/17/2023-04/03/2023 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.16 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units). issolved Solids:Total 70300 216.00 mg/L Al - Aluminum 01105 mg/L Sodium 9.02 mg/L pH (Lab) 00403 6.30 units Ba - Barium 01007 ug/L TOC 00680 0.60 mg/L Ca - Calcium 00916 mg/L Chloride 00940 <5.0 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 <5.0 mg/L• Hg - Mercury 71900 ug/L Lab Report Attached? 0 Yes (0) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Larry Holt - General Managl Permittee (or Authorized Agent) Name and Title - Please print or type Signature o Permitt(or Authorized Agent) 1,_zoz (Date) GW-59 Rev.8/2013 1710 DEPARTMENT OF ENVIRONMENT S NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: 1)IVISION OF WATER RESOURCES • INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH. NC 27699-1617 Phone: 919-007-6306 FACILITY INFORMATION Please Print Clearly or Type !INPDES PERMIT Number: W00000485 Expiration Date:3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin rA ''"' X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-7A Date sample collected: 3/17/2023 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in pH4500HB 3.86 units Temp. 000lo: 21.7 oC DRY at Depth to Water Level 82546: 6.0 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094 µMhos time of Measuring Point is 2.42 ft. above land surface Relative M.P. Elevation: ft. Odor 00085 None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan check here:❑ Samples for metals were collected unfiltered: X YES M NO and field acidified: X YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 03/17/2023-04/03/2023 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.04 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 297.00 mg/L Al - Aluminum 01105 mg/L Sodium 36.4 m /L pH (Lab) 00403 3.86 units Ba - Barium 01007 ug/L TOC 00680 1.3 mg/L Ca - Calcium 00916 mg/L Chloride 00940 117 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 20 mg/L Hg - Mercury71900 ug/L Lab Report Attached? MYes (0) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; Nlj as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg1L VOG Removal% Larry Holt - General Manager Permittee (or Authorized Agent) Name and Title - Please print or type DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date 1.+3;/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation Infiltration Gallery (City) (State) (zip) X Spray Field ❑ Remediation Contact Person: Corey. Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name Field 5 - damaged by farm equip / to replace No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-8A Date sample collected: 3/17/2023 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 4.50 units Temp. 000lo: 16.1 °C DRY at Depth to Water Level 82546: 6.9 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 2.5 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sam 0 5.0 gallons Appearance Clear/Tan Tint checl� Samples for metals were collected unfiltered: X YES NO and field acidified: X YES ❑ NO here: LABORATORY INFORMATION Date sample analyzed: 03/17/2023-04/03/2023 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.58 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.24 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): )issolved Solids:Total 70300 65.00 mg/L Al - Aluminum 01105 mg/L Sodium 1.57 mg/L pH (Lab) 00403 4.50 units Ba - Barium 01007 ug/L TOC 00680 1.00 mg/L Ca - Calcium oo916 mg/L Chloride 00940 <5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 25 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? E Yes (0) ❑ No (0) Specific Conductance 00095 )tMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; Nljas N, Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCS: mg/L Effluent Total VOC& mg/L VOC Removal% . • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIViSfONOFWATERRESOURCES-INFORMATIONPROCESSINGUNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27899-1617 Phone:919-907-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3I3V202:5 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery (City) (State) (zip) X Spray Field ❑ Remediation: Contact Person Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-9 Date sample collected: 3/17/2023 FIELD ANALYSES: WAS Well Depth: 13.73 ft. Well Diameter: 2 in. pH4500HB 6.70 units Temp. 000lo: 14.4 oC DRY at Depth to Water Level e2546: 4.9 ft. below measuring point Screened Interval: 13.73 ft. to 3.73 ft. Spec. Cond. 00094: uMhos time of Measuring Point is 3.50 ft. above land surface Relative M.P. Elevation: ft. Odor 00065: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan/Brown checl., Samples for metals were collected unfiltered: X YES NO and field acidified: X YES ❑ NO here.Lj LABORATORY INFORMATION Date sample analyzed: 03/17/2023-04/03/2023 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.07 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.15 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.22 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 213.00 mg/L Al -Aluminum 01105 mg/L Sodium 3.69 m /L pH (Lab) 00403 6.70 units Ba - Barium 01007 ug/L TOC 00660 33.0 mg/L Ca - Calcium oo916 mg/L Chloride 00940 10 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 15 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? E Yes (01 ❑ No (0) Specific Conductance 00095 uMhos K - Potassium 00937 mg/L VOC 76732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; Nljas N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 1.7 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919.807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00000485Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin (city) (state) (zip) X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-10A Date sample collected: 3/17/2023 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 4.10 units Temp. 000l( 13.4 oC DRY at Depth to Water Level 82546: 4.1 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear check here:[--] Samples for metals were collected unfiltered: XYESM NO and field acidified: X YES NO LABORATORY INFORMATION Date sample analyzed: 03/17/2023-04/03/2023 Laboratory Name: Environmental Chemists, Inc. Certification No DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.10 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 804.00 mg/L Al - Aluminum 01105 mg/L Sodium 120 mg/L pH (Lab) 00403 4.10 units Ba - Barium 01007 ug/L TOC 00680 3.6 mg/L Ca - Calcium o0916 mg/L Chloride 00940 350 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 156 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? N Yes (0) ❑ No(0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732 method # SM 6200C Total Ammonia 00610 0.50 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; Nyas N; Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L , method # TKN as N 00625 0.80 mg/L Ni- Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal Io Larry Holt - General Manager Permittee (or Authorized Agent) Name and Title - Please print or type DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: VVQOCDG485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hilf, NC 28458 County Duplin (City) (State) (zip) X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MWA IA Date sample collected: 3/17/2023 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 4.50 units Temp. 000lc 14.7 °C DRY at Depth to Water Level 52546: 5.7 Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: uMhos time of Measuring Point is 3.3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear check Samples for metals were collected unfiltered: X YES NO and field acidified: X YES NO here: LABORATORY INFORMATION Date sample analyzed. 03/17/2023-04/03/2023 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 1.28 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus. Total as P 00665 0.08 mg/L (Note: Qse MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 517.00 mg/L Al - Aluminum 01105 mg/L Sodium 68.4 mg/L pH (Lab) 00403 4.50 units Ba - Barium 01007 ug/L TOC 00680 2.50 mg/L Ca - Calcium 00916 mg/L Chloride 00940 123 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 177.0 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? E Yes (0) ❑ No (0) pecific Conductance 00095 uMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; Nyas N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs Larry Holt - General Man Permittee (or Authorized Agent) Name and Title - Please print or type mg/L Effluent Total VOCs: Signature of Pbrm Ned (or Authorized Agent) mg1L VOC Removal% -[e-7c (Date) DEPARTMENT OF ENVIRONMENT&, NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES- INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1517 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 313112025 Facillty Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin rt ty r._!n,-r - X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: 910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-12B Date sample collected: 3/17/2023 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB: 4.20 units Temp. 000lo: 15.4 °C DRY at Depth to Water Level 82546: 6.6 ft. below measuring point Screened Interval: 20 ft. to 10 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear check here:❑ Samples for metals were collected unfiltered: X YES NO and field acidified: X YES M NO LABORATORY INFORMATION Date sample analyzed: 03/17/2023-04/03/2023 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.31 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 365.00 mg/L Al - Aluminum 01105 mg/L Sodium_74.4 m_g/L pH (Lab) 00403 4.20 units Ba - Barium 01007 ug/L TOC oo68o 1.90 mg/L Ca - Calcium oo916 mg/L Chloride 00940 97 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 126 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? N Yes (0) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NFtas N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 1.20 mg/L Ni - Nickel 01067 ug/L method # For Rernediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs. mg1L VOC Removal Io DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: OIVI31ON OF WATER RESOURCES -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: 919407�5306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin 1 ' ' .1'..X Spray Field ❑ Remediation: Contact Person Corey Lanier Telephone#: (910) 660-1173 r ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-13A Date sample collected: 3/17/2023 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 4.80 units Temp. 000io: 15.4 oC DRY at Depth to Water Level 82546: 6.1 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec Cond. 00094 µMhos kime of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 000m None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Tan Tint check Samples for metals were collected unfiltered: X YES NO and field acidified: X YES NO here: LABORATORY INFORMATION Date sample analyzed: 03/17/2023-04/03/2023 Laboratory Name: Environmental Chemists. Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NOZ) as N 00615 0.08 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.10 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 50.00 mg/L Al -Aluminum 01105 mg/L Sodium 4.84 m /L pH (Lab) 00403 4.80 units Ba - Barium 01007 ug/L TOC 00680 0.80 mg/L Ca - Calcium 00916 mg/L Chloride 00940 5 mg/L Cd - Cadmium o1027 ug/L Arsenic 01002 ug/L Chromium: Total o1o34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 6.00 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? M Yes (0) ❑ No (0) Specific Conductance o0095 µMhos K - Potassium 00937 mg/L VOC 78732 method # SM 6200C Total Ammonia 00610 <0.20 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NF4as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.50 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Totai VOCs: mg/L VOC Removal Id Permittee (or Authorized Agent) Name and Title - Please print or type Signature of (or Authorizes[ Agent) DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone:919.807-6306 FACILITY INFORMATION Please PrintCleartyorType PERMIT Number: WOOOOD485 Expiration Hate: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin (cny7 ) (Zip) X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (From Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-14A Date sample collected: 3/17/2023 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 5.00 units Temp. 000lc 158 °C DRY at Depth to Water Level 82546: 4.4 ft. below measuring point Screened Interval: 10 ft. to 2.5 ft. Spec. Cord. 00094: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear check Samples for metals were collected unfiltered: X YES M NO and field acidified: X YES NO here: LABORATORY INFORMATION Date sample analyzed: 03/17/2023-04/03/2023 Laboratory Name: Environmental Chemists, Inc. Certification No DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1.0 /100mL Nitrate (NO3) as N 00620 2.27 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.06 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): )issolved Solids:Total 70300 1310.00 mg/L Al -Aluminum 01105. mg/L Sodium 143 mg/L pH (Lab) 00403 5.00 units Ba - Barium 01007 ug/L TOC 00680 4.50 mg/L Ca - Calcium 00916 mg/L Chloride 00940 220 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 375 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? M Yes (0) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.20 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; Nyas N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 0.50 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg1L Effluent Total VOCs mg(L VOC Removal Larry Holt - General Manager 9' �-'247, Permittee (or Authorized Agent) Name and Title - Please print or type Signature ck Permt a (or Authorized Agent) (Date) F7- -71 ANALYTICAL & CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Apr 03, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-05441 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-13570 Site: MW-1 3/17/2023 12:05 PM Water jcb/envirochem Test Method Results Date Analyzed Color Color Depth to water, ft. Depth to Water, Ft Sodium EPA 200.7, Rev 4.4, 1994 Sulfate EPA 300.0, Rev. 2.1, 1993 Ammonia Nitrogen EPA 350.1, Rev. 20, 1993 Gallons bailed before sampling Gallons Bailed before sampling Odor Qualitative Total Dissolved Solids (TDS) SM 2540 C-2015 Temperature SM 2550 B-2010 pH SM 4500 H B-2011 Total Phosphorus SM 4500 P (F-H)-2011 Total Organic Carbon (TOC) SM 5310 B-2014 Fecal Coliform SM 9222 D-2015 MF Chloride SM4500 Cl E-2011 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0,1993 Nitrate Nitrogen Subtraction Method Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0, 1993 Total Nitrogen Total Nitrogen Clear 03/17/2023 4.3 feet 03/17/2023 6.33 mg/L 03/29/2023 69 mg/L 03/22/2023 < 0.2 mg/L 03/23/2023 5.0 gallons 03/17/2023 N/D 03/17/2023 135 mg/L 03/20/2023 16.6 C 03/17/2023 6.4 units 03/17/2023 0.07 mg/L 03/28/2023 1.2 mg/L 03/20/2023 <1 Coloniesl100ml- 03/17/2023 8 mg/L 03/20/2023 < 0.02 mg/L 0.28 mg/L 0.28 mg/L 03/17/2023 03/21 /2023 04/03/2023 < 0.5 mg/L 03/28/2023 <0.5 mg/L 04/03/2023 Report!k: 2023-05441 F117 6enviroechem ANALYTICAL & CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Lab ID Sample ID: 23-13571 Site: MW-2 Test Color Depth to water, ft. Sodium Sulfate Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature pH Total Phosphorus Total Organic Carbon (TOC) Fecal Coliform Chloride Nitrate Nitrogen (Calc) Nitrite Nitrogen Nitrate+ N itrite-Nitrogen Nitrate Nitrogen Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) Total Nitrogen Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ' 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Apr 03, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-05441 Project ID: Monitoring Wells Collect Date/Time Matrix Sampled by 3/17/2023 11:50 AM Water jcb/envirochem Method Color Depth to Water Ft EPA 200 7, Rev 4 4 1994 EPA 300 0, Rev 2 1, 1993 EPA 350 1, Rev 2 0.1993 Gallons Bailed before sampling Qualitative SM 2540 C-2015 SM 2550 B-2010 SM 4500 H B-2011 SM 4500 P (F-H)-2011 SM 5310 B-2014 SM 9222 D-2015 MF SM4500 Cl E-2011 EPA 353 2, Rev 2 0, 1993 EPA 353 2, Rev 2 0 1993 Subtraction Method EPA 351 2, Rev 2 0, 1993 Total Nitrogen Results Date Analyzed Clear/Tan Tint 03/17/2023 13.6 feet 03/17/2023 11.8 mg/L 03/29/2023 33 mg/L 03/22/2023 < 0.2 mg/L 03/23/2023 5.0 gallons 03/17/2023 N/D 03/17/2023 288 mg/L 03/20/2023 17.2 C 03/17/2023 6.3 units 03/17/2023 0.18 mg/L 03/28/2023 1.2 mg/L 03/20/2023 <1 Colonies/100ml- 03/17/2023 11 mg/L 03/20/2023 < 0.02 mg/L 03/17/2023 0.19 mg/L 03/21/2023 0.19 mg/L 04/03/2023 1.1 mg/L 03/28/2023 1.3 mg/L 04/03/2023 Report # 2023-05441 Page 2 of 11 ,e,n,viroehem ANALYTICAL & CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Lab ID Sample ID: 23-13572 Site: MW-4 Test Color Depth to water, ft. Sodium Sulfate Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature pH Total Phosphorus Total Organic Carbon (TOC) Fecal Coliform Chloride Nitrate Nitrogen (Calc) Nitrite Nitrogen Nitrate+Nitrite-Nitrogen Nitrate Nitrogen Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) Total Nitrogen Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ' 910-347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Apr 03, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-05441 Project ID: Monitoring Wells Collect Date/Time Matrix Sampled by 3/17/2023 11:15 AM Water jcb/envirochem Method Color Depth to Water, Ft. EPA 200.7, Rev 4A 1994 EPA 300.0, Rev. 2.1, 1993 EPA 350.1, Rev. 2.0, 1993 Gallons Bailed before sampling Qualitative SM 2540 C-2015 SM 2550 B-2010 SM 4500 H B-2011 SM 4500 P (F-H)-2011 SM 5310 B-2014 SM 9222 D-2015 MF SM4500 Cl E-2011 EPA 353.2, Rev. 2.0, 1993 EPA 353.2, Rev. 2.0, 1993 Subtraction Method EPA 351.2, Rev. 2.0, 1993 Total Nitrogen Results Date Analyzed Clear 03/17/2023 6.3 feet 03/17/2023 9.02 mg/L 03/29/2023 <5 mg/L 03/22/2023 < 0.2 mg/L 03/23/2023 5.0 gallons 03/17/2023 N/D 03/17/2023 216 mg/L 03/20/2023 16.3 C 03/17/2023 6.3 units 03/17/2023 0.16 mg/L 03/28/2023 0.6 mg/L 03/20/2023 <1 Colonies/100ml- 03/17/2023 < 5 mg/L 03/20/2023 < 0.02 mg/L 03/17/2023 < 0.02 mg/L 03/21/2023 0.02 mg/L 04/03/2023 < 0.5 mg/L 03/28/2023 <0.5 mg/L 04/03/2023 Reoort 9 2023-05441 0— 9 of i i envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax info@environmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Apr 03, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-05441 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-13573 Site: MW-7A 3/17/2023 10:45 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Clear/Tan Tint 03/17/2023 Depth to water, ft. Depth to water, Ft. 5.8 feet 03/17/2023 Sodium EPA 200.7, Rev 4.4, 1994 28.6 mg/L 03/29/2023 Sulfate EPA 300.0, Rev. 2.1, 1993 20 mg/L 03/22/2023 Ammonia Nitrogen EPA 350.1, Rev. 2.0, 1993 < 0.2 mg/L 03/23/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/17/2023 Odor Qualitative N/D 03/17/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 240 mg/L 03/20/2023 Temperature SM 2550 B-2010 15.8 C 03/17/2023 pH SM 4500 H B-2011 3.7 units 03/17/2023 Total Phosphorus SM 4500 P (F-H)-2011 0.12 mg/L 03/28/2023 Total Organic Carbon (TOC) SM 5310 B-2014 1.1 mg/L 03/20/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 03/17/2023 Chloride SM4500 Cl E-2011 97 mg/L 03/20/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 < 0.02 mg/L 03/17/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 < 0.02 mg/L 03/21/2023 Nitrate Nitrogen Subtraction Method <0.02 mg/L 04/03/2023 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0, 1993 < 0.5 mg/L 03/28/2023 Total Nitrogen Total Nitrogen <0.5 mg1L 04/03/2023 Parxvi l-- !)nva-n.Sddl 0-A ns„ Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax ism, 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5943 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemistacom Darling Ingredients - Rose Hill Date of Report: Apr 03, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-05441 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-13574 Site: MW-8A 3/17/2023 10:55 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Clear/Tan Tint 03/17/2023 Depth to water, ft. Depth to Water, Ft 6.9 feet 03/17/2023 Sodium EPA 200.7, Rev 4.4,1994 1.57 mg/L 03/28/2023 Sulfate EPA 300.0, Rev. 2.1, 1993 25 mg/L 03/22/2023 Ammonia Nitrogen EPA 350.1, Rev. 2.0, 1993 < 0.2 mg/L 03/23/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/17/2023 Odor Qualitative N/D 03/17/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 65 mg/L 03/20/2023 Temperature SM 2550 B-2010 16.1 C 03/17/2023 pH SM 450D H B-2011 4.5 units 03/17/2023 Total Phosphorus SM 4500 P (F-H)-2011 0.24 mg/L 03/28/2023 Total Organic Carbon (TOC) SM 5310 B-2014 1.0 mg/L 03/20/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100m L 03/17/2023 Chloride SM4500 Cl E-2011 < 5 mg/L 03/20/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 < 0.02 mg/L 03/17/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 20,1993 0.58 mg/L 03/21/2023 Nitrate Nitrogen Subtraction Method 0.58 mg/L 04/03/2023 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0, 1993 0.5 mg/L 03/28/2023 Total Nitrogen Total Nitrogen 1.1 mg/L 04/03/2023 ;?. frf L im'4-n1,da1 0....., C -F 41 F"P7— 41 <SM� ANALYTICAL & CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Apr 03, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-05441 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-13575 Site: MW-9 3/17/2023 11:28 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Tan/Brown 03/17/2023 Depth to water, ft. Depth to Water, Ft. 4.9 feet 03/17/2023 Sodium EPA 200.7, Rev 4.4,1994 3.69 mg/L 03/28/2023 Sulfate EPA 300.0. Rev. 21, 1993 15 mg/L 03/22/2023 Ammonia Nitrogen EPA 350.1, Rev. 2.0, 1993 < 0.2 mg/L 03/23/2023 Gallons bailed before sampling Gallons Balled before sampling 5.0 gallons 03/17/2023 Odor Qualitative N/D 03/17/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 213 mg/L 03/20/2023 Temperature SM 2550 B-2010 14.4 C 03/17/2023 pH SM 4500 H B-2011 6.7 units 03/17/2023 Total Phosphorus SM 4500 P (F-H)-2011 0.22 mg/L 03/28/2023 Total Organic Carbon (TOC) SM 5310 B-2014 33.0 mg/L 03/20/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 03/17/2023 Chloride SM4500 CI E-2011 10 mg/L 03/20/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 0.07 mg/L 03/17/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0,1993 0.22 mg/L 03/21/2023 Nitrate Nitrogen Subtraction Method 0.15 mg/L 04/03/2023 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0,1993 1.7 mg/L 03/28/2023 Total Nitrogen Total Nitrogen 1.9 mg/L 04/03/2023 Report #:: 2023-05441 — _ P— A a , , F7007 -, ""7 GSM ANALYTICAL & CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392,4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Apr 03, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-05441 Project ID: Monitoring Wells Lab ID Sample ID: 23-13576 Site: MW-10A Test Collect DatelTime 3/17/2023 9:35 AM Method Matrix Sampled by Water jcb/envirochem Results Date Analyzed Color color Clear 03/17/2023 Depth to water, ft. Depth to water, Ft. 4.1 feet 03/17/2023 Sodium EPA200.7, Rev 4.4,1994 120 mg/L 03/28/2023 Sulfate EPA 300.0, Rev. 2.1, 1993 156 mg/L 03/22/2023 Ammonia Nitrogen EPA 350.1, Rev. 2.0, 1993 0.5 mg/L 03/23/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/17/2023 Odor Qualitative N/D 03/17/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 804 mg/L 03/20/2023 Temperature SM 2550 B-2010 13.4 C 03/17/2023 pH SM 4500 H B-2011 4.1 units 03/17/2023 Total Phosphorus SM 4500 P (F-H)-2011 0.10 mg/L 03/28/2023 Total Organic Carbon (TOC) SM 5310 B-2014 3.6 mg/L 03/20/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 03/17/2023 Chloride SM4500 Cl E-2011 350 mg/L 03/20/2023 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 < 0.02 mg/L 03/17/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 < 0.02 mg/L 03/21/2023 Nitrate Nitrogen Subtraction Method <0.02 mg/L 04/03/2023 Total Nitrogen (Cale) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0,1993 0.8 mg/L 03/28/2023 Total Nitrogen Total Nitrogen 0.8 mg/L 04/03/2023 P-rt It na_nredt ___ [envi7roche1m :l:;A ANALYTICAL & CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmenta lchemi sts.com Date of Report: Apr 03, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-05441 Project ID: Monitoring Wells Lab ID Sample ID: 23-13577 Site: MW-11A Test Collect Date/Time 3/17/2023 9:20 AM Method Matrix Sampled by Water jcb/envirochem Results Date Analyzed Color Color Clear 03/17/2023 Depth to water, ft. Depth to Water. Ft 5.7 feet 03/17/2023 Sodium EPA 200.7, Rev 44, 1994 68.4 mg/L 03/28/2023 Sulfate EPA 300.0, Rev 2.1, 1993 177 mg/L 03/22/2023 Ammonia Nitrogen EPA 350 1. Rev 2 0,1993 < 0.2 mg/L 03/23/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/17/2023 Odor Qualitative N/D 03/17/2023 Total Dissolved Solids (TDS) SM 2540 c-2015 517 mg/L 03/20/2023 Temperature SM 2550 B-2010 14.7 C 03/17/2023 pH SM 4500 H B-2011 4.5 units 03/17/2023 Total Phosphorus SM 4500 P (F-H)-2011 0.08 mg/L 03/28/2023 Total Organic Carbon (TOC) SM 5310 B-2014 2.5 mg/L 03/20/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 03/17/2023 Chloride SM4500 CI E-2011 123 mg/L 03/20/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 < 0.02 mg/L 03/17/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0,1993 1.28 mg/L 03/21 /2023 Nitrate Nitrogen Subtraction Method 1.28 mg/L 04/03/2023 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2 0, 1993 < 0.5 mg/L 03/28/2023 Total Nitrogen Total Nitrogen 1.3 mg/L 04/03/2023 R.n rt it•• 7n77-n.rdd1 Pan. R of l l :enviriochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Apr 03, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-05441 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-13578 Site: MW-12B 3/17/2023 10:00 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Clear 03/17/2023 Depth to water, ft. Depth to Water, Ft 6.6 feet 03/17/2023 Sodium EPA200.7, Rev 44, 1994 74.4mg/L 03/28/2023 Sulfate EPA 300.0, Rev_ 2.1, 1993 126 mg/L 03/22/2023 Ammonia Nitrogen EPA 350 1, Rev 2 0, 1993 < 0.2 mg/L 03/23/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/17/2023 Odor Qualitative N/D 03/17/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 365 mg/L 03/20/2023 Temperature SM 2550 B-2010 15.4 C 03/17/2023 pH SM4500 H B-2011 4.2 units 03/17/2023 Total Phosphorus SM 4500 P (F-H)-2011 0.31 mg/L 03/28/2023 Total Organic Carbon (TOC) SM 5310 B-2014 1.9 mg/L 03/20/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 03/17/2023 Chloride SM4500 Cl E-2011 97 mg/L 03/20/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 < 0.02 mg/L 03/17/2023 Nitrate+Nitrite-Nitrogen EPA353.2, Rev. 2.0, 1993 < 0.02 mg/L 03/21/2023 Nitrate Nitrogen Subtraction Method <0.02 mg/L 04/03/2023 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev, 2.0, 1993 1.2 mg/L 03/28/2023 Total Nitrogen Total Nitrogen 1.2 mg/L 04/03/2023 rnvirochem 6 ANALYTICAL S CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Apr 03, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-05441 Project ID: Monitoring Wells Lab ID Sample ID: Collect DatelTime Matrix w Sampled by 23-13579 Site: MW-13A 3/17/2023 9:50 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Clear/Tan Tint 03/17/2023 Depth to water, ft. Depth to water, Ft 6.1 feet 03/17/2023 Sodium EPA200.7, Rev 4.4,1994 4.84 mg/L 03/28/2023 Sulfate EPA 300.0, Rev. 2.1, 1993 6 mg/L 03/22/2023 Ammonia Nitrogen EPA 350.1, Rev. 2.0, 1993 < 0.2 mg/L 03/23/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/17/2023 Odor Qualitative N/D 03/17/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 50 mg/L 03/20/2023 Temperature SM 2550 B-2010 15.4 C 03/17/2023 pH SM 4500 H B-2011 4.8 units 03/17/2023 Total Phosphorus SM 4500 P (F-H)-2011 0.10 mg/L 03/28/2023 Total Organic Carbon (TOC) SM 5310 B-2014 0.8 mg/L 03/20/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 03/17/2023 Chloride SM4500 Cl E-2011 5 mg/L 03/20/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 0.08 mg/L 03/17/2023 Nitrate+Nitrite-Nitrogen EPA353.2, Rev. 2.0,1993 < 0.02 mg/L 03/21/2023 Nitrate Nitrogen Subtraction Method <0.02 mg/L 04/03/2023 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev 2 0,1993 < 0.5 mg/L 03/28/2023 Total Nitrogen Total Nitrogen <0.5 mg/L 04/03/2023 ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252,473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Apr 03, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-05441 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-13580 Site: MW-14A 3/17/2023 10:35 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Clear 03/17/2023 Depth to water, ft. Depth to water, Ft 4.4 feet 03/17/2023 Sodium EPA200.7, Rev 4.4, 1994 143 mg/L 03/28/2023 Sulfate EPA 300.0, Rev. 2 1, 1993 375 mg/L 03/22/2023 Ammonia Nitrogen EPA 3501. Rev 2.0, 1993 < 0.2 mg/L 03/23/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/17/2023 Odor Qualitative N/D 03/17/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 1310 mg/L 03/20/2023 Temperature SM 2550 B-2010 15.8 C 03/17/2023 pH SM 4500 H B-2011 5.0 units 03/17/2023 Total Phosphorus SM 4500 P (F-H)-2011 0.06 mg/L 03/28/2023 Total Organic Carbon (TOC) SM 5310 B-2014 4.5 mg/L 03/20/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 03/17/2023 Chloride SM4500 Cl E-2011 220 mg/L 03/20/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 < 0.02 mg/L 03/17/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 2.27 mg/L 03/22/2023 Nitrate Nitrogen Subtraction Method 2.27 mg/L 04/03/2023 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0, 1993 0.5 mg/L 03/28/2023 Total Nitrogen Total Nitrogen 2.8 mg/L 04/03/2023 Comment: Reviewed by: Report'# • 2023.05441 Pane 11 nf 114 Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmington, NC 28405 910 392.0223 Sample Receipt Checklist Clientb� N� _Date3—/ Report Number: 2023- Q __ Receipt of sample. ECHEM Pickup. Client Delivery El ❑ FeclEx El Other ❑ ❑ YE5 ❑ NO N/A 1. V�Jere custody seals present on the cooler? ❑ YES ❑ NO N/A 12. If custody seals were present, were they intact/unbroken? Original temperature upon receipt C Corrected temperature upon receipx How temperature taken: ❑ Temperature Blank Against Bottles IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0 12 YES ❑ NO 3 if temperature of Cooler exceeded 6-C, was Projece.Mgr:/QA notified? YES ❑ NO 4 Were proper custody procedures (rellnclulshed/received) followed? YES ❑ NO S Were sample ID's listed on the COC? YES ❑ NO 6 Were samples ID's listed on sample containers? YES 10 7 Were collection date and time listed on the COC? EYES �01N 8 Were tests to b� performed listed on the COC? 9 D;d samples arrive in proper containers for each test? YES ❑ NO 10 Did samples arrive in good condition for each test? YES ❑ NO 11 Was adequate sample volume available?' YES ❑ NO 12 VVere samples received within proper holding time for requested tests? YES ❑ NO 13 Were acid preserved samples received at a pH of <2? YES ❑ f•1O 14 Were cyanide 5a,nlp:e; received at a pH >12? ❑ YES ❑ NO 15 Were sulfide samples received at a pH >9? YES ❑ N0 16 Were N'-13/TKN/Pheno1 received at a chlorine residual a` <0 5 m/c? ❑ YES ❑ NO 17 "e:e 5J f.de/C+;an de rtce,ved a: a ch'orine residual o- <0.5 M/c? ❑ 'rES ❑ NO I 18 V,'ere o'thophrp'n}:e s3mp'-_; filtered In the field wi:h•n 15 minu:es? * -0�_/Vc a: _s a•= �:-I ci _:P='c a, un-e c` 2-,a •, 73:.c'ia 53T0 2. arc Cr(cC (fir Cn'Jr,')c o: - , o C^- ,J •, __o`d__7 c'•i rrh_ ben Sample Preservation j3-1i0'a(_) o, aJd n` (z rcle one) ('•1J5 be COnlp'=:ed fD' an anlp ?(s) InCO'rectiy p'Ei=rV d Or headS0a:^i mCc :=d IiCO'rEC`'� p'_ er,ed and .,ere 2J;u5:ed a:co-d - H SO_ H`JD, H-i N30H I i-ne a. p,_ser\3- 0 i n'o'e tnan Ong p`e5erva;,.e is needed, n0:ale in commen:zz bz ^: :�Oa:��i Sanlp el�) COMMENTS: = :;ere received v, th headspace DOC QA 002 Rev 1 =C Date: 4 Analyst: Jay Baker Certification k 94 Facility Name: Permit #• PH Reference Method: SM4500 H+B -2011 Calibration Time Cal Buffer4.0 s.0 Cal Buffer 10.0 sm. Check Buffer 7.0 s.u. *PH check buffer must read within t 0.1 pH units of the buffer's true value. su buffer La1#1 _ Rkca_4112869 Fsco 31173 7 su buffer Lot#/:_R'c&a 2112A38_ Exo, 12f-.3 �4 1 Sample location Sample Ti _�: Iz 2- -h- i-� 2 � 11 ► Post analY sls buffer ch k I red Instrument ID: STARA221 : R06 Comments 10anbufferLOW, RICCA2I12750 BV 5Ji3 Collection Sample Analysis pH Result ►Post -analysis Buffer su Checkvalues.u. Comments/DataQualifiers 5n _• 150 � _ - -- l `� 1 l IS 10•32 � � -� b�45 I Oy5 3.72ea — - f II $s loss L-.4-1 h ec s requr w en perrumnrng analyses at multiple sampling locations and must be within t 0.1 units ofthe buffer's true value All pH values in pH units (i.e., s.u.). Record all data to the nearest 0.01 s.u. and report to the nearest 0.1 s.u. Total Residual Chlorine (TRC) Refcrence Method: SM 4500 CI-G20I I: Hach 8l6711R_ [ Pleasc Circle applicable Method) fnstrument ID. HACH Colorimeter 15120E289091 Dail • Check Post -analysis S Time check Sample Sample Standard Result Check Std. Sample TRC Result Standard Collection Analysis Comments/Data (when analyzing Location mg/L Qualifiers µgJL or mg/L at mulliole sites) Analyzed Time Time µP,/L or m TRC Daily Check Standard true value _ _ µ A or mg/I, acceptance range µg/L or mg/L GEL STDS 11ACH A0038 Check standards must recover within f 10% of the check standard's true value Annual Calibration Curve Verification Date: 11/25/22 LOT# IDE1iDC 220129 TjeelFatp.l7a�; 2t2gr13 II}EXX220130 lTotall axp, TiW 8a3 Reagent Blank Value: (When applicable. Analyze and document a reagent blank when standards, sample dilutions or PT Samples are prepared) Dissolved Oxygen (DO) Reference Method:SM 4500 0 G-201b Instrument ID: VS] PRO 20 22D100065 Calibration variable • Post -analysis calibration Calibration/ Meter reading verification (when necessary) Verification Time Temp Barometric Salini pressure Ty oC mmH ppt Sample Location Sample Collection Time or % efficiency after calibration Theoretical Calculated Value mg/L I Value mg/L 'Sample Analysis f DO reading Time J MPA. Comments Use this row when performing a k erif3cs3lien Comments/Data Qualifiers ♦ When performing analyses at multiple locations, the meter must be recallbraled at each site before analysis or a post -analysis calibration verification must be performed. • Irsample is measured directly in the stream and/or onsile, only time analyzed would be recorded with a note that they are measured in situ or immedialeh Temperature Reference Method; SM 2550 B-2010 Instrument ID STARA221 : K06795 Sample Sample Temperature Sample Location Collection Analysis °C Comments/Data Qualifiers Time Time Sife Z 1 IS 4\50 5 H-C 4 1 l► 5 t i-e I D4S 1 I �r_,33c, I lrsample is measured direct]) in the stream and/or on site, Annual Verification Date 11-25-22 Field Pemannet Note: %V•r time analyzed Would be recorded, with a note that they are measured in situ or immediately of QA.00112101122 Rev 1-2022 ec s requr w en perrumnrng analyses at multiple sampling locations and must be within t 0.1 units ofthe buffer's true value All pH values in pH units (i.e., s.u.). Record all data to the nearest 0.01 s.u. and report to the nearest 0.1 s.u. Total Residual Chlorine (TRC) Refcrence Method: SM 4500 CI-G20I I: Hach 8l6711R_ [ Pleasc Circle applicable Method) fnstrument ID. HACH Colorimeter 15120E289091 Dail • Check Post -analysis S Time check Sample Sample Standard Result Check Std. Sample TRC Result Standard Collection Analysis Comments/Data (when analyzing Location mg/L Qualifiers µgJL or mg/L at mulliole sites) Analyzed Time Time µP,/L or m TRC Daily Check Standard true value _ _ µ A or mg/I, acceptance range µg/L or mg/L GEL STDS 11ACH A0038 Check standards must recover within f 10% of the check standard's true value Annual Calibration Curve Verification Date: 11/25/22 LOT# IDE1iDC 220129 TjeelFatp.l7a�; 2t2gr13 II}EXX220130 lTotall axp, TiW 8a3 Reagent Blank Value: (When applicable. Analyze and document a reagent blank when standards, sample dilutions or PT Samples are prepared) Dissolved Oxygen (DO) Reference Method:SM 4500 0 G-201b Instrument ID: VS] PRO 20 22D100065 Calibration variable • Post -analysis calibration Calibration/ Meter reading verification (when necessary) Verification Time Temp Barometric Salini pressure Ty oC mmH ppt Sample Location Sample Collection Time or % efficiency after calibration Theoretical Calculated Value mg/L I Value mg/L 'Sample Analysis f DO reading Time J MPA. Comments Use this row when performing a k erif3cs3lien Comments/Data Qualifiers ♦ When performing analyses at multiple locations, the meter must be recallbraled at each site before analysis or a post -analysis calibration verification must be performed. • Irsample is measured directly in the stream and/or onsile, only time analyzed would be recorded with a note that they are measured in situ or immedialeh Temperature Reference Method; SM 2550 B-2010 Instrument ID STARA221 : K06795 Sample Sample Temperature Sample Location Collection Analysis °C Comments/Data Qualifiers Time Time Sife Z 1 IS 4\50 5 H-C 4 1 l► 5 t i-e I D4S 1 I �r_,33c, I lrsample is measured direct]) in the stream and/or on site, Annual Verification Date 11-25-22 Field Pemannet Note: %V•r time analyzed Would be recorded, with a note that they are measured in situ or immediately of QA.00112101122 Rev 1-2022 Date: -3 � ( ` 123 Analyst: Jay Baker Certification # 94 Facility Name: rrccC%L� Permit #: v N 'F— ( ( o pH Reference Methods SW5M 14t11-2011 fact,- ,.t rn• -qTA R A7.71 - 14AW )C, Calibration Time Cal Buffer 4.0 s.u. Cal Buffer 10.0 s.u. Check Buffer 7.0 s u Comments Eq:'. 00 L� . O l O 10 . D 1 () --j . 0IJ (-0 *pH check buffer must read within t 0.1 pH units of the buffer's true value. 4 su buffer Lof4/,, Ricea_4] 12$69 Txo 11t23 7 su bpffer Lotik Ricca 2112A38 Exa. 1=3 ] 0 su buffer Loth _ _ RICCA 2112750 E42 5113 Sample location p Sample Collection Time* Sample Analysis Time♦ pH Result s.0 ►Post -analysis Buffer Check value s u Comments/Data Qualifiers +e i o R G13� Gt 35 +e 20 �zv 1k� 000 slizA- `1So ■ rest analysts butter check is required when pFrtanning analyses at multiple sampling locations and must be within f 0.1 units orthc buffer's true value All pH values in pH units (i.e., s.u.). Record all data to the nearest 0.01 s.u. and report to the nearest 0.1 s u Total Residual Chlorine (TRC) Reference Method: SM 4500 C602011 Hach 816711R: (Please circle applicable Meiliod insvisment ID: I-IACH Colorimeter 15120F299091 Daily Check Post -analysis Check Std. Time check Sample Sample Sample TRC Result Standard Result (when analyzing Standard Location Collection Analysis pB/L or mgIL Comments/Data Qualifiers pg/L or mg/L at multiple sites) Analyzed Time Time I KC Daily Check Standard true value µg/L or mg/L acceptance range pCJL or mglL GEL STDS HACH A0038 Check sttmdnrds must recover within t 10% of the check standard's true value Annual Cal ibration Curve Verification Bate: 11/25/22 LOT 4 _TDEXX220129 (Free) ] xp. Dale-- 21203 WE X 22��,�q CT4bd I7atet 2r1823 Reagent Blank Value: When applicable. Analyze and document a reagent blank when standards, sample dilutions or PT Samples are prepared) Dissolved Oxygen (DO) Reference Method:SM 45000 G-2016 Instrument ID: YSI PRO 20 22DI0(I065 Calibration/ Calibration variable Meter reading •Post -analysis calibration verification (when necessary) Verification Time or % efficiency after calibration Comments Temp °C Barometric pmmHressure Salinity, ppt Theoretical Value mg/L Calculated Value mg/L Use this row %hen perrorming a verification instead or Galin ti n Sample Location p Sample Collection Time *Sample Analysis Time DO reading me/L Comments/Data Qualifiers ♦ When performing analyses at multiple locations, the meter must be recWtbrated at each site before analysis or a post -analysis calibration verification must be performed Ifsample is measured directly in the stream and/or onsite, only time anal) 7ed could be recorded A%ith a note that lhe) are treasured in situ or immediateli Temperature Reference Method. SM 2550 B-2010 Instrument ID STARA221 : K06795 Sample Location Sample Collection Time *Sample Analysis Time Temperature °C Comments/Data Qualifiers f e al (24�a t28 �t-ia ire R- C1 35 Se 11 20 l23 1 ado JIDOO IS.y 'A- 3 Ar 5sp I lSa`t - 1 f sampiv is measured directh in die stream anJ/nr on site only time analyzed «ould be recorded, pith a note that ft% are measured m situ or immedmleh Annual Verification Date 11-25-22 Field Personnel Note: QA.001 12/01/22 Date: �1 k—T1 2_S Analyst: Jav Baker ` Certification # 94 Facility Name: wR1� l� r�tCn� Permit #: PR Reference Method: SM4500 H+B -2011 Insmmicnt 0 STARA221 : K06795 Calibration Time Cal Buffer 4.0 s u Cal Buffer 10.0 s.u. Check Buffer 7.0 s u. Comments ib D•oo L�,p( to•01 (41 - .L-ji n *pH check buffer must read within t 0 l pH units of the buffer's true value 4 su buffer LotiVi r w 4112869 Exy i IM 7 su buffer Lot#/: Ricca 2112A38 x e 12i13 10 su buffer Lot#.,RfCCA 2112,750 ED.. _jP3 Sample location Sample Collection Time• Sample Analysis Ttme* p11 Result s.0 ►Post -analysis Buffer Check value s.u.I've Comments/Data Qualifiers k I_D35,- . _..tn,35 l:.,! !_ _ ► Post analysis buffer check is required when performing analyses at multiplo sampling locations and must be within t 0.1 units oftha huffer's true value All pH values in pH units (i e ; s u.) Remrd altdata to themeatest-DJ01s_tt_andnport to the newest-0-1 s.0 .__ Total Residual Chlorine (TRC) Reference Method: SM 4500 CI-G201 I: Hach 8167 HR: ( Please circle applicable Method) Instrument ID: HACH Colorimeter 1512OE289091 Daily Check Post -analysis Check Std. Time check Sample Sample Sample TRC Result Standard Result (when analyzing Standard Location Collection Analysis pg/L or mg/L Comments/Data Qualifiers µg/L or mg/L at multiple sites) Analyzed Time Time TRC Daily Check Standard true t:alue µgfL or mg/L acceptance range___ _ µg/L or mg/L GEL STDS HACH A0038 Check standards must recover within t10% of the check standard's true value Annual Calibration Curve Verification Date: 11/25/22 LOT #. IDEXX 720129 (Free) Exp. Date: ga&123 iC�y24i3Q:�lot�ljExn DatrR2rlSli3 Reagent Blank Value: (Wizen applicable. Analyze and document a reagent blank when standards, sample dilutions or PT Samples are prepared) Dissolved Oxygen (DO) Reference Method SM 4500 O G -2016 Instrument ID: YSI PRO 20 221] 100065 Calibration/ Calibration variable Meter reading *Post -analysis calibration verification (when necessary) Verification Time or % efficiency after calibration Comments Temp °C Barometric pnms1lure Salinity, ppt Theoretical Value mg/L Calculated Value mg/L Use this ron when performing a verification instead of ih ti Sample Location Sample Collection Time *Sample Analysis Time DO reading me/L Comments/Data Qualifiers • When perrorming analyses w multiple locations, the meter must be recalibrated at each site before analysis or a post -analysis calibration verification must be performed If sample is measured dircctl) in the stream and/or onsne, only time =137cd N%ould be recorded with a note that they are measured in situ or immedmtel) Temperature Reference Method SM 255D B-2010 Instrument 1D: STARA221 : K06795 Sample Location Sample Collection Time *Sample Analysis Time Temperature °C Comments/Data Qualifiers L4 R Itae, 15,fs • lfsample is measured directly in the stream andlor on site, only time analyzed %tiould he reeorded, itith a note that they are measured in situ or immediatcl) Annual Verification Date 11-25-22 Field Personnel Note: QA.001 12/01122 D-1 1 '1A'1'1 mington ENVIRONMENTAL CHEMISTS, INC OFFICE: 9101392-0223iIFAX910392- 4245 Analytical 8 Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Darling Ingredients -Rose Hill PROJECT NAME: Monitoring Wells Mar/Jul/Nov REPORT NO: �L3 �yYl ADDRESS: CONTACT NAME: Susan Price PO NO: REPORT TO: Corey Lanier PHONE/FAX: COPY TO: email: Sampled By: j' SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection E C 0 COL S r, 0 c° �a r E m gz PRESERVATION ANALYSIS REQUESTED t Time Temp z z = c = o s 0 z o W o Site: ` /Go A. L MW C P X NO2, Chloride, TDS, Sulfate G G 97 �• X L NO3, NH3, TP, TN (calc G G C PL X 2f I INa G G Pit C P X Fecal Coliform G G 04 aj C P X TOC G G .0 C P X VOC (November on! )__ G G C P G G C P G G C P G G Transfer Relinquished By, Date/Time Received By: DatelTime 1. 2. 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