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HomeMy WebLinkAboutNCG030301_2022 DMR_20221019 (tDMICk Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K2J0039 Project Description Stormwater Samples-Outfalls, Monthly For: Danny Hammon AP Exhaust Technology 300 Dixie TRL Goldsboro, NC 27530 Administration Brittany Smith Tuesday, October 18,2022 Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of your report was completed by Microbac Laboratories, Inc.-Fayetteville. If you have any questions, comments, or require further assistance regarding this report, please contact your service representative listed above. I certify that all test results meet all of the requirements of the accrediting authority listed within this report.Analytical results are reported on a'as received' basis unless specified otherwise.Analytical results for solids with units ending in (dry)are reported on a dry weight basis. A statement of uncertainty for each analysis is available upon request. This laboratory report shall not be reproduced, except in full,without the written approval of Microbac Laboratories.The reported results are related only to the samples analyzed as received. Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 12 VMICROBACR Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K2J0039 AP Exhaust Technology Project Name: Stormwater Samples-Outfalls, Monthly Danny Hammon Project/PO Number: N/A 300 Dixie TRL Received: 10/03/2022 Goldsboro, NC 27530 Reported: 10/18/2022 Case Narrative OUTFALL 3: pH: 7.53 Total rain fall: .51 inches OUTFALL 5: pH: 7.56 Total rain fall: .51 inches OUTFALL 7: pH: 8.4 Total rain fall: .51 inches Sample Summary Report Sample Name Laboratory ID Client Matrix Sample Type Sample Begin Sample Taken Lab Received Outfall 3 K2J0039-01 Aqueous Grab 09/30/22 12:50 10/03/22 09:10 Outfall 5 K2J0039-02 Aqueous Grab 09/30/22 12:40 10/03/22 09:10 Outfall 7 K2J0039-03 Aqueous Grab 09/30/22 12:20 10/03/22 09:10 Page 2 of 12 (tDMICROBAC ` Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K2J0039 Analytical Testing Parameters Client Sample ID: Outfall 3 Sample Matrix: Aqueous Collected By: Paul Hastings Lab Sample ID: K2J0039-01 Collection Date: 09/30/2022 12:50 Analyses Performed by: Microbac Laboratories Inc.,-Marietta, OH Metals Total by ICP Result RL Units DF Note Prepared Analyzed Analyst EPA 200.7,Rv.4.4(1994) Zinc 0.0264 0.0200 mg/L 1 10/07/22 1002 10/10/22 1922 LSJ Metals Total by ICPMS Result RL Units DF Note Prepared Analyzed Analyst EPA 200.8,Rv.5.4(1994) Copper 0.00304 0.00200 mg/L 1 10/07/22 1021 10/07/22 1338 JYH Lead 0.00233 0.00100 mg/L 1 10/07/22 1021 10/07/22 1338 JYH Analyses Performed by: Microbac Laboratories, Inc. -Fayetteville Inorganics Total Result RL Units DF Note Prepared Analyzed Analyst EPA 1664E Oil&Grease(HEM) <7.0 7.0 mg/L 1 10/14/22 1438 10/17/22 1130 JRB SM 2540 D-2015 Total Suspended Solids(TSS) 14.0 4.17 mg/L 2 10/04/22 1304 BNS Client Sample ID: Outfall 5 Sample Matrix: Aqueous Collected By: Paul Hastings Lab Sample ID: K2J0039-02 Collection Date: 09/30/2022 12:40 Analyses Performed by: Microbac Laboratories Inc.,-Marietta, OH Metals Total by ICP Result RL Units DF Note Prepared Analyzed Analyst EPA 200.7,Rv.4.4(1994) Zinc 0.0239 0.0200 mg/L 1 10/07/22 1002 10/10/22 1926 LSJ Metals Total by ICPMS Result RL Units DF Note Prepared Analyzed Analyst EPA 200.8,Rv.5.4(1994) Copper 0.00289 0.00200 mg/L 1 10/07/22 1021 10/07/22 1340 JYH Lead <0.00100 0.00100 mg/L 1 J 10/07/22 1021 10/07/22 1340 JYH Analyses Performed by: Microbac Laboratories, Inc. -Fayetteville Inorganics Total Result RL Units DF Note Prepared Analyzed Analyst EPA 1664B Oil&Grease(HEM) <6.3 6.3 mg/L 1 10/14/22 1438 10/17/22 1130 JRB SM 2540 D-2015 Total Suspended Solids(TSS) 11.3 3.33 mg/L 1 10/04/22 1304 BNS Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 3 of 12 (tDMICROBAC ` Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K2J0039 Client Sample ID: Outfall 7 Sample Matrix: Aqueous Collected By: Paul Hastings Lab Sample ID: K2J0039-03 Collection Date: 09/30/2022 12:20 Analyses Performed by: Microbac Laboratories Inc.,-Marietta, OH Metals Total by ICP Result RL Units DF Note Prepared Analyzed Analyst EPA 200.7,Rv.4.4(1994) Zinc 0.0331 0.0200 mg/L 1 10/07/22 1002 10/10/22 1930 LSJ Metals Total by ICPMS Result RL Units DF Note Prepared Analyzed Analyst EPA 200.8,Rv.5.4(1994) Copper 0.00399 0.00200 mg/L 1 10/07/22 1021 10/07/22 1342 JYH Lead <0.00100 0.00100 mg/L 1 J 10/07/22 1021 10/07/22 1342 JYH Analyses Performed by: Microbac Laboratories, Inc. -Fayetteville Inorganics Total Result RL Units DF Note Prepared Analyzed Analyst EPA 1664B Oil&Grease(HEM) <5.5 5.5 mg/L 1 10/04/22 0855 10/04/22 1100 WPR SM 2540 D-2015 Total Suspended Solids(TSS) <3.79 3.79 mg/L 2 10/04/22 1304 BNS Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 4 of 12 (tDMICROBAC ` Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K2J0039 Batch Log Summary Method Batch Laboratory ID Client/Source ID EPA 200.7, Rv. 4.4 (1994) B2J0334 B2J0334-BLK1 B2J0334-BS1 B2J0334-SRL1 M2J0320-01 K2J0039-01 Outfall 3 K2J0039-02 Outfall 5 K2J0039-03 Outfall 7 Method Batch Laboratory ID Client/Source ID EPA 200.8, Rv. 5.4 (1994) B2J0340 B2J0340-BLK1 B2J0340-BS1 B2J0340-SRL1 M2J0068-01 K2J0039-01 Outfall 3 K2J0039-01 Outfall 3 K2J0039-02 Outfall 5 K2J0039-02 Outfall 5 K2J0039-03 Outfall 7 K2J0039-03 Outfall 7 Method Batch Laboratory ID Client/Source ID EPA 1664E KJ20023 KJ20023-DUP1 K210203-03 KJ20023-BS1 KJ20023-MS1 K210203-04 K2J0039-03 Outfall 7 KJ20023-BLK1 Method Batch Laboratory ID Client/Source ID SM 2540 D-2015 KJ20025 K2J0039-02 Outfall 5 K2J0039-01 Outfall 3 KJ20025-BS1 K2J0039-03 Outfall 7 KJ20025-DUP1 K210007-01 KJ20025-BLK1 Method Batch Laboratory ID Client/Source ID EPA 1664E KJ21407 KJ21407-MS1 K2J0105-02 K2J0039-01 Outfall 3 KJ21407-BS1 KJ21407-DUP1 K2J0105-03 KJ21407-BLK1 K2J0039-02 Outfall 5 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 5 of 12 (tDMICROBAC Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K2J0039 Batch Quality Control Summary: Microbac Laboratories, Inc.-Fayetteville Spike Source %REC RPD Inorganics Total Result RL Units Level Result %REC Limits RPD Limit Notes Batch KJ20023-Wet Chem Aqueous-EPA 1664B Blank(KJ20023-BLK1) Prepared&Analyzed: 10/04/2022 Oil&Grease(HEM) <5.0 5.0 mg/L LCS(KJ20023-BS1) Prepared&Analyzed: 10/04/2022 Oil&Grease(HEM) 35.7 5.0 mg/L 40.0 89 78-114 Duplicate(KJ20023-DUP1) Source: K210203-03 Prepared&Analyzed: 10/04/2022 Oil&Grease(HEM) 112 10.5 mg/L 41.5 92 18 Matrix Spike(KJ20023-MS1) Source: K210203-04 Prepared&Analyzed: 10/04/2022 Oil&Grease(HEM) 289 13.2 mg/L 80.0 111 222 78-114 Batch KJ20025-Wet Chem Aqueous-SM 2540 D-2015 PBW01 (KJ20025-BLK1) Prepared&Analyzed: 10/04/2022 Total Suspended Solids(TSS) <83.3 83.3 mg/L LCSW01 (KJ20025-BS1) Prepared&Analyzed: 10/04/2022 Total Suspended Solids(TSS) 94.5 2.50 mg/L 99.4 95 95-105 TPE,CompositeD(KJ20025-DUP1) Source:K2I0007-01 Prepared&Analyzed: 10/04/2022 Total Suspended Solids(TSS) 51.2 9.62 mg/L 55.0 7 10 Batch KJ21407-Wet Chem Aqueous-EPA 1664B Blank(KJ21407-BLK1) Prepared: 10/14/2022 Analyzed: 10/17/2022 Oil&Grease(HEM) <5.0 5.0 mg/L LCS(KJ21407-BS1) Prepared: 10/14/2022 Analyzed: 10/17/2022 Oil&Grease(HEM) 31.8 5.0 mg/L 40.0 80 78-114 Duplicate(KJ21407-DUP1) Source:K2J0105-03 Prepared: 10/14/2022 Analyzed: 10/17/2022 Oil&Grease(HEM) <5.1 5.1 mg/L ND 18 Matrix Spike(KJ21407-MS1) Source:K2J0105-02 Prepared: 10/14/2022 Analyzed: 10/17/2022 Oil&Grease(HEM) 28.2 5.1 mg/L 40.0 ND 71 78-114 Batch Quality Control Summary: Microbac Laboratories Inc., -Marietta,OH Spike Source %REC RPD Metals Total by ICP Result MDL RL Units Level Result %REC Limits RPD Limit Notes Batch B2J0334-200.7- EPA 200.7, Rv.4.4(1994) Blank(B2J0334-BLK1) Prepared: 10/07/2022 Analyzed: 10/10/2022 Zinc <0.0100 0.0100 0.0200 mg/L LCS(B2J0334-BS1) Prepared: 10/07/2022 Analyzed: 10/10/2022 Zinc 0.551 0.0100 0.0200 mg/L 0.500 110 85-115 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 6 of 12 VMICROBACR Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K2J0039 Spike Source %REC RPD Metals Total by ICPMS Result MDL RL Units Level Result %REC Limits RPD Limit Notes Batch B2J0340-200.8 W-EPA 200.8, Rv.5.4(1994) Blank(B2J0340-BLK1) Prepared&Analyzed: 10/07/2022 Copper <0.00100 0.00100 0.00200 mg/L Lead <0.00050 0.000500 0.00100 mg/L 0 LCS(B2J0340-BS1) Prepared&Analyzed: 10/07/2022 Copper 0.165 0.00100 0.00200 mg/L 0.160 103 85-115 Lead 0.0801 0.000500 0.00100 mg/L 0.0800 100 85-115 Definitions J: The result is an estimated quantity.The associated numerical value is the approximate concentration of the analyte in the sample. MDL: Minimum Detection Limit mg/L: Milligrams per Liter RL: Reporting Limit RPD: Relative Percent Difference Cooler Receipt Log Cooler ID: Default Cooler Temp: 15.4°C Cooler Inspection Checklist Ice Present or not required? Yes Shipping containers sealed or not required? Yes Custody seals intact or not required? Yes Chain of Custody(COC)Present? Yes COC includes customer information? Yes Relinquished and received signature on COC? Yes Sample collector identified on COC? Yes Sample type identified on COC? Yes Correct type of Containers Received Yes Correct number of containers listed on COC? Yes Containers Intact? Yes COC includes requested analyses? Yes Enough sample volume for indicated tests received? Yes Sample labels match COC(Name, Date&Time?) Yes Samples arrived within hold time? Yes Correct preservatives on COC or not required? Yes Chemical preservations checked or not required? Yes Preservation checks meet method requirements? Yes VOA vials have zero headspace,or not recd.? Yes Project Requested Certification(s) Microbac Laboratories Inc.,-Marietta,OH 583 NC Dept.of the Environment and Natural Resources Microbac Laboratories, Inc.-Fayetteville 11 North Carolina DENR NPDES Report Comments Reviewed and Approved By: Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted. P4i►-1' 'MIL The data and information on this,and other accompanying documents,represents only the - sample(s)analyzed. This report is incomplete unless all pages indicated in the footnote are Brittany Smith present and an authorized signature is included. The services were provided under and Administration subject to Microbac's standard terms and conditions which can be located and reviewed at<https://www.microbac.com/standard-terms-conditions>. Reported: 10/18/2022 21:51 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 7 of 12 Lab Manager: Brittany Smith-N * MICROBAC' Chain of Custody HMO 1I13II11I11II11I11IIII�Ell o Microbac Laboratories, Inc. - Fayetteville K2J0039 cg TAT 7 days AP Exhaust Technology Project Name: Stormwater Samples -Outfalls, Monthly Danny Hammon 300 Dixie TRL Project/PO Number: N/A Goldsboro, NC 27530 Tenatively Scheduled: 10/3/2022 Phone: (919) 580-1940 Route: Client Sample ID: Outfall 3 Lab Sample ID: K2J0039-01 Matrix: Aqueous Sampled Date&Time: 06113D f ZDUI !7.50 Type: Grab � . .�.53 Analysis Method Field Results/Comments Hold Time 200.8 Cu EPA 200.8,Rv.5.4(1994) limit 0.007 mg/1 r ai l I 180.00 days 200.8 Pb EPA 200.8,Rv.5.4(1994) Fat 1 o Gj/ 'n//,,,1A0.00 days HEM-OG E1664B EPA 1664B l V' 25.00 days TSS SM2540-D SM 2540 D-2015 7.00 days 200.7 Zn EPA 200.7,Rv.4.4(1994) limit 0.067 mg/L 180.00 days Container(s) Designator 1 L-Bottle Glass Amber-H2SO4 A 1 L-Bottle Glass Amber-H2SO4 B 1 L-Bottle HDPE C 500m1-Bottle HDPE-HNO3 D Client Sample ID: Outfall 5 Lab Sample ID: K2J0039-02 Matrix: Aqueous Sampled Date&Time: oc1/ V/201,Z 1211D Type: Grab // Analysis Method Field Results/Comments .,..D ,�f rtakte .11 ',,. 5/Hold Time 200.8 Cu EPA 200.8,Rv. 5.4(1994) limit 0.007 mg/1 '''"'""�� 180.00 days 200.8 Pb EPA 200.8,Rv.5.4(1994) 180.00 days HEM-OG E 1664B EPA 1664B 25.00 days TSS SM2540-D SM 2540 D-2015 7.00 days 200.7 Zn EPA 200.7,Rv.4.4(1994) limit 0.067 mg/L 180.00 days Container(s) Designator 1 L-Bottle Glass Amber-H2SO4 A 1 L-Bottle Glass Amber-H2SO4 B 1 L-Bottle HDPE C 500m1-Bottle HDPE-HNO3 D Client Sample ID: Outfall 7 Lab Sample ID: K2J0039-03 Matrix: Aqueous Sampled Date Time:v" ZIV/U1 T MX Type: Grab pN - �.Lj itAlf vourKc Microbac Laboratories, Inc. Page 1 of 2 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Lab Manager: Brittany Smith 45> M I C R ® B A C Chain of Custody I IIIIIII III IIIIII IIII IIIII IIIII IIIII IIII IIII Microbac Laboratories, Inc. - Fayetteville K2J003c a_ AP Exhaust Technology Project Name: Stormwater Samples-Outfalls, Monthly Danny Hammon 300 Dixie TRL Project/PO Number: N/A Goldsboro, NC 27530 Tenatively Scheduled: 10/3/2022 Phone: (919) 580-1940 Route: Analysis Method Field Results/Comments Hold Time 200.8 Cu EPA 200.8, Rv.5.4(1994) limit 0.007 mg/1 180.00 days 200.8 Pb EPA 200.8, Rv.5.4(1994) 180.00 days HEM-OG E166413 EPA 1664E3 25.00 days TSS SM2540-D SM 2540 D-2015 7.00 days 200.7 Zn EPA 200.7,Rv.4.4(1994) limit 0.067 mg/L 180.00 days Container(s) Designator 1 L-Bottle Glass Amber-H2SO4 A 1 L-Bottle Glass Amber-H2SO4 B 1L-Bottle HDPE C 500m1-Bottle HDPE-HNO3 D Sampled by/Relinquished by: Date/Time: Received by: Date/Time: Printed Name:Paul Hastings Printed Name: Relinquished by: it j ) ' Datg/�ip}��'ng7 Received by: ' , 40, ,0111 Date IIns1202,1 Printed Name: �'(,�r//V I vI(J,�O qii 0 Printed Na /,//fn%fl/— / /D pgt0 Relinquished by: Date/Time: "' Received by: �'l 'iLl/,/ Date/Time: Printed Name: Printed Name: As Received at Laboratory:On lc . Yes/ o Temp: 5•L/C Thermometer ID: ?quit Total Containers: 12.00 Microbac Laboratories may be unab e to perform a portion of the requested testing in which case we will subcontract the analysis to an appropriately accredited laboratory. By signing this document you are acknowledging that you have been informed by Microbac that testing could be subcontracted and agree with this arrangement. Notes: Microbac Laboratories, Inc. Page 2 of 2 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com N IMIC PA 13 0 cz Environmental 0_ Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form,please visit https://deq.nc.gov/about/divisions/energy-mineral-land-resources/ npdes-stormwater-gps Permit No.: N/CI / / / / / I / or Certificate of Coverage No.: N/C/G/ o/j/0 /3 /0/ 1/ Facility Name: /177 cx/M¢vcj 7 r-cl •elO6/& 1—/..- C County: G/4-0,4l6- Phone No. f(q— <c 0 — 2-6 76 Inspector: Ag , ld 5TI/l/c`S Date of Inspection: Jo SE-fr 2e22- Time of Inspection: /2 - S t7 iii Total Event Precipitation(inches): ' S ' All permits require qualitative monitoring to be performed during a"measurable storm event." A"measurable storm event"is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period,and the permittee obtains approval from the local DEMLR Regional Office. By this signature,I certify that this report is accurate and complete to the best of my knowledge: i i (Si ature of Permittee or Designee) 1. Outfall escription: Outfall No. Structure(pipe,ditch, etc.): D 1Zl /f/7-- Receiving Stream: `7,�(4('i gAV c9p s,-r�//(y (/Z ;�,- Describe the industrial activities that occur within the outfall drainage area: 1,4-A/-(4fe; L0i9/NG' 7' GrVe:67 v/r'V'4i 0/-_ ' C1-S *K2J0039* Page 1 of2 III 1111111 liii liii SWU-242,Last modified 06/01/2018 01; -7 , S-6 Environmental 0_ Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form,please visit https://deq.nc.gov/about/divisions/energy-mineral-land-resources/ npdes-stormwater-gps Permit No.: N/C/ / / / / / / / or Certificate of Coverage No.: N/C/G/0/3/0/5/&/ /l Facility Name: i f f C yfottc 7 (ffv)1,0&i&5 1,i C County: ( i i1'lt/- Phone No. qv9 e) — 0-0eW Inspector: P4'U )11 )6 Date of Inspection: Jo Seel- 2 Z- TimeofInspection: (Z- go 011 Total Event Precipitation(inches): / S I All permits require qualitative monitoring to be performed during a"measurable storm event." j ! A"measurable storm event"is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the peuruttee is able to document that a shorter interval is representative for local storm events during the sampling period,and the permittee obtains approval from the local DEMLR { Regional Office. By this s' ature,I certify that this report is accurate and complete to the best of my knowledge: (Si e of Permittee or Designee) 1. Outfall Description: Outfall No. Structure(pipe, ditch,etc.): '77A / TGFI'/P77— Receiving Stream: er/Lixvf ny vF Describe the industrial activities that occur within the outfall drainage area: r4,'.l-?.N G G047)oei UjLo,'/)/A/ of *K2J0039* Page 1 of 2 III II III II 11111111 SWU-242,Last modified 06/01/2018 cy: ? , q c\i is CV o o) Environmental c_ Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form,please visit https://deq.nc.gov/about/divisions/energy-mineral-land-resources/ npdes-stormwater-gps Permit No.: N/C/ / / / / / / / or Certificate of Coverage No.: N/C/G/0/3/0/3/©/ // Facility Name: AP r7c If qvs '%C0-/"/0 L o 6/6-3 �C County: 1,.t4j-Gf/Vt Phone No. 1 /,-- cue - 2-01F6 Inspector: PA-VL_ 40-5T/;1)63 Date of Inspection: 30 S( 2d2.-z Time of Inspection: ____47,_±20 d4 4 Total Event Precipitation(inches): i S I All permits require qualitative monitoring to be performed during a"measurable storm event." A"measurable storm event"is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period,and the permittee obtains approval from the local DEMLR Regional Office. By t s igna e,I certify that this report is accurate and complete to the best of my knowledge: r (Si ature of Permittee or Designee) 1. Outfall Description: Outfall No. -7 Structure(pipe,ditch, etc.): T I IC 1( Receiving Stream: '-7L/ovr/l/1 or 57-bNe, c , Describe the industrial activities that occur within the outfall drainage area: rill ! 3IZUZ2 Page1of2 SWU-242,Last modified 06/01/2018 0 / '