WQ0009267_Monitoring - 03-2023_20230503

Monitoring Report Submittal
Permit Number#*
Name of Facility:*
Month: * March
Report Information
Type *
GW-59
WQ0009267
City of Jacksonville WWTP
Confirmation Email Address: *
Name of Submitter: *
Signature:
Date of submittal:
Initial Review
Year:* 2023
Upload Document*
WQ0009267 March 2023 GW-59 MW Report, 22.75MB
VOCs Attached.pdf
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
[e-mail]
Amy Palaschak
5/3/2023
This will be filled in automatically
Reviewer: Wanda.Gerald

Is the project number correct?* WQ0009267
Is the monitoring report accepted?* Yes No
Regional Office* Wilmington
Reviewer: _anonymous
Review Date: 5/12/2023

GW-59A COMPLIANCE REPORT FORM Permit #_WQ0009267
(Submit one each monitoring period with GW-59 forms.)
1
Enter date monitoring results were due. (4/30/2023) Will this monitoring report (GW-59 and GW-59A) be
YES
NO
submitted after the established due date?
2
Was any required information missing on the GW-59 report forms?
YES
NO
IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Office for guidance.
4
Are any monitored constituents equal to or above the established standards?
YES
NO
If the answer to question 4 is "NO", skip to section S. If the answer to question 4 is "YES" list the affected wells
individually with constituent(s) and concentration(s) exceeding standards in the space provided below:
MW 3 — VOCs — Chloromethane 0.73 ug/L, p-Isopropyltoluene 21.5 ug/L, Toluene 13.7 ug/L
MW 5 — VOCs — p-Isopropyltoluene 0.62 ug/L
MW 10 — TDS 618.5 mg/L
5
For the constituents identified in question 4 above, have standards been exceeded previously for the same
YES
NO
constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space
provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample
collection date for each occurrence (for the last two years).
MW3 — 12/2020 (Toluene 25.0 ug/L, p-Isopropyltoluene 24.2 ug/L), 12/2022 (Toluene 10.6 ug/L,
p-Isopropyltoluene 18.8 ug/L)
MW10 — all TDS — 3/2021 (683 mg/L), 6/2021 (657 mg/L), 9/2021 (675 mg/L), 12/2021 (633 mg/L), 3/2022
(607.5 mg/L), 6/2022 (577 mg/L), 9/2022 (560.5 mg/L), 12/2022 (660 mg/L)
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE
IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact
the Regional Office.
7
Is the permittee implementing previously approved actions required by the Division involving this groundwater
YES
NO
quality problem?
If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to
question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be required to determine the
impact the waste disposal system is having at the review and compliance boundaries surrounding this facility.
Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties.
MW10 — high background TDS — noted in current permit
MW3/MW6 — Tom Tharrington (NC DEQ, DWR) was contacted on Friday, April 28, 2023 regarding the
VOC presence in MWs. VOCs will be sampled again in June 2023 with the quarterly set.
8
The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form
with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby acknowledge that the above information was evaluated and the information submitted in this
report (Compliance Report GW-59A) is true and complete to the best of my knowledge
04/28/2023
Si nature f ermittee(or Authorized Agent) Date
GW-59A 12/8/2003

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address:
716 Firetower
Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
(AY
Zip,
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-1
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-1
Date sample collected: 3/20/2023
FIELD ANALYSES:
WAS
Well Depth: 16.6 ft.
Well Diameter: 2 in.
pH 00400: 5.4 units Temp. 000lo: 12.1 °C
DRY at
Depth to Water Level 82546: 5.9 ft. below measuring point Screened Interval: 3 ft. to
13 ft. Spec. Cond. 00094: µMhos
time of
sampling,check
Measuring Point is 3.2 ft. above land surface
Relative M.P. Elevation: 2.7 ft.
Odor 000s5:
Volume of water pumped/bailed before sampling:
5.14
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/20/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 0.05
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 135.5
mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC 00680 11.7
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 44
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 17
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia oo6lo <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Permittee (orAut
G W-59
Wally Hansen - Public Services Director
!d Agent) Name and Title - Please print or tvoe
Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
DPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
Elm
DVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville Land Treatment System
Non -Discharge WQ0009267 UIC
Permit Name (if different):
NPDES Other
Facility Address:
716 Firetower
Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
X Spray Field El Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-2
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-2
Date sample collected: 3/20/2023
FIELD ANALYSES:
WAS
Well Depth: 17.0 ft.
Well Diameter: 2 in.
pH 00400: 5.6 units Temp. 000lo: 14.1 °C
DRY at
Depth to Water Level 82546: 5.2 ft. below measuring point Screened Interval: 3 ft. to
13 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 2.4 ft. above land surface
Relative M.P. Elevation: 2.8 ft.
Odor 000m:
check
Volume of water pumped/bailed before sampling:
5.66
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/20/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 0.05
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids -.Total 70300 204.5
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 5.61
units
Ba - Barium 01007
ug/L
TOC 00680 0.9
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 68
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 8
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 00610 0.24
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print
Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville Land Treatment System
Non -Discharge WQ0009267 UIC
Permit Name (if different):
NPDES Other
Facility Address:
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
Jacksonville NC
28540 County Onslow
❑ Lagoon ❑ Remediation: Infiltration Gallery
�-ity1
71,
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-3
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-3
Date sample collected: 3/22/2023
FIELD ANALYSES:
WAS
Well Depth: 17.0 ft.
Well Diameter: 2 in.
pH 00400: 5.4 units Temp. 000lo: 17.1 °C
DRY at
Depth to Water Level 82546: 5.5 ft. below measuring point Screened Interval: 3 ft. to
13 ft. Spec. Cond. 00094: µMhos
time of
sampling,check
Measuring Point is 3.2 ft. above land surface
Relative M.P. Elevation: 2.3 ft.
Odor 000m:
Volume of water pumped/bailed before sampling:
5.52
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/22/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 0.03
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids -.Total 70300 35
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 5.37
units
Ba - Barium 01007
ug/L
TOC 00680 2.1
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 11
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 6
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia omio <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese o1o55
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Agent) Name and Title - Please print or Noe

SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
• • •
•
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print
Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville Land Treatment System
Non -Discharge WQ0009267 UIC
Permit Name (if different):
NPDES Other
Facility Address:
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
,C,iyi 1,'';
'
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-4
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-4
Date sample collected: 3/22/2023
FIELD ANALYSES:
WAS
Well Depth: 16.0 ft.
Well Diameter: 2 in.
pH 00400: 4.9 units Temp. 000lo: 15.3 °C
DRY at
Depth to Water Level 82546: 5.5 ft. below measuring point Screened Interval: 5.8 ft. to
14 ft. Spec. Cond. 00094: µMhos
time of
Measuring Point is 2.68 ft. above land surface
Relative M.P. Elevation: 2.82 ft.
Odor 000ss:
sampling,check
Volume of water pumped/bailed before sampling:
5.04
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/22/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N oo615 <0.02
mg/L Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 0.03
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids -.Total 70300 177
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 4.88
units
Ba - Barium 01007
ug/L
TOC 00680 1.7
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 57
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 41
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Aqent) Name and Title - Please print or Noe
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
MIN
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville Land Treatment System
Non -Discharge WQ0009267 UIC
Permit Name (if different):
NPDES Other
Facility Address:
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
Jacksonville NC
28540 County Onslow
❑ Lagoon ❑ Remediation: Infiltration Gallery
CRY)
X Spray Field El Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-5
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-5
Date sample collected: 3/22/2023
FIELD ANALYSES:
WAS
Well Depth: 18.1 ft.
Well Diameter: 2 in.
pH 00400: 5.2 units Temp. 000lo: 17.8 °C
DRY at
Depth to Water Level 82546: 8.2 ft. below measuring point Screened Interval: 5 ft. to
15 ft. Spec. Cond. 00094: µMhos
time of
sampling,check
Measuring Point is 2.57 ft. above land surface
Relative M.P. Elevation: 5.63 ft.
Odor 00085:
Volume of water pumped/bailed before sampling:
4.75
gallons
Appearance
here:
❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/22/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 24.5
mg/L
Al - Aluminum o11o5
mg/L
pH (Lab) 00403 5.16
units
Ba - Barium 01007
ug/L
TOC oo68o 0.5
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 <5
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 <5
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCESGROUNDWATER
QUALITY MONITORING:
MIN
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print
Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name:
City of Jacksonville Land Treatment System
Non -Discharge WQ0009267 UIC
Permit Name (if different):
NPDES Other
Facility Address:
716 Firetower
Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
City)
`s`a",: 'Z'p)
X Spray Field ❑ Remediation:
Contact Person:
Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name
MW-6
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other.
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit):
MW-6
Date sample collected: 3/22/2023
FIELD ANALYSES:
WAS
Well Depth: 16.8 ft.
Well Diameter: 2 in.
pH 0040o: 5.8 units Temp. 000lo: 18.7 °C
DRY at
Depth to Water Level 82546: 4.2
ft. below measuring point Screened Interval: 3.5 ft. to
14 ft. Spec. Cond. 00094: µMhos
time of
sampling,check
Measuring Point is 2.65 ft.
above land surface
Relative M.P. Elevation: 1.55 ft.
Odor 00085:
Volume of water pumped/bailed before sampling: 6.05
gallons
Appearance
here:❑
Samples for metals were collected unfiltered:
X YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed:
3/22/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.06
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616
<1 /100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 0.24
mg/L
(Note: Use MPN method for highly turbid
samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300
287.5 mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403
5.8 units
Ba - Barium 01007
ug/L
TOC 00680
9 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940
33 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
20 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 00610
<0.2 mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia
Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Agent) Name and Title - Please print or tvr)e
GW-59 Rev.8/2013
of PDrrtftteM (or Authorized Agent)
(Date)
4/28/2023

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
Permit Name (if different):
NPDES Other
Facility Address:
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
City)
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-7
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-7
Date sample collected: 3/22/2023
FIELD ANALYSES:
WAS
Well Depth: 15.0 ft.
Well Diameter: 2 in.
pH 00400: 4.1 units Temp. 000lc 19.2 °C
DRY at
Depth to Water Level 82546: 5.7 ft. below measuring point Screened Interval: 2.5 ft. to
13 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: 2.7 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling:
4.46
gallons
Appearance
here: El
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/22/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 269.5
mg/L
Al -Aluminum oilo5
mg/L
pH (Lab) 00403 4.13
units
Ba - Barium 01007
ug/L
TOC oo68o 6.7
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 68
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 79
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Agent) Name and Title - Please print or type
(or Authorized Agent)
(Date)
4/28/2023
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
•
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville Land Treatment System
Non -Discharge WQ0009267 UIC
Permit Name (if different):
NPDES Other
Facility Address:
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
Jacksonville NC
28540 County Onslow
❑ Lagoon ❑ Remediation: Infiltration Gallery
c,ty, re�n­
_,1
X Spray Field Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-8
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-8
Date sample collected: 3/23/2023
FIELD ANALYSES:
WAS
Well Depth: 12.1 ft.
Well Diameter: 2 in.
pH 00400: 4.6 units Temp. 000lo: 17.2 °C
DRY at
Depth to Water Level 82546: 7.8 ft. below measuring point Screened Interval: 3 ft. to
9 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: 4.8 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling:
2.06
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/23/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 0.03
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 0.62
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 218.5
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 4.61
units
Ba - Barium 01007
ug/L
TOC 00680 3.2
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 6
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 99
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Aaent) Name and Title - Please print or Noe
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
Permit Name (if different):
NPDES Other
Facility Address:
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
Jacksonville NC
2.8540 County Onslow
❑ Lagoon ❑ Remediation: Infiltration Gallery
Cty, : r,i,.,
_,
X Spray Field El Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-9
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-9
Date sample collected: 3/23/2023
FIELD ANALYSES:
WAS
Well Depth: 14.0 ft.
Well Diameter: 2 in.
pH 00400: 3.86 units Temp. 000m: 18.5 °C
DRY at
Depth to Water Level 82546: 8 ft. below measuring point Screened Interval: 7 ft. to
11 ft. Spec. Cond. 00094: µMhos
time of
sampling,check
Measuring Point is 2.55 ft. above land surface
Relative M.P. Elevation: 5.45 ft.
Odor 00085:
Volume of water pumped/bailed before sampling:
2.88
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/23/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 258
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 3.86
units
Ba - Barium 01007
ug/L
TOC 00680 2.4
mg/L
Ca - Calcium oo916
mg/L
Chloride 00940 6
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 98
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen: NH3 as N: Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Aqent) Name and Title - Please print or Noe
e]►JIM4
Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
•
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville Land Treatment System
Non -Discharge WQ0009267 UIC
Permit Name (if different):
NPDES Other
Facility Address:
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
Jacksonville NC
28540 County Onslow
❑ Lagoon ❑ Remediation: Infiltration Gallery
(_'ty)
`'°
X Spray Field El Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-10
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-10
Date sample collected: 3/23/2023
FIELD ANALYSES:
WAS
Well Depth: 30.1 ft.
Well Diameter: 2 in.
pH 00400: 6.2 units Temp. 000lo 20.2 °C
DRY at
Depth to Water Level 82546: 8.9 ft. below measuring point Screened Interval: 17 ft. to
27 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 2.9 ft. above land surface
Relative M.P. Elevation: 6 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling:
10.18
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/23/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 1.24
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 618.5
mg/L
Al -Aluminum oilo5
mg/L
pH (Lab) 00403 6.23
units
Ba - Barium 01007
ug/L
TOC 00680 2.3
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 17
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 152
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Acent) Name and Title - Please print or tvpe
GW-59 Rev.8/2013
Aoent)
(Date)
4/28/2023

SUBMIT FORM ON YELLOW PAPER ONLY
•
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, INC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville Land Treatment System
Non -Discharge WQ0009267 UIC
Permit Name (if different):
NPDES Other
Facility Address:
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
city,
X Spray Field ❑Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-11
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-11
Date sample collected: 3/20/2023
FIELD ANALYSES:
WAS
Well Depth: 22.2 ft.
Well Diameter: 2 in.
pH 00400: 4.7 units Temp. 000ic 12.1 °C
DRY at
Depth to Water Level 82546: 12 ft. below measuring point
Screened Interval: 5 ft. to
20 ft. Spec. Cond. 00094: µMhos
time of
sampling,check
Measuring Point is 2.25 ft. above land surface
Relative M.P. Elevation: 9.25 ft.
Odor 00085:
Volume of water pumped/bailed before sampling:
5.14
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/20/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 0.47
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 30
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 4.69
units
Ba - Barium 01007
ug/L
TOC omm 0.6
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 6
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 <5
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Aqent) Name and Title - Please print or Noe
Aqent)
(Date)
4/28/2023
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
• • •
•
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville Land Treatment System
Non -Discharge WQ0009267 UIC
Permit Name (if different):
NPDES Other
Facility Address:
716 Firetower
Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
"Ay' "`""`
""
X Spray Field Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-12
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-12
Date sample collected: 3/22/2023
FIELD ANALYSES:
WAS
Well Depth: 18.3 ft.
Well Diameter: 2 in.
pH 00400: 5.5 units Temp. 000lo: 20.4 °C
DRY at
Depth to Water Level 82546: 7 ft. below measuring point Screened Interval: 5 ft. to
15 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 3.04 ft. above land surface
Relative M.P. Elevation: 3.96 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling:
5.42
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/22/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.05
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 140
mg/L
Al - Aluminum oil o5
mg/L
pH (Lab) 00403 5.47
units
Ba - Barium 01007
ug/L
TOC oo68o 25.9
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 6
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 8
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Aqent) Name and Title - Please print or Noe

SUBMIT FORM ON YELLOW PAPER ONLY
• .
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
•
•
1617 MAIL SERVICE CENTER, RALEIGH, INC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print
Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address:
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
`C"Y' state)
zip
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-13
No. of wells to be sampled: 17
❑ Water Source Heat Pump ElOther:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-13
Date sample collected: 3/23/2023
FIELD ANALYSES:
WAS
Well Depth: 23.2 ft.
Well Diameter: 2 in.
pH 00400: 5 units Temp. 000lc 17.8 °C
DRY at
Depth to Water Level 82546: 15 ft. below measuring point
Screened Interval: 10.5 ft. to
23.2 ft. Spec. Cond. 00094: µMhos
time of
sampling,check
Measuring Point is 2.75 ft. above land surface
Relative M.P. Elevation: 11.75 ft.
Odor 00085:
Volume of water pumped/bailed before sampling:
4.18
gallons
Appearance
here:
❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/23/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 0.04
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 76
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 5.01
units
Ba - Barium 01007
ug/L
TOC 00680 1.7
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 19
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 <5
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.8/2013
Agent)
(Date)
4/28/2023

SUBMIT FORM ON YELLOW PAPER ONLY
• •
.
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville Land Treatment System
Non -Discharge WQ0009267 UIC
Permit Name (if different):
NPDES Other
Facility Address:
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
ctv' '`ale'
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-14
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-14
Date sample collected: 3/23/2023
FIELD ANALYSES:
WAS
Well Depth: 17.9 ft.
Well Diameter: 2 in.
pH 00400: 6.4 units Temp. 000lo: 17.4 °C
DRY at
Depth to Water Level 82546: 11 ft. below measuring point
Screened Interval: 5 ft. to
15 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 11.8 ft. above land surface
Relative M.P. Elevation: -0.8 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling:
3.31
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/23/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 62.5
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 6.36
units
Ba - Barium 01007
ug/L
TOC 00680 10.5
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 11
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 <5
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 00610 0.8
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address:
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
Jacksonville NC
28540 County Onslow
❑ Lagoon ❑ Remediation: Infiltration Gallery
CAY,
ZIr
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MWA5
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-15
Date sample collected: 3/20/2023
FIELD ANALYSES:
WAS
Well Depth: 15 ft.
Well Diameter: 2 in.
pH 00400: 4.9 units Temp. 000lo: 11.5 °C
DRY at
Depth to Water Level 82546: 3.7 ft. below measuring point Screened Interval: 5 ft. to
15 ft. Spec. Cond. 00094: µMhos
time of
sampling,check
Measuring Point is 2.9 ft. above land surface
Relative M.P. Elevation: 0.8 ft.
Odor 00085:
Volume of water pumped/bailed before sampling:
5.42
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/20/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 1.63
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids -.Total 70300 105.5
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 4.87
units
Ba - Barium 01007
ug/L
TOC 00680 5.7
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 55
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 5
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Agent) Name and Title - Please print or tvoe
Authorized Agent)
(Date)
4/28/2023
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address:
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
-''°' "'
"'°
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-16
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-16
Date sample collected: 3/22/2023
FIELD ANALYSES:
WAS
Well Depth: 25 ft.
Well Diameter: 2 in.
pH 00400: 5 units Temp. 000lo: 16.7 eC
DRY at
Depth to Water Level 82546: 9.8 ft. below measuring point Screened Interval: 15 ft. to
20 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 2.4 ft. above land surface
Relative M.P. Elevation: 7.4 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling:
7.30
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/22/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 0.23
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 90
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 4.98
units
Ba - Barium 01007
ug/L
TOC om8o 2.3
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 36
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 8
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese o1o55
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs'. mg/L Effluent Total VOCs: mg/L VOC Removal%
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
Wally Hansen - Public Services Director
Permittee (or Authorized Aoent) Name and Title - Please print or type
Authorized Aoent)
(Date)
4/28/2023
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
• •
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address:
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
'-'tv' 'A°"'
"""
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-17
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-17
Date sample collected: 3/22/2023
FIELD ANALYSES:
WAS
Well Depth: 25 ft.
Well Diameter: 2 in.
pH 00400: 5.5 units Temp. 000lo 16.3 °C
DRY at
Depth to Water Level 82546: 6.9 ft. below measuring point Screened Interval: 15 ft. to
20 ft. Spec. Cond. 00094: µMhos
time of
sampling,check
Measuring Point is 1.9 ft. above land surface
Relative M.P. Elevation: 5 ft.
Odor 00085.
Volume of water pumped/bailed before sampling:
8.69
gallons
Appearance
here:
❑
Samples for metals were collected unfiltered: X
YES
El NO and field acidified: X YES El NO
LABORATORY INFORMATION
Date sample analyzed: 3/22/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 0.04
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 91.5
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 5.53
units
Ba - Barium 01007
ug/L
TOC 00680 3.1
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 35
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 12
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev.8/2013
Authorized Aqent)
(Date)
4/28/2023

-."Oqql
Environmental Chemists,
Inc.
envirochem6602
Windmill Way,
Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424
Fax
s
©
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington
Highway, Jacksonville, NC 28540 - 910.347.5843
Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
info(a,environmentalchemists.com
City of Jacksonville
Date of Report: Apr 18, 2023
Post Office Box 128
Customer PO M
Jacksonville NC 28541
Customer ID: 08110015
Attention: Amy Palaschak
Report M 2023-05616
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-14024 Site: MW-1
3/20/2023
2:12 PM Water NB
Test
Method
Results Date Analyzed
Sulfate
EPA 300.0, Rev. 2.1,1993
17 mglL
03/22/2023
Total Organic Carbon (TOC)
SM 5310 8-2014
11.7 mg/L
03/21 /2023
Chloride
SM4500 CI E-2011
44 mg/L
03/22/2023
1, 1, 1, 2-Tetrachloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
1, 1,1 -Trichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D/50308
<0.5 pg/L
03/27/2023
1,1,2-Trichooroethane
SW 846 Method 8260D/50308
<0.5 pg/L
03/27/2023
1,1-Dichloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
1,1-Dichloroethene
SW 646 Method 8260D15030B
<0.5 pg/L
03/27/2023
1,1-Dichloropropene
SW 646 Method 8260DIS0308
<0.5 pg/L
0312712023
1,2,3-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
1,2,3-Trichloropropane
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
1,2,4-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
1,2,4-Trimethylbenzene
SW 846 Method 82600/50308
<0.5 pg/L
03/27/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 82600/5030B
<0.5 pg/L
03/27/2023
1,2-Dibromoethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
1,2-Dichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
1,2-Dichloroethane
SW 846 Method 826OD150308
<0,5 pg/L
03/27/2023
1,2-Dichloropropane
SW 846 Method 8260DIS030B
<0.5 pg/L
03/27/2023
1,3,5-Trimethylbenzene
SW 846 Method 6260a15030B
<0.5 pg/L
03/27/2023
1,3-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
1,3-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
1,4-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
2,2-Dichloropropane
SW 846 Method 8260D/5030B
<0,5 pg/L
03/27/2023
2-Chlorotoluene
SW 846 Method 8260D16030B
<0,5 pg/L
03/27/2023
4-Chlorotoluene
SW 846 Method 8260DIS030B
<0,5 pg/L
03/27/2023
Report #:! 2023-05616
Page 1 of 12

-71
Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infoi�,cnvironmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC 28541
Attention: Amy Palaschak
Date of Report: Apr 18, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-05616
Project ID: Monitoring Wells
Benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
Bromobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
03/27/2023
Bromochloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/27/2023
Bromodichloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/27/2023
Bromoform
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
Bromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/27/2023
Carbon tetrachloride
SW 846 Method 826OD15030B
<0.5 pg/L
03/27/2023
Chlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
Chloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
Chloroform
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
Chloromethane
SW B46 Method 8260D/5030B
<0.5 pg/L
03/27/2023
cis-1,2-Dichlorcethene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
cis-1,3-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
Dibromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
Dibromomethane
SW 846 Method 8260D/50308
<0.5 pg/L
03/27/2023
DichlorodifIuoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
Ethylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
Hexachlorobutadiene
SW 846 Method 826OD15030B
<0.5 pg/L
03/27/2023
Isopropylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
M+P Xylene
SW 846 Method 8260D15030B
<1.0 pg/L
03/27/2023
Methylene chloride
SW 846 Method 826OD15030B
<0.5 pg/L
03/27/2023
Naphthalene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
n-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
n-Propylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
ortho-Xylene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
p-Isopropyltoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
sec -Butyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
Styrene
SW 846 Method 826OD15030B
<0.5 pg/L
03/27/2023
tert-B utyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
Tetrachloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
Report #: 2023.05816
Page 2 of 12

[env7irochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910,392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/ Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
City of Jacksonville
Post Office Sox 128
Jacksonville NC 28541
Attention: Amy Palaschak
Date of Report: Apr 18, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-05616
Project ID: Monitoring Wells
Toluene
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
Trans-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
Trans-1,3-dichloropropene
SW 846 Method 826OD15030B
<0.5 pg/L
03/27/2023
Trichioroethene
SW 846 Method 826OD15030B
<0.5 pg/L
03/27/2023
Trichlorofluoromethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/27/2023
Vinyl chloride
SW 846 Method 826OD15030B
<0.5 pg/L
03/27/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev 2 0 1993
< 0.02 mg/L
03/22/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2 0 1993
0.05mg/L
03/22/2023
Nitrate Nitrogen
Subtraction Method
0.05 mg/L
03/31/2023
Report M 2023-05616 Page 3 of 12

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info a environmentalchemists.com
City of Jacksonville Date of Report: Apr 18, 2023
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report #: 2023-05616
Project ID: Monitoring Wells
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
23-14025 Site: MW-2 3/20/2023 11:48 AM Water NB
Test Method Results Date Analyzed
Sulfate
EPA 300.0, Rev. 2.1, 1993
8 mg/L
03/22/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
0.9 mg/L
03/21 /2023
Chloride
SM4500 Ct E-2011
68 mg/L
03/22/2023
1,1,1,2-Tetrachloroethane
SW 846 Method 82600/5030B
<0.5 pg/L
03/27/2023
1,1,1-Trichloroethane
SW 646 Method 826OD15030B
<0.5 pg/L
03/27/2023
1,1,2,2-Tetrach loroethane
SW 846 Method 826oD/5030B
<0.5 pg/L
03/27/2023
1,1,2-Trichloroethane
SW 846 Method 826oD/5030B
<0.5 pg/L
03/27/2023
1, 1 -Dichloroethane
SW 846 Method 826OD/5030B
<0.5 pg/L
03/27/2023
1,1-Dichloroethene
SW 846 Method 82BOD150308
<0.5 pg/L
03/27/2023
1, 1 -Dichloropropene
SW 846 Method 826oD15030B
<0.5 pg/L
03/27/2023
1,2,3-Trichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
1,2,3-Trichloropropane
SW 846 Method 826OD/5030B
<0.5 pg/L
03/27/2023
1,2,4-Trichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
03/27/2023
1,2,4-Trimethylbenzene
SW 846 Method 8260015030E
<0.5 pg/L
03/27/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260015030E
<0.5 pg/L
03/27/2023
1,2-Dibromoethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/27/2023
1,2-Dichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
1,2-Dichloroethane
SW 846 Method 826OD/5030B
<0.5 pg/L
03/27/2023
1,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
1,3,5-Trimethylbenzene
SW 845 Method 826OD150308
<0.5 pg/L
03/27/2023
1,3-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
03/27/2023
1,3-Dichloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
03/27/2023
1,4-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
2,2-Dichloropropane
SW 846 Method 826OD/5030B
<0.5 pg/L
03/27/2023
2-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
4-Chlorotoluene
SW 846 Method 82601)150308
<0.5 pg/L
03/27/2023
Report #: 2023-05616 Page 4 of 12

[en7—ioeheirrm
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255 A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab IFax
infofd environmentalchemists com
City of Jacksonville
Date of Report: Apr 18, 2023
Post Office Box 128
Customer PO M
Jacksonville NC 28541
Customer ID: 08110015
Attention: Amy Palaschak
Report M 2023-05616
Project ID: Monitoring Wells
Benzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
Bromobenzene
SW 846 Method 82GOD150308
<0.5 pg/L
03/27/2023
Bromochloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/27/2023
Bromodichloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
Bromoform
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
Bromomethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
Carbon tetrachloride
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
Chlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
03/27/2023
Chloroethane
SW 846 Method 826OD/5030B
<0.5 pg/L
03/27/2023
Chloroform
SW 846 Method 826OD/5030B
<0.5 pg/L
03/27/2023
Chloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/27/2023
cis- 1,2-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
03/27/2023
cis-1,3-Dichloropropene
SW 846 Method 826OD15030B
<0.5 pg/L
03/27/2023
Dibromochloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
Dibromomethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
Dichlorodifluoromethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/27/2023
Ethylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
Hexachlorobutadiene
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
Isopropylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
M+P Xylene
SW 846 Method 8260D/5030B
<1.0 pg/L
03/27/2023
Methylene chloride
SW 846 Method 826OD150308
<0.5 pg/L
03/27/2023
Naphthalene
SW 846 Method 826OD15030B
<0.5 pg/L
03/27/2023
n-Butylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
n-Propylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
ortho-Xylene
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
p-Isopropyltoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/27/2023
sec- Bu tyl benzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
Styrene
SW 846 Method 8260D150308
<0.5 pg/L
03/27/2023
tert-Butyl benzene
SW 846 Method 8260D/50308
<0.5 pg/L
03/27/2023
Tetrachloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
Report*. 2023-05616
Page 5 of 12

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
City of Jacksonville
Post Office Box 128
Jacksonville NC 28541
Attention: Amy Palaschak
Date of Report: Apr 18, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-05616
Project ID: Monitoring Wells
Toluene
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
Trans-1,2-Dichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
Trans-1 ,3-dichloropropene
SW 846 Method 826OD15030B
<0.5 pg/L
03/27/2023
Trichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
Trichlorofluoromethane
SW 646 Method 6260D15030B
<0.5 pg/L
03/27/2023
Vinyl chloride
SW 846 Method 8260D15030B
<0.5 pg/L
03/27/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0, 1993
0.02 mg/L
03/22/2023
Nitrate+ N itrite-N itrogen
EPA 353.2, Rev. 2.0, 1993
0.07 mg/L
03/22/2023
Nitrate Nitrogen
Subtraction Method
0.05 mg/L
03/31/2023
Report # 2023-05616 Page 6 of 12

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
inforiz environmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC 28541
Attention: Amy Palaschak
bate of Report: Apr 18, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-05616
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-14026 Site: MW-11
3/20/2023
3:03 PM Water NB
Test
Method
Results
Date Analyzed
Sulfate
EPA 300 0 Rev 21 1993
<5 mg/L
03/22/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
0.6 mg/L
03/21/2023
Chloride
SM4500 C1 E-2011
6 mg/L
03/22/2023
1,1,1,2-Tetrachloroethane
SW 846 Method 826oD/5030B
<0.5 pg/L
03/28/2023
1,1,1-Trichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/28/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D/50308
<0.5 pg/L
03/28/2023
1,1,2-Trichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
1,1-Dichloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/28/2023
1,1-Dichloroethene
SW 846 Method 8260D/50308
<0.5 pg/L
03/28/2023
1,1-Dichloropropene
SW 846 Method 8260D/503013
<0.5 pg/L
03/28/2023
1,2,3-Trichlorobenzene
SW 846 Method 82600/50308
<0.5 pg/L
03/28/2023
1,2,3-Trichloropropane
SW 846 Method 8260D/50308
<0.5 pg/L
03/28/2023
1,2,4-Trichlorobenzene
SW 846 Method 8260015030E
<0.5 pg/L
03/28/2023
1,2,4-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
03/28/2023
1,2-Dibromoethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/28/2023
1,2-Dichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/28/2023
1,2-Dichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/28/2023
1,2-Dichloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
03/28/2023
1,3,5-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
1,3-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
1,3-Dichloropropane
SW 846 Method 8260D15030B
<0.5 pg/L
03/28/2023
1,4-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
2,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
2-Chlorotoluene
SW 846 Method 826oD/5030B
<0.5 pg/L
03/28/2023
4-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
Report # 2023-05616 Page 7 of 12

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910-392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info(ulcnvironmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC 28541
Attention: Amy Palaschak
Date of Report: Apr 18, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-05616
Project ID: Monitoring Wells
Benzene
SW 846 Method 826OD150308
<0.5 pg/L
03/28/2023
Bromobenzene
SW 846 Method 826OD150308
<0.5 pg/L
03/28/2023
Bromochlorom ethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/28/2023
Bromodichloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/28/2023
Bromoform
SW 846 Method 826OD/5030B
<0.5 pg/L
03/28/2023
Bromomethane
SW 846 Method 8260DIS030B
<0.5 pg/L
03/28/2023
Carbon tetrachloride
SW 846 Method 826OD15030B
<0.5 pg/L
03/28/2023
Chlorobenzene
SW 846 Method 8260D/S030B
<0.5 pg/L
03/28/2023
Chloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/28/2023
Chloroform
SW 846 Method 82GOD15030B
<0.5 pg/L
03/28/2023
Chloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
cis-1,2-Dichloroethene
SW 846 Method 826OD160308
<0.5 pg/L
03/28/2023
cis-1,3-Dichloropropene
SW 846 Method 826OD150308
<0.5 pg/L
03/28/2023
Dibromochloromethane
SW 846 Method 826OD/5030B
<0.5 pg/L
03/28/2023
Dibromomethane
SW s46 Method 8260D/5030B
<0.5 pg/L
03/28/2023
Dichlorodifluoromethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/28/2023
Ethylbenzene
SW 846 Method 826OD150308
<0.5 pg/L
03/28/2023
Hexachlorobutadiene
SW 846 Method 8260D15030B
<0.5 pg/L
03/28/2023
Isopropylbenzene
SW 846 Method 82BOD15030B
<0.5 pg/L
03/28/2023
M+P Xylene
SW 846 Method 826OD15030B
<1.0 pg/L
03/28/2023
Methylene chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
Naphthalene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
n-Butylbenzene
SW 846 Method 826OD/5030B
<0.5 pq/L
03/28/2023
n-Propylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
ortho-Xylene
SW 846 Method 8260D15030B
<0.5 pg/L
03/28/2023
p-Isopropyltoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
sec -Butyl benzene
SW 846 Method 826OD150308
<0.5 pg/L
03/28/2023
Styrene
SW 846 Method 8260D15030B
<0.5 pg/L
03/28/2023
te rt-B utyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
Tetrachloroethene
SW 846 Method 8260015030E
<0.5 pg/L
03/28/2023
Report # 2023.05616
Page 8 of 12

F-707 —l""17 Environmental Chemists, Inc.
envirochem6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab " 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
swy 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
City of Jacksonville
Post Office Box 128
Jacksonville NC 28541
Attention: Amy Palaschak
Date of Report: Apr 18, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-05616
Project ID: Monitoring Wells
Toluene
SW 646 Method 8260D/5030B
<0.5 µg/L
03/28/2023
Trans- 1,2-Dich loroethene
SW 646 Method 6260D/5030B
<0.5 µg/L
03/28/2023
Trans- 1,3-d ichloropropene
SW 846 Method 6260D/5030B
<0.5 µg/L
03/28/2023
Trichloroethene
SW 846 Method 6260D/5030B
<0.5 µg/L
03/28/2023
Trichlorofluoromethane
SW 846 Method 8260D/5030B
<0.5 µg/L
03/28/2023
Vinyl chloride
SW 846 Method 82SOD15030B
<0.5 µg/L
03/28/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev 2 0 1993
< 0.02 mg/L
03/22/2023
Nitrate+ N itrite-N itrogen
EPA 353 2, Rev 2 0 1993
0.47 mg/L
03/22/2023
Nitrate Nitrogen
Subtraction Method
0.47 mg/L
03/31/2023
Report # 2023-05616 Page 9 of 12

ro"7. Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
® 710 $owsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infoia environmentalchemists com
City of Jacksonville Date of Report: Apr 18, 2023
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report #: 2023-05616
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-14027 Site: MW-15 3/20/2023 1:05 PM Water NB
Test Method Results Date Analyzed
Sulfate
EPA 300.0, Rev. 2.1, 1993
5 mg/L
03/22/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
5.7 mg/L
03/21/2023
Chloride
SM4500 CI E-2011
55 mg/L
03/22/2023
1,1,1,2-Tetrachloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/28/2023
1, 1, 1 -Trichloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/28/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/28/2023
1,1,2-Trichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/28/2023
1,1-Dichloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/28/2023
1,1-Dichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
03/28/2023
1,1-Dichloropropene
SW 846 Method 8260D/50308
<0.5 pg/L
03/28/2023
1,2,3-Trichlorobenzene
SW 846 Method 826OD15030B
<0.5 pq/L
03/28/2023
1,2,3-Trichloropropane
sw 846 Method 826OD15030B
<0.5 pg/L
03/28/2023
1,2,4-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
1,2,4-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
1,2-Dibromo-3-Chloropropane
SW B46 Method 8260D/5030B
<0.5 pq/L
03/28/2023
1,2-Dibromoethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/28/2023
1,2-Dichlorobenzene
SW 846 Method 8260D150308
<0.5 pg/L
03/28/2023
1,2-Dichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/28/2023
1,2-Dichloropropane
SW 846 Method 8260D/50308
<0.5 pg/L
03/28/2023
1,3,5-Trimethyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
1,3-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
1,3-Dichloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
03/28/2023
1,4-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
2,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
2-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
4-Chlorotoluene
SW 846 Method 6260D/5030B
<0.5 pg/L
03/28/2023
Report #:: 2023-05616 Page 10 of 12

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab. Fax
info az environmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC 28541
Attention: Amy Palaschak
Date of Report: Apr 18, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-05616
Project ID: Monitoring Wells
Benzene
SW 846 Method 826OD150308
<0.5 pg/L
03/28/2023
Bromobenzene
SW 846 Method 8260DIS030B
<0.5 pg/L
03/28/2023
Bromochloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/28/2023
Bromodichloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
Bromoform
SW 846 Method 8260D15030B
<0.5 pg/L
03/28/2023
Bromomethane
SW 846 Method 826OD150308
<0.5 pg/L
03/28/2023
Carbon tetrachloride
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
Chlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/28/2023
Chloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
Chloroform
SW 846 Method 8260D/5030B
<0,5 pg/L
03/28/2023
Chloromethane
SW 846 Method 826OD15030B
<0,5 pg/L
03/28/2023
cis-1,2-Dichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
03/28/2023
cis- 1,3-Dichloropropene
SW 846 Method 826OD/5030B
<0.5 pg/L
03/28/2023
Dibromochloromethane
SW 846 Method 826OD/5030B
<0.5 pg/L
03/28/2023
Dibromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
Dichlorodifluoromethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/28/2023
Ethylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/28/2023
Hexachlorobutadiene
SW 846 Method 826OD150366
<0.5 pg/L
03/28/2023
Isopropylbenzene
SW 846 Method 8260015030E
<0.5 pg/L
03/28/2023
M+P Xylene
SW 846 Method 8260D/5030B
<1.0 pg/L
03/28/2023
Methylene chloride
SW 846 Method 8260015030E
<0.5 pg/L
03/28/2023
Naphthalene
SW 846 Method 826OD/5030B
<0.5 pg/L
03/28/2023
n-Butylbenzene
SW 846 Method 82BOD15030B
<0.5 pg/L
03/28/2023
n-Propylbenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
03/28/2023
ortho-Xylene
SW 846 Method 82BOD15030B
<0.5 pg/L
03/28/2023
p-Isopropyltoluene
SW 846 Method 8260D15030B
<0.5 pg/L
03/28/2023
sec -Butyl benzene
SW 846 Method 826OD15030B
<0.5 pg/L
03/28/2023
Styrene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
tert-Butyl benzene
SW 846 Method 82600/5030B
<0.5 pg/L
03/28/2023
Tetrachloroethene
SW 846 Method 826OD16030B
<0.5 pg/L
03/28/2023
Report # 2023-05616
Page 11 of 12

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info(a?envi ronmentalchemists.com
City of Jacksonville
Date of Report: Apr 18, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention: Amy Palaschak
Report #: 2023-05616
Project ID: Monitoring Wells
Toluene
SW 846 Method 8260D/50308
<0.5 pg/L
03/28/2023
Trans-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
Trans-1,3-dichloropropene
SW 846 Method 82SOD/5030B
<0,5 pg/L
03/28/2023
Trichloroethene
SW 846 Method 826OD/50308
<0.5 pg/L
03/28/2023
Trichlorofluoromethane
SW 846 Method 82600/5030B
<0.5 pg/L
03/28/2023
Vinyl chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
03/28/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2, Rev 20, 1993 < 0.02 mg/L 03/22/2023
Nitrate+ N itrite- Nitrogen EPA 353.2, Rev. 2 0, 1993 1.63 mg/L 03/22/2023
Nitrate Nitrogen Subtraction Method 1.63 mg/L 03/31/2023
Comment:
Reviewed by:
Report #. 2023-05616 Page 12 of 12

Environmental Chemist, Inc., Wilmington, NC tab #94
6602 Windr-niil Wa
Wilmington, NC 2840
{ Sample Receipt Checklist 910.392.022:
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Original temperature upo receipt _ T �` Seals Were present, were they intact/unbroken?
Hove temp ,C Corrected temperature.
temperature taken: O Temperature Blank upon receipt
iR Gun ID: Thomas Traceable S/N I'll 210886869 l+gainst Bottles ---.`C
YES i] A'0 . 3. if temperature of Goole exceeded 6{C, a;ason cPrr'r ~
C: 0.0
YES NO 4. Were proper custodyrote of-ct Mgr./Qq notified?
YES ❑ NO S. lNere sample ID's listed on therCOC? linquished/received) followed?
YES O NO 6. Were samples 1D's listed on sample containers?
YES O NO 7- Were collection date and time listeon the COC?
d
YES O NO 8. Were tests to be performed fisted on th
YES ❑ NO9. Did samples arrive in e COC?
YES ❑ NO proper
per containers for each test?
10. Did samples arrive in good conditi11 on for each test?
I� YES ❑ �10 11. Was adequbf
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YES ❑ NO 12. Were samples received within proarl rho
YES O NO 13. Were acid preserved samples receivedng < ime for requested
� YES q ed tests?
NO 1A Were cyanide samples received at a PH >12? 2
l] YES O NO 15. Were sulfide samples received at a pH >9?
YES ❑ NO 16. Were NH3 TKN Phe CJ YES p NG / / nol received at a chlorine r
17. Were Sulfide esidua10 f <0.5 m/! ?
Q YES p NO -1 apn'rde received at a chlorine residual
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bM
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
City of Jacksonville Date of Report: Apr 21, 2023
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention. Report #: 2023-05841
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-14709 Site: MW-3 3/22/2023 10:58 AM Water NB
Test Method Results Date Analyzed
Sulfate
EPA 300.0 Rev 2 1, 1993
6 mg/L
03/28/2023
Total Organic Carbon (TOC)
SM 6310 B-2014
2.1 mg/L
03/30/2023
Chloride
SM4500 CI E-2011
11 mg/L
03/24/2023
1,1,1,2-Tetrachloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
04/04/2023
1,1,1-Trichloroethane
SW 846 Method 8260015030B
<0.5 pg/L
04/04/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
04/04/2023
1,1,2-Trichloroethane
SW 846 Method 8260015030B
<0.5 pg/L
04/04/2023
1, 1 -Dichloroethane
SW 846 Method 8260015030E
<0.5 pg/L
04/04/2023
1, 1 -D ichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
04/04/2023
1,1-Dichloropropene
SW 846 Method 826OD15030B
<0.5 pg/L
04/04/2023
1,2,3-Trichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
04/04/2023
1,2,3-Trichloropropane
SW 846 Method 8260D15030B
<0.5 pg/L
04/04/2023
1,2,4-Trichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
04/04/2023
1,2,4-Trimethylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
04/04/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D15030B
<0.5 pg/L
04/04/2023
1,2-Dibromoethane
SW 846 Method 8260D/5030B
<0.5 pg/L
04/04/2023
1,2-Dichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
04/04/2023
1,2-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
04/04/2023
1,2-Dichloropropane
SW 846 Method 826OD150308
<0.5 pg/L
04/04/2023
1,3,5-Trimethylbenzene
SW 846 Method 826oD/5030B
<0.5 pg/L
04/04/2023
1,3-Dichlorobenzene
SW 846 Method 826oD/5030B
<0.5 pg/L
04/04/2023
1,3-Dichloropropane
SW 846 Method 8260D16030B
<0.5 pg/L
04/04/2023
1,4-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
04/04/2023
2,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
04/04/2023
2-Chlorotoluene
SW 846 Method 826015030B
<0.5 pg/L
04/04/2023
4-Chlorotoluene
SW 846 Method 826oD/50308
<0.5 pg/L
04/04/2023
Report #:: 2023.05841 Page 1 of 39

nvirochem
=u
ANALYTICAL & CONSULTING CHEMISTS
F"17-71
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab; Fax
info,u environmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Apr 21, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-05841
Project ID: Monitoring Wells
Benzene
SW 846 Method 8260D15030B
<0.5 pg/L
04/04/2023
Bromobenzene
SW 846 Method 8260D/5030B
<Q.5 pg/L
04/04/2023
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
04/04/2023
Bromodichloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
04/04/2023
Bromoform
SW 846 Method 826OD15030B
<0.5 pg/L
04/04/2023
Bromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
04/04/2023
Carbon tetrachloride
SW 846 Method 8260D15030B
<0.5 pg/L
04/04/2023
Chlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
04/04/2023
Chloroethane
SW 846 Method 8260D150308
<0.5 pg/L
04/04/2023
Chloroform
SW 846 Method 826015030B
<0.5 pg/L
04/04/2023
Chloromethane
SW 846 Method 82600/5030B
0.73 pg/L
04/04/2023
cis-1,2-Dichloroethene
SW 845 Method 8260D/5030B
<0.5 pg/L
04/04/2023
cis- 1,3-Dichloropropene
SW 846 Method 82601)/50308
<0.5 pg/L
04/04/2023
Dibromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
04/04/2023
Dibromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
04/04/2023
DichlorodifIuoromethane
SW 846 Method 82600/50306
<0.5 pg/L
04/04/2023
Ethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
04/04/2023
Hexachlorobutadiene
SW 846 Method 8260015030E
<0.5 pg/L
04/04/2023
Isopropylbenzene
SW 846 Method 826013/50306
<0.5 pg/L
04/04/2023
M+P Xylene
SW 846 Method 826OD15030B
<1.0 pg/L
04/04/2023
Methylene chloride
SW 846 Method 8260D/50308
<0.5 pg/L
04/04/2023
Naphthalene
SW 846 Method 82BOD15030B
<0.5 pg/L
04/04/2023
n-Butylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
04/04/2023
n-Propylbenzene
SW 846 Method 8260D/5030B
<0-5 pg/L
04/04/2023
ortho-Xylene
SW 846 Method 8260D/5030B
<0.5 pg/L
04/04/2023
p-Isopropyltoluene
SW 846 Method 826OD150308
21.5 pg/L
04/04/2023
sec -Butyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
04/04/2023
Styrene
SW 846 Method 8260D15030B
<0.5 pg/L
04/04/2023
tert-Butylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
04/04/2023
Tetrachloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
04/04/2023
Report #: 2023-05841
Page 2 of 39

[en7viroche]m
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
info a environmentalchemists.com
City of Jacksonville
Date of Report: Apr 21, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-05841
Project ID: Monitoring Wells
Toluene
SW 846 Method 8260D/5030B
13.7 pg/L
04/04/2023
Trans-1,2-Dichloroethene
SW 846 Method 8260D/50308
<0,5 pg/L
04/04/2023
Trans-1,3-dichloropropene
SW 846 Method 8260DI5030B
<0.5 pg/L
04/04/2023
Trichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
04/04/2023
Trichlorofluoromethane
SW 848 Method 8260Dl5030B
<0.5 pg/L
04/04/2023
Vinyl chloride
SW 846 Method 8260D/50308
<0.5 pg/L
04/04/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353 2, Rev 2 0, 1993 < 0.02 mg/L 03/23/2023
Nitrate+Nitrite-Nitrogen EPA 353 2, Rev. 2 0 1993 0.03 mg/L 03/28/2023
Nitrate Nitrogen Subtraction Method 0.03 mg/L 04/04/2023
Report # 2023-05841 page 3 of 39

F"0107
Environmental Chemists,
Inc.
' 1
6602 Windmill Way,
Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
7M
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843
Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
info(aenvironmentalchemismcom
City of Jacksonville
Date of Report: Apr 21, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report #: 2023-05841
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-14710 Site: MW-4
3/22/2023
11:58 AM Water NB
Test
Method
Results Date Analyzed
Sulfate
EPA 300 0, Rev. 2.1, 1993
41 mg/L
03/28/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
1.7 mg/L
03/30/2023
Chloride
SM4500 ci E-2011
57 mg/L
03/24/2023
1. 1, 1,2-Tetrachloroethane
SW 846 Method 826OD15030B
<0, 5 pg/L
03/29/2023
1,1,1-Trichloroethane
SW 846 Method 8260DI5030B
<0, 5 pg/L
03/29/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 8260DI5030B
<0.5 pg/L
03/29/2023
1,1,2-Trichloroethane
SW 846 Method 82SOD150308
<0.5 pg/L
03/29/2023
1,1-Dichloroethane
SW 846 Method 6260015o3oB
<0.5pg/L
03/29/2023
1,1-Dichloroethene
SW 846 Method 8260DI5030B
<0.5pg/L
03/29/2023
1,1-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2,3-Trichlorobenzene
SW 846 Method 8260DI5030B
<0.5 pg/L
03/29/2023
1,2,3-Trichloropropane
SW 848 Method 8260DI5030B
<0.5 pg/L
03/29/2023
1,2,4-Trichlorobenzene
SW 846 Method 8260DI5030B
<0,5 pg/L
03/29/2023
1,2,4-Trimethylbenzene
SW 846 Method 826OD15030B
<0.5pg/L
03/29/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 826OD150308
<0.5 pg/L
03/29/2023
1,2-Dibromoethane
SW 846 Method 8260D150308
<0.5 pg/L
03/29/2023
1,2-Dichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,2-Dichloroethane
SW 646 Method 826OD15030B
<0.5 pg/L
03/29/2023
1,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1, 3,5-Trimethyl benzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,3-Dichlorobenzene
SW 846 Method 826oD150308
<0.5 pg/L
03/29/2023
1,3-Dichloropropane
SW 846 Method 826OD150308
<0.5 pg/L
03/29/2023
1,4-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
2,2-Dichloropropane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
2-Chlorotoluene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
4-Chlorotoluene
SW 846 Method 8260D150308
<0.5 pg/L
03/29/2023
Report #:, 2023.05941
Page 4 of 39

nvirochem
ANALYTICAL 8 CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910,347.5843 Lab/Fax
info,r environmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Apr 21, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-05841
Project ID: Monitoring Wells
Benzene
SW 646 Method 826oD/503oB
<0.5 pg/L
03/29/2023
Bromobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
Bromochloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Bromodichloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Bromoform
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
Bromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Carbon tetrachloride
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Chlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Chloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Chloroform
SW 846 Method 828OD15030B
<0.5 pg/L
03/29/2023
Chloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
cis-1,2-Dichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
cis-1,3-Dichloropropene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Dibromochloromethane
SW 846 Method 8260015030B
<0.5 pg/L
03/29/2023
Dibromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Dichlorodifluoromethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Ethylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Hexachlorobutadiene
SW 846 Method 8260015030E
<0.5 pg/L
03/29/2023
Isopropylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
M+P Xylene
SW 846 Method 8260D15030B
<1.0 pg/L
03/29/2023
Methylene chloride
SW 846 Method 8260D/5G308
<0.5 pg/L
03/29/2023
Naphthalene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
n-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
n-Propylbenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
03/29/2023
ortho-Xylene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
p-Isopropyltoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
sec-Butylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Styrene
SW 846 Method 82BOD15030B
<0.5 pg/L
03/29/2023
tert-Butylbenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
03/29/2023
Tetrachloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Report # 2023-05841
Page 5 of 39

ro""57 Environmental Chemists, Inc.
nvirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255 A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info,z environmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Apr 21, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-05841
Project ID: Monitoring Wells
Toluene
SW 846 Method 828OD15030B
<0.5 pg/L
03/29/2023
Trans-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Trans-1,3-dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Trichioroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Trichlorofluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Vinyl chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 353 2, Rev 2 0, 1993
< 0.02 mg/L
03/23/2023
Nitrate+ N itrite-N itrogen
EPA 353.2. Rev. 2.0, 1993
0.03 mg/L
03/28/2023
Nitrate Nitrogen
Subtraction Method
0.03 mg/L
04/04/2023
Report # 2023-05841 Page 6 of 39

F"007
Cnviroehiem]
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info,h,environmentalchemists.com
City of Jacksonville
Date of Report: Apr 21, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report #: 2023-05841
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-14711 Site: MW-5
3/22/2023
12:35 PM Water NB
Test
Method
Results
Date Analyzed
Sulfate
EPA 300.0, Rev 2.1, 1993
<5 mg/L
03/28/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
0.5 mg/L
03/30/2023
Chloride
SM4500 CI E-2011
< 5 mg/L
03/24/2023
1,1,1, 2-Tetrachloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1, 1, 1 -Trichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,1,2-Trichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
1,1-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,1-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,1-Dichloropropene
SW 846 Method 8260D/5030B
<0, 5 pg/L
03/29/2023
1,2,3-Trichlorobenzene
SW 846 Method 8280D/5030B
<0,5 pg/L
03/29/2023
1,2,3-Trichooropropane
SW 846 Method 8260D/5030B
<0,5 pg/L
03/29/2023
1,2,4-Trichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,2,4-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,2-Dibromoethane
SW 846 Method 826OD150308
<0.5 pg/L
03/29/2023
1,2-Dichlorobenzene
SW 646 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2-Dichloropropane
SW 846 Method 826ODY50308
<0.5 pg/L
03/29/2023
1,3,5-Trimethyl benzene
SW 846 Method 8260DI503oB
<0.5 pg/L
03/29/2023
1, 3-Dichlorobenzene
SW 846 Method 826015wo!3
<0.5 pg/L
03/29/2023
1, 3-Dichloropropane
SW 846 Method 626015030B
<0.5 pg/L
03/29/2023
1,4-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
2,2-Dichloropropane
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
2-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
4-Chlorotoluene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Report M. 2023-05841
Page 7 of 39

bbil
ANALYTICAL & CONSULTING CHEMISTS
F"10-7 -:,Oqql
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Apr 21, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-05841
Project ID: Monitoring Wells
Benzene
SW 846 Method 8260D150308
<0.5 pg/L
03/29/2023
Bromobenzene
SW 846 Method 8260D150308
<0.5 pg/L
03/29/2023
Bromochloromethane
SW 846 Method 826OD150308
<0 5 pg/L
03/29/2023
Bromodichloromethane
SW 846 Method 826OD150308
<0 5 pg/L
03/29/2023
Bromoform
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Bromomethane
SW 846 Method 8260015030E
<0.5 pg/L
03/29/2023
Carbon tetrachloride
SW 846 Method 826OD1503GB
<0.5 pg/L
03/29/2023
Chlorobenzene
SW 846 Method 8260D150306
<0.5 pg/L
03/29/2023
Chloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Chloroform
SW 846 Method 82600150308
<0.5 pg/L
03/29/2023
Chloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
cis- 1,2-Dichloroethene
5W 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
cis-1,3-Dichloropropene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Dibromochloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Dibromomethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Dichlorodifluoromethane
SW 846 Method 826OD150308
<0.5 pg/L
03/29/2023
Ethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Hexachlorobutadiene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Isopropylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
M+P Xylene
SW 846 Method 826OD15030B
<1.0 pg/L
03/29/2023
Methylene chloride
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Naphthalene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
n-Butylbenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
03/29/2023
n-Propylbenzene
SW 846 Method 8260015030B
<0.5 pg/L
03/29/2023
ortho-Xylene
SW 846 Method 8260015030E
<0.5 pg/L
03/29/2023
p-Isopropyltoluene
SW 848 Method 82BOD/50300
0.62 pg/L
03/29/2023
sec -Butyl benzene
SW 846 Method 82BOD/50300
<0.5 µg/L
03/29/2023
Styrene
SW 848 Method 8260DIS0308
<0.5 pg/L
03/29/2023
tert-Butylbenzene
SW 846 Method 826ODJ5030B
<0.5 pg/L
03/29/2023
Tetrachloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Report #: ' 2023-05841
Page 8 of 39

F"Iw'" --
Environmental Chemists,
Inc.
envirochem
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
'M
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
infoiuenvironmentalchemists.com
City of Jacksonville
Date of Report: Apr 21, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report #: 2023-05841
Project ID: Monitoring Wells
Toluene
SW 846 Method 8280D/503013 <0.5 pg/L
03/29/2023
Trans-1,2-Dichloroethene
SW 846 Method 8260D/503013 <0.5 pg/L
03/29/2023
Trans-1 ,3-dichloropropene
SW 846 Method 82600/5030B <0.5 pg/L
03/29/2023
Trichloroethene
SW 848 Method 8280Dl5030B <0.5 pg/L
03/29/2023
Trichlorofluoromethane
SW 846 Method 8260D/5030B <0.5 pg/L
03/29/2023
Vinyl chloride
SW 846 Method 8260D/5030B <0.5 pg/L
03/29/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2. Rev. 2.0, 1993 < 0.02 mg/L 03/23/2023
N itrate+N itrite- Nitrogen EPA 353.2, Rev. 2.0,1993 < 0.02 mg/L 03/28/2023
Nitrate Nitrogen Subtraction Method <0.02 mg/L 04/04/2023
Report # 2023-05841 Page 9 of 39

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
y 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
[e-mail]
City of Jacksonville
Date of Report: Apr 21, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report #: 2023-05841
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-14712 Site: MW-6
3/22/2023
1:20 PM Water NB
Test
Method
Results
Date Analyzed
Sulfate
EPA 300.0, Rev 2 1, 1993
20 mg/L
03/28/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
9.0 mg/L
03/30/2023
Chloride
SM4500 CI E-2011
33 mg/L
03/24/2023
1, 1, 1,2-Tetrachloroethane
SW 846 Method 8260D150308
<0.5 pg/L
03/29/2023
1, 1, 1 -Trichloroethane
SW 846 Method 8260D/5030B
<0, 5 pg/L
03/29/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
1,1,2-Trichloroethane
SW 846 Method 8260DIS030B
<0.5 pg/L
03/29/2023
1,1-Dichloroethane
SW 846 Method 82600/5030B
<0.5 pg/L
03/29/2023
1,1-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
1,1-Dichloropropene
SW 846 Method 8260D15030B
<0,5 pg/L
03/29/2023
1,2,3-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2,3-Trichloropropane
SW 846 Method 8280D15030B
<0.5 pg/L
03/29/2023
1,2,4-Trichlorobenzene
SW 846 Method 6280D/5030B
<0.5 pg/L
03/29/2023
1,2,4-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 8280D15030B
<0.5 pg/L
03/29/2023
1,2-Dibromoethane
SW 646 Method 8280D/50308
<0.5 pg/L
03/29/2023
1,2-Dichlorobenzene
SW 846 Method 6260D/50308
<0.5 pg/L
03/29/2023
1,2-Dichloroethane
SW 846 Method 8260D150308
<0.5 pg/L
03/29/2023
1,2-Dichloropropane
SW 846 Method 8260DIS0308
<0.5 pg/L
03/29/2023
1,3,5-Trimethylbenzene
SW 846 Method 8260DIS0308
<0.5 pg/L
03/29/2023
1,3-Dichlorobenzene
SW 846 Method 826OD150308
<0.5 pg/L
03/29/2023
1, 3-Dichloropropane
SW 846 Method 8260DIS030B
<0.5 pg/L
03/29/2023
1,4-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
2,2-Dichloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
2-Chlorotoluene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
4-Chlorotoluene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Report #: 2023-05841
Page 10 of 39

F"00--. I Environmental Chemists, Inc.
envirochem6602 Windmill Way, Wilmington, NC 28405 • 910 392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
�M 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infora enviroronentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Apr 21, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-05841
Project ID: Monitoring Wells
Benzene
SW 846 Method 826OD/5030B
<0.5 pg/L
03/29/2023
Bromobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Bromodichloromethane
SW 846 Method 826OD/5030B
<0.5 pg/L
03/29/2023
Bromoform
SW 846 Method 826OD/5030B
<0.5 pg/L
03/29/2023
Bromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Carbon tetrachloride
SW 846 Method 826OD/5030B
<0.5 pg/L
03/29/2023
Chlorobenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
03/29/2023
Chloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Chloroform
SW 846 Method 826OD/5030B
<0.5 pg/L
03/29/2023
Chloromethane
SW 846 Method 82BOD15030B
<0.5 pg/L
03/29/2023
cis-1,2-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
cis-1,3-Dichloropropene
SW 846 Method 8280D/5030B
<0.5 pg/L
03/29/2023
Dibromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Dibromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Dichlorodifluoromethane
SW 846 Method 826oW50306
<0.5 pg/L
03/29/2023
Ethylbenzene
SW 846 Method 825oW5030B
<0.5 pg/L
03/29/2023
Hexachlorobutadiene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Isopropylbenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
03/29/2023
M+P Xylene
SW 846 Method 82BOD15030B
<1.0 pg/L
03/29/2023
Methylene chloride
SW 846 Method 8260DIS030B
<0.5 pg/L
03/29/2023
Naphthalene
SW 846 Method 8260015030E
<0.5 pg/L
03/29/2023
n-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
n-Propylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
ortho-Xylene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
p-Isopropyltoluene
SW 846 Method 82BOD15030B
<0.5 pg/L
03/29/2023
sec -Butyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Styrene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
tert-Butyl benzene
SW 848 Method 826OD15030B
<0.5 pg/L
03/29/2023
Tetrachloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Report 11:: 2023-05841
Page 11 of 39

-.,Oqql
Environmental Chemists, Inc.
envirochem J 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
City of Jacksonville
Date of Report: Apr 21, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-05841
Project ID: Monitoring Wells
Toluene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Trans- 1,2 -Dich loroethen e
SW 846 Method 826ODl5030B
<0.5 pg/L
03/29/2023
Trans- l,3-dichloropropene
SW 846 Method 8260Dl5030B
<0.5 pg/L
03/29/2023
Trichloroethene
SW 846 Method 8260Dl5030B
<0.5 pg/L
03/29/2023
Trichlorofluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Vinyl chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA353.2, Rev. 2.0,1993
0.06mg/L
03/23/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0, 1993
0.07 mg/L
03/28/2023
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
04/04/2023
Report #:: 2023-05841 Page 12 of 39

F7 7 � —1 ""q 4 1
Environmental Chemists,
Inc,
envirochem6602
Windmill Way,
Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
info,ti!environmentalchemists.com
City of Jacksonville
Date of Report: Apr 21, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report #: 2023-05841
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-14714 Site: MW-7
3/22/2023
2:22 PM Water NB
Test
Method
Results Date Analyzed
Sulfate
EPA 300 0 Rev. 2.1, 1993
79 mg/L
03/28/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
6.7 mg/L
03/30/2023
Chloride
SM4500 CI E-2011
68 mg/L
03/24/2023
1. 1, 1,2-Tetrachloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
1, 1, 1 -Trich loroethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,1,2-Trichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,1-Dichloroethane
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
1,1-Dichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,1-Diehloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2,3-Trichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,2,3-Trichloropropane
SW 846 Method 82BOD150308
<0.5 pg/L
03/29/2023
1,2,4-Trichlorobenzene
SW 846 Method 82600/50308
<0.5 pg/L
03/29/2023
1,2,4-Trimethylbenzene
SW 846 Method 82SOD15030B
<0.5 pg/L
03/29/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
1,2-Dibromoethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
1,2-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2-Dichloropropane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,3,5-Trimethylbenzene
SW 846 Method 826OD150308
<0.5 pg/L
03/29/2023
1,3-Dichlorobenzene
SW 846 Method 826OD150308
<0.5 pg/L
03/29/2023
1,3-Dichloropropane
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
1,4-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
2,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
2-Chlorotoluene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
4-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Report #:. 2023-05841
Page 13 of 39

—,-Oqql
Environmental Chemists, Inc.
envirochem A 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473,5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infoa environmentalchemisls.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Apr 21, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-05841
Project ID: Monitoring Wells
Benzene
SW 846 Method 82600/50308
<0.5 pg/L
03/29/2023
Bromobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Bromochloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Bromodichloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Bromoform
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Bromomethane
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
Carbon tetrachloride
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Chlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Chloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Chloroform
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Chloromethane
SW 846 Method 8260D5030B
<0.5 pg/L
03/29/2023
cis- 1,2-Dichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
cis-1,3-Dichloropropene
SW 846 Method 8260U5030B
<0.5 pg/L
03/29/2023
Dibromochloromethane
SW 846 Method 8260Dr5030B
<0.5 pg/L
03/29/2023
Dibromomethane
SW 846 Method 82601)r50306
<0.5 pg/L
03/29/2023
Dichlorodifluoromethane
SW 846 Method 8260Dr5030B
<0.5 pg/L
03/29/2023
Ethylbenzene
SW 846 Method 8260D,5030B
<0.5 pg/L
03/29/2023
Hexachlorobutadiene
SW 846 Method 8260D,5030B
<0.5 pg/L
03/29/2023
1sopropylbenzene
SW 846 Method 8260D,5030B
<0.5 pg/L
03/29/2023
M+P Xylene
SW 846 Method B260U5030B
<1.0 pg/L
03/29/2023
Methylene chloride
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Naphthalene
SW 846 Method 8260D 503013
<0.5 pg/L
03/29/2023
n-Butylbenzene
SW 846 Method 8260W503013
<0.5 pg/L
03/29/2023
n-Propylbenzene
SW 846 Method 82601)�503013
<0.5 pg/L
03/29/2023
ortho-Xylene
SW 846 Method 826oD/5030B
<0.5 pg/L
03/29/2023
p-Isopropyltoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
sec-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Styrene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
tert-Butyl benzene
SW 846 Method 826013/50308
<0.5 pg/L
03/29/2023
Tetrachloroethene
SW 846 Method 8260DIS030B
<0.5 pg/L
03/29/2023
Report #:: 2023-05841
Page 14 of 39

r000"-.— .-71 Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
M 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS '[e-mail]
City of Jacksonville
Date of Report: Apr 21, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-05841
Project ID: Monitoring Wells
Toluene
SW 846 Method 8260015030E
<0.5 pg/L
03/29/2023
Trans-1,2-Dichloroethene
SW 846 Method 8260015030B
<0.5 pg/L
03/29/2023
Trans- 1, 3-d ichloropropene
SW 846 Method 8260DIS030B
<0.5 pg/L
03/29/2023
Trichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Trichlorofluoromethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Vinyl chloride
SW 846 Method 82NM50308
<0.5 pg/L
03/29/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353 2, Rev 2.0, 1993
< 0.02 mg/L
03/23/2023
Nitrate+Nitrite-Nitrogen
EPA 353 2, Rev 2 0, 1993
< 0.02 mg/L
03/28/2023
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
04/04/2023
Report # 2023-05841 Page 15 of 39

qlenvirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
infoia,environmentalchemistscom
City of Jacksonville Date of Report: Apr 21, 2023
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Report #: 2023-05841
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-14715 Site: MW-12 3/22/2023 1:42 PM Water NB
Test Method Results Date Analyzed
Sulfate
EPA 300.0, Rev 2.1, 1993
8 mg/L
03/28/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
25.9 mg/L
03/30/2023
Chloride
SM4500 ci E-2011
6 mg/L
03/24/2023
1, 1, 1,2-Tetrachloroethane
SW 846 Method 6260D15030B
<0.5 pg/L
03/29/2023
1, 1, 1 -Trichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D/50308
<0,5 pg/L
03/29/2023
1,1,2-Trichloroethane
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
1,1-Dichloroethane
SW 846 Method 8260D15030B
<0,5 pg/L
03/29/2023
1,1-Dichloroethene
SW 846 Method 8280D/5030B
<0.5 pg/L
03/29/2023
1,1-Dichloropropene
SW 646 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2,3-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2,3-Trichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2,4-Trichlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
1, 2,4-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2-Dibromoethane
SW 848 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2-Dichlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
1,2-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2-Dichloropropane
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
1,3,5-Trimethylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
1,3-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,3-Dichloropropane
SW 646 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,4-Dichlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
2,2-Dichloropropane
SW 846 Method 826OD/50308
<0.5 pg/L
03/29/2023
2-Chlorotoluene
SW 846 Method 8260D150308
<0,5 pg/L
03/29/2023
4-Chlorotoluene
SW 846 Method 82BOD15030B
<0.5 pg/L
03/29/2023
Report A 2023-05841 Page 16 of 39

envirochem
isy
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
infoia environmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Apr 21, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-05841
Project ID: Monitoring Wells
Benzene
SW 846 Method 8260DIS030B
<0.5 pg/L
03/29/2023
Bromobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Bromodichloromethane
SW 846 Method 8260DIS030B
<0.5 pg/L
03/29/2023
Bromoform
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Bromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Carbon tetrachloride
SW 846 Method 8260DIS0308
<0.5 pg/L
03/29/2023
Chlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Chloroethane
SW 846 Method 826OD150308
<0.5 pg/L
03/29/2023
Chloroform
SW 846 Method 8260D150308
<0.5 pg/L
03/29/2023
Chloromethane
SW 846 Method 826OD150308
<0.5 pg/L
03/29/2023
cis-1,2-Dichloroethene
SW 846 Method 8260D150308
<0.5 pg/L
03/29/2023
cis-1,3-Dichloropropene
SW 846 Method 82BOD15030B
<0.5 pg/L
03/29/2023
Dibromochloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Dibromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Dichlorodifluoromethane
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
Ethylbenzene
SW 846 Method 8260DIS0308
<0.5 pg/L
03/29/2023
Hexachlorobutadiene
SW 846 Method 8260DIS0308
<0.5 pg/L
03/29/2023
1sopropylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
M+P Xylene
SW 646 Method 826OD150308
<1.0 pg/L
03/29/2023
Methylene chloride
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Naphthalene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
n-Butylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
n-Propylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
ortho-Xylene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
p-Isopropyltoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
sec-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Styrene
SW 846 Method 6260D/5030B
<0.5 pg/L
03/29/2023
te rt-Butyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Tetrachloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Reportk: 2023.05841
Page 17 of 39

F - 77""'41 "17
Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392,0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
eM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL 8 CONSULTING CHEMISTS info,cr.environmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Apr 21, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-05841
Project ID: Monitoring Wells
Toluene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Trans- 1,2-Dichloroethene
SW 846 Method 8260D/50308
<Q.5 pg/L
03/29/2023
Trans- 1,3-dichloropropene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Trich loroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Trichlorofluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Vinyl chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0, 1993
0.05 mg/L
03/23/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0, 1993
0.05 mg/L
03/28/2023
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
04/04/2023
Report ff : 2023-05841 Page 18 of 39

F07-
Cnvirochem
ANALYTICAL 8 CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
info' i environmentalchemists.com
City of Jacksonville
Date of Report: Apr 21, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report M 2023-05841
Project 10: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-14716 Site: MW-16
3/22/2023
10:03 AM Water NB
Test
Method
Results
Date Analyzed
Sulfate
EPA 300.0, Rev. 2.1, 1993
8 mg/L
03/28/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
2,3 mg/L
03/30/2023
Chloride
SM4500 CI E-2011
36 mg/L
03/24/2023
1. 1, 1,2-Tetrachloroethane
SW 846 Method 82BOD/5030B
<0.5 pg/L
03/29/2023
1,1,1-Trichloroethane
SW 846 Method 8260D/5030B
<0, 5 pg/L
03/29/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 826OD/5030B
<0.5 pg/L
03/29/2023
1,1,2-Trichloroethane
SW 846 Method 82BOD/50308
<0.5 pg/L
03/29/2023
1, 1 -Dichloroethane
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
1, 1 -Dichloroethene
SW 846 Method 82BOD/5030B
<0.5 pg/L
03/29/2023
1,1-Dichloropropene
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
1,2,3-Trichlorobenzene
SW 846 Method 626OD/50308
<0.5 pg/L
03/29/2023
1,2,3-Trichloropropane
SW 846 Method 828OD/50308
<0.5 pg/L
03/29/2023
1,2,4-Trichlorobenzene
SW 846 Method 82BOD/5030B
<0.5 pg/L
03/29/2023
1,2,4-Trimethylbenzene
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 82BOD/5030B
<0.5 pg/L
03/29/2023
1,2-Dibromoethane
SW 846 Method 82BOD/50308
<0.5 pg/L
03/29/2023
1,2-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2-Dichloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,2-Dichloropropane
SW 646 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,3,5-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,3-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,3-Dichloropropane
SW 846 Method 826OD/5030B
<0.5 pg/L
03/29/2023
1,4-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
2,2-Dichloropropane
SW 846 Method 8260D150308
<0.5 pg/L
03/29/2023
2-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
4-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Report #: 2023.05841
Page 19 of 39

F""" -- Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info(ci-environmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville INC
Attention:
28541
Date of Report: Apr 21, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-05841
Project ID: Monitoring Wells
Benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Bromobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Bromochloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Bromodichloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Bromoform
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Bromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Carbon tetrachloride
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Chlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Chloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Chloroform
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Chloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
cis- 1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
cis- 1,3-Dichloropropene
SW 846 Method 8260D/6030B
<0.5 pg/L
03/29/2023
Dibromochloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Dibromomethane
SW 846 Method 826OD150308
<0.5 pg/L
03/29/2023
Dichlorodifluoromethane
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
Ethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Hexachlorobutadiene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Isop ropylbenzene
SW 846 Method 826OD150308
<0.5 pg/L
03/29/2023
M+P Xylene
SW 846 Method 826OD150308
<1.0 pg/L
03/29/2023
Methylene chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Naphthalene
SW 846 Method 626oD/5030B
<0.5 pg/L
03/29/2023
n-Butylbenzene
SW 846 Method 8260015030E
<0.5 pg/L
03/29/2023
n-Propylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
ortho-Xylene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
p-Isopropyltoluene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
sec-Butylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Styrene
SW B46 Method 826OD15030B
<0.5 pg/L
03/29/2023
tert-Butyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Tetrachloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Report # 2023-05841
Page 20 of 39

ANALYTICAL rli CONSULTING CHEMISTS
F7- _741
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax
info environmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Apr 21, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-05841
Project ID: Monitoring Wells
Toluene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Trans-1,2-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Trans- 1, 3-dich loropropene
SW 846 Method 826OD150308
<0.5 Ng/L
03/29/2023
Trichloroethene
SW 846 Method 826OD15030B
<0,5 pg/L
03/29/2023
Trichlorofluoromethane
SW 846 Method 826OD150308
<0.5 pg/L
03/29/2023
Vinyl chloride
SW 846 Method 8260DIS0308
<0.5 Ng/L
03/29/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0. 1993
< 0.02 mg/L
03/23/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2. Rev 2.0, 1993
0.23 mg/L
03/28/2023
Nitrate Nitrogen
Subtraction Method
0.23 mg/L
04/04/2023
Report C 2023-05841 Page 21 of 39

F 7
�enviroc-he]m
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
infort, environmentalchemists.com
City of Jacksonville Date of Report: Apr 21, 2023
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Report #: 2023-05841
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-14717 Site: MW-17 3/22/2023 9:43 AM Water NB
Test Method Results Date Analyzed
Sulfate
EPA 300.0, Rev, 2.1, 1993
12 mg/L
03/28/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
3.1 mg/L
03/30/2023
Chloride
SM4500 cl E-2011
35 mg/L
03/24/2023
1,1,1,2-Tetrachloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,1,1-Trichloroethane
SW 846 Method 826013/5030
<0.5 pg/L
03/29/2023
1, 1,2,2-Tetrachloroeth a ne
SW 846 Method 8260015030B
<0.5 pg/L
03/29/2023
1,1,2-Trichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
1,1-Dichloroethane
SW 846 Method 8280D/5030B
<0.5 pg/L
03/29/2023
1,1-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,1-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2, 3-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2,3-Trichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2,4-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2,4-Trimethylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260DI5030B
<0.5 pg/L
03/29/2023
1,2-Dibromoethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2-Dichlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
1,2-Dichloroethane
SW 846 Method 8260DIS030B
<0.5 pg/L
03/29/2023
1,2-Dichloropropane
SW 846 Method 8260015030E
<0.5 pg/L
03/29/2023
1,3,5-Trimethylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,3-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,3-Dichloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
1,4-Dichlorobenzene
SW 846 Method 6260D/5030B
<0.5 pg/L
03/29/2023
2,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5pg/L
03/29/2023
2-Chlorotoluene
SW 846 Method 8260D/50308
<0.5pg/L
03/29/2023
4-Chlorotoluene
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
Report #: 2023-05841 Page 22 of 39

SN
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info a environmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Apr 21, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-05841
Project ID: Monitoring Wells
Benzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Bromobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Bromodichloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Bromoform
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Bromomethane
SW 846 Method 8260DIS030B
<0.5 pg/L
03/29/2023
Carbon tetrachloride
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Chlorobenzene
SW 846 Method 826OD150306
<0.5 pg/L
03/29/2023
Chloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Chloroform
SW 846 Method 826OD150308
<0.5 pg/L
03/29/2023
Chloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
cis- 1,2-Dichloroethene
SW 846 Method 826OD/50308
<0.5 pg/L
03/29/2023
cis-1,3-Dichloropropene
SW 846 Method 8260131503013
<0.5 pg/L
03/29/2023
Dibromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Dibromomethane
SW 846 Method 82600/5030B
<0.5 pg/L
03/29/2023
Dichlorodifluoromethane
SW 846 Method 828OD/5030B
<0.5 pg/L
03/29/2023
Ethylbenzene
SW 846 Method 826013/503013
<0.5 pg/L
03/29/2023
Hexachlorobutadiene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Isopropylbenzene
SW 846 Method 826013/50308
<0.5 pg/L
03/29/2023
M+P Xylene
SW 846 Method 8260D15030B
<1.0 pg/L
03/29/2023
Methylene chloride
SW 846 Method 826OD/50308
<0.5 pg/L
03/29/2023
Naphthalene
SW 846 Method 826OD/5030B
<0.5 pg/L
03/29/2023
n-Butylbenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
03/29/2023
n-Propylbenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
03/29/2023
ortho-Xylene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
p-Isopropyltoluene
SW 846 Method 8280D/5030B
<0.5 pg/L
03/29/2023
sec- B utyl benzene
SW 845 Method 826OD15030B
<0.5 pg/L
03/29/2023
Styrene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
tert-Butyl benzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Tetrachloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Report 9: 2023-05841
Page 23 of 39

pr
envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
City of Jacksonville Date of Report: Apr 21, 2023
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Report #: 2023-05841
Project ID: Monitoring Wells
Toluene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Trans-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Trans-1,3-dichloropropene
SW 846 Method 8260D/5030B
<0,5 ug/L
03/29/2023
Trichloroethene
SW 846 Method 8280D/5030B
<0,5 pg/L
03/29/2023
Trichlorofluoromethane
SW 846 Method 826OD/5030B
<0,5 pg/L
03/29/2023
Vinyl chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0, 1993
< 0.02 mg/L
03/23/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0, 1993
0.04 mg/L
03/28/2023
Nitrate Nitrogen
Subtraction Method
0.04 mg/L
04/04/2023
Report # 2023-05841 page 24 of 39

F"'O' -. -:,Oqql Environmental Chemists, Inc.
envirochem6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
L 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL 8 CONSULTING CHEMISTS info(a.envtronmentalchemists.com
City of Jacksonville
Date of Report: Apr 21, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report #: 2023-05841
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-14718 Site: MW-8
3/23/2023
9:16 AM Water NB
Test
Method
Results
Date Analyzed
Sulfate
EPA 300.0, Rev. 2.1, 1993
99 mg/L
03/28/2023
Total Organic Carbon (TOC)
SM 5310 8-2014
3.2 mg/L
03/30/2023
Chloride
SM4500 CI E-2011
6 mg/L
03/24/2023
1,1,1,2-Tetrachloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,1,1-Trichloroethane
SW 846 Method 8260D150308
<0.5 pg/L
03/29/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
1,1 2-Trichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
1,1-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1, 1 -Dichloroethene
SW 846 Method 8260D150308
<0.5 pg/L
03/29/2023
1,1-Dichloropropene
SW 846 Method B260D150308
<0.5 pg/L
03/29/2023
1,2,3-Trichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,2,3-Trichloropropane
SW 846 Method 8260D150308
<0.5 pg/L
03/29/2023
1,2.4-Trichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,2.4-Trimethyl benzene
SW 846 Method 826OD150308
<0.5 pg/L
03/29/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,2-Dibromoethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,2-Dichlorobenzene
SW 846 Method 8280D/5030B
<0.5 pg/L
03/29/2023
1,2-Dichloroethane
SW 846 Method 8280D/5030B
<0.5 pg/L
03/29/2023
1,2-Dichloropropane
SW 846 Method 826OD/5030B
<0.5 pg/L
03/29/2023
1,3.5-Trimethylbenzene
SW 846 Method 82BOD15030B
<0,5 pg/L
03/29/2023
1,3-Dichlorobenzene
SW 848 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,3-Dichloropropane
SW 846 Method 826013/50308
<0.5 pg/L
03/29/2023
1,4-Dichlorobenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
03/29/2023
2,2-Dichloropropane
SW 846 Method 826013/50308
<0.5 pg/L
03/29/2023
2-Chlorotoluene
SW 848 Method 826OD15030B
<0.5 pg/L
03/29/2023
4-Chlorotoluene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Report #.: 2023-05841
Page 25 of 39

FFI'ww--. -71 Environmental Chemists, Inc.
envirochem6602 Windmill Way, Wilmington, NC 28405 • 910,392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
sN 255 A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab,'Fax
ANALYTICAL & CONSULTING CHEMISTS info,a.environmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Apr 21, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-05841
Project ID: Monitoring Wells
Benzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Bromobenzene
SW 846 Method 826OD150306
<0.5 pg/L
03/29/2023
Bromochloromethane
SW 846 Method 8260015030E
<0.5 pg/L
03/29/2023
Bromodichloromethane
SW 846 Method 8260015030E
<0.5 pg/L
03/29/2023
Bromoform
SW 846 Method 8260015030E
<0.5 pg/L
03/29/2023
Bromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Carbon tetrachloride
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Chlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Chloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Chloroform
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Chloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
cis-1,2-Dichloroethene
SW 846 Method 826OD16030B
<0.5 pg/L
03/29/2023
cis-1,3-Dichloropropene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Dibromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Dibromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Dichlorodifluoromethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Ethylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Hexachlorobutadiene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Isopropylbenzene
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
M+P Xylene
SW 846 Method 826OD150308
<1.0 pg/L
03/29/2023
Methylene chloride
SW 846 Method 8260D150308
<0.5 pg/L
03/29/2023
Naphthalene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
n-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
n-Propylbenzene
SW 846 Method 828OD15030B
<0.5 pg/L
03/29/2023
ortho-Xylene
SW 846 Method 8280D15030B
<0.5 pg/L
03/29/2023
p-Isopropyltoluene
SW 846 Method 826OD150308
<0.5 pg/L
03/29/2023
sec-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Styrene
SW 846 Method 82600150308
<0.5 pg/L
03/29/2023
tert-B utyl benzene
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
Tetrachloroethene
SW 846 Method 826013150306
<0.5 pg/L
03/29/2023
Report #: 2023.05841
Page 26 of 39

Environmental Chemists, Inc.
117
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
[e-mail]
City of Jacksonville
Date of Report: Apr 21, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report #: 2023-05841
Project ID: Monitoring Wells
Toluene
SW 846 Method 8260D15030B
<0,5 pg/L
03/29/2023
Trans- 1,2-Dichloroethene
SW 846 Method 8280D/5030B
<0.5 pg/L
03/29/2023
Trans- l ,3-dichloropropene
SW 846 Method 826OD150308
<0.5 pg/L
03/29/2023
Trichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Trichlorofluoromethane
SW 846 Method 826OD160308
<0.5 pg/L
03/29/2023
Vinyl chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0, 1993
< 0.02 mg/L
03/23/2023
Nitrate+ N itrite-N itrogen
EPA 353.2, Rev. 2.0. 1993
0.03 mg/L
03/28/2023
Nitrate Nitrogen
Subtraction Method
0.03 mg/L
04/04/2023
Report M� 2023.05841 Page 27 of 39

FOP,— -- -177
SO
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info environmen talchemists.com
City of Jacksonville
Date of Report: Apr 21, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report #: 2023-05841
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-14719 Site: MW-9
3/23/2023
9:44 AM Water NB
Test
Method
Results
Date Analyzed
Sulfate
EPA 300.0, Rev 2.1, 1993
98 mg/L
03/28/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
2.4 mg/L
03/30/2023
Chloride
SM4500 CI E-2011
6 mg/L
03/24/2023
1, 1, 1,2-Tetrachloroethane
SW 846 Method 826OD15030B
<0 5 pg/L
03/29/2023
1, 1, 1 -Trichloroethane
SW 846 Method 82BOD15030B
<0.5 pg/L
03/29/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
1,1,2-Trichloroethane
SW a46 Method 82600/50309
<0.5 pg/L
03/29/2023
1,1-Dichloroethane
SW 846 Method 82600150308
<0.5 pg/L
03/29/2023
1,1-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
1,1-Dichloropropene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,2,3-Trichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,2,3-Trichloropropane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,2,4-Trichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
1,2,4-Trimethylbenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
03/29/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 826OD/5030B
<0.5 pg/L
03/29/2023
1,2-Dibromoethane
SW 846 Method 826OD/5030B
<0.5 pg/L
03/29/2023
1,2-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
1,2-Dichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
1,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,3,5-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,3-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,3-Dichloropropane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,4-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
2,2-Dichloropropane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
2-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
4-Chlorotoluene
SW 846 Method 826oD/5030B
<0.5 pg/L
03/29/2023
Report #: 2023.05841
Page 28 of 39

roll�- -- -71 Environmental Chemists, Inc.
envirochem6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Mantco, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab,' Fax
ANALYTICAL & CONSULTING CHEMISTS mf6a environmen talchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Apr 21 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-05841
Project ID: Monitoring Wells
Benzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Bromobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Bromodichloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Bromoform
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Bromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Carbon tetrachloride
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
Chlorobenzene
SW 846 Method 8280D/5030B
<0.5 pg/L
03/29/2023
Chloroethane
SW 846 Method 8260D/50308
<0 5 pg/L
03/29/2023
Chloroform
SW 846 Method 825cD150308
<0.5 pg/L
03/29/2023
Chloromethane
SW 846 Method 826oD15030B
<0.5 pg/L
03/29/2023
cis- 1,2-Dichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
cis- 1,3-Dichloropropene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Dibromochloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Dibromomethane
SW 846 Method 8260DIS030B
<0.5 pg/L
03/29/2023
Dichlorodifluoromethane
SW 846 Method 026OD15030B
<0.5 pg/L
03/29/2023
Ethylbenzene
SW 846 Method 826OD150308
<0.5 pg/L
03/29/2023
Hexachlorobutadiene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
isopropyl benzene
SW 846 Method 8260015030E
<0.5 pg/L
03/29/2023
M+P Xylene
SW 846 Method 8260015030E
<1.0 pg/L
03/29/2023
Methylene chloride
SW 846 Method 8260015030E
<0.5 pg/L
03/29/2023
Naphthalene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
n-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
n-Propylbenzene
SW 846 Method 8260DIS030B
<0.5 pq/L
03/29/2023
ortho-Xylene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
p-Isopropyltoluene
SW 845 Method 8260D/5030B
<0.5 pg/L
03/29/2023
sec -Butyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Styrene
SW 846 Method 826OD150308
<0.5 pg/L
03/29/2023
tert-Butyl benzene
SW 846 Method 826oD/5030B
<0.5 pg/L
03/29/2023
Tetrachloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Report # 2023-05841
Page 29 of 39

Environmental Chemists, Inc.
nvirocheinli 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
M 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Apr 21, 2023
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Report #: 2023-05841
Project ID: Monitoring Wells
Toluene
SW 846 Method 8260Dl5030B
<0.5 pg/L
03/29/2023
Trans-1 ,2-Dichloroethene
SW 846 Method 82WDI50308
<0.5 pg/L
03/29/2023
Trans- 1, 3-d ich loropropene
SW 846 Method 8260DIS030B
<0.5 pg/L
03/29/2023
Trichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Trichlorofluoromethane
SW 846 Method 828ODY6030B
<0.5 pg/L
03/29/2023
Vinyl chloride
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353 2, Rev. 2 0. 1993
< 0.02 mg/L
03/23/2023
Nitrate+Nitrite-Nitrogen
EPA 353 2 Rev 2 0, 1993
< 0.02 mg/L
03/28/2023
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
04/04/2023
Report # 2023-05841 Page 30 of 39

F - 77"l 0107
Environmental Chemists, Inc.
envirolchem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910 392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab;' Fax
SN 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab!Fax
ANALYTICAL & CONSULTING CHEMISTS infoiu environmentaicliemists.com
City of Jacksonville
Date of Report: Apr 21, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report #: 2023-05841
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
23-14720 Site: MW-10
3/23/2023
9:57 AM Water NB
Test
Method
Results
Date Analyzed
Sulfate
EPA 300.0, Rev. 2.1, 1993
152 mg/L
03/28/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
2.3 mg/L
03/30/2023
Chloride
SM4500 CI E-2011
17 mg/L
03/24/2023
1,1, i ,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,1,1-Trichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,1,2-Trichloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,1-Dichloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,1-Dichloroethene
SW 846 Method 8280D/5030B
<0.5 pg/L
03/29/2023
1,1-Dichloropropene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,2,3-Trichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
1,2,3-Trichloropropane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,2,4-Trichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,2,4-Trimethyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2-Dibromoethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2-Dichlorobenzene
SW 845 Method 8260D/50308
<0.5 pg/L
03/29/2023
1,2-Dichloroethane
SW 846 Method 826oD/5030B
<0.5 pg/L
03/29/2023
1,2-Dichloropropane
SW 846 Method 8260D/503oB
<0.5 pg/L
03/29/2023
1,3,5-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,3-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,3-Dichloropropane
SW 846 Method 826oD/5030B
<0.5 pg/L
03/29/2023
1,4-Dichlorobenzene
SW 646 Method 826OD15030B
<0.5 pg/L
03/29/2023
2,2-Dichloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
2-Chlorotoluene
SW 846 Method 826013/50306
<0.5 pg/L
03/29/2023
4-Chlorotoluene
SW 846 Method 8260DIS030B
<0.5 pg/L
03/29/2023
Report #: 2023.05841
Page 31 of 39

— -:",qql
F"0�0-41
Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
su 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL 8 CONSULTING CHEMISTS info-environmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Apr 21, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-05841
Project ID: Monitoring Wells
Benzene
SW 846 Method 826GD15030B
<0, 5 pg/L
03/29/2023
Bromobenzene
SW 846 Method 8260015030E
<0 5 pg/L
03/29/2023
Bromochloromethane
SW 846 Method 8260D/6030B
<0.5 pg/L
03/29/2023
Bromodichloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Bromoform
SW 846 Method 8260015030E
<0.5 pg/L
03/29/2023
Bromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Carbon tetrachloride
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Chlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Chloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Chloroform
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Chloromethane
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
cis- 1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
cis- 1,3-Dichloropropene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Dibromochloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Dibromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Dichlorodifluoromethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Ethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Hexachlorobutadiene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Isopropylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
M+P Xylene
SW 846 Method 8260D/5030B
<1.0 pg/L
03/29/2023
Methylene chloride
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Naphthalene
SW 846 Method 8260D150308
<0.5 pg/L
03/29/2023
n-Butylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
n-Propylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
ortho-Xylene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
p-Isopropyltoluene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
sec-Butylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Styrene
SW 846 Method 8280D/50308
<0.5 pg/L
03/29/2023
te rt-B utyl benzene
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
Tetrachloroethene
SW 846 Method 826013/50308
<0.5 pg/L
03/29/2023
Report #. 2023-05841
Page 32 of 39

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
inf6 a environmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Apr 21, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-05841
Project ID: Monitoring Wells
Toluene
SW 846 Method 82600/50308
<0.5 pg/L
03/29/2023
Trans- 1,2-Dichloroethene
SW 846 Method 8260DIS030B
<0.5 pg/L
03/29/2023
Trans- 1,3-dichloropropene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Trichloroethene
SW 846 Method 8260015030E
<0.5 pg/L
03/29/2023
Trichlorofluoromethane
SW 846 Method 8260015030B
<0.5 pg/L
03/29/2023
Vinyl chloride
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0, 1993
< 0.02 mg/L
03/23/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0, 1993
< 0.02 mg/L
03/28/2023
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
04/04/2023
Report # 2023-05841 Page 33 of 39

Environmental Chemists,
Inc.
' I
6602 Windmill Way,
Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown
Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
1111111h, --.A`M'
255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
infoiar env] ronmentalchemists.com
City of Jacksonville
Date of Report: Apr 21, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report #: 2023-05841
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-14721 Site: MW-13
3/23/2023
9:00 AM Water NS
Test
Method
Results Date
Analyzed
Sulfate
EPA 300.0, Rev. 2.1, 1993
<5 mg/L
03/28/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
1.7 mg/L
03/30/2023
Chloride
SM4500 CI E-2011
19 mg/L
03/24/2023
1,1,1,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,1,1-Trichloroethane
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
1,1,2-Trichloroethane
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
1,1-Dichloroethane
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
1,1-Dichloroethene
SW 846 Method 8260D/50306
<0.5 pg/L
03/29/2023
1, 1 -Dichloropropene
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
1,2,3-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2, 3-Trichloropropane
SW 846 Method 826oD/5030B
<0.5 pg/L
03/29/2023
1,2,4-Trichlorobenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
03/29/2023
1,2,4-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260015030B
<0.5 pg/L
03/29/2023
1,2-Dibromoethane
SW 846 Method 8260DIS0308
<0.5 pg/L
03/29/2023
1,2-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,3,5-Trimethyl benzene
SW 846 Method 8260D1503oB
<0.5 pg/L
03/29/2023
1,3-Dichlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
1,3-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,4-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
2,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
2-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
4-Chlorotoluene
SW 846 Method 8260D150308
<0.5 pg/L
03/29/2023
Report #:: 2023-05841
Page 34 of 39

Environmental Chemists, Inc.
gn=virochem
ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab, Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab Fax
[e-mail]
City of Jacksonville
Date of Report: Apr 21, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-05841
Project ID: Monitoring Wells
Benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Bromobenzene
SW 848 Method 826oD15030B
<0.5 pg/L
03/29/2023
Bromochloromethane
SW 846 Method 8266D/5030B
<0.5 pg/L
03/29/2023
Bromodichloromethane
SW 846 Method 8260D15D30B
<0.5 pg/L
03/29/2023
Bromoform
SW 846 Method 8260D15D30B
<0.5 pg/L
03/29/2023
Bromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Carbon tetrachloride
SW 846 Method 82BOD15030B
<0.5 pg/L
03/29/2023
Chlorobenzene
SW 846 Method 826CD15030B
<0.5 pg/L
03/29/2023
Chloroethane
SW a46 Method 8260D15030B
<0.5 pg/L
03/29/2023
Chloroform
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Chloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
cis-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
cis- 1,3-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Dibromochloromethane
SW 846 Method 8260015030E
<0.5 pg/L
03/29/2023
Dibromomethane
SW 846 Method 826oD/50308
<0.5 pg/L
03/29/2023
Dichlorodifluoromethane
SW 846 Method 826OD150308
<0.5 pg/L
03/29/2023
Ethylbenzene
SW 846 Method 826OD150308
<0.5 pg/L
03/29/2023
Hexachlorobutadiene
SW 846 Method 8260015030E
<0.5 pg/L
03/29/2023
Isopropylbenzene
SW 846 Method 8260015030E
<0.5 pg/L
03/29/2023
M+P Xylene
SW 845 Method 826OD15030B
<1.0 pg/L
03/29/2023
Methylene chloride
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Naphthalene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
n-Butylbenzene
SW 846 Method 8260DIS0308
<0.5 pg/L
03/29/2023
n-Propylbenzene
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
ortho-Xylene
SW 846 Method 8260DIS0308
<0.5 pg/L
03/29/2023
p-Isopropyltoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
sec -Butyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Styrene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
tert- Butyl benzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Tetrachloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Report M 2023-05841
Page 35 of 39

F"O�' -- —. """I Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
cM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info<,aenvironmentalchemists com
City of Jacksonville
Date of Report: Apr 21, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-05841
Project ID: Monitoring Wells
Toluene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Trans-1,2-Dichloroethene
SW 846 Method 8260Dl5030B
<0,5 pg/L
03/29/2023
Trans-1.3-dichloropropene
SW 846 Method 8260D/5030B
<0,5 pg/L
03/29/2023
Trichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Trichlorofluoromethane
SW 846 Method 8260Dl5030B
<0.5 pg/L
03/29/2023
Vinyl chloride
SW 846 Method 8260Dl5030B
<0.5 ug/L
03/29/2023
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 353.2, Rev 2.0, 1993
< 0,02 mg/L
03/23/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev 2.0, 1993
0.04 mg/L
03/28/2023
Nitrate Nitrogen
Subtraction Method
0.04 mg/L
04/04/2023
Report # 2023-05841 Page 36 of 39

F""� -- -7441
envirochem
sV
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab, Fax
infc�!a em ironmentalchemists.com
City of Jacksonville Date of Report: Apr 21, 2023
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Report #: 2023-05841
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-14722 Site: MW-14 3/23/2023 8A2 AM Water NB
Test Method Results Date Analyzed
Sulfate
EPA 300 0 Rev 2 t 1993
<5 mg/L
03/28/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
10.5 mg/L
03/30/2023
Chloride
SW500 ct E-2011
11 mg/L
03/24/2023
1,1,1,2-Tetrachloroethane
SW 846 Method 8260a 5030E
<0.5 pg/L
03/29/2023
1,1,1-Trichloroethane
SW 846 Method 8260050308
<0.5 pg/L
03/29/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,1,2-Trichloroethane
SW 846 Method 8280D/5030B
<0.5 pg/L
03/29/2023
1,1-Dichloroethane
SW 846 Method 826OD16030B
<0.5 pg/L
03/29/2023
1,1-Dichloroethene
SW 845 Method 8260DIS030B
<0.5 pg/L
03/29/2023
1, 1 -Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2,3-Trichlorobenzene
SW 846 Method 82600/5030B
<0.5 pg/L
03/29/2023
1,2,3-Trichloropropane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1, 2,4-Trichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
1,2,4-Trimethyl benzene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 826OD150308
<0.5 pg/L
03/29/2023
1,2-Dibromoethane
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
1,2-Dichlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
1,2-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,2-Dichloropropane
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
1,3,5-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1, 3-Dichlorobenzene
SW 845 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,3-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
1,4-Dichlorobenzene
SW 846 Method 826oD/5030B
<0.5 pg/L
03/29/2023
2,2-Dichloropropane
SW 846 Method 8260DI5030B
<0.5 pg/L
03/29/2023
2-Chlorotoluene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
4-Chlorotoluene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Report #: 2023.05841 Page 37 of 39

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infoa environmentalchemistscom
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Apr 21, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-05841
Project ID: Monitoring Wells
Benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Bromobenzene
SW 846 Method 8260DIS030B
<0.5 pg/L
03/29/2023
Bromochloromethane
SW 846 Method 826OD150308
<0.5 pg/L
03/29/2023
Bromodichloromethane
SW 846 Method 82600150308
<0 5 pg/L
03/29/2023
Bromoform
SW 846 Method 8260D150308
<0.5 pg/L
03/29/2023
Bromomethane
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
Carbon tetrachloride
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Chlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Chloroethane
SW 846 Method 8260015030E
<0 5 pg/L
03/29/2023
Chloroform
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Chloromethane
SW 846 Method 826GD15030B
<0.5 pg/L
03/29/2023
cis-1,2-Dichloroethene
SW 848 Method 8260015030B
<0.5 pg/L
03/29/2023
cis-1,3-Dichloropropene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Dibromochloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Dibromomethane
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Dichlorodifluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Ethylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
03/29/2023
Hexachlorobutadiene
SW 846 Method 8260D15030B
<0 5 pg/L
03/29/2023
Isopropylbenzene
SW 846 Method 8260D/5030B
<0 5 pg/L
03/29/2023
M+P Xylene
SW 846 Method 8260D/5030B
<1.0 pg/L
03/29/2023
Methylene chloride
SW 846 Method 826=5o30B
<0.5 pg/L
03/29/2023
Naphthalene
SW 846 Method 826015030B
<0.5 pg/L
03/29/2023
n-Butylbenzene
SW 846 Method 826oD/5030B
<0 5 pg/L
03/29/2023
n-Propylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
ortho-Xylene
SW 846 Method 826OD150308
<0.5 pg/L
03/29/2023
p-Isopropyltoluene
SW 846 Method 8260015030E
<0.5 pg/L
03/29/2023
sec -Butyl benzene
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Styrene
SW 846 Method 8260015030E
<0.5 pg/L
03/29/2023
tert-Butyl benzene
SW 846 Method 8260015030E
<0.5 pg/L
03/29/2023
Tetrachloroethene
SW 846 Method 8260015030B
<0.5 pg/L
03/29/2023
Report M. 2023-05841
Page 38 of 39

,,!nviroehem
t:M
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Apr 21, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-05841
Project ID: Monitoring Wells
Toluene
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Trans-1,2-Dichloroethene
SW 846 Method 8280D/50308
<0.5 pg/L
03/29/2023
Trans- 1,3-d ich loropropene
sw 846 Method 826OD150308
<0.5 pg/L
03/29/2023
Trichloroethene
SW 846 Method 8260D/50308
<0.5 pg/L
03/29/2023
Trichlorofluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
03/29/2023
Vinyl chloride
SW 846 Method 826OD15030B
<0.5 pg/L
03/29/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA353.2, Rev. 2.0, 1993
< 0.02 mg/L
03/23/2023
N itrate+N itrite- Nitrogen
EPA 353.2, Rev. 2.0, 1993
< 0.02 mg/L
03/28/2023
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
04/04/2023
Comment:
Reviewed by:
/
Report # 2023.05641 Page 39 of 39

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Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 ivindmi,; t';a
i''!rr`n4tan, NC 2840.
Sample Receipt Checklist 910.392.022_
2023
� C_' 1�`_ ie•J ii i Jj=_� 'I'' `�_. n
tL i,,G I%� ';r f j s Fares=rF on tre-
r.:
lQ',�i,lal tnrti 12. I; clstody ce31; 4'r ri c.
P=rat ire upon rccei p'e:Ere they J"irct/i: 1i'r ' 7
ternp?rature taker. ❑ Tem , ^ —I Corrected temperatUre a ;ort rac ---�—f
IR Gun ID. Thomas Traceable S/PJ 210886 369tGr� B,an., c''n`—
A�ainst Bottles �lCli
YES ❑ NO IR Gur Correction Factor'C: 0,O—
•3. I f tern + r —�
YES ❑ NO r P rature of cooker exceeded 6'C, a';as Pro•= r_
4. Were proper custody e J-Ct t",'VJQA notified?
}'ES ❑ NO y procedures {re(inquishad/receive S. Were sample (D's listed on the COC? dJ follor:ed?
YES ❑ Pd0 b. Were sampl_s 1D's listed cm sample containers?
YES ❑ 7. Were collection date and t, YES Cl r"0 me listed on the COC?
8, Were tests to be
YES ❑ F!0 performed listed on the COC?
_� Did samples arrive in proper contair�e
YES ❑ F;0 10. Dad samples arrive in , rs for each test?
good condition for each test
I$r YES ❑ NO Ill. Was adequate sample volume available —
YES ❑ NO 12. Were samples received within. C-'YES El NO proper holdin-
13. Were acid preserved samples received at a pNof<2 ttfor 7 req,�esred tesis?
❑ YES ❑ NO 14. Were cyanide samples received at a pH >12� �
El YES ❑ r"O
15. ''.'Mere sulfide samples received at a pH >5=
YES I
❑ Y-S ❑ n'q i6 v`. ere NH3/TKN/Phenol recc-ided at a C
T
❑ f.'0 i7, b:'ere h'orin_ res dua± of <r}.5 m/i
❑ Y=5 _ Sulfide/Cyanide recei,le ch.or.
d at a r,_
- NO 118 bVer- orthopizosphate sar?7 •es fiTt n-d,�a' or<0.5
T P' ere,. in the f;eld ;��'
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Sample Preservation:
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