WQ0033677_Monitoring - 11-2022_20230104

FORM: NDMR 08-11 NON -DISCHARGE MONITORING REPORT (NDMR) Page l of
Permit No.: W00033677
Facility Name: CASE FARMS HATCHERY
County: Burke
Month: November
Year: 2022
PPI: 001
Flow Measuring Point: E influent ❑ Effluent ❑ No Flow generated
Parameter Monitoring Point: ❑ influent ❑✓ Effluent ❑ Groundwater Lowering ❑✓ Surface water
Parameter Code - 1.
0050
Ihs!¢ q!niei
00400
�..s .! M'
00310
a 00610
ulilEEil91l
00530
613
Is. Int,
00940
OOb9
d lllu - '
70300
h.0062
B:E311xdwtx,se,f. .h.
00625
00600
ctlahxi'6
00665
i ,r33
p
E
O�
O
m
E r
Ci
O y
O
E[ �-
=
l I
X
f
p
m
11 C
I I Q I
cA
~ N N
p
�a
i,;"EAU
U
IU
m?v
W
~ p O
r,
,:
r
� Z
i
U)
~ d
i@
4 Ap
24-hr
hrs
PD
su
..`
`
mg/L
g L
mg/L
%1y00 mL�
mglL
NS2
mg/L
rglL, r
mg/L
!?1g/
mg/L
x
1
5:00
10ill
law
2
: �?ixMI ll{i
1�..A I ae,
, ' �
3
5:00
10.5;7200
L
'" I
4
5:00 .
11
_7 00
7.3
t-
r
._
I.
�.
MIN
7
5:00
10.57200
6.1
-.
l _ x
�, _ I�
Enum- a
8
5:00
10
?00:.
r
to
10
4:30
11.5§7y�200rt
z.y
�x .
�)
11'
5:00
11.5
142�-
0011111
_
_"
'
e
127200NEW,
13
I,MIolE...
„
y.
14
5:00
10
7.2
E t p
C­N;�?.
ON"
�p
11"
15
5:00
10.5
'�7200
s
_
='
-zowl
-
16
6: 00
7.5
sr�v7200
„ 9°"
'` I�1�,
i° f a
i ,
7Qrz3,
l
ryy
r„ti8�int
17
5:00
10
!�"200 - :.
k lw
I iws
"MINN
,
18
5:00
8200.
a
.r.
o
;r
BMW
191
1f%7A200,
elm
,�3
sus
20
14:00
2
7 200
it °
.• E.
•
IY fp'
21
5:00
10
>._ _ _'2Q9" .
9.1
22
5:00
10.5
7200
_
pMEAN
23
6:30
5
IR17l�,yy.200li
_#"
rr
a i
24
5:00
8
1
'.
26
16:00
2
7 000
_'
ram�•' _ �
� E
Nl ,
a
kg.
27
16:00
2
pp
I�H' 6. 000 IIE
17 ,.,�,,,;
j�; fig
�' V+II^Y3�r'.� .!
}j
I:�PI`P 4
M..4d8ii1�dl., ., rz
� a ....;I
l _
�p�
I!III!!
28
5:00
10"�7rQ0;0}"
6.85
_
8713r#L8
253�12750
.":
62.9
91;$- '.
700
89
• , 9Q,�8
9.46
l
29
5:00
1 10.5
7,000
NOW
ry.
A
, . .;
ulna
30
1
a,,,}}:. +
l_ap�������9 1.
- E ��
i``
31
99,,�y��7``'pII000
k1N 4B . I
,ik9 _
11 IBIRH
„ °`
a
Average
871.00
43 28
253.00
2�7�5'0 00 '
62.90
9j 60
700.00
.31 ,i3
89.00
9OEW
9.46
Daily Maximum
7200y
9.10
871:00
43T28
253.00275
0
62.90
9 8 0.
700.00
118
89.00
` 90. 8
9.46
SIWAIJIM
Daily Mlnimumlfl�Lrgy
's OOp
6.10
v `.
j[ga.
871.00
��I43,;"�S
253.00
62.90
I ."�18OQ
700.00
89.00
F 9,Q�1,8
9:46
,.
Sampling Type
�1`, ar �
31i1'
i k a
10 U-91
MINION
�?" ,,
VAN_"''
Monthly Limit
�
8000�u-
6
Daily Limit:
a __ ..1
ffil._ _
g
Sample Frequency
.... I+I! A �€
r1.ya, "R . Y.
F�
�9j��j��l!� tl'''� d
S, 6�13Z?. I:iP:ISf _
13 EE�Ih hi
,�5...'a
���9y� ,,,y
9 'n46d?idf ��"8+u.0
4`L,j yi
fi!�` 9'aPW. ,.�.. °�
'v" I°g1.::
, �p
ig� Eyre i+a �l
'e<i5iy d'

Or
FORM: NDMR 08-11
NON -DISCHARGE MONITORING REPORT (NDMR)
Page,! 2, of 6.
Sampling Person(s)
Name: James Edwards
Name: Cindy McGinnis
Name: Water Tech Labs Inc
Name:
Certified Laboratories
Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? ❑� Compliant ❑ Non -Compliant
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective
action(s) taken. Attach additional sheets if necessary.
Operator in Responsible Charge (ORC) Certification
Permittee Certification
ORC:
Cindy McGinnis
Permittee: Case Farms Hatchery
Certification No.: 992943
Signing Official: Cindy McGinnis
Grade:
SI Phone Number: 808-438-6900
Signing Official's Title: Hatchery Supervisor
Has the ORC changed since the previous NDMR? ❑ Yes 2] No
Phone Number: 828-438-6900 Permit Expiration: 12/31/2021
C-oi
911 Y"ta__ -;L
( 4;V
UBy
Date
I - dSignature Signature Date
this signature, I certify_ that this report is accurrate and complete to the best of my knowledge.
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information
submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for
gathering the information; the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations. —
Mail Original and Two Copies to:.
Division of Water Quality
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617

FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page i of

`FORM: NDAR-1 08-11
NON -DISCHARGE APPLICATION REPORT (NDAR-1)
Page 2 of
Did the application rates exceed the limits in Attachment B of your permit?
Were adequate measures taken to prevent effluent ponding in or runoff from the sites?
Was a suitable vegetative cover maintained on all sites as specified in your permit?
Were all setbacks listed in your permit maintained for every application to each permitted site?
Were all freeboards maintained in accordance with the specified freeboard heights in your permit?
❑� Compliant ❑ Non -Compliant
❑� Compliant ❑ Non -Compliant
[A Compliant ❑ Non -Compliant
E Compliant ❑ Non -Compliant
❑� Compliant ❑ Non -Compliant
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective
action(s) taken. Attach additional sheets if necessary.
Operator in Responsible Charge (ORC) Certification
Permittee Certification
ORC: Cindy McGinnis
Permittee:
Case Farms Hatchery
Certification No.: 992943
Signing Official: Cindy McGinnis
Grade: SI Phone Number: 828-438-6900
Signing Official's Title: Hatchey Supervisor
Has the ORC changed since the previous NDAR-1? ❑ yes F/I No
Phone Number: 828-438-6900 Permit Exp.: 12/31/21
®
Signature Date
Signature Date
By this signature, I certify that this report is accurrate and complete to the best of my knowledge.
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure:that all qualified personnel properly gathered and evaluated the information submitted.Based on my
inquiry of the person or persons who manage•the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
Mail Original and Two Copies to:
Division of Water Quality
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617

MOTErRiTECH LRNZ.inc.
POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR.
GRANITE FALLS, NORTH CAROLINA 28630
(828)-396 4444
SAMPLE: Case Farms -Hatchery COLLECTION DATE, 11/28/2022
PERMIT #: COLLECTION TIME: 11:30
ADDRESS: Case Farms Hatchery RECEIVED DATE: 11/28/2022
RECEIVED TIME: 1235
REPORTED: 12/9/2022
NAi
ANALYSIS
EFFLUENT
UNITS
BOD
871
mg/L
TSS
253
mg/L
NH3
43.28
mg/L
Fecal Coliform
2750
/100mL
Conductivity
918
umhos/cr
NO3-N
1.18
rng/L
TKN
89.00
rng/L
T. Nitrogen
91).18
mg/L
T. Phosphorus
9.46
mg/L
Chloride
pace.
TDS
pace
DATE
ANALYST
11 /30/22
jdg
11 /29122
jrg
1211 /22
jrg
11 /28/22
Th
12/2/22
jsd
11/30122'
jsg
1211 /22
jdg
1211 /22
jdg
12/2/22
jdg
LOG ID: :2211-407 REPORTED BY: NC CERTIFIED LAB 4 50
Tony Gragg, Lab Supervisor

fiTE, 79cm L NS.Inc.
POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR.
GRANITE FALLS, NORTH CAROLINA 28630
[phone]
SAMPLE: Case Farms-Hatchery-MW#3 COLLECTION DATE. 11/28/2022
PERMIT #: COLLECTION TIME: 10:00
ADDRESS: Case Farms Hatchery RECEIVED DATE: 11/28/2022
RECEIVED TIME: 12:35
REPORTED: 12/9/2022
ANALYSIS
ANALYSIS
RESULTS
UNITS
DATE
ANALYST
NH3
<1.0
mg/L
12/1/22
jrg
Fecal Coliform
16
/100mL
11/28/22
Th
Metals
pace
NO3-N
2.70
mg/L
11/30/22
jsg
TKN
<1.0
mg/L
12/1/22
jdg
T. Nitrogen
2.70
mg/L
1211/22
jdg
T. Phosphorus
<0.16
mg/L
12/2/22
jdg
Chloride
pace
TDS
pace
LOG ID: 2211-408 REPORTED BY: NC CERTIFIED LAB # 50
ff� *
Tony Gragg, Lab Supervisor

OTE�'R4TVCH L1195-mc.
POST OFFICE BOX 1056 #5 PINEWOOD PLAZA DR.
GRANITE FALLS, NORTH CAROLINA 28630
[phone]
SAMPLE: Case Farms-Hatchery-MW#4 COLLECTION DATE:
11/28/2022
PERMIT #: COLLECTION TIME.
11:00
ADDRESS: Case Farms Hatchery RECEIVED DATE.,
11/28/2022
RECEIVED TIME:
12:35
REPORTED:
12/9/2022
ANALYSIS
RESULTS
UNITS
DATE
ANALYST
NH3
<1.0
mg/L
12/1/22
jrg
Fecal Coliform
1
/100ml-
11/28/22
Th
Metals
pace
NO3-N
4.38
mg/L
11/30/22
jsg
TKN
<1.0
mg/L
12/1122
jdg
T. Nitrogen
.4.38
mg/L
12/1/22
jdg
T. Phosphorus
<0.16
mg/L
12/2/22
jdg
Chloride
pace
TDS
pace
LOG ID: .2211-409 REPORTED BY: NC CERTIFIED LAB 9 50
fblliE
Tony Gragg, Lab Supervisor

MATTOwRiTECH LARS.,nc.
POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR.
GRANITE FALLS, NORTH CAROLINA 28630
(828),3964444
SAMPLE., Case Farms-Hatchery-MW#5 COLLECTION DATE: 11/28/2022
PERMIT #: COLLECTION TIME: 10:30
ADDRESS: Case Farms Hatchery RECEIVED DATE.- 11/28/2022
RECEIVED TIME: 12:35
REPORTED: 12/9/2022
ANAL;YSI S'
.
ANALYSIS
RESULTS
UNITS
DATE
ANALYST
NH3
<1.0
mg/L
12/1/22
jrg
Fecal Coliform
6
/100ml-
11/28/22
Th
Metals
pace
NO3-N
2.78
mg/L
11/30/22
jsg
TKN
<1.0
mg/L
12/1122
jdg
T. Nitrogen
2.78
mg/L
1211/22
jdg
T. Phosphorus
<0,16
mg/L
12/2/22
jdg
Chloride
pace
TDS
pace
LOG ID: 2211-41.0 REPORTED BY: NC CEERTIFIED LAB # 50
fall*
Tony Gragg, Lab Supervisor

aceAnalyical
www,pacela6a,cam
ANALYTICAL RESULTS
Project: Case Farms MWs
Pace Project No.: 92638574
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
[phone]
Sample: Effluent Lab ID: 92638574004 Collected: 11/28/22 11:30 Received: 11/29/22 08:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
2540C Total Dissolved Solids Analytical Method: SM 2540C-2015
Pace Analytical Services -Asheville
Total Dissolved Solids 700 mg1L 30.9 1 1113012216:05
4500 Chloride Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride 62.9 mg1L 3.0 3 12/02/22 20:09 16887-00-6
Date: 1210812022 01:02 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 36

Contact: Cathy Gragg Report Date: 12/1/2022
Client: Water Tech Labs, Inc
5 Pinewood Plaza Drive
Granite Falls, NC 28-630 Date Sample Revd: 11/29/2022
MeritechWork 'Order # .1-1.2-92213 5aftipl e! Case Farms - MW #3 Grab 11/28/22
Parameters Result Analysis ®at
e -Rej)gr-fingjA_qjft Method
-MBAS (as LAS 340) <0.10 mg/L 11/29/22 a A0 mg/L SM5540 C
Keritech Work Order# 11292214 Sample: Case Farms w MW #4 Grab
Parameter
Aegalt Analysis Date Reag—rtLng �Uft Mothod
MBAS (A51AS 3.40) �0.10 mg/L 11/29/22 040 MgA 595.540 C
MeritechWork baler # 11292215 Sample: Case Farms - MW #5 Grab. 11/28/22
Parameters l8esaxit Analysis tiate Renbrtink.Limit Method
M-BAS (as LAS 34-0) 56A0 mg/L 11/29/22 0.10 mg/L SM 5540 C
1h&eby certify that I have reviewed and approve these data. --� �-10- WCA D:U
LaboratoryRepresentative
647. Tainco Road, Reidsville, North Carolina 27320
t,pJ.(336)3424748 fm(336)842-1922

-11003
Pace Analytical Services, LLC
J80
eAnalX cal 1 South Park Drive
Kernmersvllle, NC 27284
www.p®08103,e0in [phone]
ANALYTICAL RESULTS
Project: Case Farms MWs
Pace Project No.: 92638574
Sample: MW3
Parameters
Lab ID: 92638574001 Collected: 11/28/2210:00
Results Units Report Limit DF
Received: 11/29/22 05:40 Matrix: Water
Prepared Analyzed CAS No.
Qual
200.8 MET ICPMS
Analytical Method: EPA200.8 Rev 5A
Preparation Method: EPA200.8 Rev 5.4
Pace Analytical
Services - Asheville
Arsenic
ND
mg/L
0.0010
1
1210PJ22 15:38 12/05/22 21:07 7440-38-2
Barium
0.079
mg/L
0,0010
1
12102/2215:38 12/05/22 21:07 7440-39-3
Copper
0.0033
mg/L
0.0020
1
12/02122 15:38 12/05/22 21:07 7440-50-8
Iron
1.2
mg/L
0.060
1
12/02/22 15:38 12/05/22 21,07 7439-.89-6
Manganese
0.062
mg/L
0.0020
1
12/02/22 15:38 12/05/22 21:07 7439-96-5
Potassium
2.6
mg/L
0,10
1
12/02/22 15:38 12105/22 21:07 7440-09-7
Sodium
8.7
mg/L
1.2
5
12/02/22 15:38 12107/22 08:12 7440-23-5
Zinc
0.016
mg/L
0.010
1
12/02/22 15:38 12105/22 21:07 7440-66-6
8260D MSV
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
121,01/2214:32 67-64-1
Benzene
ND
ug/L
5.0
1
12101122 14:32 71-43-2
Bromobenzene
ND
ug1L
5.0
1
1210112214:32 108-86-1
Bromochloromethane
ND
ug1L
5.0
1
1210112214:32 74-97-5
IK
Bromodichloromethane
ND
ug/L
5.0
1
12101/2214:32 75-27-4
Bromoform
ND
ug/L
5.0
1
1210112214:32 75-25-2
Bromomethane
ND
ug/L
10.0
1
12101/2214:32 74-83-9
2-Butanone (MEK)
ND
ug/L
10.0
1
12101/22 14:32 78-93-3
IK
tert-Butyl Alcohol
ND
ug/L
100
1
12101/2214:32 75-65-0
IL,L2,v2
n-Butylbenzene
ND
ug/L
5.0
1
12101/2214:32 104-51-8
sec-Butylbenzene
ND
ug/L
5.0
1
1270112214:32 135-98-8
tort-Butylbenzene
ND
ug1L
5.0
1
12/01/22 14:32 96- "
Carbon tetrachloride
ND
ug/L
5.0
1
12/01/22 14:32 56-23�5
Chlorobenzene
ND
uglL
5.0
1
12101/2214:32 108-90-7
Chloroethane
ND
ug/L
10.0
1
12101/2214:32 75-004
Chloroform
ND
ug/L
5.0
1
12/0112214:32 67-66-3
Chloromethane
ND
ug/L
5.0
1
1210112214:32 74-87-3
2rChlorotoluene
ND
ug/L
5.0
1
1210112214:32 95-49-8
4-Chlorotoluene
ND
ug1L
5.0
1
1210112214:32 106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
12101/2214:32 96712=8
Dibromochloromethane
ND
ug/L
5.0
1
12101/2214:32 124-48-1
1,2-Dibromoethane(EDB)
ND
ug/L
5.0
1
1210112214:32 106-93-4
Dibromomethane
ND
ug/L
5.0
1
12/01/22 14:32 74-95 3
IK
1,2-Dichlorobenzene
ND
ug/L
5.0
1
12101/2214:32 95-50-1
1,3-Dichlorobenzene
ND
uglL
5.0
1
1210112214:32 541-73-1
1,4-Dichlorobenzene
ND
ug/L.
6.0
A
12/0 1122 14:32 10646-7
Dichlorodifluoromethane
ND
ug/L
5.0
1
12/0112214:32 75-71-8
M1
1,1-Dichloroethane
ND
ug/L
5.0
1
12/0112214:32 75-34-3
1,2-Dichloroethane
ND
ug/L
5.0
1
1210112214:32 107-06-2
1,2-Dichloroethene (Total)
ND
uglL
5.0
1
12/0112214:32 540-59-0
1,1-Dichloroethene
ND
ug/L
5.0
1
12/0112214:32 75-35-4
cis-1,2-Dichloroethene
ND
uglL
5.0
1
12/01/2214:32 156-59-2
trans-1,2-Dichloroethene
ND
ug/L
5.0
1
1210112214:32 156-60-5
1,2-Dichloropropane
ND
uglL
5.0
1
12101/2214:32 78-87-5
1,3-Dichloropropane
ND
ug/L
6.0
1
12/01/22 14:32 142-21-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 12/08/2022 01:02 PM without the written consent of Pace Analytical Services, LLC, Page 4 of 36

aceAnalyfical"
www,pecelabs.cam
ANALYTICAL RESULTS
Paco Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
[phone]
Project: Case Farms MWs
Pace Project No.: 92638574
Sample: MW3 Lab ID: 92638574001 Collected: 11/28/22 10:00 Received: 11/29/22 08:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
2,2-Dichloropropane
ND
ug/L
5.0
1
1210112214:32 594-20-7
1,1-Dichloropropene
ND
ug/L
5.0
1
1210112214:32 563-58-6
cis-1,3-Dichloropropene
ND
ug/L
5.0
1
1210112214:32 10001-01-5
trans-1,3-Dichloropropene
ND
ug/L
5.0
1
12/01/2214:32 10061-02-6
Diisopropyl ether
ND
ug/L
5.0
1
12/01122 14:32 108-20-3
Ethylbenzene.
ND
ug/L
5.0
1
1210112214:32 100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
1210112214:32 87-68-3
2-Hexanone
ND
ug/L
10.0
1
12101/2214:32 591-78-6
Isopropylbenzene (Cumene)
ND
ug/L
6.0
1
1210112214:32 98-82-8
p-Isopropyltoluene
ND
ug/L
5.0
1
12/01/2214:32 99-87-6
Methylene Chloride
ND
ug/L
5:0
1
12/01/22 14:32 75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
10.0
1
12/01/22 14:32 108-10-1
Methyl-tert-butyl ether
ND
ug/L
5.0
1
12/01/22 14:32 1634-04-4
Naphthalene.
ND
ug/L
5.0
1
12101/2214:32 91-20-3
n-Propylbenzene
ND
ug/L
5.0
1
12101/2214:32 103-66-1
Styrene
ND
uglL
5.0
1
12/0112214:32 100-42-5
1,11,12-Tetrachloroethane
ND
ug/L
5.0
1
12/011221.4:32 630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
5.0
1
1210112214:32 79-34-5
Tetrachloroethene
ND
ug/L
5.0
1
1210112214:32 127-18-4
Toluene
ND
ug/L
6.0
1
1210112214:32 108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
6.0
1
1210112214:32 87-61-6
1,2,4-Trichlorobenzene
ND
uglL
6.0
1.
12/0112214:32 120-82-1
1,.1;1-Trichlorcethane,
NO
ug/L
5.0
1
1210112214:32 71-55-6
1,1,2-Trichloroethane
ND
ug/L
5.0
1
12/0112214:32 79-00-5
Trichloroethene
ND
ug/L
5.0
1
12/0112214:32 79-01-6
Trichlorofluoromethane
ND
uglL
10.0
1
1210l/2214:32 75-69-4
1,2;3-Trichloropropane
ND
ug1L
5.0
1
12JO112214:32. 96-18-4 tK
1,2,4-Trimethylbenzene
ND
ug/L
5.0
1
1210112214:32 95-63-6
1,3,5-Tr1methylbenzene
ND
uglL
5.0
1
12101/2214:32 108-67-8
Vinyl acetate
ND
ug/L
10.0
1
1210112214:32 10"5-4 IK
Vinyl chloride
ND
ug/L
5.0
1
1210112214:32 75-01-4
m&p-Xylene
ND
ug/L
10.0
1
12101/2214:32 179601-23-1
o-Xylene
ND
ug/L
5.0
1
12/01/2214:32 95-47-6
Surrogates
4-Bromoflucrobenzene (S)
100
%
70-130
1
1.2101/2214:32 460-00-4
1,2-pichloroethane-d4 (S)
99
°1°
70-130
1
12/01/2214:32 17060-07-0
Toluene-cl8 (S)
1.02
%
70-130
1
12/01/22 14:32 2037-26-5
2540C Total Dissolved Solids
Analytical Method: SM 2640C-2015
Pace Analytical
Services -Asheville
Total Dissolved Solids
108
mg/L
25.0
1
11/30122 16:04
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical
Services -Asheville
Chloride 14.5 mg1L 1.0 1 12/0212219:14 16887-00-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 12/08/2022 01:02 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 36

aceAnalytfcal
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ANALYTICAL RESULTS
Project: Case Farms MWs
Pace Project No.: 92636574
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
[phone]
Sample: MW3 Lab iD: 92638574001 Collected: 11/28/22 10.00 Received:- 11/29/22 08:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
531013 TOC Analytical Method: SM 531 OB-2014
Pace Analytical Services - Asheville
Total Organic Carbon ND mg1L - 1.0 1 12101122 00:10 7440-44-0
Date: 1210812022 01:02 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 6 of 36

i
Pace Analytical Services, LLC
1377
ern
ace Analytical KamSouth Park Drive
ersvllle, NC 27284
www.pecelebs.com [phone]
ANALYTICAL RESULTS
Project: Case Farms MWs
Pace Project No.: 92638574
Sample: MW4
Parameters
Lab ID: 92638574002 Collected: 11/28122 11:00
Results Units Report Limit DF
Received: 11/29122 08:40 Matrix: Water
Prepared Analyzed CAS No.
Qua[
200.8 MET ICPMS
Analytical Method: EPA 200.8 Rev 5.4
Preparation
Method: EPA 200.8 Rev 5.4
Pace Analytical Services - Asheville
Arsenic
0.0014.
mg1L
0.0010
1
1210212215:38 12/05/22 21:47 7440-38-2
Barium
0.61
mg1L
0.0050
5
1210212215:38 12/07/22 08:23 7440-39-3
Copper
0.0096
mg/L
0,0020
1
12/02/22 15:38 12105/22 21:47 7440-50-8
iron
7.3
mg/L
0.26
5
12/02/22 15:38 12/07/22 08:23 7439-89-6
Manganese
0.47
mg1L
0.010
5
12/02/2215:38 12/07/22 08:23 7439-96-5
Potassium
4.8
mg/L
0.10
1
12/02/22 15:38 12/05/22 21:47 7440-09-7
Sodium
9.5
mg/L
1.2
5
12/02/22 15:38 12/07/22 08:23 7440-23-5
Zinc
0.028
mglL
0.010
1
12102/22 16:38 12/05/22 21:47 744.0-66-6
8260D MSV
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
36.0
ug/L
25.0
1
12101/2214:49 67-64-1
Benzene
ND
ug/L
5.0
1
12/01/2214:49 71-43-2
Bromobenzene
ND
ug/L
5.0
1
12/01/2214:49 108-86-1
Bromochloromethane
ND
ug/L
5.0
1
12/01/2214:49 74-97-5
IK
Bromodichloromethane
ND
ug/L
5.0
1
12/01/2214:49 75-27-4
Bromoform
ND
ug/L
5.0
1
12/01/2214:49 75-26-2
Bromomethane
ND
ug/L
10.0
1
12/01/2214:49 74-83-9
2-Butanone (MEK)
ND
ug/L
10.0
1
12101/2214:49 78-93-3
IK
tertButylAlcohol
ND
ug/L
1.00
1
12101/2214:49 75-65-0
IL,L2,v2
n-Butylbenzene
ND
ug/L
5.0
1
1210112214:49 104-51-8
seo-8utylbenzene
ND
ug/L
5.0
1
12/0112214:49 135-98-8
tort-Butylbenzene
ND
ug/L
6.0
1
1.210112214:49 98-06-6
Carbon tetrachloride
ND
ug/L
5.0
1
12/0112214:49 56-23-5
Chlorobenzene
ND
ug/L
5.0
1
1210112214:40 108-90-7
Chloroethane
ND
ug/L
10.0
1
1210112214:49 75-00-3
Chloroform
ND
ug/L
5.0
1
1:2/0112214:49 67-66-3
Chloromethane
ND
ug/L
5.0
1
12101/2214:49 74-87-3
2-Chlorotoluene
ND
ug/L
5.0
1
12/01/2214,49 95-49-8
4-Chlorotoluene
ND
ug/L
6.0
1
12/01/2214:49 105-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
12/01/2214:49 96-12-8
Dibromochloromethene
ND
ug/L
6.0 i
1
12/0.1/22 14:40 124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
6.0
1
12/01122 14:49 106-93-4
Dibromomethane
ND
ug/L
6.0
1
12/0112214:49 74-95-3
IK
1,2-Dichlorobenzene
ND
ug/L
5.0
1
1210112214:49 95-50-1
1,3-Dichlorobenzene
ND
ug/L
5.0
1
1210112214:49 541-73-1
1,4-Dichlorobenzene
ND
ug/L
5.0
1
12101/2214:49 106-46-7
Dichlorodifluoromethane
ND
ug/L
6.0:
1
12/01/2214:49 75-71-8
1,1-Dichloroethane
ND
ug/L
6.0'
1
1210112214-49 75-34-3
1,2-Dichloroethane
ND
ug/L
6.0
1
1210112214:49 107-06-2
1,2-Dichloroethene (Total)
ND
ug/L
6.0.
1
12101/22 14:49 540-59-0
1,1-Dichloroethene
ND
ug/L
5.0
1
12101/2214:49 75-35-4
cis-1,2-Dichloroethene
ND
ug/L
5.0
1
12101/2214:49 156-59-2
trans-1,2-Dichloroethene
ND
ug/L
5.0
1
12/0112214:49 156-60-5
1,2-Dichloropropane
ND
ug/L
5.0
1
12101/2214:49 78-87-5
1,3-Dichloropropane
ND _
ug/L
5.01
1
1210112214:49 142-28-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/08/2022 01:02 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 36

aceAnaly�ical
www.pacolabs.com
Project: Case Farms MWs
Pace Project No.: 92638574
i
I
ANALYTICAL RESULTS
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
[phone]
Sample: MW4
Lab ID: 92638574002 Collected:
11/28/22 11:00
Received: 11/29/22 08:40 Matrix: Water
Parameters
Results
Units Report Limit
❑F
Prepared Analyzed CAS No. Qual
8260D MSV
Analytical Method: EPA 8260D
i
Pace Analytical
Services - Charlotte
j
2,2-Dichloropropane
NO
ug/L
5.0
1
12101/2214:49 594-20-7
1,1-Dichloropropene
NO
ug/L
6.0
1
12101/2214:49 563-58-6
cis-1,3-Dichloropropene.
ND
ug/L
5.0
1
1210112214:49 10061-01-5
trans-11,3-Dichloropropene
NO
ug/L
5.0
1
12/0112214:49 10061-02-6
Diisopropyl ether
NO
ug1L
5.0
1
1210112214:49 108-20-3
Ethylbenzene
NO
uglL
5.0
1
1210112214:49 100-41-4
Hexachloro-1,3-butadiene
NO
ug/L
5.0
1
12/01'12214:49 87-68-3
2-Hexanone
NO
ug1L
10.0
1
'1210112214:49 591-78-6
isopropylbenzene (Cumene)
NO
ug1L.
5.0
1
1210112214:49 98782-8
p4sopropyltoluene
NO
uglL
5.0
1
12101/2214:49 99-87-6
Methylene Chloride
NO
ug/L
5.0
1
12101/2214.49 75-09-2
4-Methyl-2-pentanone (MIBK)
NO
ug/L'
1.0.0
1
12101/22 14:49 108-10-1
Methyl-tert-butyl ether
NO
ug/L
6.0
1
12/01122 14:49 1634-04-4
Naphthalene
NO
uglL
5.0
1
12/0112214:49 91-20-3
n-Propylbenzene
NO
ug1L
5.0
1
12/01/2214:49 103-65-1
Styrene
NO
ug/L
5.0
1
1210112214:49 100-42-5
1,1,1,24etrachloroethane
NO
ug/L
5.0
1
1210112214:49 630-20-6
1,1,2,2-Tetrachloroelhane
ND
ug/L.
5.0
1
12101/2214:49 79-34-5
Tetrachloroethene
NO
uglL
5.0
1
12101/2214:49 127-18-4
Toluene
NO
ug/L
5.0
1
1210112214:49 10&.88-3
1;2,3-Trichlorobenzene
NO
uglL
5.0
1
12101/2214:49 87-61-6
1,2,44richlorobenzene
NO
ug/L
5.0
1
1.2/01/2-214:49 120.82-1
1,1,1-Trichloroethane
NO
ug/L
5.0
1
12/01/22.14:49 71-55-6
1,1,2-Trichloroethane
NO
ug/L.
5.0
1
12/0112214:49 79-00-5
Trichloroethene
NO
uglL
6.0
1
1210112214:49 79-01-6
Trichlorolluoromethene
NO
ug/L
10.0
1
12101/2214A9 75-69-4
1,2,3-Trichloropropane
ND
ug/L
6.0
1
12101/2214:49 96-18-4 IK
1,2,4-Trimethylbenzene
NO
uglL
5.0
1
12/0112214:40 95.63-6
1,3,5-Trimethylbenzene
NO
ug/L.
5.0 i
1
12101/2214:49 10"7-8
Vinyl acetate
NO
ug/L
10.0
1
1210112214:49 108-05-4 IK
Vinyl chloride
NO
uglL
5.0
1
12/01/2214:49 75-01-4
m&p-Xylene
NO
ug1L
10.0
1
12101122.14:49 179601-23-1
o-Xylene
NO
ug/L
5.0
1
12/0112214:49 95-47-6
Surrogates
4-Bromotluorobenzene (S)
99.
%
70-130
1
12/01/22 14:49 460-00-4
1,2-Dichloroethane-d4 (S)
100
%
70-130
1
12/0112214:49 17.060-07-0
Toluene-d8.(S)
102
%
70-130
1
12/0112214:49 2037-26-5
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2015
Pace Analytical Services -Asheville
Total Dissolved Solids
103
mg/L
25.0 1
1
11/30/22 16:04
4500 Chloride
Chloride
Date: 12/08/2022 01:02 PM
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
16.1 mg1L 1.0 1
REPORT OF LABORATORY ANALYSIS
i
This report shall not be reproduced, except In full,
wiihout the written consent of Pace Analytical Services, LLC.
i
12/02122 19:15 16887-00-6
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aceAnalytical
www.pacclabs.cam
ANALYTICAL RESULTS
Project: Case Farms MWs
Pace Project No.: 92638574
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Sample: MW4 Lab ID: 92638574002 Collected: 1112812211:00 Received: 11/29/22 08:40 Matrix: Water
Parameters Results Units Report Limit f DF Prepared Analyzed CAS No. Qual
5310B TOC Analytical Method: SM 531 OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon ND mg/L 1.0 1 12/01/22 00:30 7440-44-0
Date: 12108/2022 01:02 PM
REPORT OF LABORATORY ANALYSIS
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without the wrllten consent of Pace Analytical Services, LLC.
Page 9 of 36

i
jPace Analytical Services, LLC
aceAnalytical ® 1377 South Park Drive
Kernersvllle, NO 27284
www.pacalabs.cam
[phone]
ANALYTICAL RESULTS
Project: Case Farms MWs
Pace Project No.: 92638574
Sample: MW5 Lab ID: 92638574003 Collected: 11128/22 10:30 Received: 11/29/22 08:40 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
200.8 MET IGPMS
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA200.8 Rev 5.4
Pace Analytical Services - Asheville
I
Arsenic
NO
mg/L
0.0010
1 12102/2215:38 12/05/22 21:51 7440-38-2
Barium
01092
mg1L
0,0010
1 12/0212215:38 12MS= 21:51 7440-39-3
Copper
NO
mg1L
0,0020 1
1 1210212215:38 12/05/22 21:51 7440-50-8.
Iron
1.0
mg/L
0.050
1 12/0212215:38 12/05/22 21:51 743la-89.8
Manganese
0.042
mg/L
0.0020
1 12/02/22 15:38 12/05/22 21:51 7439-96-5
Potassium
2.5
mg/L
0.10
1 12/02/22 15:38 12/05/22 21:51 7440-09-7
Sodium
8.8
mg/L
1.2
5 12/02/22 15:38 12107122 08.26 7440-23-5
Zinc
NO
mg/L
0.010
1 12/02/22 15:38 12/05/22 21:51 7449-66-6
8260D MSV
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
NO
ug/L
26.0
1 12/0112215:06 67-64-1
Benzene
NO
ug/L
5.0
1 1210112215:06 71-43-2
Bromobenzene
NO
ug/L
5.0
1 12/0112215:06 108-86-1
Bromochloromethane
NO
ug/L
5.0
1 12/01/2215:06 74-.97-5
IK.
Bromodichloromethane
NO
ug/L
6.0
1 12/01/2215:06 75-27-4
Bromoform
NO
ug/L
5.0
1 12/01/2215:06 75-25-2
Bromomethane
NO
ug/L
10.0
1 12/01/2215:06 74-83-9
2-Butanone (MEK)
NO
ug/L
10.0
1 12/01/22 15:06 78-93-3
1K
tert-Butyl Alcohol
NO
ug/L
100
1 12/0112215:06 75-65-0
IL,L2,v2
n-Butylbenzene
NO
ug/L
5.0
1 12/01/2215:06 104-51-8
sec-Butylbenzene.
NO
ug/L
5.0
1 1.2/011221.5:06 135-96-8
tert-Butylbenzene
NO
uglL
5.0
1 1210112215,06 98-06-6
Carbon tetrachloride
NO
uglL
6:0
1 1210112215:06 56-23-5
Chlorobenzene
ND
uglL
6.0
1 1210112216:06 108-90-7
Chloroethane
NO
uglL
10.0
1 12101/2215:06 75-00-3
Chloroform
NO
ug1L
5.0.
1 12/011221.6:06 67-66-3
Chloromethane
NO
ug/L
5.0
1 12101/2216:06 74 87-3
2-Chlorotoluene
NO
Ug1L
5.0
1 12101/221.6:06 95-49=8
4-Chlorotoluene
NO
ug/L
5.0
1 12/01/2215:06 106-43-4
1,2-Dibromo-3-chloropropane
NO
ug/L
5.0
1 12101/2215:06 96-12-8
Dlbromochloromethane
ND
ug/L
6.0
1 1210112215:.06 124-48-1
1,2-Dibromoethane_(EDB)
NO
ug/L
6.0
1 12/0112215:06 106=93-4
Dibromomethane
NO
ug/L
6.0
1 1210112215:06 74-95-3
IK
1,2-Dichlorobenzene
NO
ug/L
5.0
1 12/0112215:06 95-50-1
1,3-Dichlorobenzene
NO
ug/L
6.0
1 1210112215:06 541-73-1
1,4-Dichlorobanzene
NO
ug/L
5.0
1 12/0112218:06 106-46-7
Dichlorodifiuoromethane
NO
ug/L
5.0
1 12/0112215:06 75-71-8
1,1-Dichloroethane
ND
ug/L
5.0
1 12/01/2215:06 75-34-3
1,24Dichioroethane
NO
ug/L
5.0
1 12/01/2215:06 107-06-2
1,2-Dichloroethene (Total)
NO
ug/L
5.0
1 12/01/22 15:06 540-59-0
1,1-Dichloroethene
NO
ug/L
5.0
1 12/01/2215:06 75-35-4
ciS-1,2-Dichloroethene
NO
ug1L
5.0
1 12/01/2215:06 156-59-2
trans-1,2-Dichloroethene
NO
ug/L
5.0
1 12/01/2216:06 156-60-5
1,2-Dichloropropane
ND
ug/L
5.0
1 12/01/2215:06 78-87-5
1,3-Dichloropropane
ND
ug/L
5.0
1 12/01/2215:06 142-28-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except
in full,
Date: 12/0812022 01:02 PM
without
the written consent of Pace Analytical Services, LLC.
Page 10 of 36

aceAnalytical
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Project: Case Farms MWs
Pace Project No.: 92638574
Sample: MW5 Lab ID: 92638574003 Collected: 11/28/22 10:30 Received: 11/29/22 08:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
2,2-Dichloropropane
ND
ug/L
5.0
1
1210112215:08 594-20-7
1,1-Dichloropropene
ND
ug/L
6.0
1
12f0112216:06 563-68-6
cis-1,3-Dichloropropene
ND
uglL
6.0
1
1210112215:06 10061-01-5
trans- 1, 3-Dichloropropene
ND
ug/L
6.0
1
12101/2215:06 10061-02-6
Diisopropyl ether
ND
ug/L
6.0
1
12/01122 15:06 108-20-3
Ethylbenzene
ND
ug/L
5.0
1
12/01/22 15:06 100-41-4
Flexachloro-1,3-butadiene
ND
ug1L
6.0
1
12/01/22.15:06 87=68-3
2-Hexanone
ND
ug/L
10.0
1
12101/2215:06 591-78-6
isopropylbenzene (Cumene)
ND
ug/L
5.0
1
12101/2215:06 98-82-8
p-Isopropyltoluene
ND
ug/L
5.0
1
12101/2215:06 99-87-6
Methylene Chloride
ND
ug/L
5.0
1
1210112215:06 75-.09-2
4-Methyl-2-pentanone (MIBK)
ND
ug1L
10.0
1
12/0112215:06 108-104
Methyl-tert-butyl ether
ND
ug1L
5.0
1
1210.1/2215:06 1634-04-4
Naphthalene
ND.
ug11L
5.0
1
12101/2216:06 91-20-3
n-Propylbenzene
ND
ug/L
5.0
1
12101/2215:06 103-66-1
Styrene
ND
u91L
5.0
1
12/0112215.:06 100-42,5
1,1,1,2-Tetrachloroethane
ND
ug1L
6.0
1
1210112216:06 630-20-6
1,1,2,2-Tetrachioroethane
ND
ug/L
5.0
1
12101/2216-06 79-34-5
Tetrachloroethene
ND
ug/L
5.0
1
1210112215:06 127-18-4
Toluene
ND
ug/L
6.0
1
1'21D112215:06 108-88-3
1,2,3-Trichlorobenzene
ND
ug1L'
5.0
1
12/0112215:06 87-61-6
1,2,4-Trichlorobenzene
ND
ug./L
6.0
1
12101/2215:06 120-82-1
1,1,1-Trichloroethane
ND
ug1L
5.0
1
1210112215:06 71-55-6
1,1,2-Trichloroethane
ND
uglL
5.0
1
1210112215:06 79-00-5
Trfchloroeth.ene
ND
ug/L
5.0
1
1210112216:06 79-01-6
Tdchlorofluoromethane
ND
ug/L
10.0
1
12101/2215:06 75-69-4
1,2,3-Trichloropropane
ND
ug/L
6.0
1
1210112216:06 96-18-4
1,2,4-Trlmefhylbenzene.
ND
ug/L
5.0
1
12/0.112215:06 95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
6.0
1
121D112216:06 1013-67-8
Vinyl acetate
ND
ug/L
10.0
1
12101/22 15:06 108-05-4
Vinyl chloride
ND
ug/L
5.0
1
12/01/22 15:06 75-01-4
m&p Xylene
ND
ug/L
10.0
1
1210112215:06 179601-23-1
o-Xyiene
ND
ug1L
5.0
1
1210112215:06 95-47-6
Surrogates
4-Dromofluorobenzene (S)
100
%
70-130
1
12/01/22 15106 460-00-4
1,2-Dichloroethane-d4 (S)
102
%
70-1.30
1
12/01122 15:06 17060-07-0
Toluene-d8 (S.)
104
%
70-1$0
1
12/01/22 15:06 2037-26-5
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2016
Pace Analytical
Services -Asheville
Total Dissolved Solids
113
mg1L
26.0
1
11130/22 16:05
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical
Services -Asheville
Chloride
14.9
mg/L
1.0
1
12/02/2219:18 16887-00-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 1210812022 01:02 PM without the written consent of Pace Analytical Services, LLC.
lK
Page 11 of 36

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wiampacelabs.com
ANALYTICAL RESULTS
Project: Case Farms MWs
Pace Project No,: 92638574
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Sample: MW5 Lab ID: 92638574003 'Collected: 11/28/2210:30 Received: 11129/2208:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5310B TOC Analytical Method: SM 531 OB-2014
Pace Analytical Services - Asheville
Total Organic Carbon' ND mglL 1.0 1 12101/22 00:47 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12108/2022 01:02 PM without the written consent of Pace Analytical Services, LLC. Page 112 of 36

Page 1 of 1
Report Number: 22-335-'0892 D
Account Numbers 14135 7621 Whitepine Road, Richmond, VA 23237
Waypoint. Main 804-743-9401 ° Fax [phone]
Send To: Pace Analytical ANALYTICAL www.waypoiritanalyUcal.com
Sarah Graham "Every acre ... Everyyear"re, Grower. Case Farms Zone
9800 Kincey Ave
Suite 100
Huntersville NC 28078
SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
Date Received: 12/01/2022 Date Of Analysis: 12/42/2022 Date Of Report: 12/02/2022
HM
.- WIN
ENR.
Phosphorus
Potassium
Magr esiurn
Calcium
Sodium
pH
Acidify
C.E.0
Sample ID
Field ID
'Lab
Number%
Soil
Class
Ibs1A.
M3
ppin " Rate
ppm : Rate "
-
ppm " Rate
' K .
ppm Rate
Mg
ppm Rate
Ca
ppm Rate
Na
ppm Rate
Soil
PH
Buffer
Index
H
meq/100g.
theq/1009
Case Farms Zone #
07947
1.2
101
2 VL
22 VL
106 VH
297 L
29 L
5.6
6.85
0.8
3.4
NC=2
NC=11
Case Farms Zone #
07948
1.9
13$
5 VL
77 M
121 VH
356 . L
8 VL
5.5
6.83
1.0
4.0
2.
NC=4
NC=39
Case Farms Zone #
07949
1.8
133
4 VL
65 L
113 VH
328 L
9 VL
5.6
6.85
0.8
3.6
3
NC = 3
NC= 33
Case Farms Zone #
07950
1.8
132
3 VL
85 M
95 VH
147 VL
11 VL
5.2
6.84
0.9
2.7
NC=2"
NC=43
Percent
Base
Saturation.
Nitrate
Sulf&9
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Sield ID ID
Field ID
K
%
Mg
%
Ca
%
Na
%
H
9'o
NqN
ppm, Rate
pp
S.- "
PR m. late
Zn .
Pp m Rate "
Mn
m Rate
ppm
Fe
PP m Rate
Cu
m Rate
PP
B ,
Pp m Rate
SS
ms/cm Fate
Case Farms Zone f♦
1.7
26.0
43.7
3.7
23.5
12 L
0.9 VL
10 M
0.5 L
0.2 VL
NC=25
NC-22.5
NC=63
NC=25.0
Case Farms Zone t
4.9
25.2
44.5
0.9
25.0
6 VL
1.3 L
6 L
0.7 L
0.2 VL
2
NC=12
NC=32.5
NC=38
NC=35.0
Case Farms Zone t
4.6
26.2
45.6
1.1
22.2
7 VL
1.1 L
5 L
0.6 L
0.2 VL
3
NC=15
NQ=27.5
NC=31
NC=30.0
Case Farms Zone t
8.1
29.3
27.2
1.8
33.3
10 L
0.6 VL
3 VL
0.4 L
0.1 . VL
O. N21
NC =15.0
NC = 19
NO = 20,
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained.a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), mslcm (milli -mhos per centimeter), megll00g maximum of thirty days after testing.
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: WaypointAnalytical Virginia, Inc. by
C.E.C. - Callon Exchange Capacity. Salts ms/em x 640 - ppm. o
Pauric Mc Groary Ph.D., CPAg
v
m
m
m
O
0
0

W.". TERTE:CULAR�!K'_'
'5 Pinewbod Plaza Drive - P.O. Box 1056
Granite Falls, NC 28690
Phone [phone];
CHAIN OF CUSTODY
CLIENT- Case Farms Natche
PERMIT
TYPE SAMPLE:
8MPLERNAME�g�+-qa
PHONE #: 828F438-6900
Sample Collection
Information
TYPE
CONTAINERS
ANALYSIS REQUIRED
-Sample Location
Facility Name
DATE
TIME
TEMP. 00
Grib/
'Composite
No.
Plastic/
Glass
Effluent.
Grab
8
P
M. W611 #3
I I ag��Grab
12
PIG'
A&M
M
MR
M. Well #4
(,1
Grab
12
PIG
Same as #3
M. Well #5
1
Grab,
42
PIG
Same as #3'
S6 t L
Relinquishq'c)B
Da
Date:
Time:
Received' By:
Date:
Time.:
'Relin qujshed'By:
Date:
Time:
Received By:
Date:
Time.
PRESERVATION.
KI C06/ 600 [ I HNO3
Pq H2SO4 &/I Dechlofinatirtg Agen't
j NaOH ]-Other
SAMPLE TEMP.-@ LAB'(0c'
NC CERTIFIED LAB # 50
1 - Chlorine 136sid-ual g1l