HomeMy WebLinkAboutWQ0037555_Summary of Well Installation Actions_20230201Anchor QEA of North Carolina. PLLC ANCHOR
23- Haywood Street
Asheville. North Carolina 28801 QE A
828.281.3350
January 31, 2023
Brett Laverty
North Carolina Department of Environmental Quality
Water Quality Regional Operations
2090 U.S. Highway 70
Swannanoa, North Carolina 28778
Re: Summary of Well Installation — October 2022
Permit No. WQ0037555
Trillium Links & Village Wastewater Treatment Plant
Dear Mr. Laverty,
Anchor QEA of North Carolina, PLLC, on behalf of Trillium Links & Village (Trillium), is pleased to
present this letter summarizing the installation and sampling of three groundwater monitoring wells
constructed as compliance monitoring wells around the Trillium Links Site (Site) Rapid Infiltration
System (RIF), located at 48 Links Drive in Cashiers, North Carolina.
On February 2, 2022, the North Carolina Department of Environmental Quality (DEQ) approved
three new monitoring well locations for evaluating groundwater quality downgradient of the RIF.
The new wells were installed in October 2022. The new wells were installed to deeper depths to
replace the existing monitoring well network, which did not intersect the water table. The
abandonment of the former wells and installation of the new wells meets the requirements outlined
in the November 23, 2021, Notice of Deficiency (NOD)'.
Groundwater sampling of the three new wells was performed in November 2022. This letter includes
attachments presenting well locations, well boring and construction details, and laboratory analytical
results of the groundwater samples.
New Well Locations
Figure 1 illustrates the location of the new monitoring wells (MW-1 C, MW-2C, and MW-3C), and
Table 1 summarizes well construction information.
DEQ, 2001. Notice of Deficiency, Permit No. WQ0037555, Tracking Number: NOD-2021-PC-0520. November 23, 2021.
\\Wcl-fs1\asheville\Projects\Trillium Links\2022-0817 Well Installation Project\-Reporting\Report Components\Text\2023-0131_Trillium-New Wells Summary Report.docx
January 31, 2023
Page 2
Well Abandonment
Groundwater monitoring wells MW-2, MW-3, and MW-4 were abandoned on October 25, 2022, in
accordance with the requirements of North Carolina Administrative Code 15A Subchapter 2C, Well
Construction Standards. Well abandonment records are available in Attachment A.
Well Boring, Construction, and Development
The boreholes were advanced using a sonic drill rig. Drilling activities were performed by
M&W Drilling, a North Carolina -licensed drilling contractor. The monitoring wells were installed in
accordance with the requirements of the North Carolina Administrative Code 15A Subchapter 2C,
Well Construction Standards.
Screened intervals for the wells were selected based on drilling observations. The upgradient
well location, MW-1C, encountered bedrock at a depth of 3 feet below ground surface (bgs) and
was screened across a fractured bedrock interval. The 20-foot screen was placed at a depth interval
corresponding to 3,773.54 feet above meant sea level (feet msl) to 3,793.54 feet msl. Downgradient
well locations, MW-2C and MW3C, did not reach competent bedrock. Well MW-2C was completed
with a 20-foot screened interval from 3,618.18 feet above mean sea level (feet msl) to 3,638.18 ft msl.
Well MW-3C was completed with a 20-foot screened interval from 3,631.57 feet msl to
3,651.57 ft msl. Detailed boring logs are presented in Attachment B, and well construction records
are presented in Attachment C.
Following well construction, the new monitoring wells were developed using a surge block and
submersible pump. The surge block was lowered and raised across the screened interval of each well
and then subsequently pumped to remove turbid water. This procedure was maintained until a
turbidity of less than 10 NTUs was obtained. Attachment D provides the well development logs for
each of the wells.
Sampling Methods
The new groundwater monitoring wells were sampled on November 10, 2022. The sampling protocol
and analytical laboratory methods employed were consistent with the DEQ wastewater irrigation
permit No. WQ00375553. Anchor QEA used low -flow methods to purge and collect groundwater
samples from the three new monitoring wells in accordance with the procedures described by the
U.S. Environmental Protection Agency (EPA) in Low -Flow (Minimal Drawdown) Ground -Water
Sampling Procedures'.
z Mean sea level based on the North American Vertical Datum of 1988.
s DEQ, 2021. Permit No. WQ0037555, Trillium Links & Village WWTP High -Rate Infiltration System, Jackson County. August 13, 2021.
° EPA (U.S. Environmental Protection Agency), 1996. Low -Flow (Minimal Drawdown) Ground -Water Sampling Procedures. Office of
Land and Emergency Management, EPA/540/S-95/504.
January 31, 2023
Page 3
During purging, the field parameters (pH, SC, DO, ORP, turbidity, and temperature) were measured
and recorded every 3 minutes. Well purging continued until these parameters had stabilized for
three consecutive readings. The required stabilization criteria are determined by the EPA Region 4
Science and Ecosystem Support Division in Operating Procedure: Groundwater Samplings and are
summarized as follows:
• pH values within ±0.1 standard unit (SU)
• SC values within ±5%
• Temperature, dissolved oxygen (DO), and turbidity values within ±10%
• ORP values within ±10 millivolts (mV)
Once the parameters stabilize, a groundwater sample is collected by field personnel wearing a new
pair of nitrile gloves, using laboratory -supplied sample containers.
Anchor QEA submitted the groundwater samples to Pace Analytical Services, Inc., a North Carolina -
certified laboratory, for analysis of the parameters specified in the permit, shown in Table 2, and as
follows:
• Total organic carbon
• Chloride
• Fecal coliform
• Total ammonia
• Total nitrate
The field sampling forms are available in Attachment E.
Summary of Results
• Total phosphorous
• Total dissolved solids
• Total sulfate
• Volatile organic compounds
Table 3 presents field parameter data, static depths to water, and analytical results. The laboratory
analytical report is available in Attachment F.
The field parameter measurements for pH ranged from 5.3 to 6.1 SU and are below the 6.5 to
8.5 groundwater standard for pH.
None of the laboratory -analyzed constituents exceeded their respective NCAC 2L groundwater
standards. A summary of measured pH and the laboratory -detected analytical, their 2L groundwater
standards, and observed concentrations is below:
• The upgradient well location, MW-1C:
— pH (65. To 8.5 SU): 6.1 SU
— Chloride (250 milligrams per liter [mg/L]): 1.9 mg/L
5 EPA, 2017. Science and Ecosystem Support Division. Operating Procedure: Groundwater Sampling. April 26, 2017.
January 31, 2023
Page 4
— Nitrate (10 mg/L): 1.5 mg/L
— Total dissolved solids (500 mg/L): 64 mg/L
• The downgradient well location, MW-2C:
— pH (65. To 8.5 SU): 5.3 SU
— Chloride (250 mg/L): 3.1 mg/L
— Nitrate (10 mg/L): 0.085 mg/L
— Total dissolved solids (500 mg/L): <25.0 mg/L
• The downgradient well location, MW-3C:
— pH (65. To 8.5 SU): 5.6 SU
— Chloride (250 mg/L): 6.3 mg/L
— Nitrate (10 mg/L): 0.92 mg/L
• Total dissolved solids (500 mg/L): <25.0 mg/L
Closing
This sampling event has provided a baseline of concentration data based on the permit required
monitoring established in the facility's RIF system permit. Anchor QEA and Trillium appreciate your
assistance with this project. Please do not hesitate to contact me at (828) 771-0378 or
cpippin@anchorgea.com, if you have any questions or if you require additional information.
Sincerely, °C,ARp'',•.
` 1587
1/31/2
S •, F
O
' unuunaa
Charles G. Pippin, PG
Senior Managing Geologist
cc: Julie Babcock, Trillium POA Manager
Attachments
Figure 1 New Well Locations
Table 1 Monitoring Well Construction Summary
Table 2 Summary of Laboratory Analyses
Table 3 Analytical Results
Attachment A Well Abandonment Records
Attachment B
Boring Logs
Attachment C
Well Construction Logs
Attachment D
Well Development Logs
Attachment E
Field Sampling Forms
Attachment F
Laboratory Analytical Report
Tables
Table 1
Monitoring Well Construction Summary
Depth to
Total Well
Depth to Top
Bottom of
Ground
Depth
Approximate
of Screened
Screened
Top of
Bottom of
Surface
TOC
Stick Up
Based on
Depth to
Groundwater
Depth to
Approximate
Interval
Interval
Screen
Screen
Elevation
Elevation
(feet above
Well
Water
Elevation
Bedrock
Bedrock
(feet below
(feet below
Elevation
Elevation
Geology of
Source of Well
Facility
Date
Northing
Easting
(feet
(feet
ground
Records
(feet
(feet
(feet below
Elevation
ground
ground
(feet
(feet
Screened
Construction
Permit
Well ID
Drilled
(NAD83)
(NAD83)
NAVD88)
NAVD88)
surface)
(feet TOC)
TOC)
I NAVD88)
ground surface)
(feet NAVD88)
surface)
surface)
NAVD88)
NAVD88)
Interval
Information
Gneiss
MW-1C
10/25/2022
532948.55
764026.18
3,828.01
3,831.01
3.00
55
34.94
3,796.07
3
3825.01
35
55
3793.01
3773.01
Anchor QEA
Bedrock
W00037555
MW-2C
10/26/2022
533336.92
763754.53
3,674.74
3,674.66
-0.08
56
37.86
3,636.80
N/A
N/A
36
56
3638.74
3618.74
PWR
Anchor QEA
MW-3C
10/27/2022
533177.55
763540.22
3,677.10
3,677.02
-0.08
45
26.84
3,650.18
N/A
N/A
25
45
3652.1
3632.1
PWR
Anchor QEA
Notes:
Northing and easting location data was collected with a sub meter GPS unit on 11/18/2022. Elevation based on 2017 LIDAR data from the NC Floodplain Mapping Program. Given the scale and magnitude of potentiometric head differences,
the sub meter GPS and 2017 LIDAR data are sufficient for estimating the groundwater flow direction.
Depth to water was measured on November 10, 2022.
feet TOC: feet below the top of the well casing
N/A: not applicable
NAD83: North American Datum of 1983
NAVD88: North American Vertical Datum of 1988
PWR: partially weathered rock
TOO top of casing
Summary of Well Installation - October 2022 Page 1 of 1
Trillium Links and Village January 2023
Table 2
Summary of Laboratory Analyses
Groundwater Samples
Facility
Permit
Well ID
Sample ID
Collect Date
Total
Organic
Carbon
Chloride
Fecal
Coliform
Total
Ammonia
Total
Nitrogen
as Nitrate
Total
Phosphorus
Total
Dissolved
Solids
Total
Sulfate
Volatile
Organic
Compounds
SM 5310B
SM 4500
SM 9222D
EPA 350.1
1 EPA 353.2
EPA 365.1
SM 2540C
EPA
9056A
I SM 6200B
MW-1C
MW-1C-20221110
11/10/2022
X
X
X
X
X
X
X
X
X
WQ0037555
MW-2C
MW-2C-20221111
11/10/2022
X
X
X
X
X
X
X
X
X
MW-3C
MW-3C-20221112
11/10/2022
X
X
X
X
X
X
X
X
X
Notes:
EPA: U.S. Environmental Protection Agency
MW: monitoring well
SM: standard method
Summary of Well Installation - October 2022 Page 1 of 1
Trillium Links and Village January 2023
Table 3
Analytical Results
Total
Total
Total
Volatile
Water Level
Dissolved
Specific
Organic
Fecal
Total
Nitrogen
Total
Dissolved
Total
Organic
Depth
Temperature
ORP
Turbidity
Oxygen
pH
Conductivity
Carbon
Chloride
Coliform
Ammonia
as Nitrate
Phosphorus
Solids
Sulfate
Compounds
(feet below
(CFUs
Sample Name
Sample Date
TOC)
UP
(mV)
(NTU)
(mg/L)
(SU)
(Nmhos/cm)
(mg/L)
(mg/L)
per 100 mL)
(mg/L)
(mg/L)
(mg/L)
(mg/L)
(mg/L)
(mg/L)
2L Groundwater Standards
--
--
--
--
--
6.5 - 8.5
--
--
250
1
7.5
10
--
500
250
Groundwater Standards Provided
in Permit No. WQ0037555
--
--
--
--
--
6.5-8.5
_
250
-
7.5
10
500
250
MW-1C
11/10/2022
34.94
12.4
-59.2
12.3
9.15
6.1
73.2
<1.0
1.9
<1.0
<0.10
1.5
<0.050
64
<1.0
ND
MW-2C
11/10/2022
37.86
11.7
363.9
2.99
8.05
5.3
30.3
<1.0
3.1
<1.0
<0.10
0.085
<0.050
<25.0
<1.0
ND
MW-3C
11/10/2022
26.84
1 11.8
1 -40.7
69.3
7.63
5.6
53
<1.0
6.3
<1.0
<0.10
0.92
0.099
<25.0
<1.0
ND
Notes:
2L standards are set in North Carolina Administrative Code, Title 15A Subchapter 2L - Groundwater Classifications and Standards,
Bolded values indicate a concentration equal to or above the respective groundwater standard or outside the groundwater standard range.
pH is analyzed by Anchor QEA of North Carolina, PLLC; NC lab certification number 5445.
Monitoring is performed in accordance with Permit No. WQ0037555 issued to Trillium Links & Village on August 13, 2021.
< indicates that the constituent concentration was not detected above the analytical reporting limit
µg/L: micrograms per liter
CFU: coliform-forming unit
mg/L: milligrams per liter
mL: milliliter
SU: standard unit
ND: non detected
Summary of Well Installation - October 2022 Page 1 of 3
Trillium Links and Village January 2023
Figure
Publish Date: 2023/02/01, 10:42 AM I User: cpippin
Filepath: Q:\lobs\Trillium_2570\Maps\Figure 1_Well_lnstallation.mxd
ANCHOR
OEA
LEGEND:
0 Power Pole
Abandoned Well Location
New Well Location
General Groundwater Flow Direction
777 High Rate Infiltration System
Potential Compliance Boundary
(50 feet from Property Line)
0 Access Road
Drainage
Power Transmission Line
Contours: 20' Interval
0 Jackson County Parcels
NOTES:
GW Elv: Groundwater elevation measured on
November 10, 2022
New well positions are based on northing and
easting location data collected with a sub meter
GPS unit on 11/18/2022. The elevation data is
based on 2017 LIDAR data from the NC
Floodplain Mapping Program. Given the scale
and magnitude of potentiometric head
differences, the sub meter GPS and 2017 LIDAR
data are sufficient for estimating the
groundwater flow direction.
0
0 150
Feet
Figure 1
New Well Locations
Trillium Links & Village
Attachment A
Well Abandonment Records
WELL ABANDONMENT RECORD
1. Well Contractor Information:
Michael Patrick, Jr.
Well Contractor Name (or well owner personally abandoning well on his/her property)
4498-A
NC Well Contractor Certification Number
M&W Drilling, LLC
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (1.e. UIC County, Sate, Variance, etc.) iflaiown
3. Well use (check well use):
Water Supply Well:
❑Agricultural
❑Geothermal (Heating/Cooling Supply)
❑ Industrial/Commercial
Non -Water Supply Well:
[]Aquifer Recharge
❑Aquifer Storage and Recovery
❑Aquifer Test
❑Experimental Technology
❑Geothermal (Closed Loop)
❑Geothermal (Heating/Cooling
4. Date well(s) abandoned: 1 0/25/22
❑Municipal/Public
❑Residential Water Supply (single)
❑Residential Water Supply (shared)
❑Groundwater Remediation
❑Salinity Barrier
❑ Storrrlwater Drainage
❑Subsidence Control
❑Tracer
5a. Well location:
Trillium Links & Village
Facility/Owner Name Facility ID# (if applicable)
48 Links Drive, Cashiers, NC 28717
Physical Address, City, and Zip
Jackson
County
Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
35008'39,93" N 83008'11.88"
For Internal Use ONLY:
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed -Loop Geothermal Wells having the same
well construction/depth, only 1 GW-30 is needed. Indicate TOTAL NUMBER of
wells abandoned:
7b. Approximate volume of water remaining in well(s): 0 (gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:
7d. Amount of disinfectant used:
7e. Sealing materials used (check all that apply):
❑ Neat Cement Grout
s Bentonite Chips or Pellets
❑ Sand Cement Grout
❑ Dry Clay
❑ Concrete Grout
❑ Drill Cuttings
❑ Specialty Grout
❑ Gravel
❑ Bentonite Slurry
❑ Other (explain under 7g)
7f. For each material selected above, provide amount of materials used:
Bentonite Chips — 43.5 pounds
7g. Provide a brief description of the abandonment procedure:
Well was dry, therefore, chips were poured in from
top.
8. Certification:
M.it,. A�� 11 /9/22
Signature of Certified Well Contractor or Well Owner Date
By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.
9. Site diagram or additional well details:
W You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Aaachwell construction reconi(s)ifavailable. For multiple injection or non-watersupplywells
ONLY with the same construction/abandonment, you can submit one form.
6a. Well ID#: M W-2
6b. Total well depth: 20
6c. Borehole diameter: 2 (in.)
6d. Water level below ground surface: None (ft.)
SUBMITTAL INSTRUCTIONS
10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
10b. For Iniection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
6e. Outer casing length (if known): (ft,) 10c. For Water Supply & Iniection Wells: In addition to sending the form to the
address(es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
6f. Inner casing/tubing length (if known): (ft.) abandoned.
6g. Screen length (if known): (ft.)
Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
WELL ABANDONMENT RECORD
1. Well Contractor Information:
Michael Patrick, Jr.
Well Contractor Name (or well owner personally abandoning well on his/her property)
4498-A
NC Well Contractor Certification Number
M&W Drilling, LLC
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC County, State, Variance, etc.) ifknown
3. Well use (check well use):
❑Agricultural ❑Municipal/Public
❑Geothermal (Heating/Cooling Supply) ❑Residential Water Supply (single)
❑Industrial/Commercial ❑Residential Water Supply (shared)
Non -Water Supply Well:
❑Aquifer Recharge
❑Aquifer Storage and Recovery
❑Aquifer Test
❑Experimental Technology
❑ Geothermal (Closed Loop)
❑Geothermal (Heating/Cooling
4. Date well(s) abandoned: 10/25/22
❑Groundwater Remediation
❑Salinity Barrier
❑ Stormwater Drainage
❑ Subsidence Control
❑Tracer
❑Other (explain under 7g)
5a. Well location:
Trillium Links & Village
Facility/Owner Name Facility ID# (if applicable)
48 Links Drive, Cashiers, NC 28717
Physical Address, City, and Zip
Jackson
County
Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one tat/long is sufficient)
35008'40.50" N 83008'10.75"
For Intemal Use ONLY:
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed -Loop Geothermal Wells having the same
well construction/depth, only 1 GW-30 is needed. Indicate TOTAL NUMBER of
wells abandoned:
7b. Approximate volume of water remaining in well(s): 0 (gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:
7d. Amount of disinfectant used:
7e. Sealing materials used (check all that apply):
❑ Neat Cement Grout
a Bcntonitc Chips or Pellets
❑ Sand Cement Grout
❑ Dry Clay
❑ Concrete Grout
❑ Drill Cuttings
❑ Specialty Grout
❑ Gravel
❑ Bentorme Slurry
❑ Other (explain under 7g)
7E For each material selected above, provide amount of materials used:
Bentonite Chips - 43.5 pounds
7g. Provide a brief description of the abandonment procedure:
Well was dry, therefore, chips were poured in from
top.
8. Certifrca 'on:
'al ,t L - 11 /9/22
Signature of Certified Well Contractor or Well Owner Date
By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.
9. Site diagram or additional well details:
W You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.
CONSTRUCTION DETAILS OF WELL(SI BEING ABANDONED
Attach well construction record(s)ifavailable. For multiple injection or non-watersupplywells
ONLYwith the same constructionlabandonment, you can submit one form
6a. Well ID#: MW-3
6b. Total well depth: 20
6c. Borehole diameter: 2 (in.)
6d. Water level below ground surface: None
SUBMITTAL INSTRUCTIONS
10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
10b. For Infection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
6e. Outer casing length (if known): (ft.) 10c. For Water Suunly & Infection Wells: In addition to sending the form to the
address(es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
6f. Inner casing/tubing length (if known): (g,) abandoned.
6g. Screen length (if known): (ft.)
Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
WELL ABANDONMENT RECORD
1. Well Contractor Information:
Michael Patrick, Jr.
Well Contractor Name (or well owner personally abandoning well on his/her property)
4498-A
NC Well Contractor Certification Number
M&W Drilling, LLC
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIG County, State, Variance, etc.) tfknown
3. Well use (check well use):
Water Supply Well:
❑Agricultural
❑Geothermal (Heating/Cooling Supply)
❑ Industrial/Commercial
Non -Water Supply Well:
❑Aquifer Recharge
❑Aquifer Storage and Recovery
❑Aquifer Test
❑Experimental Technology
❑Geothermal (Closed Loop)
4. Date well(s) abandoned: 10/25/22
5a. Well location:
Trillium Links & Village
❑MumcipallPublie
❑Residential Water Supply (single)
❑Residential Water Supply (shared)
❑Groundwater Remediation
❑Salinity Barrier
❑Stormwater Drainage
❑Subsidence Control
❑Tracer
❑Other (explain under 7g)
Facility/Owner Name Facility 1139 (if applicable)
48 Links Drive, Cashiers, NC 28717
Physical Address, City, and Zip
Jackson
County
Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(ifwell field, one lattlong is sufficient)
35008'37.17" N 83008'09.07"
For Internal Use ONLY:
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed -Loop Geothermal Wells having the same
well construction/depth, only I GW-30 is needed. Indicate TOTAL NUMBER of
wells abandoned:
7b. Approximate volume of water remaining in well(s): 0 (gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:
7d. Amount of disinfectant used:
7e. Sealing materials used (check all that apply):
❑ Neat Cement Grout
a Bentonite Chips or Pellets
❑ Sand Cement Grout
❑ Dry Clay
❑ Concrete Grout
❑ Drill Cuttings
❑ Specialty Grout
❑ Gravel
❑ Bentonite Slurry
❑ Other (explain under 7g)
7E For each material selected above, provide amount of materials used:
Bentonite Chips — 43.5 pounds
7g. Provide a brief description of the abandonment procedure:
Well was dry, therefore, chips were poured in from
top.
8. Certification:
?Oe�-- 11 /9/22
Signature of Certified Well Contractor or Well Owner Date
By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 1 SA NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.
9. Site diagram or additional well details:
W You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Attach well construction record(s) ifavailable. For multiple injection or non-watersupplywells
ONLY with the same constructionlabandonment, you can submit one form.
6a. Well ON: MW-4
6b. Total well depth: 20 (ft.)
6c. Borehole diameter: 2 (in.)
6d. Water level below ground surface: None (ft.)
10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
10b. For Iniection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
6e. Outer casing length (if known): (ft.) 10c. For Water Snooty & Iniection Wells: In addition to sending the form to the
address(es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
6f. Inner casing/tubing length (if known): (ft.) abandoned.
6g. Screen length (if known): (ft.)
Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
Attachment B
Boring Logs
WELL NUMBER MW-1C
Anchor CIA of North Carollna,PLLC
ANCHOR
231 Haywood Street PAGE 1 OF 3
�
Asheville, North Carolina 28801 0 EA ; � {-
828.281.3350
CLIENT Trillium Links & Village PROJECT NAME (NUMBER) Trillium Links & Village (C22570-01.01)
NORTHING, EASTING , PROJECT LOCATION Cashiers, NC
DATE STARTED 10/25/22 COMPLETED 10/26/22 GROUND ELEVATION HOLE SIZE 6"
DRILLING CONTRACTOR GROUND WATER LEVELS:
DRILLING METHOD Sonic Z-7 AT TIME OF DRILLING 24.3 ft
LOGGED BY Katie Pressley CHECKED BY TAT END OF DRILLING 31.5 ft
NOTES 7-AFTER DRILLING 34.9 ft
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REMARKS
O
MATERIAL DESCRIPTION
WELL DIAGRAM
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0
C
0
Dark brown CLAY, low plasticity, grading to silty SAND, well
CL
graded, dry
1.2
SW
Brown silty SAND, well graded, dry
1.9
PWR, "hockey puck" at 2 feet bgs, light brown to white
SC
60
PWR
Harder drilling
•
3.0
Rock, GNEISS (quartz, feldspar, biotite, muscovite) with
GRANITE, compotent to approximiately 5.5 feet bgs,
fractures are subvertical, crushed rock (coarse SAND) at 10
feet bgs, all moist
5
-125 gallons of
OC 14
water lost to
SC
60
formation
(60)
10
—
10.0
---------------------------
SAA, "hockey puck" pattern, rock is slightly weathered,
fractures are horizontal and subvertical, moist
SC
95
(25)
Grout
15
OC14
Rod drop
SC
0
20
20.0
(Continued Next Page)
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LL
0
WELL NUMBER MW-1C
Anchor CIA of North Carollna,PLLC
ANCHOR
231 Haywood Street PAGE 2 OF 3
� 0 EA
Asheville, North Carolina 28801 ; � {-
828.281.3350
CLIENT Trillium Links & Village PROJECT NAME (NUMBER) Trillium Links & Village (C22570-01.01)
NORTHING, EASTING PROJECT LOCATION Cashiers, NC
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REMARKS
O
MATERIAL DESCRIPTION
WELL DIAGRAM
w v
0
CO
20
SAA with mechanical fractures, subvertical fractures,
foliation is parallel to apparent bedding plane
-400 total gallons of
OC
SC
80
water lost to
(22)
formation, very hard
drilling to 30' bgs
24.0
—
-Y- SAA with "hockey puck" pattern, subhorizontal fractures_
more compotent rock with some subvertical fracturing
25
OC
—
26.3
---------------------------
SAA, compotent rock with approximately 5" fracture, sub
horizontal fractures with "hockey puck" pattern, subvertical
45
fractures appear natural based on smearing at interface, wet
SC
(130)
ROC14
Bentonite
30
i
SC
63
(97)
_
33.2 _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _
SAA, compotent rock with two subhorizontal fractures - do
Filter Sand
not appear mechanical, oxidation staining at approximately
37.5 feet bgs, more schistose features observed around
36.5 feet bgs, may be smearing at fractures
35
ROC14
SC
(123)
Very hard drilling
_
39.6
40
SAA,hockey pucks", subhorizontal fractures, mechanical
fractures
ROC14
SC
62
82
(Continued Next Page)
WELL NUMBER MW-1C
Anchor CIA of North Carollna,PLLC
ANCHOR
231 Haywood Street PAGE 3 OF 3
�
Asheville, North Carolina 28801 0 EA ; � {-
828.281.3350
CLIENT Trillium Links & Village PROJECT NAME (NUMBER) Trillium Links & Village (C22570-01.01)
NORTHING, EASTING PROJECT LOCATION Cashiers, NC
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REMARKS
O
MATERIAL DESCRIPTION
WELL DIAGRAM
v
C8
co
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-
3,�-------------------------'
SAA to 46.67 feet bgs - rock type change to AMPHIBOLITE
(hornblende, plagioclase, biotite), "hockey puck" pattern, no
RQD (no returns >4"), some iron staining at 46 feet bgs
45
0.02-inch
ROC14
Slotted,
Sch-40 PVC
SC
57
47.8 ----------------------
GNEISS, "hockey puck" pattern, iron staining at 50.67 feet
bgs
OC14
50
_
50.8 _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ ----
ROC14
HORNFELS (micaceous with garnet), subhorizontal and
—
51.4 subvertical fractures
—-----------------------
GNEISS, more compotent rock, iron staining throughout
-800 total gallons of
SC
77
water lost to
(47)
formation, easy
OC
drilling
Hard drilling at 53'
bgs
53.8
No Return
55
Very hard drilling,
SC
0
-1,100 total gallons
Filter Sand
of water lost to
formation
60
60.0
Boring terminated at 60.0 feet.
WELL NUMBER MW-2C
Anchor CIA of North Carollna,PLLC
ANCHOR
231 Haywood Street PAGE 1 OF 4
�
Asheville, North Carolina 28801 0 EA ; � {-
828.281.3350
CLIENT Trillium Links & Village PROJECT NAME (NUMBER) Trillium Links & Village (C22570-01.01)
NORTHING, EASTING , PROJECT LOCATION Cashiers, NC
DATE STARTED 10/26/22 COMPLETED 10/27/22 GROUND ELEVATION HOLE SIZE 6"
DRILLING CONTRACTOR GROUND WATER LEVELS:
DRILLING METHOD Sonic Z-7 AT TIME OF DRILLING 51.8 ft
LOGGED BY Katie Pressley CHECKED BY 1 AT END OF DRILLING 40.1 ft
NOTES 7-AFTER DRILLING 37.9 ft
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REMARKS
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MATERIAL DESCRIPTION
WELL DIAGRAM
W
0
U
0
Brown very fine to fine silty SAND, poorly graded, dry to
SP
_
0.8 moist
Tan and white very fine to fine SAND, poorly graded, dry to
SP
moist, PWR at 1.83'
_
1.8_
Light brown very fine to fine silty SAND, poorly graded, dry
SC
37
to moist
SP
5
5.5
SW
• '•'
5.8 Tan to white fine to medium silty SAND, well graded, dry
PWR with tan/brown silty SAND
PWR
•
7.3
SC
80
—
PWR
---------------------------
PWR with white silty SAND
—
8.0
---------------------------
PWR with gray, white, and tan SAND, -1" SCHIST "puck"
PWR
—
9.0--------------------------
Weathered SCHIST (biotite, quartz, hornblende, muscovite)
10
PWR
10.6
SW
°
Tan brown, and gray very fine to coarse silty SAND, well
SW
•`•`•0
graded, wet
11.5 ------------------J
Gray coarse SAND, well graded, with CLAY, low plasticity,
PWR
wet
12.5 Brown and gray PWR with very fine to fine silty SAND with
SC
50
GRAVEL, well graded, dry
Grout
No Return
15
Driller reports harder
SC
0
drilling but still
considers it "easy"
drilling
20
20.0
(Continued Next Page)
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0
a
0
WELL NUMBER MW-2C
Anchor CIA of North Carollna,PLLC
ANCHOR
231 Haywood Street PAGE 2 OF 4
�
Asheville, North Carolina 28801 0 EA ; � {-
828.281.3350
CLIENT Trillium Links & Village PROJECT NAME (NUMBER) Trillium Links & Village (C22570-01.01)
NORTHING, EASTING PROJECT LOCATION Cashiers, NC
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REMARKS
0- O
MATERIAL DESCRIPTION
WELL DIAGRAM
W
0
20
White and black SCHIST with GRANITOID cobbles and fine
to coarse silty SAND, iron staining at 15.6 feet bgs, no
obvious fracture pattern, foliation parallel to boring
SC
32
PWR
25
25.0
No Return
Driller reports large
fracture somewhere
20-30' bgs, rod drop
SC
0
-25-29' bgs, -300
gallons of water lost
to formation, no
return 25-30' bgs
Bentonite
30
1
1
30.0
Dark brown, tan, and white schisty PWR with very fine tc
fine silty SAND, well graded, white sandy CLAY at 30.83
feet bgs, iron staining throughout
PWR
SC
95
132.5
White sandy CLAY with coarse SAND, low plasticity,
CL
weathered GRANITOID (PWR)
33.4
Filter Sand
Dark brown, tan, and white schisty PWR with very fine to
PWR
fine silty SAND, well graded, saturated
35
_
34.8 _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _
SAA, PWR with more compotent samples of SCHIST
PWR
36.3
SAA but more micaceous and weathered
PWR
SC
30
—
3 -- — — — — — — — — — — — — —
Tan, gray, and white very fine silty SAND, PWR, dry
PWR
40
1
41.3
Brown very fine to fine silty SAND with GRAVEL, dry
SW
_
42.2 _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _
SC
95
SP
42.6 SAAwithout gravel — — — — — — — — — — — — — — —
(Continued Next Page)
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EZ
0
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0
WELL NUMBER MW-2C
AnchorQEAotNorth Carallna,PLLC Q
ANCH
231 kaywood St, PAGE 3 OF 4
c�s .cr
Asheville, North Carolina 288C1 QEA;
828.281.3350
CLIENT Trillium Links & Village PROJECT NAME (NUMBER) Trillium Links & Village (C22570-01.01)
NORTHING, EASTING PROJECT LOCATION Cashiers, NC
w
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REMARKS
0-0
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MATERIAL DESCRIPTION
WELL DIAGRAM
co
W
SP
White coarse SAND with "hockey pucks" of parent rock
43.5 (GRANITOID) (continued)
Brown sandy CLAY, low plasticity, compotent, dry with PWR
CL
44.8
45
CIL
SAA
45.3
Brown, gray, and white very fine to fine silty SAND, well
graded, micaceous, dry
0.02-inch
SW
Slotted,
Sch-40 PVC
SC
68
Hard drilling
—
>
47.8 _____ __________________
'--
White SAND with pebbles and "hockey pucks" of weathered
SW
feldspar and quartz, dry
°
48.7
No return 50-60 feet bgs, small amount of satuarted PWR
drained out of sleeve - white and tan SAND
50
SC
0
PWR
55
SC
0
60
60.0
SCHIST, 2-3" cores, no obvious fracture pattern,
ROC143
subhoriztonal pattens
61.0
No Return
Only return from
60-70 feet bgs run,
rocks were collected
SC
20
from bottom of 65-70
foot sleeve but
unknown where rock
Filter Sand
interval was
collected from
65
(Continued Next Page)
WELL NUMBER MW-2C
Anchor CIA of North Carollna,PLLC
ANCHOR
231 Haywood Street PAGE 4 OF 4
�
Asheville, North Carolina 28801 0 EA ; � {-
828.281.3350
CLIENT Trillium Links & Village PROJECT NAME (NUMBER) Trillium Links & Village (C22570-01.01)
NORTHING, EASTING PROJECT LOCATION Cashiers, NC
Lu
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REMARKS
0-0
O
MATERIAL DESCRIPTION
WELL DIAGRAM
W
0
c
<Y
No Return (continued)
Very easy drilling,
- 600 total gallons
SC
0
lost to formation
70
70.0
Boring terminated at 70.0 feet.
WELL NUMBER MW-3C
Anchor CIA of North Carollna,PLLC
ANCHOR
231 Haywood Street PAGE 1 OF 3
�
Asheville, North Carolina 28801 0 EA ; � {-
828.281.3350
CLIENT Trillium Links & Village PROJECT NAME (NUMBER) Trillium Links & Village (C22570-01.01)
NORTHING, EASTING , PROJECT LOCATION Cashiers, NC
DATE STARTED 10/27/22 COMPLETED 10/28/22 GROUND ELEVATION HOLE SIZE 6"
DRILLING CONTRACTOR GROUND WATER LEVELS:
DRILLING METHOD Sonic Z-7 AT TIME OF DRILLING 32.1 ft
LOGGED BY Katie Pressley CHECKED BY TAT END OF DRILLING 26.2 ft
NOTES 7-AFTER DRILLING 26.8 ft
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REMARKS
O
MATERIAL DESCRIPTION
WELL DIAGRAM
W
0
U
0
SID
Dark brown very fine SAND, poorly graded, with white, fine
L SAND (weathered GRANITOID) at 7 inches bgs, moist
No Return
Only recovered 7
inches from 0-10
SC
12
feet bgs interval,
water blew the
returns out of the
core.
5
SC
0
Grout
10
10.0
White GRANITOID "sugar" SAND, very fine to medium
SAND, well graded, with SILT, dry/moist, compacted
sections throughout run except 13.75-14.25 feet bgs,
compacted sections have clayey outer skin
SW
SC
90
>
14.5
CL
Tan sandy CLAY, low plasticity, with fine to coarse SAND,
15.3 well graded, saturated
15
SP
15.8 Brown very fine SAND, poorly graded, moist
CL
16.2 Brown sandy CLAY, low plasticity, with fine SAND
Organics
White "sugar" SAND, weathered GRANITOID, wet
SW
00000 0
17.3
SC
45
15-17.25feetbgs
—
---------------------------
SAA with orange feldspar banding, moist
run all compacted
SW
20
(Continued Next Page)
WELL NUMBER MW-3C
Anchor CIA of North Carollna,PLLC
ANCHOR
231 Haywood Street PAGE 2 OF 3
�
Asheville, North Carolina 288o1 0 EA ; � {-
828.281.3350
CLIENT Trillium Links & Village PROJECT NAME (NUMBER) Trillium Links & Village (C22570-01.01)
NORTHING, EASTING PROJECT LOCATION Cashiers, NC
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REMARKS
0_ O
MATERIAL DESCRIPTION
WELL DIAGRAM
W
co
20
SAA with orange feldspar banding, moist (continued)
Bentonite
SC
100
SW
>
Filter Sand
25
—
0>0>0>
25.0
---------------------------
SAA with some larger grains of quartz and feldspar at 25
feet bgs, compacted throughout
1
Y
SC
45
SW
>
30
.30.0
_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _
SAA with brown and tan lenses of fine SAND to
_
SW
approximately 31 feet bgs
31.0
SAA without brown lenses of SAND
30-35 feett bgs
SW
SZ
SC
100
interval all
compacted except
o
` `
33.0
. .
31.25'-31.50'
—
---------------------------
SAA with more white SAND
SW
_
34.0 _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _
SAA but with larger grains of quartz (medium -gravel size
SW
..
grains), all moist
35
—0 — — — — — — — — — — — — — — — — — — — — — — — — — —
—
"sugar"
0.02-inchSlotted,
—
White SAND
Sch-40 PVC
SC
100
SW
40
40.0
PWR - same material as white SAND
PWR
_
142.3
41.3 _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _
PWR with more tan and brown, compacted sections
PWR
measure approximatey 1-3 inches
SC
85
SP
(Continued Next Page)
WELL NUMBER MW-3C
Anchor CIA of North Carollna,PLLC
ANCHOR
231 Haywood Street PAGE 3 OF 3
�
Asheville, North Carolina 28801 0 EA ; � {-
828.281.3350
CLIENT Trillium Links & Village PROJECT NAME (NUMBER) Trillium Links & Village (C22570-01.01)
NORTHING, EASTING PROJECT LOCATION Cashiers, NC
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REMARKS
0-0
O
MATERIAL DESCRIPTION
WELL DIAGRAM
W
0
S_P
43.3 Tan and brown SAND, weathered material similar to above
but more weathered with lenses of compacted material I
(contin_ue_d)____________________I
SP
Dark brown very soft, very fine SAND, very micaceous,
moist
45
45.5
SW
e °e°
46.0 Tan to orange, medium to coarse SAND, some mica, moist
Dark brown very soft, very fine SAND, some mica, moist
Sp
.'
47.0
Tan, white, and orange very fine to fine SAND, brown
45-50 feet bgs has
SC
93
clayey outer skin
SW
micaceous SAND at 48.17 feet bgs
Filter Sand
0
48.5
_
—AU
'I Tan, very fine_ to fine SAND
White SAND with PWR fragments
50
SW
SC
82
52.5
SW
Brown clayey SAND, dry
0
53.1
White SAND with PWR fragments
SW
54.1
—
_
Light brown very fine to fine SAND with SILT, poorly graded,
compacted, moist
55
SW
Bentonite
_
0
56.1 _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _
White SAND with small lenses of compacted PWR
SC
92
Harder drilling
SW
Boring terminated at 60.0 feet.
60
Attachment C
Well Construction Logs
WELL CONSTRUCTION RECORD GW-1
1. Ws lI Coariraetor ltforinaliou:
For Intemal Use
Michael Patrick, Jr.
WeLI Cwmm= NA=
44 -
N(' WClI ('cmtcxlorCcrtificattm:Nwinkxr
l}/ltLW Drilling, LL
eefflvdii.y Nam*
2. Well Construction PErMit ill.
LfalaK aAKr-mtk muff colA emmim pernlfft (.c UIC, CawW. Stwe. varravcc, ric.)
3. Well Use (check well! used
Water Supply Well --
Agricultural []MUslicijXMUbhC
Cleo herrna] (IAC86ng1Coaltng Supply) [JRCSidetltial Water Supply (yinoo)
1nldustrislli2wnmer6al DResAentlal WateT Supply (Sh")
Itlcn
i Nom-Willer Supply Well,
Aquifer Rccharge
Aquifer Storage and Recovery
Aqultcr Test
Expoimental Technolog}+
(iaathurnal (CIMW LJovp)
DCrtundweber Rbn1edL1A1011
[33-linity Barrier
Dswmwster ❑ffl=ge
1391,b36MWe Ccmtral
Tracer
ila in under ir'21 Reynvk%
4. slate Well(s) Compkted; 14- 6- Web 1D# ill 1
31 . WeU I "fipn:
TdIlium Links & Village
Feta1iiw0% uer Maine FeciGty Off (ilaWllraVc-)
48 Links Drive, Cashiers, NC 28717
Prpsoeal A*d ram,C 11y, xnd f.:
Jackson
Cotmry
Parcel Ide.ftr,ratmn No. (PIN)
5b. Lmitade ind loagilude in or decilrtol degrees'
(,FWell Held. nee l IMS iS Edf LiC100
35.14362952 K-83.13572922
6. la(are) the weD(s)�}x Permanent -or E]Temporaxy
7, le this 4 1 kir too *kI pti8dxIg well: [3Yn or ONo
ff JhA IN fJ rPWMF, frr1i f11N wrT{ PF�4+ Cf1R5'&MffWM hVarN DrJf'!r! Md rtJM fhe lr( lrrd Of the
.,rp„iry kr-2irsswnUaaerkwrewtrhotwatVAfaforai.
$, ForGeoprobefDPT or C_losed-L.00p Geothermat Urells having the sarne
03risbYUCtiQA o311y I GW-] is [seeded lnd=( gTQTAL MLIMBER ofwelIs
drilled:
9. Total Well depth below land Wrfaee: fdU
Fee mwhWe 1Fgfi Arr aft akplhs Jj &JgfeFem feAam pla, 3@2W' ¢m 2(Q10J?
10. Static watsr kertl below top ofcming:
{f barer lm, -1 u ab," GriRW& 4w "-
1 L Borehole diamckr: 6
12.Weklcuualructi&Nmethod: Sonic
{LA ajar, rosary, cable- dire= push, ere )
14. WATER
7Ai+M
PROM
To o {i1lPnnrJ
R-
fit.
R
fr,
YS OCITERCASIN(; for inu W- Casad wdFa OR UN ItE kdhte
kROm 'nl ulArr78TP.R TAK;KrCES9 MATLMAL
ft ft
in.
Lf. INMER CAMG OR I'L'BING f rlrthrrmaI rlum l-l1 h
FRgM
TG
DLi3}r,IF-H
III11'KhLsn
MATPJkLiL
fa
35 irL
2 "''
SCh 40
PVC
1k
tL
11, S RF.BN
FROM
-10
nLiMYI'iA SLATSHE
THDCKN IS
MATERIAL
35 ft-
55 fL
2 im 0.010
Sch 40
PVC
%
R,
is
1& CRoLrr
FROM
TO
MATriRlhr.
1NPLACEMENT MEULOP&A.t10Uf'JT
0 fL
27 n-
Portland Cement
Trerrtie
27 ft
32
6entonipe Chips
Pour
iB-;;i.Nn,RAYfLPAC K Ifo Heable
prt(5,rr
TV
MATERIAL
EMPLACTF4rNTRSLrnCho
32 ft.
60 ft�
02 Medium Sand
Pour
It
fti
21). I)KlLLIKG LOG qatu
addktlonakstlae#ifnJ sa
FROM
74
DF9CRI1PT[OF jular.ha.,lupry Ura&1 y emln.ecaP
ft.
fL
ft-
fL
Ft.
fr.
ft
rI.
ft.
h
fit.
FI.
fl-
rl.
Tir L7CMiARICR
21 certification:
V /Nil
93PLULre ofC*rtjfW Well contracbm
11-9-22
UWX
j4r-OK nx flr& f4rr11or ) A L"by rnNfp &W the ralf(a) wax tMVV mp onrow W Jrcow e
Kira, 1SA XC.{C 02C .01M or 13-4 r CAC 02C 02ri0 Wd1 CCnnshveA=Mwrdareh 8md ihm a
cyfy .k rhrx Fvcn d hat fh' A rJ JdZd fa f& 114f ONM1k'F.
23. Stir diagram or addltiooal well delifils:
Ysnl may use the hack of thLs page Lo provide addktiorW well site details or vml I
congouctinn detalks. You may also attach addktionel "it if txaessiry.
SI HM1'i'VAL.IM1SMr:C-11
ittl 2U. For Ali Wells: Submit this form withm 30 drays of camp]ntiau of yell
crmwuctum to the follcvwin&
(ft-) Division ofWater FLesourrez, larormatilm Proeelains. (fin it,
1617 MAII Scrvkx Crater, Raldgh, NC 27699-1617
24h- For Lniecon wells: In addition to scalding the form to fhe address in Ada
above:, also submit one copy u* this form vnthin 30 days art` completion of well
cori%tmctlnn to the folk wv4'.
Division of Watrr Resources, Undergrornd Imjmtian {Control Program,
FiDR WATT1R SGPPI N 44rLLLIi ONE. - 16A Mrtil Se"Iet Center, RaLeo, NC 27699-143b
Lair YiOd (gpm) licthod of test• 24c- For Water Stpppb' & Lnmccdo■ WOW In #d4irion In tending t1le form to
the addre*cs) abwr, also suhmit Dole copy of this form within 30 days of
13br DiainfevOun type: Amount: completion of well cowtmat1on to the county health department of the county
whine ecrostructed .
I-Orm GW-L Plar111 CnralLnu DgWirtmoll. af.En%ieorumbral Quality - INvigLoll 4rWJnCr Rep(m=m R-v4W 2.22-2016
WELL CONSTRUCTION RECORD (GW-1 �
1. Well ]contractor lnfmrmutiae.
Print FoTM
ltlteniw Ilse
Michael Patrick, Jr.
Wall Conuamr Nr
44-
NC Well Com um Cc6ficetion NuffbW
M&ill Drilling, LL
f Gmperiy Nalnc
2, Well Covslrucuo■ Permit#:
l.ur c�Y appdicabke rrdl Gontrrucir. l pemNfs 0 ff UJC, Caam% SYala. VorlwNw, ex)
3. Weil i]Lc (check wrl use);
1N5tler Sti Weu
Agricultural
[ jMunicipAVPuMJC
ieotElerrnal (HmtingJCoaliltg Supply)
[] KesRlenual Watu Supply (single)
IndustiaVComrnerciai
13ResidenWl WatEw Supply (-hamd)
IrriaaTion
Nqm-WeterSrpply Well:
M ( (MitCQnlg
R Dvery
Jm.ieetiae Well:
Recharge C)Ciraundwater RcmeriiAtim
swage and Recovery 13Salln,ty Barrier
Test [39tortnwater I}raitiage
Ienfal Technology [ISubsidefice Comae]
Ii111. (Clowd Loup) C)7rucar
loin udder #21 lxel mks
4-'hate Wells) Completed: 10-27-22 Well TDN M -
5a. Weld Location;
Trillium Links & Village _
Faratit W0wrr,g Naive Fscillry IDA (zfnppl.cehlr)
8 Links Driver Cashiers, NC 28717
Roml Address, tsily, Vid
Jackson
C%U"
Identii'iueon No. (Piro)
5b, l..aOtude and lonlgitede in degrecOhimntesfwnilds or deeinlal depreea!
(lfwca field one IRVIur;g is sutlfcimd)
35-14466462
rV -$3.13669127
t;_ ls(are) the w, ell[ejap"inaReee or OTemporary
W
7- is this a repair to aY exisiling well-' []Ves or EiNo
1f riles fs er repufr. fit ouf knotty, va8 s rrwj!i iRomwBWAfm awl d*aix the rtawre of rho
FC fa?T Wdcr r 2f jrwaFhx sea mN OF ore ehe brick of rhle form
& For Geaprobe/DPT or {lowed -Loop Geothcrmai Wells h$vblg the semae
cDmtractian, only 1 CW-I is beerier] ind ioate TOTA L AIUMBER of wells
drilled
9. Total well depth below land surrace- 74 (FL)
m r ,'ange "us Ilse W1 Qvrht OrAOrrnr (crmrgalc- JQ"' mrd 2@iR)
s#- Matic water Jcvel hrbarw top of emiog;
f f muter 0,.,W a a#x)vr. as Arq, m�e
11. Borehole dionleeerl
17- Well eomstruc#ion method; Sonic
(Le. nw+, mt y, eAk. ditca pwb. M.)
(lam)
14. W vfER ZONES
62CHM
TO
d1xW
ft
fl,
ti
il.
15, OU'MR C'A51MA Ow multi#eyed wrells GR LINE if ir�lrlrt)
PROM
1+Q I}IAhTl1'ER
'IIIICKNT;s5
Mh7r�RLlL
rr,
ft in-
lb.1FiNSR CAS1C+iCv OR T•L+RSfYf, l emhero�I elntd�o•
yl QM TO rilhMF TICK THICK_'IE58
S CEltlkl-
tr. 36 R. 2 io SO 40
PVC
fl. ft IN.
t7.9C71£EfY
FHOM TO I
DLSM€ R
I SLIVI'MM
1 T,H.,LI.C,IQIFSS lgA7'RR[a[.
36
2 l°
0.010
ch 40 PVC
ft iL
i
15. GROUT
FRIGM
TO
MATIMAL Eh]PEA{FMTW M WMI)h & AWMr
h
26 R
Pauiiard ctr1 nt Tremie
26 tL
31
Beirflr0a chips Pour
Il,
ffi
IB-$AND/oRAVELPAC
K t" lieeiblc
mom
TO
HAIERLILL
ErdFIACRMkhri'MErFrOD
31 k
70
#2 Medium Sand
Pour
ft
ft_
20, D]FULLa
G LOG fsiM nddifulmIIF its if FUM HM
FRM
Tt}
nRti[7IIP316r, eam. hmd fd4iwk even -i� 440
{�
it
ft
R-
fl.
rtr
fl.
ft,
fr.
ft.
21- R1IMARVS
22L CertificaHOm:
Sig=hac ofC4rd6cd Wd Cow+�dr dais
Ay nWriag Chia jfartn, f Aeredy+ cerr* f W adr tacos (wLc cdvwt read fa rer�Phoz*w
WA 15A WAC UC' oleo ar J3d MW jK- 02r .j?20R IYrlf Camtj"Cornm S4Q+,dar t a,rd rhar a
copy of duo ta&>fd A= beets prar"M ro AW wd, mvWr.
23, Site dhlgra rx or additional well detwlilL
You nlay use the hank of this page to provide additumal weJ1 site details or well
aonstruclion details. You Inay also Mach addrUnnat pages Ifnnuessary-
SURI I.ML INSTRUCTI(]IY4
24a. For All Well Submit thu form wittun K days of complatwri of well
cor►stneation to the fallov 1Pg--
4) flbvisins of Water Reumreea, InJtofMAdeD Processing Unit,
1617 Mail Service C enter, Rateigk NC 2709-1617
241yL Far 11 iettivn Wtila: In additiaa to Sending the from to Nee address in 24a
above, also submit one oapy of this farm wuhin W days of compli tion of wolf
cons mctiun to the following:
Division of Water Resomrom Undrrgroead Enjectioo Covirol Program,
FOR WATER SUPPLY WELLS UNLY: 106 hail nervier [`.rater, Raleigh. NC 27699-100i
13a. Yield (rpm) MetMd of teat 24c. por Watcy Supply & fa ectior %AeHs_- In addition w nmdinig *e form to
the addTC55(cs) above, also submit om oopy of they farm within 30 days of
13b. DisinfNtiou type! Am6mnt-. completion of well construcmcn to the county henilh deWment of the ooeo7ty
FommGWA NaalhCwWmaDeme[meet ofGovirun■ ntal Qmhty - DMsiao of W4 tw%Amurom Revmtil 2-32-2016
WELL CON STRU CTION RECORD (GW-1}
L WC11 COntraet4T lnformwfioo;
Michael Patrick, Jr.
Well Co=actor NaTx
449 -
NC W01 Corwulcr {;Crhlicnhnu hiur.Isa.
&W Drilling, LL
Company Name
2, Wtll COASIracfior Permit fi:
Lftr4R WfOWN9 well6WLP'mwrKw(mrmres4k. M 09nrY. Sftm. Yuriwcir, rrc)
& WO Use (check well use):
Goothemtal (HeetinWoahng Supply)
ndusLria1 CMmeftial
Non -Water Supply Well:
Aquifer R e*Tgc
A.qu i fer Storage and Rmaveay
Ayuitr Tc5t
RxpcijmcnLal Technology
Geothermal (Cngcd [Annp)
MlunociPW%blio
[]ResLdendai Water Supply (single)
OResidendalWat SrS ly(shared)
0GroundwK,T ki=ediarion
0Sallnity Barrier
DSuxmuHLer D OrMW
MSubsidence Control
DT.
tlyder 821
4. Dw Wells) Completed: 10- 7- 2 Well 3iT1 M Y _
50, well Lacotion!
Trillium Links & Village
Facility++dwoerNema Facilq TDB (ifafplicablo)
48 Links Drive, Cashiers, ND 28717
T'1Lysi"i Addnss. Ciry. and hi,
Jackson
{ aalypy
Parrml Ldw6 "ion \b. {T'[N)
51b. Latitude and WiWt■d(, in {legmeshninumilseconds or decimal degrees,
(ifw b field. one hi long isguffimmki)
35.14420257 N-83.13738535
C ls(are) tie well(S) Permanent or Temporary
7, Is this s repair to ao existing Md1! Yea or EjNo
fffhrr rF 47 roy afr, fief ma fmaxvi ,roll s rruerirw i;oh-mawian amde.Tpfuilr Ae nanum ofoh*
repulr nrtder i'21 rennaykx aecrlm or n@ the 40a qfrhu fNM.
8, For Gwprob&DPT or Clomod-Loop Geothermal Wcfls ldvirg the Berme
ComS nlCtion, only 1 OW- L is nimd1ed. Ind icate TOTAL N UMBER of wells
dolled.__
9. Total well depth bcluw land surfkee: 60 VQ
Fnrmulryil "41s1rsaulldvrkx,fd&rmr (x'ampk-3 - w)
1-0. Static water F" below tap of casing:
jyNw rfargfarra5awe Tjrg,
a1, 8orehr14e diameter 6
II Well C*omtructiion mathad: Sonic
(i.e. AVVX, nThWy, mbk. dm U puAi, ale.}
Or'.)
14. WATKR ZONES
MM
TO
I dESCI[7MN
n
tt
n,
ter
13 OUTERCASINGigrmulL>�ra11s (k1xLIN8R 'f a31a
FROM
TO
antrrSK� ea
THICKNESS MATtiR1AL
iF I
A.
I in,
IC ] KNER iUA' 1ING KI" 1HFNG lhWENl elased-loo
FWN
1V a[amlcrE:a im00;uSS
MATMAL
D rL
25 ML 2 '" SCh 40
PVC.
ft
f.
17, SCREKK
T4
ULaathrFjt
SLOTSdF.E
Tt WKNESS
MAT4RIA1.
% 45 tt
T
2 io.
0,010
Sch 44
PVC
18. GROUT
FROM
TO
MAIER1Al
1MPLA MENrMETHOU * ANQV9T
0 fL
18 �`'
perdmw comes
Tremie
18 ft
23 Ft'
Bent;anits Chips
Pour
50 fl'
60 ft.
Bent. Chips
Pour
I9. S NA%;RAYLLPAC14 i(2 iemble
FROM
TO
Mh7YlSlhL
RMFLACfMV rrNFrH u
23 r'`
50 ft'
#2 Medium Sand
Pour
n,
n.
24. D R I L L i m G LQ6 ■liaeh aairdone1 sheets if w-Tt,mi
FROPA
T4
UffiCBIPTION CriidvF, bnrdn� &Wewk Ir slxe,ate.
ft,
ft-
ft.
fA
f.
fL
ft.
ft,
F.
n
ft.
21- REMARKS
21 CcrtiiieatioO
Sl mwre ofCeltlfied Welt Coaaactar Duet
Uy mi riimg theT fiHur, I Aen4y oerr ' rhar jIm vd1f2/ wim (Wrm) e"isrrar.W IA x vra&m
�iA 15ANCAC 02C () lied or J5A NCAC n2C .02W Weil omd rhm o
pgrygfAib; nR4n+'i{Jb¢r been pwrirdrdfu aloe Keflarwlmr.
23. Site disgnim or 8dditionnl well detailir
Yau may use Lhe bade of this page to provide: 6dditional uel I site d[LaLIS or rvdl
construction details. You may also atiechadditional pages II`nommary
SUBMITTAL INSTRUCTTOI S
24iL For All Wells, Submit this Herren within 30 days of complctinn oT well
cow(tuCtlon to thefpllrnving:
VO Divisio■ of Water Reamrccs. Iuiormation Prmessiag Uait,
MI7 M1itlil Service f,:entm, RaLcighrNC 276994417
24L For li iertion Wells, Tn addition to sending the farm to the address 1n 74a
about, RISO submit one Lwpy of this form within 30 days of completion of wel I
construction to the following:
Divisinn of Water Rp murees, U ■dcrgrauud Injection Control Program,
FOR WATER SUPPLY WELLS ONLY: 1635 Mail Service [:eater, lUlrigh, NC 276"-16M
13a, Yield (Rpm) Method of test 24e, For Water Sr 11* & Talleetion Wells, In addition to sending the farm to
the addresses} above, eiso submit one copy of thl5 frlrm vrithin 30 days of
13b. Nsinfrctiou tvpt, Amgnnt< wrnplction of wr.11 construction to the County hedL#h dep$LtmenL of the a mty
VAKn C4nRtr ntEd.
Form CW-1 NorthCluoLir DepnrhnentnfEmvmsmmmnle]{m6ty-LhvisionofWaierRcsatsrcce Ltev6ed2-22-2016
Attachment D
Well Development Logs
ANCHOR
QEA
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Al Development Log
Well ID:
MU13c
Project Name:
-' y� l Im Date:
1 p -L ji 2 2-
Project Number:
C2Z tj-410 ' n 1 , 6 j Weather:
tk'�,
Project Location:
�/S Facility ID or Permit * (if applicable):
W�j
Sample Collector(s):
r
�� Sample ID (on COC):
W
Well Diamter:
2. in Sample time:
J
Screen Interval:
_
2fiJ • L+ , ft bgs Well Depth (WD):
Li.l�9 ft TOC
Packer Interval:
��j� ft Water Level in Feet (WL):
_
ft TOC
Measuring Point:
-gyp G Length of Water Column (LWQ:
ft; (WD - WL)
Water lost during drilling interval:
_
IV 3Q D 5CLAOne Casing Volume:
Volume
—euej�
gallons; (LWC x WCV)
Casing Height:
Total to be removed:
gallons
Well Type:.Ack
Up ❑Flush Mount Actual Volume Purged:
gallons
Comments:
Well Casing Volumes (WCV)
1" = 0.041 Gal/Ft
"= 016 Gal/Ftt 3" = 0.38 Gal/Ft 4" = 0.66 Gal/Ft 6" = 1.5 Gal/Ft 8" =
2.6 Gal/Ft 12" = 5.8 Gal/Ft
Purge Method: Bailer-Disp.
Bailer -Teflon Dedicated Pump ale Pump Grundfos Waterra Other:l�1dL3�T
Sample Method: Bailer-Disp.
_
Bailer -Teflon Dedicated Pump Whale Pump Grundfos Waterra Other.
Dept of
OxTdatlon
Pump
Depth to
Temperatu
Dissolved
Specific
pH (S.U.)
Reduction
Intake
Water
Gallons
re
Oxygen
Conductivity
report to
Potential
Turbidity
Reading
Time
(ft TO
(ft TOC)
Purged
('C)
(mg/L)
(Nmhos/cm)
0.1 S.U.
(mV)
(NTU)
Comments
1
2
1}'
Av
C(
3
-'
l0
4
1 2,3ci2
Q
5
el'.2
6
b+q
8
3 5
10
11
1 t
Q
q Cl
12I!L
.
13
f 1+ W
14
4
15�,.
Protective Casing (if applicable):
Pad: Lock: Vegetation:+ijar Access: `— o
Uh ,)U U 0
Sample
Sample Analysts Signatur nAnalysts
U1x
iap %
Date:
Name:
Notes:
1: Stabilization (3 successive readings, 3 minutes apart): within +/- 70% DO and turbidity,' +/- 3% Conductivity; +/ 0.1 pH unit +/- 10 mV for ORP
from EPA - Low -Flow (Minimal Drawdown) Groundwater S6mpling Procedures, April 1996 (Rev 2017)
2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
3. Samples are analyzed immediately upon collection.
Field Laboratory Certificate Number 5445
Aobreviations:
°C: degrees Celsius S.U: standard units
pmhos/cm: micromhos per centimeter ft: feet
mg/L: milligrams per liter in: inches
mV: millivolt bgs: below ground surface
NTU: nephelometric turbidity units TOC: top of casing
Method Reference:
Temperature: SM 2550 B-2010
Specific conductivity: EPA Method 120.1, Rev. 1982
DO: SM 4500 O G-2011
PH: SM 4500-H' B-2011
Turbidity: SM 2130 B-2011
U25
4,31p 2--J.-
Page of
MW-1 C Well Development
Ti►�►e Pump 1n fG ke
`t35 40
1440 LA
1; 0 5
15!0
[515
k520
_WJ TL D
2-T-. of 35 A
2i. Of 9 Ito
n (d lads
225
kZANCHOR
QEA
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Al Development Log
Well ID: �( �,�) _
Project Name:
T 'nn
1 (u r t r
Date:
L20— ZZ
Project Number:Z'LC,
—Q ; o
_W
Weather:
Project Location:
�.i Cj
Facility ID or Permit # (if applicable):
Sample Collector(s):
Sample ID (on COC): N_
Well Diamter.
A
in Sample time: N
Screen Interval:
i,� _
ft bgs Well Depth (WD): ft TOC
Packer Interval:
TN
ft Water Level in Feet (WL): ft TOC
Measuring Point:
TVD
Length of Water Column (LWQ: ft; (WD - WL)
Water lost during drilling interval:
One Casing Volume: gallons; (LWC x WCV)
Casing Height:
�} R
Total Volume to be removed: gallons
Well Type:
[�
s/Stick Up oFlush Mount
Actual Volume Purged: gallons
Comments: N 2 y n f
�vrj ►
l
- ve ►n ��t a In /T p� L'v
Well Casing Volumes (WCV)
1" = 0.041 Gal/Ft
2" = 0.16 Gal/Ft 3" = 0.38 Gal/Ft
4" = 0.66 Gal/Ft 6" = 1.S Gal/Ft 8" = 2.6 Gal/Ft 12" = 5.8 Gal/Ft
Purge Method: Bailer-Disp.
Bailer -Teflon Dedicated Pump Whale Pump Grundfos Waterra Other.
Sample Method: Bailer-Disp.
Bailer -Teflon Dedicated Pump Whale Pump Grundfos Waterra Other.
Depth o
Oxidation
Pump
Depth to
Temperatu
Dissolved
Specific
pH (S.U.)
Reduction
Intake
Water
Gallons
re
Oxygen
Conductivity
report to
Potential
Turbidity
Reading
Time
(ft TOC)
(ft TOC)
Purged
(°C)
(mg/L)
(pmhos/cm)
0.1 S.U.
(mv)
(NTU)
Comments
2
l.yz l
3
►
y
V J
4
lo
C
6
Ili
�5-
2
7
-'' A
t_11
B
40
44LS
51, 4Z
9
10
11
7. 41-
12
13
14
'
15
Protective Casing (if applicable): .�
Pad: ✓ Lock: .l
Vegetation: �J j� Access: YD p( I d
Sample
Sample Analysts Signature- A�
Analysts
Date: �'
—
Name:
1
Notes.
1: Stabilization (3 successive readings, 3 minutes apart): within +/- 70% DO and turbidity, +/- 3% Conductivity- +/- 0.1 PH unit +/- 70 mV for ORP
from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017)
2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
3. Samples are analyzed immediately upon collection.
' Field Laboratory Certificate Number 5445
Abbreviations:
°C: degrees Celsius
pmhos/cm: micromhos per centimeter
mg/L: milligrams per liter
mv: millivolt
NTU: nephelometric turbidity units
S.U.: standard units
ft: feet
in: inches
bgs: below ground surface
TOC: top of casing
Method Reference:
Temperature: SM 2550 B-2010
Specific conductivity: EPA Method 120.1, Rev. 1982
DO: SM 4500 O G-2011
pH: SM 4500-H' B-2011
Turbidity: SM 2130 B-2011
Page — of
Attachment E
Field Sampling Forms
V"r
ANCHOR
QEA
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
v-Flow Sampling Log
Well ID: s
t
Name:* Date:
Project Number: - V Weather:
Project Location: & Facility ID or Permit # (if applicable):
Sample Collector(s): Sample ID (on-COC):
Well Diameter: in Arrive at Well:
Screen Interval:. ft bgs Start Time:
Well Depth (as constructed): ft bgs Sample Time:
Depth to Water. 3 ft Leave Well:
Measuring Point: Well Type:
Depth of Pump Intake: ft Tagged Bottom:
Pump Used (circle): Peristaltic B�d, Other (describe):
Comments:
bL l
�Project ?.2
"VtU.? Q
D
7'
b '
tick Up ❑Flush Mount
ft at (time):
Purge Rate:
Total Volume Purged:
Pump Speed:
5
2a S
Time
DTW (feet)
Temperature (°C)
Dissolved Oxygen
(mg/L)
Specific
Conductivity
(pmhos/cm)
pH (S.U.)
report to 0.1 S.U.
Oxidation
Reduction
Potential (mV)
Turbidity (NTU)
1 r9C1
35"i
12.
e9-,
3
-Z'_+y .
,3
V L
I'
A
I-SISA,
4 s
'5S, 3o
o7_,
`� ''2U
2- LA�
z-
I3.Li
L
[Z.
Sample Analyst Signature:
Sample Analyst
Name:
Date:
Notes:
1: Stabilization (3 successive readings, 3 minutes apart): within +/- 70% DO and turbidity,, +/- 3% Conductivity,' +/- 0.1 pH unit +/- 10 mV (or ORP
from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017)
2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
3. Samples are analyzed immediately upon collection.
4. NC Field Laboratory Certificate Number 5445
5. 1 pmho/cm = 1 pS/cm
Abbreviations:
Method Reference:
'C: degrees Celsius S.U.: standard units
Temperature: SM 2550 B-2010
pmhos/cm: micromhos per centimeter ft: feet
Specific conductivity: EPA Method 120.1, Rev: 1982
mg/L: milligrams per liter in: inches
DO: SM 4500 0 G-2011
mv: millivolt bgs: below ground surface
pH: SM 4500-H' B-2011
NTU: nephelometric turbidity units TOO top of casing
Turbidity: SM 2130 B-2011
Page 1 of 1
1
ANCHOR
QEA
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
v-Flow Sampling Log
well ID:
Project Name: "
Project Number: n I ,0
Project Location:
Sample Collector(s):
Well Diameter: it
Screen Interval:
Well Depth (as constructed):
Depth to Water:
Measuring Point:
Depth of Pump Intake:
Pump Used (circle): Peristaltic Ladd
Comments:
Date: P 2
Weather. r
Facility ID or Permit # (if applicable): W 3
Sample ID (on COC): ZOM
in Arrive at Well:
ft bgs Start Time:,
ft bgs Sample Time:
ft Leave Well: "
Well Type: oStick Up ❑Flush Mount
ft Tagged Bottom: ft at (time):
Rate: e VOA
�� ` Purge
Other (describe):"�
(�/ Total Volume Purged:
Pump Speed Af 0 r.p Z
Time
DTW (feet)
Temperature (°C)
Dissolved Oxygen
(mg/L)
Specific
Conductivity
(pmhos/cm)
pH (S.U.)
report to 0.1 S.U.
Oxidation
Reduction
Potential (mV)
Turbidity (NTU)
I
.,b-
qq
II`!
3
D. 14
,
0
3
t.
4
i(
U
0
8r
3ti
3
L4►�,
Sample Analyst Signature:``
ample Analyst
Name:
��pp
(X. � Date:
FF
Notes:
1: Stabilization (3 successive readings, 3 minutes apart): within +/- 70% DO and turbidity; +/- 3% Conductivity, +/- 0.7 pH unit +/- 10 mV for ORP
from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017)
2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
3. Samples are analyzed immediately upon collection.
4. NC Field Laboratory Certificate Number 5445
5. 1 pmho/cm = 1 pS/cm
Abbreviations:
Method Reference:
°C: degrees Celsius S.U: standard units
Temperature: SM 2550 B-2010
pmhos/cm: micromhos per centimeter ft: feet
Specific conductivity: EPA Method 120.1, Rev. 1982
mg/L: milligrams per liter in: inches
DO: SM 4500 0 G-2011
mV: millivolt bgs: below ground surface
pH: SM 4500-H' B-2011
NTU: nephelometric turbidity units TOC:. top of casing
Turbidity: SM 2130 B-2011
Page 1 of 1
�, y2 ANCHOR
[,,, QEA
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
N-Flow Sampling Log
Well ID: M -3
Project Name: '� h ! (i'L "A
Project Number: '� �j "Q , !
Project Location:
Sample Collector(s): ]- ti/
Well Diameter: t
Screen Interval:
Well Depth (as constructed): L4
Depth to Water: ', .
Measuring Point:
Depth of Pump Intake:
Pump Used (circle): Peristaltic Bladder
Comments:'
Date: I I 10 2, 2
Weather: r1 (
Facility ID or Permit # (if applicable):
Sample ID (on COQ LL9L r7�Z. 1 I
in Arrive at Well:
^
ft bgs Start Time:If 16
ft bgs Sample Time:
ft Leave Well:
Well Type: Wick Up ❑Flush Mount
ft Tagged Bottom: ft at (time):
Other (describe): Purge Rate: �'9n 1
�i�li f Total Volume Purged:
Pump Speed:
Time
DTW (feet)
Temperature (°C)
Dissolved Oxygen
(mg/L)
Specific
Conductivity
(pmhos/cm)
pH (S.U.)
report to 0.1 S.U.
Oxidation
Reduction
Potential (mV)
Turbidity (NTU)
15
4utq
►a
1.83
s4,U
S.
To
Id d F
01
's 4
m '-i.
tj `'' Lf
`
Qyy
{fit
. � 3
i •' 9
i '✓
�
� � s
�
11
�y+y� �y
t y�
,
�
' 36.9
c��;
ra
Sample Analyst Signature.
Sample Analyst
Name: 7K
Date: 0 ��
Notes:
1: Stabilization (3 successive readings, 3 minutes apart): within +/- 10% DO and turbidity, +/- 3% Conductivity, +/- 0.1 pH unit; +/- 10 mV for ORP
from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017)
2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
3. Samples are analyzed immediately upon collection. t __ j j•
4. NC Field Laboratory Certificate Number 5445 r VVPI{�„%� + •
5. 1 pmho/cm = 1 PS/cm
Abbreviations:
°C: degrees Celsius
S.U: standard units
pmhos/cm: micromhos per centimeter
ft: feet
mg/L: milligrams per liter
in: inches
mv: millivolt
bgs: below ground surface
NTU: nephelometric turbidity units
TOC: top of casing
Method Reference:
Temperature: SM 2550 B-2010
Specific conductivity: EPA Method 120.1, Rev. 1982
DO: SM 4500 0 G-2011
PH: SM 4500-H' B-2011
Turbidity: SM 2130 B-2011
Page 1 of 1
Attachment F
Laboratory Analytical Report
leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
November 18, 2022
Jennifer Verde
Anchor QEA
231 Haywood Street
Asheville, NC 28801
RE: Project: Trillium Links & Lake 11/10
Pace Project No.: 92636078
Dear Jennifer Verde:
Enclosed are the analytical results for sample(s) received by the laboratory on November 10, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
angela.baioni@pacelabs.com
(704)875-9092
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
Project: Trillium Links & Lake 11/10
Pace Project No.: 92636078
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
VirginiaNELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Trillium Links & Lake 11/10
92636078
Analytes
Lab lD
Sample ID
Method
Analysts
Reported
Laboratory
92636078001
MW-1C
SM 6200B
CL
63
PASI-C
SM 2540C-2015
CS1
1
PASI-A
SM 9222D-2015
YEG
1
PASI-A
EPA 300.0 Rev 2.1 1993
JCM
1
PASI-A
EPA 350.1 Rev 2.0 1993
ARJ
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 365.1 Rev 2.0 1993
MDW
1
PASI-A
SM 4500-CI-E-2011
ANM
1
PASI-A
SM 531OB-2014
MJP
1
PASI-A
92636078002
MW-2C
SM 6200B
CL
63
PASI-C
SM 2540C-2015
CS1
1
PASI-A
SM 9222D-2015
YEG
1
PASI-A
EPA 300.0 Rev 2.1 1993
JCM
1
PASI-A
EPA 350.1 Rev 2.0 1993
ARJ
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 365.1 Rev 2.0 1993
MDW
1
PASI-A
SM 4500-CI-E-2011
ANM
1
PASI-A
SM 531OB-2014
MJP
1
PASI-A
92636078003
MW-3C
SM 6200B
CL
63
PASI-C
SM 2540C-2015
CS1
1
PASI-A
SM 9222D-2015
YEG
1
PASI-A
EPA 300.0 Rev 2.1 1993
JCM
1
PASI-A
EPA 350.1 Rev 2.0 1993
ARJ
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 365.1 Rev 2.0 1993
MDW
1
PASI-A
SM 4500-CI-E-2011
ANM
1
PASI-A
SM 531OB-2014
MJP
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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Asheville, NC 28804
(828)254-7176
ANALYTICAL RESULTS
Project: Trillium Links & Lake 11/10
Pace Project No.: 92636078
Sample: MWAC Lab ID: 92636078001 Collected: 11/10/22 13:48 Received: 11/10/22 15:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Benzene
ND
ug/L
0.50
1
11/15/22 20:42
71-43-2
Bromobenzene
ND
ug/L
0.50
1
11/15/22 20:42
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
11/15/22 20:42
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
11/15/22 20:42
75-27-4
Bromoform
ND
ug/L
0.50
1
11/15/22 20:42
75-25-2
Bromomethane
ND
ug/L
5.0
1
11/15/22 20:42
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
11/15/22 20:42
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
11/15/22 20:42
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
11/15/22 20:42
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
11/15/22 20:42
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
11/15/22 20:42
108-90-7
Chloroethane
ND
ug/L
1.0
1
11/15/22 20:42
75-00-3
Chloroform
ND
ug/L
0.50
1
11/15/22 20:42
67-66-3
Chloromethane
ND
ug/L
1.0
1
11/15/22 20:42
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
11/15/22 20:42
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
11/15/22 20:42
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
11/15/22 20:42
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
11/15/22 20:42
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
11/15/22 20:42
106-93-4
Dibromomethane
ND
ug/L
0.50
1
11/15/22 20:42
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
11/15/22 20:42
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
11/15/22 20:42
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
11/15/22 20:42
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
11/15/22 20:42
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
11/15/22 20:42
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
11/15/22 20:42
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
11/15/22 20:42
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
11/15/22 20:42
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
11/15/22 20:42
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
11/15/22 20:42
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
11/15/22 20:42
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
11/15/22 20:42
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
11/15/22 20:42
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
11/15/22 20:42
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
11/15/22 20:42
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
11/15/22 20:42
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
11/15/22 20:42
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
11/15/22 20:42
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
11/15/22 20:42
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
11/15/22 20:42
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
11/15/22 20:42
1634-04-4
Naphthalene
ND
ug/L
2.0
1
11/15/22 20:42
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
11/15/22 20:42
103-65-1
Styrene
ND
ug/L
0.50
1
11/15/22 20:42
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
11/15/22 20:42
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
11/15/22 20:42
79-34-5
REPORT OF LABORATORY ANALYSIS
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Date: 11 /18/2022 11:39 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 30
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ANALYTICAL RESULTS
Project: Trillium Links & Lake 11/10
Pace Project No.: 92636078
Sample: MWAC Lab ID: 92636078001 Collected: 11/10/22 13:48 Received: 11/10/22 15:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
Tetrachloroethene
ND ug/L
0.50
1
11/15/22 20:42
127-18-4
Toluene
ND ug/L
0.50
1
11/15/22 20:42
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
2.0
1
11/15/22 20:42
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
2.0
1
11/15/22 20:42
120-82-1
1,1,1-Trichloroethane
ND ug/L
0.50
1
11/15/22 20:42
71-55-6
1,1,2-Trichloroethane
ND ug/L
0.50
1
11/15/22 20:42
79-00-5
Trichloroethene
ND ug/L
0.50
1
11/15/22 20:42
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
11/15/22 20:42
75-69-4
1,2,3-Trichloropropane
ND ug/L
0.50
1
11/15/22 20:42
96-18-4
1,2,4-Trimethylbenzene
ND ug/L
0.50
1
11/15/22 20:42
95-63-6
1,3,5-Trimethylbenzene
ND ug/L
0.50
1
11/15/22 20:42
108-67-8
Vinyl chloride
ND ug/L
1.0
1
11/15/22 20:42
75-01-4
m&p-Xylene
ND ug/L
1.0
1
11/15/22 20:42
179601-23-1
o-Xylene
ND ug/L
0.50
1
11/15/22 20:42
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
99 %
70-130
1
11/15/22 20:42
17060-07-0
4-Bromofluorobenzene (S)
96 %
70-130
1
11/15/22 20:42
460-00-4
Toluene-d8 (S)
98 %
70-130
1
11/15/22 20:42
2037-26-5
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2015
Pace Analytical Services -Asheville
Total Dissolved Solids
64.0 mg/L
25.0
1
11/15/22 17:48
MBIO 9222D Fecal Coliform AVL
Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services -Asheville
Fecal Coliforms
ND CFU/100 mL
1.0
1
11/10/22 16:58 11/11/22 15:04
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Sulfate
ND mg/L
1.0
1
11/12/2215:03
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/L
0.10
1
11/14/22 14:17
7664-41-7
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
1.5 mg/L
0.040
1
11/11/22 01:16
14797-55-8
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
ND mg/L
0.050
1
11/14/22 14:39 11/14/22 20:04
7723-14-0
Date: 11 /18/2022 11:39 AM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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(828)254-7176
ANALYTICAL RESULTS
Project: Trillium Links & Lake 11/10
Pace Project No.: 92636078
Sample: MWAC
Parameters
Lab ID: 92636078001 Collected: 11/10/22 13:48
Results Units Report Limit DF
Received: 11/10/22 15:55 Matrix: Water
Prepared Analyzed CAS No. Qual
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
1.9 mg/L 1.0 1
11/15/2218:34 16887-00-6
5310B TOC
Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
ND mg/L 1.0 1
11/15/22 18:11 7440-44-0
Date: 11 /18/2022 11:39 AM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Asheville, NC 28804
(828)254-7176
ANALYTICAL RESULTS
Project: Trillium Links & Lake 11/10
Pace Project No.: 92636078
Sample: MW-2C Lab ID: 92636078002 Collected: 11/10/22 11:26 Received: 11/10/22 15:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Benzene
ND
ug/L
0.50
1
11/15/22 21:00
71-43-2
Bromobenzene
ND
ug/L
0.50
1
11/15/22 21:00
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
11/15/22 21:00
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
11/15/22 21:00
75-27-4
Bromoform
ND
ug/L
0.50
1
11/15/22 21:00
75-25-2
Bromomethane
ND
ug/L
5.0
1
11/15/22 21:00
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
11/15/22 21:00
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
11/15/22 21:00
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
11/15/22 21:00
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
11/15/22 21:00
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
11/15/22 21:00
108-90-7
Chloroethane
ND
ug/L
1.0
1
11/15/22 21:00
75-00-3
Chloroform
ND
ug/L
0.50
1
11/15/22 21:00
67-66-3
Chloromethane
ND
ug/L
1.0
1
11/15/22 21:00
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
11/15/22 21:00
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
11/15/22 21:00
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
11/15/22 21:00
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
11/15/22 21:00
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
11/15/22 21:00
106-93-4
Dibromomethane
ND
ug/L
0.50
1
11/15/22 21:00
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
11/15/22 21:00
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
11/15/22 21:00
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
11/15/22 21:00
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
11/15/22 21:00
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
11/15/22 21:00
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
11/15/22 21:00
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
11/15/22 21:00
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
11/15/22 21:00
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
11/15/22 21:00
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
11/15/22 21:00
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
11/15/22 21:00
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
11/15/22 21:00
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
11/15/22 21:00
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
11/15/22 21:00
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
11/15/22 21:00
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
11/15/22 21:00
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
11/15/22 21:00
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
11/15/22 21:00
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
11/15/22 21:00
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
11/15/22 21:00
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
11/15/22 21:00
1634-04-4
Naphthalene
ND
ug/L
2.0
1
11/15/22 21:00
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
11/15/22 21:00
103-65-1
Styrene
ND
ug/L
0.50
1
11/15/22 21:00
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
11/15/22 21:00
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
11/15/22 21:00
79-34-5
REPORT OF LABORATORY ANALYSIS
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Date: 11 /18/2022 11:39 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 30
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2225 Riverside Dr.
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ANALYTICAL RESULTS
Project: Trillium Links & Lake 11/10
Pace Project No.: 92636078
Sample: MW-2C Lab ID: 92636078002 Collected: 11/10/22 11:26 Received: 11/10/22 15:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
Tetrachloroethene
ND ug/L
0.50
1
11/15/22 21:00
127-18-4
Toluene
ND ug/L
0.50
1
11/15/22 21:00
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
2.0
1
11/15/22 21:00
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
2.0
1
11/15/22 21:00
120-82-1
1,1,1-Trichloroethane
ND ug/L
0.50
1
11/15/22 21:00
71-55-6
1,1,2-Trichloroethane
ND ug/L
0.50
1
11/15/22 21:00
79-00-5
Trichloroethene
ND ug/L
0.50
1
11/15/22 21:00
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
11/15/22 21:00
75-69-4
1,2,3-Trichloropropane
ND ug/L
0.50
1
11/15/22 21:00
96-18-4
1,2,4-Trimethylbenzene
ND ug/L
0.50
1
11/15/22 21:00
95-63-6
1,3,5-Trimethylbenzene
ND ug/L
0.50
1
11/15/22 21:00
108-67-8
Vinyl chloride
ND ug/L
1.0
1
11/15/22 21:00
75-01-4
m&p-Xylene
ND ug/L
1.0
1
11/15/22 21:00
179601-23-1
o-Xylene
ND ug/L
0.50
1
11/15/22 21:00
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
99 %
70-130
1
11/15/22 21:00
17060-07-0
4-Bromofluorobenzene (S)
97 %
70-130
1
11/15/22 21:00
460-00-4
Toluene-d8 (S)
100 %
70-130
1
11/15/22 21:00
2037-26-5
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2015
Pace Analytical Services -Asheville
Total Dissolved Solids
ND mg/L
25.0
1
11/15/22 17:48
MBIO 9222D Fecal Coliform AVL
Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services -Asheville
Fecal Coliforms
ND CFU/100 mL
1.0
1
11/10/22 16:58 11/11/22 15:04
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Sulfate
ND mg/L
1.0
1
11/12/2215:18
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/L
0.10
1
11/14/22 14:21
7664-41-7
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
0.085 mg/L
0.040
1
11/11/22 01:14
14797-55-8
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
ND mg/L
0.050
1
11/14/22 14:39 11/14/22 20:05
7723-14-0
Date: 11 /18/2022 11:39 AM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 8 of 30
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2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
ANALYTICAL RESULTS
Project: Trillium Links & Lake 11/10
Pace Project No.: 92636078
Sample: MW-2C Lab ID: 92636078002 Collected: 11/10/22 11:26 Received: 11/10/22 15:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
4500 Chloride Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride 3.1 mg/L 1.0 1 11/15/2218:35 16887-00-6
5310B TOC Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon ND mg/L 1.0 1 11/15/22 18:26 7440-44-0
Date: 11 /18/2022 11:39 AM
REPORT OF LABORATORY ANALYSIS
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2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
ANALYTICAL RESULTS
Project: Trillium Links & Lake 11/10
Pace Project No.: 92636078
Sample: MW-3C Lab ID: 92636078003 Collected: 11/10/22 12:36 Received: 11/10/22 15:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Benzene
ND
ug/L
0.50
1
11/15/22 21:18
71-43-2
Bromobenzene
ND
ug/L
0.50
1
11/15/22 21:18
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
11/15/22 21:18
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
11/15/22 21:18
75-27-4
Bromoform
ND
ug/L
0.50
1
11/15/22 21:18
75-25-2
Bromomethane
ND
ug/L
5.0
1
11/15/22 21:18
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
11/15/22 21:18
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
11/15/22 21:18
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
11/15/22 21:18
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
11/15/22 21:18
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
11/15/22 21:18
108-90-7
Chloroethane
ND
ug/L
1.0
1
11/15/22 21:18
75-00-3
Chloroform
ND
ug/L
0.50
1
11/15/22 21:18
67-66-3
Chloromethane
ND
ug/L
1.0
1
11/15/22 21:18
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
11/15/22 21:18
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
11/15/22 21:18
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
11/15/22 21:18
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
11/15/22 21:18
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
11/15/22 21:18
106-93-4
Dibromomethane
ND
ug/L
0.50
1
11/15/22 21:18
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
11/15/22 21:18
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
11/15/22 21:18
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
11/15/22 21:18
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
11/15/22 21:18
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
11/15/22 21:18
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
11/15/22 21:18
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
11/15/22 21:18
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
11/15/22 21:18
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
11/15/22 21:18
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
11/15/22 21:18
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
11/15/22 21:18
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
11/15/22 21:18
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
11/15/22 21:18
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
11/15/22 21:18
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
11/15/22 21:18
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
11/15/22 21:18
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
11/15/22 21:18
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
11/15/22 21:18
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
11/15/22 21:18
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
11/15/22 21:18
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
11/15/22 21:18
1634-04-4
Naphthalene
ND
ug/L
2.0
1
11/15/22 21:18
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
11/15/22 21:18
103-65-1
Styrene
ND
ug/L
0.50
1
11/15/22 21:18
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
11/15/22 21:18
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
11/15/22 21:18
79-34-5
REPORT OF LABORATORY ANALYSIS
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Date: 11 /18/2022 11:39 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 30
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2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
ANALYTICAL RESULTS
Project: Trillium Links & Lake 11/10
Pace Project No.: 92636078
Sample: MW-3C Lab ID: 92636078003 Collected: 11/10/22 12:36 Received: 11/10/22 15:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
Tetrachloroethene
ND ug/L
0.50
1
11/15/22 21:18
127-18-4
Toluene
ND ug/L
0.50
1
11/15/22 21:18
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
2.0
1
11/15/22 21:18
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
2.0
1
11/15/22 21:18
120-82-1
1,1,1-Trichloroethane
ND ug/L
0.50
1
11/15/22 21:18
71-55-6
1,1,2-Trichloroethane
ND ug/L
0.50
1
11/15/22 21:18
79-00-5
Trichloroethene
ND ug/L
0.50
1
11/15/22 21:18
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
11/15/22 21:18
75-69-4
1,2,3-Trichloropropane
ND ug/L
0.50
1
11/15/22 21:18
96-18-4
1,2,4-Trimethylbenzene
ND ug/L
0.50
1
11/15/22 21:18
95-63-6
1,3,5-Trimethylbenzene
ND ug/L
0.50
1
11/15/22 21:18
108-67-8
Vinyl chloride
ND ug/L
1.0
1
11/15/22 21:18
75-01-4
m&p-Xylene
ND ug/L
1.0
1
11/15/22 21:18
179601-23-1
o-Xylene
ND ug/L
0.50
1
11/15/22 21:18
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
98 %
70-130
1
11/15/22 21:18
17060-07-0
4-Bromofluorobenzene (S)
97 %
70-130
1
11/15/22 21:18
460-00-4
Toluene-d8 (S)
99 %
70-130
1
11/15/22 21:18
2037-26-5
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2015
Pace Analytical Services -Asheville
Total Dissolved Solids
ND mg/L
25.0
1
11/15/22 17:48
MBIO 9222D Fecal Coliform AVL
Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services -Asheville
Fecal Coliforms
ND CFU/100 mL
1.0
1
11/10/22 16:58 11/11/22 15:04
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Sulfate
ND mg/L
1.0
1
11/12/2216:02
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/L
0.10
1
11/14/22 14:25
7664-41-7
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
0.92 mg/L
0.040
1
11/11/22 01:15
14797-55-8
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
0.099 mg/L
0.050
1
11/14/22 14:39 11/14/22 20:07
7723-14-0
Date: 11 /18/2022 11:39 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 30
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2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
ANALYTICAL RESULTS
Project: Trillium Links & Lake 11/10
Pace Project No.: 92636078
Sample: MW-3C Lab ID: 92636078003 Collected: 11/10/22 12:36 Received: 11/10/22 15:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
4500 Chloride Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride 6.3 mg/L 1.0 1 11/15/2218:36 16887-00-6
5310B TOC Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon ND mg/L 1.0 1 11/15/22 18:43 7440-44-0
Date: 11 /18/2022 11:39 AM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 12 of 30
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2225 Riverside Dr.
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QUALITY CONTROL DATA
Project: Trillium Links & Lake 11/10
Pace Project No.: 92636078
QC Batch: 736787 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92636078001, 92636078002, 92636078003
METHOD BLANK: 3834453 Matrix:
Associated Lab Samples: 92636078001, 92636078002, 92636078003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
11/15/22 13:28
1,1,1-Trichloroethane
ug/L
ND
0.50
11/15/22 13:28
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
11/15/22 13:28
1,1,2-Trichloroethane
ug/L
ND
0.50
11/15/22 13:28
1,1-Dichloroethane
ug/L
ND
0.50
11/15/22 13:28
1,1-Dichloroethene
ug/L
ND
0.50
11/15/22 13:28
1,1-Dichloropropene
ug/L
ND
0.50
11/15/22 13:28
1,2,3-Trichlorobenzene
ug/L
ND
2.0
11/15/22 13:28
1,2,3-Trichloropropane
ug/L
ND
0.50
11/15/22 13:28
1,2,4-Trichlorobenzene
ug/L
ND
2.0
11/15/22 13:28
1,2,4-Trimethylbenzene
ug/L
ND
0.50
11/15/22 13:28
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
11/15/22 13:28
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
11/15/22 13:28
1,2-Dichlorobenzene
ug/L
ND
0.50
11/15/22 13:28
1,2-Dichloroethane
ug/L
ND
0.50
11/15/22 13:28
1,2-Dichloropropane
ug/L
ND
0.50
11/15/22 13:28
1,3,5-Trimethylbenzene
ug/L
ND
0.50
11/15/22 13:28
1,3-Dichlorobenzene
ug/L
ND
0.50
11/15/22 13:28
1,3-Dichloropropane
ug/L
ND
0.50
11/15/22 13:28
1,4-Dichlorobenzene
ug/L
ND
0.50
11/15/22 13:28
2,2-Dichloropropane
ug/L
ND
0.50
11/15/22 13:28
2-Chlorotoluene
ug/L
ND
0.50
11/15/22 13:28
4-Chlorotoluene
ug/L
ND
0.50
11/15/22 13:28
Benzene
ug/L
ND
0.50
11/15/22 13:28
Bromobenzene
ug/L
ND
0.50
11/15/22 13:28
Bromochloromethane
ug/L
ND
0.50
11/15/22 13:28
Bromodichloromethane
ug/L
ND
0.50
11/15/22 13:28
Bromoform
ug/L
ND
0.50
11/15/22 13:28
Bromomethane
ug/L
ND
5.0
11/15/22 13:28
Carbon tetrachloride
ug/L
ND
0.50
11/15/22 13:28
Chlorobenzene
ug/L
ND
0.50
11/15/22 13:28
Chloroethane
ug/L
ND
1.0
11/15/22 13:28
Chloroform
ug/L
ND
0.50
11/15/22 13:28
Chloromethane
ug/L
ND
1.0
11/15/22 13:28
cis-1,2-Dichloroethene
ug/L
ND
0.50
11/15/22 13:28
cis-1,3-Dichloropropene
ug/L
ND
0.50
11/15/22 13:28
Dibromochloromethane
ug/L
ND
0.50
11/15/22 13:28
Dibromomethane
ug/L
ND
0.50
11/15/22 13:28
Dichlorodifluoromethane
ug/L
ND
0.50
11/15/22 13:28
Diisopropyl ether
ug/L
ND
0.50
11/15/22 13:28
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 11 /18/2022 11:39 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 30
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Asheville, NC 28804
(828)254-7176
QUALITY CONTROL DATA
Project: Trillium Links & Lake 11/10
Pace Project No.: 92636078
METHOD BLANK: 3834453 Matrix:
Associated Lab Samples: 92636078001, 92636078002, 92636078003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
Ethylbenzene
ug/L
ND
0.50
11/15/22 13:28
Hexachloro-1,3-butadiene
ug/L
ND
2.0
11/15/22 13:28
Isopropylbenzene (Cumene)
ug/L
ND
0.50
11/15/22 13:28
m&p-Xylene
ug/L
ND
1.0
11/15/22 13:28
Methyl-tert-butyl ether
ug/L
ND
0.50
11/15/22 13:28
Methylene Chloride
ug/L
ND
2.0
11/15/22 13:28
n-Butylbenzene
ug/L
ND
0.50
11/15/22 13:28
n-Propylbenzene
ug/L
ND
0.50
11/15/22 13:28
Naphthalene
ug/L
ND
2.0
11/15/22 13:28
o-Xylene
ug/L
ND
0.50
11/15/22 13:28
sec-Butylbenzene
ug/L
ND
0.50
11/15/22 13:28
Styrene
ug/L
ND
0.50
11/15/22 13:28
tert-Butyl benzene
ug/L
ND
0.50
11/15/22 13:28
Tetrachloroethene
ug/L
ND
0.50
11/15/22 13:28
Toluene
ug/L
ND
0.50
11/15/22 13:28
trans-1,2-Dichloroethene
ug/L
ND
0.50
11/15/22 13:28
trans- 1,3-Dichloropropene
ug/L
ND
0.50
11/15/22 13:28
Trichloroethene
ug/L
ND
0.50
11/15/22 13:28
Trichlorofluoromethane
ug/L
ND
1.0
11/15/22 13:28
Vinyl chloride
ug/L
ND
1.0
11/15/22 13:28
1,2-Dichloroethane-d4 (S)
%
98
70-130
11/15/22 13:28
4-Bromofluorobenzene (S)
%
99
70-130
11/15/22 13:28
Toluene-d8 (S)
%
100
70-130
11/15/22 13:28
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3834454
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
54.1
108
60-140
1,1,1-Trichloroethane
ug/L
50
48.3
97
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
51.7
103
60-140
1,1,2-Trichloroethane
ug/L
50
52.1
104
60-140
1,1-Dichloroethane
ug/L
50
45.5
91
60-140
1,1-Dichloroethene
ug/L
50
47.9
96
60-140
1,1-Dichloropropene
ug/L
50
51.0
102
60-140
1,2,3-Trichlorobenzene
ug/L
50
53.6
107
60-140
1,2,3-Trichloropropane
ug/L
50
50.1
100
60-140
1,2,4-Trichlorobenzene
ug/L
50
52.9
106
60-140
1,2,4-Trimethylbenzene
ug/L
50
52.5
105
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
51.7
103
60-140
1,2-Dibromoethane (EDB)
ug/L
50
53.0
106
60-140
1,2-Dichlorobenzene
ug/L
50
52.1
104
60-140
1,2-Dichloroethane
ug/L
50
48.7
97
60-140
1,2-Dichloropropane
ug/L
50
51.8
104
60-140
1,3,5-Trimethylbenzene
ug/L
50
51.5
103
60-140
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /18/2022 11:39 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 30
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
QUALITY CONTROL DATA
Project: Trillium Links & Lake 11/10
Pace Project No.: 92636078
LABORATORY CONTROL SAMPLE:
Parameter
3834454
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3-Dichlorobenzene
ug/L
50
52.3
105
60-140
1,3-Dichloropropane
ug/L
50
50.8
102
60-140
1,4-Dichlorobenzene
ug/L
50
49.8
100
60-140
2,2-Dichloropropane
ug/L
50
47.7
95
60-140
2-Chlorotoluene
ug/L
50
49.2
98
60-140
4-Chlorotoluene
ug/L
50
50.0
100
60-140
Benzene
ug/L
50
47.0
94
60-140
Bromobenzene
ug/L
50
51.0
102
60-140
Bromochloromethane
ug/L
50
49.4
99
60-140
Bromodichloromethane
ug/L
50
52.1
104
60-140
Bromoform
ug/L
50
55.7
111
60-140
Bromomethane
ug/L
50
47.4
95
60-140
Carbon tetrachloride
ug/L
50
46.6
93
60-140
Chlorobenzene
ug/L
50
51.3
103
60-140
Chloroethane
ug/L
50
47.7
95
60-140
Chloroform
ug/L
50
46.4
93
60-140
Chloromethane
ug/L
50
48.8
98
60-140
cis-1,2-Dichloroethene
ug/L
50
46.4
93
60-140
cis-1,3-Dichloropropene
ug/L
50
52.2
104
60-140
Dibromochloromethane
ug/L
50
53.7
107
60-140
Dibromomethane
ug/L
50
53.6
107
60-140
Dichlorodifluoromethane
ug/L
50
47.9
96
60-140
Diisopropyl ether
ug/L
50
47.0
94
60-140
Ethylbenzene
ug/L
50
50.6
101
60-140
Hexachloro-1,3-butadiene
ug/L
50
53.6
107
60-140
Isopropylbenzene(Cumene)
ug/L
50
51.0
102
60-140
m&p-Xylene
ug/L
100
101
101
60-140
Methyl-tert-butyl ether
ug/L
50
48.9
98
60-140
Methylene Chloride
ug/L
50
48.5
97
60-140
n-Butylbenzene
ug/L
50
52.9
106
60-140
n-Propylbenzene
ug/L
50
49.5
99
60-140
Naphthalene
ug/L
50
54.4
109
60-140
o-Xylene
ug/L
50
51.5
103
60-140
sec-Butylbenzene
ug/L
50
49.8
100
60-140
Styrene
ug/L
50
53.3
107
60-140
tert-Butyl benzene
ug/L
50
43.6
87
60-140
Tetrachloroethene
ug/L
50
51.2
102
60-140
Toluene
ug/L
50
48.5
97
60-140
trans-1,2-Dichloroethene
ug/L
50
47.2
94
60-140
trans- 1,3-Dichloropropene
ug/L
50
52.9
106
60-140
Trichloroethene
ug/L
50
52.3
105
60-140
Trichlorofluoromethane
ug/L
50
42.1
84
60-140
Vinyl chloride
ug/L
50
48.0
96
60-140
1,2-Dichloroethane-d4 (S)
%
101
70-130
4-Bromofluorobenzene (S)
%
102
70-130
Toluene-d8 (S)
%
99
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /18/2022 11:39 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 30
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
QUALITY CONTROL DATA
Project: Trillium Links & Lake 11/10
Pace Project No.: 92636078
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3836155
3836156
MS
MSD
92635852003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
4000
4000
5480
5570
137
139
60-140
2
1,1,1-Trichloroethane
ug/L
ND
4000
4000
5890
5590
147
140
60-140
5 M1
1,1,2,2-Tetrachloroethane
ug/L
ND
4000
4000
5180
5320
130
133
60-140
3
1,1,2-Trichloroethane
ug/L
ND
4000
4000
5350
5270
134
132
60-140
2
1,1-Dichloroethane
ug/L
ND
4000
4000
5620
5330
141
133
60-140
5 M1
1,1-Dichloroethene
ug/L
ND
4000
4000
6150
5870
154
147
60-140
5 M1
1,1-Dichloropropene
ug/L
ND
4000
4000
6290
5940
157
149
60-140
6 M1
1,2,3-Trichlorobenzene
ug/L
ND
4000
4000
4750
5470
119
137
60-140
14
1,2,3-Trichloropropane
ug/L
ND
4000
4000
5330
5400
133
135
60-140
1
1,2,4-Trichlorobenzene
ug/L
ND
4000
4000
4840
5230
121
131
60-140
8
1,2,4-Trimethylbenzene
ug/L
678
4000
4000
5860
5930
130
131
60-140
1
1,2-Dibromo-3-chloropropane
ug/L
ND
4000
4000
4850
5080
121
127
60-140
5
1,2-Dibromoethane (EDB)
ug/L
ND
4000
4000
5500
5460
138
137
60-140
1
1,2-Dichlorobenzene
ug/L
ND
4000
4000
5150
5280
129
132
60-140
2
1,2-Dichloroethane
ug/L
ND
4000
4000
5660
5350
142
134
60-140
6 M1
1,2-Dichloropropane
ug/L
ND
4000
4000
5780
5610
145
140
60-140
3 M1
1,3,5-Trimethylbenzene
ug/L
137
4000
4000
5300
5370
129
131
60-140
1
1,3-Dichlorobenzene
ug/L
ND
4000
4000
5150
5150
129
129
60-140
0
1,3-Dichloropropane
ug/L
ND
4000
4000
5430
5390
136
135
60-140
1
1,4-Dichlorobenzene
ug/L
ND
4000
4000
4960
5030
124
126
60-140
1
2,2-Dichloropropane
ug/L
ND
4000
4000
5570
5180
139
129
60-140
7
2-Chlorotoluene
ug/L
ND
4000
4000
5050
5100
126
128
60-140
1
4-Chlorotoluene
ug/L
ND
4000
4000
5000
4950
125
124
60-140
1
Benzene
ug/L
16100
4000
4000
21500
21600
136
137
60-140
0
Bromobenzene
ug/L
ND
4000
4000
5210
5160
130
129
60-140
1
Bromochloromethane
ug/L
ND
4000
4000
5720
5410
143
135
60-140
6 M1
Bromodichloromethane
ug/L
ND
4000
4000
5550
5420
139
135
60-140
2
Bromoform
ug/L
ND
4000
4000
5260
5300
132
133
60-140
1
Bromomethane
ug/L
ND
4000
4000
5870
5980
147
150
60-140
2 M1
Carbon tetrachloride
ug/L
ND
4000
4000
5350
5290
134
132
60-140
1
Chlorobenzene
ug/L
ND
4000
4000
5370
5340
134
133
60-140
1
Chloroethane
ug/L
ND
4000
4000
6890
6640
172
166
60-140
4 M1
Chloroform
ug/L
ND
4000
4000
5390
5150
135
129
60-140
5
Chloromethane
ug/L
ND
4000
4000
6770
6350
169
159
60-140
6 M1
cis-1,2-Dichloroethene
ug/L
ND
4000
4000
5610
5250
140
131
60-140
7
cis-1,3-Dichloropropene
ug/L
ND
4000
4000
5500
5340
138
133
60-140
3
Dibromochloromethane
ug/L
ND
4000
4000
5360
5320
134
133
60-140
1
Dibromomethane
ug/L
ND
4000
4000
5580
5580
139
140
60-140
0
Dichlorodifluoromethane
ug/L
ND
4000
4000
7400
7130
185
178
60-140
4 M1
Diisopropyl ether
ug/L
2350
4000
4000
7980
7480
141
128
60-140
6 M1
Ethylbenzene
ug/L
1290
4000
4000
6560
6650
132
134
60-140
1
Hexachloro-1,3-butadiene
ug/L
ND
4000
4000
4910
5100
123
127
60-140
4
Isopropylbenzene (Cumene)
ug/L
ND
4000
4000
5220
5300
130
132
60-140
2
m&p-Xylene
ug/L
4440
8000
8000
14900
15200
131
134
60-140
2
Methyl-tert-butyl ether
ug/L
1900
4000
4000
7730
7410
146
138
60-140
4 M1
Methylene Chloride
ug/L
ND
4000
4000
5520
5000
138
125
60-140
10
Results presented on this page are in
the units indicated by the
"Units" column except where
an alternate unit is presented
to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /18/2022 11:39 AM without the written consent of Pace Analytical Services, LLC. Page 16 of 30
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
QUALITY CONTROL DATA
Project: Trillium Links & Lake 11/10
Pace Project No.: 92636078
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3836155
3836156
MS
MSD
92635852003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
n-Butylbenzene
ug/L
ND
4000
4000
4940
5120
124
128
60-140
3
n-Propylbenzene
ug/L
81.1J
4000
4000
5110
5070
126
125
60-140
1
Naphthalene
ug/L
214J
4000
4000
5100
5780
122
139
60-140
13
o-Xylene
ug/L
2300
4000
4000
7610
7620
133
133
60-140
0
sec-Butylbenzene
ug/L
ND
4000
4000
5030
5120
126
128
60-140
2
Styrene
ug/L
ND
4000
4000
5390
5460
135
136
60-140
1
tert-Butyl benzene
ug/L
ND
4000
4000
4430
4420
111
111
60-140
0
Tetrachloroethene
ug/L
ND
4000
4000
5350
5390
134
135
60-140
1
Toluene
ug/L
25900
4000
4000
31000
31400
128
139
60-140
1
trans-1,2-Dichloroethene
ug/L
ND
4000
4000
5920
5550
148
139
60-140
6 M1
trans- 1,3-Dichloropropene
ug/L
ND
4000
4000
5330
5250
133
131
60-140
2
Trichloroethene
ug/L
ND
4000
4000
5740
5690
143
142
60-140
1 M1
Trichlorofluoromethane
ug/L
ND
4000
4000
5690
5560
142
139
60-140
2 M1
Vinyl chloride
ug/L
ND
4000
4000
6430
6100
161
152
60-140
5 M1
1,2-Dichloroethane-d4 (S)
%
101
101
70-130
4-Bromofluorobenzene (S)
%
99
102
70-130
Toluene-d8(S)
%
99
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /18/2022 11:39 AM without the written consent of Pace Analytical Services, LLC.
Page 17 of 30
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
QUALITY CONTROL DATA
Project: Trillium Links & Lake 11/10
Pace Project No.: 92636078
QC Batch: 737250 Analysis Method: SM 2540C-2015
QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92636078001, 92636078002, 92636078003
METHOD BLANK: 3836961 Matrix: Water
Associated Lab Samples: 92636078001, 92636078002, 92636078003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Dissolved Solids mg/L ND 25.0 11/15/22 17:46
LABORATORY CONTROL SAMPLE: 3836962
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Dissolved Solids mg/L 250 242 97 90-110
SAMPLE DUPLICATE: 3836963
92636075022 Dup
Parameter Units Result Result RPD Qualifiers
Total Dissolved Solids mg/L 19300 18800 3 1g
SAMPLE DUPLICATE: 3836964
92636049001 Dup
Parameter Units Result Result RPD Qualifiers
Total Dissolved Solids mg/L 163000 ug/L 162 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /18/2022 11:39 AM without the written consent of Pace Analytical Services, LLC. Page 18 of 30
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
QUALITY CONTROL DATA
Project: Trillium Links & Lake 11/10
Pace Project No.: 92636078
QC Batch: 736603 Analysis Method: SM 9222D-2015
QC Batch Method: SM 9222D-2015 Analysis Description: 9222D Fecal Coliform(MF) -AVL
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92636078001, 92636078002, 92636078003
METHOD BLANK: 3833580 Matrix: Water
Associated Lab Samples: 92636078001, 92636078002, 92636078003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms CFU/100 mL ND 1.0 11/11/22 15:04
SAMPLE DUPLICATE: 3833581
Parameter
Fecal Coliforms
92636023001 Dup
Units Result Result RPD Qualifiers
CFU/100 mL ND ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /18/2022 11:39 AM without the written consent of Pace Analytical Services, LLC.
Page 19 of 30
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
QUALITY CONTROL DATA
Project: Trillium Links & Lake 11/10
Pace Project No.: 92636078
QC Batch: 736435 Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92636078001, 92636078002, 92636078003
METHOD BLANK: 3832738
Matrix:
Water
Associated Lab Samples: 92636078001, 92636078002, 92636078003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Sulfate
mg/L
ND
1.0
11/12/2213:05
LABORATORY CONTROL SAMPLE:
3832739
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Sulfate
mg/L
50
47.5
95 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3832740 3832741
MS MSD
92635572001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L 802 50 50 850 834 97 64 90-110 2 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3832742 3832743
MS MSD
92636066001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L 1.6 50 50 51.4 51.5 100 100 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /18/2022 11:39 AM without the written consent of Pace Analytical Services, LLC.
Page 20 of 30
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
QUALITY CONTROL DATA
Project: Trillium Links & Lake 11/10
Pace Project No.: 92636078
QC Batch: 736820 Analysis Method: EPA 350.1 Rev 2.0 1993
QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92636078001, 92636078002, 92636078003
METHOD BLANK: 3834554
Matrix:
Water
Associated Lab Samples: 92636078001, 92636078002, 92636078003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Ammonia
mg/L
ND
0.10
11/14/22 14:11
LABORATORY CONTROL SAMPLE:
3834555
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Nitrogen, Ammonia
mg/L
5
5.0
100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3834556 3834557
MS MSD
92636078001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/L ND 5 5 5.1 5.0 101 101 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3834558 3834559
MS MSD
92636078002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/L ND 5 5 5.0 5.0 101 100 90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /18/2022 11:39 AM without the written consent of Pace Analytical Services, LLC.
Page 21 of 30
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
QUALITY CONTROL DATA
Project: Trillium Links & Lake 11/10
Pace Project No.: 92636078
QC Batch: 736393 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92636078001, 92636078002, 92636078003
METHOD BLANK: 3832648
Matrix:
Water
Associated Lab Samples: 92636078001, 92636078002, 92636078003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Nitrate
mg/L
ND
0.040
11/11/22 00:49
LABORATORY CONTROL SAMPLE:
3832649
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Nitrogen, Nitrate
mg/L
1.5
1.5
100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3832650 3832651
MS MSD
92635469011 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Nitrate mg/L 1.9 1.5 1.5 3.4 3.5 99 105 90-110 2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3832652 3832653
MS MSD
92635469007 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Nitrate mg/L 1.3 1.5 1.5 2.8 2.9 102 103 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /18/2022 11:39 AM without the written consent of Pace Analytical Services, LLC.
Page 22 of 30
leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
QUALITY CONTROL DATA
Project: Trillium Links & Lake 11/10
Pace Project No.: 92636078
QC Batch: 736800 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92636078001, 92636078002, 92636078003
METHOD BLANK: 3834485
Matrix:
Water
Associated Lab Samples: 92636078001, 92636078002, 92636078003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Phosphorus
mg/L
ND
0.050
11/14/2219:47
LABORATORY CONTROL SAMPLE:
3834486
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Phosphorus
mg/L
2.5
2.6
102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3834487 3834488
MS MSD
92636078002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/L ND 2.5 2.5 2.7 2.6 107 105 90-110 2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3834489 3834490
MS MSD
92636078003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/L 0.099 2.5 2.5 2.8 2.7 106 106 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /18/2022 11:39 AM without the written consent of Pace Analytical Services, LLC.
Page 23 of 30
leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
QUALITY CONTROL DATA
Project: Trillium Links & Lake 11/10
Pace Project No.: 92636078
QC Batch: 737203 Analysis Method: SM 4500-CI-E-2011
QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92636078001, 92636078002, 92636078003
METHOD BLANK: 3836640
Matrix:
Water
Associated Lab Samples: 92636078001, 92636078002, 92636078003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Chloride
mg/L
ND
1.0
11/15/2218:21
LABORATORY CONTROL SAMPLE:
3836641
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Chloride
mg/L
20
20.0
100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3836642 3836643
MS MSD
92635629001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chloride mg/L 8.4 10 10 18.4 18.6 100 102 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3836644 3836645
MS MSD
92635629002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chloride mg/L 41.5 10 10 51.1 51.0 96 95 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /18/2022 11:39 AM without the written consent of Pace Analytical Services, LLC.
Page 24 of 30
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
QUALITY CONTROL DATA
Project: Trillium Links & Lake 11/10
Pace Project No.: 92636078
QC Batch: 737146 Analysis Method: SM 531 OB-2014
QC Batch Method: SM 531 OB-2014 Analysis Description: 5310E TOC
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92636078001, 92636078002, 92636078003
METHOD BLANK: 3836271
Matrix:
Water
Associated Lab Samples: 92636078001, 92636078002, 92636078003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Organic Carbon
mg/L
ND
1.0
11/15/22 14:10
LABORATORY CONTROL SAMPLE:
3836272
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Total Organic Carbon
mg/L
25
23.3
93 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3836273 3836274
MS MSD
92636071013 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Total Organic Carbon mg/L ND 25 25 25.5 24.9 99 97 90-110 2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3836275 3836276
MS MSD
92634709005 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Total Organic Carbon mg/L 27700 25 25 28500 28900 3210 5160 90-110 2 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /18/2022 11:39 AM without the written consent of Pace Analytical Services, LLC.
Page 25 of 30
leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
QUALIFIERS
Project: Trillium Links & Lake 11/10
Pace Project No.: 92636078
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
1 g Constant weight could not be achieved for this sample after 4 drying cycles. The final weight change was 0.0065 grams.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /18/2022 11:39 AM without the written consent of Pace Analytical Services, LLC. Page 26 of 30
leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Trillium Links & Lake 11/10
92636078
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92636078001
MWAC
SM 6200E
736787
92636078002
MW-2C
SM 6200B
736787
92636078003
MW-3C
SM 6200B
736787
92636078001
MWAC
SM 2540C-2015
737250
92636078002
MW-2C
SM 2540C-2015
737250
92636078003
MW-3C
SM 2540C-2015
737250
92636078001
MWAC
SM 9222D-2015
736603
SM 9222D-2015
736604
92636078002
MW-2C
SM 9222D-2015
736603
SM 9222D-2015
736604
92636078003
MW-3C
SM 9222D-2015
736603
SM 9222D-2015
736604
92636078001
MWAC
EPA 300.0 Rev 2.1 1993
736435
92636078002
MW-2C
EPA 300.0 Rev 2.1 1993
736435
92636078003
MW-3C
EPA 300.0 Rev 2.1 1993
736435
92636078001
MWAC
EPA 350.1 Rev 2.01993
736820
92636078002
MW-2C
EPA 350.1 Rev 2.0 1993
736820
92636078003
MW-3C
EPA 350.1 Rev 2.0 1993
736820
92636078001
MWAC
EPA 353.2 Rev 2.0 1993
736393
92636078002
MW-2C
EPA 353.2 Rev 2.0 1993
736393
92636078003
MW-3C
EPA 353.2 Rev 2.0 1993
736393
92636078001
MWAC
EPA 365.1 Rev 2.0 1993
736800
EPA 365.1 Rev 2.0 1993
736994
92636078002
MW-2C
EPA 365.1 Rev 2.0 1993
736800
EPA 365.1 Rev 2.0 1993
736994
92636078003
MW-3C
EPA 365.1 Rev 2.0 1993
736800
EPA 365.1 Rev 2.0 1993
736994
92636078001
MWAC
SM 4500-CI-E-2011
737203
92636078002
MW-2C
SM 4500-CI-E-2011
737203
92636078003
MW-3C
SM 4500-CI-E-2011
737203
92636078001
MWAC
SM 5310E-2014
737146
92636078002
MW-2C
SM 5310B-2014
737146
92636078003
MW-3C
SM 5310B-2014
737146
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /18/2022 11:39 AM without the written consent of Pace Analytical Services, LLC. Page 27 of 30
DC#_Title: ENV-FRM-HUN1-0083 01_Sample Condition Upon Receipt
ilaCC,
Effective Date: 05/12/2022
Laboratory recei ing samples:
Asheville Eden❑ Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑ Atlanta❑ KernersvilleF�
ConditionSample Client fame: 92636D?3
., Project ft:
4t_Gt r- I
Courier: ❑Fed Ex. ❑UPS ❑LISPS Client
❑ Commercial []Pace❑111111111
Other: ll
92635078
Custody Seal Present? ❑Yes o Seals Intact? ❑Yes
Date/Initials Person Examining Contents: ff ! D
Packing Material: Bubble Wrap ❑Bubble Bags ❑None ❑ Other Biological Tissue Fr en?
Thermomet
❑Yes ❑No [2N/A
IR Gun ID: Type of Ice: et ❑Blue ❑None
S Correction Factor: �1
Cooler Temp: ? Add/Subtract(°C)
Cooler Temp Corrected (°C 3
USDA Regulated Soil ( N/A, water sample)
Did samples originate in a quarantine zone Mthin the United States: CA, NY, or SC
1rhor4 mnn07 MYF-K €—INn
Temp should be above freezing to 6T
❑Samples out of temp criteria. Samples on ice, cooling process
has begun
0d samples originate From a foreign source (internationally,
includine Hawaii and Puerto Ricol? rlYes MNO
Comments/Discrepancy:
Chain of Custody Present?
J21rLs
[]No
❑N/A
1.
Samples Arrived within Hold Time?
2fes
❑No
[:]N/A
2-
Short Hold Time Analysis (02 hr.)?
2<
❑No
[]N/A
3.
Rush Turn Around Time Requested?
❑Yes
DICO
❑N/A
4.
Sufficient Volume?
CJVrS
i]NO
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
Yes
es
❑No
❑No
❑N/A
❑NIA
6.
Containers Intact?
es
[—]No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
❑No
N/A
8.
Sample Labels Match COC?s
-Includes Date/Time/ID/Analysis Matrix:
" !
❑No
❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
❑Yes
❑No
N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
❑Na
❑No
/A
A
11.
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Lot ID of split containers:
Date/Time:
Date:
Date:
Field Data Required? LlYes LJNo
Page 28 of 30
Qualtrax ID: 69614 Page 1 of 2
/-9
I ace
DC# Title: ENV-FRM-HUN1-0083 v01 Sample Condition Upon Receipt
Effective Date: 05112/2022
*Check mark top half of box if pH and/or dechlorination is verified and
within the acceptance range for preservation samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottles
***Check all unpreserved Nitrates for chlorine
Project # WO# : 92636478
PM: AMB Due Dale: 11/17/22
CLIENT: 93-ALTAMONT
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pH Adjustment log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot H
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DENR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 29 of 30
Qualtrax ID: 69614 Page 2 of 2
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TOC by 5310
Chloride, Sulfate
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Page 30 of 30