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Home My WebLink About820466_Compliance Report_202211074 ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab ■ 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax info@environmentalchemists.com Smithfield Hog Productions - Warsaw Date of Report: Oct 26, 2022 Post Office Box 856 Customer PO #: Warsaw NC 28398 Customer ID: 08110011 Attention: Amy Elmore Report #: 2022-18161 Project ID: Wastewater/Digester Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-44546 Site: Effluent - Goodson 9/14/2022 9:18 AM Water Derek Brown Test Method Results Date Analyzed Sulfur EPA 200.7 51.2 mg/L 10/25/2022 Copper EPA 200.7, Rev 4.4,1994 1.28 mg/L 10/13/2022 Zinc EPA 200.7, Rev 4.4,1994 1.07 mg/L 10/13/2022 Ammonia Nitrogen EPA 350.1, Rev. 2.0, 1993 650 mg/L 09/19/2022 Total Phosphorus SM 4500 P (F-H)-2011 85.1 mg/L 09/21/2022 Fecal Coliform SM 9222 D-2015 MF 140000 Colon ies/100mL 09/14/2022 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0,1993 746 mg/L 09/21/2022 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0,1993 0.97 mg/L 09/16/2022 Total Nitrogen Total Nitrogen 747 mg/L 09/23/2022 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-44547 Site: Influent - Goodson 9/14/2022 Water Derek Brown Test Method Results Date Analyzed Sulfur EPA 200.7 85.8 mg/L 10/25/2022 Copper EPA 200.7, Rev 4.4,1994 4.92 mg/L 10/13/2022 Zinc EPA 200.7, Rev 4.4,1994 4.76 mg/L 10/13/2022 Ammonia Nitrogen EPA 350.1, Rev. 2.0,1993 680 mg/L 09/19/2022 Total Phosphorus SM 4500 P (F-H)-2011 127 mg/L 09/21/2022 Fecal Coliform SM 9222 D-2015 MF >60000 Colonies/100ml- 09/14/2022 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0,1993 1070 mg/L 09/21/2022 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0,1993 1.19 mg/L 09/16/2022 Total Nitrogen Total Nitrogen 1070 mg/L 09/23/2022 Comment: �Al Reviewed by: 7T Report #:: 2022-18161 Page 1 of 1 Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmington, NC 28405 910.392.0223 Sample Receipt Checklist Client: t C�4M Date: % Li- 2Z ReportNumber: Receipt of sample: ECHEM PickupJ& Client Delivery ❑ UPS ❑ FeclEx ❑ Other ❑ ❑ YES ID NO N/A 11. Were custody seals present on the cooler? ❑ YES I0 NO N/A liz If custody seals were present, were they intact/unbroken? Original temperature upon receipt , °C Corrected temperature upon receipt °C How temperature taken: ❑ Temperature Blank Against Bottles IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0 YES ❑ NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified? YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed? YES ❑ NO 5. Were sample ID's listed on the COC? YES ❑ NO 6. Were samples ID's listed on sample containers? YES ❑ NO 7. Were collection date and time listed on the COC? YES ❑ NO 8. Were tests to be performed listed on the COC? YES ❑ NO 9. Did samples arrive in proper containers for each test? YES ❑ NO 10. Did samples arrive in good condition for each test? YES ❑ NO 11. Was adequate sample volume availableT YES ❑ NO 12. Were samples received within proper holding time for requested tests? YES ❑ NO 13. Were acid preserved samples received at a pH of <2? ❑ YES ❑ NO 14. Were cyanide samples received at a pH >12? ❑ YES ❑ NO 15. Were sulfide samples received at a pH >9? YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ** ❑ YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? ❑ YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H2SO4 HNO3 HCI NaOH Time of preservation: If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. Who was notified, date and time: Volatiles Sample(s) were received with headspace COMMENTS: DOC. QA.002 Rev 1 Analytical & Consulting Chemists Client: Smithfield ADDRESS: Sam Production Sample Identification Influent Efflluent Date I Time ENVIRONMENTAL CHEMISTS INC 6602WindmillWayWilmington,NC28405 OFFICE: 910-392-0223 FAX 910-392-4424 NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY PROJECT NAME: Wastewater/Digester REPORT NO: cell — CONTACT NAME: PO NO: REPORT TO: Amy Elmore/Warsaw PHONE/FAX: COPY TO: email: W d a `E F�, SAMPLE w c c o` c7 TYPE: t o o a`o I = Influent, c J o f " E E o W m? 3 Z = Effluent, PRESERVATION W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: ANALYSIS REQUESTED ion Temp z Z=_= u y " = z o w 0 0 C P 144 b- i to X Fecal JTN, TP, NH3 G G N ��J C P L�'� X G X G C G P Copper, Sulfur, Zinc G G C P G G C P c� � X � Fecal TN, TP, NH3 G G} C P L X .L 4 X G c G P Copper, Sulfur, Zinc G C G P G G C P G G C P G G Transfer Relinquished By: Date/Time _ Received Bv: 1. 2. Temperature when Delivered By: ` Comments: Date/Time `C: Accepted: ejected: Resample Requested: Received By: ►� �-Yh 1t Date: Time: iS n o TIIDK ADnilKrn.