WQ0013419_Sludge Landfill Monitoring Report November 2022_20230327

Laverty, Brett
From: Cody, David M. <[e-mail]>
Sent: Monday, March 27, 2023 6:24 PM
To: Davidson, Landon; Laverty, Brett
Cc: Urey, Jill L.
Subject: [External] Nov 2022 Sludge Landfill Environmental Monitoring Report Facility Permit # WQ001319
Attachments: 2022 Nov Sludge Landfill Detects vs 2L Std.pdf; 2022 Nov Sludge Landfill 92634407_EQUIS.zip; 2022
Nov Pace Sludge Landfill Report 92634407_frc.pdf
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Emailed To:
Landon Davidson
Regional Supervisor - Water Resources
Water Quality Regional Operations
2090 U.S. 70 Highway
Swannanoa, NC 28778-8211
828-296-4690
[e-mail]
Email From:
David M. Cody
DMC Remediation & Laboratory Consulting LLC
214 Camelot Dr.
Clyde, NC 28721
828-246-1388
[e-mail]
Email Is Sent For:
Jill L. Urey
Vice President
Deputy General Counsel & Corporate Secretary
Glatfelter
Capitol Towers South
4350 Congress Street
Suite 600
Charlotte, NC 28209
717-225-2048
[e-mail]
Submittal of:
The Sludge Landfill Environmental Monitoring Report Facility Permit # WQ001319 located on 1Ecusta Road Pisgah
Forest, NC 28768.
Attached to this Email are Three (3) Attachments;
1. 2022 Nov Sludge Landfill Detects vs 2L Std
2. 2022 Nov Sludge Landfill 92634407_EQUIS
3. 2022 Nov Sludge Landfill Pace Well Testing Report 92634407_frc
1

Please REPLY TO THIS EMAIL as VERIFICATION OF SUBMITAL.
D. Mike Cody
Glatfelter Contract Consultant
214 Camelot Drive
Clyde, NC 28721
Mobile [phone]
David.Cody(�alatfelter.com
www.glatfelter.com
b", G L A T F E L T E R
Beyond Paper...
is everything we do above and beyond making great paper— that makes us unique.
Our Safety Mission: Injury Free Every Day.
NOTICE: This message, and anything transmitted with it, may be confidential and is solely for the intended recipient(s). If
you are not the intended recipient or have received this message in error, (1) immediately notify the sender, (2)
permanently delete this message from your system, and (3) do not use, disclose, forward, print or copy the information
contained in this message or any attachments. Glatfelter does not accept liability for any damage caused by the
transmission of this message. Please see the following link for Glatfelter's Privacy Notice for Business Partners.
N

Sludge Landfill
QO6V09 Monitoring Well - Located on west side of Sludge Landfill dam
2L
Date Sam Is Collected
Standard
07/06/10
11/08/10
07/19/11
11/15/11
07/10/12
11/06/12
07/02/13
11/19/13
07/10/14
11/12/14
07/30/15
11/06/15
07/12/16
11/08/16
07/11/17
11/07/17
07/10/18
11/16/18
07/09/19
11/08/20
07/07/20
11/17/20
07/13/21
11/02/21
07/19/22
11/03/22
Field pH
6.5 to 8.5
6.35
6.43
6.3
6.3
6.6
6.2
6.4
6.4
6.0
6.4
6.2
6.2
6.5
6.7
6.1
6.4
6.3
6.4
6.4
6.5
6.4
6.5
6.3
6.5
6.4
6.3
Field Temperature de C
NE
17.62
16.55
17.15
15.56
19.7
13.72
17.23
15.95
16.80
17.0
19.2
19.5
26.7
15.2
18.6
16.5
18.1
17.2
19.9
16.7
17.4
16.8
18.0
14.9
22.1
15.9
Static Water Level feet
NE
29.76
30.92
30.06
31.58
30.75
31.22
29.38
30.61
29.78
30.46
30.25
29.43
30.00
31.25
29.31
29.75
28.86
27.83
27.94
29.10
28.04
27.64
28.55
29.68
28.21
29.51
Field Specific Conductance umhos/cm
NE
1436
1436
1470
1427
1406
1497
1476
1487
1445
1466
1444
1377
1486
1441
1410
1402
1438
1163
1374
1347
1423
1382
1450
1331
1358
1398
TurbidityNTU
Substance Detects Only)
NE
9.88
2.95
30
3.67
14.8
9.00
3.41
2.42
3.11
3.14
1.60
9.26
19.50
21.43
12.58
4.03
10.65
3.10
7.70
16.80
11.72
13.29
4.84
22.10
15.00
15.85
Antimony1
ND
ND
ND
ND
ND
ND
ND
ND
ND
4.1 J
5.6
5.4
6.8
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
3.0 J
ND
6.0 J
Arsenic
10
6.5
ND
ND
ND
ND
ND
6.3 J
ND
ND
ND
ND
ND
ND
3.1 J
ND
5.6 J
ND
ND
ND
ND
ND
ND
ND
5.3 J
ND
6.7 J
Barium
700
331
290
306
272
304
288
309
316
296
297
301
317
283
301
303
315
280
302
296
288
290
328
285
304
266
294
Cadmium
2
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
.591
ND
ND
ND
ND
Calcium
NE
189000
167000
161000
207000
149000
185000
183000
200000
183000
181000
160000
179000
184000
158000
178000
120000
163000
179000
160000
164000
175000
189000
168000
161000
168000
171000
Chromium
10
ND
ND
ND
ND
ND
ND
ND
ND
5.2
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Cobalt
1
15.7
14.5
19.2
14.6
15.0
11.9
25.2
17.2
13.3
14.0
13.3
13.3
16.1
13.4
11.7
10.5
12.4
11.9
11.7
13.1
10.1
10.5
10.2
11.9
18.0
13.2
Copper m /I
1
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0034 J
0.0044 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
Lead
15
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
7.4
ND
ND
ND
ND
ND
3.5 J
ND
ND
ND
ND
ND
ND
ND
Magnesium
NE
85100
77500
81300
78800
79800
82500
84800
83300
79300
83900
84000
82300
77200
80200
81900
82000
80600
82000
80500
81500
80800
87100
80300
82900
79800
78800
Mercury
1
0.000623
0.000629
0.000561
0.00228
0.000799
0.000763
ND
0.000551
ND
ND
0.001190
0.000937 B
0.000421 J
0.000453 J
0.000557
0.000522
0.000612
ND
0.006830
ND
0.000334 J
0.000612
0.000573
ND
0.005080
ND
Nickel
100
12.3
10.4
18.2
16.8
18.2
16.1
18.1
15.9
19.2
19.3
17.9
18.0
20.3
16.5
16.2
16.0
15.1
14.7
14.0
15.2
13.8
17.4
14.2
16.9
12.2
17.0
Potassium
NE
7340
6520
7310
7980
7310
6810
7040
7460
6500
5000 J
4730 J
5200
5200
4730 J
4970 J
5050
5350
4910 J
4930 J
5140
4780 J
ND
4760 J
4880 J
4760 J
4570 J
Selenium
20
ND
ND
ND
ND
ND
ND
ND
ND
18.5
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Sodium
NE
29200
28400
30400
34200
31600
33500
34500
36300
34800
28000
27500
28600
29600
28000
29600
29300
28900
30900
30800
31900
30800
34000
31100
33900
31600
30000
Vanadium
NE
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
5.5
8.9
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
43.1
ND
ND
Zinc m /L
1
ND
ND
ND
ND
ND
ND
ND
ND
0.0108
ND
0.0093 J
0.0092 J
0.0149
ND
ND
ND
0.0143 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
1,4 Dichlorbenzene
6
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2.8 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
Acetone m /L
6
ND
ND
0.0054 J
ND
0.0023 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Benzene
1
ND
ND
0.26 J
ND
ND
0.27 J
0.27 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Alkalinity, Total as CaCO3 m /L
NE
872
385
879
829
788
779
873
815
811
790
767
776
842
812
806
860
772
946
837
787
802
842
829
745
756
828
Total Dissolved Solids m /L
500
888
834
836
878
857
858
892
892
871
874
851
110
869
836
835
690
852
814
802
778
828
846
824
780
804
780
Sulfate m /L
250
6.1
ND
5.7
5.9
6.7
6.7
6.0
5.0
5.4
5.1
5.3
5.1
4.7
4.6
3.2
3.5
3.5
3.3
3.6
2.8
3.8
3.2
3.5
2.5
3.1
2.6
Chloride m /L
250
52.6
51.4
53.8
59.7
57.5
56.9
46.4
56.5
54.4
54.9
53.8
57.3
57.6
57.8
64.3
52.2
52
56.6
51.8
52.5
50.9
50.2
48.1
48.4
51.1
47.8
Total Organic Carbon m /L
NE
26.4
29.9
25.5
23.5
21.1
29.2
30.5
33.8
13.6
7.8
6.7
4.7
4.7
4.1
4.5
3.9
5.6
5.4
9.1
8.7
4.6
4.4
4.2
4.5
4.0
4.1
0
All concentrations are in micrograms per liter (ug/L) unless otherwise noted.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
NA - Not Applicable
ND - Not Detected
NE - Not Established
B - Analyyte was dected in the assoicated method blank
1 of 5

Sludge Landfill
Q06V10 Monitoring Well - Located on former Temporary Sludge Landfill dam
Date SamDle Collected
Field D
Standard 07/06/10
11/08/10
01/19/11
11/15/11
07/10/12
11/06/12
07/02/13
11/19/13
07/10/14 11/12/14
07/30/15
11/06/15
07/12/16
11/08/16
07/11/17
11/07/17
07/10/18
11/16/18
07/09/19
11/08/19
07/07/20
11/17/20
07/13/21
11/OZ/21r
/22
Field pH
6.5 to 8.5
6.20
5.58
5.7
5.3
5.9
5.3
5.4
4.7
5.9
5.8
6.6
6.8
5.7
6.8
6.3
5.9
6.0
6.2
7.8
5.4
5.5
5.8
6.0
5.4
Field Temperature de C
NE
14.15
15.13
17.68
15.38
17.2
13.57
14.82
14.74
14.20
15.7
15.7
16.7
22.3
14.8
18.3
15.5
16.1
14.3
16.4
13.2
15.4
14.4
15.3
13.9
Static Water Level feet
NE
27.68
27.54
27.69
28.15
28.03
27.78
26.98
27.94
27.25
27.63
28.11
24.23
28.34
28.52
27.54
25.74
27.17
20.38
27.30
26.02
27.33
25.00
27.97
27.Field
S ecific Conductance umhos/cm
NE
33
41
60
41
39
30
22
30
17
30.0
39.0
24.0
42.2
42.0
35.0
29.4
22.0
25.6
82.0
24.8
22.0
18.5
290333
Turbidit NTU
Substance Detects O
NE
93.5
81.3
14
3.33
30
5.58
0.70
1.47
4.05
2.03
4.54
19.57
46.40
18.52
20.27
2.67
4.17
68.40
5.20
1.40
1.93
83.78
6.85
6.00
Arsenic
10
ND
6.0
ND
ND
ND
ND
ND
ND
7.2 J
ND
ND
ND
4.7 J
4.6 J
ND
ND
ND
ND
14.3
ND
ND
ND
ND
ND
6.2 J
ND
Barium
700
7.4
24.4
8.0
8.8
7.9
7.8
5.6
6.0
8.1
5.1
5.9
11.9
17.0
11.1
9.0 B
7.4
10.3
11.1
41.6
6.2
7.1
17.4
4.7 J
5.7
22.2
6.3 J
Calcium
NE
2820
2690
3200
3080
2860
2730
1400
2210
1250
2350
2670
1220
2430
2200
2300
1250
1290
1930
1380
1130
1140
956
1980
2220
2310
2770
Lead
15
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2.6 J
Chromium
10
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
5.8
ND
ND
ND
ND
828
4.1 J
ND
Cobalt
1
ND
7.6
ND
ND
ND
ND
ND
ND
ND
ND
ND
2.7 J
5.5
ND
ND
ND
ND
ND
10.1
ND
ND
5.0 J
ND
ND
6.1
ND
Copper
1000
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2.6 J
4.4 J
ND
ND
ND
ND
ND
12.6
ND
ND
4.3 J
ND
ND
5.0 J
ND
Magnesium
NE
842
1110
978
1020
914
944
808
760
788
799
893
832
962
849
938
828
852
627
1250
800
835
1010
718
826
1070
996
Nickel
100
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
10.5
ND
ND
5.7
ND
ND
4.3 J
ND
Potassium
NE
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1710 J
ND
ND
ND
ND
ND
ND
294 J
Sodium
NE
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2880 J
2160 J
1420 J
1340 J
1220 J
1450 J
1340 J
1200 J
1100 J
1670 J
2280 J
1870 J
1980 J
Vanadium
NE
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
7.3
ND
ND
ND
ND
ND
4.2 J
ND
Mercury
1
0.000694
0.0057
0.00302
0.00557
0.0157
0.0243
0.0149
0.00475
0.00312
0.00338
0.01860
0.05270
0.01830 D3
0.09550 D3
0.07700 D31
0.11200 D3
0.01400
0.02190
0.06220
0.00064
0.02400
0.01640
0.00461 J
0.00283
0.01170
ND
Nickel
100
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
4.3 J
ND
ND
ND
ND
ND
ND
ND
ND
5.7
ND
ND
ND
ND
Zinc m /L
1
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0074 J
0.0102
ND
ND
0.0063 J
0.0067 J
ND
0.0248
ND
ND
0.0117
ND
ND
10.1
ND
1,4 Dichlorbenzene
6
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
3.3 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
Acetone m /L
6
ND
ND
0.0043 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
11.6
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Alkalinity, Total as CaCO3 m /L
NE
23.3
22.3
11.5
12.8
646
9.9
6.4
8.8
6.8
9.4
9.6
6.0
10.1
ND
10.9
8.4
7.2
6.5
5.3
ND
ND
ND
ND
12.1
10.1
10.3
Total Dissolved Solids m /L
500
38.8
ND
39.0
88.0
ND
ND
32.0
29.0
ND
28.0
35.0
62.0
40.0
ND
ND
ND
ND
ND
ND
ND
ND
43.0
8.3
ND
ND
33.0
Sulfate m /L
250
ND
ND
ND
ND
2.8
2.3
2.0
2.3
2.2
2.5
2.5
2.3
2.0
2.4
1.1
0.8 J
0.6 J
1.3
0.64 J
0.61 J
0.79 J
ND
0.77 J
0.85 J
1.00
1.00
Chloride m /L
250
ND
ND
ND
ND
1.2
1.7
1.2
1.7
0.90 J
1.0
2.0
3.4
1.4
1.7
1.4
1.2
1.4
1.2
0.8 J
1.0
0.89 J
0.99 J
3.00
2.50
1.40
1.50
Total Organic Carbon m /L
NE
1.4
24.0
2.0
2.7
1.8
2.7
1.4
1.8
3.2
ND
ND
ND
ND
ND
1.0 J
0.5 J
ND
1.2
ND
ND
0.9 J
0.7 J
ND
ND
ND
ND
All concentrations are in micrograms per liter (ug/L) unless otherwise noted.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
NA - Not Applicable
ND - Not Detected
NE - Not Established
D3 - Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
2 of5

Sludge Landfill
Q06V11 Monitoring Well - Located west of former Temporary Sludge Landfill detention basin
Date SamDle Collected
Standard 07/06/10
11/09/10
07/19/11
11/15/11
07/10/12
11/06/12
07/02/13
11/19/13
07/10/14
11/12/14
08/30/15
11/06/15
07/12/16
11/08/16
07/11/17
11/07/17
07/10/18
11/16/18
07/09/19
11/08/19
07/07/20
11/17/20
07/13/21
11/OZ/21
07/19/22
11/03/22
Field pH
6.5 to 8.5
6.29
6.23
5.6
5.4
6.2
5.2
5.4
5.2
5.9
5.9
6.0
6.2
5.8
6.1
5.5
5.8
5.8
6.0
6.2
5.7
5.6
5.8
5.8
Field Temperature de C
NE
15.26
14.09
17.47
14.1
17.3
12.23
17.22
15.16
14.94
14.3
18.0
15.4
28.7
14.9
17.7
14.9
16.3
14.5
15.7
13.1
15.3
14.2
15.3
12.9
19.0
13.8
Static Water Level feet
NE
39.54
40.06
39.03
41.30
40.83
40.31
38.60
40.67
39.03
40.06
40.69
35.43
40.40
41.52
38.33
37.44
37.95
33.86
38.07
38.05
38.52
35.50
30.43
40.01
38.83
40.80
Field Specific Conductance umhos/cm
NE
85
86
88
81
92
82
76
78
79
97.0
96.1
75.0
72.3
83.0
78.0
74.5
64.0
63.9
74.0
63.0
59.2
52.1
66.0
62.5
78.1
68.3
TurbidityNTU
Substance Detects 0
NE
13.1
8.08
18
6.16
3.92
3.25
2.58
1.12
4.72
3.34
9.77
9.02
25.60
18.71
13.10
13.32
7.15
11.60
19.00
9.60
11.59
5.84
8.75
7.00
37.50
10.15
Barium
700
11.1
10.4
9.9
9.6
7.1
9.7
6.4
6.8
5.5
6.0
7.5
6.9
8.9
7.9
8.8 B
16.6
6.0
9.0
10.6
8.3
7.1
6.9
5.7
6.9
8.5
7.1 J
Calcium
NE
5950
5300
5940
6010
5840
6000
5710
5890
5720
6660
5830
6540
4210
7010
6300
6480
4180
5360
4290
4370
3920
4270
4620
4460
4290
4700
Chromium
10
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2.5 J
ND
ND
ND
ND
ND
1.9 J
ND
ND
ND
ND
ND
ND
Cobalt
1
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.1 J
ND
ND
ND
ND
ND
ND
ND
Copper
15
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
5.4
4.0 J
2.8 J
10.6
ND
4.7 J
5.6
2.4 J
ND
ND
ND
ND
6.9
2.7 J
Magnesium
NE
2720
2480
2620
2710
2650
2880
2520
2810
2580
2880
2660
2870
1850
3020
2790
2980
1950
2490
2130
2160
2020
2010
2140
2150
2080
2260
Nickel
100
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
3.7 J
2.5 J
3.4j
ND
3.2 J
2.2 J
2.4 J
ND
ND
ND
ND
ND
1.7 J
Potassium
NE
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
937 J
ND
ND
ND
ND
ND
ND
653 J
Mercury
1
ND
ND
0.000568
ND
OM049e J
0.00274
0.000682
0.000910
0.000916
0.00105
0.00172
0.00107 B
0.00206
0.00131
0.0011
0.0011
0.00134 J
ND
0.009
0.001
0.0027
0.0013
0.0015
0.0012
0.0068
ND
Sodium
NE
ND
ND
ND
6000
5080
5010
ND
ND
ND
4260 J
5130
4090 J
3910 J
4830 J
4000 J
3920 J
3840 J
3610 J
4120 J
4920 J
3810 J
3440 J
4000 J
5110
4470J
4100
Zinc m /L
1
ND
ND
ND
ND
ND
0.0209
ND
ND
ND
ND
0.0073 J
ND
0.0251
0.0055 J
0.0055 J
0.0094 J
ND
ND
5.5 J
9.2 J
ND
ND
ND
12.7
26.4
ND
Acetone m /L
6
ND
ND
0.0065 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
16.8
ND
ND
ND
ND
ND
Alkalinity, Total as CaCO3 m /L
NE
23.3
28.3
29.3
28.8
9.8
28.1
25.8
28.0
27.1
29.2
26.5
27.3
16.9
30.0
30.4
28.4
22.4
25.5
20.2
16.2
45.0
17.3
24.5
22.4
23.2
23.9
Total Dissolved Solids m /L
500
69.0
50.0
51.0
115
ND
45.0
58.0
64.0
48.0
77.0
59.0
72.0
53.0
56.0
50.0 D6
46.0
52.0
29.0
52.0
54.0
45.0
51.0
40.0
43.0
44.0
48.0
Sulfate m /L
250
5.1
6.2
ND
ND
5.2
4.6
5.4
5.7
5.4
5.8
5.1
4.8
3.1
6.1
5.8
4.4
2.8
ND
3.6
2.9
3.7
2.6
3.5
3.0
2.8
3.1
Chloride m /L
250
ND
ND
ND
ND
2.3
2.3
2.1
2.0
2.0
1.5
2.2
1.7
1.6
1.5
1.8
1.6
1.9
1.7
1.4
1.6
1.5
1.3
1.6
1.9
2.3
1.5
Total Organic Carbon m /L
NE
2.8
40.3
2.7
26.2
25.7
5.4
4.4
27.5
3.9
1.1
20.5
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
All concentrations are in micrograms per liter (ug/L) unless otherwise noted.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
NA - Not Applicable
ND - Not Detected
NE - Not Established
B - Analyyte was dected in the assoicated method blank
3 of

Sludge Landfill
SW P1 Stormwater/Leachate Pipe - Located at toe of Sludge Landfill dam
2L
Date Sam Is Collected
Field Data
Standard
07/06/10=7.427.4
/11
11/14/11
07/10/12
11/06/12
07/01/13=39.413.2
/14
11/11/14
07/30/15
11/05/15
07/11/16=7.67.2
/17=7.27.2
/18
11/16/18
07/09/19Z7.67.3
6/20
11/16/20
07/12/21
2
11/02/22
Field pH
7.42
8.0
7.6
7.8
7.6
7.4
7.4
7.6
7.2
7.2
7.2
7.4
7.1
6.7
Field Tem erature de C21.12
14.62
20.9
11.35
21.09
16.6
20.3
18.4
19.0
15.2
19.7
16.8
20.1
17.2
Static Water Level feet
NANA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
=7.97.3
NA
Field S ecific Conductance1161
7(umhos/cm)NE
1326
1252
1463
1156
1229
1230
1034
1003
952
5.79
921
845
1458
Turbidit NTU
Detects OnlArsenic
10557.8
74.3
61.4
47.8
28.1
40
106.9
130.2
73.46
175
76.14
61.02
36.84
8.8
.
ND
ND
ND
ND
J
ND
ND
ND
2.6 J
ND
ND
9.7 J
ND
.
9.6 J
Barium
230
215
198
217
229
212
213
222
129
187
211
182
188
204
259
201
229
175
209
187
178
167
184
184
312
319
Boron
700
90.2
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Calcium
NE
96000
99000
91000
122000
97700
114000
87100
97400
38400
94800
91900
39600
79600
95900
109000
175000
87000
91500
76000
90200
75600
78200
70500
95200
132000
160000
Chromium
10
ND
7.7
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Cobalt
1
35.4
30.2
27.5
18.9
22.2
8.2
21.4
37.8
5.7
17.9
18.6
9.3
18.8
19.4
13.4
8.8
23.5
12.1
19.0
14.4
16.8
14.2
18.2
12.9
28.5
9.0 J
Copper m /I
1
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0026 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Iron
300
15000
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Magnesium
NE
68100
76700
71400
85000
72600
90900
62300
59800
18500
64800
66600
48000
49300
66400
87000
65600
50300
41100
42300
41500
43300
42300
37400
45300
61600
51500
Manganese
50
4610
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Mercury
1
ND
ND
ND
ND
0.000418 J
0.000795
ND
0.000597
0.00875
0.000531
0.000567
0.000643 B
0.000666
0.000513
ND
0.000678
ND
ND
0.00739
0.000378 J
0.000889
0.000416 J
0.000658
ND
0.00343
ND
Nickel
100
ND
ND
ND
5.4
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.1 J
1.0 J
ND
ND
ND
ND
ND
ND
Potassium
NE
12700
17200
16200
22800
16800
22000
10700
13900
18200
12200
12700
12100
8200
12400
17700
15500
8720
9650
7440
9400
7750
8260
6360
9810
15000
13700
Silcon
NE
8320
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Sodium
NE
43100
41800
41900
50000
44300
44800
39900
42200
9730
33800
38700
20300
35600
35700
38200
26500
37600
20500
33600
25200
28700
24500
28900
26300
21600
13200
Strontium
NE
570
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Zinc m /L
1
ND
ND
ND
ND
ND
ND
ND
0.0106
ND
ND
ND
ND
0.009 J
0.0056 J
ND
ND
ND
ND
0.0080
ND
ND
ND
ND
ND
1,200
117
Benzoic Acid
30000
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
34 J
Vanadium
NE
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
3.3 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
8.1
ND
22.8
ND
2.9 J
Acetone m /L
6
NR
NR
0.0080 J
ND
0.0034 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Naphthalene
6
NR
NR
ND
ND
ND
ND
0.67 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
3&4-Meth I henol
40
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
8.40 J
7.50 i
Toluene
600
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.00 j
Alkalinity, Total as CaCO3 m /L
NE
688
760
651
748
27.3
752
654
589
210
628
591
549
528
651
789
639
535
567
478
492
485
474
415
543
706
754
Total Dissolved Solids m /L
500
633
671
633
635
639
741
617
558
256
607
595
420
512
594
670
586
504
442
440
479
461
484
409
494
660
656
Total Suspended Solids m /L
NE
35.3
29.8
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
BOD, 5 Da m /L
NE
4.5
8.1
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
Chemical Oxygen Demand m /L
NE
53
58
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
Sulfate m /L
250
ND
ND
ND
ND
2.4
ND
ND
ND
3.2
1.8 J
2.6
2.0
1.8 J
2.0
1.1
0.78 J
ND
ND
0.74
0.73 J
ND
ND
0.52 J
0.65 J
2.70
0.52 J
Chloride m /L
250
NR
NR
46
52.8
50.4
48.9
45.0
37.9
13.4
39.2
41.9
30.8
37.6
44.4
44.7
40.4
35.7
25.5
30.6
26.7
28.0
25.1
24.2
27.9
24.2
19.0
Total Organic Carbon m /L
NE
NR
NR
24.7
27.4
22.6
28.3
23.2
33.0
18.9
51.0
13.5
8.1
8.3
10.1
14.8
10.4
9.1
7.1
7.8
7.4
5.9
6.8
5.4
7.3
18.4
14.7
All concentrations are in micrograms per liter (ug/L) unless otherwise noted.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
NA - Not Applicable
ND - Not Detected
NE - Not Established
NR - Not Reported
B - Analyte was detected in the assoicated method blank
4 of

Sludge Landfill
SW P2 Stormwater/Groundwater Pipe - Located at toe of former Temporary Sludge Landfill dam
Date SamDle Collected
Field D
Standard 07/06/10 11/08/10
07/19/11
11/14/11
07/10/12
11/06/12
07/01/13
11/18/13
07/10/14 11/11/14
07/30/15
11/05/15
07/11/16
11/07/16
07/10/17
11/06/17
07/09/18
11/16/18
07/09/19
11/07/19
07/06/20
11/16/20
07/12/21
11/01/21
07/18/22:.n
Field pH
6.5 to 8.5
7.23
7.44
7.4
7.6
7.4
7.0
7.1
7.0
7.5
6.9
7.2
7.5
6.5
7.0
8.2
7.4
7.4
7.1
7.5
8.0
7.9
7.4
7.0
6.9
8.68
Field Temperature de C
NE
19.02
13.20
19.85
12.95
20.2
11.88
18.08
14.56
17.90
12.9
18.1
16.3
18.6
14.1
29.1
16.2
17.5
10.4
17.6
14.8
17.6
13.8
17.1
13.1
29.3
Static Water Level feet
NE
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Field Specific Conductance umhos/cm
NE
490
486
482
429
408
429
422
394
383
349
299
280
1020
265
262
279.2
300
234.5
256
237.8
250
218
241
242.1
249.3
TurbidityNTU
Substance Detects 0
NE
56.7
58
14
35.7
32.7
27.2
15.3
12.5
20.6
6.51
10.08
17.65
115.20
18.11
8.20
22.90
12.14
6.96
6.18
14.30
20.47
37.94
5.16
27.40
11.64
Arsenic
10
ND
6.3
ND
ND
5.0
ND
6.5 J
ND
5.1 J
ND
ND
ND
ND
ND
5A J
ND
ND
ND
ND
ND
5.9 J
ND
ND
ND
ND
Barium
700
162
148
164
127
142
157
150
159
121
107
102
89.8
93.9
89.9
45.2
118
99.1
29.6
94.5
35.9
89
65.3
85.6
107
72.7
74.2
Calcium
NE
55700
55300
58000
46900
44000
45000
45300
45900
38600
34300
30200
41700
29400
28600
40000
36500
33900
31100
29100
32000
27000
25000
24500
28500
22800
22800
Cobalt
1
12.4
13.1
9.9
ND
ND
ND
5.3
20.3
ND
4.2 J
4.1 J
3.3 J
6.8
5.8
ND
4.6 J
8.6
ND
9.1
ND
9.9
8.3
11.6
11.4
13.1
12.6
Copper m /I
1
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0064
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Lead
15
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
5.2
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Magnesium
NE
15500
14700
13900
13500
12700
13900
12000
10900
8940
9200
8320
5930
7570
7630
8790
7170
7130
5950
5810
6750
5770
4440
5260
5950
5150
5320
Nickel
100
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
1.3 J
Potassium
NE
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
9470
ND
ND
3340 J
1850 J
4060 J
ND
ND
ND
ND
ND
1140
Mercury
1
ND
ND
ND
ND
0.000405 J
ND
0.000565
0.000534
ND
ND
0.000482 J
o.000726 B
o.000474 J
o.000mo J
o.007850
0.000472 J
ND
0.003360
0.006880
0.004046
0.002910
0.000694
0.000912
ND
ND
ND
Sodium
NE
26300
27000
25400
28700
24400
26700
19900
19600
16600
16500
16000
11100
14100
15100
9470
12600
12300
6280
10400
6930
9830
7460
9570
11400
9250
8960
Vanadium
NE
ND
ND
ND
ND
ND
ND
5.9
ND
ND
ND
2.8 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
4.4 J
ND
26.7
ND
ND
Zinc m /L
1
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0055 J
ND
0.0058 J
ND
ND
0.0312
ND
ND
0.0052 J
0.0059 J
ND
ND
ND
ND
ND
ND
ND
Acetone m /L
6
NR
NR
0.0052 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Methylene Chloride
5
NR
NR
1.7 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Hexachloro-1,3-butadiene
0.44
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.92 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Alkalinity, Total as CaCO3 m /L
NE
285
260
232
234
205
215
228
193
178
169
138
140
144
139
88.8
153
148
106
125
95.3
122
108
109
110
102
N105
Total Dissolved Solids m /L
500
321
270
260
216
ND
231
236
193
191
185
148
122
125
140
153
166
168
127
137
143
132
ND
121
132
113
116
Total Suspended Solids m /L
NE
NR
18.8
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
BOD,5Day m /L
NE
NR
2.1
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
Chemical Oxygen Demand m /L
NE
NR
99.0
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
Sulfate m /L
250
ND
8.3
8.8
5.0
5.2
5.8
8.4
7.5
6.8
5.0
4.1
8.6
4.4
3.6
42.2
7.4
5.6
24.4
6.3
25.7
4.0
4.4
3.1
3.4
5.6
2.5
Chloride m /L
250
7.7
NR
5.8
7.0
5.7
5.4
4.5
4.1
3.7
4.0
4.1
2.6
3.9
4.3
4.4
2.8
3.6
3.1
2.5
3.2
2.8
2.0
3.8
3.2
2.6
2.7
Total Organic Carbon m /L
NE
5.9
NR
5.7
5.6
4.6
40.2
36.8
5.7
4.5
17.9
0.69 J
0.72 J
ND
ND
9.8
ND
ND
6.1
0.78 J
7.5
0.54 J
ND
ND
ND
ND
ND
All concentrations are in micrograms per liter (ug/L) unless otherwise noted.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
NA - Not Applicable
ND - Not Detected
NE - Not Established
NR - Not Reported
B - Analyte was detected in the assoicated method blank
5 of

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
December 21, 2022
Mr. Mike Cody
Glatfelter Corp.
228 South Main Street
Spring Grove, PA 17362
RE: Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Dear Mr. Cody:
Enclosed are the analytical results for sample(s) received by the laboratory between November 02, 2022 and November
03, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable
TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the
report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Ormond Beach
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lord Patton
[e-mail]
1(828)254-7176
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Pace Analytical Services Ormond Beach
8 East Tower Circle, Ormond Beach, FL 32174
Alaska DEC- CS/UST/LUST
Alabama Certification #: 41320
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maine Certification #: FLO1264
Maryland Certification: #346
Massachusetts Certification #: M-FL1264
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification M E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
New Hampshire Certification #: 2958
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Ohio DEP 87780
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FLO1264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
SLUDGE LANDFILL 11/22
92634407
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92634407001
SWP-1
EPA 6010
AME
18
PASI-O
EPA 8270E
PKS
74
PASI-C
EPA 8260D
SAS
63
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
SMS
1
PASI-A
SM 2540C-2015
CS1
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
SM 4500-CI-E-2011
ANM
1
PASI-A
SM 531OB-2014
MJP
1
PASI-A
92634407002
SWP-2
EPA 6010
AME
18
PASI-O
EPA 8270E
PKS
74
PASI-C
EPA 8260D
SAS
63
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
SMS
1
PASI-A
SM 2540C-2015
CS1
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
SM 4500-CI-E-2011
ANM
1
PASI-A
SM 531OB-2014
MJP
1
PASI-A
92634407003
Q06V09
EPA 6010
AME
18
PASI-0
EPA 8270E
PKS
74
PASI-C
EPA 8260D
SAS
63
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
SMS
1
PASI-A
SM 2540C-2015
CS1
1
PASI-A
EPA 300.0 Rev 2.1 1993
JCM
1
PASI-A
SM 4500-CI-E-2011
ANM
1
PASI-A
SM 531OB-2014
MJP
1
PASI-A
92634407004
Q06V10
EPA 6010
AME
18
PASI-0
EPA 8270E
PKS
74
PASI-C
EPA 8260D
SAS
63
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
SMS
1
PASI-A
SM 2540C-2015
CS1
1
PASI-A
EPA 300.0 Rev 2.1 1993
JCM
1
PASI-A
SM 4500-CI-E-2011
ANM
1
PASI-A
SM 531OB-2014
MJP
1
PASI-A
92634407005
Q06V11
EPA 6010
AME
18
PASI-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
EPA 8270E
PKS
74
PASI-C
EPA 8260D
SAS
63
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
SMS
1
PASI-A
SM 2540C-2015
CS1
1
PASI-A
EPA 300.0 Rev 2.1 1993
JCM
1
PASI-A
SM 4500-CI-E-2011
ANM
1
PASI-A
SM 531OB-2014
MJP
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-O = Pace Analytical Services - Ormond Beach
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SUMMARY OF DETECTION
Project:
SLUDGE LANDFILL 11/22
Pace Project No.:
92634407
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed Qualifiers
92634407001
SWP-1
Performed by
Pace
11/08/22 20:35
Collected By
S.Kline
11/08/22 20:35
Collected Date
11/2/22
11/08/22 20:35
Collected Time
11:20
11/08/22 20:35
pH
6.67
Std. Units
11/08/22 20:35
Temperature
17.2
deg C
11/08/22 20:35
Specific Conductance
1458
umhos/cm
11/08/22 20:35
Oxygen, Dissolved
6.48
mg/L
11/08/22 20:35
REDOX
-90.3
mV
11/08/22 20:35
Turbidity
36.84
NTU
11/08/22 20:35
Odor
None
11/08/22 20:35
Appearance
Clear, few
11/08/22 20:35
rusty solids
EPA 6010
Arsenic
9.6J
ug/L
10.0
12/08/22 02:29
EPA 6010
Barium
319
ug/L
10.0
12/08/22 02:29
EPA 6010
Calcium
160000
ug/L
500
12/08/22 02:29
EPA 6010
Cobalt
9.01
ug/L
10.0
12/08/22 02:29
EPA 6010
Magnesium
51500
ug/L
500
12/08/22 02:29
EPA 6010
Potassium
13700
ug/L
1000
12/08/22 02:29
EPA 6010
Sodium
13200
ug/L
2000
12/08/22 02:29
EPA 6010
Vanadium
2.9J
ug/L
10.0
12/08/22 02:29
EPA 6010
Zinc
117
ug/L
20.0
12/08/22 02:29
EPA 8270E
Benzoic Acid
34.OJ
ug/L
43.5
11/09/22 18:09
EPA 8270E
3&4-Methyl phenol (m&p Cresol)
7.5J
ug/L
8.7
11/09/2218:09
EPA 8260D
Toluene
1.0J
ug/L
1.0
11/07/22 01:35
SM 2320B-2011
Alkalinity, Total as CaCO3
754
mg/L
5.0
11/04/22 09:43
SM 2540C-2015
Total Dissolved Solids
656
mg/L
50.0
11/02/22 20:50
EPA 300.0 Rev 2.1 1993 Sulfate
0.52J
mg/L
1.0
11/04/22 00:01
SM 4500-CI-E-2011
Chloride
19.0
mg/L
1.0
11/10/22 17:18
SM 5310B-2014
Total Organic Carbon
14.7
mg/L
1.0
11/03/22 23:12
92634407002
SWP-2
Performed by
Pace
11/09/22 06:23
Collected By
S.Kline
11/09/22 06:23
Collected Date
11/2/22
11/09/22 06:23
Collected Time
12:32
11/09/22 06:23
pH
7.46
Std. Units
11/09/22 06:23
Temperature
13.9
deg C
11/09/22 06:23
Specific Conductance
200.8
umhos/cm
11/09/22 06:23
Oxygen, Dissolved
6.46
mg/L
11/09/22 06:23
REDOX
-22.0
mV
11/09/22 06:23
Turbidity
15.78
NTU
11/09/22 06:23
Odor
No odor
11/09/22 06:23
Appearance
Low water
11/09/22 06:23
level, lots of
leaves
EPA 6010
Barium
74.2
ug/L
10.0
12/08/22 02:33
EPA 6010
Calcium
22800
ug/L
500
12/08/22 02:33
EPA 6010
Cobalt
12.6
ug/L
10.0
12/08/22 02:33
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Lab Sample ID
Method
92634407002
EPA 6010
EPA 6010
EPA 6010
EPA 6010
SM 2320B-2011
SM 2540C-2015
EPA 300.0 Rev 2.1 1993
SM 4500-CI-E-2011
92634407003
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
SM 2320B-2011
SM 2540C-2015
EPA 300.0 Rev 2.1 1993
SM 4500-CI-E-2011
SM 5310B-2014
92634407004
SUMMARY OF DETECTION
Client Sample ID
Parameters
Result
Units
Report Limit
Analyzed
SWP-2
Magnesium
5320
ug/L
500
12/08/22 02:33
Nickel
1.3J
ug/L
5.0
12/08/22 02:33
Potassium
1140
ug/L
1000
12/08/22 02:33
Sodium
8960
ug/L
2000
12/08/22 02:33
Alkalinity, Total as CaCO3
105
mg/L
5.0
11/03/22 17:06
Total Dissolved Solids
116
mg/L
25.0
11/02/22 20:50
Sulfate
2.5
mg/L
1.0
11/04/22 00:33
Chloride
2.7
mg/L
1.0
11/10/2217:19
Q06V09
Performed by
Pace
11/09/22 06:26
Collected By
M.Swann
11/09/22 06:26
Collected Date
11/3/22
11/09/22 06:26
Collected Time
11:10
11/09/22 06:26
pH
6.30
Std. Units
11/09/22 06:26
Temperature
15.9
deg C
11/09/22 06:26
Static Water Level
29.51
feet
11/09/22 06:26
Specific Conductance
1398
umhos/cm
11/09/22 06:26
Oxygen, Dissolved
3.91
mg/L
11/09/22 06:26
Total Well Depth
69.80
feet
11/09/22 06:26
REDOX
-39.8
mV
11/09/22 06:26
Turbidity
15.85
NTU
11/09/22 06:26
Odor
No odor
11/09/22 06:26
Appearance
Clear
11/09/22 06:26
Antimony
6.OJ
ug/L
15.0
12/08/22 02:37
Arsenic
6.7J
ug/L
10.0
12/08/22 02:37
Barium
294
ug/L
10.0
12/08/22 02:37
Calcium
171000
ug/L
500
12/08/22 02:37
Cobalt
13.2
ug/L
10.0
12/08/22 02:37
Magnesium
78800
ug/L
500
12/08/22 02:37
Nickel
17.0
ug/L
5.0
12/08/22 02:37
Potassium
4570
ug/L
1000
12/08/22 02:37
Sodium
30000
ug/L
2000
12/08/22 02:37
Alkalinity, Total as CaCO3
828
mg/L
5.0
11/08/22 11:14
Total Dissolved Solids
780
mg/L
50.0
11/07/22 10:16
Sulfate
2.6
mg/L
1.0
11/05/22 22:14
Chloride
47.8
mg/L
3.0
11/10/2217:22
Total Organic Carbon
4.1
mg/L
1.0
11/15/22 09:09
Q06V10
Performed by
Pace
11/09/22 10:06
Collected By
M.Swann
11/09/22 10:06
Collected Date
11/3/22
11/09/22 10:06
Collected Time
10:20
11/09/22 10:06
pH
5.52
Std. Units
11/09/22 10:06
Temperature
14.4
deg C
11/09/22 10:06
Static Water Level
28.18
feet
11/09/22 10:06
Specific Conductance
39.1
umhos/cm
11/09/22 10:06
REPORT OF LABORATORY ANALYSIS
Qualifiers
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 6 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Lab Sample ID Client Sample ID
Method Parameters
92634407004
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
SM 2320B-2011
SM 2540C-2015
EPA 300.0 Rev 2.1 1993
SM 4500-CI-E-2011
92634407005
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
SM 2320B-2011
SM 2540C-2015
EPA 300.0 Rev 2.1 1993
SM 4500-CI-E-2011
Q06V10
Oxygen, Dissolved
Total Well Depth
REDOX
Turbidity
Odor
Appearance
Barium
Calcium
Lead
Magnesium
Potassium
Sodium
Alkalinity, Total as CaCO3
Total Dissolved Solids
Sulfate
Chloride
Q06V11
Performed by
Collected By
Collected Date
Collected Time
pH
Temperature
Static Water Level
Specific Conductance
Oxygen, Dissolved
Total Well Depth
REDOX
Turbidity
Odor
Appearance
Barium
Calcium
Copper
Magnesium
Nickel
Potassium
Sodium
Alkalinity, Total as CaCO3
Total Dissolved Solids
Sulfate
Chloride
SUMMARY OF DETECTION
Result Units Report Limit Analyzed Qualifiers
8.98
32.30
35.0
8.98
No odor
Clear
6.2J
2770
2.6J
995
294J
19801
10.3
33.0
1.0
1.5
Pace
M.Swann
11 /3/22
10:35
5.51
13.8
40.80
68.3
10.15
56.90
-12.1
10.15
No odor
Clear
7.1 J
4700
2.7J
2260
1.7J
653J
4100
23.9
48.0
3.1
1.5
mg/L
feet
my
NTU
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
mg/L
mg/L
mg/L
Std. Units
deg C
feet
umhos/cm
mg/L
feet
my
NTU
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
mg/L
mg/L
mg/L
REPORT OF LABORATORY ANALYSIS
10.0
500
10.0
500
1000
2000
5.0
25.0
1.0
1.0
10.0
500
5.0
500
5.0
1000
2000
5.0
25.0
1.0
1.0
11 /09/22 10:06
11 /09/22 10:06
11 /09/22 10:06
11 /09/22 10:06
11 /09/22 10:06
11 /09/22 10:06
12/08/22 02:40
12/08/22 02:40
12/08/22 02:40
12/08/22 02:40
12/08/22 02:40
12/08/22 02:40
11 /05/22 14:22
11 /07/22 10:20
11 /05/22 22:30
11 /10/22 17:23
11 /09/22 10:08
11 /09/22 10:08
11 /09/22 10:08
11 /09/22 10:08
11 /09/22 10:08
11 /09/22 10:08
11 /09/22 10:08
11 /09/22 10:08
11 /09/22 10:08
11 /09/22 10:08
11 /09/22 10:08
11 /09/22 10:08
11 /09/22 10:08
11 /09/22 10:08
12/08/22 02:52
12/08/22 02:52
12/08/22 02:52
12/08/22 02:52
12/08/22 02:52
12/08/22 02:52
12/08/22 02:52
11 /05/22 14:27
11 /07/22 10:20
11 /05/22 23:17
11 /10/22 17:26
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 7 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Sample: SWP-1 Lab ID: 92634407001 Collected: 11/02/22 11:30 Received: 11/02/22 16:45 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Performed by
Pace
1
11/08/22 20:35
Collected By
S.Kline
1
11/08/22 20:35
Collected Date
11/2/22
1
11/08/22 20:35
Collected Time
11:20
1
11/08/22 20:35
pH
6.67
Std. Units
1
11/08/22 20:35
Temperature
17.2
deg C
1
11/08/22 20:35
Specific Conductance
1458
umhos/cm
1
11/08/22 20:35
Oxygen, Dissolved
6.48
mg/L
1
11/08/22 20:35
7782-44-7
REDOX
-90.3
mV
1
11/08/22 20:35
Turbidity
36.84
NTU
1
11/08/22 20:35
Odor
None
1
11/08/22 20:35
Appearance
Clear, few
1
11/08/22 20:35
rusty
solids
6010 MET ICP
Analytical Method: EPA 6010 Preparation
Method:
EPA 3010
Pace Analytical Services - Ormond Beach
Antimony
ND
ug/L
15.0
1
12/04/22 18:12
12/08/22 02:29
7440-36-0
Arsenic
9.6J
ug/L
10.0
1
12/04/22 18:12
12/08/22 02:29
7440-38-2
Barium
319
ug/L
10.0
1
12/04/22 18:12
12/08/22 02:29
7440-39-3
Cadmium
ND
ug/L
1.0
1
12/04/22 18:12
12/08/22 02:29
7440-43-9
Calcium
160000
ug/L
500
1
12/04/22 18:12
12/08/22 02:29
7440-70-2
Chromium
ND
ug/L
5.0
1
12/04/22 18:12
12/08/22 02:29
7440-47-3
Cobalt
9.01
ug/L
10.0
1
12/04/22 18:12
12/08/22 02:29
7440-48-4
Copper
ND
ug/L
5.0
1
12/04/22 18:12
12/08/22 02:29
7440-50-8
Lead
ND
ug/L
10.0
1
12/04/22 18:12
12/08/22 02:29
7439-92-1
Magnesium
51500
ug/L
500
1
12/04/22 18:12
12/08/22 02:29
7439-95-4
Nickel
ND
ug/L
5.0
1
12/04/22 18:12
12/08/22 02:29
7440-02-0
Potassium
13700
ug/L
1000
1
12/04/22 18:12
12/08/22 02:29
7440-09-7
Selenium
ND
ug/L
15.0
1
12/04/22 18:12
12/08/22 02:29
7782-49-2
Silver
ND
ug/L
5.0
1
12/04/22 18:12
12/08/22 02:29
7440-22-4
Sodium
13200
ug/L
2000
1
12/04/22 18:12
12/08/22 02:29
7440-23-5
Thallium
ND
ug/L
15.0
1
12/04/22 18:12
12/08/22 02:29
7440-28-0
Vanadium
2.9J
ug/L
10.0
1
12/04/22 18:12
12/08/22 02:29
7440-62-2
Zinc
117
ug/L
20.0
1
12/04/22 18:12
12/08/22 02:29
7440-66-6
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Acenaphthene
ND
ug/L
8.7
1
11/07/2217:45
11/09/2218:09
83-32-9
Acenaphthylene
ND
ug/L
8.7
1
11/07/2217:45
11/09/2218:09
208-96-8
Aniline
ND
ug/L
8.7
1
11/07/2217:45
11/09/2218:09
62-53-3
Anthracene
ND
ug/L
8.7
1
11/07/2217:45
11/09/2218:09
120-12-7
Benzo(a)anthracene
ND
ug/L
8.7
1
11/07/2217:45
11/09/2218:09
56-55-3
Benzo(a)pyrene
ND
ug/L
8.7
1
11/07/2217:45
11/09/2218:09
50-32-8
Benzo(b)fluoranthene
ND
ug/L
8.7
1
11/07/2217:45
11/09/2218:09
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
8.7
1
11/07/2217:45
11/09/2218:09
191-24-2
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 12/21 /2022 11:11 AM
without
the written consent of Pace Analytical Services,
LLC.
Page 8 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Sample: SWP-1
Lab ID: 92634407001 Collected:
11/02/22
11:30
Received: 11/02/22 16:45 Matrix: Water
Parameters
Results
Units PQL
DF
Prepared
Analyzed
CAS No. Qual
8270E RVE
Analytical Method:
EPA 8270E Preparation Method: EPA 3510C
Pace Analytical
Services - Charlotte
Benzo(k)fluoranthene
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
207-08-9
Benzoic Acid
34.OJ
ug/L
43.5
1
11/07/22 17:45
11/09/22 18:09
65-85-0
Benzyl alcohol
ND
ug/L
17.4
1
11/07/22 17:45
11/09/22 18:09
100-51-6
4-Bromophenylphenyl ether
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
101-55-3
Butylbenzylphthalate
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
59-50-7
4-Chloroaniline
ND
ug/L
17.4
1
11/07/22 17:45
11/09/22 18:09
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
111-44-4
2-Chloronaphthalene
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
91-58-7
2-Chlorophenol
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
7005-72-3
Chrysene
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
53-70-3
Dibenzofuran
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
132-64-9
1,2-Dichlorobenzene
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
95-50-1
1,3-Dichlorobenzene
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
541-73-1
1,4-Dichlorobenzene
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
17.4
1
11/07/22 17:45
11/09/22 18:09
91-94-1
2,4-Dichlorophenol
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
120-83-2
Diethylphthalate
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
84-66-2
2,4-Dimethylphenol
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
105-67-9 v2
Dimethylphthalate
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
131-11-3
Di-n-butylphthalate
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
17.4
1
11/07/22 17:45
11/09/22 18:09
534-52-1
2,4-Dinitrophenol
ND
ug/L
43.5
1
11/07/22 17:45
11/09/22 18:09
51-28-5
2,4-Dinitrotoluene
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
121-14-2
2,6-Dinitrotoluene
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
606-20-2
Di-n-octylphthalate
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.2
1
11/07/22 17:45
11/09/22 18:09
117-81-7
Fluoranthene
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
206-44-0
Fluorene
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
87-68-3
Hexachlorobenzene
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
77-47-4
Hexachloroethane
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
193-39-5
Isophorone
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
78-59-1
1-Methylnaphthalene
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
90-12-0
2-Methylnaphthalene
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
95-48-7
3&4-Methyl phenol (m&p Cresol)
7.5J
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
15831-10-4
Naphthalene
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
91-20-3
2-Nitroaniline
ND
ug/L
17.4
1
11/07/22 17:45
11/09/22 18:09
88-74-4
3-Nitroaniline
ND
ug/L
17.4
1
11/07/22 17:45
11/09/22 18:09
99-09-2
4-Nitroaniline
ND
ug/L
17.4
1
11/07/22 17:45
11/09/22 18:09
100-01-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Sample: SWP-1 Lab ID: 92634407001 Collected: 11/02/22 11:30 Received: 11/02/22 16:45 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical
Services - Charlotte
Nitrobenzene
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
98-95-3
2-Nitrophenol
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
88-75-5
4-Nitrophenol
ND
ug/L
43.5
1
11/07/22 17:45
11/09/22 18:09
100-02-7
N-Nitrosodimethylamine
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
108-60-1
Pentachlorophenol
ND
ug/L
17.4
1
11/07/22 17:45
11/09/22 18:09
87-86-5
Phenanthrene
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
85-01-8
Phenol
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
108-95-2
Pyrene
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
120-82-1
2,4,5-Trichlorophenol
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
95-95-4
2,4,6-Trichlorophenol
ND
ug/L
8.7
1
11/07/22 17:45
11/09/22 18:09
88-06-2
Surrogates
Nitrobenzene-d5 (S)
37
%
10-144
1
11/07/22 17:45
11/09/22 18:09
4165-60-0
2-Fluorobiphenyl (S)
24
%
10-130
1
11/07/22 17:45
11/09/22 18:09
321-60-8
Terphenyl-d14 (S)
107
%
34-163
1
11/07/22 17:45
11/09/22 18:09
1718-51-0
Phenol-d6 (S)
37
%
10-130
1
11/07/22 17:45
11/09/22 18:09
13127-88-3
2-Fluorophenol (S)
39
%
10-130
1
11/07/22 17:45
11/09/22 18:09
367-12-4
2,4,6-Tribromophenol (S)
93
%
10-144
1
11/07/22 17:45
11/09/22 18:09
118-79-6
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
11/07/22 01:35
67-64-1
Benzene
ND
ug/L
1.0
1
11/07/22 01:35
71-43-2
Bromobenzene
ND
ug/L
1.0
1
11/07/22 01:35
108-86-1
Bromochloromethane
ND
ug/L
1.0
1
11/07/22 01:35
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
11/07/22 01:35
75-27-4
Bromoform
ND
ug/L
1.0
1
11/07/22 01:35
75-25-2
Bromomethane
ND
ug/L
2.0
1
11/07/22 01:35
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
11/07/22 01:35
78-93-3
Carbon tetrachloride
ND
ug/L
1.0
1
11/07/22 01:35
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
11/07/22 01:35
108-90-7
Chloroethane
ND
ug/L
1.0
1
11/07/22 01:35
75-00-3
Chloroform
ND
ug/L
1.0
1
11/07/22 01:35
67-66-3
Chloromethane
ND
ug/L
1.0
1
11/07/22 01:35
74-87-3
2-Chlorotoluene
ND
ug/L
1.0
1
11/07/22 01:35
95-49-8
4-Chlorotoluene
ND
ug/L
1.0
1
11/07/22 01:35
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
11/07/22 01:35
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
11/07/22 01:35
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
11/07/22 01:35
106-93-4
Dibromomethane
ND
ug/L
1.0
1
11/07/22 01:35
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
11/07/22 01:35
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.0
1
11/07/22 01:35
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
11/07/22 01:35
106-46-7
REPORT OF LABORATORY ANALYSIS
v2
v2
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Sample: SWP-1
Parameters
8260D MSV Low Level Landfill
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
ANALYTICAL RESULTS
Lab ID: 92634407001 Collected: 11/02/22 11:30 Received: 11/02/22 16:45 Matrix: Water
Results Units
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
1.0J
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
96 %
89 %
102 %
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
ND ug/L
PQL DF Prepared Analyzed CAS No
1.0
1
11/07/22 01:35
75-71-8
1.0
1
11/07/22 01:35
75-34-3
1.0
1
11/07/22 01:35
107-06-2
1.0
1
11/07/22 01:35
75-35-4
1.0
1
11/07/22 01:35
156-59-2
1.0
1
11/07/22 01:35
156-60-5
1.0
1
11/07/22 01:35
78-87-5
1.0
1
11/07/22 01:35
142-28-9
1.0
1
11/07/22 01:35
594-20-7
1.0
1
11/07/22 01:35
563-58-6
1.0
1
11/07/22 01:35
10061-01-5
1.0
1
11/07/22 01:35
10061-02-6
1.0
1
11/07/22 01:35
108-20-3
1.0
1
11/07/22 01:35
100-41-4
2.0
1
11/07/22 01:35
87-68-3
5.0
1
11/07/22 01:35
591-78-6
1.0
1
11/07/22 01:35
99-87-6
5.0
1
11/07/22 01:35
75-09-2
5.0
1
11/07/22 01:35
108-10-1
1.0
1
11/07/22 01:35
1634-04-4
1.0
1
11/07/22 01:35
91-20-3
1.0
1
11/07/22 01:35
100-42-5
1.0
1
11/07/22 01:35
630-20-6
1.0
1
11/07/22 01:35
79-34-5
1.0
1
11/07/22 01:35
127-18-4
1.0
1
11/07/22 01:35
108-88-3
1.0
1
11/07/22 01:35
87-61-6
1.0
1
11/07/22 01:35
120-82-1
1.0
1
11/07/22 01:35
71-55-6
1.0
1
11/07/22 01:35
79-00-5
1.0
1
11/07/22 01:35
79-01-6
1.0
1
11/07/22 01:35
75-69-4
1.0
1
11/07/22 01:35
96-18-4
2.0
1
11/07/22 01:35
108-05-4
1.0
1
11/07/22 01:35
75-01-4
1.0
1
11/07/22 01:35
1330-20-7
2.0
1
11/07/22 01:35
179601-23-1
1.0
1
11/07/22 01:35
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
11/07/22 01:35 460-00-4
11/07/22 01:35 17060-07-0
11/07/22 01:35 2037-26-5
ifi0110��'iIll W45iPaS1iIll
l
Qual
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Sample: SWP-1 Lab ID: 92634407001 Collected: 11/02/22 11:30 Received: 11/02/22 16:45 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8260D MSV SIM Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
Surrogates
1,2-Dichloroethane-d4 (S)
110 %
70-130
1
11/03/22 14:29
17060-07-0
Toluene-d8 (S)
99 %
70-130
1
11/03/22 14:29
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
754 mg/L
5.0
1
11/04/22 09:43
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2015
Pace Analytical Services -Asheville
Total Dissolved Solids
656 mg/L
50.0
1
11/02/22 20:50
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1
1993
Pace Analytical Services -Asheville
Sulfate
0.52J mg/L
1.0
1
11/04/22 00:01
14808-79-8
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
19.0 mg/L
1.0
1
11/10/2217:18
16887-00-6
5310B TOC
Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
14.7 mg/L
1.0
1
11/03/22 23:12
7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Sample: SWP-2 Lab ID: 92634407002 Collected: 11/02/22 12:45 Received: 11/02/22 16:45 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Performed by
Pace
1
11/09/22 06:23
Collected By
S.Kline
1
11/09/22 06:23
Collected Date
11/2/22
1
11/09/22 06:23
Collected Time
12:32
1
11/09/22 06:23
pH
7.46
Std. Units
1
11/09/22 06:23
Temperature
13.9
deg C
1
11/09/22 06:23
Specific Conductance
200.8
umhos/cm
1
11/09/22 06:23
Oxygen, Dissolved
6.46
mg/L
1
11/09/22 06:23
7782-44-7
REDOX
-22.0
mV
1
11/09/22 06:23
Turbidity
15.78
NTU
1
11/09/22 06:23
Odor
No odor
1
11/09/22 06:23
Appearance
Low water
1
11/09/22 06:23
level, lots
of leaves
6010 MET ICP
Analytical Method: EPA 6010 Preparation
Method:
EPA 3010
Pace Analytical Services - Ormond Beach
Antimony
ND
ug/L
15.0
1
12/04/22 18:12
12/08/22 02:33
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/04/22 18:12
12/08/22 02:33
7440-38-2
Barium
74.2
ug/L
10.0
1
12/04/22 18:12
12/08/22 02:33
7440-39-3
Cadmium
ND
ug/L
1.0
1
12/04/22 18:12
12/08/22 02:33
7440-43-9
Calcium
22800
ug/L
500
1
12/04/22 18:12
12/08/22 02:33
7440-70-2
Chromium
ND
ug/L
5.0
1
12/04/22 18:12
12/08/22 02:33
7440-47-3
Cobalt
12.6
ug/L
10.0
1
12/04/22 18:12
12/08/22 02:33
7440-48-4
Copper
ND
ug/L
5.0
1
12/04/22 18:12
12/08/22 02:33
7440-50-8
Lead
ND
ug/L
10.0
1
12/04/22 18:12
12/08/22 02:33
7439-92-1
Magnesium
5320
ug/L
500
1
12/04/22 18:12
12/08/22 02:33
7439-95-4
Nickel
1.3J
ug/L
5.0
1
12/04/22 18:12
12/08/22 02:33
7440-02-0
Potassium
1140
ug/L
1000
1
12/04/22 18:12
12/08/22 02:33
7440-09-7
Selenium
ND
ug/L
15.0
1
12/04/22 18:12
12/08/22 02:33
7782-49-2
Silver
ND
ug/L
5.0
1
12/04/22 18:12
12/08/22 02:33
7440-22-4
Sodium
8960
ug/L
2000
1
12/04/22 18:12
12/08/22 02:33
7440-23-5
Thallium
ND
ug/L
15.0
1
12/04/22 18:12
12/08/22 02:33
7440-28-0
Vanadium
ND
ug/L
10.0
1
12/04/22 18:12
12/08/22 02:33
7440-62-2
Zinc
ND
ug/L
20.0
1
12/04/22 18:12
12/08/22 02:33
7440-66-6
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Acenaphthene
ND
ug/L
8.3
1
11/07/2217:45
11/09/2218:35
83-32-9
Acenaphthylene
ND
ug/L
8.3
1
11/07/2217:45
11/09/2218:35
208-96-8
Aniline
ND
ug/L
8.3
1
11/07/2217:45
11/09/2218:35
62-53-3
Anthracene
ND
ug/L
8.3
1
11/07/2217:45
11/09/2218:35
120-12-7
Benzo(a)anthracene
ND
ug/L
8.3
1
11/07/2217:45
11/09/2218:35
56-55-3
Benzo(a)pyrene
ND
ug/L
8.3
1
11/07/2217:45
11/09/2218:35
50-32-8
Benzo(b)fluoranthene
ND
ug/L
8.3
1
11/07/2217:45
11/09/2218:35
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
8.3
1
11/07/2217:45
11/09/2218:35
191-24-2
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 12/21 /2022 11:11 AM
without
the written consent of Pace Analytical Services,
LLC.
Page 13 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Sample: SWP-2 Lab ID: 92634407002 Collected: 11/02/22 12:45 Received: 11/02/22 16:45 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical
Services - Charlotte
Benzo(k)fluoranthene
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
207-08-9
Benzoic Acid
ND
ug/L
41.7
1
11/07/22 17:45
11/09/22 18:35
65-85-0
Benzyl alcohol
ND
ug/L
16.7
1
11/07/22 17:45
11/09/22 18:35
100-51-6
4-Bromophenylphenyl ether
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
101-55-3
Butylbenzylphthalate
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
59-50-7
4-Chloroaniline
ND
ug/L
16.7
1
11/07/22 17:45
11/09/22 18:35
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
111-44-4
2-Chloronaphthalene
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
91-58-7
2-Chlorophenol
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
7005-72-3
Chrysene
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
53-70-3
Dibenzofuran
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
132-64-9
1,2-Dichlorobenzene
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
95-50-1
1,3-Dichlorobenzene
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
541-73-1
1,4-Dichlorobenzene
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
16.7
1
11/07/22 17:45
11/09/22 18:35
91-94-1
2,4-Dichlorophenol
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
120-83-2
Diethylphthalate
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
84-66-2
2,4-Dimethylphenol
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
105-67-9
Dimethylphthalate
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
131-11-3
Di-n-butylphthalate
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
16.7
1
11/07/22 17:45
11/09/22 18:35
534-52-1
2,4-Dinitrophenol
ND
ug/L
41.7
1
11/07/22 17:45
11/09/22 18:35
51-28-5
2,4-Dinitrotoluene
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
121-14-2
2,6-Dinitrotoluene
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
606-20-2
Di-n-octylphthalate
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.0
1
11/07/22 17:45
11/09/22 18:35
117-81-7
Fluoranthene
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
206-44-0
Fluorene
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
87-68-3
Hexachlorobenzene
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
77-47-4
Hexachloroethane
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
193-39-5
Isophorone
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
78-59-1
1-Methylnaphthalene
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
90-12-0
2-Methylnaphthalene
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
15831-10-4
Naphthalene
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
91-20-3
2-Nitroaniline
ND
ug/L
16.7
1
11/07/22 17:45
11/09/22 18:35
88-74-4
3-Nitroaniline
ND
ug/L
16.7
1
11/07/22 17:45
11/09/22 18:35
99-09-2
4-Nitroaniline
ND
ug/L
16.7
1
11/07/22 17:45
11/09/22 18:35
100-01-6
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Sample: SWP-2 Lab ID: 92634407002 Collected: 11/02/22 12:45 Received: 11/02/22 16:45 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical
Services - Charlotte
Nitrobenzene
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
98-95-3
2-Nitrophenol
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
88-75-5
4-Nitrophenol
ND
ug/L
41.7
1
11/07/22 17:45
11/09/22 18:35
100-02-7
N-Nitrosodimethylamine
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
108-60-1
Pentachlorophenol
ND
ug/L
16.7
1
11/07/22 17:45
11/09/22 18:35
87-86-5
Phenanthrene
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
85-01-8
Phenol
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
108-95-2
Pyrene
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
120-82-1
2,4,5-Trichlorophenol
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
95-95-4
2,4,6-Trichlorophenol
ND
ug/L
8.3
1
11/07/22 17:45
11/09/22 18:35
88-06-2
Surrogates
Nitrobenzene-d5 (S)
34
%
10-144
1
11/07/22 17:45
11/09/22 18:35
4165-60-0
2-Fluorobiphenyl (S)
22
%
10-130
1
11/07/22 17:45
11/09/22 18:35
321-60-8
Terphenyl-d14 (S)
94
%
34-163
1
11/07/22 17:45
11/09/22 18:35
1718-51-0
Phenol-d6 (S)
23
%
10-130
1
11/07/22 17:45
11/09/22 18:35
13127-88-3
2-Fluorophenol (S)
27
%
10-130
1
11/07/22 17:45
11/09/22 18:35
367-12-4
2,4,6-Tribromophenol (S)
69
%
10-144
1
11/07/22 17:45
11/09/22 18:35
118-79-6
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
11/07/22 01:53
67-64-1
Benzene
ND
ug/L
1.0
1
11/07/22 01:53
71-43-2
Bromobenzene
ND
ug/L
1.0
1
11/07/22 01:53
108-86-1
Bromochloromethane
ND
ug/L
1.0
1
11/07/22 01:53
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
11/07/22 01:53
75-27-4
Bromoform
ND
ug/L
1.0
1
11/07/22 01:53
75-25-2
Bromomethane
ND
ug/L
2.0
1
11/07/22 01:53
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
11/07/22 01:53
78-93-3
Carbon tetrachloride
ND
ug/L
1.0
1
11/07/22 01:53
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
11/07/22 01:53
108-90-7
Chloroethane
ND
ug/L
1.0
1
11/07/22 01:53
75-00-3
Chloroform
ND
ug/L
1.0
1
11/07/22 01:53
67-66-3
Chloromethane
ND
ug/L
1.0
1
11/07/22 01:53
74-87-3
2-Chlorotoluene
ND
ug/L
1.0
1
11/07/22 01:53
95-49-8
4-Chlorotoluene
ND
ug/L
1.0
1
11/07/22 01:53
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
11/07/22 01:53
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
11/07/22 01:53
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
11/07/22 01:53
106-93-4
Dibromomethane
ND
ug/L
1.0
1
11/07/22 01:53
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
11/07/22 01:53
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.0
1
11/07/22 01:53
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
11/07/22 01:53
106-46-7
REPORT OF LABORATORY ANALYSIS
v2
v2
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Sample: SWP-2
Parameters
8260D MSV Low Level Landfill
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
ANALYTICAL RESULTS
Lab ID: 92634407002 Collected: 11/02/22 12:45 Received: 11/02/22 16:45 Matrix: Water
Results Units
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
96 %
86 %
102 %
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
ND ug/L
PQL DF Prepared Analyzed CAS No
1.0
1
11/07/22 01:53
75-71-8
1.0
1
11/07/22 01:53
75-34-3
1.0
1
11/07/22 01:53
107-06-2
1.0
1
11/07/22 01:53
75-35-4
1.0
1
11/07/22 01:53
156-59-2
1.0
1
11/07/22 01:53
156-60-5
1.0
1
11/07/22 01:53
78-87-5
1.0
1
11/07/22 01:53
142-28-9
1.0
1
11/07/22 01:53
594-20-7
1.0
1
11/07/22 01:53
563-58-6
1.0
1
11/07/22 01:53
10061-01-5
1.0
1
11/07/22 01:53
10061-02-6
1.0
1
11/07/22 01:53
108-20-3
1.0
1
11/07/22 01:53
100-41-4
2.0
1
11/07/22 01:53
87-68-3
5.0
1
11/07/22 01:53
591-78-6
1.0
1
11/07/22 01:53
99-87-6
5.0
1
11/07/22 01:53
75-09-2
5.0
1
11/07/22 01:53
108-10-1
1.0
1
11/07/22 01:53
1634-04-4
1.0
1
11/07/22 01:53
91-20-3
1.0
1
11/07/22 01:53
100-42-5
1.0
1
11/07/22 01:53
630-20-6
1.0
1
11/07/22 01:53
79-34-5
1.0
1
11/07/22 01:53
127-18-4
1.0
1
11/07/22 01:53
108-88-3
1.0
1
11/07/22 01:53
87-61-6
1.0
1
11/07/22 01:53
120-82-1
1.0
1
11/07/22 01:53
71-55-6
1.0
1
11/07/22 01:53
79-00-5
1.0
1
11/07/22 01:53
79-01-6
1.0
1
11/07/22 01:53
75-69-4
1.0
1
11/07/22 01:53
96-18-4
2.0
1
11/07/22 01:53
108-05-4
1.0
1
11/07/22 01:53
75-01-4
1.0
1
11/07/22 01:53
1330-20-7
2.0
1
11/07/22 01:53
179601-23-1
1.0
1
11/07/22 01:53
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
11/07/22 01:53 460-00-4
11/07/22 01:53 17060-07-0
11/07/22 01:53 2037-26-5
Qual
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 16 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Sample: SWP-2
Lab ID: 92634407002 Collected: 11/02/22 12:45
Received: 11/02/22 16:45 Matrix: Water
Parameters
Results Units PQL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
Surrogates
1,2-Dichloroethane-d4 (S)
110 % 70-130
1
11/03/22 14:48
17060-07-0
Toluene-d8 (S)
101 % 70-130
1
11/03/22 14:48
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
105 mg/L 5.0
1
11/03/22 17:06
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2015
Pace Analytical Services -Asheville
Total Dissolved Solids
116 mg/L 25.0
1
11/02/22 20:50
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Sulfate
2.5 mg/L 1.0
1
11/04/22 00:33
14808-79-8
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
2.7 mg/L 1.0
1
11/10/2217:19
16887-00-6
5310B TOC
Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
ND mg/L 1.0
1
11/04/22 00:27
7440-44-0
Date: 12/21 /2022 11:11 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Sample: Q06V09 Lab ID: 92634407003 Collected: 11/03/22 11:10 Received: 11/03/22 15:30 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Performed by
Pace
1
11/09/22 06:26
Collected By
M.Swann
1
11/09/22 06:26
Collected Date
11/3/22
1
11/09/22 06:26
Collected Time
11:10
1
11/09/22 06:26
pH
6.30
Std. Units
1
11/09/22 06:26
Temperature
15.9
deg C
1
11/09/22 06:26
Static Water Level
29.51
feet
1
11/09/22 06:26
Specific Conductance
1398
umhos/cm
1
11/09/22 06:26
Oxygen, Dissolved
3.91
mg/L
1
11/09/22 06:26
7782-44-7
Total Well Depth
69.80
feet
1
11/09/22 06:26
REDOX
-39.8
mV
1
11/09/22 06:26
Turbidity
15.85
NTU
1
11/09/22 06:26
Odor
No odor
1
11/09/22 06:26
Appearance
Clear
1
11/09/22 06:26
6010 MET ICP
Analytical Method: EPA 6010 Preparation
Method:
EPA 3010
Pace Analytical Services - Ormond Beach
Antimony
6.OJ
ug/L
15.0
1
12/04/22 18:12
12/08/22 02:37
7440-36-0
Arsenic
6.7J
ug/L
10.0
1
12/04/22 18:12
12/08/22 02:37
7440-38-2
Barium
294
ug/L
10.0
1
12/04/22 18:12
12/08/22 02:37
7440-39-3
Cadmium
ND
ug/L
1.0
1
12/04/22 18:12
12/08/22 02:37
7440-43-9
Calcium
171000
ug/L
500
1
12/04/22 18:12
12/08/22 02:37
7440-70-2
Chromium
ND
ug/L
5.0
1
12/04/22 18:12
12/08/22 02:37
7440-47-3
Cobalt
13.2
ug/L
10.0
1
12/04/22 18:12
12/08/22 02:37
7440-48-4
Copper
ND
ug/L
5.0
1
12/04/22 18:12
12/08/22 02:37
7440-50-8
Lead
ND
ug/L
10.0
1
12/04/22 18:12
12/08/22 02:37
7439-92-1
Magnesium
78800
ug/L
500
1
12/04/22 18:12
12/08/22 02:37
7439-95-4
Nickel
17.0
ug/L
5.0
1
12/04/22 18:12
12/08/22 02:37
7440-02-0
Potassium
4570
ug/L
1000
1
12/04/22 18:12
12/08/22 02:37
7440-09-7
Selenium
ND
ug/L
15.0
1
12/04/22 18:12
12/08/22 02:37
7782-49-2
Silver
ND
ug/L
5.0
1
12/04/22 18:12
12/08/22 02:37
7440-22-4
Sodium
30000
ug/L
2000
1
12/04/22 18:12
12/08/22 02:37
7440-23-5
Thallium
ND
ug/L
15.0
1
12/04/22 18:12
12/08/22 02:37
7440-28-0
Vanadium
ND
ug/L
10.0
1
12/04/22 18:12
12/08/22 02:37
7440-62-2
Zinc
ND
ug/L
20.0
1
12/04/22 18:12
12/08/22 02:37
7440-66-6
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Acenaphthene
ND
ug/L
8.3
1
11/09/2213:28
11/11/2217:18
83-32-9
Acenaphthylene
ND
ug/L
8.3
1
11/09/2213:28
11/11/2217:18
208-96-8
Aniline
ND
ug/L
8.3
1
11/09/2213:28
11/11/2217:18
62-53-3
Anthracene
ND
ug/L
8.3
1
11/09/2213:28
11/11/2217:18
120-12-7
Benzo(a)anthracene
ND
ug/L
8.3
1
11/09/2213:28
11/11/2217:18
56-55-3
Benzo(a)pyrene
ND
ug/L
8.3
1
11/09/2213:28
11/11/2217:18
50-32-8
Benzo(b)fluoranthene
ND
ug/L
8.3
1
11/09/2213:28
11/11/2217:18
205-99-2
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 12/21 /2022 11:11 AM
without
the written consent of Pace Analytical Services,
LLC.
Page 18 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Sample: Q06V09 Lab ID: 92634407003 Collected: 11/03/22 11:10 Received: 11/03/22 15:30 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical
Services - Charlotte
Benzo(g,h,i)perylene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
191-24-2
Benzo(k)fluoranthene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
207-08-9
Benzoic Acid
ND
ug/L
41.7
1
11/09/22 13:28
11/11/22 17:18
65-85-0
Benzyl alcohol
ND
ug/L
16.7
1
11/09/22 13:28
11/11/22 17:18
100-51-6
4-Bromophenylphenyl ether
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
101-55-3
Butylbenzylphthalate
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
59-50-7
4-Chloroaniline
ND
ug/L
16.7
1
11/09/22 13:28
11/11/22 17:18
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
111-44-4
2-Chloronaphthalene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
91-58-7
2-Chlorophenol
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
7005-72-3
Chrysene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
53-70-3
Dibenzofuran
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
132-64-9
1,2-Dichlorobenzene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
95-50-1
1,3-Dichlorobenzene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
541-73-1
1,4-Dichlorobenzene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
16.7
1
11/09/22 13:28
11/11/22 17:18
91-94-1
2,4-Dichlorophenol
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
120-83-2
Diethylphthalate
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
84-66-2
2,4-Dimethylphenol
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
105-67-9
Dimethylphthalate
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
131-11-3
Di-n-butylphthalate
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
16.7
1
11/09/22 13:28
11/11/22 17:18
534-52-1
2,4-Dinitrophenol
ND
ug/L
41.7
1
11/09/22 13:28
11/11/22 17:18
51-28-5
2,4-Dinitrotoluene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
121-14-2
2,6-Dinitrotoluene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
606-20-2
Di-n-octylphthalate
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.0
1
11/09/22 13:28
11/11/22 17:18
117-81-7
Fluoranthene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
206-44-0
Fluorene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
87-68-3
Hexachlorobenzene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
77-47-4
Hexachloroethane
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
193-39-5
Isophorone
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
78-59-1
1-Methylnaphthalene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
90-12-0
2-Methylnaphthalene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
15831-10-4
Naphthalene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
91-20-3
2-Nitroaniline
ND
ug/L
16.7
1
11/09/22 13:28
11/11/22 17:18
88-74-4
3-Nitroaniline
ND
ug/L
16.7
1
11/09/22 13:28
11/11/22 17:18
99-09-2
REPORT OF LABORATORY ANALYSIS
v1
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Sample: Q06V09 Lab ID: 92634407003 Collected: 11/03/22 11:10 Received: 11/03/22 15:30 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical
Services - Charlotte
4-Nitroaniline
ND
ug/L
16.7
1
11/09/22 13:28
11/11/22 17:18
100-01-6
Nitrobenzene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
98-95-3
2-Nitrophenol
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
88-75-5
4-Nitrophenol
ND
ug/L
41.7
1
11/09/22 13:28
11/11/22 17:18
100-02-7
N-Nitrosodimethylamine
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
108-60-1
Pentachlorophenol
ND
ug/L
16.7
1
11/09/22 13:28
11/11/22 17:18
87-86-5
Phenanthrene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
85-01-8
Phenol
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
108-95-2
Pyrene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
120-82-1
2,4,5-Trichlorophenol
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
95-95-4
2,4,6-Trichlorophenol
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:18
88-06-2
Surrogates
Nitrobenzene-d5 (S)
92
%
10-144
1
11/09/22 13:28
11/11/22 17:18
4165-60-0
2-Fluorobiphenyl (S)
88
%
10-130
1
11/09/22 13:28
11/11/22 17:18
321-60-8
Terphenyl-d14 (S)
123
%
34-163
1
11/09/22 13:28
11/11/22 17:18
1718-51-0
Phenol-d6 (S)
46
%
10-130
1
11/09/22 13:28
11/11/22 17:18
13127-88-3
2-Fluorophenol (S)
38
%
10-130
1
11/09/22 13:28
11/11/22 17:18
367-12-4
2,4,6-Tribromophenol (S)
54
%
10-144
1
11/09/22 13:28
11/11/22 17:18
118-79-6
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
11/07/22 02:12
67-64-1
Benzene
ND
ug/L
1.0
1
11/07/22 02:12
71-43-2
Bromobenzene
ND
ug/L
1.0
1
11/07/22 02:12
108-86-1
Bromochloromethane
ND
ug/L
1.0
1
11/07/22 02:12
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
11/07/22 02:12
75-27-4
Bromoform
ND
ug/L
1.0
1
11/07/22 02:12
75-25-2
Bromomethane
ND
ug/L
2.0
1
11/07/22 02:12
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
11/07/22 02:12
78-93-3
Carbon tetrachloride
ND
ug/L
1.0
1
11/07/22 02:12
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
11/07/22 02:12
108-90-7
Chloroethane
ND
ug/L
1.0
1
11/07/22 02:12
75-00-3
Chloroform
ND
ug/L
1.0
1
11/07/22 02:12
67-66-3
Chloromethane
ND
ug/L
1.0
1
11/07/22 02:12
74-87-3
2-Chlorotoluene
ND
ug/L
1.0
1
11/07/22 02:12
95-49-8
4-Chlorotoluene
ND
ug/L
1.0
1
11/07/22 02:12
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
11/07/22 02:12
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
11/07/22 02:12
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
11/07/22 02:12
106-93-4
Dibromomethane
ND
ug/L
1.0
1
11/07/22 02:12
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
11/07/22 02:12
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.0
1
11/07/22 02:12
541-73-1
REPORT OF LABORATORY ANALYSIS
v2
v2
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 20 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Sample: Q06V09 Lab ID: 92634407003 Collected: 11/03/22 11:10 Received: 11/03/22 15:30 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 12/21 /2022 11:11 AM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
96 %
90 %
103 %
1.0
1
11/07/22 02:12
106-46-7
1.0
1
11/07/22 02:12
75-71-8
1.0
1
11/07/22 02:12
75-34-3
1.0
1
11/07/22 02:12
107-06-2
1.0
1
11/07/22 02:12
75-35-4
1.0
1
11/07/22 02:12
156-59-2
1.0
1
11/07/22 02:12
156-60-5
1.0
1
11/07/22 02:12
78-87-5
1.0
1
11/07/22 02:12
142-28-9
1.0
1
11/07/22 02:12
594-20-7
1.0
1
11/07/22 02:12
563-58-6
1.0
1
11/07/22 02:12
10061-01-5
1.0
1
11/07/22 02:12
10061-02-6
1.0
1
11/07/22 02:12
108-20-3
1.0
1
11/07/22 02:12
100-41-4
2.0
1
11/07/22 02:12
87-68-3
5.0
1
11/07/22 02:12
591-78-6
1.0
1
11/07/22 02:12
99-87-6
5.0
1
11/07/22 02:12
75-09-2
5.0
1
11/07/22 02:12
108-10-1
1.0
1
11/07/22 02:12
1634-04-4
1.0
1
11/07/22 02:12
91-20-3
1.0
1
11/07/22 02:12
100-42-5
1.0
1
11/07/22 02:12
630-20-6
1.0
1
11/07/22 02:12
79-34-5
1.0
1
11/07/22 02:12
127-18-4
1.0
1
11/07/22 02:12
108-88-3
1.0
1
11/07/22 02:12
87-61-6
1.0
1
11/07/22 02:12
120-82-1
1.0
1
11/07/22 02:12
71-55-6
1.0
1
11/07/22 02:12
79-00-5
1.0
1
11/07/22 02:12
79-01-6
1.0
1
11/07/22 02:12
75-69-4
1.0
1
11/07/22 02:12
96-18-4
2.0
1
11/07/22 02:12
108-05-4
1.0
1
11/07/22 02:12
75-01-4
1.0
1
11/07/22 02:12
1330-20-7
2.0
1
11/07/22 02:12
179601-23-1
1.0
1
11/07/22 02:12
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
11/07/22 02:12 460-00-4
11/07/22 02:12 17060-07-0
11/07/22 02:12 2037-26-5
Page 21 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Sample: Q06V09
Lab ID: 92634407003 Collected: 11/03/22 11:10
Received: 11/03/22 15:30 Matrix: Water
Parameters
Results Units PQL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
1
11/06/22 23:11
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
94 % 70-130
1
11/06/22 23:11
17060-07-0
Toluene-d8(S)
99 % 70-130
1
11/06/22 23:11
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
828 mg/L 5.0
1
11/08/22 11:14
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2015
Pace Analytical Services -Asheville
Total Dissolved Solids
780 mg/L 50.0
1
11/07/22 10:16
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Sulfate
2.6 mg/L 1.0
1
11/05/22 22:14
14808-79-8
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
47.8 mg/L 3.0
3
11/10/2217:22
16887-00-6
5310B TOC
Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
4.1 mg/L 1.0
1
11/15/22 09:09
7440-44-0
Date: 12/21 /2022 11:11 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 22 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Sample: Q06V10 Lab ID: 92634407004 Collected: 11/03/22 10:20 Received: 11/03/22 15:30 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Performed by
Pace
1
11/09/22 10:06
Collected By
M.Swann
1
11/09/22 10:06
Collected Date
11/3/22
1
11/09/22 10:06
Collected Time
10:20
1
11/09/22 10:06
pH
5.52
Std. Units
1
11/09/22 10:06
Temperature
14.4
deg C
1
11/09/22 10:06
Static Water Level
28.18
feet
1
11/09/22 10:06
Specific Conductance
39.1
umhos/cm
1
11/09/22 10:06
Oxygen, Dissolved
8.98
mg/L
1
11/09/22 10:06
7782-44-7
Total Well Depth
32.30
feet
1
11/09/22 10:06
REDOX
35.0
mV
1
11/09/22 10:06
Turbidity
8.98
NTU
1
11/09/22 10:06
Odor
No odor
1
11/09/22 10:06
Appearance
Clear
1
11/09/22 10:06
6010 MET ICP
Analytical Method: EPA 6010 Preparation
Method:
EPA 3010
Pace Analytical Services - Ormond Beach
Antimony
ND
ug/L
15.0
1
12/04/22 18:12
12/08/22 02:40
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/04/22 18:12
12/08/22 02:40
7440-38-2
Barium
6.2J
ug/L
10.0
1
12/04/22 18:12
12/08/22 02:40
7440-39-3
Cadmium
ND
ug/L
1.0
1
12/04/22 18:12
12/08/22 02:40
7440-43-9
Calcium
2770
ug/L
500
1
12/04/22 18:12
12/08/22 02:40
7440-70-2
Chromium
ND
ug/L
5.0
1
12/04/22 18:12
12/08/22 02:40
7440-47-3
Cobalt
ND
ug/L
10.0
1
12/04/22 18:12
12/08/22 02:40
7440-48-4
Copper
ND
ug/L
5.0
1
12/04/22 18:12
12/08/22 02:40
7440-50-8
Lead
2.6J
ug/L
10.0
1
12/04/22 18:12
12/08/22 02:40
7439-92-1
Magnesium
995
ug/L
500
1
12/04/22 18:12
12/08/22 02:40
7439-95-4
Nickel
ND
ug/L
5.0
1
12/04/22 18:12
12/08/22 02:40
7440-02-0
Potassium
294J
ug/L
1000
1
12/04/22 18:12
12/08/22 02:40
7440-09-7
Selenium
ND
ug/L
15.0
1
12/04/22 18:12
12/08/22 02:40
7782-49-2
Silver
ND
ug/L
5.0
1
12/04/22 18:12
12/08/22 02:40
7440-22-4
Sodium
19801
ug/L
2000
1
12/04/22 18:12
12/08/22 02:40
7440-23-5
Thallium
ND
ug/L
15.0
1
12/04/22 18:12
12/08/22 02:40
7440-28-0
Vanadium
ND
ug/L
10.0
1
12/04/22 18:12
12/08/22 02:40
7440-62-2
Zinc
ND
ug/L
20.0
1
12/04/22 18:12
12/08/22 02:40
7440-66-6
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Acenaphthene
ND
ug/L
8.3
1
11/09/2213:28
11/11/2217:44
83-32-9
Acenaphthylene
ND
ug/L
8.3
1
11/09/2213:28
11/11/2217:44
208-96-8
Aniline
ND
ug/L
8.3
1
11/09/2213:28
11/11/2217:44
62-53-3
Anthracene
ND
ug/L
8.3
1
11/09/2213:28
11/11/2217:44
120-12-7
Benzo(a)anthracene
ND
ug/L
8.3
1
11/09/2213:28
11/11/2217:44
56-55-3
Benzo(a)pyrene
ND
ug/L
8.3
1
11/09/2213:28
11/11/2217:44
50-32-8
Benzo(b)fluoranthene
ND
ug/L
8.3
1
11/09/2213:28
11/11/2217:44
205-99-2
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 12/21 /2022 11:11 AM
without
the written consent of Pace Analytical Services,
LLC.
Page 23 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Sample: Q06V10 Lab ID: 92634407004 Collected: 11/03/22 10:20 Received: 11/03/22 15:30 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical
Services - Charlotte
Benzo(g,h,i)perylene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
191-24-2
Benzo(k)fluoranthene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
207-08-9
Benzoic Acid
ND
ug/L
41.7
1
11/09/22 13:28
11/11/22 17:44
65-85-0
Benzyl alcohol
ND
ug/L
16.7
1
11/09/22 13:28
11/11/22 17:44
100-51-6
4-Bromophenylphenyl ether
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
101-55-3
Butylbenzylphthalate
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
59-50-7
4-Chloroaniline
ND
ug/L
16.7
1
11/09/22 13:28
11/11/22 17:44
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
111-44-4
2-Chloronaphthalene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
91-58-7
2-Chlorophenol
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
7005-72-3
Chrysene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
53-70-3
Dibenzofuran
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
132-64-9
1,2-Dichlorobenzene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
95-50-1
1,3-Dichlorobenzene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
541-73-1
1,4-Dichlorobenzene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
16.7
1
11/09/22 13:28
11/11/22 17:44
91-94-1
2,4-Dichlorophenol
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
120-83-2
Diethylphthalate
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
84-66-2
2,4-Dimethylphenol
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
105-67-9
Dimethylphthalate
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
131-11-3
Di-n-butylphthalate
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
16.7
1
11/09/22 13:28
11/11/22 17:44
534-52-1
2,4-Dinitrophenol
ND
ug/L
41.7
1
11/09/22 13:28
11/11/22 17:44
51-28-5
2,4-Dinitrotoluene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
121-14-2
2,6-Dinitrotoluene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
606-20-2
Di-n-octylphthalate
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.0
1
11/09/22 13:28
11/11/22 17:44
117-81-7
Fluoranthene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
206-44-0
Fluorene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
87-68-3
Hexachlorobenzene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
77-47-4
Hexachloroethane
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
193-39-5
Isophorone
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
78-59-1
1-Methylnaphthalene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
90-12-0
2-Methylnaphthalene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
15831-10-4
Naphthalene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
91-20-3
2-Nitroaniline
ND
ug/L
16.7
1
11/09/22 13:28
11/11/22 17:44
88-74-4
3-Nitroaniline
ND
ug/L
16.7
1
11/09/22 13:28
11/11/22 17:44
99-09-2
REPORT OF LABORATORY ANALYSIS
v1
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 24 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Sample: Q06V10 Lab ID: 92634407004 Collected: 11/03/22 10:20 Received: 11/03/22 15:30 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical
Services - Charlotte
4-Nitroaniline
ND
ug/L
16.7
1
11/09/22 13:28
11/11/22 17:44
100-01-6
Nitrobenzene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
98-95-3
2-Nitrophenol
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
88-75-5
4-Nitrophenol
ND
ug/L
41.7
1
11/09/22 13:28
11/11/22 17:44
100-02-7
N-Nitrosodimethylamine
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
108-60-1
Pentachlorophenol
ND
ug/L
16.7
1
11/09/22 13:28
11/11/22 17:44
87-86-5
Phenanthrene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
85-01-8
Phenol
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
108-95-2
Pyrene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
120-82-1
2,4,5-Trichlorophenol
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
95-95-4
2,4,6-Trichlorophenol
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 17:44
88-06-2
Surrogates
Nitrobenzene-d5 (S)
104
%
10-144
1
11/09/22 13:28
11/11/22 17:44
4165-60-0
2-Fluorobiphenyl (S)
104
%
10-130
1
11/09/22 13:28
11/11/22 17:44
321-60-8
Terphenyl-d14 (S)
121
%
34-163
1
11/09/22 13:28
11/11/22 17:44
1718-51-0
Phenol-d6 (S)
46
%
10-130
1
11/09/22 13:28
11/11/22 17:44
13127-88-3
2-Fluorophenol (S)
65
%
10-130
1
11/09/22 13:28
11/11/22 17:44
367-12-4
2,4,6-Tribromophenol (S)
98
%
10-144
1
11/09/22 13:28
11/11/22 17:44
118-79-6
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
11/07/22 02:30
67-64-1
Benzene
ND
ug/L
1.0
1
11/07/22 02:30
71-43-2
Bromobenzene
ND
ug/L
1.0
1
11/07/22 02:30
108-86-1
Bromochloromethane
ND
ug/L
1.0
1
11/07/22 02:30
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
11/07/22 02:30
75-27-4
Bromoform
ND
ug/L
1.0
1
11/07/22 02:30
75-25-2
Bromomethane
ND
ug/L
2.0
1
11/07/22 02:30
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
11/07/22 02:30
78-93-3
Carbon tetrachloride
ND
ug/L
1.0
1
11/07/22 02:30
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
11/07/22 02:30
108-90-7
Chloroethane
ND
ug/L
1.0
1
11/07/22 02:30
75-00-3
Chloroform
ND
ug/L
1.0
1
11/07/22 02:30
67-66-3
Chloromethane
ND
ug/L
1.0
1
11/07/22 02:30
74-87-3
2-Chlorotoluene
ND
ug/L
1.0
1
11/07/22 02:30
95-49-8
4-Chlorotoluene
ND
ug/L
1.0
1
11/07/22 02:30
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
11/07/22 02:30
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
11/07/22 02:30
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
11/07/22 02:30
106-93-4
Dibromomethane
ND
ug/L
1.0
1
11/07/22 02:30
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
11/07/22 02:30
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.0
1
11/07/22 02:30
541-73-1
REPORT OF LABORATORY ANALYSIS
v2
v2
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 25 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Sample: Q06V10 Lab ID: 92634407004 Collected: 11/03/22 10:20 Received: 11/03/22 15:30 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 12/21 /2022 11:11 AM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
95 %
85 %
104 %
1.0
1
11/07/22 02:30
106-46-7
1.0
1
11/07/22 02:30
75-71-8
1.0
1
11/07/22 02:30
75-34-3
1.0
1
11/07/22 02:30
107-06-2
1.0
1
11/07/22 02:30
75-35-4
1.0
1
11/07/22 02:30
156-59-2
1.0
1
11/07/22 02:30
156-60-5
1.0
1
11/07/22 02:30
78-87-5
1.0
1
11/07/22 02:30
142-28-9
1.0
1
11/07/22 02:30
594-20-7
1.0
1
11/07/22 02:30
563-58-6
1.0
1
11/07/22 02:30
10061-01-5
1.0
1
11/07/22 02:30
10061-02-6
1.0
1
11/07/22 02:30
108-20-3
1.0
1
11/07/22 02:30
100-41-4
2.0
1
11/07/22 02:30
87-68-3
5.0
1
11/07/22 02:30
591-78-6
1.0
1
11/07/22 02:30
99-87-6
5.0
1
11/07/22 02:30
75-09-2
5.0
1
11/07/22 02:30
108-10-1
1.0
1
11/07/22 02:30
1634-04-4
1.0
1
11/07/22 02:30
91-20-3
1.0
1
11/07/22 02:30
100-42-5
1.0
1
11/07/22 02:30
630-20-6
1.0
1
11/07/22 02:30
79-34-5
1.0
1
11/07/22 02:30
127-18-4
1.0
1
11/07/22 02:30
108-88-3
1.0
1
11/07/22 02:30
87-61-6
1.0
1
11/07/22 02:30
120-82-1
1.0
1
11/07/22 02:30
71-55-6
1.0
1
11/07/22 02:30
79-00-5
1.0
1
11/07/22 02:30
79-01-6
1.0
1
11/07/22 02:30
75-69-4
1.0
1
11/07/22 02:30
96-18-4
2.0
1
11/07/22 02:30
108-05-4
1.0
1
11/07/22 02:30
75-01-4
1.0
1
11/07/22 02:30
1330-20-7
2.0
1
11/07/22 02:30
179601-23-1
1.0
1
11/07/22 02:30
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
11/07/22 02:30 460-00-4
11/07/22 02:30 17060-07-0
11/07/22 02:30 2037-26-5
Page 26 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Sample: Q06V10
Lab ID: 92634407004 Collected: 11/03/22 10:20
Received: 11/03/22 15:30 Matrix: Water
Parameters
Results Units PQL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
1
11/06/22 17:28
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
90 % 70-130
1
11/06/22 17:28
17060-07-0
Toluene-d8 (S)
94 % 70-130
1
11/06/22 17:28
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
10.3 mg/L 5.0
1
11/05/22 14:22
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2015
Pace Analytical Services -Asheville
Total Dissolved Solids
33.0 mg/L 25.0
1
11/07/22 10:20
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Sulfate
1.0 mg/L 1.0
1
11/05/22 22:30
14808-79-8
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
1.5 mg/L 1.0
1
11/10/2217:23
16887-00-6
5310B TOC
Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
ND mg/L 1.0
1
11/15/22 09:29
7440-44-0
Date: 12/21 /2022 11:11 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 27 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Sample: Q06V11 Lab ID: 92634407005 Collected: 11/03/22 10:35 Received: 11/03/22 15:30 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Performed by
Pace
1
11/09/22 10:08
Collected By
M.Swann
1
11/09/22 10:08
Collected Date
11/3/22
1
11/09/22 10:08
Collected Time
10:35
1
11/09/22 10:08
pH
5.51
Std. Units
1
11/09/22 10:08
Temperature
13.8
deg C
1
11/09/22 10:08
Static Water Level
40.80
feet
1
11/09/22 10:08
Specific Conductance
68.3
umhos/cm
1
11/09/22 10:08
Oxygen, Dissolved
10.15
mg/L
1
11/09/22 10:08
7782-44-7
Total Well Depth
56.90
feet
1
11/09/22 10:08
REDOX
-12.1
mV
1
11/09/22 10:08
Turbidity
10.15
NTU
1
11/09/22 10:08
Odor
No odor
1
11/09/22 10:08
Appearance
Clear
1
11/09/22 10:08
6010 MET ICP
Analytical Method: EPA 6010 Preparation
Method:
EPA 3010
Pace Analytical Services - Ormond Beach
Antimony
ND
ug/L
15.0
1
12/04/22 18:12
12/08/22 02:52
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/04/22 18:12
12/08/22 02:52
7440-38-2
Barium
7.1J
ug/L
10.0
1
12/04/22 18:12
12/08/22 02:52
7440-39-3
Cadmium
ND
ug/L
1.0
1
12/04/22 18:12
12/08/22 02:52
7440-43-9
Calcium
4700
ug/L
500
1
12/04/22 18:12
12/08/22 02:52
7440-70-2
Chromium
ND
ug/L
5.0
1
12/04/22 18:12
12/08/22 02:52
7440-47-3
Cobalt
ND
ug/L
10.0
1
12/04/22 18:12
12/08/22 02:52
7440-48-4
Copper
2.7J
ug/L
5.0
1
12/04/22 18:12
12/08/22 02:52
7440-50-8
Lead
ND
ug/L
10.0
1
12/04/22 18:12
12/08/22 02:52
7439-92-1
Magnesium
2260
ug/L
500
1
12/04/22 18:12
12/08/22 02:52
7439-95-4
Nickel
1.7J
ug/L
5.0
1
12/04/22 18:12
12/08/22 02:52
7440-02-0
Potassium
653J
ug/L
1000
1
12/04/22 18:12
12/08/22 02:52
7440-09-7
Selenium
ND
ug/L
15.0
1
12/04/22 18:12
12/08/22 02:52
7782-49-2
Silver
ND
ug/L
5.0
1
12/04/22 18:12
12/08/22 02:52
7440-22-4
Sodium
4100
ug/L
2000
1
12/04/22 18:12
12/08/22 02:52
7440-23-5
Thallium
ND
ug/L
15.0
1
12/04/22 18:12
12/08/22 02:52
7440-28-0
Vanadium
ND
ug/L
10.0
1
12/04/22 18:12
12/08/22 02:52
7440-62-2
Zinc
ND
ug/L
20.0
1
12/04/22 18:12
12/08/22 02:52
7440-66-6
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Acenaphthene
ND
ug/L
8.3
1
11/09/2213:28
11/11/2218:09
83-32-9
Acenaphthylene
ND
ug/L
8.3
1
11/09/2213:28
11/11/2218:09
208-96-8
Aniline
ND
ug/L
8.3
1
11/09/2213:28
11/11/2218:09
62-53-3
Anthracene
ND
ug/L
8.3
1
11/09/2213:28
11/11/2218:09
120-12-7
Benzo(a)anthracene
ND
ug/L
8.3
1
11/09/2213:28
11/11/2218:09
56-55-3
Benzo(a)pyrene
ND
ug/L
8.3
1
11/09/2213:28
11/11/2218:09
50-32-8
Benzo(b)fluoranthene
ND
ug/L
8.3
1
11/09/2213:28
11/11/2218:09
205-99-2
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 12/21 /2022 11:11 AM
without
the written consent of Pace Analytical Services,
LLC.
Page 28 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Sample: Q06V11 Lab ID: 92634407005 Collected: 11/03/22 10:35 Received: 11/03/22 15:30 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical
Services - Charlotte
Benzo(g,h,i)perylene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
191-24-2
Benzo(k)fluoranthene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
207-08-9
Benzoic Acid
ND
ug/L
41.7
1
11/09/22 13:28
11/11/22 18:09
65-85-0
Benzyl alcohol
ND
ug/L
16.7
1
11/09/22 13:28
11/11/22 18:09
100-51-6
4-Bromophenylphenyl ether
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
101-55-3
Butylbenzylphthalate
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
59-50-7
4-Chloroaniline
ND
ug/L
16.7
1
11/09/22 13:28
11/11/22 18:09
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
111-44-4
2-Chloronaphthalene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
91-58-7
2-Chlorophenol
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
7005-72-3
Chrysene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
53-70-3
Dibenzofuran
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
132-64-9
1,2-Dichlorobenzene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
95-50-1
1,3-Dichlorobenzene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
541-73-1
1,4-Dichlorobenzene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
16.7
1
11/09/22 13:28
11/11/22 18:09
91-94-1
2,4-Dichlorophenol
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
120-83-2
Diethylphthalate
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
84-66-2
2,4-Dimethylphenol
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
105-67-9
Dimethylphthalate
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
131-11-3
Di-n-butylphthalate
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
16.7
1
11/09/22 13:28
11/11/22 18:09
534-52-1
2,4-Dinitrophenol
ND
ug/L
41.7
1
11/09/22 13:28
11/11/22 18:09
51-28-5
2,4-Dinitrotoluene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
121-14-2
2,6-Dinitrotoluene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
606-20-2
Di-n-octylphthalate
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.0
1
11/09/22 13:28
11/11/22 18:09
117-81-7
Fluoranthene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
206-44-0
Fluorene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
87-68-3
Hexachlorobenzene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
77-47-4
Hexachloroethane
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
193-39-5
Isophorone
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
78-59-1
1-Methylnaphthalene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
90-12-0
2-Methylnaphthalene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
15831-10-4
Naphthalene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
91-20-3
2-Nitroaniline
ND
ug/L
16.7
1
11/09/22 13:28
11/11/22 18:09
88-74-4
3-Nitroaniline
ND
ug/L
16.7
1
11/09/22 13:28
11/11/22 18:09
99-09-2
REPORT OF LABORATORY ANALYSIS
v1
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 29 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Sample: Q06V11 Lab ID: 92634407005 Collected: 11/03/22 10:35 Received: 11/03/22 15:30 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical
Services - Charlotte
4-Nitroaniline
ND
ug/L
16.7
1
11/09/22 13:28
11/11/22 18:09
100-01-6
Nitrobenzene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
98-95-3
2-Nitrophenol
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
88-75-5
4-Nitrophenol
ND
ug/L
41.7
1
11/09/22 13:28
11/11/22 18:09
100-02-7
N-Nitrosodimethylamine
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
108-60-1
Pentachlorophenol
ND
ug/L
16.7
1
11/09/22 13:28
11/11/22 18:09
87-86-5
Phenanthrene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
85-01-8
Phenol
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
108-95-2
Pyrene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
120-82-1
2,4,5-Trichlorophenol
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
95-95-4
2,4,6-Trichlorophenol
ND
ug/L
8.3
1
11/09/22 13:28
11/11/22 18:09
88-06-2
Surrogates
Nitrobenzene-d5 (S)
99
%
10-144
1
11/09/22 13:28
11/11/22 18:09
4165-60-0
2-Fluorobiphenyl (S)
91
%
10-130
1
11/09/22 13:28
11/11/22 18:09
321-60-8
Terphenyl-d14 (S)
124
%
34-163
1
11/09/22 13:28
11/11/22 18:09
1718-51-0
Phenol-d6 (S)
43
%
10-130
1
11/09/22 13:28
11/11/22 18:09
13127-88-3
2-Fluorophenol (S)
60
%
10-130
1
11/09/22 13:28
11/11/22 18:09
367-12-4
2,4,6-Tribromophenol (S)
101
%
10-144
1
11/09/22 13:28
11/11/22 18:09
118-79-6
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
11/07/22 02:48
67-64-1
Benzene
ND
ug/L
1.0
1
11/07/22 02:48
71-43-2
Bromobenzene
ND
ug/L
1.0
1
11/07/22 02:48
108-86-1
Bromochloromethane
ND
ug/L
1.0
1
11/07/22 02:48
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
11/07/22 02:48
75-27-4
Bromoform
ND
ug/L
1.0
1
11/07/22 02:48
75-25-2
Bromomethane
ND
ug/L
2.0
1
11/07/22 02:48
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
11/07/22 02:48
78-93-3
Carbon tetrachloride
ND
ug/L
1.0
1
11/07/22 02:48
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
11/07/22 02:48
108-90-7
Chloroethane
ND
ug/L
1.0
1
11/07/22 02:48
75-00-3
Chloroform
ND
ug/L
1.0
1
11/07/22 02:48
67-66-3
Chloromethane
ND
ug/L
1.0
1
11/07/22 02:48
74-87-3
2-Chlorotoluene
ND
ug/L
1.0
1
11/07/22 02:48
95-49-8
4-Chlorotoluene
ND
ug/L
1.0
1
11/07/22 02:48
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
11/07/22 02:48
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
11/07/22 02:48
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
11/07/22 02:48
106-93-4
Dibromomethane
ND
ug/L
1.0
1
11/07/22 02:48
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
11/07/22 02:48
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.0
1
11/07/22 02:48
541-73-1
REPORT OF LABORATORY ANALYSIS
v2
v2
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 30 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Sample: Q06V11 Lab ID: 92634407005 Collected: 11/03/22 10:35 Received: 11/03/22 15:30 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 12/21 /2022 11:11 AM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
97 %
90 %
106 %
1.0
1
11/07/22 02:48
106-46-7
1.0
1
11/07/22 02:48
75-71-8
1.0
1
11/07/22 02:48
75-34-3
1.0
1
11/07/22 02:48
107-06-2
1.0
1
11/07/22 02:48
75-35-4
1.0
1
11/07/22 02:48
156-59-2
1.0
1
11/07/22 02:48
156-60-5
1.0
1
11/07/22 02:48
78-87-5
1.0
1
11/07/22 02:48
142-28-9
1.0
1
11/07/22 02:48
594-20-7
1.0
1
11/07/22 02:48
563-58-6
1.0
1
11/07/22 02:48
10061-01-5
1.0
1
11/07/22 02:48
10061-02-6
1.0
1
11/07/22 02:48
108-20-3
1.0
1
11/07/22 02:48
100-41-4
2.0
1
11/07/22 02:48
87-68-3
5.0
1
11/07/22 02:48
591-78-6
1.0
1
11/07/22 02:48
99-87-6
5.0
1
11/07/22 02:48
75-09-2
5.0
1
11/07/22 02:48
108-10-1
1.0
1
11/07/22 02:48
1634-04-4
1.0
1
11/07/22 02:48
91-20-3
1.0
1
11/07/22 02:48
100-42-5
1.0
1
11/07/22 02:48
630-20-6
1.0
1
11/07/22 02:48
79-34-5
1.0
1
11/07/22 02:48
127-18-4
1.0
1
11/07/22 02:48
108-88-3
1.0
1
11/07/22 02:48
87-61-6
1.0
1
11/07/22 02:48
120-82-1
1.0
1
11/07/22 02:48
71-55-6
1.0
1
11/07/22 02:48
79-00-5
1.0
1
11/07/22 02:48
79-01-6
1.0
1
11/07/22 02:48
75-69-4
1.0
1
11/07/22 02:48
96-18-4
2.0
1
11/07/22 02:48
108-05-4
1.0
1
11/07/22 02:48
75-01-4
1.0
1
11/07/22 02:48
1330-20-7
2.0
1
11/07/22 02:48
179601-23-1
1.0
1
11/07/22 02:48
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
11/07/22 02:48 460-00-4
11/07/22 02:48 17060-07-0
11/07/22 02:48 2037-26-5
Page 31 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Sample: Q06V11
Lab ID: 92634407005 Collected: 11/03/22 10:35
Received: 11/03/22 15:30 Matrix: Water
Parameters
Results Units PQL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
1
11/06/22 17:47
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
86 % 70-130
1
11/06/22 17:47
17060-07-0
Toluene-d8 (S)
96 % 70-130
1
11/06/22 17:47
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
23.9 mg/L 5.0
1
11/05/22 14:27
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2015
Pace Analytical Services -Asheville
Total Dissolved Solids
48.0 mg/L 25.0
1
11/07/22 10:20
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Sulfate
3.1 mg/L 1.0
1
11/05/22 23:17
14808-79-8
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
1.5 mg/L 1.0
1
11/10/2217:26
16887-00-6
5310B TOC
Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
ND mg/L 1.0
1
11/15/22 09:48
7440-44-0
Date: 12/21 /2022 11:11 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 32 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
QC Batch: 876516 Analysis Method: EPA 6010
QC Batch Method: EPA 3010 Analysis Description: 6010 MET
Laboratory: Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92634407001, 92634407002, 92634407003, 92634407004, 92634407005
METHOD BLANK: 4822741 Matrix: Water
Associated Lab Samples: 92634407001, 92634407002, 92634407003, 92634407004, 92634407005
Blank Reporting
Parameter Units Result Limit Analyzed
Antimony
ug/L
ND
15.0
12/08/22 01:03
Arsenic
ug/L
ND
10.0
12/08/22 01:03
Barium
ug/L
ND
10.0
12/08/22 01:03
Cadmium
ug/L
ND
1.0
12/08/22 01:03
Calcium
ug/L
ND
500
12/08/22 01:03
Chromium
ug/L
ND
5.0
12/08/22 01:03
Cobalt
ug/L
ND
10.0
12/08/22 01:03
Copper
ug/L
ND
5.0
12/08/22 01:03
Lead
ug/L
ND
10.0
12/08/22 01:03
Magnesium
ug/L
ND
500
12/08/22 01:03
Nickel
ug/L
ND
5.0
12/08/22 01:03
Potassium
ug/L
ND
1000
12/08/22 01:03
Selenium
ug/L
ND
15.0
12/08/22 01:03
Silver
ug/L
ND
5.0
12/08/22 01:03
Sodium
ug/L
ND
2000
12/08/22 01:03
Thallium
ug/L
ND
15.0
12/08/22 01:03
Vanadium
ug/L
ND
10.0
12/08/22 01:03
Zinc
ug/L
ND
20.0
12/08/22 01:03
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
4822742
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
250
257
103
80-120
Arsenic
ug/L
250
251
101
80-120
Barium
ug/L
250
263
105
80-120
Cadmium
ug/L
25
26.5
106
80-120
Calcium
ug/L
12500
13100
105
80-120
Chromium
ug/L
250
260
104
80-120
Cobalt
ug/L
250
262
105
80-120
Copper
ug/L
250
256
102
80-120
Lead
ug/L
250
266
106
80-120
Magnesium
ug/L
12500
13200
105
80-120
Nickel
ug/L
250
261
105
80-120
Potassium
ug/L
12500
12200
97
80-120
Selenium
ug/L
250
262
105
80-120
Silver
ug/L
25
26.2
105
80-120
Sodium
ug/L
12500
12200
98
80-120
Thallium
ug/L
250
261
104
80-120
Vanadium
ug/L
250
257
103
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 33 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
LABORATORY CONTROL SAMPLE: 4822742
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits
Zinc ug/L 1250 1310 105 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
4822743
MS
92634409001
Spike
Parameter
Units
Result
Conc.
Antimony
ug/L
ND
250
Arsenic
ug/L
ND
250
Barium
ug/L
37.0
250
Cadmium
ug/L
ND
25
Calcium
ug/L
7720
12500
Chromium
ug/L
ND
250
Cobalt
ug/L
ND
250
Copper
ug/L
ND
250
Lead
ug/L
ND
250
Magnesium
ug/L
3140
12500
Nickel
ug/L
ND
250
Potassium
ug/L
2050
12500
Selenium
ug/L
ND
250
Silver
ug/L
ND
25
Sodium
ug/L
3290
12500
Thallium
ug/L
ND
250
Vanadium
ug/L
1.8J
250
Zinc
ug/L
ND
1250
Qualifiers
4822744
MSD
Spike
MS
MSD
MS
MSD
% Rec
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
250
256
256
102
102
75-125
0
250
249
251
99
100
75-125
1
250
302
297
106
104
75-125
2
25
26.4
26.5
106
106
75-125
0
12500
20700
20400
104
101
75-125
2
250
261
262
104
104
75-125
0
250
262
264
105
105
75-125
1
250
257
258
102
103
75-125
0
250
264
267
105
107
75-125
1
12500
16300
16000
105
103
75-125
2
250
260
261
104
104
75-125
0
12500
14600
14300
100
98
75-125
2
250
260
260
104
104
75-125
0
25
26.1
26.3
103
103
75-125
1
12500
15800
15500
100
98
75-125
2
250
260
263
104
105
75-125
1
250
258
259
103
103
75-125
0
1250
1310
1320
104
105
75-125
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC.
Qual
Page 34 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
QC Batch: 735210 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92634407001, 92634407002, 92634407003, 92634407004, 92634407005
METHOD BLANK: 3826560 Matrix: Water
Associated Lab Samples: 92634407001, 92634407002, 92634407003, 92634407004, 92634407005
Blank Reporting
Parameter Units Result Limit Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
11/07/22 00:05
1,1,1-Trichloroethane
ug/L
ND
1.0
11/07/22 00:05
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
11/07/22 00:05
1,1,2-Trichloroethane
ug/L
ND
1.0
11/07/22 00:05
1,1-Dichloroethane
ug/L
ND
1.0
11/07/22 00:05
1,1-Dichloroethene
ug/L
ND
1.0
11/07/22 00:05
1,1-Dichloropropene
ug/L
ND
1.0
11/07/22 00:05
1,2,3-Trichlorobenzene
ug/L
ND
1.0
11/07/22 00:05
1,2,3-Trichloropropane
ug/L
ND
1.0
11/07/22 00:05
1,2,4-Trichlorobenzene
ug/L
ND
1.0
11/07/22 00:05
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
11/07/22 00:05
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
11/07/22 00:05
1,2-Dichlorobenzene
ug/L
ND
1.0
11/07/22 00:05
1,2-Dichloroethane
ug/L
ND
1.0
11/07/22 00:05
1,2-Dichloropropane
ug/L
ND
1.0
11/07/22 00:05
1,3-Dichlorobenzene
ug/L
ND
1.0
11/07/22 00:05
1,3-Dichloropropane
ug/L
ND
1.0
11/07/22 00:05
1,4-Dichlorobenzene
ug/L
ND
1.0
11/07/22 00:05
2,2-Dichloropropane
ug/L
ND
1.0
11/07/22 00:05
2-Butanone (MEK)
ug/L
ND
5.0
11/07/22 00:05
2-Chlorotoluene
ug/L
ND
1.0
11/07/22 00:05
2-Hexanone
ug/L
ND
5.0
11/07/22 00:05
4-Chlorotoluene
ug/L
ND
1.0
11/07/22 00:05
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
11/07/22 00:05
Acetone
ug/L
ND
25.0
11/07/22 00:05
Benzene
ug/L
ND
1.0
11/07/22 00:05
Bromobenzene
ug/L
ND
1.0
11/07/22 00:05
Bromochloromethane
ug/L
ND
1.0
11/07/22 00:05
Bromodichloromethane
ug/L
ND
1.0
11/07/22 00:05
Bromoform
ug/L
ND
1.0
11/07/22 00:05
Bromomethane
ug/L
ND
2.0
11/07/22 00:05
Carbon tetrachloride
ug/L
ND
1.0
11/07/22 00:05
Chlorobenzene
ug/L
ND
1.0
11/07/22 00:05
Chloroethane
ug/L
ND
1.0
11/07/22 00:05
Chloroform
ug/L
ND
1.0
11/07/22 00:05
Chloromethane
ug/L
ND
1.0
11/07/22 00:05
cis-1,2-Dichloroethene
ug/L
ND
1.0
11/07/22 00:05
cis-1,3-Dichloropropene
ug/L
ND
1.0
11/07/22 00:05
Dibromochloromethane
ug/L
ND
1.0
11/07/22 00:05
Dibromomethane
ug/L
ND
1.0
11/07/22 00:05
v2
v2
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 35 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
METHOD BLANK: 3826560 Matrix: Water
Associated Lab Samples: 92634407001, 92634407002, 92634407003, 92634407004, 92634407005
Blank Reporting
Parameter Units Result Limit Analyzed
Dichlorodifluoromethane
ug/L
ND
1.0
11/07/22 00:05
Diisopropyl ether
ug/L
ND
1.0
11/07/22 00:05
Ethylbenzene
ug/L
ND
1.0
11/07/22 00:05
Hexachloro-1,3-butadiene
ug/L
ND
2.0
11/07/22 00:05
m&p-Xylene
ug/L
ND
2.0
11/07/22 00:05
Methyl-tert-butyl ether
ug/L
ND
1.0
11/07/22 00:05
Methylene Chloride
ug/L
ND
5.0
11/07/22 00:05
Naphthalene
ug/L
ND
1.0
11/07/22 00:05
o-Xylene
ug/L
ND
1.0
11/07/22 00:05
p-Isopropyltoluene
ug/L
ND
1.0
11/07/22 00:05
Styrene
ug/L
ND
1.0
11/07/22 00:05
Tetrachloroethene
ug/L
ND
1.0
11/07/22 00:05
Toluene
ug/L
ND
1.0
11/07/22 00:05
trans-1,2-Dichloroethene
ug/L
ND
1.0
11/07/22 00:05
trans- 1,3-Dichloropropene
ug/L
ND
1.0
11/07/22 00:05
Trichloroethene
ug/L
ND
1.0
11/07/22 00:05
Trichlorofluoromethane
ug/L
ND
1.0
11/07/22 00:05
Vinyl acetate
ug/L
ND
2.0
11/07/22 00:05
Vinyl chloride
ug/L
ND
1.0
11/07/22 00:05
Xylene (Total)
ug/L
ND
1.0
11/07/22 00:05
1,2-Dichloroethane-d4 (S)
%
87
70-130
11/07/22 00:05
4-Bromofluorobenzene (S)
%
96
70-130
11/07/22 00:05
Toluene-d8 (S)
%
101
70-130
11/07/22 00:05
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3826561
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
56.1
112
70-130
1,1,1-Trichloroethane
ug/L
50
52.1
104
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
53.1
106
70-130
1,1,2-Trichloroethane
ug/L
50
55.1
110
70-130
1,1-Dichloroethane
ug/L
50
51.4
103
70-130
1,1-Dichloroethene
ug/L
50
51.1
102
70-130
1,1-Dichloropropene
ug/L
50
55.6
111
70-130
1,2,3-Trichlorobenzene
ug/L
50
54.9
110
70-130
1,2,3-Trichloropropane
ug/L
50
52.2
104
70-130
1,2,4-Trichlorobenzene
ug/L
50
55.3
111
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
50.1
100
70-131
1,2-Dibromoethane (EDB)
ug/L
50
56.6
113
70-130
1,2-Dichlorobenzene
ug/L
50
55.1
110
70-130
1,2-Dichloroethane
ug/L
50
49.4
99
70-130
1,2-Dichloropropane
ug/L
50
56.4
113
70-130
1,3-Dichlorobenzene
ug/L
50
54.4
109
70-130
1,3-Dichloropropane
ug/L
50
54.4
109
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 36 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
LABORATORY CONTROL SAMPLE:
Parameter
3826561
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,4-Dichlorobenzene
ug/L
50
54.9
110
70-130
2,2-Dichloropropane
ug/L
50
49.5
99
68-135
2-Butanone (MEK)
ug/L
100
100
100
70-134
2-Chlorotoluene
ug/L
50
50.6
101
70-130
2-Hexanone
ug/L
100
95.9
96
70-131
4-Chlorotoluene
ug/L
50
50.6
101
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
97.6
98
70-130
Acetone
ug/L
100
91.7
92
70-133
Benzene
ug/L
50
53.8
108
70-130
Bromobenzene
ug/L
50
54.5
109
70-130
Bromochloromethane
ug/L
50
57.8
116
70-130
Bromodichloromethane
ug/L
50
52.4
105
70-130
Bromoform
ug/L
50
54.4
109
70-130
Bromomethane
ug/L
50
37.3
75
45-151 v3
Carbon tetrachloride
ug/L
50
52.3
105
70-130
Chlorobenzene
ug/L
50
55.4
111
70-130
Chloroethane
ug/L
50
36.0
72
39-152 v3
Chloroform
ug/L
50
50.7
101
70-130
Chloromethane
ug/L
50
50.2
100
58-130
cis-1,2-Dichloroethene
ug/L
50
51.8
104
70-130
cis-1,3-Dichloropropene
ug/L
50
55.3
111
70-130
Dibromochloromethane
ug/L
50
54.8
110
70-130
Dibromomethane
ug/L
50
56.3
113
70-130
Dichlorodifluoromethane
ug/L
50
52.2
104
54-133
Diisopropyl ether
ug/L
50
53.1
106
70-130
Ethylbenzene
ug/L
50
53.1
106
70-130
Hexachloro-1,3-butadiene
ug/L
50
53.7
107
70-135
m&p-Xylene
ug/L
100
108
108
70-130
Methyl-tert-butyl ether
ug/L
50
54.5
109
70-130
Methylene Chloride
ug/L
50
48.7
97
66-130
Naphthalene
ug/L
50
55.5
111
70-130
o-Xylene
ug/L
50
54.5
109
70-130
p-Isopropyltoluene
ug/L
50
52.4
105
70-130
Styrene
ug/L
50
55.5
111
70-130
Tetrachloroethene
ug/L
50
55.5
111
70-130
Toluene
ug/L
50
54.7
109
70-130
trans-1,2-Dichloroethene
ug/L
50
52.8
106
70-130
trans- 1,3-Dichloropropene
ug/L
50
54.1
108
70-130
Trichloroethene
ug/L
50
58.7
117
70-130
Trichlorofluoromethane
ug/L
50
44.0
88
62-130
Vinyl acetate
ug/L
100
107
107
70-144
Vinyl chloride
ug/L
50
53.5
107
62-130
Xylene (Total)
ug/L
150
162
108
70-130
1,2-Dichloroethane-d4 (S)
%
91
70-130
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-d8(S)
%
102
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 37 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3826562
3826563
MS
MSD
92634614007
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
21.5
21.8
107
109
70-141
2
1,1,1-Trichloroethane
ug/L
ND
20
20
19.7
19.4
98
97
70-150
2
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
21.5
20.5
108
103
69-142
5
1,1,2-Trichloroethane
ug/L
ND
20
20
20.9
20.9
105
104
70-138
0
1,1-Dichloroethane
ug/L
ND
20
20
19.7
19.7
99
98
70-150
0
1,1-Dichloroethene
ug/L
ND
20
20
20.5
20.5
102
102
70-156
0
1,1-Dichloropropene
ug/L
ND
20
20
21.0
21.2
105
106
70-150
1
1,2,3-Trichlorobenzene
ug/L
ND
20
20
22.2
21.8
111
109
70-148
2
1,2,3-Trichloropropane
ug/L
ND
20
20
21.1
20.9
106
104
70-140
1
1,2,4-Trichlorobenzene
ug/L
ND
20
20
20.8
21.4
104
107
70-146
3
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
21.8
20.9
109
104
68-146
4
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.9
22.1
110
110
70-138
1
1,2-Dichlorobenzene
ug/L
ND
20
20
21.7
21.8
108
109
70-141
1
1,2-Dichloroethane
ug/L
ND
20
20
19.4
19.0
97
95
69-143
2
1,2-Dichloropropane
ug/L
ND
20
20
21.9
21.6
109
108
68-156
1
1,3-Dichlorobenzene
ug/L
ND
20
20
21.3
21.7
106
109
70-143
2
1,3-Dichloropropane
ug/L
ND
20
20
21.8
21.8
109
109
70-138
0
1,4-Dichlorobenzene
ug/L
ND
20
20
20.9
21.1
104
106
70-142
1
2,2-Dichloropropane
ug/L
ND
20
20
19.4
19.4
97
97
52-170
0
2-Butanone (MEK)
ug/L
ND
40
40
40.3
37.9
101
95
60-157
6
2-Chlorotoluene
ug/L
ND
20
20
21.6
22.1
108
110
70-147
2
2-Hexanone
ug/L
ND
40
40
41.7
40.2
104
101
68-146
4
4-Chlorotoluene
ug/L
ND
20
20
21.1
21.7
106
109
70-142
3
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
41.1
38.9
103
97
70-141
5
Acetone
ug/L
ND
40
40
38.0
35.8
95
89
58-157
6
Benzene
ug/L
ND
20
20
20.6
20.5
103
103
70-142
0
Bromobenzene
ug/L
ND
20
20
21.7
21.8
109
109
70-143
0
Bromochloromethane
ug/L
ND
20
20
21.2
21.8
106
109
70-146
3
Bromodichloromethane
ug/L
ND
20
20
21.0
20.9
105
105
70-139
0
Bromoform
ug/L
ND
20
20
21.2
21.1
106
106
64-140
0
Bromomethane
ug/L
ND
20
20
15.0
15.6
75
78
28-192
4 v3
Carbon tetrachloride
ug/L
ND
20
20
21.1
21.3
106
106
70-148
1
Chlorobenzene
ug/L
ND
20
20
21.4
21.3
107
106
70-141
1
Chloroethane
ug/L
ND
20
20
22.4
21.2
112
106
58-191
6
Chloroform
ug/L
ND
20
20
20.1
18.3
100
91
70-148
9
Chloromethane
ug/L
ND
20
20
19.1
19.0
95
95
43-162
1
cis-1,2-Dichloroethene
ug/L
ND
20
20
20.3
20.0
101
100
68-151
2
cis-1,3-Dichloropropene
ug/L
ND
20
20
21.0
20.8
105
104
70-139
1
Dibromochloromethane
ug/L
ND
20
20
21.9
21.6
110
108
70-144
1
Dibromomethane
ug/L
ND
20
20
21.1
21.5
105
107
70-139
2
Dichlorodifluoromethane
ug/L
ND
20
20
15.5
15.3
78
76
39-171
2
Diisopropyl ether
ug/L
ND
20
20
20.0
19.6
100
98
67-142
2
Ethylbenzene
ug/L
ND
20
20
20.9
21.2
105
106
70-143
1
Hexachloro-1,3-butadiene
ug/L
ND
20
20
24.4
23.3
122
117
64-163
4
m&p-Xylene
ug/L
ND
40
40
42.1
42.7
105
107
70-144
1
Methyl-tert-butyl ether
ug/L
ND
20
20
20.1
19.1
100
96
65-143
5
Results presented on this page are in
the units indicated by the
"Units" column except where
an alternate unit is presented
to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 38 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3826562
3826563
MS
MSD
92634614007
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Methylene Chloride
ug/L
ND
20
20
17.2
17.2
86
86
62-149
0
Naphthalene
ug/L
ND
20
20
22.1
21.5
110
107
67-147
3
o-Xylene
ug/L
ND
20
20
21.5
21.6
107
108
70-145
0
p-Isopropyltoluene
ug/L
ND
20
20
21.1
21.4
105
107
70-147
1
Styrene
ug/L
ND
20
20
21.2
21.5
106
107
70-143
1
Tetrachloroethene
ug/L
ND
20
20
20.5
20.4
102
102
70-145
0
Toluene
ug/L
ND
20
20
20.0
20.2
100
101
70-142
1
trans-1,2-Dichloroethene
ug/L
ND
20
20
20.3
19.4
102
97
70-151
5
trans- 1,3-Dichloropropene
ug/L
ND
20
20
21.3
21.0
106
105
70-139
2
Trichloroethene
ug/L
ND
20
20
21.5
21.2
108
106
62-146
2
Trichlorofluoromethane
ug/L
ND
20
20
18.5
18.3
92
91
63-153
1
Vinyl acetate
ug/L
ND
40
40
40.1
37.7
100
94
61-162
6
Vinyl chloride
ug/L
ND
20
20
20.7
19.9
104
99
61-163
4
Xylene (Total)
ug/L
ND
60
60
63.5
64.3
106
107
70-143
1
1,2-Dichloroethane-d4 (S)
%
93
90
70-130
4-Bromofluorobenzene (S)
%
97
96
70-130
Toluene-d8(S)
%
99
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 39 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
QC Batch: 734715 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92634407001, 92634407002
METHOD BLANK: 3823845
Associated Lab Samples: 92634407001, 92634407002
Parameter Units
1,4-Dioxane (p-Dioxane) ug/L
1,2-Dichloroethane-d4 (S) %
Toluene-d8 (S) %
Matrix: Water
Blank Reporting
Result Limit Analyzed
ND 2.0 11 /03/22 13:31
108 70-130 11/03/2213:31
99 70-130 11/03/2213:31
Qualifiers
LABORATORY CONTROL SAMPLE: 3823846
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 18.3 91 70-130
1,2-Dichloroethane-d4 (S) % 107 70-130
Toluene-d8 (S) % 100 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3823847
3823848
MS
MSD
92634407001 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 19.7
17.6 99
88
63-136 12
1,2-Dichloroethane-d4 (S)
%
110
113
70-130
Toluene-d8(S)
%
100
101
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 40 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
QC Batch: 735200 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92634407004, 92634407005
METHOD BLANK: 3826521
Associated Lab Samples: 92634407004, 92634407005
Parameter Units
1,4-Dioxane (p-Dioxane) ug/L
1,2-Dichloroethane-d4 (S) %
Toluene-d8 (S) %
Matrix: Water
Blank Reporting
Result Limit Analyzed
ND 2.0 11 /06/22 10:29
93 70-130 11/06/2210:29
101 70-130 11 /06/22 10:29
Qualifiers
LABORATORY CONTROL SAMPLE: 3826522
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 18.3 92 70-130
1,2-Dichloroethane-d4 (S) % 98 70-130
Toluene-d8(S) % 104 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3826523
3826524
MS
MSD
92634789005 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane(p-Dioxane)
ug/L 1.3J 20
20 21.3
22.0 100
103
63-136 3
1,2-Dichloroethane-d4 (S)
%
87
80
70-130
Toluene-d8(S)
%
99
95
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 41 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
QC Batch: 735222 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92634407003
METHOD BLANK: 3826572
Matrix:
Water
Associated Lab Samples: 92634407003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
11/06/22 22:33
1,2-Dichloroethane-d4 (S)
%
94
70-130
11/06/22 22:33
Toluene-d8 (S)
%
97
70-130
11/06/22 22:33
LABORATORY CONTROL SAMPLE: 3826573
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 18.7 94 70-130
1,2-Dichloroethane-d4 (S) % 91 70-130
Toluene-d8 (S) % 99 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3826574
3826575
MS
MSD
92634407003 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 19.5
21.1 98
105
63-136 8
1,2-Dichloroethane-d4 (S)
%
87
90
70-130
Toluene-d8(S)
%
102
93
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 42 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
QC Batch: 735269 Analysis Method: EPA 8270E
QC Batch Method: EPA 3510C Analysis Description: 8270E Water MSSV RVE
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92634407001, 92634407002
METHOD BLANK: 3826705
Associated Lab Samples: 92634407001, 92634407002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
8.3
11/07/22 14:25
1,2-Dichlorobenzene
ug/L
ND
8.3
11/07/22 14:25
1,3-Dichlorobenzene
ug/L
ND
8.3
11/07/22 14:25
1,4-Dichlorobenzene
ug/L
ND
8.3
11/07/22 14:25
1-Methylnaphthalene
ug/L
ND
8.3
11/07/22 14:25
2,2'-Oxybis(1-chloropropane)
ug/L
ND
8.3
11/07/22 14:25
2,4,5-Trichlorophenol
ug/L
ND
8.3
11/07/22 14:25
2,4,6-Trichlorophenol
ug/L
ND
8.3
11/07/22 14:25
2,4-Dichlorophenol
ug/L
ND
8.3
11/07/22 14:25
2,4-Dimethylphenol
ug/L
ND
8.3
11/07/22 14:25
2,4-Dinitrophenol
ug/L
ND
41.7
11/07/22 14:25
2,4-Dinitrotoluene
ug/L
ND
8.3
11/07/22 14:25
2,6-Dinitrotoluene
ug/L
ND
8.3
11/07/22 14:25
2-Chloronaphthalene
ug/L
ND
8.3
11/07/22 14:25
2-Chlorophenol
ug/L
ND
8.3
11/07/22 14:25
2-Methylnaphthalene
ug/L
ND
8.3
11/07/22 14:25
2-Methylphenol(o-Cresol)
ug/L
ND
8.3
11/07/22 14:25
2-Nitroaniline
ug/L
ND
16.7
11/07/22 14:25
2-Nitrophenol
ug/L
ND
8.3
11/07/22 14:25
3&4-Methyl phenol (m&p Cresol)
ug/L
ND
8.3
11/07/22 14:25
3,3'-Dichlorobenzidine
ug/L
ND
16.7
11/07/22 14:25
3-Nitroaniline
ug/L
ND
16.7
11/07/22 14:25
4,6-Dinitro-2-methyl phenol
ug/L
ND
16.7
11/07/22 14:25
4-Bromophenylphenyl ether
ug/L
ND
8.3
11/07/22 14:25
4-Chloro-3-methyl phenol
ug/L
ND
8.3
11/07/22 14:25
4-Chloroaniline
ug/L
ND
16.7
11/07/22 14:25
4-Chlorophenylphenyl ether
ug/L
ND
8.3
11/07/22 14:25
4-Nitroaniline
ug/L
ND
16.7
11/07/22 14:25
4-Nitrophenol
ug/L
ND
41.7
11/07/22 14:25
Acenaphthene
ug/L
ND
8.3
11/07/22 14:25
Acenaphthylene
ug/L
ND
8.3
11/07/22 14:25
Aniline
ug/L
ND
8.3
11/07/22 14:25
Anthracene
ug/L
ND
8.3
11/07/22 14:25
Benzo(a)anthracene
ug/L
ND
8.3
11/07/22 14:25
Benzo(a)pyrene
ug/L
ND
8.3
11/07/22 14:25
Benzo(b)fluoranthene
ug/L
ND
8.3
11/07/22 14:25
Benzo(g,h,i)perylene
ug/L
ND
8.3
11/07/22 14:25
Benzo(k)fluoranthene
ug/L
ND
8.3
11/07/22 14:25
Benzoic Acid
ug/L
ND
41.7
11/07/22 14:25
Benzyl alcohol
ug/L
ND
16.7
11/07/22 14:25
v2
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 43 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
METHOD BLANK: 3826705
Associated Lab Samples: 92634407001, 92634407002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
bis(2-Chloroethoxy)methane
ug/L
ND
8.3
11/07/22 14:25
bis(2-Chloroethyl) ether
ug/L
ND
8.3
11/07/22 14:25
bis(2-Ethylhexyl)phthalate
ug/L
ND
5.0
11/07/22 14:25
Butylbenzylphthalate
ug/L
ND
8.3
11/07/22 14:25
Chrysene
ug/L
ND
8.3
11/07/22 14:25
Di-n-butylphthalate
ug/L
ND
8.3
11/07/22 14:25
Di-n-octylphthalate
ug/L
ND
8.3
11/07/22 14:25
Dibenz(a,h)anthracene
ug/L
ND
8.3
11/07/22 14:25
Dibenzofuran
ug/L
ND
8.3
11/07/22 14:25
Diethylphthalate
ug/L
ND
8.3
11/07/22 14:25
Dimethylphthalate
ug/L
ND
8.3
11/07/22 14:25
Fluoranthene
ug/L
ND
8.3
11/07/22 14:25
Fluorene
ug/L
ND
8.3
11/07/22 14:25
Hexachloro-1,3-butadiene
ug/L
ND
8.3
11/07/22 14:25
Hexachlorobenzene
ug/L
ND
8.3
11/07/22 14:25
Hexachlorocyclopentadiene
ug/L
ND
8.3
11/07/22 14:25
Hexachloroethane
ug/L
ND
8.3
11/07/22 14:25
Indeno(1,2,3-cd)pyrene
ug/L
ND
8.3
11/07/22 14:25
Isophorone
ug/L
ND
8.3
11/07/22 14:25
N-Nitroso-di-n-propylamine
ug/L
ND
8.3
11/07/22 14:25
N-Nitrosodimethylamine
ug/L
ND
8.3
11/07/22 14:25
N-Nitrosodiphenylamine
ug/L
ND
8.3
11/07/22 14:25
Naphthalene
ug/L
ND
8.3
11/07/22 14:25
Nitrobenzene
ug/L
ND
8.3
11/07/22 14:25
Pentachlorophenol
ug/L
ND
16.7
11/07/22 14:25
Phenanthrene
ug/L
ND
8.3
11/07/22 14:25
Phenol
ug/L
ND
8.3
11/07/22 14:25
Pyrene
ug/L
ND
8.3
11/07/22 14:25
2,4,6-Tribromophenol (S)
%
88
10-144
11/07/22 14:25
2-Fluorobiphenyl (S)
%
58
10-130
11/07/22 14:25
2-Fluorophenol(S)
%
52
10-130
11/07/22 14:25
Nitrobenzene-d5 (S)
%
82
10-144
11/07/22 14:25
Phenol-d6 (S)
%
49
10-130
11/07/22 14:25
Terphenyl-d14 (S)
%
147
34-163
11/07/22 14:25
Qualifiers
LABORATORY CONTROL SAMPLE:
3826706
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
50
29.5
59
18-130
1,2-Dichlorobenzene
ug/L
50
16.5
33
20-130
1,3-Dichlorobenzene
ug/L
50
12.5
25
18-130
1,4-Dichlorobenzene
ug/L
50
13.6
27
18-130
1-Methylnaphthalene
ug/L
50
45.3
91
29-130
2,2'-Oxybis(1-chloropropane)
ug/L
50
37.2
74
28-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 44 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
LABORATORY CONTROL SAMPLE:
Parameter
3826706
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
2,4,5-Trichlorophenol
ug/L
50
39.3
79
35-130
2,4,6-Trichlorophenol
ug/L
50
31.8
64
31-130
2,4-Dichlorophenol
ug/L
50
41.4
83
35-130
2,4-Dimethylphenol
ug/L
50
53.3
107
34-130 v3
2,4-Dinitrophenol
ug/L
250
34.9J
14
10-153
2,4-Dinitrotoluene
ug/L
50
54.0
108
37-136
2,6-Dinitrotoluene
ug/L
50
56.0
112
33-136
2-Chloronaphthalene
ug/L
50
49.4
99
26-130
2-Chlorophenol
ug/L
50
36.0
72
37-130
2-Methylnaphthalene
ug/L
50
41.2
82
29-130
2-Methylphenol(o-Cresol)
ug/L
50
42.2
84
35-130
2-Nitroaniline
ug/L
100
89.4
89
37-130
2-Nitrophenol
ug/L
50
38.9
78
32-130
3&4-Methyl phenol (m&p Cresol)
ug/L
50
39.7
79
34-130
3,3'-Dichlorobenzidine
ug/L
100
109
109
34-136
3-Nitroaniline
ug/L
100
108
108
37-138
4,6-Dinitro-2-methyl phenol
ug/L
100
37.5
38
21-157
4-Bromophenylphenyl ether
ug/L
50
53.5
107
38-130
4-Chloro-3-methyl phenol
ug/L
100
92.9
93
37-130
4-Chloroaniline
ug/L
100
94.3
94
38-130
4-Chlorophenylphenyl ether
ug/L
50
51.3
103
33-130
4-Nitroaniline
ug/L
100
95.5
95
42-137
4-Nitrophenol
ug/L
250
30.9J
12
10-130
Acenaphthene
ug/L
50
53.3
107
33-130
Acenaphthylene
ug/L
50
52.0
104
35-130
Aniline
ug/L
50
33.3
67
22-130
Anthracene
ug/L
50
52.6
105
48-130
Benzo(a)anthracene
ug/L
50
55.6
111
48-137
Benzo(a)pyrene
ug/L
50
55.4
111
49-138
Benzo(b)fluoranthene
ug/L
50
56.0
112
52-138
Benzo(g,h,i)perylene
ug/L
50
56.7
113
48-140
Benzo(k)fluoranthene
ug/L
50
59.0
118
48-139
Benzoic Acid
ug/L
250
43.OJ
17
10-130
Benzyl alcohol
ug/L
100
86.4
86
35-130
bis(2-Chloroethoxy)methane
ug/L
50
47.2
94
34-130
bis(2-Chloroethyl) ether
ug/L
50
43.9
88
36-130
bis(2-Ethylhexyl)phthalate
ug/L
50
58.9
118
32-165
Butylbenzylphthalate
ug/L
50
58.8
118
34-161
Chrysene
ug/L
50
56.7
113
47-131
Di-n-butylphthalate
ug/L
50
52.1
104
39-144
Di-n-octylphthalate
ug/L
50
58.6
117
30-170
Dibenz(a,h)anthracene
ug/L
50
58.9
118
49-138
Dibenzofuran
ug/L
50
53.2
106
33-130
Diethylphthalate
ug/L
50
51.1
102
38-131
Dimethylphthalate
ug/L
50
52.4
105
37-130
Fluoranthene
ug/L
50
54.7
109
46-137
Fluorene
ug/L
50
53.7
107
37-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 45 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
LABORATORY CONTROL SAMPLE:
Parameter
3826706
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Hexachloro-1,3-butadiene
ug/L
50
20.2
40
11-130
Hexachlorobenzene
ug/L
50
54.1
108
38-130
Hexachlorocyclopentadiene
ug/L
50
33.1
66
10-130
Hexachloroethane
ug/L
50
10.6
21
14-130
Indeno(1,2,3-cd)pyrene
ug/L
50
57.8
116
41-130
Isophorone
ug/L
50
47.7
95
33-130
N-Nitroso-di-n-propylamine
ug/L
50
46.9
94
36-130
N-Nitrosodimethylamine
ug/L
50
43.1
86
34-130
N-Nitrosodiphenylamine
ug/L
50
55.2
110
37-130
Naphthalene
ug/L
50
35.0
70
30-130
Nitrobenzene
ug/L
50
43.3
87
36-130
Pentachlorophenol
ug/L
100
43.1
43
23-149
Phenanthrene
ug/L
50
55.3
111
44-130
Phenol
ug/L
50
27.1
54
18-130
Pyrene
ug/L
50
61.1
122
47-134
2,4,6-Tribromophenol (S)
%
86
10-144
2-Fluorobiphenyl (S)
%
87
10-130
2-Fluorophenol (S)
%
46
10-130
Nitrobenzene-d5 (S)
%
92
10-144
Phenol-d6 (S)
%
55
10-130
Terphenyl-d14(S)
%
129
34-163
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3826710
MS
92634631001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3826711
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,2,4-Trichlorobenzene
ug/L
ND
83.3
83.3
38.2
38.0
46
46
10-130
1
1,2-Dichlorobenzene
ug/L
ND
83.3
83.3
14.6J
15.1J
18
18
10-130
1,3-Dichlorobenzene
ug/L
ND
83.3
83.3
10.3J
11.3J
12
14
10-130
1,4-Dichlorobenzene
ug/L
ND
83.3
83.3
11.91
12.7J
14
15
10-130
1-Methylnaphthalene
ug/L
ND
83.3
83.3
70.0
67.7
84
81
10-130
3
2,2'-Oxybis(1-chloropropane)
ug/L
ND
83.3
83.3
46.2
41.3
55
50
12-142
11
2,4,5-Trichlorophenol
ug/L
ND
83.3
83.3
74.3
87.4
89
105
10-143
16
2,4,6-Trichlorophenol
ug/L
ND
83.3
83.3
54.5
78.1
65
94
10-147
36 R1
2,4-Dichlorophenol
ug/L
ND
83.3
83.3
69.0
76.0
83
91
10-138
10
2,4-Dimethylphenol
ug/L
ND
83.3
83.3
84.0
81.9
101
98
25-130
3 v3
2,4-Dinitrophenol
ug/L
ND
417
417
ND
100
4
24
10-165
M1
2,4-Dinitrotoluene
ug/L
ND
83.3
83.3
92.6
90.7
111
109
29-148
2
2,6-Dinitrotoluene
ug/L
ND
83.3
83.3
96.0
94.6
115
114
26-146
1
2-Chloronaphthalene
ug/L
ND
83.3
83.3
79.8
78.9
96
95
11-130
1
2-Chlorophenol
ug/L
ND
83.3
83.3
49.3
51.2
59
61
10-133
4
2-Methylnaphthalene
ug/L
ND
83.3
83.3
64.2
61.3
77
74
13-130
5
2-Methylphenol(o-Cresol)
ug/L
ND
83.3
83.3
61.9
59.8
74
72
20-130
4
2-Nitroaniline
ug/L
ND
167
167
157
150
94
90
24-136
5
2-Nitrophenol
ug/L
ND
83.3
83.3
59.7
61.8
72
74
10-153
4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC.
Page 46 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3826710
MS
Parameter
3&4-Methyl phenol (m&p
Cresol)
3,3'-Dichlorobenzidine
3-Nitroaniline
4,6-Din itro-2-methyl phenol
4-Bromophenylphenyl ether
4-Chloro-3-methyl phenol
4-Chloroaniline
4-Chlorophenylphenyl ether
4-Nitroaniline
4-Nitrophenol
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Ethylhexyl)phthalate
Butylbenzylphthalate
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Dibenz(a,h)anthracene
Dibenzofuran
Diethylphthalate
Dimethylphthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
N-Nitroso-di-n-propylamine
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
92634631001 Spike
Units Result Conc.
ug/L ND 83.3
3826711
MSD
Spike MS
Conc. Result
83.3 59.9
MSD MS MSD % Rec
Result % Rec % Rec Limits RPD Qual
60.4 72 73 16-130 1
ug/L
ND
167
167
173
176
104
106
10-153
ug/L
ND
167
167
180
171
108
103
22-151
ug/L
ND
167
167
46.0
104
28
62
10-180
ug/L
ND
83.3
83.3
94.4
90.7
113
109
25-130
ug/L
ND
167
167
153
151
92
91
25-133
ug/L
ND
167
167
135
136
81
82
14-132
ug/L
ND
83.3
83.3
86.9
83.1
104
100
19-130
ug/L
ND
167
167
155
145
93
87
29-150
ug/L
ND
417
417
31.6J
95.7
8
23
10-130
ug/L
ND
83.3
83.3
87.6
85.7
105
103
16-130
ug/L
ND
83.3
83.3
87.5
84.4
105
101
15-137
ug/L
ND
83.3
83.3
43.0
42.1
52
50
10-130
ug/L
ND
83.3
83.3
92.9
86.9
112
104
37-136
ug/L
ND
83.3
83.3
97.7
96.4
117
116
40-145
ug/L
ND
83.3
83.3
99.1
97.4
119
117
41-146
ug/L
ND
83.3
83.3
101
99.2
121
119
39-151
ug/L
ND
83.3
83.3
101
101
121
121
40-147
ug/L
ND
83.3
83.3
105
103
126
124
40-146
ug/L
ND
417
417
64.5J
67.3J
15
16
10-130
ug/L
ND
167
167
131
124
79
75
25-130
ug/L
ND
83.3
83.3
70.1
64.8
84
78
23-130
ug/L
ND
83.3
83.3
58.4
55.8
70
67
25-130
ug/L
ND
83.3
83.3
106
103
127
124
28-166
ug/L
ND
83.3
83.3
108
106
129
127
33-165
ug/L
ND
83.3
83.3
98.5
96.1
118
115
38-141
ug/L
ND
83.3
83.3
93.0
88.4
112
106
32-153
ug/L
ND
83.3
83.3
108
105
129
126
30-175
ug/L
ND
83.3
83.3
104
102
124
122
39-148
ug/L
ND
83.3
83.3
89.2
86.5
107
104
20-130
ug/L
ND
83.3
83.3
88.7
86.1
106
103
28-142
ug/L
ND
83.3
83.3
89.6
87.0
108
104
26-136
ug/L
ND
83.3
83.3
96.0
91.2
115
109
39-143
ug/L
ND
83.3
83.3
89.8
87.3
108
105
24-132
ug/L
ND
83.3
83.3
20.6
21.3
25
26
10-130
ug/L
ND
83.3
83.3
93.3
90.4
112
108
29-130
ug/L
ND
83.3
83.3
47.1
45.7
57
55
10-130
ug/L
ND
83.3
83.3
8.1J
8.3J
10
10
10-130
ug/L
ND
83.3
83.3
103
102
123
123
39-148
ug/L
ND
83.3
83.3
76.0
73.2
91
88
23-130
ug/L
ND
83.3
83.3
70.2
65.9
84
79
25-130
ug/L
ND
83.3
83.3
59.3
57.4
71
69
22-130
ug/L
ND
83.3
83.3
97.2
92.1
117
110
26-134
ug/L
ND
83.3
83.3
47.5
45.8
57
55
14-130
ug/L
ND
83.3
83.3
59.6
54.8
72
66
25-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC.
2
5
77 R1
4
1
1
4
7
M1
2
4
2
7
1
2
2
0
2
5
8
5
3
2
2
5
2
2
3
3
3
5
3
3
3
3
0
4
6
3
5
4
8
Page 47 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3826710
3826711
MS
MSD
92634631001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Pentachlorophenol
ug/L
ND
167
167
78.4
134
47
80
10-175
52 R1
Phenanthrene
ug/L
ND
83.3
83.3
98.6
92.0
118
110
36-133
7
Phenol
ug/L
ND
83.3
83.3
38.2
39.6
46
48
10-130
4
Pyrene
ug/L
ND
83.3
83.3
109
107
131
128
40-143
2
2,4,6-Tribromophenol (S)
%
92
107
10-144
2-Fluorobiphenyl (S)
%
64
73
10-130
2-Fluorophenol(S)
%
37
55
10-130
Nitrobenzene-d5(S)
%
68
75
10-144
Phenol-d6 (S)
%
44
51
10-130
Terphenyl-d14(S)
%
127
128
34-163
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC.
Page 48 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
QC Batch: 735838 Analysis Method: EPA 8270E
QC Batch Method: EPA 3510C Analysis Description: 8270E Water MSSV RVE
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92634407003, 92634407004, 92634407005
METHOD BLANK: 3829525 Matrix:
Associated Lab Samples: 92634407003, 92634407004, 92634407005
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
10.0
11/10/22 09:56
1,2-Dichlorobenzene
ug/L
ND
10.0
11/10/22 09:56
1,3-Dichlorobenzene
ug/L
ND
10.0
11/10/22 09:56
1,4-Dichlorobenzene
ug/L
ND
10.0
11/10/22 09:56
1-Methylnaphthalene
ug/L
ND
10.0
11/10/22 09:56
2,2'-Oxybis(1-chloropropane)
ug/L
ND
10.0
11/10/22 09:56
2,4,5-Trichlorophenol
ug/L
ND
10.0
11/10/22 09:56
2,4,6-Trichlorophenol
ug/L
ND
10.0
11/10/22 09:56
2,4-Dichlorophenol
ug/L
ND
10.0
11/10/22 09:56
2,4-Dimethylphenol
ug/L
ND
10.0
11/10/22 09:56
2,4-Dinitrophenol
ug/L
ND
50.0
11/10/22 09:56
2,4-Dinitrotoluene
ug/L
ND
10.0
11/10/22 09:56
2,6-Dinitrotoluene
ug/L
ND
10.0
11/10/22 09:56
2-Chloronaphthalene
ug/L
ND
10.0
11/10/22 09:56
2-Chlorophenol
ug/L
ND
10.0
11/10/22 09:56
2-Methylnaphthalene
ug/L
ND
10.0
11/10/22 09:56
2-Methylphenol(o-Cresol)
ug/L
ND
10.0
11/10/22 09:56
2-Nitroaniline
ug/L
ND
20.0
11/10/22 09:56
2-Nitrophenol
ug/L
ND
10.0
11/10/22 09:56
3&4-Methyl phenol (m&p Cresol)
ug/L
ND
10.0
11/10/22 09:56
3,3'-Dichlorobenzidine
ug/L
ND
20.0
11/10/22 09:56
3-Nitroaniline
ug/L
ND
20.0
11/10/22 09:56
4,6-Dinitro-2-methyl phenol
ug/L
ND
20.0
11/10/22 09:56
4-Bromophenylphenyl ether
ug/L
ND
10.0
11/10/22 09:56
4-Chloro-3-methyl phenol
ug/L
ND
10.0
11/10/22 09:56
4-Chloroaniline
ug/L
ND
20.0
11/10/22 09:56
4-Chlorophenylphenyl ether
ug/L
ND
10.0
11/10/22 09:56
4-Nitroaniline
ug/L
ND
20.0
11/10/22 09:56
4-Nitrophenol
ug/L
ND
50.0
11/10/22 09:56
Acenaphthene
ug/L
ND
10.0
11/10/22 09:56
Acenaphthylene
ug/L
ND
10.0
11/10/22 09:56
Aniline
ug/L
ND
10.0
11/10/22 09:56
Anthracene
ug/L
ND
10.0
11/10/22 09:56
Benzo(a)anthracene
ug/L
ND
10.0
11/10/22 09:56
Benzo(a)pyrene
ug/L
ND
10.0
11/10/22 09:56
Benzo(b)fluoranthene
ug/L
ND
10.0
11/10/22 09:56
Benzo(g,h,i)perylene
ug/L
ND
10.0
11/10/22 09:56
Benzo(k)fluoranthene
ug/L
ND
10.0
11/10/22 09:56
Benzoic Acid
ug/L
ND
50.0
11/10/22 09:56
Benzyl alcohol
ug/L
ND
20.0
11/10/22 09:56
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 49 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
METHOD BLANK: 3829525 Matrix:
Associated Lab Samples: 92634407003, 92634407004, 92634407005
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
11/10/22 09:56
bis(2-Chloroethyl) ether
ug/L
ND
10.0
11/10/22 09:56
bis(2-Ethylhexyl)phthalate
ug/L
ND
6.0
11/10/22 09:56
Butylbenzylphthalate
ug/L
ND
10.0
11/10/22 09:56
Chrysene
ug/L
ND
10.0
11/10/22 09:56
Di-n-butylphthalate
ug/L
ND
10.0
11/10/22 09:56
Di-n-octylphthalate
ug/L
ND
10.0
11/10/22 09:56
Dibenz(a,h)anthracene
ug/L
ND
10.0
11/10/22 09:56
Dibenzofuran
ug/L
ND
10.0
11/10/22 09:56
Diethylphthalate
ug/L
ND
10.0
11/10/22 09:56
Dimethylphthalate
ug/L
ND
10.0
11/10/22 09:56
Fluoranthene
ug/L
ND
10.0
11/10/22 09:56
Fluorene
ug/L
ND
10.0
11/10/22 09:56
Hexachloro-1,3-butadiene
ug/L
ND
10.0
11/10/22 09:56
Hexachlorobenzene
ug/L
ND
10.0
11/10/22 09:56
Hexachlorocyclopentadiene
ug/L
ND
10.0
11/10/22 09:56
Hexachloroethane
ug/L
ND
10.0
11/10/22 09:56
Indeno(1,2,3-cd)pyrene
ug/L
ND
10.0
11/10/22 09:56
Isophorone
ug/L
ND
10.0
11/10/22 09:56
N-Nitroso-di-n-propylamine
ug/L
ND
10.0
11/10/22 09:56
N-Nitrosodimethylamine
ug/L
ND
10.0
11/10/22 09:56
N-Nitrosodiphenylamine
ug/L
ND
10.0
11/10/22 09:56
Naphthalene
ug/L
ND
10.0
11/10/22 09:56
Nitrobenzene
ug/L
ND
10.0
11/10/22 09:56
Pentachlorophenol
ug/L
ND
20.0
11/10/22 09:56
Phenanthrene
ug/L
ND
10.0
11/10/22 09:56
Phenol
ug/L
ND
10.0
11/10/22 09:56
Pyrene
ug/L
ND
10.0
11/10/22 09:56
2,4,6-Tribromophenol (S)
%
81
10-144
11/10/22 09:56
2-Fluorobiphenyl (S)
%
39
10-130
11/10/22 09:56
2-Fluorophenol (S)
%
49
10-130
11/10/22 09:56
Nitrobenzene-d5 (S)
%
65
10-144
11/10/22 09:56
Phenol-d6 (S)
%
38
10-130
11/10/22 09:56
Terphenyl-d14 (S)
%
89
34-163
11/10/22 09:56
v1
Qualifiers
LABORATORY CONTROL SAMPLE:
3829526
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
50
25.0
50
18-130
1,2-Dichlorobenzene
ug/L
50
14.4
29
20-130
1,3-Dichlorobenzene
ug/L
50
11.6
23
18-130
1,4-Dichlorobenzene
ug/L
50
12.7
25
18-130
1-Methylnaphthalene
ug/L
50
38.4
77
29-130
2,2'-Oxybis(1-chloropropane)
ug/L
50
29.5
59
28-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 50 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
LABORATORY CONTROL SAMPLE:
Parameter
3829526
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2,4,5-Trichlorophenol
ug/L
50
47.4
95
35-130
2,4,6-Trichlorophenol
ug/L
50
48.9
98
31-130
2,4-Dichlorophenol
ug/L
50
43.7
87
35-130
2,4-Dimethylphenol
ug/L
50
54.2
108
34-130
2,4-Dinitrophenol
ug/L
250
171
68
10-153
2,4-Dinitrotoluene
ug/L
50
56.8
114
37-136
2,6-Dinitrotoluene
ug/L
50
52.9
106
33-136
2-Chloronaphthalene
ug/L
50
42.3
85
26-130
2-Chlorophenol
ug/L
50
34.3
69
37-130
2-Methylnaphthalene
ug/L
50
36.8
74
29-130
2-Methylphenol(o-Cresol)
ug/L
50
35.2
70
35-130
2-Nitroaniline
ug/L
100
95.0
95
37-130
2-Nitrophenol
ug/L
50
45.5
91
32-130
3&4-Methyl phenol (m&p Cresol)
ug/L
50
32.4
65
34-130
3,3'-Dichlorobenzidine
ug/L
100
99.2
99
34-136
3-Nitroaniline
ug/L
100
100
100
37-138
4,6-Dinitro-2-methyl phenol
ug/L
100
93.6
94
21-157
4-Bromophenylphenyl ether
ug/L
50
44.6
89
38-130
4-Chloro-3-methyl phenol
ug/L
100
86.9
87
37-130
4-Chloroaniline
ug/L
100
79.1
79
38-130
4-Chlorophenylphenyl ether
ug/L
50
46.1
92
33-130
4-Nitroaniline
ug/L
100
100
100
42-137
4-Nitrophenol
ug/L
250
130
52
10-130
Acenaphthene
ug/L
50
43.6
87
33-130
Acenaphthylene
ug/L
50
44.1
88
35-130
Aniline
ug/L
50
28.8
58
22-130
Anthracene
ug/L
50
41.9
84
48-130
Benzo(a)anthracene
ug/L
50
48.2
96
48-137
Benzo(a)pyrene
ug/L
50
45.9
92
49-138
Benzo(b)fluoranthene
ug/L
50
49.3
99
52-138
Benzo(g,h,i)perylene
ug/L
50
49.8
100
48-140
Benzo(k)fluoranthene
ug/L
50
45.1
90
48-139
Benzoic Acid
ug/L
250
43.3J
17
10-130
Benzyl alcohol
ug/L
100
76.1
76
35-130
bis(2-Chloroethoxy)methane
ug/L
50
40.0
80
34-130
bis(2-Chloroethyl) ether
ug/L
50
35.2
70
36-130
bis(2-Ethylhexyl)phthalate
ug/L
50
54.4
109
32-165
Butylbenzylphthalate
ug/L
50
55.8
112
34-161
Chrysene
ug/L
50
47.3
95
47-131
Di-n-butylphthalate
ug/L
50
50.8
102
39-144
Di-n-octylphthalate
ug/L
50
50.2
100
30-170
Dibenz(a,h)anthracene
ug/L
50
51.9
104
49-138
Dibenzofuran
ug/L
50
45.3
91
33-130
Diethylphthalate
ug/L
50
50.4
101
38-131
Dimethylphthalate
ug/L
50
48.0
96
37-130
Fluoranthene
ug/L
50
47.6
95
46-137
Fluorene
ug/L
50
45.9
92
37-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 51 of 94

Pace Analytical Services, LLC
leac,yficalAnal2225 Riverside Dr.
Asheville, NC 28804
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
LABORATORY CONTROL SAMPLE:
Parameter
3829526
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Hexachloro-1,3-butadiene
ug/L
50
18.3
37
11-130
Hexachlorobenzene
ug/L
50
46.0
92
38-130
Hexachlorocyclopentadiene
ug/L
50
31.1
62
10-130
Hexachloroethane
ug/L
50
10.1
20
14-130
Indeno(1,2,3-cd)pyrene
ug/L
50
53.0
106
41-130
Isophorone
ug/L
50
44.2
88
33-130
N-Nitroso-di-n-propylamine
ug/L
50
44.7
89
36-130
N-Nitrosodimethylamine
ug/L
50
38.3
77
34-130 v1
N-Nitrosodiphenylamine
ug/L
50
45.2
90
37-130
Naphthalene
ug/L
50
28.2
56
30-130
Nitrobenzene
ug/L
50
40.4
81
36-130
Pentachlorophenol
ug/L
100
96.5
97
23-149
Phenanthrene
ug/L
50
44.9
90
44-130
Phenol
ug/L
50
24.8
50
18-130
Pyrene
ug/L
50
48.2
96
47-134
2,4,6-Tribromophenol (S)
%
106
10-144
2-Fluorobiphenyl (S)
%
69
10-130
2-Fluorophenol(S)
%
54
10-130
Nitrobenzene-d5 (S)
%
75
10-144
Phenol-d6 (S)
%
46
10-130
Terphenyl-d14 (S)
%
99
34-163
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3829527
MS
92634614004 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3829528
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,2,4-Trichlorobenzene
ug/L
ND
83.3
83.3
21.9
24.4
26
29
10-130
11
1,2-Dichlorobenzene
ug/L
ND
83.3
83.3
10.3J
12.9J
12
16
10-130
1,3-Dichlorobenzene
ug/L
ND
83.3
83.3
7.9J
9AJ
9
11
10-130
M1
1,4-Dichlorobenzene
ug/L
2.8J
83.3
83.3
12.7J
16.5J
12
16
10-130
1-Methylnaphthalene
ug/L
ND
83.3
83.3
47.0
55.1
56
66
10-130
16
2,2'-Oxybis(1-chloropropane)
ug/L
ND
83.3
83.3
38.5
42.6
46
51
12-142
10
2,4,5-Trichlorophenol
ug/L
ND
83.3
83.3
65.4
78.8
79
95
10-143
19
2,4,6-Trichlorophenol
ug/L
ND
83.3
83.3
59.2
77.7
71
93
10-147
27
2,4-Dichlorophenol
ug/L
ND
83.3
83.3
56.0
72.9
67
87
10-138
26
2,4-Dimethylphenol
ug/L
ND
83.3
83.3
72.6
91.9
87
110
25-130
24
2,4-Dinitrophenol
ug/L
ND
417
417
91.6
152
22
36
10-165
49 R1
2,4-Dinitrotoluene
ug/L
ND
83.3
83.3
94.1
99.9
113
120
29-148
6
2,6-Dinitrotoluene
ug/L
ND
83.3
83.3
84.4
94.5
101
113
26-146
11
2-Chloronaphthalene
ug/L
ND
83.3
83.3
53.8
62.0
65
74
11-130
14
2-Chlorophenol
ug/L
ND
83.3
83.3
44.3
48.9
53
59
10-133
10
2-Methylnaphthalene
ug/L
ND
83.3
83.3
42.5
49.7
51
60
13-130
16
2-Methylphenol(o-Cresol)
ug/L
ND
83.3
83.3
45.7
53.2
55
64
20-130
15
2-Nitroaniline
ug/L
ND
167
167
151
166
90
100
24-136
10
2-Nitrophenol
ug/L
ND
83.3
83.3
56.4
71.6
68
86
10-153
24
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC.
Page 52 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3829527
MS
Parameter
3&4-Methyl phenol (m&p
Cresol)
3,3'-Dichlorobenzidine
3-Nitroaniline
4,6-Din itro-2-methyl phenol
4-Bromophenylphenyl ether
4-Chloro-3-methyl phenol
4-Chloroaniline
4-Chlorophenylphenyl ether
4-Nitroaniline
4-Nitrophenol
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Ethylhexyl)phthalate
Butylbenzylphthalate
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Dibenz(a,h)anthracene
Dibenzofuran
Diethylphthalate
Dimethylphthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
N-Nitroso-di-n-propylamine
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
92634614004 Spike
Units Result Conc.
ug/L ND 83.3
3829528
MSD
Spike MS
Conc. Result
83.3 44.7
MSD MS MSD % Rec
Result % Rec % Rec Limits RPD
53.9 54 65 16-130 19
ug/L
ND
167
167
185
184
111
110
10-153
ug/L
ND
167
167
169
176
102
106
22-151
ug/L
ND
167
167
92.2
126
55
76
10-180
ug/L
ND
83.3
83.3
71.2
80.2
85
96
25-130
ug/L
ND
167
167
127
151
76
91
25-133
ug/L
ND
167
167
107
139
64
84
14-132
ug/L
ND
83.3
83.3
67.3
78.7
81
94
19-130
ug/L
ND
167
167
176
175
106
105
29-150
ug/L
ND
417
417
107
145
26
35
10-130
ug/L
ND
83.3
83.3
60.7
71.7
73
86
16-130
ug/L
ND
83.3
83.3
61.1
70.5
73
85
15-137
ug/L
ND
83.3
83.3
38.8
45.5
47
55
10-130
ug/L
ND
83.3
83.3
74.5
78.8
89
95
37-136
ug/L
ND
83.3
83.3
86.4
87.6
104
105
40-145
ug/L
ND
83.3
83.3
87.7
85.5
105
103
41-146
ug/L
ND
83.3
83.3
86.9
85.9
104
103
39-151
ug/L
ND
83.3
83.3
93.2
85.5
112
103
40-147
ug/L
ND
83.3
83.3
90.1
87.0
108
104
40-146
ug/L
ND
417
417
ND
ND
0
7
10-130
ug/L
ND
167
167
105
119
63
72
25-130
ug/L
ND
83.3
83.3
51.2
66.1
61
79
23-130
ug/L
ND
83.3
83.3
48.7
55.8
58
67
25-130
ug/L
ND
83.3
83.3
97.8
99.4
117
119
28-166
ug/L
ND
83.3
83.3
102
101
123
121
33-165
ug/L
ND
83.3
83.3
87.6
85.8
105
103
38-141
ug/L
ND
83.3
83.3
94.3
96.2
113
115
32-153
ug/L
ND
83.3
83.3
93.5
92.7
112
111
30-175
ug/L
ND
83.3
83.3
94.4
90.5
113
109
39-148
ug/L
ND
83.3
83.3
65.5
78.5
79
94
20-130
ug/L
ND
83.3
83.3
85.1
90.4
102
109
28-142
ug/L
ND
83.3
83.3
76.0
85.7
91
103
26-136
ug/L
ND
83.3
83.3
86.2
87.2
103
105
39-143
ug/L
ND
83.3
83.3
69.1
78.5
83
94
24-132
ug/L
ND
83.3
83.3
9.5J
12.2J
11
15
10-130
ug/L
ND
83.3
83.3
81.6
86.0
98
103
29-130
ug/L
ND
83.3
83.3
31.0
32.0
37
38
10-130
ug/L
ND
83.3
83.3
3.5J
5.5J
4
7
10-130
ug/L
ND
83.3
83.3
95.7
90.2
115
108
39-148
ug/L
ND
83.3
83.3
61.3
76.6
74
92
23-130
ug/L
ND
83.3
83.3
62.9
73.2
76
88
25-130
ug/L
ND
83.3
83.3
53.9
60.2
65
72
22-130
ug/L
ND
83.3
83.3
78.1
83.8
94
101
26-134
ug/L
ND
83.3
83.3
28.7
32.6
34
39
14-130
ug/L
ND
83.3
83.3
51.9
61.6
62
74
25-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC.
1
4
31 R1
12
18
26
16
0
31 R1
17
14
16
6
1
2
1
9
3
M1
13
25
13
2
1
2
2
1
4
18
6
12
1
13
5
3
M1
6
22
15
11 v1
7
13
17
Qual
Page 53 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3829527
3829528
MS
MSD
92634614004
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Pentachlorophenol
ug/L
ND
167
167
70.0
126
42
76
10-175
57 R1
Phenanthrene
ug/L
ND
83.3
83.3
81.1
85.4
97
102
36-133
5
Phenol
ug/L
ND
83.3
83.3
30.5
35.9
37
43
10-130
16
Pyrene
ug/L
ND
83.3
83.3
88.9
84.5
107
101
40-143
5
2,4,6-Tribromophenol (S)
%
98
110
10-144
2-Fluorobiphenyl (S)
%
51
55
10-130
2-Fluorophenol(S)
%
37
44
10-130
Nitrobenzene-d5(S)
%
59
70
10-144
Phenol-d6 (S)
%
34
39
10-130
Terphenyl-d14(S)
%
110
104
34-163
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC.
Page 54 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
QC Batch: 734641 Analysis Method: SM 2320B-2011
QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92634407001, 92634407002
METHOD BLANK: 3823420
Matrix:
Water
Associated Lab Samples: 92634407001, 92634407002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Alkalinity, Total as CaCO3
mg/L
ND
5.0
11/03/22 14:42
LABORATORY CONTROL SAMPLE:
3823421
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Alkalinity, Total as CaCO3
mg/L
50
50.4
101 80-120
LABORATORY CONTROL SAMPLE: 3823422
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Alkalinity, Total as CaCO3 mg/L 50 51.4 103 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3823423 3823424
MS MSD
92634407002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Alkalinity, Total as CaCO3 mg/L 105 50 50 159 160 108 112 80-120 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3823425 3823426
MS MSD
92634422001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Alkalinity, Total as CaCO3 mg/L 213 50 50 283 274 141 123 80-120 3 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC.
Page 55 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
QC Batch: 735164 Analysis Method: SM 2320B-2011
QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92634407003, 92634407004, 92634407005
METHOD BLANK: 3826383
Matrix:
Water
Associated Lab Samples: 92634407003, 92634407004, 92634407005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Alkalinity, Total as CaCO3
mg/L
ND
5.0
11/05/22 13:50
LABORATORY CONTROL SAMPLE:
3826384
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Alkalinity, Total as CaCO3
mg/L
50
49.7
99 80-120
LABORATORY CONTROL SAMPLE: 3826385
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Alkalinity, Total as CaCO3 mg/L 50 49.7 99 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3826386 3826387
MS MSD
92634935002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Alkalinity, Total as CaCO3 mg/L 61.0 50 50 109 108 96 94 80-120 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3826388 3826389
MS MSD
92634937001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Alkalinity, Total as CaCO3 mg/L 198 50 50 268 258 141 120 80-120 4 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC.
Page 56 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
QC Batch: 734509 Analysis Method: SM 2540C-2015
QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92634407001, 92634407002
METHOD BLANK: 3822956 Matrix: Water
Associated Lab Samples: 92634407001, 92634407002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Dissolved Solids mg/L ND 25.0 11/02/22 20:47
LABORATORY CONTROL SAMPLE: 3822957
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Dissolved Solids mg/L 250 254 102 90-110
SAMPLE DUPLICATE: 3822958
92633836001 Dup
Parameter Units Result Result RPD Qualifiers
Total Dissolved Solids mg/L 257 252 2
SAMPLE DUPLICATE: 3822959
92634294002 Dup
Parameter Units Result Result RPD Qualifiers
Total Dissolved Solids mg/L 33.0 33.0 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 57 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
QC Batch: 735205 Analysis Method: SM 2540C-2015
QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92634407003
METHOD BLANK: 3826541
Associated Lab Samples: 92634407003
Parameter
Units
Total Dissolved Solids
mg/L
LABORATORY CONTROL SAMPLE:
3826542
Parameter
Units
Total Dissolved Solids
mg/L
SAMPLE DUPLICATE: 3826543
Parameter
Units
Total Dissolved Solids
mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25.0 11 /07/22 10:13
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 252 101 90-110
92634640001 Dup
Result Result RPD Qualifiers
114 106 7
SAMPLE DUPLICATE: 3826544
92634657002 Dup
Parameter Units Result Result
Total Dissolved Solids mg/L 58.0 59.0
RPD Qualifiers
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 58 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
QC Batch: 735206 Analysis Method: SM 2540C-2015
QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92634407004, 92634407005
METHOD BLANK: 3826545 Matrix: Water
Associated Lab Samples: 92634407004, 92634407005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Dissolved Solids mg/L ND 25.0 11/07/22 10:18
LABORATORY CONTROL SAMPLE: 3826546
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Dissolved Solids mg/L 250 248 99 90-110
SAMPLE DUPLICATE: 3826547
92634656001 Dup
Parameter Units Result Result RPD Qualifiers
Total Dissolved Solids mg/L 125 128 2
SAMPLE DUPLICATE: 3826548
92634409008 Dup
Parameter Units Result Result RPD Qualifiers
Total Dissolved Solids mg/L 51.0 47.0 8
SAMPLE DUPLICATE: 3830539
92634656004 Dup
Parameter Units Result Result RPD Qualifiers
Total Dissolved Solids mg/L 186 191 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 59 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
QC Batch: 734581 Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92634407001, 92634407002
METHOD BLANK: 3823140
Matrix:
Water
Associated Lab Samples: 92634407001, 92634407002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Sulfate
mg/L
ND
1.0
11/03/2217:10
LABORATORY CONTROL SAMPLE:
3823141
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Sulfate
mg/L
50
49.2
98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3823142 3823143
MS MSD
92633842001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L ND 50 50 49.9 50.5 99 100 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3823144 3823145
MS MSD
92634338004 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L 81.6 50 50 127 127 90 91 90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC.
Page 60 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
QC Batch: 735083 Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92634407003, 92634407004
METHOD BLANK: 3825976
Matrix:
Water
Associated Lab Samples: 92634407003, 92634407004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Sulfate
mg/L
ND
1.0
11/05/2211:37
LABORATORY CONTROL SAMPLE:
3825977
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Sulfate
mg/L
50
49.9
100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3825978 3825979
MS MSD
92634672001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L 64.0 50 50 106 109 84 89 90-110 2 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3825980 3825981
MS MSD
92634409007 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L 25.5 50 50 75.9 76.8 101 103 90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC.
Page 61 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
QC Batch: 735085 Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92634407005
METHOD BLANK: 3825986
Associated Lab Samples: 92634407005
Parameter Units
Sulfate mg/L
LABORATORY CONTROL SAMPLE: 3825987
Parameter Units
Sulfate mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 1.0 11 /05/22 22:45
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
50 48.7 97 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3825988 3825989
MS MSD
92634407005 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L 3.1 50 50 53.6 54.5 101 103 90-110 2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3825990 3825991
MS MSD
92634656006 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L 1260 50 50 1310 1300 102 92 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC.
Page 62 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
QC Batch: 736047 Analysis Method: SM 4500-CI-E-2011
QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92634407001, 92634407002, 92634407003, 92634407004
METHOD BLANK: 3830888
Matrix:
Water
Associated Lab Samples: 92634407001, 92634407002, 92634407003, 92634407004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Chloride
mg/L
ND
1.0
11/10/2216:52
LABORATORY CONTROL SAMPLE:
3830889
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Chloride
mg/L
20
21.0
105 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3830890 3830891
MS MSD
92635249002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chloride mg/L 105 10 10 113 113 78 81 90-110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3830892 3830893
MS MSD
92635495001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chloride mg/L 10.3 10 10 20.7 21.0 104 108 90-110 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC.
Page 63 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
QC Batch: 736048 Analysis Method: SM 4500-CI-E-2011
QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92634407005
METHOD BLANK: 3830894
Associated Lab Samples: 92634407005
Parameter Units
Chloride mg/L
LABORATORY CONTROL SAMPLE: 3830895
Parameter Units
Chloride mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 1.0 11 /10/22 17:24
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
20 20.8 104 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3830896 3830897
MS MSD
92634407005 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chloride mg/L 1.5 10 10 12.1 12.1 106 106 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3830898 3830899
MS MSD
92634789001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chloride mg/L 6.2 10 10 16.7 16.8 106 106 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC.
Page 64 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
QC Batch: 734737 Analysis Method: SM 531 OB-2014
QC Batch Method: SM 531 OB-2014 Analysis Description: 5310E TOC
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92634407001, 92634407002
METHOD BLANK: 3824084
Matrix:
Water
Associated Lab Samples: 92634407001, 92634407002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Organic Carbon
mg/L
ND
1.0
11/03/22 17:06
LABORATORY CONTROL SAMPLE:
3824085
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Total Organic Carbon
mg/L
25
24.7
99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3824086 3824087
MS MSD
92634383001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Total Organic Carbon mg/L 3.9 25 25 28.1 28.2 97 97 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3824088 3824089
MS MSD
92633735002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Total Organic Carbon mg/L ND 25 25 26.7 26.6 106 105 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC.
Page 65 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
QC Batch: 736855 Analysis Method: SM 531 OB-2014
QC Batch Method: SM 531 OB-2014 Analysis Description: 5310E TOC
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92634407003, 92634407004, 92634407005
METHOD BLANK: 3834668
Matrix:
Water
Associated Lab Samples: 92634407003, 92634407004, 92634407005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Organic Carbon
mg/L
ND
1.0
11/14/22 13:09
LABORATORY CONTROL SAMPLE:
3834669
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Total Organic Carbon
mg/L
25
24.4
98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3834670 3834671
MS MSD
92635495001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Total Organic Carbon mg/L 3.2 25 25 29.4 29.5 105 105 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3834672 3834673
MS MSD
92634409008 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Total Organic Carbon mg/L ND 25 25 25.6 25.7 101 102 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC.
Page 66 of 94

Pace Analytical Services, LLC
leac,yficalAnal2225 Riverside Dr.
Asheville, NC 28804
www.pacelabs.com [phone]
QUALIFIERS
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 67 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
SLUDGE LANDFILL 11/22
92634407
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92634407001
SWP-1
92634407002
SWP-2
92634407003
Q06V09
92634407004
Q06V10
92634407005
Q06V11
92634407001
SWP-1
EPA 3010
876516
EPA 6010
876541
92634407002
SWP-2
EPA 3010
876516
EPA 6010
876541
92634407003
Q06V09
EPA 3010
876516
EPA 6010
876541
92634407004
Q06V10
EPA 3010
876516
EPA 6010
876541
92634407005
Q06V11
EPA 3010
876516
EPA 6010
876541
92634407001
SWP-1
EPA 3510C
735269
EPA 8270E
735330
92634407002
SWP-2
EPA 3510C
735269
EPA 8270E
735330
92634407003
Q06V09
EPA 3510C
735838
EPA 8270E
736139
92634407004
QO6V10
EPA 3510C
735838
EPA 8270E
736139
92634407005
Q06V11
EPA 3510C
735838
EPA 8270E
736139
92634407001
SWP-1
EPA 8260D
735210
92634407002
SWP-2
EPA 8260D
735210
92634407003
Q06V09
EPA 8260D
735210
92634407004
Q06V10
EPA 8260D
735210
92634407005
Q06V11
EPA 8260D
735210
92634407001
SWP-1
EPA 8260D Mod.
734715
92634407002
SWP-2
EPA 8260D Mod.
734715
92634407003
Q06V09
EPA 8260D Mod.
735222
92634407004
QO6V10
EPA 8260D Mod.
735200
92634407005
Q06V11
EPA 8260D Mod.
735200
92634407001
SWP-1
SM 2320E-2011
734641
92634407002
SWP-2
SM 2320E-2011
734641
92634407003
Q06V09
SM 2320B-2011
735164
92634407004
Q06V10
SM 2320B-2011
735164
92634407005
Q06V11
SM 2320B-2011
735164
92634407001
SWP-1
SM 2540C-2015
734509
92634407002
SWP-2
SM 2540C-2015
734509
92634407003
Q06V09
SM 2540C-2015
735205
92634407004
Q06V10
SM 2540C-2015
735206
92634407005
Q06V11
SM 2540C-2015
735206
92634407001
SWP-1
EPA 300.0 Rev 2.1 1993
734581
92634407002
SWP-2
EPA 300.0 Rev 2.1 1993
734581
92634407003
Q06V09
EPA 300.0 Rev 2.1 1993
735083
92634407004
Q06V10
EPA 300.0 Rev 2.1 1993
735083
92634407005
Q06V11
EPA 300.0 Rev 2.1 1993
735085
92634407001
SWP-1
SM 4500-CI-E-2011
736047
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2022 11:11 AM
without the written consent of Pace Analytical Services, LLC.
Page 68 of 94

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SLUDGE LANDFILL 11/22
Pace Project No.: 92634407
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92634407002
SWP-2
SM
4500-CI-E-2011
736047
92634407003
Q06V09
SM
4500-CI-E-2011
736047
92634407004
Q06V10
SM
4500-CI-E-2011
736047
92634407005
Q06V11
SM
4500-CI-E-2011
736048
92634407001
SWP-1
SM
5310E-2014
734737
92634407002
SWP-2
SM
5310E-2014
734737
92634407003
Q06V09
SM
531OB-2014
736855
92634407004
Q06V10
SM
531OB-2014
736855
92634407005
Q06V11
SM
531OB-2014
736855
Date: 12/21 /2022 11:11 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
Page 69 of 94

DC#_Title: ENV-FRM-HUN1-0063 v01 -Sample Condition Upon Receipt
= ace
lllll[i'„IY,11ii
Effective Cate: 05112/2022
Laboratory receiving samples -
Asheville Eden❑ Greenwood ❑ Huntersville ❑ Raleigh[] Mechanicsville❑ Atlanta[—] Kernersville❑
'; Client Name: Project #: WO# : 92634407
Ad
Courier: ❑Fed Ex []UPS' [—]LISPS []Client
❑ Commercial [�Race []other: II `
92634407
Custody Seal Present? ❑Yes [�Ko
Packing Material: ❑Bubble Wrap
Seals Intact? ❑Yes No
Bubble Bags [-]None ❑ Other
Thermometer: _
❑ I R Gun ID: 1 c' 7 Type of Ice: P(Wet
.36 Correction Factor:
Cooler Temp: " Add/Subtract ('C)
Cooler Temp Corrected (*C):
USDA Regulated Sol] (❑ N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC
1,Horle -.01 MVoc MHn
Date/Initials Person Examining Contents: i I i 1_� K
❑Blue []None
Biological Tissue Frozen?
❑Yes [_]No ❑NIA
Temp should be above freezing to 6°C
❑Samples out of temp criteria. Samples on ice, cooling process
has begun
Did samples originate from a foreign source (internationally,
includine Hawaii and Puerto Rico)? rlYes MNo
Comments/Discrepancy:
Chain of Custody Present?
Yes
[]NO
❑NIA
1.
Samples Arrived within Hold Time?
Yes
[]No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
[]Yes
grNo
❑N/A
3.
Rush Turn Around Time Requested?
[]Yes
allo
❑N/A
4.
Sufficient Volume?
wyes
❑No
[]N/A
5.
Correct Containers Used?
-Pace Containers Used?
(Yes
Yes
❑No
[:]No
❑N/A
❑N/A
6.
Containers Intact?
Yes
❑No
[-]NIA
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
Nrgo
❑N/A
8.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix: WL0
(Yes
[:]No
[]N/A
9.
Headspace in VOA Vials (>5.6mmJ?
❑Yes
No
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
JpNo
o
❑N/A
❑N/A
11.
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Lot ID of split containers:
Date/Time:
Field data Required? UYes UNo
Date: iJl r ),�� }
Date:
Qualtrax ID: 69614
Page 1 of 2
Page 70 of 94

DC#_Title: ENV-FRM-HUN1-0084 v01_Tech Spec Sample Condition
Upon Receipt
,/9ce-
1 wtv„--s
Effective Date: 05/12/2022
*Check mark top half of box if pH and/or dechlorination Project #
is verified and within the acceptance range for
preservation samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottles
***Check all unpreserved Nitrates for chlorine
fro# : 92634407,
pM: LJP
CLIENr: Due 9f3-01atlteale I�116122
uc
C
d
V
Z
c
Y
a
E
v,
rq
rl
V
a.
m
Z
c
4
b
J
E
o
N
f=r1
a
m
Z
v
c
7
u
cY,
E
o
O
N
a
m
\
Z
a
a
=
'-I
�-t
a
m
N
v
O
iv
=
U
m
a
,,,
eN-I
a.
m
N
V
Z
z
u
.N
E
a
N
M
a
m
Z
'z
Z
N
v
ro
E
„n
ti
II
a
Co
r-I
n
O�
Z
u
_..
b
a
E
cn
II
0.
m
C
a
N
a
L
a
❑
._-
v
°
c
❑
61
E
d
`m
=
j
•i
[7
C
N
a
U
z
W
E
Q
`m
=
i
rl
0
¢
V
a,
m
m
n
Q
4
of
Ln
M
0
Q
N
a
v
_
y
Q
`m
=
J
•i
0
¢
y
a
a
O
N
M:
2
E
E
a
J�
M
0
¢
v
z
20
E
E
d
M
Q
❑
Q
?
=
o
>
E
o
=
M
C7
❑
Z
m
Z
a
>>
E
f
M
0
>
Q
v
Z
y
v
>
E
0
7
(n
0
>
C
?
O
_
b
>
E
o
>
0%
C7
O
Q
Z
O
=
Q
O>
J
C1
C7
❑
Z
co
a+
Y
`m
°
r'
>
0
�
>
f0
in
E
N
l~[7
p,
Vf
f0
ro
m
i^
E
aN
iV
d
w
h'1
O
N
Z
u
a
E
oc
rn
a
co
a
v
j
¢
of
o
D
O
t7
d
=
h
o
—
E
�n
E
o
3
t+]
vs
7
a
Z
>
c
E
Q
E
v
G1
l7
❑
'Na
�
t
3
a
3
4
\—\�s
I
5
6
\-
N\\N
8
9
10
11
12
N\N
pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot It
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office {Le.
Out of hold, incorrect preservative, out of temp, incorrect containers)
Qua[trax Document ID: 70677
Page 2 of 2
Page 71 of 94

-1 Z Z
m A M
a„ o
b A D
i ; y
m rn Z
m
V I m
TEMP in C I I 16)
Received on Ice
(YIN)
Custody Sealed
Cooler
{Y!N)
i
Samples Intact
(YIN)
a
a
0
0
3
3
m
z
ti
y o m m F Ir vl sx w Iv E I ttYl #
N �
m
v�
�n
ape
y �m
�V@ m
Cr
v
a x
c '
m
11
a p
� o
CODE (sea valid md" to left}
TYPE (G=GRA6 C=COMPp
m
0
Cm
5
m
❑
oA
M
z
n
�
re
m
SAMPLE TEMP AT COLLECTION
# OF CONTAINERS
Unpreserved
fD
m
M
to
H2SO4
HNO3
HCI
NaOH
Na25203
Methanol
Other
Analyses Test
YIN
metals 2007
LL Hg
Alkalinily
Chloride, 50rale
TDS
TOG by 5310
VOC by 8250
Trip Blank (GOP must make
SVOC 6V0
LL Hg Blank
VOC by 8260-1.4 0ioxane O
Residual Chlorine (YIN)
SO
tC0 N - N S3 b p
N N � � �
n Z n y
❑ 0 Cl
C N {p
Co m
m
r n
rn
C
T
x �
m
m
3
.D
m
c
N
n
a
_W
9 Q. a 0 A N �
A m N, o
u o o a m N
3 O v o
° a C
C 3 N
cn o —
G a �'
O
m m N
m
Z j
a o
� g
r m
r
Z to 0
ro 3
=ten
tiL
9'
N @ o O
v
� C
� N 1
; <n0 n0
n m m a 3° `< C
V -0 0N 7 �' N-U N N
F_ O
m a m i m
3 0 p
a m mCP
A m Q
� C �
3 0 S1
_a Fri
o -1
° CL N /�
N ^ 0
^�
N CD
N N
�f
3 ❑
� C
0 a 0
w or 0
vrt, C
"0
n o
S @
❑.
n
C
n
z
0
Page 72 of 94

m a rn
Q
[A
3 3 N
b a Q
a
z 70 M
m
D
UM■
1
TEMP in C
Rece ved on Ice
(YIN)
Custody Sealed
Cooler
(YIN)
Intact
m
A
0
r?
u
z
0
�S t}Ivtfi
N)
� p r w cn
A w �v
I I GEYI ff
T!
O iJ
U
a
m m
j j
<
3 0 cn
.a
p
O
r—yb�
�
O
N N91
n T
o
r
n
c v M
z
o v
%
yp D�Ofnv�g�O
Ny Ly�r- 7
v
h1ATRTX CODE (see -fid codes to tell)
SAMPLE TYPE (G=GRAB C-COMP)
O
rl on
a
� p
I � �
J
r•. � 1 C-
I I SAMPLE TEMP AT COLLECTION
# OF CONTAINERS
Unpreserved
H2SO4
HNO3
V
Q
I j HCI
NaOH
w_
Na25203
C
m
N
Methanol
Other 16 f
Analyses Test
Y)
x
x metals 200.7
x
x LL Fig
x
x Alkalinity
x
x Chloride. Sulfata
x
x TDS
x
x TOC by 5310
x
x V01: by 6260
Trip Blank (COP -mull make
x
x SVOC 6270
LL Hg Blank
x
VOC by 6260-1,4 Dinxane 0
1>1
Residual Chlorine (YIN)
Q
S
G W
IN S
d
o
m
O
V °
10 sA
ro � O
O
N0 ` U
° o
°
a v'
— U7
— c
T
3
N
3
V
C,
N
S
7
N
m' m'
o a a
n m
= �.
it
c
-An a0. CW
3 o
n
ro o
° a
#
n
o
�p
w
C
0
a �
m
O Su
z
n
0
o
n
r-
r-
g
m
Z
n
0
a
3 0
M
Cr
�
'(°2
0 D
CL
N
7
Ov
57 0 -9
N
m m
� /1
rn p EF ` J
a 3 M° 4. 3� C/�
a(n0
o 0 0 m O
ro D
N �
� VI ❑ 1
A
O
a
C
°
�.
D!
K _
v
m
z�
0
o' �1
a
0
Nn�
a
o
m
a.
Q
m w` tD
" m CD
0
vcv
n n 0
D v t7
n 3
o °
3 -0 RD
� m �
v m
N f1
a in
0 n
M C
ui N
0
0
p
pl
d K
� .
C3 e
N
Page 73 of 94

Aace,
DC#_Title: ENV-FRM-HUN1-0083 01_5ample Condition Upon Receipt
Effective Date: 05/1212022
Laboratory re iving samples:
Asheville
Eden❑ Greenwood ❑ Huntersville ❑
Raleigh[:] Mechanicsville[]AtlantaF Kprnorc%AlI-r
Sample Condition
Client Name:
rUpon
Receipt
C-1 I
� � r J.�
Project #: WO : 92634447
Courier:
❑Fed Ex
[—]clientPM:
WP Due Dale: i1/18/22
❑UPS ❑LISPS
❑ Commercial
10pare
❑other:
CLIENT: 93-G l atf el to
Custody Seat Present? ❑Yes ZIVa Seals Intact? ❑Yes XNo
Packing Material: ❑Bubble Wrap ❑Bubble Bags KIU3None ❑ Other
Thermometer:
❑IRGunID: g3TC 71
Type of ice: �iM1let
?.� • �} h•`1,;. 7f 4-1,7/ �.3 Correction Factor: (V
Cooler Temp: Add/Subtract ("C)
Cooler Temp Corrected ('C): Ll .�, ¢� '� %r • 7r `
USDA Regulated Soil ( NIN/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or 5C
fcherk mansl? nYes MN❑
Date/Initials Person Examining Contents: I ! 2 r1
❑Blue ❑None
Biological Tissue Frozen?
[-]Yes ❑No ❑N/A
Temp should be above freezing to VC
[]Samples out of temp criteria. Samples on ice, cooling process
hasbegun
Did samples originate from a foreign source (internationally,
indudini, Hawaii and Puerto Ricol? r7Yes MNn
Comments/Discrepancy:
Chain of Custody Present?
ffYes
[]No
[]N/A
1.
Samples Arrived within Hold Time?
&es
❑No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes
[$No
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
r
o
[-]N/A
4,
Sufficient Volume?
Wes
❑No
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
Tyes
Mes
❑too
[:]No
❑NIA
❑N/A
6.
Containers Intact?
es
[]No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
[]Yes
Mo
❑N/A
B.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
Yes
L'o I
❑No
❑N/A
9.
Headspace in VOA Vials (>5.6mm)?
❑Yes
No
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
[]Yes
❑Yes
MNo
MNo
❑N/A
❑N/A
11.
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Lot ID of solit containers:
Date/Time:
Date:
Date:
Field Data Required? ❑Yes ❑No
Page 74 of 94
Qualtrax ID: 69614 Page 1 of 2

DC# Title: ENV-FRM-HUN1-0084 v01 Tech Spec Sample Condition
/ f aC1
Upon Receipt _
r 'mma Mcas
Effective Date: 05/12/2022
*Check mark top half of box if pH and/or dechlorination
is verified and within the acceptance range for
preservation samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottles
***Check all unpreserved Nitrates for chlorine
Proje WOE ; 926344Q7I
PM: LJP Due Date: 11/16/22
CLIENT: 93-Glatfelte
#
G
d
u
?
a
7
u
a
E
N
N
7
Q
a
m
Z
a
a
1
E
O
N
7
M
a
m
Z
n
a
E
O
In
7
N
a
m
Z
m
C
V
fo
a
w
+'
_
N
eel
a
m
U
N
v
O
N
a
E
eN-i
yr
Q
a
m
v
Q
2
U
o.
E
o
N
Z
M
a
M
O
Z
¢
Z
V
a
E
iN.{
N
Q
a.
m
n
O
Z
U
a
E
yr
N
m
Q
a
co
m
O
L
E
v
a
u
a
y
w
o
C
N
E
d
a
—
•--I
❑
H
c7
¢
N
v
n
_
CJ
7+
E
¢
m
—
N
2
N
V
4
a
c
E
d
E
o
N
7
rM
C7
4
V
a
Q
O
N
n
E
a
rH
N
H
t7
¢
S
a
O
2
E
¢
E
N
i%1
M
l7
4
?
=
z
E
Q
E
O
M
N
a
M
t9
❑
z
=
¢
O
E
❑
Q
2
in
0
in
4
Z
N
Z
C
p
J
E
O
[�
H
SI
0
N
v
Q
a
O
E
O
Q
7
M
C7
7
Q
Z
0.
a
O
E
O
Q
>
M
C7
❑
_
d
Z
v
O
n
a
O
?
E
O
Q
of
M
47
d
a
m
Q
>
A.
10
}
.M..
0
7
?
u
"
E
y
vi
E
Ln
.N-1
F,
In
a
vi
?
u
V
d
Ln
E
O
N
'L
N
a
N
Z
y
m
E
O
vi
N
Cr
M
a
m
a
a
c
E
Q
E
o
O
N
7
O
C7
¢
y
C
O
c
an
E
O
N
t}
v+
7
Z.
v
Q
C
fl
Q
E
O
Q
7
Cn
t7
O
3
4
f
1
5
6
7
8
9
to
11
12
N
NNNI
I
...
pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot #
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers)
Qualtrax Document ID: 70677
Page 2 of 2
Page 75 of 94

0
aceAnalytical
Report of Analysis
Pace Analytical Services, LLC
2225 Riverside Drive
Asheville, NC 28804
Attention: Lord Patton
Project Name: Sludge Landfill 11-22
Project Number: 92634407
Lot Number:XL05027
Date Completed:12/13/2022
12/14/2022 9:02 PM
Approved and released by:
Project Coordinator 1: Jenna S. Holliday
pCC/►F0
ANSI National Accreditation Board
qe�
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 76 of 94
Page 1 of 17

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Pace Analytical Services, LLC
Lot Number: XL05027
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPS or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 77 of 94
Page 2 of 17

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Pace Analytical Services, LLC
Lot Number: XL05027
Project Name: Sludge Landfill 11-22
Project Number: 92634407
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
SWP-1
Aqueous
11/02/20221130
12/03/2022
002
SWP-2
Aqueous
11/02/20221245
12/03/2022
003
Q06V09
Aqueous
11/03/20221110
12/03/2022
004
Q06V10
Aqueous
11/03/20221020
12/03/2022
005
Q06V11
Aqueous
11/03/20221035
12/03/2022
006
FIELD BLANK
Aqueous
11/03/2022 1130
12/03/2022
(6 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 78 of 94
Page 3 of 17

PACE ANALYTICAL SERVICES,
LLC
Detection Summary
Pace Analytical Services, LLC
Lot Number: XL05027
Project Name: Sludge Landfill 11-22
Project Number: 92634407
Sample Sample ID
Matrix Parameter Method
Result Q
Units
Page
001 SWP-1
Aqueous Mercury (CVAFS) 1631E
2.77
ng/L
5
004 Q06V10
Aqueous Mercury (CVAFS) 1631E
14.2
ng/L
8
005 Q06V11
Aqueous Mercury (CVAFS) 1631E
1.48
ng/L
9
(3 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 79 of 94
Page 4 of 17

Mercury (CVAFS)
Client: Pace Analytical Services, LLC Laboratory ID:XL05027-001
Description: SWP-1 Matrix: Aqueous
Date Sampled:11/02/2022 1130 Project Name: Sludge Landfill 11-22
Date Received:12/03/2022 Project Number: 92634407
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 12/08/2022 1230 JA132 12/06/2022 1155 61800
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Mercury (CVAFS) 7439-97-6 1631 E 2.77 0.625 ng/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 17
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 80 of 94

Mercury (CVAFS)
Client: Pace Analytical Services, LLC Laboratory ID:XL05027-002
Description: SWP-2 Matrix: Aqueous
Date Sampled:11/02/2022 1245 Project Name: Sludge Landfill 11-22
Date Received:12/03/2022 Project Number: 92634407
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 12/08/2022 1235 JA132 12/06/2022 1155 61800
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Mercury(CVAFS) 7439-97-6 1631E ND 0.625 ng/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 17
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 81 of 94

Mercury (CVAFS)
Client: Pace Analytical Services, LLC Laboratory ID:XL05027-003
Description: Q06V09 Matrix: Aqueous
Date Sampled:11/03/2022 1110 Project Name: Sludge Landfill 11-22
Date Received:12/03/2022 Project Number: 92634407
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 12/08/2022 1241 JA132 12/06/2022 1155 61800
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Mercury(CVAFS) 7439-97-6 1631E ND 0.625 ng/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 17
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 82 of 94

Mercury (CVAFS)
Client: Pace Analytical Services, LLC Laboratory ID:XL05027-004
Description: Q06V10 Matrix: Aqueous
Date Sampled:11/03/2022 1020 Project Name: Sludge Landfill 11-22
Date Received:12/03/2022 Project Number: 92634407
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 12/08/2022 1246 JA132 12/06/2022 1155 61800
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Mercury (CVAFS) 7439-97-6 1631 E 14.2 0.625 ng/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 17
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 83 of 94

Mercury (CVAFS)
Client: Pace Analytical Services, LLC Laboratory ID:XL05027-005
Description: Q06V11 Matrix: Aqueous
Date Sampled:11/03/2022 1035 Project Name: Sludge Landfill 11-22
Date Received:12/03/2022 Project Number: 92634407
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 1631 E 1 12/08/2022 1252 JAB2 12/06/2022 1155 61800
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Mercury (CVAFS) 7439-97-6 1631 E 1.48 0.625 ng/L 2
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 17
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 84 of 94

Mercury (CVAFS)
Client: Pace Analytical Services, LLC Laboratory ID:XL05027-006
Description: FIELD BLANK Matrix: Aqueous
Date Sampled:11/03/2022 1130 Project Name: Sludge Landfill 11-22
Date Received:12/03/2022 Project Number: 92634407
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 12/08/2022 0956 JA132 12/06/2022 1155 61800
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Mercury(CVAFS) 7439-97-6 1631E ND 0.625 ng/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 17
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 85 of 94

QC Summary
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: XL05027
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 86 of 94
Page 11 of 17

Mercury (CVAFS) - MB
Sample ID: XQ61800-001 Matrix: Aqueous
Batch: 61800 Prep Method:
Analytical Method: 1631 E Prep Date: 12/06/2022 1155
Parameter Result Q Dil LOQ Units Analysis Date
Mercury (CVAFS) ND 1 0.500 ng/L 12/07/2022 0520
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 17
QC Data for Lot Number: XL05027
Page 87 of 94

Mercury (CVAFS) - MB
Sample ID: XQ61800-101 Matrix: Aqueous
Batch: 61800 Prep Method:
Analytical Method: 1631 E Prep Date: 12/06/2022 1155
Parameter Result Q Dil LOQ Units Analysis Date
Mercury (CVAFS) ND 1 0.500 ng/L 12/07/2022 0525
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of 17
QC Data for Lot Number: XL05027
Page 88 of 94

Mercury (CVAFS) - LCS
Sample ID: XQ61800-002 Matrix: Aqueous
Batch: 61800 Prep Method:
Analytical Method: 1631 E Prep Date: 12/06/2022 1155
Spike
Amount Result %Rec
Parameter (ng/L) (ng/L) Q Dil % Rec Limit Analysis Date
Mercury (CVAFS) 6.25 5.96 1 95 75-125 12/07/2022 0531
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 14 of 17
QC Data for Lot Number: XL05027
Page 89 of 94

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 90 of 94
Page 15 of 17

PACE ANALYTICAL SERVICES, LLC
1 a T
c LS i
r
�
e+
1 G
Gs
3
� q
u
4 Cv #
"'J a
r
tri
7_
0T Euili
�
C
[a tJ O
sr
43
at
�x+F7G;.G151
m
J'}
E
{y
"
`m
r
lip
Q . iy
a)
7f J
-0 C3 '�
r cw
en
4i
qo
1-2
La
J
Al 4F
O4
fi
4
c
OS '9 -
a
^ " 7t
J u
[+} =
E
fm N
n
e4
k3
❑ Ai
r3
*l
i�d
r
yak•
[Y qa
�y1�rIv,
5[J
Sim
I�
I
c,�ryy
U ,
# I
•�
_
_73
}
m
L
3 N g13
m
T L
n
�
5.V
Jwl
AA�Qy
ti V 5
yN .r
J L I E
J2
1
03
d Z
o
d
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 16 of 17
Page 91 of 94

PACE ANALYTICAL SERVICES, LLC
D _1A1e: EPIV-FRM-WCO)[ i)286 vU2=52rnpl4as Reconlpt Checklt-,t (SR-Cl
EffgCtrVe DaU: 8j2/2422
Sample Receipt Cheddist (,SR C
Cheul : Face .. CQ' Jam' 1 il; t;p Wd by1(JAtP.: KD-K' ' j I J,M 2022 Foi l: XIM27
�e Cliedt L)UPS L6FOdEx O! ei _
1. kVw ea5to srais pfuIs 011 the corder?
2. IfulsIvdy 6Ca15 wefe prescle. vret- Umv jMMt aw UUb]y1kr-n7
pH SUIp [D: MA MlTnine StLip ID: NA 7�sted by: NA
O" irlal tempest[" ttpm rece:ptl DeAved (CcwtWcd) tcgteratilfe ttpolj rtjct<ip1 %Solid Sj]aj C ID. NA
15,3 r'i63 0 NA VNA Dj— LdA ETA °- TxA fyj —
etLutl: ❑ emptmturc 131awk ©A4 inst Botan IR Gwi iD: s 1R Giza Corticctjon Fts ac°
M4etbud Ofcoplmir [VA( Wei Icc ice Pads M F)r w rcc Ncue
ElYts [two a -A a. well' coolm received at or
LJ L�-JJ I���l�ti P was Notified by:111MO r` r
E;5,
rao A 4. is fhe corim=iw cotulcr's liar
No 5. %3p`erc p er Ctutodv 7ixxndw
1;ke-:+mace (circle o¢rc),
Clip avached to this f=t
1�Tar fi. Were sample IDs iistcd m the COC wad rill qa na le ca
as Collection date &. lime listed i�t the C'OC auld all
T Tn S_ Did ail =Itniiler ISM iulomlation (D, dalt- 'i c) agl
No 9_ WCX un1x to br. PM-C lad Used tut the COC?
follawa[l'�
tttloCc?
npk cantai .ESI
wilt the CO
Zy ❑""TD 10, Did all &urrples arriv-c [31 acproper c(ntlaiucrs for each tc56FUldfor ill good cuudilion
ivabrokcrl, Lids on, cx.)?
� 1'-eS Nn 11 _ '���aS ad.gttate sa>�Ic ��a]tttne g�raitablc't
Yes Nr 12. 14'cra all sxutplcx ripeived within fhc h ldiu^ rinse or 48 hmnq, whichnmr comps first''
ZYtS No 1.3, V4`M all sank t-On#:tiflen accounted for'' (No inissirrZ*w:ss)
YestNOA
14.1� eie VOA, W15C and RSK-175 satuples fire -af lutbbles >`lpea_.q ' (Y."or 61tit711 a
diameter) in am,' of dw VOA ALL?
'cs f 5. Vl�cre all DR h wafsiurtt�eut san lrtts roceived al a aH ot< 2?
des16. wcra Art do ; I-ci v1CS recehwal a PK > 12 and Sulu& sarvplL,� irc"ived eta .�QYes _residmd�Ycs 18. Vd$s Lire a2ra'cuttu�bet listed o>l llhc container Jaoel7liy-,s, {quote i€
58knple ft- servatiou (Musl he caurplUrd f0l- any Ott I�ple(Sj fik` 7lecd pmscrvcd or wilt heAds[ c.)
samplc(s) rre were received ineorrectlyprcwt-wLt and we[e adjusted accorffiig.ly
u SR]n rlc recel� Xlth MA- Tul- of circle otne- Id2SO4, I TNO3, HCJ- NaOE1 asitlg SR -0 p,
Mile Ofplestxvattiarl N #� _ If arc �]sur Vttr preset v:�ti ve is ueedell, Please note in the ru�Trr nts below_
xaYtp] (s) . were received ih th bubbles-6 tnut iu die meter_
ittt1111 s) wcre receirrd l irh'1'RC > 0, 5 mgrL (If # l is rry ) and weir
djt41,"d accorduO; in Sample receiving with sodhwi ijdoSul Fite (NahS,05j with Uni€ tic ID: N�
��o�luaixatt�:
Qualtrax 10:563f0 Pace' A ftaFyfiripl Servkea, LLC page I of 1
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 17 of 17
Page 92 of 94

N
O
-n
P
C7
> O O
r n
CJ �?
fD
O a
I
9
o
a
3 0
m c-
m rho
l
1
S
v
C � f
uj p s N p
a o
n �
n N
m
Page 9.3 of 94

r ro
G
0
I
C\
o
r n
o �
0
o
6'
+Gd
�
r
0rD
cV
.'
O
(�
.
t.
� �
Y
�
S
�
r
f•
n
Co.
`
1F age 94 of 94
r