NC0086827_Issuance of Permit_20051114

I f , • Michael F. Easley
of WAr9 Governor
0 G fro William G.Ross,Jr., Secretary
7 NCDENR North Carolina Department of Environment and Natural Resources
Alan W. Klimek,P.E., Director
Division of Water Quality
November 14,2005
Mr.Bruce Biehl
Director of Engineering/Regulatory Affairs
Brenntag Southeast,Inc.
2000 E.Pettygrew St.
Durham,North Carolina 27703
Subject:Issuance of NPDES Permit NCD086827
Brenntag Southeast,Inc.
Durham County
Dear Mr.Biehl:
Division personnel have reviewed and approved your application for renewal of the subject permit.
Accordingly,we are forwarding the attached NPDES discharge permit. This permit is issued pursuant to the
requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between North
Carolina and the U.S.Environmental Protection Agency dated May9, 1994 (or as subsequently amended).
This final permit includes no major changes from the draft permit sent to you on September 28,2005.
If any parts,measurement frequencies or sampling requirements contained in this permit are unacceptable to
you,you have the right to an adjudicatory hearing upon written request within thirty(30) days following receipt of
this letter. This request must be in the form of a written petition,conforming to Chapter 150B of the North Carolina
General Statutes,and filed with the Office of Administrative Hearings (6714 MfirService Center,Raleigh,North
Carolina 27699-6714). Unless such demand is made,this decision shall be final and binding.
Please note that this permit is not transferable except after notice to the Division. The Division may require
modification or revocation and reissuance of the permit. This permit does not affect the legal requirements to obtain
other permits which maybe required bythe Division of Water Quality or permits required bythe Division of Land
Resources,the Coastal Area Management Act or any other Federal or Local governmental permit that may be
required. If you have any questions concerning this permit,please contact Sergei Chemikov at telephone number
[phone],extension 594.
Sincerely,
l.rkrr--J
fes—'Alan W.Klimek,P.E.
cc: Central Files
NPDES Permit File
Raleigh Regional Office/Surface Water Protection
Aquatic Toxicology Unit
Mr.James E.Shilliday,III,L.G.
Arcadis G&M of North Carolina,Inc.
801 Corporate Center Dr..,Suite 300
Raleigh,NC 27607-5073
N.C.Division of Water Quality!NPDES Unit Phone:[phone]
1617 Mail Service Center,Raleigh,NC 27699-1617 fax:[phone]
Internet:h2o.enr.state.nc.us DENR Customer Service Center 1 800623-7748

Permit Number: NC0086827
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
PERMIT
TO DISCHARGE WASTEWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
Brenntag Southeast, Inc.
is hereby authorized to discharge wastewater from a facility located at
Brenntag Southeast, Inc.Groundwater Remediation System
2000 East Pettigrew Street
Durham County
to receiving waters designated as Unnamed Tributary to Third Fork Creek in the Cape Fear River
Basin in accordance with effluent limitations, monitoring requirements, and other conditions set
forth in Parts I,II,III and IV hereof.
This permit shall become effective December 1, 2005.
This permit and authorization to discharge shall expire at midnight on October 30, 2010.
Signed this day November 14, 2005.
A1
Alan Klimek,P.E.,Director
Division of Water Quality
By Authority of the Environmental Management Commission

•
•
Permit Number: NC0086827
SUPPLEMENT TO PERMIT COVER SHEET
All previous NPDES Permits issued to this facility,whether for operation or discharge are hereby revoked.
As of this permit issuance,any previously issued permit bearing this number is no longer effective.
Therefore,the exclusive authority to operate and discharge from this facility arises under the permit
conditions,requirements,terms, and provisions included herein.
Brenntag Southeast,Inc.
is hereby authorized to:
1. Discharge treated groundwater from said treatment works at the location specified on the
attached map through outfall(s) 001, into an unnamed tributary to Third Fork Creek,
which is classified C-NSW waters in the Cape Fear River Basin.
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Southchem Inc. Facility
Latitude: 35°58'44" Sub-Basin: 03-06-05 Location
Longitude: 78°52'51"
Quad#: D 23 NW-SW Durham
Stream Class: C-NSW Southchem Inc.
Receiving Stream: Unnamed Tributary to Third Fork Creek Nor/'
Permitted Flow: 0.0144 MGD / V I Groundwater Remediation System

Permit Number: NC0086827
A. (1.) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS
During the period beginning on the effective date of the permit and lasting until expiration, the
Permittee is authorized to discharge treated groundwater from outfall(s) 001. Such discharges
shall be limited and monitored by the Permittee as specified below:
Effluent Characterise Limits Monitoring Requirements
Monthly Weekly Daily Measurement Sample Type Sample
Average Average Maximum Frequency Location'
Flow' 0.0144 Continuous Recording E or I
MGD
Total Suspended Solids 30.0 mg/L Monthly Grab E
Oil and Grease2 Monthly Grab E
Iron Monthly Grab E
Manganese Monthly Grab E
Benzene Quarterly Grab E
/-Bis(2-ethylhexyl)phthalate Quarterly Grab E
1,1—Dichloroethene Quarterly Grab E
/Tetrachloroethene Quarterly Grab E
./Trichloroethene Quarterly Grab E
/Toluene Quarterly Grab E
-"Vinyl Chloride Quarterly Grab E
Xylenes(Total) Quarterly Grab E
EPA Method 624/625(Full Annually Grab E
Suite)
Total Nitrogen Monthly Grab E
Chronic Toxicity' Quarterly Grab E
Footnotes:
1. Sample Location: E—Effluent,I—Influent
2. The grab sample for oil and grease should be skimmed from the surface in a quiescent zone,
such as a holding tank, if possible.
3. Chronic P/F (Ceriodaphnia)@ 90%, January,April, July, and October.
The discharge shall contain no floating solids or foam visible in other than trace amounts.

Permit Number: NC0086827
A. (2.) CHRONIC TOXICITY PERMIT LIMIT (QRTRLY)
The effluent discharge shall at no time exhibit observable inhibition of reproduction or significant mortality to
Ceriodaphnia dubia at an effluent concentration of 90%.
The permit holder shall perform at a minimum, quarterly monitoring using test procedures outlined in the "North
Carolina Ceriodaphnia Chronic Effluent Bioassay Procedure," Revised February 1998, or subsequent versions or
"North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure"(Revised-February 1998) or subsequent
versions. The tests will be performed during the months of January,April, July, and October. Effluent sampling for
this testing shall be performed at the NPDES permitted fmal effluent discharge below all treatment processes.
If the test procedure performed as the first test of any single quarter results in a failure or ChV below the permit
limit, then multiple-concentration testing shall be performed at a minimum, in each of the two following months as
described in"North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure"(Revised-February 1998)or
subsequent versions.
The chronic value for multiple concentration tests will be determined using the geometric mean of the highest
concentration having no detectable impairment of reproduction or survival and the lowest concentration that does
have a detectable impairment of reproduction or survival. The definition of"detectable impairment," collection
methods, exposure regimes, and further statistical methods are specified in the "North Carolina Phase II Chronic
Whole Effluent Toxicity Test Procedure"(Revised-February 1998)or subsequent versions.
All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge
Monitoring Form(MR-1) for the months in which tests were performed, using the parameter code TGP3B for the
pass/fail results and THP3B for the Chronic Value. Additionally, DWQ Form AT-3 (original) is to be sent to the
following address:
Attention: North Carolina Division of Water Quality
Environmental Sciences Section
1621 Mail Service Center
Raleigh,North Carolina 27699-1621
Completed Aquatic Toxicity Test Forms shall be filed with the Environmental Sciences Branch no later than 30 days
after the end of the reporting period for which the report is made.
Test data shall be complete, accurate, include all supporting chemical/physical measurements and all
concentration/response data, and be certified by laboratory supervisor and ORC or approved designate signature.
Total residual chlorine of the effluent toxicity sample must be measured and reported if chlorine is employed for
disinfection of the waste stream
Should there be no discharge of flow from the facility during a month in which toxicity monitoring is required, the
permittee will complete the information located at the top of the aquatic toxicity (AT) test form indicating the
facility name,permit number,pipe number, county,and the month/year of the report with the notation of"No Flow"
in the comment area of the form. The report shall be submitted to the Environmental Sciences Branch at the address
cited above.
Should the permittee fail to monitor during a month in which toxicity monitoring is required, monitoring will be
required during the following month.
Should any test data from this monitoring requirement or tests performed by the North Carolina Division of Water
Quality indicate potential impacts to the receiving stream, this permit may be re-opened and modified to include
alternate monitoring requirements or limits.
NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control organism
survival, minimum control organism reproduction, and appropriate environmental controls, shall constitute an
invalid test and will require immediate follow-up testing to be completed no later than the last day of the month
following the month of the initial monitoring.

imap://[e-mail]:143/f...
Subject: Draft Permit Reviews (2)
From: John Giorgino <[e-mail]>
Date: Thu, 13 Oct 2005 14:15:40-0400
To: sergei chernikov<[e-mail]>
Sergei, I have reviewed the following:
NC0086827 Brentag Southeast - No Comments
NC0086088 Girmes Site Remediation - sample is listed as a composite, this facility has
been taking a grab sample.
Thanks for forwarding the drafts.
-John
John Giorgino
Environmental Biologist
North Carolina Division of Water Quality
Environmental Sciences Section
Aquatic Toxicology Unit
Mailing Address:
1621 MSC
Raleigh, NC 27699-1621
Office: 919 733-2136
Fax: [phone]
Email: [e-mail]
Web Page: http://www.esb.enr.state.nc.us
1 of 1 10/14/2005 8:19 AM

09/28/2005 16:37 FAX [phone] HERALD SUN CLASSIFIEDS
Z001
Name (Primary) NCDINR
Start Date : 10/3/2005
Stop Date 10/3/2005 Q
ALlja41-
Publication HE - Hera .d Sun
Ad # 42132 q /llL M"'1-
Ad Sales Rep. 02 - Dolma Minor ` i-( _ T j -- 6! I 3
PUBLIC NOTICE
STATE OF NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT
COMMISSION/NPDES UNIT
1617 MAIL SERVICE CENTER
RALEIGH,NC 27699-1817
NOA NPOES
T TISSUE
WASTEWATER PERMIT
T
On the base.of thorough staff review end applica-
tion of NC General Statue 143.21.Public 13W 52-
600 and other lawful standards and re9ullonone,
the NorTh Commission proposina es toIssuenaal Na National Management
olu-
wastewater disse charge(permit to n the perem (on(s)Slatt)ed below erfecttic 45 days from the publisehh date
of this notice.
Wratten comments regarding the propo=cd Permit
will be accepted until 30 days after the pubileh
date of bulla nonce.All Comments receNed prof to
Mat date aria considered,n the final determi-
nations regarding the proposed Penni[The 0'r c-
tor of the NC Oive on of Water Oue4ty may decide
to hold o puollc meeting for the proposed permit
should the Division receive a significant degree of
public Interest
Copies of the drag permit and other supporting in-
formation on flue used to determine conditions
present In the draft permit arc available upon re-
quc t and payment of the costs of reproduction.
Mad comment.and/or requests for ofOfineDOn to
me NC Division of Water Quality pt the above ad-
drape or call the Point Source Branch at(919)733-
5083,extension 520 Please include the NPOES
permit number(attached)In any communication.
Intercoted persons may also vlsit the Division of
Water Quality at 512 N.Salisbury Street,Raleigh,
NC 27604-1148 between the hours of 5•DO a.m.
and 5.00 p.m to review information on fie.
The Brenntag Southeast Inc. (2000 East Petti-
grew St,Durham,NC 27'f03)nee applied for re-
newal Of NPOES permit NC0066827 for the Brcn-
ntag facility in Durham County This permitted fa-
cility discharges treated groundwater to the un-
named tributary tO Third Fork Creek In the Cape
Fear River Basin.Cu9rr�ently TSS are water quality
uture
dons limited This 011e portion of the Cede Fear affect f River Basin.
H-S.October 3,2005

DENR/DWQ
FACT SHEET FOR NPDES PERMIT DEVELOPMENT
NPDES No. NC0086827
Facility Information
Applicant/Facility Name: Brenntag Southeast,Inc.
Applicant Address: 2000 East Pettigrew Street,Durham,NC 27702
Facility Address: 2000 East Pettigrew Street,Durham,NC
Permitted Flow 0.0144 MGD
Type of Waste: Remediated Groundwater
Facility/Permit Status: Renewal
County: Durham
Miscellaneous
Receiving Stream: UT to Third Fork Regional Office: Raleigh
Creek
Stream Classification: C NSW USGS Topo Quad: D 23 NW—SW Durham
303(d)Listed?: No Permit Writer: Sergei Chernikov
Subbasin: 03-06-05 Date: September 14,2005
Drainage Area(mi2): <0.1 mi2
Summer 7Q10(cfs) 0.0
Winter 7Q10(cfs): 0.0s
Average Flow(cfs): m.1
IWC(%): 100%
Primary SIC Code: 5196
SUMMARY
Brenntag Southeast, Inc. has applied for renewal of NPDES permit to discharge remediated groundwater
into a storm drain located in Durham County. The only viable option,other than discharge to surface water,
is to discharge to the City of Durham. However,the City of Durham is unwilling to accept the remediated
groundwater. Leaving the only other economically viable option as discharge to surface water.
The facility is requesting a permitted flow of 0.0144MGD. Groundwater sampling events from 1996 to
present have detected the following compounds including chlorinated solvents:
Isopropyl ether#
Benzene
Carbon disulfide
Chloroethane#
Chloroform#
1,1-Dichloroethane
1,1-Dichloroethene
1,2-Dichloroethane(total)
1,3,5-Trimethylbenzene#
tert-butylbenzene#
1,2,4-Trimethlybenzene#
sec-butylbenzene#
ethylbenzene#
Methlyene chloride#
Tetrachloroethene
Toluene
1,1,1-Trichlorethane#
Trichloroethene
Vinyl chloride
Xylenes(total)
Bis(2ethylhexyl) phthalate
Naphthalene#
Fact Sheet
NPDES Renewal
Page I

Phenol
Methyl isobutyl ketone#
# - Major Modification for the permit was issued on 03/19/2004 and monitoring for these parameters was
removed based on the fact that these constituents were not found at detectable levels in the effluent for at
least past 12 months.
In addition to solvent contamination groundwater samples indicate contamination from petroleum sources,
therefore the conditions of the general permit for groundwater remediation systems have been incorporated
into this permit. The general permit assumes zero dilution in developing the permit limits and monitoring
requirements. Assuming zero dilution is appropriate for this site since discharge is to a zero flow stream.
A vacuum-enhanced recovery system will be used to pump groundwater from 10 extraction wells at a
maximum rate of 10 gpm per well. This equates to 0.0144 MGD.
The discharge will be to an unnamed tributary to Third Fork Creek Though the unnamed tributary is not
listed as impaired, according to the state's 303(d) list, Third Fork Creek is listed as impaired. The cause of
impairment is uncertain but urbanization is suspected.
TOXICITY TESTING:
Current Requirement:Chronic Toxicity(Ceriodaphnia)P/F at 90%
Recommended Requirement:Chronic Toxicity(Ceriodaphnia) P/F at 90% •
This facility has failed three chronic toxicity tests during the previous 4.5 years. The subsequent tests have
passed.
INSTREAM MONITORING: _ _, '
None.
COMPLIANCE SUMMARY:
DMRs have been reviewed for the period January 2001 through August 2005. The facility has a mixed
compliance record. The following Notices of Violation were issued: 12/06/02 - to; 11/25/02 - to;
9/16/02 - to; 9/23/02 - to; 9/04/02 - to; 06/20/02 - to; 12/21/01 - to; 11/06/01 - TSS,
tetrachloethene, 1,1 dichloroethene.
PROPOSED CHANGES:
• MonitoringFr xis: The monitoring for carbon disulfide and phenol have been eliminated based on
DMRs review(non-detect for 20 months). The monitoring frequency for vinyl chloride and xylenes has
been reduced to quarterly based on DMRs review(non-detect for 20 months).
• Linin: Based on DMRs review (non-detect for 20 months) limits for benzene, bis (2-ethylhexyl)
phtalaet, 1,1 - dichloroethene, tetrachloroethene, trichloroethene, and toluene have been eliminated.
Monitoring frequency for these parameters have been reduced to quarterly due to the elimination of the
limits.
PROPOSED SCHEDULE FOR PERMIT ISSUANCE:
Draft Permit to Public Notice: September 28,2005
Permit Scheduled to Issue: November 14,2005
STATE CONTACT:
If you have any questions on any of the above information or on the attached permit,please contact Sergei
Chernikov at(919) 733-5038 ext. 594.
Fact Sheet
NPDES Renewal
Page 2

ARCAD1S
Infrastructure, buildings, environment, communications ARCADIS G&M of North Carolina,
.. ... Inc.
.+:P.-'T'.r....MP,�I•�IIYIM'"R[teN'inli.s1M•WIOt.r..•..:.FnMM•.
801 Corporate Center Drive
Suite 300
a nnl `'J Raleigh,
Mr.Charles H. Weaver,Jr. lM I North Carolina 27607-5073
NC DENR I 1 I Tel [phone]
Division of Water Quality APR 2 8 2005 _ Fax [phone]
NPDES Unit APR Owww.arcadis-us.com
1617 Mail Service Center i
Raleigh, NC 27699-1617 "R -WATER QUALITY
POINT SOUr,CE BRANCH ENVIRONMENTAL
Subject: Date:
NPDES Permit Renewal Application,Groundwater Remediation System, Brenntag 26 April 2005
Southeast, Inc. (former Southchem facility), Durham, North Carolina.
Contact:
Jim Shilliday
Dear Mr. Weaver:
Extension:
246
On behalf of Brenntag Southeast, Inc. (Brenntag Southeast), ARCADIS G&M of
North Carolina, Inc. (ARCADIS) has enclosed one original and two copies of the E-mail:
National Pollutant Discharge Elimination System(NPDES) permit renewal jshilliday@arcadis-
application for the continued discharge of effluent from a groundwater remediation us.com
system at the Brenntag Southeast facility(formerly Southchem) in Durham, North
Carolina. Treated groundwater from the remediation system is discharged to an on- Our ref:
site storm sewer that, in turn,discharges to a drainage ditch located along the NC000368.0015
southern boundary of the site. This drainage ditch conveys surface water to an
unnamed tributary of Third Fork Creek. Other items enclosed with this letter in
support of the NPDES permit renewal application include: a copy of the March 2005
Discharge Monitoring Report(Attachment A) which summarizes the most recent
analytical data for the system effluent;a USGS topographic map of the project area
that depicts the location of the system outfall (Figure 1); and a site map that depicts
the route of the treated water to the discharge point(Figure 2).
Sludge is neither generated nor discharged by the groundwater remediation system;
therefore,a sludge management plan has not been included with this application.
Any solids(i.e. silt, iron and manganese precipitate)generated during the
groundwater extraction and/or treatment process are filtered from the treatment
stream using bag filters and granular activated carbon units. The treated effluent is
sampled on a monthly basis for total suspended solids in compliance with the
monitoring requirements for the site(see Attachment A).
Part of a bigger picture

ARCADIS
If you have any questions regarding the information presented in the NPDES permit
application or any of the supporting material, please call us at [phone].
Sincerely,
ARCADIS G&M of North Carolina, Inc.
"41"/C44141.1.26-
Christopher J. Kalinowski, E.I.
Staff Engineer
OP- 0•3‘;
mo .
es E. Shilliday, III,O .G.
nior Scientist/Project Manager
Copies:
Mr. Bruce Biehl, Brenntag Southeast, Inc.
File
G:\ENV\Soodhchem\NC0368.015\NPDES Peend Reneeal\Cover Lefler for NPDES Permit Renewal.doc
Page:
2/2

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ARCAD1S 801 Corporate Center Drive,
• `cil' 0 Suite 300
-.--')
' . Raleigh.NC 27607
--,-
-- 2-‘-+ 919-854-1282
G&M of North Carolina, Inc.
QUADRANGLE LOCATION REV. DRAWING DATE: ACAD FILE:
SCALE 4/19/05
SITE LOCATION
o 2000 4000
CLIENT: PM:
11111111 BRENNTAG SOUTHEAST, INC. JS
LOCATION: FORMER SOUTHCHEM FACILITY PE/RG:
SOURCE:TOPOGRAPHY TAKEN FROM USGS 7.5 MINUTE QUADRANGLE DURHAM,NORTH CAROLINA
SOUTHEAST DURHAM AND SOUTHWEST DURHAM DESIGNED: DETAILED: PROJECT NO: FIGURE:
PJB NC000368.0015 1

•
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• RAILROAD
® RECOVERY WELL
U
Z
_x
W
I
Z i ` DIESEL
STORAGE
TANK
LUBRICANT
I 'ACKAGING
I
I PLATFORM
--------�
I 1 ►
1 .
—II
---------
RETENSION TAI
mme
DISCHARGE TO
DRAINAGE DITCH
I
SCALE IN FEET
0 100 200
ARCAD1S FIGURE
SITE 2
ARCADIS of North Carolina, Inc. MAP
801 Corporate Center Drive, Suite 300
Raleigh. NC 27607
Tel: [phone] Fax: [phone]
www.arcadis—us.com
J

FACT SHEET FOR EXPEDITED RENEWAL
Permit Number /v, 00 $(f) —7
Facility Name
Reviewer
Basin/Sub-basin
Receiving Stream
Stream Classification in permit
Stream Classification in BIMS
Is the stream impaired (listed on 303(d))?
Is stream monitoring required?
Do they need NH3 limit(s)?
Do they need TRC limit(s)?
Do they have whole-effluent toxicity testing?
Are there special conditions?
Existing Expiration Date
Proposed Expiration Date
Miscellaneous Comments:
of 4 o APO
If expedited, is this a simpler permit or a more difficult one?