WQ0003698_Groundwater Monitoring Report March 2023_20230425

1
Enter date monitoring results were due. ( l' Z) Will this monitoring report (GW-59 and GW-59A)
YES
NO
be submitted after the established due date?
X
2
Was any required information missing on the GW-59 report forms?
YES
NO
IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc.)? If the answer is "Yes ", contact the Regional Office for guidance.
4
Are any monitored constituents equal to or above the established standards?
YES
NO
If the answer to question 4 is "NO", skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the provided below:
space
A'�G�P e�
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
YES
NO
same constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is NO", skip to section 8.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
cJveA
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
If the answer is "YES". a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells maybe improperly
located; contact the Regional Office.
Com
7
Is the permittee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem?
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation,
fines, and/or penalties.
g
The person completing this portion (G W-59A) of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby acknowledge thatthe above informafipn wasr.evaluated and theinform submitted in this
report (Compliance Report GW-59A) is; true and complete to the best of my knowledge. '<
�Signa re of Permittee (oRrAut rized Age t) Date

Question #4
LAB DATA WHICH EXCEEDS PERMIT
DATE
MONITORING WELL #
PARAMETER
REPORTED
DATA
3.23.23
1
pH
5.9
2
Ammonia
5.9 mg/L
Cobalt
1.1 ug/L
Iron
50,400 ug/L
Manganese
1,310 ug/L
3
pH
5.2
Cobalt
2.2 ug/L
Manganese
70.6 ug/L
4
pH
5.0
Cobalt
3.3 ug/L
Manganese
126 ug/L

QUESTION #5
LAB DATA WHICH EXCEEDS PERMIT FOR LAST 2 PREVIOUS YEARS
5/18 & 6/1/2021
1
Iron
0.948 mg/L
pH
5.9
2
Ammonia
7.3 mg/L
Iron
39.5mg/L
Manganese
1060 ug/L
3
Nitrate
21.2mg/L
Iron
0.937mg/L
Manganese
265 ug/L
pH
4.9
4
Manganese
207 ug/L
pH
5
11.30.21
1
pH
5.9
2
Ammonia
6.0 mg/L
Iron
28.4mg/L
Manganese
1080 ug/L
pH
6
3
Nitrate
12.1mg/L
Manganese
132 ug/L
pH
5
4
Manganese
119 ug/L
pH
5.1
5/27-6/9/2022
1
pH
5.7
2
Ammonia
6.4 mg/L
Iron
43.9 mg/L
Manganese
1,200 ug/L
pH
6.3
3
Manganese
107 ug/L
4
pH
5.0
Manganese
172 ug/L
pH
5.0
11.3.22
1
pH
5.9
2
Ammonia
5.4 mg/L
Iron
27,100ug/L
Manganese
1,250 ug/L
pH
6.4
3
Cobalt
2.5 ug/L
Manganese
98.5 ug/L
pH
5.1
4
Manganese
86 ug/L
pH
4.9

3.23.23
1
pH
5.9
2
Ammonia
5.9 mg/L
Cobalt
1.1 ug/L
Iron
50,400 ug/L
Manganese
1,310 ug/L
3
pH
5.2
Cobalt
2.2 ug/L
Manganese
70.6 ug/L
4
pH
5
Cobalt
3.3 ug/L
Manganese
126 ug/L

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aceAr�alytic�l
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r
April 03, 2023
Mr. Tim Horton
City of Marion
3982 NC Hwy 226 South
Marion, NC 28752
RE: Project: MONITORING WELLS
Pace Project No.: 92658357
Dear Mr. Horton:
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on March 22, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNUNELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Jonathan W Biddix
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 22

a�ceAna! ica��
Y www:p>�iBbs.Co�
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Project: MONITORING WELLS
Pace Project No.: 92658357
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804 South Carolina Laboratory ID: 99030
Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001
North Carolina Drinking Water Certification #: 37712 Virginia/VELAP Certification #: 460222
North Carolina Wastewater Certification #: 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 22

laceAnalXkal
1 W: ahs"M
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f
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE SUMMARY
Project: MONITORING WELLS
Pace Project No.: 92658357
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92658357001
MW-1R
Water
03/2212311:25
03/22/2316:51
92658357002
MWA
Water
03/2212312:35
03/22/2316:51
92658357003
MW-2
Water
03/2212313:35
03/2212316:51
92658357004
MW-3
Water
03/2212314:55
03/2212316:51
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 22

alueAnal cal e
W9V81. �S.CC16
7:
f
SAMPLE ANALYTE COUNT
Project: MONITORING WELLS
Pace Project No.: 92658357
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Analyses
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92658357001
MWA R
EPA 200.8 Rev 5.4 1994
CRW, KRL
6
PASI-A
SM 4500-H+B-2011
SMS
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
4
PASI-A
EPA350.1 Rev 2.01993
ARJ
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
92658357002
MW-4
EPA 200.8 Rev 5.4 1994
CRW, KRL
6
PASI-A
SM 4500-H+B-2011
SMS
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
4
PASI-A
EPA350.1 Rev 2.01993
ARJ
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
92658357003
MW-2
EPA 200.8 Rev 5.4 1994
CRW, KRL
6
PASI-A
SM 4500-H+B-2011
SMS
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
4
PASI-A
EPA350.1 Rev 2.01993
ARJ
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
SM 4500-P E-2011
J131
1
PASI-A
92658357004
MW-3
EPA 200.8 Rev 5.4 1994
CRW, KRL
6
PASI-A
SM 4500-H+B-2011
SMS
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
4
PASI-A
EPA350.1 Rev 2.0 1993
ARJ
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
PASI-A = Pace Analytical Services -Asheville
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 22

8G6A /aijit a1
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i
f
Project: MONITORING WELLS
Pace Project No.: 92658357
Sample: MW-1R
Parameters
200.8 MET ICPMS
Barium
Boron
Cadmium
Cobalt
Iron
Manganese
4500H+ pH, Electrometric
pH at 25 Degrees C
300.0 IC Anions 28 Days
Bromide
Chloride
Fluoride
Sulfate
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
Nitrogen, Nitrite
SM4500P-E, Phosphate, Ortho
Orthophosphate as P
Date: 04/03/2023 02:58 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Lab ID: 92658357001 Collected: 03/22/23 11:25 Received: 03/22/23 16:51 Matrix: Water
Results
Units
PQL
MDL
DF
Prepared
Analyzed
CAS No.
Analytical
Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994
Pace Analytical Services -Asheville
33.9
ug/L
1.0
0.21
1
03129/2311:14
04/02/2316:56
7440-39-3
ND
ug/L
50.0
8.5
1
03/29/23 11:14
04/02/2316:56
7440-42-8
ND
ug/L
0.20
0.060
1
03/29/23 11:14
03/30/23 02:56
7440-43-9
0.11J
ug/L
1.0
0.050
1
03/29/23 11:14
03/30/23 02:56
7440-48-4
76.1
ug/L
50.0
20.9
1
03/29/23 11:14
03/30/23 02:56
7439-89-0
12.8
ug/L
2.0
1.0
1
03/29/23 11:14
03/30/23 02:56
7439-96-5
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services -Asheville
6.4 Std. Units 0.10 0.10 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Qual
03/29/23 17:49 H3
ND mg/L 0.10
0.060
1
03/23/23 21:04
24959-67-9
ND mg/L 1.0
0.60
1
03/23/23 21:04
16887-00-6
ND mg/L 0.10
0.050
1
03/23/23 21:04
16984-48-8
ND mg/L 1.0
0.50
1
03/23/23 21:04
14808-79-8
Analytical Method: EPA 350.1 Rev 2.0
1993
Pace Analytical Services -Asheville
ND mg/L 0.10
0.031
1
03/31/2311:41
7664-41-7
Analytical Method: EPA 351.2 Rev 2.0
1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services -Asheville
ND mg/L 0.50
0.25
1
03/29/23 15:29 03/30/23 05:57
7727-37-9
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
0.072 mg/L 0.040
0.010
1
03/23/23 02:09
14797-55-8
ND mg/L 0.040
0.031
1
03/23/23 02:09
14797-65-0
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
0.0181 mg/L 0.050 0.012 1 03/23/23 03:11
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
F6
Page 5 of 22

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www:Puslabs m
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Project: MONITORING WELLS
Pace Project No.: 92658357
Sample: MW-2
Parameters
200.8 MET ICPMS
Barium
Boron
Cadmium
Cobalt
Iron
Manganese
4500H+ pH, Electrometric
pH at 25 Degrees C
300.0 IC Anions 28 Days
Bromide
Chloride
Fluoride
Sulfate
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
Nitrogen, Nitrite
SM4500P-E, Phosphate, Ortho
Orthophosphate as P
Date: 04/03/2023 02:58 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Lab ID: 92658357003 Collected: 03/22/23 13:35 Received: 03/22/23 16:51 Matrix: Water
Results
Units
PQL
MDL
DF
Prepared
Analyzed
CAS No. Qual
Analytical
Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994
Pace Analytical Services - Asheville
60.2
ug/L
1.0
0.21
1
03129/2311:14
04/02/2317:03
7440-39-3
45.0.11
ug/L
50.0
8.5
1
03/29/23 11:14
04/02/2317:03
7440-42-8
ND
ug/L
0.20
0.060
1
03/29/23 11:14
03/30/23 03:03
7440-43-9
1.1
ug/L
1.0
0.050
1
03/29/23 11:14
03/30/23 03:03
7440-48-4
50400
ug/L
1000
419
20
03/29/23 11:14
04/02/2319:43
7439-8M
1310
ug/L
40.0
20.4
20
03129/2311:14
04102/2319:43
7439-96-5
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services -Asheville
6.7 Std. Units 0.10 0.10 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
0.11 mg/L 0.10
0.060 1
1.4 mg/L 1.0
0.60 1
0.094J mg/L 0.10
0.050 1
ND mg/L 1.0
0.50 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
03/29/23 17:57
03/23/23 21:35 24959-67-9
03/23/23 21:35 16887-00-6
03/23/23 21:35 16984-48-8
03/23/23 21:35 14808-79-8
5.9 mg/L 0.10 0.031
1
03/31/2311:44 7664-41-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation
Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services -Asheville
6.6 mg/L 0.50 0.25
1
03/29/23 15:29 03/30/23 05:59 7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
ND mg/L 0.040 0.010
1
03/23/23 02:14 14797-55-8
0.069 mg/L 0.040 0.031
1
03/23/23 02:14 14797-65-0
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
ND mg/L 0.050 0.012 1 03/23/23 03:12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
H3
F6
Page 7 of 22

VirAnalXic l
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7.
f-
ANALYTICAL RESULTS
Project: MONITORING WELLS
Pace Project No.: 92658357
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-3 Lab ID: 92658357004 Collected: 03/22/23 14:55 Received: 03/22/23 16:51 Matrix: Water
Parameters
Results
Units
PQL
MDL
DF
Prepared
Analyzed
CAS No. Qual
200.8 MET ICPMS
Analytical
Method: EPA 200.8 Rev 5.4
1994 Preparation Method: EPA 200.8 Rev 5.4 1994
Pace Analytical Services -Asheville
Barium
320
ug/L
5.0
1.1
5
03/29/23 11:14
03/30/2314:05
7440-39-3
Boron
ND
ug/L
50.0
8.5
1
03/29/23 11:14
04/02/23 17:07
7440- 42-8
Cadmium
0.60
ug/L
0.20
0.060
1
03129/2311:14
03/30/23 03:07
7440-43-9
Cobalt
2.2
ug/L
1.0
0.050
1
03/29/23 11:14
03/30/23 03:07
744014814
Iron
123
ug/L
50.0 '
20.9
1
03/29/23 11:14
03/30/23 03:07
7439-89-6
Manganese
70.6
ug/L
2.0
1.0
1
03/29/23 11:14
03/30/23 03:07
7439-96-5
4500H+ pH, Electrometric
pH at 25 Degrees C
300.0 IC Anions 28 Days
Bromide
Chloride
Fluoride
Sulfate
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
Nitrogen, Nitrite
SM4500P-E, Phosphate, Ortho
Orthophosphate as P
Date: 04/03/2023 02:58 PM
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services -Asheville
5.6 Std. Units 0.10 0.10 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
0.11 mg/L 0.10 0.060 1
8.4 mg/L 1.0 0.60 1
ND mg/L 0.10 0.050 1
ND mg/L 1.0 0.50 1
03/29/23 15:04
03/23/23 21:51 24959-67-9
03/23/23 21:51 16887-00-6
03/23/23 21:51 16984-48-8
03/23/23 21:51 14808-79-8
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
ND mg/L 0.1,0 0.031 1 03131/2312:17 766441-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services -Asheville
ND mg/L 0.50 0.25 1 03/29/23 15:29 03/30/23 06:00 7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
7.4 mg/L 0.20 0.050 5
ND mg/L 0.040 0.031 1
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
0.012J mg/L 0.050 0.012 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
03/23/23 02:23 14797-55-8
03/23/23 02:15 14797-65-0
03/23/23 03:13
H3
F6
Page 8 of 22

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ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: MONITORING WELLS
Pace Project No.: 92658357
Sample: MW-4
Lab ID: 92658357002 Collected: 03/22/23 12:35 Received: 03/22/23 16:51 Matrix: Water
Parameters
Results Units PQL MDL DF Prepared
Analyzed
CAS No. Qual
200.8 MET ICPMS
Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994
Pace Analytical Services -Asheville
Barium
93.9 ug/L 1.0 0.21 1 03/29/23 11:14
04/02/2317:00
7440-39-3
Boron
ND ug/L 50.0 8.5 1 03129/2311:14
04/02/2317:00
7440-42-8
Cadmium
0.13.1 ug/L 0.20 0.060 1 03/29/23 11:14
03/30/23 03:00
7440-43-9
Cobalt
3.3 ug/L 1.0 0.050 1 03/29/23 11:14
03/30/23 03:00
7440-48-4
Iron
122 ug/L 50.0 20.9 1 03/29/23 11:14
03/30/23 03:00
7439-89-6
Manganese
126 ug/L 2.0 1.0 1 03/29/23 11:14
03/30/23 03:00
7439-06-5
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services -Asheville
pH at 25 Degrees C
5.6 Std. Units 0.10 0.10 1
03/29/23 17:53
H3
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Bromide
0.19 mg/L 0.10 0.060 1
03/23/23 21:20
24959-67-9
Chloride
2.3 mg/L 1.0 0.60 1
03/23/23 21:20
16887-00-6
Fluoride
ND mg/L 0.10 0.050 1
03/23/23 21:20
16984-48-8
Sulfate
ND mg/L 1.0 0.50 1
03/23/23 21:20
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/L 0.10 0.031 1
03/31/23 11:43
766441-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Kjeldahl, Total
ND mg/L 0.50 0.25 1 03/29/23 15:29
03/30/23 05:58
7727-37-9
353.2 Nitrogen, NO2IN03 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
2.7 mg/L 0.040 0.010 1
03/23/23 02:12
14797-55-8
Nitrogen, Nitrite
ND mg/L 0.040 0.031 1
03/23/23 02:12
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.014.1 mg/L 0.050 0.012 1
03/23/23 03:12
F6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/03/2023 02:58 PM
without the written consent of Pace Analytical Services, LLC.
Page 6 of 22

acoAnalytical
1gWIN:BbS.0018
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: MONITORING WELLS
Pace Project No.: 92658357
QC Batch: 764491
Analysis Method: EPA 200.8 Rev 5.4 1994
QC Batch Method: EPA 200.8 Rev 5.4
1994
Analysis Description: 200.8 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92658357001, 92658357002, 92658357003, 92658357004
METHOD BLANK: 3969830
Matrix: Water
Associated Lab Samples: 92658357001, 92658357002, 92658357003, 92658357004
Blank Reporting
Parameter
Units
Result Limit MDL Analyzed Qualifiers
Barium
ug/L
ND 1.0 0.21 03/30/2313:45
Boron
ug/L
ND 50.0 8.5 04/02/2316:48
Cadmium
ug/L
ND 0.20 0.060 03/30/23 02:29
Cobalt
ug/L
ND 1.0 0.050 03/30/23 02:29
Iron
ug/L
ND 50.0 20.9 03/30/23 02:29
Manganese
ug/L
ND 2.0 1.0 03/30/23 02:29
LABORATORY CONTROL SAMPLE:
3969831
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Barium
ug/L
50 46.8 94 85-115
Boron
ug/L
50 51.3 103 85-115
Cadmium
ug/L
50 54.4 109 85-115
Cobalt
ug/L
50 55.1 110 85-115
Iron
ug/L
1250 1330 107 85-115
Manganese
ug/L
50 51.2 102 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3969832 3969833
MS MSD
92658283001
Spike Spike MS MSD MS MSD % Rec
Max
Parameter Units
Result
Conc. Conc. Result Result % Rec % Rec Limits
RPD RPD Qua[
Barium ug/L
17.4
50 50 71.2 71.9 108 109 70-130
1 20
Boron ug/L
ND
50 50 147J 140J 103 87 70-130
20 CL
Cadmium ug/L
ND
50 50 53.5 52.6 107 105 70-130
2 20
Cobalt ug/L
ND
50 50 55.4 53.8 110 107 70-130
3 20
Iron ug/L
692
1250 1250 2020 1960 106 101 70-130
3 20
Manganese ug/L
44.6
50 50 95.2 93.5 101 98 70-130
2 20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3969834 3969835
MS MSD
92658687001
Spike Spike MS MSD MS MSD % Rec
Max
Parameter Units
Result
Conc. Conc. Result Result % Rec % Rec Limits
RPD RPD Qual
Barium ug/L
20.2
50 50 74.7 74.8 109 109 70-130
0 20
Boron ug/L
839
50 50 913 918 147 158 70-130
1 20 CL,E,
M1
Cadmium ug/L
ND
50 50 54.0 52.1 108 104 70-130
4 20
Results presented on this page are in the units
indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/03/2023 02:58 PM
without the written consent of Pace Analytical Services, LLC.
Page 9 of 22

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QUALITY CONTROL DATA
Project: MONITORING WELLS
Pace Project No.: 92658357
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3969834
MS
92658687001 Spike
Parameter Units Result Conc.
Cobalt ug/L 5.5 50
Iron ug/L 145 1250
Manganese ug/L 24.5 50
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
3969835
MSD
Spike
MS
MSD
MS
MSD
% Rec
Max
Conc.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qual
50
61.6
60.0
112
109
70-130
3 20
1250
1500
1500
108
108
70-130
0 20
50
76.9
76.2
105
104
70-130
1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/03/2023 02:58 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 22

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I,AaceAnalXical
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QUALITY CONTROL DATA
Project: MONITORING WELLS
Pace Project No.: 92658357
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QC Batch: 764543 Analysis Method: SM 4500-H+B-2011
QC Batch Method: SM 4500-H+B-2011 Analysis Description: 4500H+B pH
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92658357001, 92658357002, 92658357003, 92658357004
SAMPLE DUPLICATE: 3969975
92658850001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
pH at 25 Degrees C Std. Units 8.4 8.4 0 10 H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/03/2023 02:58 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 22

Aar 1:
8iceAna1Xica10
wtvetptuxiabscals
;
QUALITY CONTROL DATA
Project: MONITORING WELLS
Pace Project No.: 92658357
QC Batch: 763179 Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92658357001, 92658357002, 92658357003, 92658357004
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
METHOD BLANK: 3963599
Matrix: Water
Associated Lab Samples:
92658357001, 92658357002, 92658357003, 92658357004
Blank Reporting
Parameter
Units
Result Limit
MDL
Analyzed Qualifiers
Bromide
mg/L
ND 0.10
0.060
03/23/2314:20
Chloride
mg/L
ND 1.0
0.60
03/23/2314:20
Fluoride
mg/L
ND 0.10
0.050
03/23/2314:20
Sulfate
mg/L
ND 1.0
0.50
03/23/2314:20
LABORATORY CONTROL SAMPLE:
3963600
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
% Rec
Limits Qualifiers
Bromide
mg/L
2.5
2.5
102
90-110
Chloride
mg/L
50
51.1
102
90-110
Fluoride
mg/L
2.5
2.6
106
90-110
Sulfate
mg/L
50
51.9
104
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3963601
3963602
MS
MSD
92658356012
Spike
Spike
MS
MSD
MS MSD
% Rec
Max
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec % Rec
Limits
RPD
RPD Qual
Bromide
mg/L
0.16
2.5
2.5
2.7
2.6
100 99
90-110
1
10
Chloride
mg/L
13.7
50
50
63.9
64.0
100 100
90-110
0
10
Fluoride
mg/L
0.12
2.5
2.5
3.1
3.1
118 117
90-110
0
10 M1
Sulfate
mg/L
ND
50
50
52.3
52.2
104 104
90-110
0
10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3963603
3963604
MS
MSD
92658347007
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Bromide
mg/L
0.092J
2.5
2.5
2.5
2.5
95
96
90-110
0
10
Chloride
mg/L
8.4
50
50
56.3
57.1
96
97
90-110
1
10
Fluoride
mg/L
0.065J
2.5
2.5
2.7
2.7
104
104
90-110
1
10
Sulfate
mg/L
1.7
50
50
50.0
50.7
97
98
90-110
1
10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/03/2023 02:58 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 22

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QUALITY CONTROL DATA
Project: MONITORING WELLS
Pace Project No.: 92658357
QC Batch: 764779 Analysis Method: EPA 350.1 Rev 2.0 1993
QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92658357001, 92658357002, 92658357003
METHOD BLANK: 3971179 Matrix: Water
Associated Lab Samples: 92658357001, 92658357002, 92658357003
Blank Reporting
Parameter Units Result Limit
Nitrogen, Ammonia mg/L ND 0.10
LABORATORY CONTROL SAMPLE: 3971180
Spike LCS
Parameter Units Conc. Result
Nitrogen, Ammonia mg/L 5 5.0
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
MDL Analyzed Qualifiers
0.031 03/31 /23 11:02
LCS % Rec
% Rec Limits Qualifiers
100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3971181 3971182
MS MSD
92659234002 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Nitrogen, Ammonia mg/L 1290 5 5 1320 1320 516 466 90-110 0 10 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3971183 3971184
MS MSD
92659234004 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Nitrogen, Ammonia mg/L 2180 5 5 2270 2260 1640 1620 90-110 0 10 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/03/2023 02:58 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 22

aceAnalj6cal
.• W9VM:iI�S.0016
1:
QUALITY CONTROL DATA
Project: MONITORING WELLS
Pace Project No.: 92658357
QC Batch: 765095 Analysis Method: EPA 350.1 Rev 2.0 1993
QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92658357004
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
METHOD BLANK: 3972752 Matrix: Water
Associated Lab Samples: 92658357004
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Nitrogen, Ammonia mg/L ND 0.10 0.031 03/31/23 12:02
LABORATORY CONTROL SAMPLE: 3972753
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Ammonia mg/L 5 5.0 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3972754 3972755
MS MSD
92659558001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Nitrogen, Ammonia mg/L 1.4 5 5 6.6 6.6 103 103 90-110 0 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3972756 3972757
MS MSD
92659558002 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Nitrogen, Ammonia mg/L 2.0 5 5 6.9 7.0 99 100 90-110 0 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/03/2023 02:58 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 22

aceAnalytical*
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t
QUALITY CONTROL DATA
Project: MONITORING WELLS
Pace Project No.: 92658357
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QC Batch: 764579 Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92658357001, 92658357002, 92658357003, 92658357004
METHOD BLANK: 3970097 Matrix: Water
Associated Lab Samples: 92658357001, 92658357002, 92658357003, 92658357004
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg/L ND 0.50 0.25 03/30/23 05:27
LABORATORY CONTROL SAMPLE: 3970098
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total mg/L 10 9.6 96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3970099 3970100
MS MSD
92658177001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Nitrogen, Kjeldahl, Total mg/L 1.3 10 10 11 A 11.6 101 103 90-110 2 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3970101 3970102
MS MSD
92658177002 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Nitrogen, Kjeldahl, Total mg/L 1.0 10 10 10.2 11.0 91 100 90-110 8 10
Results presented on this page are in the units indicated by the "Units" column except where an altemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/03/2023 02:58 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 22

accAnalyiical
wwlr.pewahs"M
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f
QUALITY CONTROL DATA
Project: MONITORING WELLS
Pace Project No.: 92658357
QC Batch: 763142 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92658357001, 92658357002, 92658357003, 92658357004
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
METHOD BLANK: 3963513 Matrix: Water
Associated Lab Samples: 92658357001, 92658357002, 92658357003, 92658357004
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Nitrogen, Nitrate mg/L ND 0.040 0.010 03/23/23 02:02
Nitrogen, Nitrite mg/L ND 0.040 0.031 03/23/23 02:02
LABORATORY CONTROL SAMPLE: 3963514
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/L 1.5 1.5 101 90-110
Nitrogen, Nitrite mg/L 1 1.0 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3963515
3963516
MS
MSD
92658196002 Spike
Spike
MS MSD MS
MSD
% Rec
Max
Parameter
Units
Result Conc.
Conc.
Result Result % Rec
% Rec
Limits
RPD RPD Qual
Nitrogen, Nitrate
mg/L
0.15 1.5
1.5
1.7 1.7 105
104
90-110
1 10
Nitrogen, Nitrite
mg/L
ND 1
1
1.1 1.1 106
105
90-110
1 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/03/2023 02:58 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 22

Air N
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: MONITORING WELLS
Pace Project No.: 92658357
QC Batch: 763152
Analysis Method:
SM 4500-P E-2011
QC Batch Method: SM 4500-P E-2011
Analysis Description:
SM450OP-E Phosphorus, Ortho
Laboratory:
Pace Analytical Services -Asheville
Associated Lab Samples: 92658357001, 92658357002, 92658357003, 92658357004
METHOD BLANK: 3963548
Matrix: Water
Associated Lab Samples: 92658357001, 92658357002, 92658357003, 92658357004
Blank Reporting
Parameter Units
Result Limit
IV1DL Analyzed Qualifiers
Orthophosphate as P mg/L
ND 0.050 0.012 03/23/23 03:06
LABORATORY CONTROL SAMPLE: 3963549
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Orthophosphate as P mg/L
0.25 0.24
98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3963550 3963551
MS MSD
92658179001
Spike Spike MS
MSD MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD RPD Qual
Orthophosphate as P mg/L 0.066
0.25 0.25 0.32
0.33 101 107 90-110 5 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/03/2023 02:58 PM without the written consent of Pace Analytical Services, LLC.
Page 17 of 22

accAnalyiical�
wwrt:pa�absto�s
f
f:
QUALIFIERS
Project: MONITORING WELLS
Pace Project No.: 92658357
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
CL The continuing calibration for this compound is outside of Pace Analytical acceptance limits. The results may be biased
low.
E Analyte concentration exceeded the calibration range. The reported result is estimated.
F6 Sample was not filtered within 15 minutes of collection and does not meet sampling and/or regulatory requirements.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/03/2023 02:58 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 22

w aiceAraJyiicaf
wwq:pa�eia6scom
f
f
QUALIFIERS
Project: MONITORING WELLS
Pace Project No.: 92658357
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
'Total' may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
CL The continuing calibration for this compound is outside of Pace Analytical acceptance limits. The results may be biased
low.
E Analyte concentration exceeded the calibration range. The reported result is estimated.
F6 Sample was not filtered within 15 minutes of collection and does not meet sampling and/or regulatory requirements.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/03/2023 02:58 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 22

Air 0
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: MONITORING WELLS
Pace Project No.: 92658357
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92658357001
MW-1 R
EPA 200.8 Rev 5.4 1994
764491
EPA 200.8 Rev 5.4 1994 764624
92658357002
MWA
EPA 200.8 Rev 5.4 1994
764491
EPA 200.8 Rev 5.4 1994 764624
92658357003
MW-2
EPA 200.8 Rev 5.4 1994
764491
EPA 200.8 Rev 5.4 1994 764624
92658357004
MW3
EPA 200.8 Rev 5.4 1994
764491
EPA 200.8 Rev 5.4 1994 764624
92658357001
MW-1R
SM 4500-H+B-2011
764543
92658357002
MW-4
SM 4500-H+6-2011
764543
92658357003
MW-2
SM 4500-H+B-2011
764543
92658357004
MW3
SM 4500-H+B-2011
764543
92658357001
MWA R
EPA 300.0 Rev 2.1 1993
763179
92658357002
MW-4
EPA 300.0 Rev 2.1 1993
763179
92658357003
MW-2
EPA 300.0 Rev 2.1 1993
763179
92658357004
MW3
EPA 300.0 Rev 2.1 1993
763179
92658357001
MW-1 R
EPA 350.1 Rev 2.0 1993
764779
92658357002
MW-4
EPA 350.1 Rev 2.0 1993
764779
92658357003
MW-2
EPA 350.1 Rev 2.0 1993
764779
92658357004
MW3
EPA 350.1 Rev 2.0 1993
765095
92658357001
MWAR
EPA 351.2 Rev 2.0 1993
764579
EPA 351.2 Rev 2.0 1993 764762
92658357002
MWA
EPA 351.2 Rev 2.0 1993
764579
EPA 351.2 Rev 2.0 1993 764762
92658357003
MW-2
EPA 351.2 Rev 2.0 1993
764579
EPA 351.2 Rev 2.0 1993 764762
92658357004
MW3
EPA 351.2 Rev 2.0 1993
764579
EPA 351.2 Rev 2.0 1993 764762
92658357001
MW-1 R
EPA 353.2 Rev 2.0 1993
763142
92658357002
MWA
EPA 353.2 Rev 2.0 1993
763142
92658357003
MW-2
EPA 353.2 Rev 2.0 1993
763142
92658357004
MW3
EPA 353.2 Rev 2.0 1993
763142
92658357001
MW-1R
SM 4500-P E-2011
763152
92658357002
MW-4
SM 4500-P E-2011
763152
92658357003
MW-2
SM 4500-P E-2011
763152
92658357004
MW3
SM 4500-P E-2011
763152
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/03/2023 02:58 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 22

p C." 04.4' U lot
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Page 20 of 22

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Page 21 of 22

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TEMP in C
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SAMPLE TYPE (13-GRAB C=COMP)
Q.
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SAMPLE TEMP AT COLLECTION
# OF CONTAINERS
Unpreserved
H2SO4
HNO3 1
NCI
NaOH
Na2S203
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99
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Ammonia, TKN
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pl I by 450oH+
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Page 22 of 22

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Date Collect: j2 3 Tngea1leeEed t 2 3 '5
Sam'Equiprnent'Used- strument IL). y5t D -Loq ITO 15,61P
Rofac-Type Preservation. Analysi&.Requirect
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Belt. Mea6urementgObIffyations
Sample Temp (!C):: 11-1 5 T-4rWcu ty (ptu).• 0.11 Time., 1 2
lass OXY-
Time: Fe 2+.m
g/ Tim
--
Specific con& (us): 5-1. 1 Time. 113 5
Res. Cl (nig/t
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le siu
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Time.
General/Weathvr Obsewation4.L...
Sampler .
Signature.
Stabilization Test
qtWy) Texnp__c�S wuntj 3 —(mph)
-3112-12,3
Spec,
V.QIUML
Time
Purged
Temp;
Din Oxy.
Cond.:
pH (8,U)
ReDox
Turbidity
removed
Water
-level
Other
(mg/L)
(US)
(inV)
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(gallons/#01 I
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SAMPLE TEMP AT COLLECTION
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w
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m
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300.0
353.2
a
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e
pH by 4500H-
N
r�
W
w
v
TEMP in C
Residual Chlorine (Y/N)
y
A
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Ice
(YlN)
us o y
Sealed
Cooler
YIN
)
Samples
Intact
(YIN)
a
.
3 Y
D
J
Cb