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HomeMy WebLinkAboutWQ0004972_Monitoring - 02-2023_20230330Monitoring Report Submittal ................................................... Permit Number#* WQ0004972 Name of Facility:* Forest Lakes Preserve ELS Month: * February Year: * 2023 Report Information Type* Upload Document* NDMR, NDAR-1, NDAR-2, NDMLR Forest Lakes_February.pdf 1.83MB PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Confirmation Email Address: * Jessica. Mize@pacelabs.com Name of Submitter: * Jessica Mize Signature: je"&A jot Date of submittal: 3/30/2023 This will be filled in automatically Initial Review Reviewer: Wanda.Gerald Is the project number correct?* W00004972 Is the monitoring report accepted?* Yes NO Regional Office* Winston-Salem Reviewer: _anonymous Review Date: 4/24/2023 Page 1 of 2 NON -DISCHARGE WASTE WATER MONITORING REPORT PERMIT NUMBER: W00004972 MONTH: February YEAR: 2023 FACILITY NAME: Forest Lakes Preserve ELS COUNTY: Davie Flow Monitoring Point: Effluent: y I Influent: Parameter Monitoring Point: Effluent: I Influent I Surface Water(SW):,SW Code/Name: Was There Effluent Flow for this Month Generated At This Facility: Yes N N D A T N. Operator Arrival Time 2400 Clock Operator Time on Site ORC on Site? 50050 00400 1 50060 00310 1 00610 00530 31616 00665 00625 00630 00600 1 00620 70300 0094C Daily Rate (Flow) into Treatment S)stan pH Residual Chlorine OOD-5 20*C NH-3-N TSS Fecal Col,f rot (Goo -metric Mcen•I Total ph. Total Kieldhal Nitrogen NO.' `,us Total Nitrogen Nitrate N0.3-N Total Dissohcd Solids Mori& HRS YIN GPD 'NITS mg'L xt(1'L MG L fU I. 100ML MG L MG/L 1 MG L M(i MG L MG t 17annuuus - t _ 1 ' i,i',... `.: �.'. '.', oni 4 ont )' ont •.' `.' '.: `.: ... _..' t 1715 0.25 B 13,241 6.6 <0.01 1515 0.25 It 11.874 6.6 <0.01 3 0900 0.25 B 10,092 6.7 <0.01 1 12.131 5 12,131 a 1251) 0.50 B 12,131 7.3 <0.01 7 1505 0.25 B 9,237 1 7.3 <0.01 s 1 1610 1 0.25 B 11,911 7.4 <0.01 9 1550 0.25 B 8,823 7.4 <0.01 to 1445 0.25 It 7,797 7.5 <0.01 11 12,531 12 12.531 13 1435 0.25 B 12,531 7.3 <0.01 46.4 44.7 11.7 24211 6.1 62.7 <0.040 62.7 <0.040 14 1425 0.25 1 It 9.5553 7.3 <0.01 15 1235 0.25 B 10,189 7.3 <0.01 16 1510 0.25 It 10.237 7.8 <0.11I 17 1025 0.25 B 10.252 7.4 <0.01 IN 12.841 19 12,841 20 1450 0.25 It 12.841 7.5 <0.01 21 1350 0.25 1 B 6.293 7.5 <0.01 22 0945 0.25 B 6.685 7.4 <0.01 23 1405 0.25 B 6,916 7.6 <0.01 24 1055 0.25 B 6,631 7.4 <0.01 25 9,277 26 9,277 27 1600 0.25 B 9,277 7.5 <0.01 2s 1225 0.25 B 10.943 7.6 <0.01 29 30 It Average 10,393 <0,01 6. 11.7 '_-l-11 7 6_. < , <0.040 Daily Maximum 13,241 7.8 <0.01 11.7 24211 6.1 fi_. <0.040 <0.040 Daily Minimum 6.293 6.6 <0.01 46.4 44.7 11.7 24211 6.1 62.7 <0.040 62.7 <0.040 Monthly Limits hl 24400 Composite -: / Grab (G) Operator in Responsible Charge (ORC): Glenn Price Grade: 11 Phone: 336-996-2841 Check Box if ORC Has Changed: I ORC Certification Number: 987931/20771 Certified Laboratories (1): Pace Analytical Serivices (2): Person(s) Collecting Samples: Glenn Price Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit X _ DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) Division of Water Quality By this signature, 1 certify that this report is accurate and 16117 Mail Service Center complete to the best of my knowledge. RALEIGH, NC 27699-1617 DENR Form NDAR-1 (5/2003) NON DISCHARGE WASTEWATER MONITORING REPORT FACILITY STATUS: Please answer the following question: Com liant Y,N) 1. Does all monitoring data and sampling frequencies meet permit requirements? If the facility is non-comoliant, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 17— -__� 3, 3d ` Baron Neal McDuffie (Signature of Permitee)* 4V Date (Name of Signing Official -Please print or type) Baron Neal McDuffie (Authorized Agent) (Permittee-Please print or type) 2N Riverside Plaza , Suite 800 Chicago, Il 60606 (Permittee Address) 01002 Arsenic 01022 Boron 00310 BOD5 01027 Cadmium 00916 Calcium 00940 Chloride 50060 Chlorine, Total Residual 01034 Chromium 00340 COD 31504 Coliform, Total 00094 Conductivity 01042 Copper 00300 Dissolved Oxygen 31616 Fecal Coliform 01051 Lead 00927 Magnesium 71900 Mercury 00610 NH3 as N 01067 Nickel Field Services Director (Pace Analytical Services) (Position or Title) 3/31/21 (Permit Exp. Date) 00600 Nitrogen, Total 00630 NO2 & NO3 00620 NO3 00556 Oil & Grease WQ09 PAN Plant Available) 00400 pH 32730 Phenols 00665 Phosphorus, Total 00937 Potassium 00545 Settleable Matter 00929 Sodium 00931 SAR 00745 Sulfide 00515 TDS 00010 Temperature 00625 TKN 00680 TOC 00530 TSS/TSR 00076 Turbidity 01092 Zinc Parameter Code assistance may be obtained by calling the Water Quality Compliance/Enforcement Unit at (919) 733-5083, extension 529. The monthly average for Fecal Coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting facility's permit for reporting data. * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 213.0506 (b) (2) (D). Page 2 of 2 NON-DISCIIARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED PERMIT NUMBER: W00004972 MONTH: February YEAR: 2023 FACILITY NAME: Forest Lakes Preserve ELS. COUNTY: Davie Formulas: Daily Loading (inches) = [Volume Applied (gallons) x 0.1336 (cubic feetigallon) x 12 (incheslfoot)] / [Area Sprayed (acres) x 43.560 (square feet/acre) or = [Volume Applied (gallons) / [Area Sprayed (acres) x 27,152 (gallons/acre-inch). Mawmum Hourly Loading (inches) = Daily Loading (inches) / (Time irrigated (minutes) / 60 (minutes/hour)] Monthly Loading (inches) =Sum of Daily Loading (inches) 12 Month Floating Total (inches) = Sum of this month's Monthly Loading (inches) and previous 11 month's Monthly Loadings (inches) Average Weekly Loading (inches) = [Monthly Loading (inchestmonth) / Number of days in the month (days/month )] x 7 (daystweek) b�cijringiifion Occur At This Facility: Did Irrigation Occur On This Field Did Irrigation Occur On This Field .r • • •Permitted Yearly Rate (inches) n enmer 1-1; l -near. --I y --y, l lrrloutly, K-ralll. Nn-nnaw, it-sicrr Spray Irrigation Operator in Responsible ('harge (ORC): Glenn Price Phone: 336 996-2841 ORC Certification Number: 987931/20771 Check Box if ORC Has Changed: 0 Mail ORIGINAL, and TNo COPIES to: A-I"I'N: Non -Discharge Compliance Unit \ �( DENII (SIGNA'11111F. OF OPERATOR IN RESPONSIBLE (11ARGE) Division of Water Quality By this signature, I certify that this report is accurate and 1617.Nlail Service ('enter complete to the best of my knowledge. RALEIGII, N(- 27699-1617 DENR Form NDAR-1 (5/2003) NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) FACILITY STATUS: Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been compliant with the following permit requirements: (Note: If a requirement does not apply to your facility put (NA) in the compliant box.) Compliant (Y,N) 1. The application rate(s) did not exceed the limit(s) specified in the permit. Z Adequate measures were taken to prevent wastewater runoff from the site(s). 3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit. 4 4. All buffer zones as specified in the permit were maintained during each application. 5. The freeboard in the treatment and/or storage lagoon(s) was not less than the limit(s) specified in the permit. If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 3 Baron Neal MCDUffie (Signature of Permitee)* Date (Name of Signing Official -Please print or type) Baron Neal McDuffie (Authorized Aeent) (Permittee-Please print or type) 2N. Riverside Plaza, Suite 800 Chicago, 11 60606 (Permittee Address) Field Services Director (Pace Analytical Services) (Position or Title) 3/31 /202 l (Permit Exp. Date) * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 213.0506 (b) (2) (D). aceAnalytical www.pacelabs.com March 23, 2023 Tracy Overdurf Forest Lake 192 Thousand Trails Dr. Advance, NC 27006 RE: Project: Forest Lake Pace Project No.: 92656585 Dear Tracy Overdurf: Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Enclosed are the analytical results for sample(s) received by the laboratory on March 13, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Eden If you have any questions concerning this report, please feel free to contact me. Sincerely, c�t�tt.dX.� Stephanie Knott stephanie.knott@pacelabs.com 704-977-0981 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 16 IeAnalytical OD + www.pacelabs.com I CERTIFICATIONS Project: Forest Lake Pace Project No.: 92656585 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 South Carolina Laboratory ID: 99030 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 North Carolina Drinking Water Certification #: 37712 VirginiaNELAP Certification #: 460222 North Carolina Wastewater Certification #: 40 Pace Analytical Services Eden 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633 North Carolina Drinking Water Certification #: 37738 VirginiaNELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 16 aceAnalytical + www.pacelabs.com I SAMPLE ANALYTE COUNT Project: Forest Lake Pace Project No.: 92656585 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92656585001 Effluent SM 254OD-2015 VLG 1 PASI-E EPA 353.2 Rev 2.0 1993 SRS 2 PASI-E SM 521OB-2016 SRS 1 PASI-E Colilert-18 VLG 1 PASI-E TKN+NO3+NO2 Calculation MAB2 1 PASI-A EPA 350.1 Rev 2.0 1993 ARJ 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 365.1 Rev 2.0 1993 Zip 1 PASI-A PASI-A = Pace Analytical Services - Asheville PASI-E = Pace Analytical Services - Eden REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 16 aceAnalytical KWV.p8C818bII.C6t[I I ANALYTICAL RESULTS Project: Forest Lake Pace Project No.: 92656585 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Sample: Effluent Lab ID: 92656585001 Collected: 03/13/23 14:35 Received: 03/13/23 16:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 254OD-2015 Pace Analytical Services - Eden Total Suspended Solids 11.7 mg/L 6.7 1 03/14/23 14:31 353.2 NO2/NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, NO2 plus NO3 ND mg/L 0.040 1 03/14/23 17:13 Nitrogen, Nitrate ND mg/L 0.040 1 03114123 17:13 14797-55-8 5210B BOD, 5 day EDN Analytical Method: SM 521 OB-2016 Preparation Method: SM 521OB-2016 Pace Analytical Services - Eden BOD, 5 day 46.4 mg1L 2.0 1 03/14/23 10:01 03/19/23 12:05 Colltert-18 Fecal Coliform EDN Analytical Method: Colilert-18 Preparation Method: Colilert-18 Pace Analytical Services - Eden Fecal Coliforms 2420 MPN/100ml- 1.0 1 03/13/23 18:05 03/14/23 12:52 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services - Asheville Total Nitrogen 62.7 mg/L 0.040 1 03/21123 14:18 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia 44.7 mg/L 1.0 10 03/22/23 11:37 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Kjeldahl, Total 62.7 mg/L 2.5 5 03/17/23 16:40 03/18/23 05:16 7727-37-9 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 6.1 mg/L 0.10 2 03/23/2311:39 03/23/2315:23 7723-14-0 Date: 03/23/2023 05:26 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.L.C. B 1. B3, L1 El Page 4 of 16 1�5aceAnalyti+cal + www.pacelabs.com i QUALITY CONTROL DATA Project: Forest Lake Pace Project No.: 92656585 QC Batch: 761195 Analysis Method: SM 254OD-2015 QC Batch Method: SM 254OD-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92656585001 METHOD BLANK: 3953720 Associated Lab Samples: 92656585001 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 3953721 Parameter Units Total Suspended Solids mg/L Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 03/14/2314:27 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 256 102 90-110 SAMPLE DUPLICATE: 3953722 92656412001 Dup Parameter Units Result Result Total Suspended Solids mg/L ND ND SAMPLE DUPLICATE: 3953723 92656585001 Dup Parameter Units Result Result Total Suspended Solids mg/L 11.7 11.5 RPD Qualifiers RPD Qualifiers 2 Results presented on this page are In the units Indlcated by the "Units" column except where an alternate unit Is presented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/23/2023 05:26 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 16 aceAnalytical www.pacerabs.com QUALITY CONTROL DATA Project: Forest Lake Pace Project No.: 92656585 QC Batch: 761304 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92656585001 METHOD BLANK: 3954405 Matrix: Water Associated Lab Samples: 92656585001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg/L ND 0.040 03/14/23 17:06 Nitrogen, NO2 plus NO3 mg/L ND 0.040 03/14/23 17:06 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3954406 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 1.5 1.5 100 90-110 Nitrogen, NO2 plus NO3 mg/L 2.5 2.4 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3954407 3954408 MS MSD 92656494001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L ND 1.5 1.5 1.6 1.5 108 102 90-110 5 Nitrogen, NO2 plus NO3 mg/L 0.62 2.5 2.5 3.3 3.2 108 104 90-110 3 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/23/2023 05:26 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 16 aceAnalytical 1 www,pacolabs.com I QUALITY CONTROL DATA Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Project: Forest Lake Pace Project No.: 92656585 QC Batch: 761186 Analysis Method: SM 521OB-2016 QC Batch Method: SM 521OB-2016 Analysis Description: 5210E BOD, 5 day Final EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92656585001 METHOD BLANK: 3953687 Matrix: Water Associated Lab Samples: 92656585001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers BOD, 5 day mg/L ND 2.0 03/19/23 11:47 B3 LABORATORY CONTROL SAMPLE: 3953688 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers BOD, 5 day mg/L 198 302 153 84.6-115 B3,1-1 SAMPLE DUPLICATE: 3953690 92656449001 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mg/L 2120 2070 3 133,1-1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 03123/2023 05:26 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 16 aceAnalytical www.pacelabi.com QUALITY CONTROL DATA Project: Forest Lake Pace Project No.: 92656585 QC Batch: 761115 Analysis Method: Colilert-18 QC Batch Method: Colilert-18 Analysis Description: Colilert-18 Fecal Coliform EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92656585001 SAMPLE DUPLICATE: 3953514 92656585001 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms MPN1100mL 2420 2420 0 El Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/23/2023 05:26 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 16 1�55'neAnalyficalo J www.pacelabs.com I QUALITY CONTROL DATA Project: Forest Lake Pace Project No.: 92656585 QC Batch: 762607 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.01993 Analysis Description: 350.1 Ammonia Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92656585001 METHOD BLANK: 3960479 Associated Lab Samples: 92656585001 Parameter Units Nitrogen, Ammonia mg/L LABORATORY CONTROL SAMPLE: 3960480 Parameter Units Nitrogen, Ammonia mg/L Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.10 03/22/2310:56 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 5 5.0 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3960481 3960482 MS MSD 92657433001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L 13.7 5 5 18.8 18.9 103 104 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3960483 3960484 MS MSD 92657612001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L ND 5 5 5.3 5.3 106 106 90-110 0 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/23/2023 05:26 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 16 aceAnaljftal aww.pacelaEs.com Project: Forest Lake Pace Project No.: 92656585 QC Batch: 762117 QC Batch Method: EPA 351.2 Rev 2.01993 Associated Lab Samples: 92656585001 METHOD BLANK: 3958575 Associated Lab Samples: 92656585001 Parameter Units Nitrogen, Kjeldahl, Total mg/L QUALITY CONTROL DATA Analysis Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services - Asheville Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.50 03/18/23 03:46 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3958576 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 10.6 106 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3958577 3958576 MS MSD 92656582002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 69.0 10 10 79.2 76.6 102 76 90-110 3 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3958579 3958580 MS MSD 92656582003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 58.3 10 10 68.9 69.7 106 114 90-110 1 M1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 03/23/2023 05:26 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 16 aceAnalytical www.pscelabs.com I QUALITY CONTROL DATA Project: Forest Lake Pace Project No.: 92656585 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 762990 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92656585001 METHOD BLANK: 3962417 Matrix: Water Associated Lab Samples: 92656585001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg1L ND 0.050 03/23/2315:15 LABORATORY CONTROL SAMPLE: 3962418 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.5 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3962419 3962420 MS MSD 92655582010 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 1.5 2.5 2.5 4.2 4.2 107 106 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3962421 3962422 MS MSD 92656551001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 4.5 2.5 2.5 7.1 7.2 105 107 90-110 1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 0312312023 05:26 PM without the written consent of Pace Analytical Services, I.I.C. Page 11 of 16 aceAnalytical xwp.pacelabsxam QUALIFIERS Project: Forest Lake Pace Project No.: 92656585 DEFINITIONS OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. NO - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 PQL - Practical Quantitation Limit. RL - Reporting limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS B1 Less than 1.0 mg/L DO remained for all dilutions set. The reported value is an estimated greater than value and is calculated for the dilution using the least amount of sample. 83 The dissolved oxygen depletion of the dilution water blank exceeded 0.2 mg/L. El Reported value should be considered a minimum estimate since it is the maximum reportable number for this method based on the sample volume used. The true value is likely greater than the value reported. L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples may be biased high. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/23/2023 05:26 PM without the written consent of Pace Analytical Services, L.L.C. Page 12 of 16 W aceAnalytical www.pacelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Forest Lake Pace Project No.: 92656585 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92656585001 Effluent SM 254OD-2015 761195 92656585001 Effluent EPA 353.2 Rev 2.0 1993 761304 92656585001 Effluent SM 521OB-2016 761186 SM 521OB-2016 761462 92656585001 Effluent Colilert-18 761115 Colilert-18 761116 92656585001 Effluent TKN+NO3+NO2 762748 Calculation 92666585001 Effluent EPA 350.1 Rev 2.0 1993 762607 92656585001 Effluent EPA 351.2 Rev 2.0 1993 762117 EPA 351.2 Rev 2.0 1993 762266 92656585001 Effluent EPA 365.1 Rev 2.0 1993 762990 EPA 365.1 Rev 2.0 1993 763338 Date: 03/23/2023 05:26 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 13 of 16 CHAIN -OF -CUSTODY / Analytical Request Document ace The Chain -Dr Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. 11 - ---I A AAA f—pa 1,1 - 0— T.....-n r fitu,nc (mind nr Anne /fmfn naeelnhs com/huhfsloas-standard-telms.Ddf Section A B Section C Required Cliant information: Required ProJoet Information: Invoice Information: If 1 Required WOE a 92656586 nY' Forest Lake aeon To Tracy Overme n n ess 10 Thousand Trails Dr Y To. nce. NC 27006 rats: !11 mail ovardu0 u com 7aseOrderffi auote: 8Z836S83 no" NONE FeX Name. Forest Lake Monthly xe project Manor: sleohane.knc equested Due Dam' lea N aco Profile t: 12254 �... Fiftared tN c o a COLLECTED Preservatives LZ NXTIUX LODE omk.v W� Dw yy X V V Q W Wsw NT wa,ew, Ww SAMPLE ID o p � OL one Character per box- vfD' VIPiiyyy� (A-Z. 0-9 1, •) On.r oT Sample Ids must be unique Ti— TS 7tff g c7 {= s� �i START END V F a F iz w Z i n a v� 1� O O Q a _ a DATE T ME DATE TIME 1 EFFL,:"T f X x X X X % 2 3 4 6 6 7 6 8 10 11 12 ADD MX" COst1101"" lit"QuL41,11H) BY IAfnUAT10N DATE TIME ACCEPM ff f Aff=7M DATE TM SAMME CONomxs $3/15 PLEB Waft: AND SMTQ V � $ a c z � e E 2 PRINT Name of SAMPL22 SIGM7URE of SAMPLER DATE SI d: ? qno DC#_Title: ENV-FRM-HUNI.0084 v01_Tech Spec Sample Condition f�aCg Upon Receipt Effective Date: 05R212022 Laboratory receiving samples: Asheville ❑ Eden ❑ Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville[] Atlanta[] Kernersville[l Sample Condition Upon Client Name: Receipt Project It: -_ ------------- __ ___ _ _ __ _. _ _ __ _ __ F 0 r e ,t Courier: Fed Ex ❑UPS ❑USPS ❑Client El Commercial Pace ❑Other:_.__ Carrier Tracking Number: Custody Seal Present? ❑Yes [ZNo Seals Intact? ❑Yes []No Date/Initials Person Examining Contents: Packing Material: ❑Bubble Wrap ❑Bubble Bags None ❑ Other Biological Tissue Frozen? [Dyes []No ❑N/A Thermometer: ❑ IR Gun ID: " T 0 0 2,Type of Ice: ❑ Wet []Blue ❑ None Cooler Temp ('C ): ' _± Correction Factor: Add / Subtract ('C ) Temp should be above freezing to 6'C 0 ❑Samples out of temp criteria. Samples on ice, cooling process Corrected Cooler Temp ('C 1: has begun USDA Regulated Soil ( 16 N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? 0 d samples ong nate from a foreign source (internationally, ❑Yes QNo including Hawaii and Puerto Rico)? ❑Yes ❑No Comments/Discrepancy: Chain of Custody Present? Elyes []No ❑N/A 1. Samples Arrived within Hold Time? OYes rINo N A 2. Short Hold Time Analysis (<72 hr.)? EfYes EJNo N/A 3. Rush Turn Around Time Requested? []Yes [TNo []N/A 4. Sufficient Volume? ZYes No N/A 5. Correct Containers Used? -Pace Containers Used? ('' Yes Yes ❑No []NO ❑N/A ❑N/A 6. Containers Intact? CrYes No N/A 7. Dissolved analysis: Samples Field Filtered? Yes No [3f4/A B. Sample Labels Match COC? Includes Oate/Time/10/Analysis Matrix: p]Yes sV7 []No ❑N/A 4 Headspace in VOA Vials (>5.6mm)? Yes No N/A 10. Trip Blank Present? Trip Blank Custody Seals Present? []Yes Ye; []No No ❑N/A N/A 11. COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes ❑No Temp Log: Temp must be maintained at <6 C during login, record temp every ZO minutes. Time opened: I b 0 0 Temp: Time: j d 0 put in cooler Time: Temp: Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person Contacted: __ ........ _........... Date/Time: Project Manager SCURF Review: Date: Project Manager SRF Review: Date: Qualtrax Document ID: 70677 Page 1 of 2 Page 15 of 16 DC# Title: ENV-FRM-HUN1.0084 v01 Tech Spec Sample Condition �ce Upon Receipt Effective Date: 05112/2022 I WVIiWHMd1 *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/9015 (water) DOC, LLHg **Bottom half of box is to list number of bottles ***Check all unpreserved Nitrates for chlorine Project # I 2 W 2 W Z W z N V ry V x Z - a Z) 9 .x N V V i a ? C C C d p 0 m z V Q n Z a •i0 l'J U`I a Q C [r Q i V N '_ .Z.,. Z \ Z 2 m ON ; LN z C ? Q 0.X N 1— N S d C =y ? C yZ Q J 7 J c = a = a S a r2j S Z a is j ¢ d E a' E Q U a r Z 4¢ > a Q O 0 } a, N d N 2 d 7 E E E V of A E N 7 �r J E Q E Ln Z f+l E N N R E N t0 C v 3 {=L V. e — N c` — •� o T d - ►r E E N IT O M E O F- Of E aQf O� E O > O� E O N Of N 3 Y C7 E u~t E O N _ E N G' HI pE O O E O N 7 l7 E O V Oh w s ri CO IL Co a m a m a CO a CO a as 6 to 3 (! at l7 a t7 a t9 a t9 a o Q o C7 > l9 > t7 o t7 o > M In a M 4 m �7 a u+ > Q c 1 ZtiN\ z a 4 6 7 ti 9 10 a I1 A 12 \NM: I I I I I H I I J pH Adjustment Log for Preserved Samples Sample 10 Type of Preservative pit upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot N I I i t Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, Incorrect containers) Qualtrax Document ID: 70677 Page 2 of 2 Page 16 of 16