WQ0013419_DWR ARO Groundwater Split Sampling Results_20221103

PO Number #
Loc. Descr.:ECUSTA SLUDGE LANDFILL MONITORING WELL Q88V2
Loc. Type:Monitoring Well
Collector:B LAVERTY
Collect Date:11/03/2022
Collect Time:10:05
Date Received:11/08/2022
Time Received:07:00
Location ID:1P88MWQ88V2
County:Transylvania
Region:Asheville
Labworks LoginID TASCENZO1Sample Matrix:GROUNDWATER
Report Print Date:
North Carolina Division of Water Resources Water Sciences Section Laboratory Results
VisitID
Sample Depth
AROReport To
River Basin
04/10/2023
Emergency
COC Yes/No
Sample ID:AD04135
12/14/22Final Report Date:
Final Report
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
NC CourierDelivery Method
ROUTINEPriority
Analysis
Date
Method
Reference
Result/
QualifierPQLAnalyte NameCAS #Units Validated by
AD04135
LAB
MSWIFT°CSample temperature at receipt by lab 11/8/221.2
NUT
EPA 350.1 REV 2 ALWILLIAMSmg/L as NUNH3 as N in liquid7664-41-7 11/10/220.02 0.02
EPA 353.2 REV 2 ALWILLIAMSmg/L as NNO2+NO3 as N in liquidE701177 11/10/220.02 0.23
EPA 365.1 REV 2 ALWILLIAMSmg/L as PUPhosphorus_total as P in liquid7723-14-0 11/22/220.02 0.02
EPA 351.2 REV 2 ALWILLIAMSmg/L as NUTotal Kjeldahl N as N in liquidTKN_N 11/23/220.3 0.3
MET
EPA 200.8 Rev5.4 JJURGEVICHug/LUAntimony by ICPMS7440-36-0 11/17/221010
EPA 200.8 Rev5.4 JJURGEVICHug/LUAs by ICPMS7440-38-2 11/17/222.0 2.0
EPA 200.7 Rev4.4 JJURGEVICHug/LUBa by ICP7440-38-3 11/17/221010
EPA 200.7 Rev4.4 JJURGEVICHmg/LCa by ICP7440-70-2 11/17/220.10 0.92
EPA 200.8 Rev5.4 JJURGEVICHug/LUCd by ICPMS7440-43-9 11/17/220.50 0.50
EPA 200.7 Rev4.4 JJURGEVICHug/LUCobalt by ICP7440-48-4 11/17/225050
EPA 200.8 Rev5.4 JJURGEVICHug/LUCr by ICPMS7440-47-3 11/17/225.0 5.0
EPA 200.8 Rev5.4 JJURGEVICHug/LUCu by ICPMS7440-50-8 11/17/222.0 2.0
EPA 200.7 Rev4.4 JJURGEVICHug/LFe by ICP7439-89-6 11/17/2250280
EPA 200.7 Rev4.4 JJURGEVICHmg/LMg by ICP7439-95-4 11/17/220.10 0.63
EPA 200.7 Rev4.4 JJURGEVICHug/LMn by ICP7439-96-5 11/17/221014
EPA 200.8 Rev5.4 JJURGEVICHug/LUMo by ICPMS7439-98-7 11/17/221010
EPA 200.7 Rev4.4 JJURGEVICHmg/LNa by ICP7440-23-5 11/17/220.10 1.3
EPA 200.8 Rev5.4 JJURGEVICHug/LUNi by ICPMS7440-02-0 11/17/222.0 2.0
EPA 200.8 Rev5.4 JJURGEVICHug/LUPb by ICPMS7439-92-1 11/17/222.0 2.0
EPA 200.8 Rev5.4 JJURGEVICHug/LUSe by ICPMS7782-49-2 11/17/221.0 1.0
EPA 200.7 Rev4.4 JJURGEVICHug/LUV by ICP7440-62-2 11/17/221010
EPA 200.8 Rev5.4 JJURGEVICHug/LUZn by ICPMS7440-66-6 11/17/221010
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
Page 1 of 1
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
PO Number #
Loc. Descr.:ECUSTA SLUDGE LANDFILL MONITORING WELL Q06V10
Loc. Type:Monitoring Well
Collector:B LAVERTY
Collect Date:11/03/2022
Collect Time:10:22
Date Received:11/08/2022
Time Received:07:00
Location ID:1P88MWQ06V10
County:Transylvania
Region:Asheville
Labworks LoginID TASCENZO1Sample Matrix:GROUNDWATER
Report Print Date:
North Carolina Division of Water Resources Water Sciences Section Laboratory Results
VisitID
Sample Depth
AROReport To
River Basin
04/10/2023
Emergency
COC Yes/No
Sample ID:AD04136
12/14/22Final Report Date:
Final Report
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
NC CourierDelivery Method
ROUTINEPriority
Analysis
Date
Method
Reference
Result/
QualifierPQLAnalyte NameCAS #Units Validated by
AD04136
LAB
MSWIFT°CSample temperature at receipt by lab 11/8/221.2
NUT
EPA 350.1 REV 2 ALWILLIAMSmg/L as NUNH3 as N in liquid7664-41-7 11/10/220.02 0.02
EPA 353.2 REV 2 ALWILLIAMSmg/L as NNO2+NO3 as N in liquidE701177 11/10/220.02 0.09
EPA 365.1 REV 2 ALWILLIAMSmg/L as PPhosphorus_total as P in liquid7723-14-0 11/22/220.02 0.03
EPA 351.2 REV 2 ALWILLIAMSmg/L as NUTotal Kjeldahl N as N in liquidTKN_N 11/23/220.3 0.3
MET
EPA 200.8 Rev5.4 JJURGEVICHug/LUAntimony by ICPMS7440-36-0 11/17/221010
EPA 200.8 Rev5.4 JJURGEVICHug/LAs by ICPMS7440-38-2 11/17/222.0 7.2
EPA 200.7 Rev4.4 JJURGEVICHug/LBa by ICP7440-38-3 11/17/221032
EPA 200.7 Rev4.4 JJURGEVICHmg/LCa by ICP7440-70-2 11/17/220.10 2.4
EPA 200.8 Rev5.4 JJURGEVICHug/LUCd by ICPMS7440-43-9 11/17/220.50 0.50
EPA 200.7 Rev4.4 JJURGEVICHug/LUCobalt by ICP7440-48-4 11/17/225050
EPA 200.8 Rev5.4 JJURGEVICHug/LUCr by ICPMS7440-47-3 11/17/225.0 5.0
EPA 200.8 Rev5.4 JJURGEVICHug/LUCu by ICPMS7440-50-8 11/17/222.0 8.5
EPA 200.7 Rev4.4 JJURGEVICHug/LFe by ICP7439-89-6 11/17/22507800
EPA 200.7 Rev4.4 JJURGEVICHmg/LMg by ICP7439-95-4 11/17/220.10 1.2
EPA 200.7 Rev4.4 JJURGEVICHug/LMn by ICP7439-96-5 11/17/2210220
EPA 200.8 Rev5.4 JJURGEVICHug/LUMo by ICPMS7439-98-7 11/17/221010
EPA 200.7 Rev4.4 JJURGEVICHmg/LNa by ICP7440-23-5 11/17/220.10 2.3
EPA 200.8 Rev5.4 JJURGEVICHug/LNi by ICPMS7440-02-0 11/17/222.0 6.5
EPA 200.8 Rev5.4 JJURGEVICHug/LPb by ICPMS7439-92-1 11/17/222.0 4.3
EPA 200.8 Rev5.4 JJURGEVICHug/LUSe by ICPMS7782-49-2 11/17/221.0 1.0
EPA 200.7 Rev4.4 JJURGEVICHug/LUV by ICP7440-62-2 11/17/221010
EPA 200.8 Rev5.4 JJURGEVICHug/LZn by ICPMS7440-66-6 11/17/221017
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
Page 1 of 1
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
PO Number #
Loc. Descr.:ECUSTA SLUDGE LANDFILL MONITORING WELL Q06V11
Loc. Type:Monitoring Well
Collector:B LAVERTY
Collect Date:11/03/2022
Collect Time:10:45
Date Received:11/08/2022
Time Received:07:00
Location ID:1P88MWQ06V11
County:Transylvania
Region:Asheville
Labworks LoginID TASCENZO1Sample Matrix:GROUNDWATER
Report Print Date:
North Carolina Division of Water Resources Water Sciences Section Laboratory Results
VisitID
Sample Depth
AROReport To
River Basin
04/10/2023
Emergency
COC Yes/No
Sample ID:AD04137
12/14/22Final Report Date:
Final Report
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
NC CourierDelivery Method
ROUTINEPriority
Analysis
Date
Method
Reference
Result/
QualifierPQLAnalyte NameCAS #Units Validated by
AD04137
LAB
MSWIFT°CSample temperature at receipt by lab 11/8/221.2
NUT
EPA 350.1 REV 2 ALWILLIAMSmg/L as NUNH3 as N in liquid7664-41-7 11/10/220.02 0.02
EPA 353.2 REV 2 ALWILLIAMSmg/L as NNO2+NO3 as N in liquidE701177 11/10/220.02 0.46
EPA 365.1 REV 2 ALWILLIAMSmg/L as PPhosphorus_total as P in liquid7723-14-0 11/22/220.02 0.02
EPA 351.2 REV 2 ALWILLIAMSmg/L as NUTotal Kjeldahl N as N in liquidTKN_N 11/23/220.3 0.3
MET
EPA 200.8 Rev5.4 JJURGEVICHug/LUAntimony by ICPMS7440-36-0 11/17/221010
EPA 200.8 Rev5.4 JJURGEVICHug/LUAs by ICPMS7440-38-2 11/17/222.0 2.0
EPA 200.7 Rev4.4 JJURGEVICHug/LUBa by ICP7440-38-3 11/17/221010
EPA 200.7 Rev4.4 JJURGEVICHmg/LCa by ICP7440-70-2 11/17/220.10 5.0
EPA 200.8 Rev5.4 JJURGEVICHug/LUCd by ICPMS7440-43-9 11/17/220.50 0.50
EPA 200.7 Rev4.4 JJURGEVICHug/LUCobalt by ICP7440-48-4 11/17/225050
EPA 200.8 Rev5.4 JJURGEVICHug/LUCr by ICPMS7440-47-3 11/17/225.0 5.0
EPA 200.8 Rev5.4 JJURGEVICHug/LUCu by ICPMS7440-50-8 11/17/222.0 2.0
EPA 200.7 Rev4.4 JJURGEVICHug/LFe by ICP7439-89-6 11/17/225071
EPA 200.7 Rev4.4 JJURGEVICHmg/LMg by ICP7439-95-4 11/17/220.10 2.4
EPA 200.7 Rev4.4 JJURGEVICHug/LMn by ICP7439-96-5 11/17/221018
EPA 200.8 Rev5.4 JJURGEVICHug/LUMo by ICPMS7439-98-7 11/17/221010
EPA 200.7 Rev4.4 JJURGEVICHmg/LNa by ICP7440-23-5 11/17/220.10 5.6
EPA 200.8 Rev5.4 JJURGEVICHug/LUNi by ICPMS7440-02-0 11/17/222.0 2.0
EPA 200.8 Rev5.4 JJURGEVICHug/LUPb by ICPMS7439-92-1 11/17/222.0 2.0
EPA 200.8 Rev5.4 JJURGEVICHug/LUSe by ICPMS7782-49-2 11/17/221.0 1.0
EPA 200.7 Rev4.4 JJURGEVICHug/LUV by ICP7440-62-2 11/17/221010
EPA 200.8 Rev5.4 JJURGEVICHug/LUZn by ICPMS7440-66-6 11/17/221010
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
Page 1 of 1
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
PO Number #
Loc. Descr.:ECUSTA SLUDGE LANDFILL MONITORING WELL Q06V9
Loc. Type:Monitoring Well
Collector:B LAVERTY
Collect Date:11/03/2022
Collect Time:11:16
Date Received:11/08/2022
Time Received:07:00
Location ID:1P88MWQ06V9
County:Transylvania
Region:Asheville
Labworks LoginID TASCENZO1Sample Matrix:GROUNDWATER
Report Print Date:
North Carolina Division of Water Resources Water Sciences Section Laboratory Results
VisitID
Sample Depth
AROReport To
River Basin
04/10/2023
Emergency
COC Yes/No
Sample ID:AD04138
12/14/22Final Report Date:
Final Report
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
NC CourierDelivery Method
ROUTINEPriority
Analysis
Date
Method
Reference
Result/
QualifierPQLAnalyte NameCAS #Units Validated by
AD04138
LAB
MSWIFT°CSample temperature at receipt by lab 11/8/221.2
NUT
EPA 350.1 REV 2 ALWILLIAMSmg/L as NUNH3 as N in liquid7664-41-7 11/10/220.02 0.02
EPA 353.2 REV 2 ALWILLIAMSmg/L as NUNO2+NO3 as N in liquidE701177 11/10/220.02 0.02
EPA 365.1 REV 2 ALWILLIAMSmg/L as PPhosphorus_total as P in liquid7723-14-0 11/22/220.02 0.07
EPA 351.2 REV 2 ALWILLIAMSmg/L as NUTotal Kjeldahl N as N in liquidTKN_N 11/23/220.3 0.3
MET
EPA 200.8 Rev5.4 JJURGEVICHug/LUAntimony by ICPMS7440-36-0 11/17/221010
EPA 200.8 Rev5.4 JJURGEVICHug/LUAs by ICPMS7440-38-2 11/17/222.0 2.0
EPA 200.7 Rev4.4 JJURGEVICHug/LBa by ICP7440-38-3 11/17/2210300
EPA 200.7 Rev4.4 JJURGEVICHmg/LPCa by ICP7440-70-2 11/17/221.0 170
EPA 200.8 Rev5.4 JJURGEVICHug/LUCd by ICPMS7440-43-9 11/17/220.50 0.50
EPA 200.7 Rev4.4 JJURGEVICHug/LUCobalt by ICP7440-48-4 11/17/225050
EPA 200.8 Rev5.4 JJURGEVICHug/LUCr by ICPMS7440-47-3 11/17/225.0 5.0
EPA 200.8 Rev5.4 JJURGEVICHug/LUCu by ICPMS7440-50-8 11/17/222.0 2.0
EPA 200.7 Rev4.4 JJURGEVICHug/LFe by ICP7439-89-6 11/17/22503700
EPA 200.7 Rev4.4 JJURGEVICHmg/LPMg by ICP7439-95-4 11/17/220.5 85
EPA 200.7 Rev4.4 JJURGEVICHug/LPMn by ICP7439-96-5 11/17/22505700
EPA 200.8 Rev5.4 JJURGEVICHug/LUMo by ICPMS7439-98-7 11/17/221010
EPA 200.7 Rev4.4 JJURGEVICHmg/LNa by ICP7440-23-5 11/17/220.10 34
EPA 200.8 Rev5.4 JJURGEVICHug/LNi by ICPMS7440-02-0 11/17/222.0 13
EPA 200.8 Rev5.4 JJURGEVICHug/LUPb by ICPMS7439-92-1 11/17/222.0 2.0
EPA 200.8 Rev5.4 JJURGEVICHug/LUSe by ICPMS7782-49-2 11/17/221.0 1.0
EPA 200.7 Rev4.4 JJURGEVICHug/LUV by ICP7440-62-2 11/17/221010
EPA 200.8 Rev5.4 JJURGEVICHug/LUZn by ICPMS7440-66-6 11/17/221010
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
Page 1 of 1
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
X X
X
X
Thallium (Tl)
X Tin (Sn)
X Titanium (Ti)
X X Vanadium (V)
X Zinc (Zn)
X Mercury 1631, low-level
X
X
X
X
X
X
X
X X
X X
X Residue: Suspended (Suspended Solids )A
Residue: Volatile/Fixed, Suspended A X
TDS - Total Dissolved Solids A X
Silica A
Sulfide A - J X
X Phytoplankton / Algae
Field Parameters (optional):
Preservative : Y
Composite
Grab
De-chlorinated in Field
ChlorinatedSampling
Method:
Other:Dissolved analysis: Enter "DIS" in
check-boxes for parameters
Sample
Depth:
Lab Comments:
Sodium (Na)E
Cyanotoxins:
C - L
Organochlorine Pesticides
Organonitrogen Pesticides
/ /
Lithium (Li)A - C
A - C
Chromium (Cr), Total
Ecusta Sludge Landfill - Monitoring Well Q88V2Location Description:
DWR Region:
(based on county)
River Basin:
Surface
Ground
Water SupplyFoam
Other:
E
Secchi
Depth:
Lot #s /
Collector
Comments:
Filtered
in Field
Water Temp (oC):pH (s.u.):
Nitric Acid Lot #NA1286140; Sulfuric Acid Lot#SA2263030
Filter Blank
Lab Use Only:
Time Received:
(24 hr format)
Date Received:
M/D/Y
:
Received By:
E
E PCBs (polychlorinated biphenyls)
E
E
E
Tag
ID
Hand Delivered
State Courier
.
Canal
Stormwater
LakeRiver/Stream
Estuary
Effluent
QATime (24 hr):
(begin/end)10:05 AM :
11/3/2022
Visit ID:
(optional)
Laboratory
Sample Number:
Collector:
DWR Office:
(or agency name)
Date
(m/d/y):
(begin/end)
1
Priority:
Ambient
Location Code:1P88MWQ88V2
Brett Laverty Location Type:
Monitoring Well
Trip Blank
/ /
Influent
Other:
E
A - C
Login file:
Conductivity
(µmhos/cm):
Metals Parameters:
North Carolina Division of Water Resources
Laboratory (Water Sciences Section)Water Sample Collection & Submittal Form
Waste
Blank
Notes:
County:Transylvania Water Matrix:
ARO
Solution
Routine
Compliance
COC
Emergency
Temperature on
Arrival (°C):
Delivery Method:
Barium (Ba)
Beryllium (Be)
Cadmium (Cd)
Copper (Cu)
Iron (Fe)
Lead (Pb)
E
E
E
E
E
E
Field Blank
Calcium (Ca)
Selenium (Se)
Silver (Ag)
Total Kjeldahl Nitrogen as N (TKN)
TPH Diesel Range
Boron (B)
Hardness, Total as CaCO3 - by titration
Acid Herbicides
Molybdenum (Mo)
Nickel (Ni)
A
A
Microcystin
E
Cobalt (Co)
Oil and Grease, HEM, Total Recoverable
TPH Gasoline Range
A - D - MA - C - D
Potassium (K)A - Z
E
A
A - I
Preservative
Antimony (Sb)
Chlorophyll a
Y
E
E
Nitrite as N (NO2-N)
Total Phosphorus as P (TP)
Nitrate as N (NO3-N calculated)
Phenols, Total Recoverable
Residue: Total (Total Solids )
Residue: Volatile/Fixed, Total
Preservative
A
Specific Conductance, at 25 oC
TOC - Total Organic Carbon
Turbidity
pH
Bromide
Chloride
A
Other Parameters:
Microbiology Parameters:Wet Chemistry Parameters:
Aluminum (Al)
A - D
A - D
A
Orthophosphate as P (PO4)
Ammonia as N (NH3-N)
Nitrate-Nitrite as N (NO3+NO2-N)
A
A - D
Arsenic (As)
Color: Platinum Cobalt
A
B - C
A
A - G
Fluoride
Sulfate
A
A
Hexavalent Chromium (Cr6+)
MBAS (surfactants)
A
A - D
A
Color: ADMI
Cyanide, Total
Preservative
E
E
E
E
E
E
E
Preservative
Alkalinity, as CaCO3, to pH 4.5/8.3
BOD: Biochemical Oxygen Demand, 5-day
cBOD: Carbonaceous BOD, 5-day
Coliform: Fecal MF
Coliform: Total MF
Nutrients Parameters:
A - H - P
COD: Chemical Oxygen Demand
A
A
A
A
B - C
A - C
A - R
Biological:
E
Tannin & Lignin
Perfluorinated Compounds (PFAS)
Organics Parameters:
Dissolved Oxygen
(ppm):
Salinity
(ppt):
Metals Parameters Con't:
A - C
A - C
Semi-Volatile Organics (BNAs)
E
E
Organophosphorus Pesticides
A - T
A - C - F - LVolatile Organics (VOA)
1,4-Dioxane
A - D
A - C - F - L
A - C
Magnesium (Mg)
E
Manganese (Mn)
Mercury (Hg)
Strontium (Sr)
E
Revision 4/4/2022Required: 1) Collector Initials and Date, 2) Circle each preservative option utilized next to each parameter.
Preservative Legend (circle above as needed): (A) cool ≤6°C, (B) cool <10°C, (C) 0.008% Na2S2O3 [when chlorine is present], (D) H2SO4 to pH <2, (E) HNO3 to pH <2, (F) HCl to pH <2, (G) H3PO4 to pH <2, (H) 6N NaOH to pH >10<11, (I) (NH4)2SO4 pH=9.3-9.7, (J) zinc acetate
& NaOH to pH to >9, (K) pH 6-9 ascorbic acid [when chlorine is present], (L) leave no headspace, (M) ferrous ammonium sulfate [when chlorine is present], (P) ascorbic acid [when chlorine is present], (R) Lugols, (T) Trizma [when chlorine is present], (Y) analyzed within
15 minutes of sample collection, (Z) filtered in field within 15 minutes using 0.45um pore size
X X
X
X
Thallium (Tl)
X Tin (Sn)
X Titanium (Ti)
X X Vanadium (V)
X Zinc (Zn)
X Mercury 1631, low-level
X
X
X
X
X
X
X
X X
X X
X Residue: Suspended (Suspended Solids )A
Residue: Volatile/Fixed, Suspended A X
TDS - Total Dissolved Solids A X
Silica A
Sulfide A - J X
X Phytoplankton / Algae
Field Parameters (optional):
Preservative : Y
Composite
Grab
De-chlorinated in Field
ChlorinatedSampling
Method:
Other:Dissolved analysis: Enter "DIS" in
check-boxes for parameters
Sample
Depth:
Lab Comments:
Sodium (Na)E
Cyanotoxins:
C - L
Organochlorine Pesticides
Organonitrogen Pesticides
/ /
Lithium (Li)A - C
A - C
Chromium (Cr), Total
Ecusta Sludge Landfill - Monitoring Well Q06V10Location Description:
DWR Region:
(based on county)
River Basin:
Surface
Ground
Water SupplyFoam
Other:
E
Secchi
Depth:
Lot #s /
Collector
Comments:
Filtered
in Field
Water Temp (oC):pH (s.u.):
Nitric Acid Lot #NA1286140; Sulfuric Acid Lot#SA2263030
Filter Blank
Lab Use Only:
Time Received:
(24 hr format)
Date Received:
M/D/Y
:
Received By:
E
E PCBs (polychlorinated biphenyls)
E
E
E
Tag
ID
Hand Delivered
State Courier
.
Canal
Stormwater
LakeRiver/Stream
Estuary
Effluent
QATime (24 hr):
(begin/end)10:22 AM :
11/3/2022
Visit ID:
(optional)
Laboratory
Sample Number:
Collector:
DWR Office:
(or agency name)
Date
(m/d/y):
(begin/end)
2
Priority:
Ambient
Location Code:1P88MWQ06V10
Brett Laverty Location Type:
Monitoring Well
Trip Blank
/ /
Influent
Other:
E
A - C
Login file:
Conductivity
(µmhos/cm):
Metals Parameters:
North Carolina Division of Water Resources
Laboratory (Water Sciences Section)Water Sample Collection & Submittal Form
Waste
Blank
Notes:
County:Transylvania Water Matrix:
ARO
Solution
Routine
Compliance
COC
Emergency
Temperature on
Arrival (°C):
Delivery Method:
Barium (Ba)
Beryllium (Be)
Cadmium (Cd)
Copper (Cu)
Iron (Fe)
Lead (Pb)
E
E
E
E
E
E
Field Blank
Calcium (Ca)
Selenium (Se)
Silver (Ag)
Total Kjeldahl Nitrogen as N (TKN)
TPH Diesel Range
Boron (B)
Hardness, Total as CaCO3 - by titration
Acid Herbicides
Molybdenum (Mo)
Nickel (Ni)
A
A
Microcystin
E
Cobalt (Co)
Oil and Grease, HEM, Total Recoverable
TPH Gasoline Range
A - D - MA - C - D
Potassium (K)A - Z
E
A
A - I
Preservative
Antimony (Sb)
Chlorophyll a
Y
E
E
Nitrite as N (NO2-N)
Total Phosphorus as P (TP)
Nitrate as N (NO3-N calculated)
Phenols, Total Recoverable
Residue: Total (Total Solids )
Residue: Volatile/Fixed, Total
Preservative
A
Specific Conductance, at 25 oC
TOC - Total Organic Carbon
Turbidity
pH
Bromide
Chloride
A
Other Parameters:
Microbiology Parameters:Wet Chemistry Parameters:
Aluminum (Al)
A - D
A - D
A
Orthophosphate as P (PO4)
Ammonia as N (NH3-N)
Nitrate-Nitrite as N (NO3+NO2-N)
A
A - D
Arsenic (As)
Color: Platinum Cobalt
A
B - C
A
A - G
Fluoride
Sulfate
A
A
Hexavalent Chromium (Cr6+)
MBAS (surfactants)
A
A - D
A
Color: ADMI
Cyanide, Total
Preservative
E
E
E
E
E
E
E
Preservative
Alkalinity, as CaCO3, to pH 4.5/8.3
BOD: Biochemical Oxygen Demand, 5-day
cBOD: Carbonaceous BOD, 5-day
Coliform: Fecal MF
Coliform: Total MF
Nutrients Parameters:
A - H - P
COD: Chemical Oxygen Demand
A
A
A
A
B - C
A - C
A - R
Biological:
E
Tannin & Lignin
Perfluorinated Compounds (PFAS)
Organics Parameters:
Dissolved Oxygen
(ppm):
Salinity
(ppt):
Metals Parameters Con't:
A - C
A - C
Semi-Volatile Organics (BNAs)
E
E
Organophosphorus Pesticides
A - T
A - C - F - LVolatile Organics (VOA)
1,4-Dioxane
A - D
A - C - F - L
A - C
Magnesium (Mg)
E
Manganese (Mn)
Mercury (Hg)
Strontium (Sr)
E
Revision 4/4/2022Required: 1) Collector Initials and Date, 2) Circle each preservative option utilized next to each parameter.
Preservative Legend (circle above as needed): (A) cool ≤6°C, (B) cool <10°C, (C) 0.008% Na2S2O3 [when chlorine is present], (D) H2SO4 to pH <2, (E) HNO3 to pH <2, (F) HCl to pH <2, (G) H3PO4 to pH <2, (H) 6N NaOH to pH >10<11, (I) (NH4)2SO4 pH=9.3-9.7, (J) zinc acetate
& NaOH to pH to >9, (K) pH 6-9 ascorbic acid [when chlorine is present], (L) leave no headspace, (M) ferrous ammonium sulfate [when chlorine is present], (P) ascorbic acid [when chlorine is present], (R) Lugols, (T) Trizma [when chlorine is present], (Y) analyzed within
15 minutes of sample collection, (Z) filtered in field within 15 minutes using 0.45um pore size
X X
X
X
Thallium (Tl)
X Tin (Sn)
X Titanium (Ti)
X X Vanadium (V)
X Zinc (Zn)
X Mercury 1631, low-level
X
X
X
X
X
X
X
X X
X X
X Residue: Suspended (Suspended Solids )A
Residue: Volatile/Fixed, Suspended A X
TDS - Total Dissolved Solids A X
Silica A
Sulfide A - J X
X Phytoplankton / Algae
Field Parameters (optional):
Preservative : Y
Composite
Grab
De-chlorinated in Field
ChlorinatedSampling
Method:
Other:Dissolved analysis: Enter "DIS" in
check-boxes for parameters
Sample
Depth:
Lab Comments:
Sodium (Na)E
Cyanotoxins:
C - L
Organochlorine Pesticides
Organonitrogen Pesticides
/ /
Lithium (Li)A - C
A - C
Chromium (Cr), Total
Ecusta Sludge Landfill - Monitoring Well Q06V11Location Description:
DWR Region:
(based on county)
River Basin:
Surface
Ground
Water SupplyFoam
Other:
E
Secchi
Depth:
Lot #s /
Collector
Comments:
Filtered
in Field
Water Temp (oC):pH (s.u.):
Nitric Acid Lot #NA1286140; Sulfuric Acid Lot#SA2263030
Filter Blank
Lab Use Only:
Time Received:
(24 hr format)
Date Received:
M/D/Y
:
Received By:
E
E PCBs (polychlorinated biphenyls)
E
E
E
Tag
ID
Hand Delivered
State Courier
.
Canal
Stormwater
LakeRiver/Stream
Estuary
Effluent
QATime (24 hr):
(begin/end)10:45 AM :
11/3/2022
Visit ID:
(optional)
Laboratory
Sample Number:
Collector:
DWR Office:
(or agency name)
Date
(m/d/y):
(begin/end)
3
Priority:
Ambient
Location Code:1P88MWQ06V11
Brett Laverty Location Type:
Monitoring Well
Trip Blank
/ /
Influent
Other:
E
A - C
Login file:
Conductivity
(µmhos/cm):
Metals Parameters:
North Carolina Division of Water Resources
Laboratory (Water Sciences Section)Water Sample Collection & Submittal Form
Waste
Blank
Notes:
County:Transylvania Water Matrix:
ARO
Solution
Routine
Compliance
COC
Emergency
Temperature on
Arrival (°C):
Delivery Method:
Barium (Ba)
Beryllium (Be)
Cadmium (Cd)
Copper (Cu)
Iron (Fe)
Lead (Pb)
E
E
E
E
E
E
Field Blank
Calcium (Ca)
Selenium (Se)
Silver (Ag)
Total Kjeldahl Nitrogen as N (TKN)
TPH Diesel Range
Boron (B)
Hardness, Total as CaCO3 - by titration
Acid Herbicides
Molybdenum (Mo)
Nickel (Ni)
A
A
Microcystin
E
Cobalt (Co)
Oil and Grease, HEM, Total Recoverable
TPH Gasoline Range
A - D - MA - C - D
Potassium (K)A - Z
E
A
A - I
Preservative
Antimony (Sb)
Chlorophyll a
Y
E
E
Nitrite as N (NO2-N)
Total Phosphorus as P (TP)
Nitrate as N (NO3-N calculated)
Phenols, Total Recoverable
Residue: Total (Total Solids )
Residue: Volatile/Fixed, Total
Preservative
A
Specific Conductance, at 25 oC
TOC - Total Organic Carbon
Turbidity
pH
Bromide
Chloride
A
Other Parameters:
Microbiology Parameters:Wet Chemistry Parameters:
Aluminum (Al)
A - D
A - D
A
Orthophosphate as P (PO4)
Ammonia as N (NH3-N)
Nitrate-Nitrite as N (NO3+NO2-N)
A
A - D
Arsenic (As)
Color: Platinum Cobalt
A
B - C
A
A - G
Fluoride
Sulfate
A
A
Hexavalent Chromium (Cr6+)
MBAS (surfactants)
A
A - D
A
Color: ADMI
Cyanide, Total
Preservative
E
E
E
E
E
E
E
Preservative
Alkalinity, as CaCO3, to pH 4.5/8.3
BOD: Biochemical Oxygen Demand, 5-day
cBOD: Carbonaceous BOD, 5-day
Coliform: Fecal MF
Coliform: Total MF
Nutrients Parameters:
A - H - P
COD: Chemical Oxygen Demand
A
A
A
A
B - C
A - C
A - R
Biological:
E
Tannin & Lignin
Perfluorinated Compounds (PFAS)
Organics Parameters:
Dissolved Oxygen
(ppm):
Salinity
(ppt):
Metals Parameters Con't:
A - C
A - C
Semi-Volatile Organics (BNAs)
E
E
Organophosphorus Pesticides
A - T
A - C - F - LVolatile Organics (VOA)
1,4-Dioxane
A - D
A - C - F - L
A - C
Magnesium (Mg)
E
Manganese (Mn)
Mercury (Hg)
Strontium (Sr)
E
Revision 4/4/2022Required: 1) Collector Initials and Date, 2) Circle each preservative option utilized next to each parameter.
Preservative Legend (circle above as needed): (A) cool ≤6°C, (B) cool <10°C, (C) 0.008% Na2S2O3 [when chlorine is present], (D) H2SO4 to pH <2, (E) HNO3 to pH <2, (F) HCl to pH <2, (G) H3PO4 to pH <2, (H) 6N NaOH to pH >10<11, (I) (NH4)2SO4 pH=9.3-9.7, (J) zinc acetate
& NaOH to pH to >9, (K) pH 6-9 ascorbic acid [when chlorine is present], (L) leave no headspace, (M) ferrous ammonium sulfate [when chlorine is present], (P) ascorbic acid [when chlorine is present], (R) Lugols, (T) Trizma [when chlorine is present], (Y) analyzed within
15 minutes of sample collection, (Z) filtered in field within 15 minutes using 0.45um pore size
X X
X
X
Thallium (Tl)
X Tin (Sn)
X Titanium (Ti)
X X Vanadium (V)
X Zinc (Zn)
X Mercury 1631, low-level
X
X
X
X
X
X
X
X X
X X
X Residue: Suspended (Suspended Solids )A
Residue: Volatile/Fixed, Suspended A X
TDS - Total Dissolved Solids A X
Silica A
Sulfide A - J X
X Phytoplankton / Algae
Field Parameters (optional):
Preservative : Y
Composite
Grab
De-chlorinated in Field
ChlorinatedSampling
Method:
Other:Dissolved analysis: Enter "DIS" in
check-boxes for parameters
Sample
Depth:
Lab Comments:
Sodium (Na)E
Cyanotoxins:
C - L
Organochlorine Pesticides
Organonitrogen Pesticides
/ /
Lithium (Li)A - C
A - C
Chromium (Cr), Total
Ecusta Sludge Landfill - Monitoring Well Q06V9Location Description:
DWR Region:
(based on county)
River Basin:
Surface
Ground
Water SupplyFoam
Other:
E
Secchi
Depth:
Lot #s /
Collector
Comments:
Filtered
in Field
Water Temp (oC):pH (s.u.):
Nitric Acid Lot #NA1286140; Sulfuric Acid Lot#SA2263030
Filter Blank
Lab Use Only:
Time Received:
(24 hr format)
Date Received:
M/D/Y
:
Received By:
E
E PCBs (polychlorinated biphenyls)
E
E
E
Tag
ID
Hand Delivered
State Courier
.
Canal
Stormwater
LakeRiver/Stream
Estuary
Effluent
QATime (24 hr):
(begin/end)11:16 AM :
11/3/2022
Visit ID:
(optional)
Laboratory
Sample Number:
Collector:
DWR Office:
(or agency name)
Date
(m/d/y):
(begin/end)
4
Priority:
Ambient
Location Code:1P88MWQ06V9
Brett Laverty Location Type:
Monitoring Well
Trip Blank
/ /
Influent
Other:
E
A - C
Login file:
Conductivity
(µmhos/cm):
Metals Parameters:
North Carolina Division of Water Resources
Laboratory (Water Sciences Section)Water Sample Collection & Submittal Form
Waste
Blank
Notes:
County:Transylvania Water Matrix:
ARO
Solution
Routine
Compliance
COC
Emergency
Temperature on
Arrival (°C):
Delivery Method:
Barium (Ba)
Beryllium (Be)
Cadmium (Cd)
Copper (Cu)
Iron (Fe)
Lead (Pb)
E
E
E
E
E
E
Field Blank
Calcium (Ca)
Selenium (Se)
Silver (Ag)
Total Kjeldahl Nitrogen as N (TKN)
TPH Diesel Range
Boron (B)
Hardness, Total as CaCO3 - by titration
Acid Herbicides
Molybdenum (Mo)
Nickel (Ni)
A
A
Microcystin
E
Cobalt (Co)
Oil and Grease, HEM, Total Recoverable
TPH Gasoline Range
A - D - MA - C - D
Potassium (K)A - Z
E
A
A - I
Preservative
Antimony (Sb)
Chlorophyll a
Y
E
E
Nitrite as N (NO2-N)
Total Phosphorus as P (TP)
Nitrate as N (NO3-N calculated)
Phenols, Total Recoverable
Residue: Total (Total Solids )
Residue: Volatile/Fixed, Total
Preservative
A
Specific Conductance, at 25 oC
TOC - Total Organic Carbon
Turbidity
pH
Bromide
Chloride
A
Other Parameters:
Microbiology Parameters:Wet Chemistry Parameters:
Aluminum (Al)
A - D
A - D
A
Orthophosphate as P (PO4)
Ammonia as N (NH3-N)
Nitrate-Nitrite as N (NO3+NO2-N)
A
A - D
Arsenic (As)
Color: Platinum Cobalt
A
B - C
A
A - G
Fluoride
Sulfate
A
A
Hexavalent Chromium (Cr6+)
MBAS (surfactants)
A
A - D
A
Color: ADMI
Cyanide, Total
Preservative
E
E
E
E
E
E
E
Preservative
Alkalinity, as CaCO3, to pH 4.5/8.3
BOD: Biochemical Oxygen Demand, 5-day
cBOD: Carbonaceous BOD, 5-day
Coliform: Fecal MF
Coliform: Total MF
Nutrients Parameters:
A - H - P
COD: Chemical Oxygen Demand
A
A
A
A
B - C
A - C
A - R
Biological:
E
Tannin & Lignin
Perfluorinated Compounds (PFAS)
Organics Parameters:
Dissolved Oxygen
(ppm):
Salinity
(ppt):
Metals Parameters Con't:
A - C
A - C
Semi-Volatile Organics (BNAs)
E
E
Organophosphorus Pesticides
A - T
A - C - F - LVolatile Organics (VOA)
1,4-Dioxane
A - D
A - C - F - L
A - C
Magnesium (Mg)
E
Manganese (Mn)
Mercury (Hg)
Strontium (Sr)
E
Revision 4/4/2022Required: 1) Collector Initials and Date, 2) Circle each preservative option utilized next to each parameter.
Preservative Legend (circle above as needed): (A) cool ≤6°C, (B) cool <10°C, (C) 0.008% Na2S2O3 [when chlorine is present], (D) H2SO4 to pH <2, (E) HNO3 to pH <2, (F) HCl to pH <2, (G) H3PO4 to pH <2, (H) 6N NaOH to pH >10<11, (I) (NH4)2SO4 pH=9.3-9.7, (J) zinc acetate
& NaOH to pH to >9, (K) pH 6-9 ascorbic acid [when chlorine is present], (L) leave no headspace, (M) ferrous ammonium sulfate [when chlorine is present], (P) ascorbic acid [when chlorine is present], (R) Lugols, (T) Trizma [when chlorine is present], (Y) analyzed within
15 minutes of sample collection, (Z) filtered in field within 15 minutes using 0.45um pore size