WQ0000672_2022 Residual Annual Report_20230301

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * WQ0000672
Applicant/Permittee City of Lumberton
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Fayetteville
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Enviro-Choice Recycling, LLC
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
9107385311
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0000672
Has Current Existing permit number
Applicant/Permittee Address*
POST OFFICE BOX 1388, LUMBERTON, NORTH CAROLINA 28359
Facility Name*
City of Lumberton Class B Residuals Program
Please provide comments/notes
on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2022 Annual Report.pdf 29.22MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, INC 27699-1617
Signature /� A
Submission Date 3/1/2023

ENVIRO.. H ICE
W
PO Box 309
Lumberton, NC 28359
Phone: [phone]
Fax: [phone]
February 28, 2023
NC Environmental Quality-DWQ
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Attention: Compliance Representative
Subject: 2022 Annual Report for City of Lumberton Land Application Program
(City of Lumberton WQ0000672)
Dear Compliance Representative,
Enclosed is (1) copy of the monitoring and reporting information as requited in the referenced
permit for the City of Lumberton, North Carolina. This report was complied from land
application records provided by the City of Lumberton and Enviro-Choice Recycling. The report
includes: 1) a state required annual certification for and facility information page, 2) the 2022
annual application summary table, 3) annual residual sampling summary form and laboratory
analysis reports, 4) field loading reports, 5) pathogen and vector reduction documentation, and 6)
soil analysis reports.
Should you need more information regarding this land application program, please contact me at
910-738-5311 or envirochoicencgggmaiLcom.
A �Lj
Michael C. Hunt
Enviro-Choice Recycling
CC: Henry Harper, Wastewater ORC, City of Lumberton WWTP
Office: 910-671-3859 hharperkci.lumberton.nc.us

ANNUAL LAND APPLICATION CERTIFICATION FORM
W Permit#: WQ0000672 County:. Robeson Year: _
Fac lity Name (as shown on permit): City of Lumberton
Land Application Operator: Enviro-Choice Recycling, LLC Phone:
Land application of residuals as allowed by the permit occurred during the past calendar year?
0 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Pa A - Residuals Application Summary.
2022
910-738-5311
Total number of application fields in thepermit:
43
Total number of fields utilized for land application during the year:
18
Total amount of dry tons applied during the year for all application sites:
1993.02
Total number of acres utilizes for land application during the year:
460
Facility was compliant during calendar year 2022 with all conditions of the land application permit
(inc uding but not limited to items 1-13 below) issued by the Division of Water Resources. 21 Yes ❑ No
If n please, provide a written description why the facility was not compliant, the dates, and explain corrective action
tak n.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
he limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
f laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T A 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
03 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
03 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) o contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
ttached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
pecified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Par C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
WW •bgC
Permide N'ame' And Title (type or print) Sig atu e ofKermittee Date
A:LJ on
4J
Signature of Preparer* Date Signature of Land Applier Date
(if d�fferent from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T. 1102 (26) DENR FORM ACF (1212006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0000672 Laboratory: 1) Pace Analytical
Facility Name: City of Lumberton 2) Cameron Testing Services, Inc.
Residual Source WQ # or 3) Enco Laboratories
NPDES #: WQ0000672 4
WWTP Name: City of Lumberton 5)
Residual Analvsis Data
Parameter
(mg/kg)
Conc.
Limit
(m k )a
Sample or Composite Date
2/17/22
4/6/2022
8/20/22
11/17/22
Percent Solids (%)
NA
2.41
2.48
2.57
2.66
Arsenic
75
83
11.6
19.3
75.2
Cadmium
85
20.7
2.02
0.95
18.8
Copper
4,300
450
595
523
523
Chromium
NA
4.15
132
235
136
Lead
840
20.7
21.6
26.8
18.8
Mercury
57
1.6
00.008
0.33
1.5
Molybdenum
75
20.7
6.66
13.7
13.7
Nickel
420
83
26.1
54.6
54.6
Selenium
100
83
8.06
1.95
75.2
Zinc
7,500
827
953
890
890
Total Phosphorus
NA
20400
17300
5603
15300
TKN
NA
44600
36100
7549
61400
Ammonia -Nitrogen
NA
6270
6880
2074
465
Nitrate and Nitrite
NA
830
806
1988
752
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
D 1-� +LA 2/28/2023
Signature of Preparer *
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Ozzell Baker
Owner: James Campen Predominant Soil Series:
Acres Permitted: 5 Site #: 16 Field #:
25.01
WaB-Wagram
NC-RO-16-16
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/17/22
2j
4/6/22
3
8/20/22
4j
11/17/22
5
6
7
81
9
0
11
12
% Solids
2.41
2.48
2.57
1 2.66
Arsenic
83
11.6
19.3
75.2
Cadmium
20.7
2.02
0.95
18.8
Copper
450
595
523
523
Chromium
4.15
132
235
136
Lead
20.7
21.6
26.8
18.8
Mercury
1.66
0.008
0.33
1.5
Molyb-
denum
20.7
6.66
13.7
1 13.7
Nickel
83
26.1
54.6
54.6
Selenium
83
8.06
1.95
75.2
Zinc
827
953
890
890
Total
Phos-
horus
20400
17300
5603
15300
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
10
11
12
DT/Ac./
_9L
0
App.
Event
2.05
2.95
Arsenic
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
0.000
0.000
3.085
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.085
Chromium
0.000
0.000
1.386
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.386
Lead
0.000
0.000
0.158
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.158
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
5.249
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.249
Total
Phos-
0.000
70.999
33.046
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
104.046
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Adl/� A 44W4
Signature of Land Applier
2/ 16/2023
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton
Land Owner: James Campen
Operator: Ozzell Baker
Crop 1 Name: Bermuda
WQ Permit #: WQ0000672 Field #: NC-RO-16-16
Annual Dry Tons Applied: 25.0060 Site #: 16
Predominant Soil Series: WaB-Wauram
Crop 1 Max. PAN:
192
Crop 2 Name:
Acres Utilized: 5
Acres Permitted: 5
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
Q
Volume applied
enter one Solids/
( )
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
PP P
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
past 24
Hrs.
inches
a
o
0 w
o
?:
-
N
��,
=
TKN
mg/kg
36100
Z a
o
°�
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/5/22
55800
2.48
1.154
WQ0000672
Dry
0
S
0.5
0.3
6880
806
30.035
NA
Bermuda
7/6/22
43400
2.48
0.898
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
23.360
NA
Bermuda
9/l/22
142600
2.48
2.949
WQ0000672
Dry
0
S
0.5
0.3
7549
2074
1988
27.533
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
241So0
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
80.928
0.000
Lime Applied
Annuallbs/acre
0.000
0.000
3.085
1.386
0.158
0.000
0.000
0.000
0.000
5.249 104.046
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.278
0.127
39.385
3.861
0.044
3.283
0.25
32.459
Current Cumulative lbs/ac
0.278
0.127
42.470
1.386
4.019
0.044
0.000
3.283
0.250
37.708
Permitted C. P. L. R.****
36
34
1 1338
1
1 267
1 15
374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1 192
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/16/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 14.11
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Tracy Bullard Owner: Tracy Bullard Predominant Soil Series: Ly-Lynchburg
Acres Used: 3.8 Acres Permitted: 3.8 Site #: 5 Field #: NC-RO-39-05
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/17/22
2j
4/6/22
3
8/20/22
4j
11/17/22
5
6
7
81
9
0
11
12
% Solids
2.41
2.48
2.57
1 2.66
Arsenic
83
11.6
19.3
75.2
Cadmium
20.7
2.02
0.95
18.8
Copper
450
595
523
523
Chromium
4.15
132
235
136
Lead
20.7
21.6
26.8
18.8
Mercury
1.66
0.008
0.33
1.5
Molyb-
denum
20.7
6.66
13.7
1 13.7
Nickel
83
26.1
54.6
54.6
Selenium
83
8.06
1.95
75.2
Zinc
827
953
890
890
Total
Phos-
horus
20400
17300
5603
15300
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
10
11
12
DT/Ac./
_9L
0
App.
Event
3.71
Arsenic
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Chromium
0.000
0.980
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.980
Lead
0.000
0.160
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.160
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Total
Phos-
0.000
128.435
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
128.435
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
U " LuV�u.l7! � 4j
Signature of Land Applie
2/ 16/2023
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-39-05 Acres Utilized: 3.8
Land Owner: Tracy Bullard
Operator: Tracy Bullard
Crop 1 Name: Bermuda
Annual Dry Tons Applied: 14.1059
Site #: 5
Predominant Soil Series: Ly-Lynchburg
Crop 1 Max. PAN: 129 Crop 2 Name:
Acres Permitted: 3.8
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
p
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
t
Moist)
Precip.
Past 24
11rs.
inches
a
F 2
w
o
o
°�
7
w
°�
TKN
mg/kg
Z a
;
o
ac o
�.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
6/16/22
136400
2.48
3.712
WQ0000672
Dry
0
S
0.5
1 0.3
361001
6880
806
96.603
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
136400
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
96.603
o.000
Lime Applied
Annuallbs/acre
0.000
0.000
0.000
0.980
0.160
0.000
0.000
0.000
0.000
0.000
128.435
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.001
0
0.024
0.001
0
0
0.002
0.001
0.102
Current Cumulative lbs/ac
0.001
0.000
0.024
0.980
0.161
0.000
0.000
0.002
0.001
0.102
Permitted C. P. L. R.****
36
34
1 1338
267
15
1 N/A
1 374
89
1 2498
Permit PAN Limit 1 st/2nd Crop
129
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
4J *Application Method: S - Surface, IN - Injection, INC - Incorporation
y( 2/16/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 52.58
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Ronald G. Hammonds Owner: Taylco, INC Predominant Soil Series: GOA-Goldsboro
Acres Used: 10.6 Acres Permitted: 10.6 Site #: 14 Field #: NC-RO-20-14
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
L 1 J
2/17/22
2j
4/6/22
3j
8/20/22
4
11/17/22
5
6
zi
81
9
10
11
12
% Solids
2.41
2.48
1 2.57
2.66
Arsenic
83
11.6
19.3
75.2
Cadmium
20.7
2.02
0.95
18.8
Copper
450
595
523
523
Chromium
4.15
132
235
136
Lead
20.7
21.6
26.8
18.8
Mercury
1.66
0.008
0.33
1.5
Molyb-
denum
20.7
6.66
13.7
1 13.7
Nickel
83
26.1
54.6
54.6
Selenium
83
8.06
1.95
75.2
Zinc
827
953
890
890
Total
Phos-
horus
20400
17300
5603
15300
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
L I J
2
3
4
5
6
7
8j
9
10
11
12
DT/Ac./
0
App.
Event
4.96
Arsenic
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
0.000
0.000
5.188
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.188
Chromium
0.000
0.000
2.331
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.331
Lead
0.000
0.000
0.266
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.266
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Selenium
0.000
0.0001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
8.829
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
8.829
Total
Phos-
0.000
0.000
55.582
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
55.582
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information
submitted. I am aware that there are significant penalties for submitting false information, including the possibility
of fines and imprisonment for knowing violations".
A�j ��� 4W�
Signature of Land Applier
2/ 16/2023
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton
Land Owner: Taylco, Inc
Operator: Ronald G. Hammonds
Crop 1 Name: Corn
WQ Permit #: WQ0000672 Field #: NC-RO-20-14
Annual Dry Tons Applied: 52.5767 Site #: 14
Predominant Soil Series: GoA-Goldsboro
Crop 1 Max. PAN:
147
Crop 2 Name:
Acres Utilized: 10.6
Acres Permitted: 10.6
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
Q
Volume applied
enter one Solids/
( )
Liquid
Cu. Yds Gallons
186000
o
/o
Solids
1 2.48
Volume
Applied per
PP P
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
past 24
Hrs.
inches
a
o
0 w
o
?:
-
N
��,
� =
N
TKN
mg/kg
Z a
o
°�
�
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
10/4/22
1.815
WQ0000672
Dry
0
S
0.5
0.3
7549
1 2074
1988
16.940
NA
Corn
11/9/22
111600
2.48
1.089
WQ0000672
Dry
0
S
0.5
0.3
7549
2074
1988
10.164
NA
Corn
11/10/22
105400
2.48
1.028
WQ0000672
Dry
0
S
0.5
0.3
7549
2074
1988
9.599
NA
Corn
11/14/22
105400
2.48
1.028
WQ0000672
Dry
0
S
0.5
0.3
7549
2074
1988
9.599
NA
Corn
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
322400
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
46.302
0.000
Lime Applied
Annuallbs/acre
0.000
0.000
5.188
2.331
0.266
0.000
0.000
0.000
0.000
8.829
55.582
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.001
0
10.033
0.33
0
0
0
0
14.341
11/22
0.54
Current Cumulative lbs/ac
0.001
0.000
15.221
2.331
0.596
0.000
0.000
0.000
0.000
23.170
Permitted C. P. L. R.****
36
34
1 1338
1
267
1 15
1 N/A
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1 147
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
4. *Application Method: S - Surface, IN - Injection, INC - Incorporation
2/16/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Ronald G. Hammonds Owner: Ronald G. Hammonds Predominant Soil Series:
6.7 Acres Permitted: 6.7 Site #:
Field #
35.26
NoA - Norfolk
NC-RO-20-06
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/17/22
2j
4/6/22
3
8/20/22
4j
11/17/22
5
6
7
81
9
0
11
12
% Solids
2.41
2.48
2.57
1 2.66
Arsenic
83
11.6
19.3
75.2
Cadmium
20.7
2.02
0.95
18.8
Copper
450
595
523
523
Chromium
4.15
132
235
136
Lead
20.7
21.6
26.8
18.8
Mercury
1.66
0.008
0.33
1.5
Molyb-
denum
20.7
6.66
13.7
1 13.7
Nickel
83
26.1
54.6
54.6
Selenium
83
8.06
1.95
75.2
Zinc
827
953
890
890
Total
Phos-
horus
20400
17300
5603
15300
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
10
11
12
DT/Ac./
_9L
0
App.
Event
5.26
Arsenic
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
0.000
0.000
5.505
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.505
Chromium
0.000
0.000
2.474
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.474
Lead
0.000
0.000
0.282
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.282
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
9.368
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
9.368
Total
Phos-
0.000
0.000
58.977
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
58.977
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
AAJ
Signature of Land Applier
2/ 16/2023
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-20-06 Acres Utilized: 6.7
Land Owner: Ronald G. Hammonds Annual Dry Tons Applied: 35.2649 Site #: 6 Acres Permitted: 6.7
Operator: Ronald G. Hammonds Predominant Soil Series: NoA-Norfolk Cation Exchange Capacity (non 503):
Crop 1 Name: Corn Crop 1 Max. PAN: 131 Crop 2 Name: Crop 2 Max. PAN:
Q
Volume applied
enter one Solids/
� )
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
PP � P
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
past 24
Ms.
inches
a
S
o
0 w
* °�
o
?:
� �
-
N
o
��,
=
N
o
TKN
mg/kg
Z a
o �
°�
�
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
9/27/22
192200
2.48
2.967
WQ0000672
Dry
0
S
0.5
0.3
7549
2074
1988
27.694
NA
Corn
9/28/22
148800
2.48
2.297
WQ0000672
Dry
0
S
0.5
0.3
7549
2074
1988
21.440
NA
Corn
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this forEP
0.000
0.000
TOTALS:
0
341000
As
Cd
Cu
Cr
Pb
H
Mo
Ni
Se
Zn
49.134
0.000
Lime Applied
Annuallbs/acre
0.000
0.000
5.505
2.474
0.282
0.000
0.000
0.000
0.000
9.368
58.977
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.007
0.001
2.625
1.562
0
0.069
0.391
0.003
5.839
11/22
0.54
Current Cumulative lbs/ac
0.007
0.001
8.130
2.474
1.844
0.000
0.069
0.391
0.003
15.207
Permitted C. P. L. R.****
36
34
1338
1 267
1 15
1 N/A
1 374
1 89
1 2498
Permit PAN Limit I st/2nd Crop
1 131
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
`�' n *Application Method: S - Surface, IN - Injection, INC - Incorporation
V �1 4J 2/16/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 303.90
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Delois Allen Owner: City of Lumberton Predominant Soil Series: Jo -Johns Sandy
Acres Used: 47.7 Acres Permitted: 47.7 Site #: 4 Field #: NC-RO-17-04
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/17/22
2j
4/6/22
3
8/20/22
4j
11/17/22
5
6
7
81
9
0
11
12
% Solids
2.41
2.48
2.57
1 2.66
Arsenic
83
11.6
19.3
75.2
Cadmium
20.7
2.02
0.95
18.8
Copper
450
595
523
523
Chromium
4.15
132
235
136
Lead
20.7
21.6
26.8
18.8
Mercury
1.66
0.008
0.33
1.5
Molyb-
denum
20.7
6.66
13.7
1 13.7
Nickel
83
26.1
54.6
54.6
Selenium
83
8.06
1.95
75.2
Zinc
827
953
890
890
Total
Phos-
horus
20400
17300
5603
15300
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
10
11
12
DT/Ac./
_9L
0
App.
Event
6.37
Arsenic
0.000
0.148
0.000
1 0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.148
Cadmium
0.000
0.026
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.026
Copper
0.000
7.581
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
7.581
Chromium
0.000
1.682
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.682
Lead
0.000
0.275
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.275
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.085
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.085
denum
Nickel
0.000
0.333
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.333
Selenium
0.000
0.103
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.103
Zinc
0.000
12.143
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
12.143
Total
Phos-
0.000
220.437
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
220.437
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applie
2/ 16/2023
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton
Land Owner: City of Lumberton
Operator: Delois Allen
Crop 1 Name: Soybeans
WQ Permit #: WQ0000672 Field #: NC-RO-17-04
Annual Dry Tons Applied: 303.9189 Site #: 4
Predominant Soil Series: Jo -Johns Sandy
Crop 1 Max. PAN: 174 Crop 2 Name:
Acres Utilized: 47.7
Acres Permitted: 47.7
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
y
Volume applied
enter one Solids/
( )
Liquid
4
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
PP P
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal Waste,
etc)
Soil
Cond.
fin'
Wet,
Moist)
Precip.
past 24
Ms.
inches
a
o w
°
o
N
`;
w
*
TKN
mg/kg
36100
Z a
o
ac 0
CD
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
lbs/acre
( )
Name of Crop Type
ReceivingResidual
Application
PP
Crop 1
Crop 2
Crop 1
Crop 2
5/9/22
260400
2.48
0.565
WQ0000672
Dry
0
S
0.5
1 0.3
6880
1 806
14.692
NA
Soybeans
5/10/22
390600
2.48
0.847
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
22.038
NA
Soybeans
5/11/22
378200
2.48
0.820
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
21.339
NA
Soybeans
5/12/22
217000
2.48
0.470
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
12.243
NA
Soybeans
5/17/22
341000
2.48
0.739
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
19.240
NA
Soybeans
5/18/22
173600
2.48
0.376
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
9.795
NA
Soybeans
5/19/22
93000
2.48
0.202
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
5.247
NA
Soybeans
5/20/22
117800
2.48
0.255
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
6.646
NA
Soybeans
5/23/22
167400
2.48
0.363
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
9.445
NA
Soybeans
5/24/221
173600
2.48
0.376
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
9.795
NA
Soybeans
5/25/22
179800
2.48
0.390
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
10.145
NA
Soybeans
5/26/22
142600
2.48
0.309
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
8.046
NA
Soybeans
0
303800
0.659
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp to this form):
17.141
0.000
TOTALS:
01
2938800
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
165.8111
0.000
Lime Applied
Annuallbs/acre
0.148
0.026
7.581
1.682
0.275
0.000
0.085
0.333
0.103
12.143 220.437
1.
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.157
0.073
28.421
1.75
0.017
0.461
1.698
0.108
16.43
28.573
2498
1/22
0.64
Current Cumulative lbs/ac
0.305
0.099
36.002
1.682
2.025
0.017
0.546
2.031
0.211
Permitted C. P. L. R.****
36
1 34
1 1338
1
1 267
15
N/A
1 374
89
Permit PAN Limit 1 st/2nd Crop
F 174
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/16/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically
digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Supplemental Information
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-17-04 Acres Utilized: 47.7
Land Owner: City of Lumberton Annual Dry Tons Applied: 303.9189408 Site #: 4 Acres Permitted: 47.7
Operator: Delois Allen
Crop 1 Name: Soybeans
Predominant Soil Series: Jo -Johns Sandy
Crop 1 Max. PAN: 174.00 Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max PAN:
o +'
Volume applied (enter
one )
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
pp p
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
D
Wets
Moist)
Preci p
Past 24
Hrs.
inches
y
ro '5
0 w
cl,o
o
o
`�°
CD N
w
o
TKN
mg/kg
36100
Z
o
m o
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
ReceivingResidual
Application
Crop 1
Crop 2
Crop 1
Crop 2
5/31/22
173600
2.48
0.376
WQ0000672
Dry
0
S
0.5
0.3
6880
806
9.795
NA
Soybeans
6/1/22
130200
2.48
0.282
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
7.346
NA
Soybeans
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
TOTALS:
0
3771
0.659
1
17.141
0.000
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
A�tj LL -�LA 2/16/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of L d Applier Date ***C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (SUPP) (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 60.28
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Delois Allen Owner: City of Lumberton Predominant Soil Series: Jo -Johns Sandy
Acres Used: 36.4 Acres Permitted: 36.4 Site #: 1 Field #: NC-RO-17-01
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/17/22
L2J
4/6/22
3j
8/20/22
4
11/17/22
5
6
7
8
9
10
11
12
% Solids
2.41
2.48
2.57
1 2.66
Arsenic
83
11.6
19.3
75.2
Cadmium
20.7
2.02
0.95
18.8
Copper
450
595
523
523
Chromium
4.15
132
235
136
Lead
20.7
21.6
26.8
18.8
Mercury
1.66
0.008
0.33
1.5
Molyb-
denum
20.7
6.66
13.7
13.7
Nickel
83
26.1
54.6
54.6
Selenium
83
8.06
1.95
75.2
Zinc
827
953
890
890
Total
Phos-
horus
20400
17300
5603
15300
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
I 1 I
L2]3
4
5
6
7
8
9
10
11
12
DT/Ac./
0
App.
Event
1.66
Arsenic
1 0.000
0.038
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.038
Cadmium
0.000
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
0.000
1.971
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.971
Chromium
0.000
0.437
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.437
Lead
0.000
0.072
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.072
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.022
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.022
denum
Nickel
0.000
0.086
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.086
Selenium
0.000
0.027
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.027
Zinc
0.000
3.156
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.156
Total
Phos-
0.000
57.298
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
57.298
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
A-,J,j
4j
Signature of Land Applier
2/ 16/2023
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton
Land Owner: City of Lumberton
Operator: Delois Allen
WQ Permit #: WQ0000672 Field #: NC-RO-17-01
Annual Dry Tons Applied: 60.2708 Site #: j
Predominant Soil Series: Jo -Johns San
Crop 1 Name: Soybeans Crop 1 Max. PAN:
174
Crop 2 Name:
Acres Utilized: 36.4
Acres Permitted: 36.4
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
Q
Volume applied
enter one Solids/
( )
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
PP P
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
past 24
Ms.
inches
a
�
o
0 w
o
?:
-
N
��,
� =
TKN
mg/kg
361001
Z a
o
°�
�
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
6/2/22
142600
2.48
0.405
WQ0000672
Dry
0
S
0.5
0.3
6880
806
10.543
NA
Soybeans
6/3/22
148800
2.48
0.423
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
11.002
NA
Soybeans
6/6/22
179800
2.48
0.511
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
13.294
NA
Soybeans
6/9/22
105400
2.48
0.299
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
7.793
NA
Soybeans
6/10/221
6200
1 2.48
0.018
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
0.458
NA
Soybeans
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
5S2SOO
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
43.090
1 0.000
Lime Applied
Annuallbs/acre
0.038
0.007
1.971
0.437
0.072
0.000
0.022
0.086
0.027
3.156 57.298
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.09
0.04
11.175
1.87
0.02
0.624
1.052
0.0178
8.745
1/22
0.64
Current Cumulative lbs/ac
0.128
1 0.047
13.146
0.437
1.942
0.020
0.646
1.138
0.044
11.901
Permitted C. P. L. R.****
1 36
34
1338
1
1 267
1 15
1 N/A
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1
1 174
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/16/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Ozzell Baker
Owner: James Campen Predominant Soil Series:
Acres Permitted: 6 Site #: 17 Field #:
29.49
WaB-Wagram
NC-RO-16-17
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/17/22
2j
4/6/22
3
8/20/22
4j
11/17/22
5
6
7
81
9
0
11
12
% Solids
2.41
2.48
2.57
1 2.66
Arsenic
83
11.6
19.3
75.2
Cadmium
20.7
2.02
0.95
18.8
Copper
450
595
523
523
Chromium
4.15
132
235
136
Lead
20.7
21.6
26.8
18.8
Mercury
1.66
0.008
0.33
1.5
Molyb-
denum
20.7
6.66
13.7
1 13.7
Nickel
83
26.1
54.6
54.6
Selenium
83
8.06
1.95
75.2
Zinc
827
953
890
890
Total
Phos-
horus
20400
17300
5603
15300
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
10
11
12
DT/Ac./
_9L
0
App.
Event
2.03
2.89
Arsenic
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
0.000
0.000
3.018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.018
Chromium
0.000
0.000
1.356
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.356
Lead
0.000
0.000
0.155
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.155
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
5.135
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.135
Total
Phos-
0.000
70.238
32.329
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
102.567
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
ALi Le
�Lj
Signature of Land Applier
2/ 16/2023
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-16-17 Acres Utilized: 6
Land Owner: James Campen
Operator: Ozzell Baker
Crop 1 Name
Bermuda
Annual Dry Tons Applied: 29.4942
Site #: 17
Predominant Soil Series: WaB-Wagram
Crop 1 Max. PAN: 192 Crop 2 Name:
Acres Permitted: 6.0
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
t�
Moist)
Precip.
past 24
Hrs.
inches
>
0 w
o
o
N
°�0
w� `;
w
TKN
mg/kg
Z >
o
ac o
CDNitrite
mg/kg
Nitrate
and
mg/kg
PAN Applied (lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/6/22
86800
2.48
1.496
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
38.934
NA
Bermuda
7/7/22
31000
2.48
0.534
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
13.905
NA
Bermuda
9/l/22
43400
2.48
0.748
WQ0000672
Dry
0
S
0.5
0.3
7549
2074
1988
6.983
NA
Bermuda
9/2/22
124000
2.48
2.137
WQ0000672
Dry
0
S
0.5
0.3
7549
2074
1988
19.951
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
285200
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
79.773
1 0.000
Lime Applied
Annuallbs/acre
0.000
0.000
3.018
1.356
0.155
0.000
0.000
0.000
0.000
5.135
102.567
1
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.196
0.118
37.845
3.94
0.169
0.751
3.02
0.16
32.775
Current Cumulative lbs/ac
0.196
1 0.118
40.863
1.356
4.095
0.169
0.751
3.020
0.160
37.910
Permitted C. P. L. R.****
36
34
1 1338
1
267
15
N/A
374
89
1 2498
Permit PAN Limit 1 st/2nd Crop
1
1 192
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
k1i 44 *Application Method: S - Surface, IN - Injection, INC - Incorporation
2/16/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Sature of Land A rrt;a,- D *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3,
ign
ate
raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 56.42
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Tracy Bullard Owner: Tracy Bullard Predominant Soil Series: Ly-Lynchburg
Acres Used: 14.8 Acres Permitted: 14.8 Site #: 4 Field #: NC-RO-39-04
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/17/22
2j
4/6/22
3
8/20/22
4j
11/17/22
5
6
7
81
9
0
11
12
% Solids
2.41
2.48
2.57
1 2.66
Arsenic
83
11.6
19.3
75.2
Cadmium
20.7
2.02
0.95
18.8
Copper
450
595
523
523
Chromium
4.15
132
235
136
Lead
20.7
21.6
26.8
18.8
Mercury
1.66
0.008
0.33
1.5
Molyb-
denum
20.7
6.66
13.7
1 13.7
Nickel
83
26.1
54.6
54.6
Selenium
83
8.06
1.95
75.2
Zinc
827
953
890
890
Total
Phos-
horus
20400
17300
5603
15300
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
10
11
12
DT/Ac./
_9L
0
App.
Event
3.81
Arsenic
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Chromium
0.000
1.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.006
Lead
0.000
0.165
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.165
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Total
Phos-
0.000
131.895
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
131.895
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/ 16/2023
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-39-04 Acres Utilized: 14.8
Land Owner: Tracy Bullard
Operator: Tracy Bullard
Crop 1 Name: Bermuda
Annual Dry Tons Applied: 56.4238
Site #: 4
Predominant Soil Series: Ly-Lynchburg
Crop 1 Max. PAN: 129 Crop 2 Name:
Acres Permitted: 14.8
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
p
Q
Volume applied
(eater one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
t
Moist)
Precip.
Past 24
11rs.
inches
a
F 2
w
o
o
°�
7
w
°�
TKN
mg/kg
361001
Z a
;
o
ac o
�.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
6/20/22
68200
2.48
0.477
WQ0000672
Dry
0
S
0.5
1 0.3
6880
806
12.402
12.402
6/22/22
99200
2.48
0.693
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
18.039
18.039
6/23/22
93000
2.48
0.650
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
16.912
16.912
6/24/22
93000
2.48
0.650
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
16.912
16.912
6/27/22
124000
2.48
0.866
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
22.549
22.549
6/30/22
68200
2.48
0.477
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
12.402
12.402
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
3.812
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
545600
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
99.214
99.214
Lime Applied
Annuallbs/acre
0.000
0.000
0.000
1.006
0.165
0.000
0.000
0.000
0.000
0.000
131.895
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.001
0
0.023
0.001
0
0
0.002
0.001
0.1
Current Cumulative lbs/ac
0.001
1 0.000
0.023
1.006
0.166
0.000
0.000
0.002
0.001
0.100
Permitted C. P. L. R.****
36
34
1338
267
15
1 N/A
1 374
89
1 2498
Permit PAN Limit 1 st/2nd Crop
129
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/16/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Ronald Hammonds Owner: Ronald Hammonds Predominant Soil Series:
73.2 Acres Permitted: 73.2 Site #:
Field #
349.53
GoA-Goldsboro
NC-RO-20-08
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/17/22
2j
4/6/22
3
8/20/22
4j
11/17/22
5
6
7
81
9
0
11
12
% Solids
2.41
2.48
2.57
1 2.66
Arsenic
83
11.6
19.3
75.2
Cadmium
20.7
2.02
0.95
18.8
Copper
450
595
523
523
Chromium
4.15
132
235
136
Lead
20.7
21.6
26.8
18.8
Mercury
1.66
0.008
0.33
1.5
Molyb-
denum
20.7
6.66
13.7
1 13.7
Nickel
83
26.1
54.6
54.6
Selenium
83
8.06
1.95
75.2
Zinc
827
953
890
890
Total
Phos-
horus
20400
17300
5603
15300
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
10
11
12
DT/Ac./
_9L
0
App.
Event
3.58
1.19
Arsenic
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
3.226
0.000
1.246
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.471
Chromium
0.030
0.000
0.560
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.590
Lead
0.148
0.000
0.064
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.212
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
5.928
0.000
2.120
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
8.048
Total
Phos-
146.227
0.000
13.346
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
159.574
horus
1
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
&kj (?St4 �L4 2/ 16/2023
Signature of Land Applier 0 Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
Facility Name: City of Lumberton
Land Owner: Ronald Hammonds
Operator: Ronald Hammonds
Crop 1 Name: Corn
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
WQ Permit #: WQ0000672 Field #: NC-RO-20-08 Acres Utilized: 73.2
Annual Dry Tons Applied: 349.5176 Site #: 8 Acres Permitted: 73.2
Predominant Soil Series: GoA-Goldsboro Cation Exchange Capacity (non 503):
Crop 1 Max. PAN: 147 Crop 2 Name:
Crop 2 Max. PAN:
U
aLiquid
Volume applied
(enter one) Solids/
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Sod
Cond.
�et
Moist)
Precip.
Past 24
Hrs.
inches
y
rn
0
* °�
o
N'
o'
0
:L
* �'
o
0
TKN
mg/kg
Z
o 5
as o
g �.
mg/kg
Nitrate
and
Nitrite
mgikg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
1/7/22
105400
2.41
0.145
W00000672
Dry
0
S
0.5
0.3
44600
6270
830
4.475
NA
Corn
1/8/22
111600
2.41
0.153
WQ0000672
Dry
0
S
0.5
1 0.3
446001
6270
830
4.739
NA
Corn
1/14/22
31000
2.41
0.043
WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
1.316
NA
Corn
1/26/22
31000
2.41
0.043
WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
1.316
NA
Corn
1/27/22
124000
2.41
0.170
WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
5.265
NA
Corn
1/28/22
136400
2.41
0.187
WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
5.792
NA
Corn
1/31/22
142600
2.41
0.196
WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
6.055
NA
Corn
2/l/22
130200
2.41
0.179
WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
5.528
NA
Corn
2/2/22
124000
2.41
0.170
WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
5.265
NA
Corn
2/3/22
142600
2.41
0.196
WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
6.055
NA
Corn
2/10/22
111600
2.41
0.153
WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
4.739
NA
Corn
2/11/22
99200
2.41
0.136
1 WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
4.212
NA
Corn
2/14/22
99200
2.41
0.136
WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
4.212
NA
Corn
2/15/22
99200
2.41
0.136
W00000672
Dry
0
S
0.5
0.3
44600
6270
830
4.212
NA
Corn
2/16/22
130200
2.41
0.179
WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
5.528
NA
Corn
2/17/22
99200
2.41
0.136
WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
4.212
NA
Corn
2/21/22
93000
2.41
0.128
WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
3.949
NA
Corn
2/22/22
124000
2.41
0.170
1 WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
5.265
NA
Corn
2/23/22
148800
2.41
0.204
WQ0000672
Dry
0
S
1 0.5
0.3
44600
6270
830
6.318
NA
Corn
2/24/22
155000
2.41
0.213
WQ0000672
Dry
0
S
0.5
0.3
44600
1 6270
830
6.582
NA
Corn
3/1/22
105400
2.41
0.145
WQ0000672
Dry
0
S
1 0.5
1 0.3
1446001
6270
830
4.475
NA
Corn
0
1109800
4.775
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
45.138
0.000
TOTALS:
01
3453400
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
144.650
0.000
Lime Applied
Annuallbs/acre
0.000
0.000
4.471
0.590
0.212
0.000
0.000
0.000
0.000
8.048
159.574
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.074
0.003
3.84
1.208
0.01
0.063
0.327
0.093
6.684
11/22
0.54
Current Cumulative lbs/ac
0.074
0.003
8.311
0.590
1.420
0.010
0.063
0.327
0.093
14.732
Permitted C.P. L. R.****
36
34
1338
267
15
N/A
374
89
2498
Permit PAN Limit 1st/2nd Crop
F 147
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/16/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
* * * * C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Supplemental Information
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: W00000672 Field #: NC-RO-20-08 Acres Utilized: 73.2
Land Owner: Ronald Hammonds Annual Dry Tons Applied: 349.5176406 Site #: 8 Acres Permitted: 73.2
Operator: Ronald Hammonds
Crop 1 Name: Corn
Predominant Soil Series: GoA-Goldsboro
Crop 1 Max. PAN: 147.00 Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max PAN:
o +'
Volume applied (enter
one )
Cu. Yds Gallons
111600
o
/o
Solids
2.41
Volume
Applied per
pp p
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
D
Wets
Moist)
Preci p
Past 24
Hrs.
inches
y
ro '5
0 w
cl,o
o
o
`�°
w
o
TKN
mg/kg
44600
Z
o
m o
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
ReceivingResidual
Application
Crop 1
Crop 2
Crop 1
Crop 2
3/2/22
0.153
WQ0000672
Dry
0
S
0.5
0.3
6270
830
4.739
NA
Corn
3/3/22
86800
2.41
0.119
WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
3.686
NA
Corn
3/4/22
68200
2.41
0.094
WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
2.896
NA
Corn
10/5/22
167400
2.48
0.237
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
1988
6.714
NA
Corn
10/6/22
179800
2.48
0.254
WQ0000672
Dry
0
S
1 0.5
0.3
36100
6880
1988
1 7.211
NA
Corn
10/7/22
167400
2.48
0.237
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
1988
6.714
NA
Corn
11/7/22
161200
2.48
0.228
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
1988
6.465
NA
Corn
11/8/22
167400
2.48
0.237
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
1988
6.714
NA
Corn
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
TOTALS:
0
1109800
1.557
45.138
0.0070
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/16/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Lan Applier Date ***C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (SUPP) (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Ronald Hammonds Owner: Charles Brown Predominant Soil Series:
31.2 Acres Permitted: 31.2 Site #: 4 Field #
52.57
WkB-Wakulla
NC-RO-20-4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/17/22
2j
4/6/22
3
8/20/22
4j
11/17/22
5
6
7
81
9
0
11
12
% Solids
2.41
2.48
2.57
1 2.66
Arsenic
83
11.6
19.3
75.2
Cadmium
20.7
2.02
0.95
18.8
Copper
450
595
523
523
Chromium
4.15
132
235
136
Lead
20.7
21.6
26.8
18.8
Mercury
1.66
0.008
0.33
1.5
Molyb-
denum
20.7
6.66
13.7
1 13.7
Nickel
83
26.1
54.6
54.6
Selenium
83
8.06
1.95
75.2
Zinc
827
953
890
890
Total
Phos-
horus
20400
17300
5603
15300
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
10
11
12
DT/Ac./
_9L
0
App.
Event
1.69
Arsenic
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Chromium
0.000
0.445
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.445
Lead
0.000
0.073
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.073
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Total
Phos-
0.000
58.301
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
58.301
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
tw /�R 41
Signature of Land Applier
2/ 15/2023
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton
Land Owner: Charles Brown
Operator: Ronald Hammond
Crop 1 Name: Bermuda
WQ Permit #: WQ0000672 Field #: NC-RO-20-04
Annual Dry Tons Applied: 52.5767 Site #: 4
Predominant Soil Series: wkB-Wakulla
Crop 1 Max. PAN:
147
Crop 2 Name:
Acres Utilized: 31.2
Acres Permitted: 31.2
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
y
Volume applied
enter one Solids/
( )
Liquid
4
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
PP P
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal Waste,
etc)
Soil
Cond.
fin'
Wet,
Moist)
Precip.
past 24
Hrs.
inches
a
o w
°
o
N
`;
w
*
TKN
mg/kg
36100
Z a
o
ac o
CD
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
lbs/acre
( )
Name of Crop Type
ReceivingResidual
Application
PP
Crop 1
Crop 2
Crop 1
Crop 2
4/15/22
161200
2.48
0.534
WQ0000672
Dry
0
S
0.5
0.3
6880
806
13.905
NA
Bermuda
4/16/22
117800
2.48
0.390
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
10.161
NA
Bermuda
4/19/22
37200
2.48
0.123
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
3.209
NA
Bermuda
4/21/22
68200
2.48
0.226
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
5.883
NA
Bermuda
4/22/221
124000
1 2.48
0.411
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
10.696
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
Ar
Cd
Cu
Cr
Pb
Hgy
Mo
Ni
Se
Zn P
43.854
0.000
Lime Applied
Annuallbs/acre
0.000
0.000
0.000
0.445
0.073
0.000
0.000
0.000
0.000
0.000 58.30
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.249
0.078
17.582
1.957
0.038
0.364
2.001
0.183
31.217
1/22
0.869
Current Cumulative lbs/ac
0.249
0.078
17.582
0.445
2.030
0.038
0.364
2.001
0.183
31.217
Permitted C. P. L. R.****
36
34
1 1338
1
1 267
1 15
1 N/A
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1 147
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
`1- "4 *Application Method: S - Surface, IN - Injection, INC - Incorporation
A�Ilj Ll;,�2/16/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land A
Date
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual):
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Delois Allen Owner: City of Lumberton Predominant Soil Series:
Acres Used: 25.4 Acres Permitted: 25.4 Site #: 2 Field #:
167.34
Lu-Lumbee
NC-RO-17-02
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/17/22
2
4/6/22
3_j
8/20/22
4
11/17/22
5
6
_7j
8j
91
LO J
11 j
12
% Solids
2.41
2.48
2.57
1 2.66
Arsenic
83
11.6
19.3
75.2
Cadmium
20.7
2.02
0.95
18.8
Copper
450
595
523
523
Chromium
4.15
132
235
136
Lead
20.7
21.6
26.8
18.8
Mercury
1.66
0.008
0.33
1.5
Molyb-
denum
20.7
6.66
13.7
1 13.7
Nickel
83
26.1
54.6
54.6
Selenium
83
8.06
1.95
75.2
Zinc
827
953
890
890
Total
Phos-
horus
20400
17300
5603
15300
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
91
10
11
12
DT/Ac./
0
App.
Event
6.59
Arsenic
0.000
0.153
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.153
Cadmium
0.000
0.027
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.027
Copper
0.000
7.840
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
7.840
Chromium
0.000
1.739
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.739
Lead
0.000
0.285
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.285
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.088
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.088
denum
Nickel
0.000
0.344
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.344
Selenium
0.000
0.106
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.106
Zinc
0.000
12.557
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
12.557
Total
Phos-
0.000
227.945
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
227.945
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
&_ a /� R _�L4
LeGuoy
Signature of Land Applier
2/16/2023
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton
Land Owner: City of Lumberton
Operator: Delois Allen
Crop 1 Name: Soybeans
WQ Permit #: WQ0000672 Field #: NC-RO-17-02
Annual Dry Tons Applied: 167.3478 Site #: 2
Predominant Soil Series: Lu-Lumbee
Crop 1 Max. PAN:
174
Crop 2 Name:
Acres Utilized: 25.4
Acres Permitted: 25.4
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
Q
Volume applied
enter one Solids/
( )
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
PP P
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
past 24
Ms.
inches
a
�
o
0 w
o
?:
-
N
��,
� =
TKN
mg/kg
361001
Z a
o
°�
�
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/23/22
130200
2.48
0.530
WQ0000672
Dry
0
S
0.5
0.3
6880
806
13.796
NA
Soybeans
4/27/22
43400
2.48
0.177
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
4.599
NA
Soybeans
4/29/22
204600
2.48
0.833
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
21.679
NA
Soybeans
5/2/22
161200
2.48
0.656
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
17.080
NA
Soybeans
5/3/22
1
279000
2.48
1.136
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
29.562
NA
Soybeans
5/4/22
341000
2.48
1.388
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
36.131
NA
Soybeans
5/5/22
328600
2.48
1.338
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
34.817
NA
Soybeans
5/6/22
130200
2.48
0.530
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
1 13.796
NA
Soybeans
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
161S200
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
171.4591
0.000
Lime Applied
Annuallbs/acre
0.153
0.027
7.840
1.739
0.285
0.000
0.088
0.344
0.106
12.557 227.945
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.16
0.087
20.128
1.667
0.035
0.419
1.969
0.193
20.616
1/22
0.64
Current Cumulative lbs/ac
0.313
0.114
27.968
1.739
1.952
0.035
0.507
2.313
0.299
33.173
Permitted C. P. L. R.****
36
34
1338
1
1 267
1 15
1 N/A
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1 174
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
(-�wI ,4 *Application Method: S - Surface, IN - Injection, INC - Incorporation
�2/16/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Ozzell Baker
12.3
Owner: James Campen Predominant Soil Series:
Acres Permitted: 12.3 Site #: 18 Field #:
44.88
WaB-Wagram
NC-RO-16-18
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/17/22
2j
4/6/22
3
8/20/22
4j
11/17/22
5
6
7
81
9
0
11
12
% Solids
2.41
2.48
2.57
1 2.66
Arsenic
83
11.6
19.3
75.2
Cadmium
20.7
2.02
0.95
18.8
Copper
450
595
523
523
Chromium
4.15
132
235
136
Lead
20.7
21.6
26.8
18.8
Mercury
1.66
0.008
0.33
1.5
Molyb-
denum
20.7
6.66
13.7
1 13.7
Nickel
83
26.1
54.6
54.6
Selenium
83
8.06
1.95
75.2
Zinc
827
953
890
890
Total
Phos-
horus
20400
17300
5603
15300
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
10
11
12
DT/Ac./
_9L
0
App.
Event
2.09
1.56
Arsenic
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
0.000
0.000
1.636
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.636
Chromium
0.000
0.550
0.735
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.286
Lead
0.000
0.090
0.084
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.174
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
2.784
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.784
Total
Phos-
0.000
72.141
17.526
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
89.667
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
A�jj uz', 44
Signature of Land Applier
2/ 16/2023
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
Facility Name: City of Lumberton
Land Owner: James Campen
Operator: Ozzell Baker
Crop 1 Name: Bermuda
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
WQ Permit #: WQ0000672 Field #: NC-RO-16-18 Acres Utilized: 12.3
Annual Dry Tons Applied: 44.8825 Site #: 18 Acres Permitted: 12.3
Predominant Soil Series: WaB-Wagram
Crop 1 Max. PAN: 192 Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o y
[�
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Cod
may'
Wet,
Moist)
Precip.
Past 24
Hrs.
inches
o
rn "'
o w'
+ o
Z
o
� �
N
°�
w w
TKN
mg/kg
Z. >
� O
rn '�
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/7/22
99200
2.48
0.834
W00000672
Dry
0
S
0.5
0.3
36100
6880
806
21.705
NA
Bermuda
7/8/22
117800
2.48
0.990
W00000672
Dry
0
S
0.5
0.3
36100
6880
806
25.775
NA
Bermuda
7/12/22
31000
2.48
0.261
W00000672
Dry
0
S
0.5
0.3
36100
6880
806
6.783
NA
Bermuda
9/2/22
31000
2.48
0.261
W00000672
Dry
0
S
0.5
0.3
7549
2074
1988
2.433
NA
Bermuda
9/7/22
155000
2.48
1.303
W00000672
Dry
0
S
0.5
0.3
7549
2074
1988
12.165
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
434000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
68.862
0.000
Lime Applied
Annuallbs/acre
0.000
0.000
1.636
1.286
0.174
0.000
0.000
0.000
0.000
2.784
89.667
.<
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.282
0.127
44.95
4.36
0.047
0.777
3.11
0.257
41.931
Current Cumulative lbs/ac
0.282
0.127
46.586
1.286
4.534
0.047
0.777
3.110
0.257
44.715
Permitted C. P. L. R.****
36
34
1338
267
15
N/A
374
89
2498
Permit PAN Limit 1st/2nd Crop
F 192
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
i r A le j 2/16/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
* * * *C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 126.31
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Tracy Bullard Owner: Tracy Bullard Predominant Soil Series: Wab-Wagram
Acres Used: 62.5 Acres Permitted: 62.5 Site #: 9 Field #: NC-RO-39-09
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/17/22
2j
4/6/22
3
8/20/22
4j
11/17/22
5
6
7
81
9
0
11
12
% Solids
2.41
2.48
2.57
1 2.66
Arsenic
83
11.6
19.3
75.2
Cadmium
20.7
2.02
0.95
18.8
Copper
450
595
523
523
Chromium
4.15
132
235
136
Lead
20.7
21.6
26.8
18.8
Mercury
1.66
0.008
0.33
1.5
Molyb-
denum
20.7
6.66
13.7
1 13.7
Nickel
83
26.1
54.6
54.6
Selenium
83
8.06
1.95
75.2
Zinc
827
953
890
890
Total
Phos-
horus
20400
17300
5603
15300
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
10
11
12
DT/Ac./
_9L
0
App.
Event
2.02
Arsenic
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Chromium
0.000
0.534
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.534
Lead
0.000
0.087
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.087
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Total
Phos-
0.000
69.927
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
69.927
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
&kj �_e� 41 2/ 16/2023
Signature of Land ApplicrU Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-39-09 Acres Utilized: 62.5
Land Owner: Tracy Bullard
Operator: Tracy Bullard
Crop 1 Name: Bermuda
Annual Dry Tons Applied: 126.3123
Site #: 9
Predominant Soil Series: WaB-Wagram
Crop 1 Max. PAN: 192 Crop 2 Name:
Acres Permitted: 62.5
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
p
Q
Volume applied
(eater one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
t
Moist)
Precip.
Past 24
11rs.
inches
a
F 2
w
o
o
°�
7
w
°�
TKN
mg/kg
Z a
;
o
ac o
�.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/18/22
117800
2.48
0.195
WQ0000672
Dry
0
S
0.5
1 0.3
36100
1 6880
806
5.073
NA
Bermuda
7/19/22
99200
2.48
0.164
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
4.272
NA
Bermuda
7/20/22
105400
2.48
0.174
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
4.539
NA
Bermuda
7/21/22
93000
2.48
0.154
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
4.005
NA
Bermuda
7/25/22
80600
2.48
0.133
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
3.471
NA
Bermuda
7/26/22
86800
2.48
0.144
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
3.738
NA
Bermuda
7/27/22
93000
2.48
0.154
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
4.005
NA
Bermuda
7/28/22
117800
2.48
0.195
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
5.073
NA
Bermuda
7/29/22
62000
2.48
0.103
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
2.670
NA
Bermuda
8/l/22
136400
2.48
0.226
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
5.873
NA
Bermuda
8/2/22
117800
2.48
0.195
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
5.073
NA
Bermuda
8/3/22
111600
2.48
0.185
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
4.806
NA
Bermuda
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
1221400
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
52.594
o.000
Lime Applied
Annuallbs/acre
0.000
0.000
0.000
0.534
0.087
0.000
0.000
0.000
0.000
0.000
69.927
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.03
0.002
7.196
0.692
0.004
0.082
0.456
0.036
13.331
Current Cumulative lbs/ac
0.030
1 0.002
7.196
0.534
0.779
0.004
0.082
0.456
0.036
13.331
Permitted C. P. L. R.****
36
34
1 1338
267
15
1 N/A
1 374
89
1 2498
Permit PAN Limit 1 st/2nd Crop
192
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
l� *Application Method: S - Surface, IN - Injection, INC - Incorporation
2/16/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 370.25
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Carrell Locklear Owner: Robert Baskersville Predominant Soil Series: GoA
Acres Used: 56.9 Acres Permitted: 56.9 Site #: 2 Field #: NC-RO-28-2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/17/22
2
4/6/22
3
8/20/22
4
11/17/22
5
6
7
8
9
10 j
11
12
% Solids
2.41
2.48
2.57
1 2.66
Arsenic
83
11.6
19.3
75.2
Cadmium
20.7
2.02
0.95
18.8
Copper
450
595
523
523
Chromium
4.15
132
235
136
Lead
20.7
21.6
26.8
18.8
Mercury
1.66
0.008
0.33
1.5
Molyb-
denum
20.7
6.66
13.7
13.7
Nickel
83
26.1
54.6
54.6
Selenium
83
8.06
1.95
75.2
Zinc
827
953
890
890
Total
Phos-
horus
20400
17300
5603
15300
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
10
11
12
DT/Ac./
_9L
App.
Event
2.17
0.76
3.58
Arsenic
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
1.951
0.000
3.749
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.700
Chromium
0.018
0.199
1.684
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.902
Lead
0.090
0.000
0.192
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.282
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
3.586
0.000
6.380
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
9.965
Total
Phos-
88.454
26.123
40.162
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
154.740
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for
knowing violations".
U 2/16/2023
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: W00000672 Field #: NC-RO-28-2 Acres Utilized: 56.9
Land Owner: Robert Baskerville Annual Dry Tons Applied: 370.2241 Site #: 2 Acres Permitted:
Operator: Carnell Locklear
Crop 1 Name: Corn
Predominant Soil Series: Goldsboro GoA
Crop 1 Max. PAN: 147
Crop 2 Name:
Cation Exchange Capacity (non 503):
Wheat Crop 2 Max. PAN:
56.9
135
p =
�'
-2
Volume applied
(enter one) Solids/
Li uid
4
Cu. Yds Gallons
142600
%
Solids
2.41
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
Past 24
ems-
inches
a
4 �
"
*
o
CD .�
# N
o'
p
4
5
aY ,
`D
*
* o
TKN
mg/kg
44600
Z
F7 1
o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
PP
Crop 1
Crop 2
Crop 1
Crop 2
3/7/22
0.252
WQ0000672
Dry
0
S
0.5
0.3
6270
830
7.790
NA
Corn
3/8/22
179800
2.41
0.318
WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
9.822
NA
Corn
3/15/22
173600
2.41
0.307
WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
9.483
NA
Corn
3/16/22
186000
2.41
0.329
WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
10.160
NA
Corn
3/21/221
117800
2.41
0.208
WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
6.435
NA
Corn
3/22/22
117800
2.41
0.208
WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
6.435
NA
Corn
3/23/22
68200
2.41
0.120
WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
3.725
NA
Corn
3/28/22
161200
2.41
0.285
WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
8.806
NA
Corn
3/29/22
80600
2.41
1 0.142
WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
4.403
1 NA
Corn
4/4/22
1
105400
2.48
0.192
WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
5.925
NA
Corn
4/5/22
117800
2.48
0.214
WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
6.622
NA
Corn
4/11/22
192200
2.48
0.349
WQ0000672
Dry
0
S
0.5
0.3
44600
6270
830
10.804
NA
Corn
0
1971600
3.583
Residuals Applications totals on FORM FSF supp ( attach FORM
FSF supp to this form):
0.000
40.340
TOTALS:
01
3614600
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
90.408
40.340
Lime A lied
Annuallbs/acre
0.000
0.000
5.700
1.902
0.282
0.000
0.000
0.000
0.000
9.965 154.7401
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.061
0.012
3.569
0.236
0.006
0.066
0.501
0.062
4.955
11/22
0.59
Current Cumulative lbs/ac
0.061
0.012
9.269
1.902
0.518
0.006
0.066
0.501
0.062
14.920
Permitted C. P. L. R.****
0.061
34
1 1998
267
15
1 N/A
374
89
2498
Permit PAN Limit I st/2nd Crop1
147 135
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including
the possibility of fines and imprisonment for knowing violations."
Q `� *Application Method: S - Surface, IN - Injection, INC - Incorporation
2/16/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier
Date
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically
digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Supplemental Information
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: W00000672 Field #: NC-RO-28-2 Acres Utilized: 56.9
Land Owner: Robert Baskerville Annual Dry Tons Applied: 370.2241092 Site #: 2 Acres Permitted: 56.9
Operator: Carnell Locklear
Crop 1 Name:
Corn
Predominant Soil Series: Goldsboro GoA
Crop 1 Max. PAN: 147.00 Crop 2 Name:
Cation Exchange Capacity (non 503):
Wheat Crop 2 Max PAN:
135
o
o
Volume applied (enter
one)
Cu. Yds G8110nS
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
NPDES #, W #,
( Q
Fert., Animal
Waste, etc)
Soil
Cond.
D
( ry'
Wet'
Moist)
Precip.
Past 24
Hrs.
inches
y
a
a '�
Ex
o w
o
°�
o
n N'
o'
CD
m
co N'
o'
TKN
mg/kg
Z
o
ua o
m'
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
9/8/22
173600
2.48
0.316
WQ0000672
Dry
0
S
0.5
0.3
7549
6880
1988
Na
3.552
Wheat
9/9/22
173600
2.48
0.316
WQ0000672
Dry
0
S
0.5
0.3
7549
6880
1988
Na
3.552
Wheat
9/13/22
186000
2.48
0.338
WQ0000672
Dry
0
S
0.5
0.3
7549
6880
1988
Na
3.806
Wheat
9/14/22
167400
2.48
0.304
WQ0000672
Dry
0
S
0.5
0.3
7549
6880
1988
Na
3.425
Wheat
9/15/221
179800
2.48
0.327
WQ0000672
Dry
0
S
0.5
0.3
7549
6880
1988
Na
3.679
Wheat
9/16/22
148800
2.48
0.270
WQ0000672
Dry
0
S
0.5
0.3
7549
6880
1988
Na
3.045
Wheat
9/19/22
173600
2.48
0.316
WQ0000672
Dry
0
S
0.5
0.3
7549
6880
1988
Na
3.552
Wheat
9/20/22
186000
2.48
0.338
WQ0000672
Dry
0
S
0.5
0.3
7549
6880
1988
Na
3.806
Wheat
9/21/22
142600
2.48
0.259
WQ0000672
Dry
0
S
0.5
0.3
7549
6880
1988
Na
2.918
Wheat
9/22/221
117800
2.48
0.214
WQ0000672
Dry
0
S
0.5
0.3
7549
6880
1988
Na
2.410
Wheat
9/23/22
148800
2.48
0.270
WQ0000672
Dry
0
S
0.5
0.3
7549
6880
1988
Na
3.045
Wheat
9/26/22
173600
2.48
0.316
WQ0000672
Dry
0
S
0.5
0.3
7549
6880
1988
Na
3.552
Wheat
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
TOTALS:
0
1977671
3.583
0.000
40.340
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
2/16/2022
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (SUPP) (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Ronald G. Hammonds Owner: Ronald G Hammonds Predominant Soil Series:
13 Acres Permitted: 13 Site #:
Field #
42.32
GoA-Goldsboro
NC-RO-20-07
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/17/22
2j
4/6/22
3
8/20/22
4j
11/17/22
5
6
7
81
9
0
11
12
% Solids
2.41
2.48
2.57
1 2.66
Arsenic
83
11.6
19.3
75.2
Cadmium
20.7
2.02
0.95
18.8
Copper
450
595
523
523
Chromium
4.15
132
235
136
Lead
20.7
21.6
26.8
18.8
Mercury
1.66
0.008
0.33
1.5
Molyb-
denum
20.7
6.66
13.7
1 13.7
Nickel
83
26.1
54.6
54.6
Selenium
83
8.06
1.95
75.2
Zinc
827
953
890
890
Total
Phos-
horus
20400
17300
5603
15300
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
10
11
12
DT/Ac./
_9L
0
App.
Event
1.83
1.43
Arsenic
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
0.000
0.000
1.496
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.496
Chromium
0.000
0.482
0.672
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.154
Lead
0.000
0.079
0.077
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.155
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
2.545
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.545
Total
Phos-
0.000
63.145
16.025
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
79.170
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/ 16/2023
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-20-07 Acres Utilized: 13
Land Owner: Ronald G. Hammonds Annual Dry Tons Applied: 42.3178 Site #: 7 Acres Permitted: 13
Operator: Ronald G. Hammonds Predominant Soil Series: GoA-Goldsboro Cation Exchange Capacity (non 503):
Crop 1 Name: Corn Crop 1 Max. PAN: 147 Crop 2 Name: Crop 2 Max. PAN:
Q
Volume applied
enter one Solids/
( )
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
PP � P
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
past 24
Ms.
inches
a
S
o
0 w
* °�
o
?:
� �
-
N
o
��,
=
N
o
TKN
mg/kg
Z a
o �
°�
�
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
9/28/22
24800
2.48
0.197
WQ0000672
Dry
0
S
0.5
0.3
7549
2074
1988
1.842
NA
Corn
9/29/22
204600
2.48
1.628
WQ0000672
Dry
0
S
0.5
0.3
7549
2074
1988
15.194
NA
Corn
10/3/22
179800
2.48
1.430
WQ0000672
Dry
0
S
0.5
0.3
7549
2074
1988
13.352
NA
Corn
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
409200
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
30.387
1 0.000
Lime Applied
Annuallbs/acre
0.000
0.000
1.496
1.154
0.155
0.000
0.000
0.000
0.000
2.545
79.170
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.05
0.006
4.093
1.758
0.003
0.767
0.559
0.048
9.417
11/22
0.54
Current Cumulative lbs/ac
0.050
0.006
5.589
1.154
1.913
0.003
0.767
0.559
0.048
11.962
Permitted C. P. L. R.****
1 36
34
1 1338
267
1 15
1 N/A
374
1 89
2498
Permit PAN Limit 1 st/2nd Crop
1
1 147
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
r I *Application Method: S - Surface, IN - Injection, INC - Incorporation
t�w�J( 2/16/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Ronald Hammonds Owner: Ronald Hammonds Predominant Soil Series:
24.9 Acres Permitted: 24.9 Site #:
Field #
79.51
WkB-Wakulla
NC-RO-20-03
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/17/22
2j
4/6/22
3
8/20/22
4j
11/17/22
5
6
7
81
9
0
11
12
% Solids
2.41
2.48
2.57
1 2.66
Arsenic
83
11.6
19.3
75.2
Cadmium
20.7
2.02
0.95
18.8
Copper
450
595
523
523
Chromium
4.15
132
235
136
Lead
20.7
21.6
26.8
18.8
Mercury
1.66
0.008
0.33
1.5
Molyb-
denum
20.7
6.66
13.7
1 13.7
Nickel
83
26.1
54.6
54.6
Selenium
83
8.06
1.95
75.2
Zinc
827
953
890
890
Total
Phos-
horus
20400
17300
5603
15300
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
10
11
12
DT/Ac./
_9L
0
App.
Event
3.19
Arsenic
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Chromium
0.000
0.843
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.843
Lead
0.000
0.138
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.138
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Total
Phos-
0.000
110.478
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
110.478
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
A�tj (?�,4 4j
Signature of Land Applier
2/ 16/2023
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton
Land Owner: Ronald Hammonds
Operator: Ronalld Hammonds
Crop 1 Name: Bermuda
WQ Permit #: WQ0000672 Field #: NC-RO-20-03
Annual Dry Tons Applied: 79.5062 Site #: 3
Predominant Soil Series: Wkb-Wakulla
Crop 1 Max. PAN:
110.25
Crop 2 Name:
Acres Utilized: 24.9
Acres Permitted: 24.9
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
Q
Volume applied
enter one Solids/
( )
Liquid
Cu. Yds Gallons
80600
o
/o
Solids
Volume
Applied per
pP P
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
past 24
Ms.
inches
a
o
0 w
o
?:
-
N
h
� =
N
TKN
mg/kg
36100
Z a
o
°�
�
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/25/22
r 2.48
0.335
WQ0000672
Dry
0
S
0.5
0.3
r 6880
806
8.712
NA
Bermuda
4/26/22
105400
2.48
0.438
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
11.392
NA
Bermuda
4/29/22
80600
2.48
0.335
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
8.712
NA
Bermuda
5/2/22
117800
2.48
0.489
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
12.732
NA
Bermuda
5/3/22
93000
2.48
1 0.386
WQ0000672
Dry
0
1 S
0.5
0.3
36100
6880
1 806
10.052
NA
Bermuda
5/16/22
291400
2.48
1.210
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
31.496
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
76SSO(
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
83.095
1 0.000
Lime Applied
Annuallbs/acre
0.000
0.000
0.000
0.843
0.138
0.000
0.000
0.000
0.000
0.000
110.478
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.15
0.062
12.305
2.036
0.026
0.261
1.433
0.13
22.131
1/22
0.869
Current Cumulative lbs/ac
0.150
0.062
12.305
0.843
2.174
0.026
0.261
1.433
0.130
22.131
Permitted C. P. L. R.****
36
34
1 1338
267
1 15
374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1
1 110.25
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
A
n *Application Method: S - Surface, IN - Injection, INC - Incorporation
tJ (' L42/16/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of LaiM Applier
Date
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual):
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Delois Allen Owner: City of Lumberton Predominant Soil Series:
Acres Used: 28 Acres Permitted: 28 Site #: 3 Field #:
175.67
Lu-Lumbee
NC-RO-17-03
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/17/22
2
4/6/22
3
8/20/22
4
11/17/22
5
6
7
8
9
I Oj
11 j
12
% Solids
2.41
2.48
2.57
1 2.66
Arsenic
83
11.6
19.3
75.2
Cadmium
20.7
2.02
0.95
18.8
Copper
450
595
523
523
Chromiurn
4.15
132
235
136
Lead
20.7
21.6
26.8
18.8
Mercury
1.66
0.008
0.33
1.5
Molyb-
denum
20.7
6.66
13.7
13.7
Nickel
83
26.1
54.6
54.6
Selenium
83
8.06
1.95
75.2
Zinc
827
953
890
890
Total
Phos-
hones
20400
17300
5603
15300
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
91
10
11
12
DT/Ac./
App.
14
Event
6.27
Arsenic
0.000
1 0.146
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.146
Cadmium
0.000
0.025
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.025
Copper
0.000
7.466
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
7.466
Chromium
0.000
1.656
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.656
Lead
0.000
0.271
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.271
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.084
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.084
denum
Nickel
0.000
0.328
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.328
Selenium
0.000
0.101
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.101
Zinc
0.000
1 11.958
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
11.958
Total
Phos-
0.000
217.080
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
217.080
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/ 16/2023
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
Facility Name: City of Lumberton
Land Owner: City of Lumberton
Operator: Delois Allen
Crop 1 Name: Soybeans
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
WQ Permit #: WQ0000672 Field #: NC-RO-17-03
Annual Dry Tons Applied: 175.6831 Site #: 3
Predominant Soil Series: Lu-Lumbee
Crop 1 Max. PAN:
174
Crop 2 Name:
Acres Utilized: 28
Acres Permitted: 28
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
C) =
Q
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
Past 24
ems-
inches
a
4 �
c�
"
*
o
,.d
CD .�
* w
o'
p
4
aY ,
co �
*
* o
TKN
mg/kg
36100
Z
F7 I
o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
PP
Crop 1
Crop 2
Crop 1
Crop 2
4/12
204600
2.48
0.756
WQ0000672
Dry
0
S
0.5
0.3
6880
806
19.666
NA
Soybeans
4/13
179800
2.48
0.664
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
17.282
NA
Soybeans
4/14
192200
2.48
0.710
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
18.474
NA
Soybeans
4/19
99200
2.48
0.366
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
9.535
NA
Soybeans
4/20
1
241800
2.48
0.893
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
23.241
NA
Soybeans
4/21
155000
2.48
0.572
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
14.898
NA
Soybeans
4/25
93000
2.48
0.343
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
8.939
NA
Soybeans
4/27
260400
2.48
0.962
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
25.029
NA
Soybeans
4/28
272800
2.48
1 1.008
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
26.221
NA
Soybeans
0.000
0.000
0.000
0.000
+-4
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
1698800
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
163.285
0.000
Lime Applied
Annuallbs/acre
0.146
0.025
7.466
1.656
0.271
0.000
0.084
0.328
0.101
11.958 217.080
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.1
0.06
9.674
0.494
0.012
0.192
0.963
0.14
15.75
1/22
0.64
Current Cumulative lbs/ac
0.246
0.085
17.140
1.656
0.765
0.012
0.276
1.291
0.241
27.708
Permitted C. P. L. R.****
36
34
1 1338
267
1 15
1 N/A
374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1 174
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
2/16/2023
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Ozzell Baker
1.6
Owner: James Campen Predominant Soil Series:
Acres Permitted: 1.6 Site #: 19 Field #:
7.69
WaB-Wagram
NC-RO-16-19
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/17/22
2j
4/6/22
3
8/20/22
4j
11/17/22
5
6
7
81
9
0
11
12
% Solids
2.41
2.48
2.57
1 2.66
Arsenic
83
11.6
19.3
75.2
Cadmium
20.7
2.02
0.95
18.8
Copper
450
595
523
523
Chromium
4.15
132
235
136
Lead
20.7
21.6
26.8
18.8
Mercury
1.66
0.008
0.33
1.5
Molyb-
denum
20.7
6.66
13.7
1 13.7
Nickel
83
26.1
54.6
54.6
Selenium
83
8.06
1.95
75.2
Zinc
827
953
890
890
Total
Phos-
horus
20400
17300
5603
15300
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
10
11
12
DT/Ac./
_9L
0
App.
Event
2.00
2.81
Arsenic
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
0.000
0.000
2.934
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.934
Chromium
0.000
0.000
1.318
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.318
Lead
0.000
0.000
0.150
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.150
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
4.993
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.993
Total
Phos-
0.000
69.338
31.433
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
100.771
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applies
2/ 16/2023
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton
Land Owner: James Campen
Operator: Ozzell Baker
Crop 1 Name:
Bermuda
WQ Permit #: WQ0000672 Field #: NC-RO-16-19
Annual Dry Tons Applied: 7.6942 Site #: 19
Predominant Soil Series: WaB-Wagram
Crop 1 Max. PAN: 192 Crop 2 Name:
Acres Utilized: 1.6
Acres Permitted: 1.6
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
Q
Volume applied
enter one Solids/
� )
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
PP � P
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
past 24
Ms.
inches
a
S
o
0 w
o
?:
� �
-
N
��,
=
TKN
mg/kg
Z a
o �
°�
�
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/12/22
24800
2.48
1.603
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
41.715
NA
Bermuda
7/15/22
6200
2.48
0.401
WQ0000672
Dry
0
S
0.5
0.3
36100
6880
806
10.429
NA
Bermuda
9/8/22
43400
2.48
2.805
WQ0000672
Dry
0
S
0.5
0.3
7549
2074
1988
26.186
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
74400
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
78.330
1 0.000
Lime Applied
Annuallbs/acre
0.000
0.000
2.934
1.318
0.150
0.000
0.000
0.000
0.000
4.993 100.771
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.153
0.12
39.48
4.905
0.236
0.388
2.401
0.612
24.46
Current Cumulative lbs/ac
0.153
0.120
42.414
1.318
5.055
0.236
0.388
2.401
0.612
29.453
Permitted C. P. L. R.****
36
34
1 1338
267
1 15
1 N/A
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1 192
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
(1 *Application Method: S - Surface, IN - Injection, INC - Incorporation
�( 2/16/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
ki Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

13
ace Analytical ' ANALYTICAL REPORT
March 10, 2022
Hunt Environmental Associates
Sample Delivery Group: L1463165
Samples Received: 02/18/2022
Project Number:
Description: Enviro-Choice Recycling
Report To: Cody Hunt
3330 Saddletree Road
Lumberton, NC 28359
Entire Report Reviewed By: q�"h
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1463165 03/10/22 09:13 1 of 59

TABLE OF CONTENTS
Cp: Cover Page
FP
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
Fss]
WW-1 L1463165-01
5
Fn
WW-1 L1463165-02
7
WW-1 L1463165-03
9
Fr
Qc: Quality Control Summary
11
Total Solids by Method 2540 G-2011
11
Rc
Wet Chemistry by Method 350.1
12
F
Wet Chemistry by Method 351.2
14
Wet Chemistry by Method 353.2
15
[Al
Wet Chemistry by Method 365.4
16
Wet Chemistry by Method 365.4M
17
RC
Wet Chemistry by Method 4500 CN E-2016
18
Wet Chemistry by Method 4500 S2 D-2011
19
Wet Chemistry by Method 4500H+ B-2011
20
Wet Chemistry by Method 4500NOrg C-2011
21
Wet Chemistry by Method 9012B
22
Wet Chemistry by Method 9045D
23
Wet Chemistry by Method 9056A
24
Wet Chemistry by Method D93/1010A
25
Mercury by Method 245.1
27
Mercury by Method 7470A
28
Mercury by Method 7471B
29
Metals (ICP) by Method 200.7
30
Metals (ICP) by Method 6010D
32
Volatile Organic Compounds (GC/MS) by Method 8260D
36
Chlorinated Acid Herbicides (GC) by Method 8151A
38
Pesticides (GC) by Method 8081B
39
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
40
GI: Glossary of Terms
42
Al: Accreditations & Locations
44
Sc: Sample Chain of Custody
45
ACCOUNT: PROJECT: SDG:
DATE/TIME:
PAGE:
Hunt Environmental Associates L1463165
03/10/22 09:13
2 of 59

SAMPLE SUMMARY
Collected by Collected date/time Received date/time
WW-1 L1463165-01 WW Carrigan Harris 02/17/2210:30 02/18/22 09:30
Method
Wet Chemistry by Method 350.1
Wet Chemistry by Method 351.2
Wet Chemistry by Method 353.2
Wet Chemistry by Method 365.4
Wet Chemistry by Method 4500 CN E-2016
Wet Chemistry by Method 4500 S2 D-2011
Wet Chemistry by Method 4500H+ B-2011
Wet Chemistry by Method D93/1010A
Mercury by Method 245.1
Metals (ICP) by Method 200.7
Metals (ICP) by Method 200.7
WW-1 L1463165-02 Waste
Method
Preparation by Method 1311
Preparation by Method 1311
Mercury by Method 7470A
Metals (ICP) by Method 6010D
Volatile Organic Compounds (GC/MS) by Method 8260D
Chlorinated Acid Herbicides (GC) by Method 8151A
Pesticides (GC) by Method 8081B
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WW-1 L1463165-03 Solid
Method
Total Solids by Method 2540 G-2011
Wet Chemistry by Method 350.1
Wet Chemistry by Method 365.4M
Wet Chemistry by Method 4500NOrg C-2011
Wet Chemistry by Method 9012B
Wet Chemistry by Method 9045D
Wet Chemistry by Method 9056A
Wet Chemistry by Method D93/1010A
Mercury by Method 7471B
Metals (ICP) by Method 6010D
Subcontracted Analyses
Batch
WG1823467
WG1824691
WG1823045
WG1828980
WG1821200
WG1820714
WG1820604
WG1821032
WG1821092
WG1820696
WG1820696
Batch
WG1822928
WG1823891
WG1824898
WG1824957
WG1824485
WG1825661
WG1825495
WG1824791
Batch
WG1823409
WG1821201
WG1821989
WG1828073
WG1821197
WG1821960
WG1821500
WG1821036
WG1820889
WG1820840
WG1822438
Dilution
Preparation
date/time
20
02/25/2217:51
20
03/03/22 2111
5
03/07/22 00:06
1
03/03/22 2111
50
02/21/22 2144
50
02/21/2212:54
1
02/22/2210:00
1
02/21/22 0100
10
02/22/22 09:17
1
02/20/22 07:50
50
02/20/22 07:50
Collected by
Carrigan Harris
Dilution Preparation
date/time
1 02/24/2214:03
1 02/26/22 09:26
1 02/28/2212:29
1 02/28/2213:46
1 02/27/2218:01
1 03/02/22 08:02
1 03/02/22 08:42
1 03/04/22 06:25
Collected by
Carrigan Harris
Dilution Preparation
date/time
1 02/24/22 20:54
1 02/22/2212:27
5 02/27/2218:04
5 02/22/221103
1 02/21/22 2138
1 02/22/2214:00
1 02/21/22 2102
1 02/21/22 0100
1 02/22/22 08:43
1 02/20/2212:04
1 03/02/22 00:00
Analysis
Analyst
Location
date/time
02/25/2217:51
SL
Mt. Juliet, TN
03/08/2213:10
LDT
Mt. Juliet, TN
03/07/22 00:06
CAT
Mt. Juliet, TN
03/08/2213:01
LDT
Mt. Juliet, TN
02/22/2214:42
LDT
Mt. Juliet, TN
02/21/2212:54
PSN
Mt. Juliet, TN
02/22/2210:00
GI
Mt. Juliet, TN
02/21/22 0100
WOS
Mt. Juliet, TN
02/23/2213:08
MRW
Mt. Juliet, TN
02/21/2216:26
ZSA
Mt. Juliet, TN
02/22/2212:02
ZSA
Mt. Juliet, TN
Collected date/time Received date/time
02/17/2210:30 02/18/22 09:30
Analysis
Analyst
Location
date/time
02/24/2214:03
JWS
Mt. Juliet, TN
02/26/22 09:26
JWS
Mt. Juliet, TN
03/02/22 08:52
ABL
Mt. Juliet, TN
03/01/2210:16
ZSA
Mt. Juliet, TN
02/27/22 18:01
BMB
Mt. Juliet, TN
03/02/2219:40
CCW
Mt. Juliet, TN
03/02/2214:48
AO
Mt. Juliet, TN
03/04/2216:17
LEA
Mt. Juliet, TN
Collected date/time Received date/time
02/17/2210:30 02/18/22 09:30
Analysis
date/time
02/24/22 2110
02/22/2217:25
03/08/2217:31
03/06/2212:35
02/22/2213:46
02/23/22 09:00
02/22/22 02:41
02/21/22 0100
02/23/2213:16
02/21/22 20:38
03/02/22 00:00
Analyst
BRG
LDT
LDT
MCG
LDT
GI
RAF
WOS
MRW
CCE
Location
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Subcontract
FP
FC
w
Fn
Fr
Rc
�GI
SAI
RC
ACCOUNT: PROJECT: SDG:
Hunt Environmental Associates L1463165
DATE/TIME:
03/10/22 09:13
PAGE:
3 of 59

CASE NARRATIVE
FP
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
0
Fr
Rc
4�z
F,
Heather J Wagner
[Al
Project Manager
RC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 4500 CN E-2016.
All Reactive Sulfide results reported in the attached report were determined as totals using method 4500 S2 D-2011.
L1463165 -03 contains subout data that is included after the chain of custody.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1463165 03/10/22 09:13 4 of 59

SAMPLE RESULTS - 01
L1463165
WW-1
Collected date/time: 02/17/22 10:30
Wet Chemistry by Method 350.1
Result
Qualifier RDL
Analyte mg/I
mg/I
Ammonia Nitrogen 120
5.00
Wet Chemistry by Method 351.2
Result
Qualifier RDL
Analyte mg/I
mg/I
Kjeldahl Nitrogen, TKN 228
5.00
Wet Chemistry by Method 353.2
Dilution Analysis Batch
date / time
20 02/25/202217:51 WG1823467
Dilution Analysis Batch
date / time
20 03/08/202213:10 WG1824691
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date / time
Nitrate -Nitrite ND
0.500
5 03/07/2022 00:06 WG1823045
Sample Narrative:
L1463165-01 WG1823045: Dilution due to iron hit.
Wet Chemistry by Method 365.4
Result Qualifier
RDL
Dilution Analysis Batch
Analyte mg/I
mg/I
date / time
Phosphorus, Total 1.42
0.100
1 03/08/202213:01 WG1828980
Wet Chemistry by Method 4500 CN E-2016
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date / time
Reactive Cyanide ND 0.250 50 02/22/202214:42 WG1821200
Wet Chemistry by Method 4500 S2 D-2011
Result Qualifier RDL
Analyte mg/I mg/I
Reactive Sulfide 32.9 2.50
Wet Chemistry by Method 4500H+ B-2011
Dilution Analysis Batch
date / time
50 02/21/202212:54 WG1820714
Result Qualifier Dilution Analysis Batch
Analyte su date / time
pH 7.07 T8 1 02/22/202210:00 WG1820604
Sample Narrative:
L1463165-01 WG1820604: 7.07 at 24.5C
Wet Chemistry by Method D93/1010A
Result Qualifier Dilution Analysis Batch
Analyte deg F date/time
Flashpoint DNF at170 1 02/21/2022 0100 WG1821032
Mercury by Method 245.1
Analyte
Mercury
Result Qualifier RDL Dilution Analysis Batch
mg/I mg/I date / time
0.00469 0.00200 10 02/23/202213:08 WG1821092
— FP
— Fc
FS
-
Fn-
-
Rc
F,
[Al
— Rc
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1463165 03/10/22 09:13 5 of 59

WW-1
SAMPLE RESULTS - 01
Collected date/time:
02/17/22 10:30
L1463165
Metals (ICP) by
Method 200.7
Result
Qualifier RDL
Dilution Analysis
Batch
FPAnalyte
mg/I
mg/I
date / time
Aluminum
ND
0.200
1 02/21/202216:26
WG1820696
F
Arsenic
ND
0.0100
1 02/21/202216:26
WG1820696
Cadmium
ND
0.00200
1 02/21/202216:26
WG1820696
Calcium
21.4
1.00
1 02/21/202216:26
WG1820696
SS
F
Copper
ND
0.0100
1 02/21/202216:26
WG1820696
Lead
ND
0.00500
1 02/21/202216:26
WG1820696
Fn
Magnesium
6.33
1.00
1 02/21/202216:26
WG1820696
Molybdenum
0.793
0.00500
1 02/21/202216:26
WG1820696
Nickel
0.0394
0.0100
1 02/21/202216:26
WG1820696
Potassium
271
B 50.0
50 02/22/202212:02
WG1820696
Selenium
ND
0.0100
1 02/21/202216:26
WG1820696
F
Sodium
1060
50.0
50 02/22/202212:02
WG1820696
Zinc
ND
0.0500
1 02/21/202216:26
WG1820696
F,
F
RC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1463165 03/10/22 09:13 6 of 59

SAMPLE RESULTS - 02
L1463165
WW-1
Collected date/time: 02/17/22 10:30
Preparation by Method 1311
Result
Qualifier Prep
Batch
Analyte
date / time
TCLP Extraction
2/26/2022 9:26:12 AM
WG1823891
TCLP ZHE Extraction -
2/24/2022 2:03:42 PM
WG1822928
Fluid 1
2/26/2022 9:26:12 AM
WG1823891
Initial pH 7.96
2/26/2022 9:26:12 AM
WG1823891
Final pH 5.05
2/26/2022 9:26:12 AM
WG1823891
Mercury by Method 7470A
Result
Qualifier RDL Limit
Dilution Analysis Batch
Analyte mg/I
mg/I mg/I
date/time
Mercury ND
0.0100 0.20
1 03/02/2022 08:52 WG1824898
Metals (ICP) by Method 6010D
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
Arsenic
ND
0.100
5
1 03/01/202210:16
WG1824957
Barium
0.103
0.100
100
1 03/01/202210:16
WG1824957
Cadmium
ND
0.100
1
1 03/01/202210:16
WG1824957
Chromium
ND
0.100
5
1 03/01/202210:16
WG1824957
Lead
ND
0.100
5
1 03/01/202210:16
WG1824957
Selenium
ND
0.100
1
1 03/01/202210:16
WG1824957
Silver
ND
0.100
5
1 03/01/202210:16
WG1824957
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
Benzene
ND
0.0500
0.50
1 02/27/202218:01
WG1824485
Carbon tetrachloride
ND
0.0500
0.50
1 02/27/202218:01
WG1824485
Chlorobenzene
ND
0.0500
100
1 02/27/202218:01
WG1824485
Chloroform
ND
0.250
6
1 02/27/202218:01
WG1824485
1,2-Dichloroethane
ND
0.0500
0.50
1 02/27/202218:01
WG1824485
1,1-Dichloroethene
ND
0.0500
0.70
1 02/27/202218:01
WG1824485
2-Butanone (MEK)
ND
0.500
200
1 02/27/202218:01
WG1824485
Tetrachloroethene
ND
0.0500
0.70
1 02/27/202218:01
WG1824485
Trichloroethene
ND
0.0500
0.50
1 02/27/202218:01
WG1824485
Vinyl chloride
ND
0.0500
0.20
1 02/27/202218:01
WG1824485
(S) Toluene-dH
98.6
80.0-120
021271202218.01
WG1824485
(S) 4-Bromofluorobenzene
85.6
77.0-126
021271202218.01
WG1824485
(S) 1,2-Dichloroethane-d4
113
70.0-130
021271202218.01
WG1824485
Chlorinated Acid Herbicides (GC)
by Method 8151A
Result Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
2,4,5-TP (Silvex)
ND
0.00200
1
1 03/02/2022 19:40
WG1825661
2,4-D
ND
0.00200
10
1 03/02/202219:40
WG1825661
(S) Z4-Dichlorophenyl Acetic Acid
73.4
14.0-158
031021202219.40
WG1825661
Pesticides (GC) by Method
8081B
Result Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
Chlordane
ND
0.00500
0.03
1 03/02/202214:48
WG1825495
Endrin
ND
0.00500
0.02
1 03/02/202214:48
WG1825495
Heptachlor
ND
0.00500
0.0080
1 03/02/202214:48
WG1825495
Lindane
ND
0.00500
0.40
1 03/02/202214:48
WG1825495
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1463165 03/10/22 09:13 7 of 59

WW-1
Collected date/time: 02/17/22 10:30
Pesticides (GC) by Method 8081B
Result
Analyte mg/I
Methoxychlor ND
Toxaphene ND
(S) Decochlorobiphenyl 84.3
(S) Tetrochloro-m-xylene 71.5
Semi Volatile Organic Compounds
SAMPLE RESULTS
L1463165
Qualifier RDL Limit Dilution
mg/I mg/I
0.00500 10 1
0.0100 0.50 1
10.0-128
10.0-127
(GC/MS) by Method 8270E
- 02
Analysis
date/time
03/02/202214:48
03/02/202214:48
0310212022 14.48
0310212022 14.48
Batch
WG1825495
WG1825495
WG1825495
WG1825495
F
Fc
SS
F
Fn
Result
Qualifier RDL
Limit Dilution
Analysis
Batch
Analyte mg/I
mg/I
mg/I
date/time
1,4-Dichlorobenzene ND
0.100
7.50 1
03/04/202216:17
WG1824791
2,4-Dinitrotoluene ND
0.100
0.13 1
03/04/202216:17
WG1824791
6
Hexachlorobenzene ND
0.100
0.13 1
03/04/202216:17
WG1824791
QC
Hexachloro-1,3-butadiene ND
0.100
0.50 1
03/04/202216:17
WG1824791
Hexachloroethane ND
0.100
3 1
03/04/202216:17
WG1824791
F
Nitrobenzene ND
0.100
2 1
03/04/202216:17
WG1824791
Pyridine ND
0.100
5 1
03/04/202216:17
WG1824791
e
3&4-Methyl Phenol ND
0.100
400 1
03/04/202216:17
WG1824791
AI
2-Methylphenol ND
0.100
200 1
03/04/202216:17
WG1824791
Pentachlorophenol ND
0.100
100 1
03/04/202216:17
WG1824791
F
2,4,5-Trichlorophenol ND
0.100
400 1
03/04/202216:17
WG1824791
2,4,6-Trichlorophenol ND
0.100
2 1
03/04/202216:17
WG1824791
(S) 2-Fluorophenol 37.4
10.0-120
031041202216.17
WG1824791
(S) Phenol-d5 22.8
10.0-120
031041202216.17
WG1824791
(S) Nitrobenzene-d5 77.1
10.0-127
031041202216.17
WG1824791
(S) 2-Fluorobiphenyl 73.8
10.0-130
031041202216.17
WG1824791
(S)2,4,6-Tribromophenol 75.0
10.0-155
031041202216.17
WG1824791
(S) p-Terphenyl-d14 86.1
10.0-128
031041202216.17
WG1824791
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Hunt Environmental Associates
L1463165
03/10/22 09:13
3 of 59

SAMPLE RESULTS - 03
L1463165
WW-1
Collected date/time: 02/17/22 10:30
Total Solids by Method 2540 G-2011
Result
Qualifier Dilution Analysis
Batch
Analyte %
date / time
Total Solids 2.41
1 02/24/2022 2110
WG1823409
Wet Chemistry by Method 350.1
Result (dry)
Qualifier RDL (dry) Dilution
Analysis Batch
Analyte mg/kg
mg/kg
date / time
Ammonia Nitrogen 6270
415 1
02/22/202217:25 WG1821201
Wet Chemistry by Method 365.4M
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Phosphorus, Total 20400 4150 5 03/08/202217:31 WG1821989
Wet Chemistry by Method 4500NOrg C-2011
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Kjeldahl Nitrogen, TKN 44600 4150 5 03/06/202212:35 WG1828073
Wet Chemistry by Method 9012B
Result (dry)
Qualifier RDL (dry) Dilution
Analysis Batch
Analyte mg/kg
mg/kg
date / time
Cyanide ND
10.4 1
02/22/202213:46 WG1821197
Wet Chemistry by Method 9045D
Result
Qualifier Dilution Analysis
Batch
Analyte su
date / time
pH 7.23
T8 1 02/23/2022 09:00
WG1821960
Sample Narrative:
L1463165-03 WG1821960: 7.23 at 21.9C
Wet Chemistry by Method 9056A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Nitrate -Nitrite ND 830 1 02/22/2022 02:41 WG1821500
Wet Chemistry by Method D93/1010A
Result Qualifier Dilution Analysis Batch
Analyte Deg. F date / time
Ignitability DNI at170 1 02/21/2022 0100 WG1821036
Mercury by Method 7471B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 1.66 1 02/23/202213:16 WG1820889
Metals (ICP) by Method 6010D
Result (dry)
Qualifier RDL (dry)
Dilution Analysis
Batch
Analyte
mg/kg
mg/kg
date / time
Aluminum
19700
830
1 02/21/2022 20:38
WG1820840
Arsenic
ND
83.0
1 02/21/2022 20:38
WG1820840
Cadmium
ND
20.7
1 02/21/2022 20:38
WG1820840
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1463165 03/10/22 09:13 9 of 59

WW-1
Collected date/time: 02/17/22 10:30
Metals (ICP) by Method 6010D
SAMPLE
RESULTS - 03
L1463165
Result (dry)
Qualifier RDL (dry)
Dilution Analysis
Batch
FPAnalyte
mg/kg
mg/kg
date / time
Calcium 11200
4150
1 02/21/2022 20:38
WG1820840
F
Copper 450
83.0
1 02/21/2022 20:38
WG1820840
Lead ND
20.7
1 02/21/2022 20:38
WG1820840
Magnesium ND
4150
1 02/21/2022 20:38
WG1820840
Fss]
Molybdenum ND
20.7
1 02/21/2022 20:38
WG1820840
Nickel ND
83.0
1 02/21/2022 20:38
WG1820840
Fn
Selenium ND
83.0
1 02/21/2022 20:38
WG1820840
Sodium 33900
4150
1 02/21/2022 20:38
WG1820840
Zinc 827
207
1 02/21/2022 20:38
WG1820840
Rc
F,
F
RC
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Hunt Environmental Associates
L1463165
03/10/22 09:13
10 of 59

WG1823409
Total Solids by Method 2540 G-2011
Method Blank (MB)
(MB) R3764041-1 02/24/22 2110
MB Result
Analyte
Total Solids 0.000
MB Qualifier MB MDL MB RDL
L1463401-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1463165-03
(OS) L1463401-01 02/24/22 21:10 • (DUP) R3764041-3 02/24/22 2110
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte % % %_
Total Solids 23.6 23.2 1 1.71 10
Laboratory Control Sample (LCS)
(LCS) R3764041-2 02/24/22 2110
Spike Amount LCS Result
Analyte
Total Solids 50.0 50.0
LCS Rec. Rec. Limits LCS Qualifier
100 85.0-115
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1463165 03/10/22 09:13 11 of 59

WG1821201 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 350.1 L1463165-03
Method Blank (MB)
(MB) R3762709-1 02/22/22 1710
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Ammonia Nitrogen U 7.00 10.0
L1462503-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1462503-01 02/22/22 17:31 • (DUP) R3762709-3 02/22/22 1716
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
(dry) (dry) Limits
Analyte mg/kg mg/kg %_
Ammonia Nitrogen ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3762709-2 02/22/22 17:11
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Ammonia Nitrogen 500 550 110
Rec. Limits LCS Qualifier
90.0-110
L1463401-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1463401-01 02/22/22 17:26 • (MS) R3762709-4 02/22/22 17:27 • (MSD) R3762709-5 02/22/22 17:29
Spike Amount Original Result
MS Result (dry)
MSD Result MS Rec.
MSD Rec. Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD RPD Limits
(dry) (dry)
(dry)
Analyte mg/kg mg/kg
mg/kg
mg/kg
Ammonia Nitrogen 2120 83.4
2330
2330 106
106 1 80.0-120
0.000 20
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Hunt Environmental Associates
L1463165
03/10/22 09:13 12 of 59

WG1823467
Wet Chemistry by Method 350.1
Method Blank (MB)
(MB) R3764031-1 02/25/22 16:43
MB Result
Analyte mg/I
Ammonia Nitrogen U
MB Qualifier MB MDL MB RDL
mg/I mg/I
0.117 0.250
L1462522-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1463165-01
(OS) L1462522-01 02/25/22 16:57 • (DUP) R3764031-5 02/25/22 16:59
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I %_
Ammonia Nitrogen ND ND 1 0.000 10
L1463337-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1463337-01 02/25/22 17:30 • (DUP) R3764031-7 02/25/22 17:32
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I
Ammonia Nitrogen 1.15 1.12 1 2.47 10
Laboratory Control Sample (LCS)
(LCS) R3764031-2 02/25/22 16:50
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
Ammonia Nitrogen 7.50 7.46 99.4
Rec. Limits LCS Qualifier
90.0-110
L1462516-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1462516-01 02/25/22 16:53 • (MS) R3764031-3 02/25/22 16:54 • (MSD) R3764031-4 02/25/22 16:56
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Ammonia Nitrogen 5.00
ND
5.05
5.03 101 101 1 90.0-110 0.436 10
L1463336-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1463336-01 02/25/22 17:27 • (MS) R3764031-6 02/25/22 17:29
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/I mg/I mg/I
Ammonia Nitrogen 5.00 ND 5.09 102 1 90.0-110
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1463165 03/10/22 09:13 13 of 59

WG1824691
Wet Chemistry by Method 351.2
Method Blank (MB)
(MB) R3767476-1 03/03/22 1220
MB Result
Analyte mg/I
Kjeldahl Nitrogen, TKN U
MB Qualifier MB MDL MB RDL
mg/I mg/I
0.140 0.250
L1462965-02 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1463165-01
(OS) L1462965-02 03/03/22 12:28 • (DUP) R3767476-6 03/03/22 12:29
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I
Kjeldahl Nitrogen, TKN 0.869 0.766 1 12.6 20
L1462965-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1462965-01 03/03/22 12:52 • (DUP) R3767476-9 03/03/22 12:54
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I
Kjeldahl Nitrogen, TKN 51.7 53.1 10 2.67 20
Laboratory Control Sample (LCS)
(LCS) R3767476-2 03/08/22 12:21
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
Kjeldahl Nitrogen, TKN 10.2 11.2 110
Rec. Limits LCS Qualifier
75.2-121
L1462965-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1462965-01 03/03/22 12:24 • (MS) R3767476-5 03/03/22 12:27
Spike Amount Original Result MS Result MS Rec.
Analyte mg/I mg/I mg/I
Kjeldahl Nitrogen, TKN 5.00 30.5 30.8 6.00
Dilution Rec. Limits MS Qualifier
1 90.0-110 E V
L1462965-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1462965-02 03/03/22 12:28 • (MS) R3767476-7 03/03/22 12:31 • (MSD) R3767476-8 03/03/22 12:32
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I
Kjeldahl Nitrogen, TKN 5.00 0.869 6.44 6.29 111 108 1 90.0-110 J5 2.36 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1463165 03/10/22 09:13 14 of 59

WG1823045
Wet Chemistry by Method 353.2
Method Blank (MB)
(MB) R3766937-1 03/06/22 23:56
MB Result
Analyte mg/I
Nitrate -Nitrite U
MB Qualifier MB MDL MB RDL
mg/I mg/I
0.0500 0.100
L1463112-03 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1463165-01
(OS) L1463112-03 03/07/22 00:01 • (DUP) R3766937-3 03/07/22 00:02
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I %_
Nitrate -Nitrite 1.55 1.56 1 0.643 20
L1463389-03 Original Sample (OS) • Duplicate (DUP)
(OS) L1463339-03 03/07/22 00:17 • (DUP) R3766937-6 03/07/22 00:19
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I
Nitrate -Nitrite ND 0.113 1 16.4 20
Laboratory Control Sample (LCS)
(LCS) R3766937-2 03/06/22 23:57
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
Nitrate -Nitrite 2.50 2.56 102 90.0-110
L1463112-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1463112-03 03/07/22 00:01 • (MS) R3766937-4 03/07/22 00:03 • (MSD) R3766937-5 03/07/22 00:05
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I
Nitrate -Nitrite 2.50 1.55 4.12 4.12 103 103 1 90.0-110 0.000 20
L1463389-03 Original Sample (OS) • Matrix Spike (MS)
(OS) L1463339-03 03/07/22 00:17 • (MS) R3766937-7 03/07/22 00:20
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/I mg/I mg/I
Nitrate -Nitrite 2.50 ND 2.84 110 1 90.0-110
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1463165 03/10/22 09:13 15 of 59

WG1828980
QUALITY CONTROL SUMMARY
Wet Chemistry by Method 365.4
L1463165-01
Method Blank (MB)
C p
(MB) R3767431-1 03/03/22 12:41
MB Result MB Qualifier MB MDL MB RDL
z
Analyte mg/I mg/I mg/I
TC
Phosphorus, Total U 0.0350 0.100
FSS
L1462965-02 Original Sample (OS) • Duplicate (DUP)
[�n]
(OS) L1462965-02 03/03/22 12:46 • (DUP) R3767431-4 03/03/22 12:47
Original Result DUP Result Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
5
Sr
Analyte mg/I mg/I
—
Phosphorus, Total 0.796 0.790 1 0.757
20
L1462965-01 Original Sample (OS) • Duplicate (DUP)
GI
(OS) L1462965-01 03/03/22 13:07 • (DUP) R3767431-7 03/03/22 13:11
Original Result DUP Result Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
FAI
Analyte mg/I mg/I
Phosphorus, Total 11.4 11.2 5 2.22
20
FS
Laboratory Control Sample (LCS)
(LCS) R3767481-2 03/08/22 12:42
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
Phosphorus, Total 1.33 1.33 100
Rec. Limits LCS Qualifier
81.2-118
L1462965-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1462965-02 03/03/22 12:46 • (MS) R3767431-5 03/03/22 12:48 • (MSD) R3767431-6 03/03/22 12:50
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I
Phosphorus, Total 2.50 0.796 3.16 3.14 94.6 93.8 1 90.0-110 0.635 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1463165 03/10/22 09:13 16 of 59

WG1821989 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 365.4M L1463165-03
Method Blank (MB)
(MB) R3767623-1 03/03/22 17:21
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Phosphorus, Total U 5.00 20.0
L1452156-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1452156-01 03/03/22 17:23 • (DUP) R3767623-3 03/03/22 17:24
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
(dry) (dry) Limits
Analyte
Phosphorus, Total 307 308 2 0.274 25
Laboratory Control Sample (LCS)
(LCS) R3767623-2 03/08/22 1722
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Phosphorus, Total 53.2 53.6 101
Rec. Limits LCS Qualifier
78.9-121
L1452156-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1452156-02 03/03/22 17:26 • (MS) R3767623-4 03/03/22 17:27 • (MSD) R3767623-5 03/03/22 17:28
Spike Amount Original Result
MS Result (dry) MSD Result MS Rec.
MSD Rec. Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD RPD Limits
(dry) (dry)
(dry)
Analyte mg/kg
Phosphorus, Total 53.2 210
290 317 134
180 1 50.0-150
E E J5 8.96 25
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Hunt Environmental Associates
L1463165
03/10/22 09:13 17 of 59

WG1821200
Wet Chemistry by Method 4500 CN E-2016
Method Blank (MB)
(MB) R3762603-1 02/22/22 1436
MB Result
Analyte mg/I
Reactive Cyanide U
QUALITY CONTROL SUMMARY
L1463165-01
MB Qualifier MB MDL MB RDL
mg/I mg/I
0.00180 0.00500
L1463324-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1463324-02 02/22/22 14:50 • (DUP) R3762603-3 02/22/22 14:51
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I %_
Reactive Cyanide ND ND 1 0.000 20
L1463331-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1463331-02 02/22/22 14:57 • (DUP) R3762603-4 02/22/22 15:00
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I
Reactive Cyanide ND ND 1 55.8 P1 20
Laboratory Control Sample (LCS)
(LCS) R3762603-2 02/22/22 1437
Spike Amount LCS Result
Analyte mg/I mg/I
Reactive Cyanide 0.100 0.101
LCS Rec. Rec. Limits LCS Qualifier
101 87.1-120
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1463165 03/10/22 09:13 13 of 59

WG1820714
Wet Chemistry by Method 4500 S2 D-2011
Method Blank (MB)
(MB) R3762066-1 02/21/22 12:44
MB Result
Analyte mg/I
Reactive Sulfide U
MB Qualifier MB MDL MB RDL
mg/I mg/I
0.0250 0.0500
L1462970-02 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1463165-01
(OS) L1462970-02 02/21/22 12:53 • (DUP) R3762066-3 02/21/22 12:54
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I %_
Reactive Sulfide ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3762066-2 02/21/22 12:44
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
Reactive Sulfide 0.500 0.558 112 85.0-115
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1463165 03/10/22 09:13 19 of 59

WG1820604 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 4500H+ B-2011 L1463165-01
L1457993-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1457993-01 02/22/22 10:00 • (DUP) R3762347-2 02/22/22 10:00
Original Result DUP Result Dilution DUP RPD
Analyte su su
pH 8.06 8.03 1 0.373
Sample Narrative:
OS: 8.06 at18.1C
DUP: 8.03 at 20.9C
L1462511-01 Original Sample (OS) • Duplicate (DUP)
DUP Qualifier DUP RPD
Limits
(OS) L1462511-01 02/22/22 10:00 • (DUP) R3762347-3 02/22/22 10:00
Original Result DUP Result
Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte su su
pH 7.85 7.85
1 0.000 1
Sample Narrative:
OS: 7.85 at18C
DUP: 7.85 at18C
Laboratory Control Sample (LCS)
(LCS) R3762347-1 02/22/22 10:00
Spike Amount LCS Result
LCS Rec. Rec. Limits LCS Qualifier
Analyte su su
pH 10.0 10.0
100 99.0-101
Sample Narrative:
LCS :10.01 at20.4C
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates
L1463165 03/10/22 09:13 20 of 59

WG1828073
Wet Chemistry by Method 4500NOrg C-2011
Method Blank (MB)
(MB) R3766323-1 03/06/22 1110
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Kjeldahl Nitrogen, TKN 5.22 J 4.48 20.0
L1462444-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1463165-03
(OS) L1462444-01 03/06/22 11:14 • (DUP) R3766828-3 03/06/22 1115
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
(dry) (dry) Limits
Analyte mg/kg mg/kg %_
Kjeldahl Nitrogen, TKN 76200 73400 20 3.63 20
Laboratory Control Sample (LCS)
(LCS) R3766828-2 03/06/22 1111
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Kjeldahl Nitrogen, TKN 408 365 89.4
Rec. Limits LCS Qualifier
75.2-121
L1462444-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1462444-01 03/06/22 11:14 • (MS) R3766828-4 03/06/22 1119 • (MSD) R3766828-5 03/06/22 1121
Spike Amount Original Result
MS Result (dry)
MSD Result MS Rec.
MSD Rec. Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD RPD Limits
(dry) (dry)
(dry)
Analyte mg/kg mg/kg
mg/kg
mg/kg
Kjeldahl Nitrogen, TKN 2800 76200
72600
76200 0.000
3.02 20 90.0-110
V V 4.92 20
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Hunt Environmental Associates
L1463165
03/10/22 09:13 21 of 59

WG1821197
Wet Chemistry by Method 9012B
Method Blank (MB)
(MB) R3762532-1 02/22/22 1322
MB Result
Analyte mg/kg
Cyanide U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
0.0733 0.250
L1462850-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1463165-03
(OS) L1462350-01 02/22/22 13:30 • (DUP) R3762532-3 02/22/22 13:31
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg
Cyanide 0.424 0.437 1 3.02 20
L1462872-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1462372-01 02/22/22 13:36 • (DUP) R3762532-6 02/22/22 13:37
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg
Cyanide 0.638 0.583 1 8.98 20
Laboratory Control Sample (LCS)
(LCS) R3762532-2 02/22/22 1323
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg
Cyanide 2.50 2.52 101 85.0-115
L1462850-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1462350-01 02/22/22 13:30 • (MS) R3762532-4 02/22/22 13:34 • (MSD) R3762532-5 02/22/22 13:35
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec.
Analyte mg/kg mg/kg mg/kg mg/kg
Cyanide 1.67 0.424 0.595 0.438 10.2 0.855
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
1 75.0-125 J6 J3 J6 30.3 20
L1462970-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1462970-01 02/22/22 13:33 • (MS) R3762532-7 02/22/22 13:39 • (MSD) R3762532-8 02/22/22 13:40
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Cyanide 1.67 ND 1.00 1.11 60.0 66.8 1 75.0-125 J6 J6 10.7 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1463165 03/10/22 09:13 22 of 59

WG1821960 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9045D L1463165-03
L1463540-03 Original Sample (OS) • Duplicate (DUP)
(OS) L1463540-03 02/23/22 09:00 • (DUP) R3762301-2 02/23/22 09:00
Original Result DUP Result Dilution DUP RPD
Analyte pH su
pH 8.87 8.86 1 0.113
Sample Narrative:
OS: 8.87 at 21.7C
DUP: 8.86 at21.4C
L1463542-03 Original Sample (OS) • Duplicate (DUP)
DUP Qualifier DUP RPD
Limits
(OS) L1463542-03 02/23/22 09:00 • (DUP) R3762301-3 02/23/22 09:00
Original Result DUP Result
Dilution
DUP RPD DUP Qualifier DUP RPD
Limits
Analyte pH su
pH 8.54 8.53
1
0.117 1
Sample Narrative:
OS: 8.54 at 21.7C
DUP:8.53 at23.4C
Laboratory Control Sample (LCS)
(LCS) R3762301-1 02/23/22 09:00
Spike Amount LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte su su
pH 10.0 10.0
100
99.0-101
Sample Narrative:
LCS:10 at 21.1C
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates
L1463165 03/10/22 09:13 23 of 59

WG1821500
Wet Chemistry by Method 9056A
Method Blank (MB)
(MB) R3762330-2 02/21/22 22:05
MB Result
Analyte mg/kg
Nitrate -Nitrite U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
1.06 20.0
L1462455-11 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1463165-03
(OS) L1462455-11 02/22/22 00:33 • (DUP) R3762330-4 02/22/22 00:49
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
(dry) (dry) Limits
Analyte mg/kg mg/kg
Nitrate -Nitrite ND ND 1 0.0273 15
L1463426-07 Original Sample (OS) • Duplicate (DUP)
(OS) L1463426-07 02/22/22 03:12 • (DUP) R3762330-7 02/22/22 03:23
Original Result DUP Result DUP RPD
Dilution DUP RPD DUP Qualifier
(dry) (dry) Limits
Analyte mg/kg mg/kg
Nitrate -Nitrite ND ND 1 2.74 15
Laboratory Control Sample (LCS)
(LCS) R3762330-3 02/21/22 22:21
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Nitrate -Nitrite 40.0 40.3 101
Rec. Limits LCS Qualifier
80.0-120
L1462455-11 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1462455-11 02/22/22 00:33 • (MS) R3762330-5 02/22/22 01:05 • (MSD) R3762330-6 02/22/22 0153
Spike Amount Original Result
MS Result (dry)
MSD Result MS Rec.
MSD Rec. Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD RPD Limits
(dry) (dry)
(dry)
Analyte mg/kg mg/kg
mg/kg
mg/kg
Nitrate -Nitrite 105 ND
122
124 98.1
99.4 1 80.0-120
1.09 15
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Hunt Environmental Associates
L1463165
03/10/22 09:13 24 of 59

WG1821032 QUALITY CONTROL SUMMARY
Wet Chemistry by Method D93/1010A L1463165-01
L1463036-28 Original Sample (OS) • Duplicate (DUP)
(OS) L1463036-23 02/21/22 01:00 • (DUP) R3762217-3 02/21/22 0100
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte deg F deg F
Flashpoint 160 168 1 4.89 10
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3762217-1 02/21/22 01:00 • (LCSD) R3762217-2 02/21/22 0100
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte deg F deg F deg F
Flashpoint 126 130 128 103 101 96.0-104 1.56 10
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1463165 03/10/22 09:13 25 of 59

WG1821036 QUALITY CONTROL SUMMARY
Wet Chemistry by Method D93/1010A L1463165-03
L1463101-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1463101-02 02/21/22 01:00 • (DUP) R3762219-3 02/21/22 0100
Original Result DUP Result Dilution DUP RPD
Analyte Deg. F Deg. F
Ignitability 132 140 1 5.90
DUP Qualifier DUP RPD
Limits
i
10
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3762219-1 02/21/22 01:00 • (LCSD) R3762219-2 02/21/22 0100
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte Deg. F Deg. F Deg. F
Ignitability 126 128 122 101 96.5 95.6-104 4.82 10
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1463165 03/10/22 09:13 26 of 59

WG1821092
Mercury by Method 245.1
Method Blank (MB)
(MB) R3762991-1 02/23/22 12:17
MB Result MB Qualifier MB MDL
Analyte mg/I mg/I
Mercury U 0.000100
Laboratory Control Sample (LCS)
(LCS) R3762991-2 02/23/22 12:19
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
Mercury 0.00300 0.00285 94.9
QUALITY CONTROL SUMMARY
L1463165-01
MB RDL
mg/I
0.000200
Rec. Limits LCS Qualifier
85.0-115
L1462342-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1462342-01 02/23/22 12:21 • (MS) R3762991-3 02/23/22 12:23 • (MSD) R3762991-4 02/23/22 12:25
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Mercury 0.00300
ND
0.00290
0.00282 96.7 93.9 �1 70.0-130 2.90 20
L1463488-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1463433-01 02/23/22 12:26 • (MS) R3762991-5 02/23/22 12:23 • (MSD) R3762991-6 02/23/22 12:30
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I
Mercury 0.00300 ND 0.00302 0.00300 101 100 1 70.0-130 0.663 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1463165 03/10/22 09:13 27 of 59

WG1824898 QUALITY CONTROL SUMMARY
Mercury by Method 7470A L1463165-02
Method Blank (MB)
(MB) R3765416-1 03/02/22 08:23
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mg/I
Mercury U 0.00330 0.0100
Laboratory Control Sample (LCS)
(LCS) R3765416-2 03/02/22 08:25
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
Mercury 0.0300 0.0330 110
Rec. Limits LCS Qualifier
80.0-120
L1462970-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1462970-01 03/02/22 08:27 • (MS) R3765416-3 03/02/22 08:29 • (MSD) R3765416-4 03/02/22 08:31
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Mercury 0.0300
ND
0.0330
0.0312 110 104 1 75.0-125 5.35 20
L1462970-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1462970-02 03/02/22 08:33 • (MS) R3765416-5 03/02/22 08:35 • (MSD) R3765416-6 03/02/22 08:37
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I
Mercury 0.0300 ND 0.0322 0.0315 107 105 1 75.0-125 2.18 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1463165 03/10/22 09:13 23 of 59

WG1820889
Mercury by Method 7471B
Method Blank (MB)
(MB) R3762990-1 02/23/22 12:30
MB Result MB Qualifier MB MDL
Analyte mg/kg mg/kg
Mercury U 0.0180
Laboratory Control Sample (LCS)
(LCS) R3762990-2 02/23/22 12:33
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Mercury 0.500 0.508 102
QUALITY CONTROL SUMMARY
L1463165-03
MB RDL
mg/kg
0.0400
Rec. Limits LCS Qualifier
80.0-120
L1463121-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1463121-03 02/23/22 12:35 • (MS) R3762990-3 02/23/22 12:33 • (MSD) R3762990-4 02/23/22 12:40
Spike Amount Original Result
MS Result (dry)
MSD Result MS Rec.
MSD Rec. Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD RPD Limits
(dry) (dry)
(dry)
Analyte mg/kg mg/kg
mg/kg
mg/kg
Mercury 0.642 ND
0.598
0.601 93.1
93.6 1 75.0-125
0.552 20
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Hunt Environmental Associates
L1463165
03/10/22 09:13 29 of 59

WG1820696 QUALITY CONTROL SUMMARY
Metals (ICP) by Method 200.7 L1463165-01
Method Blank (MB)
(MB) R3762284-1 02/21/22 1535
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Aluminum
U
0.0592
0.200
Arsenic
U
0.00645
0.0100
Cadmium
U
0.000552
0.00200
Calcium
U
0.0473
1.00
Copper
U
0.00226
0.0100
Lead
U
0.00227
0.00500
Magnesium
U
0.115
1.00
Molybdenum
U
0.000982
0.00500
Nickel
U
0.00182
0.0100
Potassium
0.882
J
0.313
1.00
Selenium
U
0.00616
0.0100
Sodium
0.553
J
0.444
1.00
Zinc
U
0.00578
0.0500
Laboratory Control Sample (LCS)
(LCS) R3762234-2 02/21/22 15:33
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/I
mg/I
Aluminum
10.0
10.0
100
85.0-115
Arsenic
1.00
0.952
95.2
85.0-115
Cadmium
1.00
1.01
101
85.0-115
Calcium
10.0
10.0
100
85.0-115
Copper
1.00
1.01
101
85.0-115
Lead
1.00
0.987
98.7
85.0-115
Magnesium
10.0
9.96
99.6
85.0-115
Molybdenum
1.00
0.992
99.2
85.0-115
Nickel
1.00
0.997
99.7
85.0-115
Potassium
10.0
9.96
99.6
85.0-115
Selenium
1.00
0.973
97.3
85.0-115
Sodium
10.0
10.5
105
85.0-115
Zinc
1.00
0.955
95.5
85.0-115
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1463165 03/10/22 09:13 30 of 59

WG1820696
Metals (ICP) by Method 200.7
QUALITY CONTROL SUMMARY
L1463165-01
L1461234-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1461234-03 02/21/22 15:41 • (MS) R3762234-4 02/21/22 15:46 • (MSD) R3762234-5 02/21/22 15:49
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
Aluminum
10.0
ND
10.2
10.4
101
102
Arsenic
1.00
ND
0.988
1.00
98.8
100
Cadmium
1.00
ND
1.05
1.06
105
106
Calcium
10.0
69.9
80.6
81.8
107
119
Copper
1.00
ND
1.03
1.05
103
105
Lead
1.00
ND
1.01
1.02
100
102
Magnesium
10.0
11.7
21.6
21.9
99.0
102
Molybdenum
1.00
0.497
1.48
1.51
98.4
101
Nickel
1.00
0.0112
1.05
1.07
104
105
Potassium
10.0
131
142
144
114
135
Selenium
1.00
ND
1.02
1.03
102
103
Sodium
10.0
149
161
163
112
137
Zinc
1.00
ND
1.02
1.03
97.5
98.7
L1461362-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD
(OS) L1461362-03 02/21/22 15:52 • (MS) R3762234-6 02/21/22 15:55 • (MSD) R3762234-7 02/21/22 15:57
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
Aluminum
10.0
ND
10.0
10.1
100
101
Arsenic
1.00
ND
0.964
0.964
96.4
96.4
Cadmium
1.00
ND
1.03
1.03
103
103
Calcium
10.0
32.3
41.9
41.6
95.6
92.8
Copper
1.00
ND
1.02
1.02
101
101
Lead
1.00
ND
0.997
0.998
99.7
99.8
Magnesium
10.0
19.7
28.9
28.8
92.3
90.9
Molybdenum
1.00
0.0101
1.00
0.997
99.3
98.7
Nickel
1.00
ND
1.02
1.01
102
101
Potassium
10.0
6.88
16.3
16.1
94.4
92.6
Selenium
1.00
ND
0.991
0.994
99.1
99.4
Sodium
10.0
46.3
54.4
53.8
81.3
74.6
Zinc
1.00
0.0714
1.02
1.02
95.2
94.6
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 70.0-130
1.87
20
1 70.0-130
1.68
20
1 70.0-130
1.36
20
1 70.0-130
1.49
20
1 70.0-130
1.55
20
1 70.0-130
1.67
20
1 70.0-130
1.45
20
1 70.0-130
1.64
20
1 70.0-130
1.57
20
1 70.0-130
V_ 1.43
20
1 70.0-130
1.24
20
1 70.0-130
V_ 1.51
20
1 70.0-130
1.12
20
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 70.0-130
0.394
20
1 70.0-130
0.0455
20
1 70.0-130
0.589
20
1 70.0-130
0.659
20
1 70.0-130
0.0697
20
1 70.0-130
0.116
20
1 70.0-130
0.461
20
1 70.0-130
0.584
20
1 70.0-130
0.692
20
1 70.0-130
1.13
20
1 70.0-130
0.317
20
1 70.0-130
1.24
20
1 70.0-130
0.587
20
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1463165 03/10/22 09:13 31 of 59

WG1820840
Metals (ICP) by Method 6010D
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1463165-03
(MB) R3762297-1 02/21/22 1927
MB Result
MB Qualifier MB MDL
MB RDL
Analyte mg/kg
mg/kg
mg/kg
Aluminum U
6.08
20.0
Arsenic U
0.518
2.00
Cadmium U
0.0471
0.500
Calcium U
10.6
100
Copper U
0.400
2.00
Lead U
0.208
0.500
Magnesium U
7.38
100
Molybdenum U
0.109
0.500
Nickel U
0.132
2.00
Selenium U
0.764
2.00
Sodium U
41.2
100
Zinc U
0.832
5.00
Laboratory Control Sample (LCS)
(LCS) R3762297-2 02/21/22 1929
Spike Amount
LCS Result
LCS Rec.
Analyte
mg/kg
mg/kg
Aluminum
1000
962
96.2
Arsenic
100
95.5
95.5
Cadmium
100
99.6
99.6
Calcium
1000
964
96.4
Copper
100
102
102
Lead
100
101
101
Magnesium
1000
941
94.1
Molybdenum
100
105
105
Nickel
100
100
100
Selenium
100
100
100
Sodium
1000
1010
101
Zinc
100
97.3
97.3
Rec. Limits LCS Qualifier
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
L1463490-21 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1463490-21 02/21/22 19:32 • (MS) R3762297-5 02/21/22 19:40 • (MSD) R3762297-6 02/21/22 19:43
Spike Amount
Original Result
MS Result (dry)
MSD Result
MS Rec.
MSD Rec.
(dry)
(dry)
(dry)
Analyte mg/kg
mg/kg
mg/kg
mg/kg
Aluminum 1170
35400
31600
31500
0.000
0.000
Arsenic 117
8.77
178
111
144
86.7
ACCOUNT:
Hunt Environmental Associates
PROJECT:
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
1 75.0-125 V_ V_ 0.309
1 75.0-125 J5 J3 46.7
SDG: DATE/TIME:
L1463165 03/10/22 09:13
RPD Limits
20
20
PAGE:
32 of 59

WG1820840 QUALITY CONTROL SUMMARY
Metals (ICP) by Method 6010D L1463165-03
L1463490-21 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1463490-21 02/21/22 19:32 • (MS) R3762297-5 02/21/22 19:40 • (MSD) R3762297-6 02/21/22 19:43
Spike Amount
Original Result
MS Result (dry)
MSD Result
MS Rec.
MSD Rec.
(dry)
(dry)
(dry)
Analyte
mg/kg
mg/kg
mg/kg
mg/kg
Cadmium
117
ND
112
114
94.8
96.7
Calcium
1170
1320
2790
3870
125
218
Copper
117
29.7
153
149
105
101
Lead
117
20.2
160
146
119
107
Magnesium
1170
5690
7760
7820
177
182
Molybdenum
117
ND
103
107
87.8
90.9
Nickel
117
81.5
204
186
105
89.0
Selenium
117
ND
111
113
92.9
94.2
Sodium
1170
991
2220
2140
105
98.0
Zinc
117
73.3
177
193
87.9
102
ACCOUNT:
Hunt Environmental Associates
PROJECT:
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 75.0-125
2.00
20
1 75.0-125
J3 J5 32.5
20
1 75.0-125
2.91
20
1 75.0-125
8.75
20
1 75.0-125
V_ V_ 0.737
20
1 75.0-125
3.37
20
1 75.0-125
9.44
20
1 75.0-125
1.39
20
1 75.0-125
3.68
20
1 75.0-125
9.03
20
SDG:
DATE/TIME:
PAGE:
L1463165
03/10/22 09:13
33 of 59

WG1824957
Metals (ICP) by Method 6010D
Method Blank (MB)
(MB) R3765000-1 03/01/22 09:21
MB Result
MB Qualifier MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
Arsenic U
0.0333
0.100
Barium U
0.0333
0.100
Cadmium U
0.0333
0.100
Chromium U
0.0333
0.100
Lead U
0.0333
0.100
Selenium 0.0924
J 0.0333
0.100
Silver U
0.0333
0.100
Laboratory Control Sample (LCS)
(LCS) R3765000-2 03/01/22 09:23
QUALITY CONTROL SUMMARY
L1463165-02
Spike Amount
LCS Result
LCS Rec.
Rec. Limits
Analyte
mg/I
mg/I
Arsenic
10.0
9.46
94.6
80.0-120
Barium
10.0
9.76
97.6
80.0-120
Cadmium
10.0
9.73
97.3
80.0-120
Chromium
10.0
9.55
95.5
80.0-120
Lead
10.0
9.63
96.3
80.0-120
Selenium
10.0
9.80
98.0
80.0-120
Silver
2.00
1.69
84.7
80.0-120
LCS Qualifier
L1462962-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1462962-01 03/01/22 09:26 • (MS) R3765000-4 03/01/22 09:32 • (MSD) R3765000-5 03/01/22 09:35
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
Arsenic
10.0
0.784
11.5
11.3
108
105
Barium
10.0
107
127
125
202
184
Cadmium
10.0
ND
10.5
10.5
105
105
Chromium
10.0
0.277
9.76
9.77
94.8
95.0
Lead
10.0
0.245
9.87
9.89
96.2
96.4
Selenium
10.0
0.141
11.7
11.8
116
116
Silver
2.00
ND
1.96
1.95
98.2
97.7
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 75.0-125
1.96
20
1 75.0-125
V_ V_ 1.40
20
1 75.0-125
0.0823
20
1 75.0-125
0.146
20
1 75.0-125
0.225
20
1 75.0-125
0.643
20
1 75.0-125
0.545
20
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1463165 03/10/22 09:13 34 of 59

WG1824957 QUALITY CONTROL SUMMARY
Metals (ICP) by Method 6010D L1463165-02
L1462970-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1462970-01 03/01/22 09:33 • (MS) R3765000-6 03/01/22 09:41 • (MSD) R3765000-7 03/01/22 09:44
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
Arsenic
10.0
ND
9.40
9.38
94.0
93.8
Barium
10.0
0.250
9.88
9.94
96.3
96.9
Cadmium
10.0
ND
9.64
9.70
96.4
97.0
Chromium
10.0
ND
9.42
9.49
94.2
94.9
Lead
10.0
ND
9.46
9.53
94.6
95.3
Selenium
10.0
ND
9.72
9.85
96.4
97.6
Silver
2.00
ND
1.68
1.67
84.1
83.6
ACCOUNT:
Hunt Environmental Associates
PROJECT:
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 75.0-125
0.192
20
1 75.0-125
0.608
20
1 75.0-125
0.585
20
1 75.0-125
0.670
20
1 75.0-125
0.746
20
1 75.0-125
1.29
20
1 75.0-125
0.655
20
SDG:
DATE/TIME:
PAGE:
L1463165
03/10/22 09:13
35 of 59

WG1824485 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1463165-02
Method Blank (MB)
(MB) R3764360-3 02/27/22 1405
MB Result
Analyte
mg/I
Benzene
U
Carbon tetrachloride
U
Chlorobenzene
U
Chloroform
U
1,2-Dichloroethane
U
1,1-Dichloroethene
U
2-Butanone (MEK)
U
Tetrachloroethene
U
Trichloroethene
U
Vinyl chloride
U
(S) Toluene-dH
100
(S) 4-Bromofluorobenzene
80.0
(S) 1,2-Dichloroethane-d4
112
MB Qualifier MB MDL
mg/I
MB RDL
mg/I
0.0167
0.0500
0.0167
0.0500
0.0167
0.0500
0.0833
0.250
0.0167
0.0500
0.0167
0.0500
0.167
0.500
0.0167
0.0500
0.0167
0.0500
0.0167
0.0500
80.0-120
77.0-126
70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3764360-1 02/27/22 11:29 • (LCSD) R3764360-2 02/27/22 12:58
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mg/I
mg/I
mg/I
Benzene
0.250
0.218
0.213
87.2
85.2
70.0-123
Carbon tetrachloride
0.250
0.231
0.190
92.4
76.0
68.0-126
Chlorobenzene
0.250
0.241
0.226
96.4
90.4
80.0-121
Chloroform
0.250
0.229
0.230
91.6
92.0
73.0-120
1,2-Dichloroethane
0.250
0.219
0.232
87.6
92.8
70.0-128
1,1-Dichloroethene
0.250
0.211
0.194
84.4
77.6
71.0-124
2-Butanone (MEK)
1.25
1.12
1.26
89.6
101
44.0-160
Tetrachloroethene
0.250
0.247
0.202
98.8
80.8
72.0-132
Trichloroethene
0.250
0.220
0.207
88.0
82.8
78.0-124
Vinyl chloride
0.250
0.206
0.183
82.4
73.2
67.0-131
(S) Toluene-dH
99.4
98.6
80.0-120
(S) 4-Bromofluorobenzene
85.8
87.6
77.0-126
(S) 1,2-Dichloroethane-d4
103
109
70.0-130
ACCOUNT:
Hunt Environmental Associates
PROJECT:
LCS Qualifier LCSD Qualifier RPD
RPD Limits
2.32
20
19.5
20
6.42
20
0.436
20
5.76
20
8.40
20
11.8
20
20.0
20
6.09
20
11.8
20
SDG:
DATE/TIME: PAGE:
L1463165
03/10/22 09:13 36 of 59

WG1824485 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1463165-02
L1463155-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1463155-04 02/27/22 17:39 • (MS) R3764360-4 02/27/22 22:26 • (MSD) R3764360-5 02/27/22 22:43
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
Benzene
0.250
ND
0.211
0.224
84.4
89.6
Carbon tetrachloride
0.250
ND
0.241
0.255
96.4
102
Chlorobenzene
0.250
ND
0.243
0.256
97.2
102
Chloroform
0.250
ND
ND
ND
98.4
99.6
1,2-Dichloroethane
0.250
ND
0.232
0.238
92.8
95.2
1,1-Dichloroethene
0.250
ND
0.203
0.209
81.2
83.6
2-Butanone (MEK)
1.25
ND
1.31
1.28
105
102
Tetrachloroethene
0.250
ND
0.229
0.242
91.6
96.8
Trichloroethene
0.250
ND
0.209
0.230
83.6
92.0
Vinyl chloride
0.250
ND
0.170
0.188
68.0
75.2
(S) Toluene-dH
102
101
(S) 4-Bromofluorobenzene
87.4
84.7
(S) 1,2-Dichloroethane-d4
108
108
ACCOUNT:
Hunt Environmental Associates
PROJECT:
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 17.0-158
5.98
27
1 23.0-159
5.65
28
1 33.0-152
5.21
27
1 29.0-154
1.21
28
1 29.0-151
2.55
27
1 11.0-160
2.91
29
1 10.0-160
2.32
32
1 10.0-160
5.52
27
1 10.0-160
9.57
25
1 10.0-160
10.1
27
80.0-120
77.0-126
70.0-130
SDG:
DATE/TIME:
PAGE:
L1463165
03/10/22 09:13
37 of 59

WG1825661
Chlorinated Acid Herbicides (GC) by Method 8151A
Method Blank (MB)
(MB) R3765374-1 03/02/22 16:58
MB Result
Analyte mg/I
2,4,5-TP (Silvex) U
2,4-D U
(S) Z4-Dichlorophenyl Acetic 70.0
Acid
QUALITY CONTROL SUMMARY
L1463165-02
MB Qualifier MB MDL
MB RDL
mg/I
mg/I
0.000667
0.00200
0.000667
0.00200
14.0-158
Laboratory Control Sample (LCS)
(LCS) R3765874-2 03/02/22 1713
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
2,4,5-TP (Silvex) 0.0500
0.0417
83.4
50.0-125
2,4-D 0.0500
0.0451
90.2
50.0-120
(S) Z4-Dichlorophenyl Acetic
74.0
14. 0-158
Acid
L1463588-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1463533-01 03/02/22 20:24 • (MS) R3765874-3 03/02/22 20:38 • (MSD) R3765874-4 03/02/22 20:53
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
2,4,5-TP (Silvex)
0.0500
ND
0.0416
0.0359
83.2
71.8
2,4-D
0.0500
ND
0.0401
0.0407
80.2
81.4
(S) Z4-Dichlorophenyl Acetic
74.4
74.2
Acid
ACCOUNT:
Hunt Environmental Associates
PROJECT:
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
1 50.0-125 14.7 20
1 50.0-120 1.49 20
14.0-158
SDG: DATE/TIME: PAGE:
L1463165 03/10/22 09:13 33 of 59

WG1825495
Pesticides (GC) by Method 8081B
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1463165-02
(MB) R3765616-1 03/02/22 1337
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Chlordane
U
0.00167
0.00500
Endrin
U
0.00167
0.00500
Heptachlor
U
0.00167
0.00500
Gamma BHC
U
0.00167
0.00500
Methoxychlor
U
0.00167
0.00500
Toxaphene
U
0.00333
0.0100
(S) Decachlorobiphenyl
89.0
10.0-128
(S) Tetrochloro-m-xylene
71.5
10.0-127
Laboratory Control Sample (LCS)
(LCS) R3765616-2 03/02/22 13:46
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/I
mg/I
Endrin
0.0100
0.00938
93.8
57.0-134
Heptachlor
0.0100
0.00904
90.4
27.0-132
Gamma BHC
0.0100
0.00965
96.5
55.0-129
Methoxychlor
0.0100
0.0110
110
54.0-155 P
(S) Decachlorobiphenyl
94.7
10.0-128
(S) Tetrochloro-m-xylene
81.1
10.0-127
L1462872-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1462372-01 03/02/22 14:03 • (MS) R3765616-3 03/02/22 14:12 • (MSD) R3765616-4 03/02/22 14:21
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
Endrin
0.0100
ND
0.00939
0.00836
93.9
83.6
Heptachlor
0.0100
ND
0.00884
0.00793
88.4
79.3
Gamma BHC
0.0100
ND
0.00973
0.00856
97.3
85.6
Methoxychlor
0.0100
ND
0.0110
0.00987
110
98.7
(S) Decachlorobiphenyl
96.6
87.2
(S) Tetrochloro-m-xylene
80.2
68.8
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
1 10.0-160
11.6
1 16.0-136
10.9
1 14.0-141
12.8
1 10.0-160
P P 10.8
10.0-128
10.0-127
RPD Limits
39
40
40
34
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1463165 03/10/22 09:13 39 of 59

WG1824791 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1463165-02
Method Blank (MB)
(MB) R3766433-2 03/04/22 1141
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
U
0.0333
0.100
2,4-Dinitrotoluene
U
0.0333
0.100
Hexachlorobenzene
U
0.0333
0.100
Hexachloro-1,3-butadiene
U
0.0333
0.100
Hexachloroethane
U
0.0333
0.100
Nitrobenzene
U
0.0333
0.100
Pyridine
U
0.0333
0.100
3&4-Methyl Phenol
U
0.0333
0.100
2-Methylphenol
U
0.0333
0.100
Pentachlorophenol
U
0.0333
0.100
2,4,5-Trichlorophenol
U
0.0333
0.100
2,4,6-Trichlorophenol
U
0.0333
0.100
(S) 2-Fluorophenol
45.8
10.0-120
(S) Phenol-d5
28.0
10.0-120
(S) Nitrobenzene-d5
80.8
10.0-127
(S) 2-Fluorobiphenyl
83.4
10.0-130
(S) 2,4, 6-Tribromophenol
83.5
10. 0-155
(S) p-Terphenyl-d14
93.2
10.0-128
Laboratory Control Sample (LCS)
(LCS) R3766483-1 03/04/22 1120
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
1,4-Dichlorobenzene 0.500
0.443
88.6
18.0-120
2,4-Dinitrotoluene 0.500
0.610
122
49.0-124
Hexachlorobenzene 0.500
0.545
109
44.0-120
Hexachloro-1,3-butadiene 0.500
0.336
67.2
19.0-120
Hexachloroethane 0.500
0.456
91.2
15.0-120
Nitrobenzene 0.500
0.422
84.4
27.0-120
Pyridine 0.500
0.158
31.6
10.0-120
3&4-Methyl Phenol 0.500
0.410
82.0
31.0-120
2-Methylphenol 0.500
0.396
79.2
28.0-120
Pentachlorophenol 0.500
0.422
84.4
23.0-120
2,4,5-Trichlorophenol 0.500
0.498
99.6
44.0-120
2,4,6-Trichlorophenol 0.500
0.452
90.4
42.0-120
(S) 2-Fluorophenol
48.5
10.0-120
(S) Phenol-d5
32.2
10.0-120
(S) Nitrobenzene-d5
80.0
10.0-127
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates
L1463165 03/10/22 09:13 40 of 59

WG1824791 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1463165-02
Laboratory Control Sample (LCS)
(LCS) R3766483-1 03/04/22 1120
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
(S) 2-Fluorobiphenyl 88.4 10.0-130
(S) 2,4, 6-Tribromophenol 99.0 10. 0-155
(S) p-Terphenyl-d14 89.9 10.0-128
L1462338-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1462333-02 03/04/22 13:27 • (MS) R3766483-3 03/04/22 13:48 • (MSD) R3766483-4 03/04/22 14:09
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
Analyte
mg/I
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
0.500
ND
0.356
0.346
71.2
69.2
1 17.0-120
2.85
2,4-Dinitrotoluene
0.500
ND
0.505
0.482
101
96.4
1 39.0-125
4.66
Hexachlorobenzene
0.500
ND
0.460
0.441
92.0
88.2
1 35.0-122
4.22
HexachIaro-1,3-butadiene
0.500
ND
0.285
0.299
57.0
59.8
1 12.0-120
4.79
Hexachloroethane
0.500
ND
0.383
0.378
76.6
75.6
1 10.0-120
1.31
Nitrobenzene
0.500
ND
0.381
0.385
76.2
77.0
1 12.0-120
1.04
Pyridine
0.500
ND
0.120
0.127
24.0
25.4
1 10.0-120
5.67
3&4-Methyl Phenol
0.500
ND
0.447
0.445
89.4
89.0
1 10.0-120
0.448
2-Methylphenol
0.500
0.171
0.502
0.501
66.2
66.0
1 10.0-120
0.199
Pentachlorophenol
0.500
ND
0.390
0.378
78.0
75.6
1 10.0-128
3.12
2,4,5-Trichlorophenol
0.500
ND
0.406
0.397
81.2
79.4
1 33.0-120
2.24
2,4,6-Trichlorophenol
0.500
ND
0.381
0.372
76.2
74.4
1 26.0-120
2.39
(S) 2-Fluorophenol
41.3
39.2
10.0-120
(S) Phenol-d5
27.6
26.9
10.0-120
(S) Nitrobenzene-d5
76.1
74.9
10.0-127
(S) 2-Fluorobiphenyl
75.4
72.9
10.0-130
(S)2,4,6-Tribromophenol
89.0
83.0
10.0-155
(S) p-Terphenyl-d14
83.9
80.6
10.0-128
RPD Limits
40
25
24
34
40
30
37
36
30
37
31
31
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1463165 03/10/22 09:13 41 of 59

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contactyour project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
u
Fc
Fss]
(dry)
Results are reported based on the dry weight ofthe sample. [this will only be present on a dry report basis for soils].
MDL
Method Detection Limit.
Fn
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Fr
RDL (dry)
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
Fc
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
F
reported.
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
R
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
B
The same analyte is found in the associated blank.
E
The analyte concentration exceeds the upper limit ofthe calibration range ofthe instrument established by the initial
calibration (ICAL).
J The identification ofthe analyte is acceptable, the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J5 The sample matrix interfered with the abilityto make any accurate determination, spike value is high.
J6 The sample matrix interfered with the abilityto make any accurate determination, spike value is low.
P RPD between the primary and confirmatory analysis exceeded 40%.
P1 RPD value not applicable for sample concentrations less than 5 times the reporting limit.
T8 Sample(s) received past/too close to holding time expiration.
ACCOUNT: PROJECT: SDG: DATE/TIME
Hunt Environmental Associates
L1463165 03/10/22 09:13
PAGE:
42 of 59

GLOSSARY OF TERMS
Qualifier Description
v
The sample concentration is too high to evaluate accurate spike recoveries.
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1463165 03/10/22 09:13 43 of 59

ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
Nebraska
N E-OS-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TNO02
California
2932
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704 _
Georgia
NELAP
North Carolina 3
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky' 6
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee'"
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas5
LABO152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A2 LA
A2LA— ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1463165 03/10/22 09:13 44 of 59

r
Company Name/Address: Billing Information: Analysis/Container/Preservative Chain of Custody Page —of—
' Hunt Environmental Accounts Payable
PO Box 390
3330 Saddletree Road Lumberton, NC 28359 OESC
Lumberton, NC 28359
L•A•B S-C-I-E•N-C•E-5
� I
Report to: Email To: O I v 12065 Lebanon Rd
P har Y 5
Mount J6.1I5.t
Cody Hunt [e-mail] a O Phoe:
N Phone: 80D-17,65T87N--553a67
5
Projectcity/state fFax: 615-758-5859
Enviro-Choice Recycling aDescription: Collected: O 51822
❑❑i_ Ce�- •-
❑
Phone: Client Project # Lab Project # M i I = L O H 148 ib t
—} �q I N I
Fax: { J �]S �, l --- — I = Z E CD
Ta411---- --
i (1fec.ted by (printl: Site/Facility It) # P.O. # I Q @ E Acctnum: HUN E NVLNC
oi N E � - = d p Template:
Col ected by (sig ature): Rush? (tab MUST Be Natiiied} Date Results Needed p Q NO W Lr)
I '- E U O 11 N N Prelogin:
I _ Same Day ...........................200% E_ i O N ❑ r
_Next Day............................10746 Email?_No VYes Q �? C a- CV N N Z U iTSR: Eiunt
ImmediatelyTwo Day............................-50% 4_ N J try
1Packedon1c N — Y \X�u
.� Three Day ....................... -25% FAX? _No _Yes of • - I L y ZO Cooler:
to j to I �- ' 4 Q Shipped Via:
arrpleID Comp/Grab Matrix' Depth Date Time ntrs Z _m aCr Q7 T Z W W -- — -
{� LL LL LL C Z Z Q Rem.JC�ntammant SamPk r (Vah .fyl
)C a
5;1=, :a �FF ._�•_21 *. �Y.�^:;115t � I �I
Saai I faaar•r,' I nt 9-t i
Signed,Accu.at_e: YW VC•A Ze=-
$_tt,oe arri-ve intact: _ ]' _N
�Ct-tle5 used: }'—_ f7
PAC,' cr,eenITIt <,c. F e
rp
i
• Matrix: SS - Soil GW - Groundwater WW - Wastewater DW - Drinking Water OT - ether_ pH Temp
Remarks: A. Flow other Hold#
ReiingUistted b� : (Sig natu`el Date: Time: — Receiv Si mples returned via: 13 UPS Condition: (lah vse only}
��' Lr� J . FedEx ❑ Courier ❑
,Leh ws� by : (S r Da : Time: R ce-ived hy: (Signature) T p:r I to °C Bottles Received:
COC Seal intact: Y N NA
Relinquis by . Date: Time: Received for lab by: (Signature Date: Time: 3 pH Checked: NCF;

urofins
Environment Testing
America
ANALYTICAL REPORT
Eurofins Chicago
2417 Bond Street
University Park, IL 60484
Tel: [phone]
Laboratory Job ID: 500-212789-1
Client Project/Site: WG1822438
Foi
Pace Analytical National
12065 Lebanon Rd
Mt Juliet, Tennessee 37122
Attn: Jimmy Huckaba
Authorized for release by.
3/2/2022 2:50:33 PM
Sandie Fredrick, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval from the laboratory. For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
12
13
14

Client: Pace Analytical National
Project/Site: WG1822438
Laboratory Job ID: 500-212789-1
Table of Contents
Cover Page ..............................................
Table of Contents .........................................
2
Case Narrative ...........................................
3
Detection Summary ........................................
4
Method Summary .........................................
5
Sample Summary .........................................
6
Client Sample Results ......................................
7
Definitions ...............................................
8
QC Association ...........................................
9
QC Sample Results ........................................
10
Chronicle................................................
11
Certification Summary ......................................
12
Chain of Custody ..........................................
13
Receipt Checklists .........................................
14
12
13
14
Eurofins Chicago
Page 2 of 14 3/2/2022

Case Narrative
Client: Pace Analytical National
Project/Site: WG1822438
Job ID: 500-212789-1
Laboratory: Eurofins Chicago
Narrative
Job Narrative
500-212789-1
Comments
No additional comments
Job ID: 500-212789-1
Receipt
The sample was received on 2/24/2022 10:00 AM. Unless otherwise noted below, the sample arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 1.20 C.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
12
13
14
Eurofins Chicago
Page 3 of 14 3/2/2022

Detection Summary
Client: Pace Analytical National
Project/Site: WG1822438
Job ID: 500-212789-1
Client Sample ID: WW-1 Lab Sample ID: 500-212789-1
CAnalyte Result Qualifier LOQ LOD Unit Dil Fac D Method Prep Type
Sulfide 1330 393 186 mg/Kg 1 * 9034 Total/NA
This Detection Summary does not include radiochemical test results.
F47
12
13
14
Eurofins Chicago
Page 4 of 14 3/2/2022

Method Summary
Client: Pace Analytical National
Project/Site: WG1822438
Job ID: 500-212789-1
Method
Method Description
Protocol
Laboratory
9034
Sulfide, Acid soluble and Insoluble (Titrimetric)
SW846
TAL CHI
Moisture
Percent Moisture
EPA
TAL CHI
9030B
Sulfide, Distillation (Acid Soluble and Insoluble)
SW846
TAL CHI
Protocol References:
EPA= US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL CHI = Eurofins Chicago, 2417 Bond Street, University Park, IL 60484, TEL [phone]
12
13
14
Eurofins Chicago
Page 5 of 14 3/2/2022

Sample Summary
Client: Pace Analytical National
Project/Site: WG1822438
Lab Sample ID Client Sample ID
500-212789-1 WW-1
Matrix Collected Received
Solid 02/17/2210:30 02/24/2210:00
Job I D: 500-212789-1
12
13
14
Page 6 of 14
Eurofins C31Vp92022

Client Sample Results
Client: Pace Analytical National
Project/Site: WG1822438
Job ID: 500-212789-1
Client Sample ID: WW-1 Lab Sample ID: 500-212789-1
Date Collected: 02/17/22 10:30 Matrix: Solid
Date Received: 02/24/22 10:00 Percent Solids: 2.5
General Chemistry
Analyte Result Qualifier LOQ LOD Unit D Prepared Analyzed Dil Fac
Sulfide 1330 393 186 mg/Kg * 02/24/22 19:33 03/01/22 20:45 1
12
13
14
Eurofins Chicago
Page 7 of 14 3/2/2022

Definitions/Glossary
Client: Pace Analytical National
Project/Site: WG1822438
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
II Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level'
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRIES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Job ID: 500-212789-1
0
12
13
14
Eurofins Chicago
Page 8 of 14 3/2/2022

QC Association Summary
Client: Pace Analytical National
Project/Site: WG1822438
General Chemistry
Analysis Batch: 644340
Lab Sample ID
Client Sample ID
500-212789-1
WW-1
Prep Batch: 644397
Lab Sample ID
Client Sample ID
500-212789-1
WW-1
MB 500-644397/1-A
Method Blank
LCS 500-644397/2-A
Lab Control Sample
Analysis Batch: 645294
Lab Sample ID
Client Sample ID
500-212789-1
WW-1
MB 500-644397/1-A
Method Blank
LCS 500-644397/2-A
Lab Control Sample
Job ID: 500-212789-1
Prep Type Matrix Method Prep Batch
Total/NA Solid Moisture
Prep Type
Matrix
Method
Prep Batch
Total/NA
Solid
9030B
Total/NA
Solid
9030B
Total/NA
Solid
9030B
Prep Type
Matrix
Method
Prep Batch
Total/NA
Solid
9034
644397
Total/NA
Solid
9034
644397
Total/NA
Solid
9034
644397
12
13
14
Page 9 of 14
Eurofins Chicago
3/2/2022

QC Sample Results
Client: Pace Analytical National
Project/Site: WG1822438
Job I D: 500-212789-1
Method: 9034 - Sulfide, Acid soluble and Insoluble (Titrimetric)
Lab Sample ID: MB 500-644397/1-A Client Sample ID: Method Blank
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 645294 Prep Batch: 644397
MB MB
Analyte Result Qualifier LOQ LOD Unit D Prepared Analyzed Dil Fac
Sulfide <4.7 10.0 4.7 mg/Kg 02/24/22 19:24 03/01/22 20:31 1
Lab Sample ID: LCS 500-644397/2-A Client Sample ID: Lab Control Sample
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 645294 Prep Batch: 644397
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
Sulfide 198 161.8 mg/Kg 82 80 -120
12
13
14
Eurofins Chicago
Page 10 of 14 3/2/2022

Lab Chronicle
Client: Pace Analytical National
Job ID: 500-212789-1
Project/Site: WG1822438
Client Sample ID: WW-1
Lab Sample ID: 500-212789-1
Date Collected: 02/17/22 10:30
Matrix: Solid
Date Received: 02/24/22 10:00
Batch Batch
Dilution Batch Prepared
Prep Type Type Method
Run Factor Number or Analyzed Analyst Lab
Total/NA Analysis Moisture
1 644340 02/24/22 12:04 LWN TAL CHI
Client Sample ID: WW-1
Lab Sample ID: 500-212789-1
Date Collected: 02/17/22 10:30
Matrix: Solid
Date Received: 02/24/22 10:00
Percent Solids: 2.5
Batch
Batch
Dilution Batch
Prepared
Prep Type Type
Method
Run Factor Number
or Analyzed Analyst Lab
Total/NA Prep
9030B
644397
02/24/22 19:33 TMS TAL CHI
Total/NA Analysis
9034
1 645294
03/01/22 20:45 TMS TAL CHI
Laboratory References:
TAL CHI = Eurofins Chicago, 2417
Bond Street, University
Park, IL 60484, TEL [phone]
11
12
13
14
Page 11 of 14
Eurofins Chicago
3/2/2022

Accreditation/Certification Summary
Client: Pace Analytical National
Project/Site: WG1822438
Laboratory: Eurofins Chicago
The accreditations/certifications listed below are applicable to this report.
Job ID: 500-212789-1
Authority Program Identification Number Expiration Date
North Carolina (WW/SW) State 291 12-31-22
12
13
74
Eurofins Chicago
Page 12 of 14 3/2/2022

Sub -Contract Chain of Custody
Batch Date/Time: 02/23/22 11 12
Sub -Contract Lab 'I AUPI1.
��
aceAnalytical
lddress: 2417 Bond Street
r
City/State: UniversaN Park 11,
60484
12065 I ebanon Rd
Contact*
500.212789 COC
Mt Juliet TN 37122
Sandra.Fredrick, ( lEurofinset com
Phone [phone]
Owner Lab PACLMTJL
CVO. WG1822438
Fax [phone]
4ddress: 12065 I ebanon Rd
Email. M'IR SubOUtIearn &pacelabs corn
C ity/State: Mt Juliet 'IN 37122
Results Due Date: 03/04/22
Phone. (615) 773 t9756
LSC Purchase Order #: 11463165
Fax: [phone]
Send Reports to: James C Huckaba
Sample ID Me Collect Date Sample Number Sample Comments
Matrix State Cllate Description Container ID Lab Use Only Lab Use Only
WW-1 SS NC 02/17/22 10 30 Miscellaneous Analysis 2. L1463165-03 SULFIDE
Relinquished by:
-3 .i _ Datc
Recieved by: ti I Date
Relinquished by: Date
Reeieved by:
Page 13 of 14 3/2/2022

Client: Pace Analytical National
Login Number: 212789
List Number: 1
Creator: Scott, Sherri L
Question
Login Sample Receipt Checklist
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
True
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
N/A
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
1.2
Job Number: 500-212789-1
List Source: Eurofins Chicago
12
13
14
Eurofins Chicago
Page 14 of 14 3/2/2022

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lumberton
WWTP Name: City of Lumberton
Monitoring Period: From l/l/2022 To
WQ Permit Number:
NPDES Number:
3/31/2022
WQ0000672
NCL-024571
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)❑
Alt. C (Prior Testing)❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray 01
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density p
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
1 Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g �
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -pique
M inimu
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
725000
5540000
8.4E+07
CFU/ g
l
Quarterly
Grab
9222-MF
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 WN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
I Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
I Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
1 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Michael C Hunt, ORC
Preparer Name and Title (type or print)
Signature of Prepare *
Michael C Hunt, ORC
Land Applier Name and Title (if applicable)(type or print)
2/28/2023
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Cameron Testing Services, Inc. Laboratory Report
NC DEN R#654
NC PHHS 937799
US EPA #NC01918
Client;
Enviro-Choice Recycling CTS Proj.
2202-0160
DWCert#37799
Project:
City of Lumberton Regulatory
Yes
Sample Information
Sampled
C. Harris Date 02/17/22 Received ; J. Cameron
Date
02/17/22
Analyses and Results
Lab !D
x a
Sample ID '�°
o Anaiyte Result
_
c°, E
y
y �'
—' +'
Std. Methods
U
a
=
Reference
a
2202-0160 01
L1 Sludge Gr Fec. Coliform-S 3161114.86 CFUIg
79000
02/17/22 DPK
9222DY-MF
L2 84470000 CFutg
9310o
L3 12600000 CFurg
114000
L4 6620000 CFUlg
110060
L5 6530000 CFUr9
109000
L6 1520000 CFU1g
117000
L7 725000 CFUlg
121000
Geomean 5540000
2202-0160 01 L1 Sludge Gr TS (%)
2.68
%
0.01 02/17/22 DPK 2540 G -TS
L2
2.69
%
0.01
0
2.68
%
0.01
L4
2.68
,c
0.01
L5
2.71
%
0.01
L6
2.69
%
0.01
L7
2.69
ro
0.01
Report
Review
Project Manager Date
219 S. Steele Str, 919-208-4240
Sanford NC 27330 chris@camerontesting,com

!h
Cn
CL
i]
G1 . • �
�
w o K
Im
CL
50
v
\
fFJ
L
O
c
3
LJ'
_
z '
5
a O
H >
co
Z
_
E N
�ayao
ofco
Ms VOA
-o
1
t)
61
O,
ai
w
+
to
J i l
a�
'Y
R
to
r
euaeg
CS
d 009
� M
�
d ozz
<
Z
le`J Zll
N/A)
w z
G
X11jew
-7
�S
M
3
E
�+ C-j
c
/ dwoo
`c
6
ale(]
d
v
CL
0 ..
E
d
U
;i3
a
a
Q.
N
c�
t
V
C
O
a
Q
is
O
Q
CL
cU
0
CL
N
Z3
Cr
N
O
3
ZI
Of

13
ace Analytical ' ANALYTICAL REPORT
April 29, 2022
Hunt Environmental Associates
Sample Delivery Group: L1479OO4
Samples Received: 04/06/2022
Project Number:
Description: Enviro-Choice Recycling
Report To: Cody Hunt
3330 Saddletree Road
Lumberton, NC 28359
Entire Report Reviewed By: q�"h
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1479004 04/29/22 13:52 1 of 44

TABLE OF CONTENTS
Cp: Cover Page
FP
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
,i
Fss]
WW-2 L1479004-01
5
Fn
WW-2 L1479004-02
7
Qc: Quality Control Summary
Fr
Total Solids by Method 2540 B-2015
9
Total Solids by Method 2540 G-2011
10
Rc
Wet Chemistry by Method 350.1
11
F
Wet Chemistry by Method 351.2
13
Wet Chemistry by Method 353.2
14
[Al
Wet Chemistry by Method 365.4
15
Wet Chemistry by Method 365.4M
16
RC
Wet Chemistry by Method 4500 CN E-2016
17
Wet Chemistry by Method 4500NOrg C-2011
18
Wet Chemistry by Method 9012 B
20
Wet Chemistry by Method 9034-9030B
21
Wet Chemistry by Method 9040C
22
Wet Chemistry by Method 9045D
23
Wet Chemistry by Method 9056A
24
Wet Chemistry by Method D93/1010A
25
Mercury by Method 7470A
27
Mercury by Method 7471B
28
Metals (ICP) by Method 6010D
29
GI: Glossary of Terms
34
Al: Accreditations & Locations
35
Sc: Sample Chain of Custody
36
ACCOUNT: PROJECT: SDG:
DATE/TIME:
PAGE:
Hunt Environmental Associates L1479004
04/29/22 13:52
2 of 44

SAMPLE SUMMARY
Collected by Collected date/time Received date/time
WW-2 L1479004-01 Solid Carrigan Harris 04/05/2210:00 04/06/22 09:00 , C
P
Method
Total Solids by Method 2540 G-2011
Wet Chemistry by Method 350.1
Wet Chemistry by Method 365.4M
Wet Chemistry by Method 4500NOrg C-2011
Wet Chemistry by Method 9012 B
Wet Chemistry by Method 9034-9030B
Wet Chemistry by Method 9045D
Wet Chemistry by Method 9056A
Wet Chemistry by Method D93/1010A
Mercury by Method 7471B
Metals (ICP) by Method 6010D
WW-2 L1479004-02 GW
Method
Total Solids by Method 2540 B-2015
Wet Chemistry by Method 350.1
Wet Chemistry by Method 351.2
Wet Chemistry by Method 353.2
Wet Chemistry by Method 365.4
Wet Chemistry by Method 4500 CN E-2016
Wet Chemistry by Method 9040C
Wet Chemistry by Method D93/1010A
Mercury by Method 7470A
Metals (ICP) by Method 6010D
Metals (ICP) by Method 6010D
WW-2 L1479004-03 GW
Method
Subcontracted Analyses
WW-2 L1479004-04 Solid
Method
Subcontracted Analyses
Batch
Dilution Preparation
Analysis
date/time
date/time
WG1846469
1 04/11/2216:19
04/11/2216:48
WG1844429
1 04/07/22 05:23
04/09/22 14:13
WG1843982
5 04/13/221155
04/16/2210:34
WG1842878
2 04/10/22 09:32
04/13/22 09:39
WG1844268
1 04/11/22 07:50
04/12/2210:42
WG1844020
1 04/07/22 08:00
04/07/2217:00
WG1844496
1 04/07/22 07:00
04/07/22 09:00
WG1852617
1 04/22/22 00:15
04/22/22 03:12
WG1846803
1 04/12/22 02:25
04/12/22 02:25
WG1845221
1 04/09/2218:30
04/11/22 08:10
WG1844550
.1 04/07/2214:30
04/10/22 23:09
Analyst
MMF
LDT
LDT
LDT
LDT
CAG
GI
LBR
WOS
ABL
CCE
Location
FC
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fn
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fr
Mt. Juliet, TN
Mt. Juliet, TN
Rc
Mt. Juliet, TN
FGI
Collected by
Collected date/time
Received date/time
Carrigan Harris
04/05/22 10:00
04/06/22 09:00
SAI
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
1
04/08/221141
04/08/2212:03
MMF
Mt. Juliet, TN
RCWG1845394
WG1847045
50
04/12/2218:13
04/12/2218:13
SL
Mt. Juliet, TN
WG1846359
20
04/13/2217:53
04/15/2213:07
LDT
Mt. Juliet, TN
WG1845414
50
04/11/22 00:32
04/11/22 00:32
CAT
Mt. Juliet, TN
WG1849126
20
04/13/2217:53
04/15/221141
LDT
Mt. Juliet, TN
WG1844265
5
04/08/22 00:06
04/09/22 14:01
LDT
Mt. Juliet, TN
WG1845209
1
04/08/2214:45
04/08/2214:45
EPW
Mt. Juliet, TN
WG1846802
1
04/12/22 02:20
04/12/22 02:20
WOS
Mt. Juliet, TN
WG1847144
1
04/13/22 08:39
04/14/22 07:59
ABL
Mt. Juliet, TN
WG1846701
9
04/13/22 00:09
04/13/2215:50
ZSA
Mt. Juliet, TN
WG1848927
1
04/14/22 23:24
04/15/22 09:35
CCE
Mt. Juliet, TN
Collected by Collected date/time Received date/time
Carrigan Harris 04/05/22 10:00 04/06/22 09:00
Batch Dilution Preparation Analysis
date/time date/time
WG1844213 1 04/21/22 00:00 04/21/22 00:00
Analyst Location
Subcontract
Collected by Collected date/time Received date/time
Carrigan Harris 04/05/22 10:00 04/06/22 09:00
Batch Dilution Preparation Analysis Analyst Location
date/time date/time
WG1844213 1 04/21/22 00:00 04/21/22 00:00 Subcontract
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1479004 04/29/22 13:52 3 of 44

CASE NARRATIVE
FP
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
0
Fr
Rc
4�z
F,
Heather J Wagner
[Al
Project Manager
RC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 4500 CN E-2016.
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012 B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034-903013.
Sample WW-2 (11479004-02) could not be analyzed as a liquid for reactive sulfide or ortho phosphate due to the matrix ofthe
sample.
L1479004 -03, -04 contains subout data that is included after the chain of custody.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1479004 04/29/22 13:52 4 of 44

SAMPLE RESULTS - 01
L1479004
WW-2
Collected date/time: 04/05/22 10:00
Total Solids by Method 2540 G-2011
Result
Qualifier Dilution Analysis
Batch
Analyte %
date / time
Total Solids 2.48
1 04/11/202216:48
WG1846469
Wet Chemistry by Method 350.1
Result (dry)
Qualifier RDL (dry) Dilution
Analysis
Analyte mg/kg
mg/kg
date / time
Ammonia Nitrogen 6880
403 1
04/09/202214:13
Wet Chemistry by Method 365.4M
Batch
WG1844429
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Phosphorus, Total 17300 B 4030 5 04/16/202210:34 WG1843982
Wet Chemistry by Method 4500NOrg C-2011
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Kjeldahl Nitrogen, TKN 36100 1610 2 04/13/2022 09:39 WG1842878
Wet Chemistry by Method 9012 B
Result Qualifier
RDL
Analyte mg/kg
mg/kg
Reactive Cyanide ND
0.250
Wet Chemistry by Method 9034-9030B
Result Qualifier
RDL
Analyte mg/kg
mg/kg
Reactive Sulfide ND
75.0
Wet Chemistry by Method 9045D
Dilution Analysis Batch
date / time
1 04/12/202210:42 WG1844268
Dilution Analysis Batch
date / time
1 04/07/202217:00 WG1844020
Result Qualifier Dilution Analysis Batch
Analyte su date / time
pH 7.37 T8 1 04/07/2022 09:00 WG1844496
Sample Narrative:
L1479004-01 WG1844496: 7.37 at21C
Wet Chemistry by Method 9056A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Nitrate -Nitrite ND 806 1 04/22/2022 03:12 WG1852617
Phosphate,Ortho 619 202 1 04/22/2022 03:12 WG1852617
Wet Chemistry by Method D93/1010A
Result
Qualifier Dilution Analysis
Batch
Analyte Deg. F
date / time
Ignitability DNI at170
1 04/12/2022 02:25
WG1846803
Mercury by Method 7471B
Result (dry)
Qualifier RDL (dry) Dilution
Analysis
Analyte mg/kg
mg/kg
date / time
Mercury ND
1.61 1
04/11/2022 08:10
Batch
WG1845221
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1479004 04/29/22 13:52 5 of 44

SAMPLE RESULTS - 01
L1479004
WW-2
Collected date/time: 04/05/22 10:00
Metals (ICP) by Method 6010D
Result (dry)
Analyte
mg/kg
Aluminum
24900
Arsenic
11.6
Cadmium
ND
Calcium
13500
Chromium
132
Copper
595
Iron
18200
Lead
21.6
Magnesium
2470
Manganese
386
Molybdenum
6.66
Nickel
26.1
Potassium
4690
Selenium
ND
Sodium
23600
Sulfur
12800
Zinc
953
Qualifier RDL (dry)
mg/kg
80.6
8.06
2.02
403
4.03
8.06
40.3
2.02
403
4.03
2.02
8.06
202
8.06
403
403
20.2
Dilution Analysis
date / time
.1 04/10/2022 23:09
.1 04/10/2022 23:09
.1 04/10/2022 23:09
.1 04/10/2022 23:09
.1 04/10/2022 23:09
.1 04/10/2022 23:09
.1 04/10/2022 23:09
.1 04/10/2022 23:09
.1 04/10/2022 23:09
.1 04/10/2022 23:09
.1 04/10/2022 23:09
.1 04/10/2022 23:09
.1 04/10/2022 23:09
.1 04/10/2022 23:09
.1 04/10/2022 23:09
.1 04/10/2022 23:09
.1 04/10/2022 23:09
Batch
WG1844550
WG1844550
WG1844550
WG1844550
WG1844550
WG1844550
WG1844550
WG1844550
WG1844550
WG1844550
WG1844550
WG1844550
WG1844550
WG1844550
WG1844550
WG1844550
WG1844550
ACCOUNT: PROJECT: SDG: DATE/TIME:
Hunt Environmental Associates L1479004 04/29/22 13:52
PAGE:
6 of 44

SAMPLE RESULTS - 02
L1479004
WW-2
Collected date/time: 04/05/22 10:00
Total Solids by Method 2540 B-2015
Result
Qualifier Dilution
Analysis Batch
Analyte mg/I
date / time
Total Solids 35700
1
04/08/202212:03 WG1845394
Wet Chemistry by Method 350.1
Result
Qualifier RDL
Dilution Analysis Batch
Analyte mg/I
mg/I
date / time
Ammonia Nitrogen 174
12.5
50 04/12/2022 18:13 WG1847045
Wet Chemistry by Method 351.2
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date / time
Kjeldahl Nitrogen, TKN 248
Wet Chemistry by Method 353.2
5.00 20 04/15/202213:07 WG1846359
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date / time
Nitrate -Nitrite ND 5.00 50 04/11/2022 00:32 WG1845414
Sample Narrative:
L1479004-02 WG1845414: Dilution due to sulfide and iron hit.
Wet Chemistry by Method 365.4
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date / time
Phosphorus, Total 67.2 2.00 20 04/15/202211:41 WG1849126
Wet Chemistry by Method 4500 CN E-2016
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date / time
Reactive Cyanide ND 0.0250 5 04/09/202214:01 WG1844265
Sample Narrative:
L1479004-02 WG1844265: Dilution due to matrix.
Wet Chemistry by Method 9040C
Result Qualifier
Dilution Analysis
Batch
Analyte su
date / time
pH 7.44 T8
1 04/08/202214:45
WG1845209
Sample Narrative:
L1479004-02 WG1845209: 7.44 at17.8C
Wet Chemistry by Method D93/1010A
Result Qualifier
Dilution Analysis
Batch
Analyte deg F
date/time
Flashpoint DNF at170
1 04/12/2022 02:20
WG1846802
Mercury by Method 7470A
Analyte
Mercury
Result Qualifier RDL Dilution Analysis Batch
mg/I mg/I date / time
ND 0.000200 1 04/14/2022 07:59 WG1847144
— FP
— Fc
FS
-
Fn-
-
Rc
F,
[Al
Rc
ACCOUNT:
Hunt Environmental Associates
PROJECT:
SDG: DATE/TIME: PAGE:
L1479004 04/29/22 13:52 7 of 44

SAMPLE RESULTS - 02
L1479004
WW-2
Collected date/time: 04/05/22 10:00
Metals (ICP) by Method 6010D
Result
Analyte mg/I
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Sodium
Sulfur
Zinc
599
0.305
0.0196
341
3.17
16.2
404
0.357
63.9
9.65
0.163
0.452
115
0.0920
594
307
25.7
Qualifier
B
RDL
Dilution
Analysis
Batch
FPmg/I
date / time
1.80
9
04/13/202215:50
WG1846701
F
0.0900
9
04/13/202215:50
WG1846701
0.0180
9
04/13/202215:50
WG1846701
9.00
9
04/13/202215:50
WG1846701
Fss]
0.0900
9
04/13/202215:50
WG1846701
0.0900
9
04/13/202215:50
WG1846701
Fn
0.900
9
04/13/202215:50
WG1846701
0.0540
9
04/13/202215:50
WG1846701
9.00
9
04/13/202215:50
WG1846701
0.0900
9
04/13/202215:50
WG1846701
0.0450
9
04/13/202215:50
WG1846701
6
QC
0.0100
1
04/15/2022 09:35
WG1848927
18.0
9
04/13/202215:50
WG1846701
7GI
0.0900
9
04/13/202215:50
WG1846701
27.0
9
04/13/202215:50
WG1846701
9.00
9
04/13/202215:50
WG1846701
F
0.450
9
04/13/202215:50
WG1846701
RC
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1479004 04/29/22 13:52 3 of 44

WG1845394 QUALITY CONTROL SUMMARY
Total Solids by Method 2540 B-2015 L1479004-02
Method Blank (MB)
(MB) R3779657-1 04/03/22 12:03
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mg/I
Total Solids 1.00
L1477732-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1477732-01 04/03/22 12:03 • (DUP) R3779657-3 04/03/22 12:03
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I %_
Total Solids 3.00 5.00 1 0.000 5
Laboratory Control Sample (LCS)
(LCS) R3779657-2 04/03/22 12:03
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
Total Solids 9500 9530 100 92.5-108
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1479004 04/29/22 13:52 9 of 44

WG1846469
Total Solids by Method 2540 G-2011
Method Blank (MB)
(MB) R3730293-1 04/11/22 16:48
MB Result
Analyte
Total Solids 0.000
MB Qualifier MB MDL MB RDL
L1479814-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1479004-01
(OS) L1479314-01 04/11/22 16:48 • (DUP) R3730293-3 04/11/22 16:48
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte
Total Solids 11.5 10.6 1 8.22 10
Laboratory Control Sample (LCS)
(LCS) R3780293-2 04/11/22 16:48
Spike Amount LCS Result
Analyte
Total Solids 50.0 50.0
LCS Rec. Rec. Limits LCS Qualifier
100 85.0-115
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1479004 04/29/22 13:52 10 of 44

WG1844429 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 350.1 L1479004-01
Method Blank (MB)
(MB) R3779240-1 04/09/22 13:54
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Ammonia Nitrogen U 7.00 10.0
L1478842-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1473342-01 04/09/22 14:10 • (DUP) R3779240-5 04/09/22 1412
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
(dry) (dry) Limits
Analyte mg/kg mg/kg
Ammonia Nitrogen 1900 2070 1 8.63 20
Laboratory Control Sample (LCS)
(LCS) R3779240-2 04/09/22 13:55
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Ammonia Nitrogen 500 510 102
Rec. Limits LCS Qualifier
90.0-110
L1478149-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1473149-01 04/09/22 14:02 • (MS) R3779240-3 04/09/22 14:03 • (MSD) R3779240-4 04/09/22 14:04
Spike Amount Original Result
MS Result (dry)
MSD Result MS Rec.
MSD Rec. Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD RPD Limits
(dry) (dry)
(dry)
Analyte mg/kg mg/kg
mg/kg
mg/kg
Ammonia Nitrogen 40300 ND
40300
40700 100
101 1 80.0-120
0.995 20
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Hunt Environmental Associates
L1479004
04/29/22 13:52 11 of 44

WG1847045
Wet Chemistry by Method 350.1
Method Blank (MB)
(MB) R3730433-1 04/12/22 18:03
MB Result
Analyte mg/I
Ammonia Nitrogen U
MB Qualifier MB MDL MB RDL
mg/I mg/I
0.117 0.250
L1479003-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1479004-02
(OS) L1479003-01 04/12/22 18:10 • (DUP) R3730433-5 04/12/22 1812
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I %_
Ammonia Nitrogen 13.2 13.3 5 0.858 10
L1480106-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1430106-01 04/12/22 18:33 • (DUP) R3730433-7 04/12/22 18:34
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I
Ammonia Nitrogen ND ND 1 0.000 10
Laboratory Control Sample (LCS)
(LCS) R3780438-2 04/12/22 18:04
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
Ammonia Nitrogen 7.50 7.29 97.1
Rec. Limits LCS Qualifier
90.0-110
L1478920-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1473920-01 04/12/22 18:06 • (MS) R3730433-3 04/12/22 18:07 • (MSD) R3730433-4 04/12/22 18:09
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Ammonia Nitrogen 5.00
ND
4.83
4.83 96.6 96.5 1 90.0-110 0.104 10
L1479859-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1479359-01 04/12/22 18:30 • (MS) R3730433-6 04/12/22 18:31
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/I mg/I mg/I
Ammonia Nitrogen 5.00 ND 4.87 97.5 1 90.0-110
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1479004 04/29/22 13:52 12 of 44

WG1846359
Wet Chemistry by Method 351.2
Method Blank (MB)
(MB) R3731542-1 04/15/22 1141
MB Result
Analyte mg/I
Kjeldahl Nitrogen, TKN U
MB Qualifier MB MDL MB RDL
mg/I mg/I
0.140 0.250
L1478983-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1479004-02
(OS) L1473933-01 04/15/22 13:03 • (DUP) R3731542-7 04/15/22 13:05
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I %_
Kjeldahl Nitrogen, TKN 25.0 24.6 2 1.61 20
Laboratory Control Sample (LCS)
(LCS) R3781542-2 04/15/22 1142
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
Kjeldahl Nitrogen, TKN 12.7 14.2 112
Rec. Limits LCS Qualifier
75.2-120
L1478983-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1473933-01 04/15/22 1149 • (MS) R3731542-5 04/15/22 1152 • (MSD) R3731542-6 04/15/22 1153
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec.
Analyte mg/I mg/I mg/I mg/I
Kjeldahl Nitrogen, TKN 5.00 22.0 24.8 24.4 56.0 48.0
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
1 90.0-110 E V E V 1.63
RPD Limits
20
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1479004 04/29/22 13:52 13 of 44

WG1845414
Wet Chemistry by Method 353.2
Method Blank (MB)
(MB) R3779476-1 04/11/22 0013
MB Result
Analyte mg/I
Nitrate -Nitrite U
MB Qualifier MB MDL MB RDL
mg/I mg/I
0.0500 0.100
L1478743-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1479004-02
(OS) L1473743-01 04/11/22 00:17 • (DUP) R3779476-3 04/11/22 00:13
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I %_
Nitrate -Nitrite ND ND 1 0.000 20
L1479025-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1479025-02 04/11/22 00:37 • (DUP) R3779476-6 04/11/22 00:39
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I
Nitrate -Nitrite 0.160 ND 1 1.89 20
Laboratory Control Sample (LCS)
(LCS) R3779476-2 04/11/22 00:14
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
Nitrate -Nitrite 2.50 2.63 105 90.0-110
L1478743-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1473743-01 04/11/22 00:17 • (MS) R3779476-4 04/11/22 00:20 • (MSD) R3779476-5 04/11/22 00:21
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I
Nitrate -Nitrite 2.50 ND 2.64 2.43 106 97.2 1 90.0-110 8.28 20
L1479025-02 Original Sample (OS) • Matrix Spike (MS)
(OS) L1479025-02 04/11/22 00:37 • (MS) R3779476-7 04/11/22 00:40
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/I mg/I mg/I
Nitrate -Nitrite 2.50 0.160 2.84 107 1 90.0-110
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1479004 04/29/22 13:52 14 of 44

WG1849126
QUALITY CONTROL SUMMARY
Wet Chemistry by Method 365.4
L1479004-02
Method Blank (MB)
C p
(MB) R3731516-1 04/15/22 10:27
MB Result MB Qualifier MB MDL MB RDL
z
Analyte mg/I mg/I mg/I
TC
Phosphorus, Total U 0.0350 0.100
FSS
L1478983-01 Original Sample (OS) • Duplicate (DUP)
[�n]
(OS) L1473933-01 04/15/22 1127 • (DUP) R3731516-7 04/15/22 1128
Original Result DUP Result Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
5
Sr
Analyte mg/I mg/I
—
Phosphorus, Total 16.9 18.0 5 6.03
20
L1478996-01 Original Sample (OS) • Duplicate (DUP)
GI
(OS) L1473996-01 04/15/22 12:49 • (DUP) R3731516-8 04/15/22 12:51
Original Result DUP Result Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
FAI
Analyte mg/I mg/I
Phosphorus, Total 5.76 5.50 2 4.62
20
FS
Laboratory Control Sample (LCS)
(LCS) R3781516-2 04/15/22 10:28
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
Phosphorus, Total 3.78 3.54 93.7
Rec. Limits LCS Qualifier
83.2-116
L1478983-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1473933-01 04/15/22 10:36 • (MS) R3731516-4 04/15/22 10:38 • (MSD) R3731516-5 04/15/22 10:42
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I
Phosphorus, Total 2.50 16.1 18.0 17.8 76.0 68.0 1 90.0-110 E V E V 1.12 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1479004 04/29/22 13:52 15 of 44

WG1843982 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 365.4M L1479004-01
Method Blank (MB)
(MB) R3731737-1 04/15/22 15:56
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Phosphorus, Total 8.74 J 5.00 20.0
L1479695-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1479695-01 04/16/22 10:36 • (DUP) R3731737-7 04/16/22 10:37
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
(dry) (dry) Limits
Analyte %_
Phosphorus, Total 494 554 5 11.6 25
Laboratory Control Sample (LCS)
(LCS) R3781787-2 04/15/22 15:57
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Phosphorus, Total 151 131 86.5
Rec. Limits LCS Qualifier
78.9-121
L1479695-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1479695-02 04/16/22 10:39 • (MS) R3731737-8 04/16/22 10:40 • (MSD) R3731737-9 04/16/22 10:41
Spike Amount Original Result
MS Result (dry) MSD Result MS Rec.
MSD Rec. Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD RPD Limits
(dry) (dry)
(dry)
Analyte mg/kg
Phosphorus, Total 53.2 682
871 731 240
63.0 5 50.0-150
V 17.4 25
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Hunt Environmental Associates
L1479004
04/29/22 13:52 16 of 44

WG1844265
Wet Chemistry by Method 4500 CN E-2016
Method Blank (MB)
(MB) R3779236-1 04/09/22 1329
MB Result
Analyte mg/I
Reactive Cyanide U
QUALITY CONTROL SUMMARY
L1479004-02
MB Qualifier MB MDL MB RDL
mg/I mg/I
0.00180 0.00500
L1478929-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1473929-01 04/09/22 13:37 • (DUP) R3779236-3 04/09/22 13:33
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I %_
Reactive Cyanide ND ND 1 0.000 20
L1478996-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1473996-02 04/09/22 13:59 • (DUP) R3779236-8 04/09/22 14:00
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I
Reactive Cyanide ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3779236-2 04/09/22 13:30
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
Reactive Cyanide 0.100 0.102 102
Rec. Limits LCS Qualifier
87.1-120
L1478937-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1473937-02 04/09/22 13:43 • (MS) R3779236-4 04/09/22 13:44 • (MSD) R3779236-5 04/09/22 13:45
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Reactive Cyanide 0.100
ND
0.0961
0.0929 96.1 92.9 1 90.0-110 3.39 20
L1478977-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1473977-02 04/09/22 13:54 • (MS) R3779236-6 04/09/22 13:55 • (MSD) R3779236-7 04/09/22 13:56
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I
Reactive Cyanide 0.100 ND 0.0928 0.0985 92.8 98.5 1 90.0-110 5.96 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1479004 04/29/22 13:52 17 of 44

WG1842878
Wet Chemistry by Method 4500NOrg C-2011
Method Blank (MB)
(MB) R3730253-1 04/12/22 15:01
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Kjeldahl Nitrogen, TKN 5.60 J 4.48 20.0
L1479234-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1479004-01
(OS) L1479234-01 04/12/22 15:50 • (DUP) R3730253-10 04/12/22 15:51
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
(dry) (dry) Limits
Analyte mg/kg mg/kg %_
Kjeldahl Nitrogen, TKN 1340 1350 2 0.472 20
L1478842-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1473342-01 04/13/22 15:12 • (DUP) R3730253-11 04/13/22 1513
Original Result DUP Result DUP RPD
Dilution DUP RPD DUP Qualifier
(dry) (dry) Limits
Analyte mg/kg mg/kg
Kjeldahl Nitrogen, TKN 47600 43000 20 10.1 20
Laboratory Control Sample (LCS)
(LCS) R3780258-2 04/12/22 15:02
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Kjeldahl Nitrogen, TKN 508 456 89.8
Rec. Limits LCS Qualifier
75.2-121
L1478842-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1473342-01 04/12/22 15:23 • (MS) R3730253-6 04/12/22 15:26
Spike Amount Original Result MS Result (dry) MS Rec.
(dry) (dry)
Analyte mg/kg mg/kg mg/kg
Kjeldahl Nitrogen, TKN 1580 6520 6430 0.000
Dilution Rec. Limits MS Qualifier
1 90.0-110 E V
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1479004 04/29/22 13:52 13 of 44

WG1842878 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 4500NOrg C-2011 L1479004-01
L1479234-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1479234-01 04/12/22 15:23 • (MS) R3730253-8 04/12/22 15:34 • (MSD) R3730253-9 04/12/22 15:35
Spike Amount Original Result MS Result (dry) MSD Result MS Rec. MSD Rec.
(dry) (dry) (dry)
Analyte mg/kg mg/kg mg/kg mg/kg
Kjeldahl Nitrogen, TKN 476 1080 1080 1310 1.45 50.0
Dilution Rec. Limits MS Qualifier
1 90.0-110 E J6
MSD Qualifier RPD
E J6 19.3
RPD Limits
20
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1479004 04/29/22 13:52 19 of 44

WG1844268
Wet Chemistry by Method 9012 B
Method Blank (MB)
(MB) R3730034-1 04/12/22 10:35
MB Result
Analyte mg/kg
Reactive Cyanide U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
0.0390 0.250
L1479164-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1479004-01
(OS) L1479164-01 04/12/22 10:43 • (DUP) R3730034-3 04/12/22 10:44
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg
Reactive Cyanide 0.262 ND 1 94.2 P1 20
L1479171-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1479171-02 04/12/22 10:56 • (DUP) R3730034-6 04/12/22 10:57
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg
Reactive Cyanide ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3780084-2 04/12/22 10:36
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Reactive Cyanide 2.50 2.13 85.2
Rec. Limits LCS Qualifier
85.0-115
L1479164-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1479164-03 04/12/22 10:48 • (MS) R3730034-4 04/12/22 10:49 • (MSD) R3730034-5 04/12/22 10:50
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 1.67 ND 0.993 0.714 59.6 42.8 1 75.0-125 J6 J3 J6 32.8 20
L1479302-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1479302-02 04/12/22 11:05 • (MS) R3730034-7 04/12/22 11:04 • (MSD) R3730034-8 04/12/22 1106
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 1.67 ND 1.14 1.25 56.4 63.5 1 75.0-125 J6 J6 9.85 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1479004 04/29/22 13:52 20 of 44

WG1844020
Wet Chemistry by Method 9034-9030B
Method Blank (MB)
(MB) R3778746-1 04/07/22 1700
MB Result MB Qualifier MB MDL
Analyte mg/kg mg/kg
Reactive Sulfide U 30.0
Laboratory Control Sample (LCS)
(LCS) R3778746-2 04/07/22 17:00
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Reactive Sulfide 100 71.1 71.1
QUALITY CONTROL SUMMARY
L1479004-01
MB RDL
mg/kg
75.0
Rec. Limits LCS Qualifier
53.8-124
L1478931-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1473931-01 04/07/22 17:00 • (MS) R3778746-3 04/07/22 17:00 • (MSD) R3778746-4 04/07/22 17:00
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Sulfide 100 ND ND ND 59.2 55.8 1 10.0-136 0.000 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1479004 04/29/22 13:52 21 of 44

WG1845209 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9040C L1479004-02
L1478935-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1473935-01 04/03/22 14:45 • (DUP) R3779072-2 04/03/22 14:45
Original Result DUP Result Dilution DUP RPD
Analyte su su
pH 8.41 8.39 1 0.238
Sample Narrative:
OS: 8.41 at18.1C
DUP: 8.39 at18.4C
L1479188-05 Original Sample (OS) • Duplicate (DUP)
DUP Qualifier DUP RPD
Limits
(OS) L1479133-05 04/03/22 14:45 • (DUP) R3779072-3 04/03/22 14:45
Original Result DUP Result
Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte su su
pH 6.04 6.05
1 0.165 1
Sample Narrative:
OS: 6.04 at 18.5C
DUP: 6.05 at18.6C
Laboratory Control Sample (LCS)
(LCS) R3779072-1 04/03/22 14:45
Spike Amount LCS Result
LCS Rec. Rec. Limits LCS Qualifier
Analyte su su
pH 10.0 9.94
99.4 99.0-101
Sample Narrative:
LCS: 9.94 at19.4C
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates
L1479004 04/29/22 13:52 22 of 44

WG1844496 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9045D L1479004-01
L1478855-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1473355-02 04/07/22 09:00 • (DUP) R3773437-2 04/07/22 09:00
Original Result DUP Result Dilution DUP RPD
Analyte su su
pH 8.24 8.21 1 0.365
Sample Narrative:
OS: 8.24 at 21.2C
DUP: 8.21 at21.2C
L1479144-05 Original Sample (OS) • Duplicate (DUP)
DUP Qualifier DUP RPD
Limits
(OS) L1479144-05 04/07/22 09:00 • (DUP) R3773437-3 04/07/22 09:00
Original Result DUP Result
Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte su su
pH 7.79 7.79
1 0.000 1
Sample Narrative:
OS: 7.79 at21C
DUP 7.79 at21C
Laboratory Control Sample (LCS)
(LCS) R3773437-1 04/07/22 09:00
Spike Amount LCS Result
LCS Rec. Rec. Limits LCS Qualifier
Analyte su su
pH 10.0 9.93
99.3 99.0-101
Sample Narrative:
LCS:9.93 at20.2C
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates
L1479004 04/29/22 13:52 23 of 44

WG1852617 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9056A L1479004-01
Method Blank (MB)
(MB) R3734331-1 04/22/22 0110
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Nitrate -Nitrite U 1.06 20.0
Phosphate,Ortho U 1.19 5.00
L1480668-11 Original Sample (OS) • Duplicate (DUP)
(OS) L1430663-11 04/22/22 03:47 • (DUP) R3734331-3 04/22/22 04:22
Original Result
DUP Result
Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
Analyte mg/kg
mg/kg
Nitrate -Nitrite ND
ND
1 0.000
15
Phosphate,Ortho 7.08
6.23
1 12.8
15
L1480668-21 Original Sample (OS) • Duplicate (DUP)
(OS) L1430663-21 04/22/22 07:16 • (DUP) R3734331-4 04/22/22 09:01
Original Result
DUP Result
Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
Analyte mg/kg
mg/kg
Nitrate -Nitrite ND
ND
1 0.0981
15
Phosphate,Ortho 9.85
9.61
1 2.45
15
Laboratory Control Sample (LCS)
(LCS) R3784381-2 04/22/22 0145
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/kg
mg/kg
Nitrate -Nitrite 40.0
40.0
100
80.0-120
Phosphate,Ortho 20.0
18.3
91.6
80.0-120
L1480668-21 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1430663-21 04/22/22 07:16 • (MS) R3734331-5 04/22/22 09:36 • (MSD) R3734331-6 04/22/22 10:11
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
Analyte mg/kg
mg/kg
mg/kg
mg/kg
Nitrate -Nitrite 100
ND
118
118
104
104
1 80.0-120
0.106
Phosphate,Ortho 50.0
9.85
26.8
26.7
34.0
33.7
1 80.0-120
J6 J6 0.488
RPD Limits
15
15
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1479004 04/29/22 13:52 24 of 44

WG1846802 QUALITY CONTROL SUMMARY
Wet Chemistry by Method D93/1010A L1479004-02
L1479254-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1479254-01 04/12/22 02:20 • (DUP) R3779333-3 04/12/22 02:20
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte deg F deg F
Flashpoint 152 148 1 2.67 10
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3779888-1 04/12/22 02:20 • (LCSD) R3779888-2 04/12/22 02:20
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte deg F deg F deg F
Flashpoint 126 126 130 99.9 103 96.0-104 3.13 10
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1479004 04/29/22 13:52 25 of 44

WG1846803 QUALITY CONTROL SUMMARY
Wet Chemistry by Method D93/1010A L1479004-01
L1478633-04 Original Sample (OS) • Duplicate (DUP)
(OS) L1473633-04 04/12/22 02:25 • (DUP) R3779339-3 04/12/22 02:25
Original Result DUP Result Dilution DUP RPD
Analyte Deg. F Deg. F
Ignitability 120 124 1 3.28
L1479284-01 Original Sample (OS) • Duplicate (DUP)
DUP Qualifier DUP RPD
Limits
i
10
(OS) L1479234-01 04/12/22 02:25 • (DUP) R3779339-4 04/12/22 02:25
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte Deg. F Deg. F
Ignitability 162 158 1 2.50 10
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3779339-1 04/12/22 02:25 • (LCSD) R3779339-2 04/12/22 02:25
Spike Amount LCS Result LCSD Result LCS Rec.
LCSD Rec.
Rec. Limits LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyte Deg. F Deg. F Deg. F
Ignitability 126 124 126 98.3
99.9
95.6-104 1.60
10
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Hunt Environmental Associates
L1479004
04/29/22 13:52 26 of 44

WG1847144
Mercury by Method 7470A
Method Blank (MB)
(MB) R3730979-1 04/14/22 07:49
MB Result MB Qualifier MB MDL
Analyte mg/I mg/I
Mercury U 0.000100
Laboratory Control Sample (LCS)
(LCS) R3780979-2 04/14/22 07:51
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
Mercury 0.00300 0.00331 110
QUALITY CONTROL SUMMARY
L1479004-02
MB RDL
mg/I
0.000200
Rec. Limits LCS Qualifier
80.0-120
L1478817-16 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1473317-16 04/14/22 07:53 • (MS) R3730979-3 04/14/22 07:55 • (MSD) R3730979-4 04/14/22 07:57
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I
Mercury 0.00300 ND 0.00330 0.00322 110 107 1 75.0-125 2.27 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1479004 04/29/22 13:52 27 of 44

WG1845221
Mercury by Method 7471B
Method Blank (MB)
(MB) R3779633-1 04/11/22 07:58
MB Result MB Qualifier MB MDL
Analyte mg/kg mg/kg
Mercury U 0.0180
Laboratory Control Sample (LCS)
(LCS) R3779683-2 04/11/22 08:01
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Mercury 0.500 0.475 95.0
QUALITY CONTROL SUMMARY
L1479004-01
MB RDL
mg/kg
0.0400
Rec. Limits LCS Qualifier
80.0-120
L1479618-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1479613-02 04/11/22 08:03 • (MS) R3779683-3 04/11/22 08:05 • (MSD) R3779683-4 04/11/22 08:08
Spike Amount Original Result
MS Result (dry)
MSD Result MS Rec.
MSD Rec. Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD RPD Limits
(dry) (dry)
(dry)
Analyte mg/kg mg/kg
mg/kg
mg/kg
Mercury 0.582 ND
0.573
0.607 98.3
104 1 75.0-125
5.73 20
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Hunt Environmental Associates
L1479004
04/29/22 13:52 23 of 44

WG1844550
Metals (ICP) by Method 6010D
QUALITY CONTROL SUMMARY
L1479004-01
Method Blank (MB)
(MB) R3779526-1 04/10/22 22:49
MB Result MB Qualifier
Analyte
mg/kg
Aluminum
U
Arsenic
U
Cadmium
U
Calcium
U
Chromium
U
Copper
U
Iron
U
Lead
U
Magnesium
U
Manganese
U
Molybdenum
U
Nickel
U
Potassium
U
Selenium
U
Sodium
U
Sulfur
U
Zinc
U
Laboratory Control Sample (LCS)
(LCS) R3779526-2 04/10/22 22:52
Spike Amount
LCS Result
Analyte
mg/kg
mg/kg
Aluminum
1000
1040
Arsenic
100
101
Cadmium
100
103
Calcium
1000
1030
Chromium
100
103
Copper
100
106
Iron
1000
1030
Lead
100
105
Magnesium
1000
1030
Manganese
100
101
Molybdenum
100
108
Nickel
100
106
Potassium
1000
1010
Selenium
100
103
Sodium
1000
1070
Sulfur
1000
1030
MB MDL
mg/kg
6.08
0.518
0.0471
10.6
0.133
0.400
2.24
0.208
7.38
0.133
0.109
0.132
20.9
0.764
41.2
13.5
0.832
LCS Rec.
104
101
103
103
103
106
103
105
103
101
108
106
101
103
107
103
MB RDL
mg/kg
20.0
2.00
0.500
100
1.00
2.00
10.0
0.500
100
1.00
0.500
2.00
50.0
2.00
100
100
5.00
Rec. Limits
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
LCS Qualifier
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1479004 04/29/22 13:52 29 of 44

WG1844550
Metals (ICP) by Method 6010D
Laboratory Control Sample (LCS)
QUALITY CONTROL SUMMARY
L1479004-01
(LCS) R3779526-2 04/10/22 22:52
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg
Zinc 100 104 104 80.0-120
L1479076-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1479076-01 04/10/22 22:54 • (MS) R3779526-5 04/10/22 23:02 • (MSD) R3779526-6 04/10/22 23:04
Spike Amount
Original Result
MS Result (dry)
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
(dry)
(dry)
(dry)
Analyte
mg/kg
mg/kg
mg/kg
mg/kg
Aluminum
1010
3210
3840
6050
62.3
282
1 75.0-125
Arsenic
101
ND
104
95.0
102
92.5
1 75.0-125
Cadmium
101
ND
104
94.0
103
93.2
1 75.0-125
Calcium
1010
5400
8050
9820
263
440
1 75.0-125
Chromium
101
8.60
108
98.0
98.5
88.9
1 75.0-125
Copper
101
18.5
126
125
107
106
1 75.0-125
Iron
1010
5750
6250
9180
49.2
341
1 75.0-125
Lead
101
12.8
114
103
100
89.9
1 75.0-125
Magnesium
1010
2040
2620
4380
57.7
233
1 75.0-125
Manganese
101
220
342
363
121
141
1 75.0-125
Molybdenum
101
1.07
108
97.2
107
95.6
1 75.0-125
Nickel
101
10.9
119
114
107
103
1 75.0-125
Potassium
1010
739
1480
1520
73.2
77.4
1 75.0-125
Selenium
101
ND
105
93.3
104
92.7
1 75.0-125
Sodium
1010
244
1300
1630
105
138
1 75.0-125
Sulfur
1010
375
1430
1340
105
95.9
1 75.0-125
Zinc
101
50.5
153
156
101
105
1 75.0-125
MS Qualifier
MSD Qualifier
RPD
RPD Limits
J6
J3 J5
44.8
20
9.40
20
10.1
20
V
V
19.8
20
9.42
20
1.08
20
V
J3 V
38.0
20
9.74
20
J6
J3 J5
50.3
20
J5
5.92
20
10.8
20
4.09
20
J6
2.87
20
11.6
20
J3 J5
22.6
20
6.55
20
2.39
20
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1479004 04/29/22 13:52 30 of 44

WG1846701 QUALITY CONTROL SUMMARY
Metals (ICP) by Method 6010D L1479004-02
Method Blank (MB)
C
Fp
(MB) R3730757-1 04/13/22 15:10
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
E
Aluminum U
0.0561
0.200
Arsenic U
0.00440
0.0100
FS
Cadmium U
0.000479
0.00200
Calcium U
0.0793
1.00
Chromium 0.0246
0.00140
0.0100
FC n
Copper 0.00503
J
0.00368
0.0100
Iron 0.137
0.0180
0.100
E
Lead U
0.00299
0.00600
Magnesium U
0.0853
1.00
Manganese 0.00260
J
0.000934
0.0100
Molybdenum 0.00301
J
0.00116
0.00500
Potassium U
0.261
2.00
FG I
Selenium U
0.00735
0.0100
Sodium U
0.504
3.00
Sulfur 0.398
J
0.124
1.00
FA I
Zinc U
0.00652
0.0500
E
Laboratory Control Sample (LCS)
(LCS) R3730757-2 04/13/22 15:21
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
Aluminum 10.0
9.81
98.1
80.0-120
Arsenic 1.00
0.993
99.3
80.0-120
Cadmium 1.00
0.962
96.2
80.0-120
Calcium 10.0
9.85
98.5
80.0-120
Chromium 1.00
0.966
96.6
80.0-120
Copper 1.00
1.03
103
80.0-120
Iron 10.0
10.2
102
80.0-120
Lead 1.00
0.999
99.9
80.0-120
Magnesium 10.0
10.1
101
80.0-120
Manganese 1.00
0.924
92.4
80.0-120
Molybdenum 1.00
1.07
107
80.0-120
Potassium 10.0
9.25
92.5
80.0-120
Selenium 1.00
1.02
102
80.0-120
Sodium 10.0
9.72
97.2
80.0-120
Sulfur 10.0
9.45
94.5
80.0-120
Zinc 1.00
0.993
99.3
80.0-120
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1479004 04/29/22 13:52 31 of 44

WG1846701 QUALITY CONTROL SUMMARY
Metals (ICP) by Method 6010D L1479004-02
L1479441-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1479441-01 04/13/22 15:23 • (MS) R3730757-4 04/13/22 15:23 • (MSD) R3730757-5 04/13/22 15:31
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
mg/I
Aluminum
10.0
ND
10.1
9.88
99.9
98.1
1 75.0-125
1.85
20
Arsenic
1.00
ND
1.02
0.998
102
99.8
1 75.0-125
2.17
20
Cadmium
1.00
ND
0.973
0.955
97.3
95.5
1 75.0-125
1.88
20
Calcium
10.0
31.0
40.5
40.0
94.4
89.9
1 75.0-125
1.13
20
Chromium
1.00
ND
0.986
0.975
98.6
97.5
1 75.0-125
1.14
20
Copper
1.00
ND
1.06
1.05
106
105
1 75.0-125
0.534
20
Iron
10.0
0.162
10.6
10.4
104
103
1 75.0-125
1.76
20
Lead
1.00
ND
1.01
0.990
101
99.0
1 75.0-125
2.12
20
Magnesium
10.0
5.25
15.4
15.2
102
99.9
1 75.0-125
1.21
20
Manganese
1.00
0.191
1.12
1.11
92.5
91.7
1 75.0-125
0.682
20
Molybdenum
1.00
ND
1.09
1.06
109
106
1 75.0-125
2.44
20
Potassium
10.0
ND
10.6
10.4
92.1
90.0
1 75.0-125
1.97
20
Selenium
1.00
ND
1.05
1.02
105
102
1 75.0-125
2.64
20
Sodium
10.0
ND
10.7
10.5
97.8
95.4
1 75.0-125
2.21
20
Sulfur
10.0
2.35
11.6
11.4
92.9
90.9
1 75.0-125
1.70
20
Zinc
1.00
ND
1.02
0.993
101
98.2
1 75.0-125
2.32
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1479004 04/29/22 13:52 32 of 44

WG1848927
Metals (ICP) by Method 6010D
Method Blank (MB)
(MB) R3731521-1 04/15/22 09:09
MB Result
MB Qualifier MB MDL
Analyte mg/I
mg/I
Nickel 0.00196
J 0.00161
Laboratory Control Sample (LCS)
(LCS) R3781521-2 04/15/22 09:12
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
Nickel 1.00 0.959 95.9
QUALITY CONTROL SUMMARY
L1479004-02
MB RDL
mg/I
0.0100
Rec. Limits LCS Qualifier
80.0-120
L1480306-09 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1430306-09 04/15/22 09:15 • (MS) R3731521-4 04/15/22 09:20 • (MSD) R3731521-5 04/15/22 09:23
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I
Nickel 1.00 ND 0.972 0.973 96.7 96.8 1 75.0-125 0.0976 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1479004 04/29/22 13:52 33 of 44

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contactyour project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
u
Fc
Fss]
(dry)
Results are reported based on the dry weight ofthe sample. [this will only be present on a dry report basis for soils].
MDL
Method Detection Limit.
Fn
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Fr
RDL (dry)
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
Fc
SDG
Sample Delivery Group.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
F
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Rc
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
B
The same analyte is found in the associated blank.
E
The analyte concentration exceeds the upper limit ofthe calibration range ofthe instrument established by the initial
calibration (ICAL).
J
The identification ofthe analyte is acceptable, the reported value is an estimate.
J3
The associated batch QC was outside the established quality control range for precision.
J5
The sample matrix interfered with the ability to make any accurate determination, spike value is high.
J6
The sample matrix interfered with the ability to make any accurate determination, spike value is low.
P1
RPD value not applicable for sample concentrations less than 5 times the reporting limit.
T8
Sample(s) received past/too close to holding time expiration.
v
The sample concentration is too high to evaluate accurate spike recoveries.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates
L1479004 04/29/22 13:52 34 of 44

ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
Nebraska
N E-OS-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TNO02
California
2932
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704 _
Georgia
NELAP
North Carolina 3
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky' 6
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee'"
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas5
LABO152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A2 LA
A2LA— ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1479004 04/29/22 13:52 35 of 44

Company Name/Address
Billing Information:
An 1 cm
I rnntninpr
I Pr
�pruarivp
Chain of Custody Page _of _
Hunt Environmental Associates
Accounts Payable Pres
3330
Po sox 39D chk
ace-
Saddletree Road
Lumberton, NC 28359
Lumberton, NC 28359
PEOVtE 0.CVANCIN6 SEIENCe
i
Q
MT JULIET, TN
Report to:
Email To: [e-mail]
Cody Hunt
N
17WS Lebanon Rd M-1 h 1.t. TN 37122
LL.I
a
to
`
M
y
Svbe,m,ng a sample via this cham of cunndv
ecrutWe,nk—led,mentandaueptanceofthe
Vacs T.— nd Candilenc rcund a[.
hrt'ir-ma """ "' w rsrpa:-,t:-m.a-
Project Description:
Enviro-Choice Recycling
Cit State %
Y/ /
Collected: L
I ease Circle:
7PT
,
,i',l/�(,�W'
MT CT
'A
a
_
p
M
2
r,r., pol
Phone: 9i$-G,34w&9M
Client Project #
Lab Project #
n
Q
HUNTENVLNC-ENVIRO
E
E
5nr,
10 73 S311
a
v
¢
�,
`0.
Z
Q
N
a
E
z
U
1079
9
CAI ected by (print):
Site/Facility ID #
P.O- #Ln
r I i.1
W
�
o
o
N
C:
d
�
O
E
i
U
p
o`
O
CL
O
�
H
rn
4�
+
�
ad
p
Z
l�Pr
Z
Acctnum: HUNEll
Template:T177683
Collected (signatur ):
Quote 9
Rush? (Lab MUST Be Notified) Q
Same Day Five Day
Md,�
Day 5 Day (Rad Only) Date Results Needed
E
'�
E
V
O
q.
,z
fl.
a
artI
P912250
.Ne>R
p
z,I
PM: 673 - Heather J Wagner
: 873:
_Two Day _ SD Day (Rad Only} No
0
C
✓�1
N
E
Packed on ice N_ Y %�
_ Three Day
tof
=
/ti
r"i
tj
Q
_
LA
.M
us
M
C)
{,j
a
a
to
�.i
V
PB: ya
Sample ID
Comp/Grab Matrix' Depth Date
Time ntrs
Shipped Via: Fed EX Ground
Remarks sample n jla6 only}
c
Q
ai
y
=
Z
`
O
L
O
=
t1
w
aC
5S r� : o 6
X
X
X
X
d f
kf "�.....-._
GW
ZZ
c
_
X
X
X
X
X
X
�L o
+77
' Matrix:
emarks:Metals= AI,As,Cd,Ca,Cr,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,S,Se,Na,Zn,Hg
Sargple Receipth tl
SS - Soil AIR - Air F- Filter
pH
Temp
COC Zeal Present/intact: _N
GW- Groundwater 8-Bioassay
_Y
COC Signed/Accurate: N
WW- WasteWater
Flow
Other
Bottles arrive intact: N
-Drinking Water
^orrect bottles used: I,,
v*
OT
OT -Other
Samples returned via:
Tracking #
UPS FedEx
O
ev
Sufficient volume sent:
It Apol ry; le
_ _ —Courier
�/
VCA Zero Headspace: Y _N
Relin uish by - Si ature)
Date: Time: Receiv : [Signature]
2 Trip Blank Received: Yes / o
Presezvation Correct/checked: _Y _N
HCLeoH
RAD Screen <0.5 mR/hr: Jf N
T
(� r
TBR
d b ignature
I)Atee: f
Time:
Received b o ignature)
Temp pC Bottles Received:
If preservation required by Login: Date/Time
P
1-5
d by : ignature)
Date:
Time:
Rec v d f lab by: f Signatures
Dat
Time'
Hold:
d9ciom
f✓
©
C / OK

Company Name/Address Billing Information:
Hunt Environmental Associates Accounts Payable LCh
PO Box 390
3330 Saddletree Road Lumberton, NC 28359
Lumberton, NC 28359
Report to Email To: [e-mail]
Cody Hunt
Project Description:
Pro1 P
N
City/State /State
ll
Please Circle
Enviro-Choice Recycling
Collected: G 'V
PT MT CT
Na
`
Phone:910- -
Client Project #
Lab Project #
HUNTENVLNC-ENVIRO
a �b i3� rj3i1
°
z
In
Q
QJollected
Collected by {print):
Site/Facility ID #
P.C.tr
Q
E
=
N
Z
Z
Li.l
0.
b Ignature): 1�
Rush) [Lab MUST Be Notified} Quote #
Five Day
Same Day _
5 Day Only) Needed I
Q
_ Next Day (Rad Date Results
N
�
Z
Z
Immediately
X
Two Day _ 10 Day (Rod Only} I No
rrj
Packed on Ice N_ Y
Three Day of
4�n
<
co
rm
Z
z
0
Lt1
rV
Sample ID
Comp/Grab
Matrix'
Depth
Date
rI� ntrs
Time 1
la -I
IA
ss
I ASIA
I Ll]Ai
-11
1 1 Y 10
1 6
Matrix:
- Soil AIR -Air F - Filter
N - Groundwater B - Bioassay
W - WasteWater
N - prinking W
f - Other / A
by
rks:Metals= AI,As,Cd,Ca,Cr,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,S,Se,Na,Zn,Hg
Samples returned via:
UPS _ FedEx _ Courier
Date:
4/s/2 L
Date:
Date:
Tracking # 1
Time: Received (Signature)
,21--
Time: Received by: (Si ature)
Time: I RekeivN fo la by: (Signature)
pH
Temp_
Flow
Other_
rip Blank RWeiveof.
Yes N�
HcL'7 n
TBR
Temp;y
pC Botttes Reu
Datel I
Time:
Chain of Custody Page _ of
ace,
p EOPLE aeYaNLINS SCIENCE
MT JULIET, TN
L2065 Lebanon lad Mount lulwt, TN a)Iil
Subm-t "I a Sa"e na Ihy chain of-stody
pns ..v acknowle g—t and acceptance of the
0— Terms and com4dwns Iound at:
Zps'Mnfo. parelabt. rom)hubItfpas standard
te,—.pdf
SDG #
Table d j
4cctnum: HUNENVLNC
remplate7177683
PreloQin: P912250
PM: 873 - Heather J Wagner
PB: 7-/7_' JV2a —
Shipped Via: Ill Ground
Remarks I Sample k (lab only)
61
Sample Receipt Checklist
CDC Seal Present;lntact: NP Y N
CDC Signed/Accurate: Y -_ N
Bottles arrive intake.: Y N
Correct bottles used: _ Y _N
Sufficient volu-le sent: Y _N
.; A oa
VoA Zero Headspace: _Y __N
Preservation Correct/Checked: _YN
RAD Screen <0.5 mR/hr: /Y ,N
I if preservation required by Login:
Hold:
Coalition:
�/ OK

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lumberton
WWTP Name: City of Lumberton
Monitoring Period: From 4/l/2022 To
WQ Permit Number:
NPDES Number:
6/30/2022
WQ0000672
NCL-024571
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)❑
Alt. C (Prior Testing)❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray 01
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density p
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
1 Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g �
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -pique
M inimu
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
785000
1240000
1.3E+07
CFU/ g
l
Quarterly
Grab
9222-MF
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 WN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
I Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
I Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
1 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Michael C Hunt, ORC
Preparer Name and Title (type or print)
Signature of Prepare *
Michael C Hunt, ORC
Land Applier Name and Title (if applicable)(type or print)
2/28/2023
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Cameron Testing Services, Inc. Laboratory Report
Cl' Enviro-Choice Recycling CTS Proj.
R City of Lumberton Regulatory
Sample Information
Sampled Date 04/05/22 Received
Analyses and Results
2204-0046
Yes
M. Sims
NC DENR #654
NC PHHS 937799
US EPA #NC01918
DW Cert # 37799
Date 04/05/22
ID
Sample ID
E
Q
Analyte
Result
`
O
°'fl �Lab +=
Std. Methods
rY
o
Reference
2204-0046
-01
3ludgi
Gr
Fec. Coliform-S
604000
CFUrg
245000
04/06/22 CSC
9222D - MF
-02
920000
CFUrg
101000
-03
1180000
CFU1g
102000
-04
785000
CFU1g
90800
-05
789000
CFUIg
87300
-06
12800000
CFUIg
113000
-p7
874000
CFUIg
122000
Geomean
1240000
97100
2204-0046
-01
nudge
Gr
TS (%)
2.74
%
0.01
04/07/22 CSC
2540 G -TS
-02
2.73
%
0.01
-03
2.72
%
0.01
-04
2.73
%
0.01
-05
2.86
%
0.01
-06
2.76
%
0.01
-07
2.74
%
0.01
Report
Review
Project Manager Date
219 S. Steele Str, 919-208-4240
Sanford NC 27330 [e-mail]

a
0
a
U d
O
C
\�
E �
4
i
Ck
I
EE
CL
�
CD
� z O
I ! �
❑
�
�i I j
H
r
a
s o
mrn�
_E z _
N N_
N
mar
a
�I
U
\
aay10
Of
;as don
I
I
en
d -1 G
I
L
01
�
LIJs�jJB�
I j 1 I �
y
d OQ9
E
d ON
�5
Z
L
y
p
N/A) GO]'
o;
xla;LW
J
0
�j
c
dwoo
a!
`1
E
avaicc l
E
a
u? CI
'- a
v V W

13
ace Analytical ' ANALYTICAL REPORT
October 04, 2022
Hunt Environmental Associates
Sample Delivery Group: L152752O
Samples Received: 08/20/2022
Project Number:
Description: Enviro-Choice Recycling
Report To: Cody Hunt
3330 Saddletree Road
Lumberton, NC 28359
Entire Report Reviewed By: q�"h
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1527520 10/04/22 11:22 1 of 20

TABLE OF CONTENTS
Cp: Cover Page
FP
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
,i
Fss]
WW-3 L1527520-01
5
Fn
WW-3 L1527520-02
6
Qc: Quality Control Summary
Fr
Wet Chemistry by Method 350.1
7
Wet Chemistry by Method 351.2
8
Rc
Wet Chemistry by Method 365.4
9
F
Wet Chemistry by Method 4500H+ B-2011
10
Wet Chemistry by Method 9012 B
11
[Al
Wet Chemistry by Method 9034-9030B
12
Wet Chemistry by Method 9056A
13
RC
Wet Chemistry by Method D93/1010A
14
Mercury by Method 245.1
15
Metals (ICP) by Method 200.7
16
GI: Glossary of Terms
18
Al: Accreditations & Locations
19
Sc: Sample Chain of Custody
20
ACCOUNT: PROJECT:
SDG: DATE/TIME:
PAGE:
Hunt Environmental Associates
L1527520 10/04/22 11:22
2 of 20

SAMPLE SUMMARY
WW-3 L1527520-01 WW
Collected by
Carrigan Harris
Collected date/time
08/18/22 09:00
Received date/time
08/20/22 09:00
FP
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
F
Wet Chemistry by Method 350.1
WG1916267
50
08/25/2218:07
08/25/2218:07
BMD
Mt. Juliet, TN
Wet Chemistry by Method 351.2
WG1917750
20
08/30/22 06:56
08/31/22 00:59
LDT
Mt. Juliet, TN
Wet Chemistry by Method 365.4
WG1918910
50
08/30/22 06:56
08/30/2217:40
LDT
Mt. Juliet, TN
Wet Chemistry by Method 4500H+ B-2011
WG1918225
1
08/29/2218:00
08/29/2218:00
CRB
Mt. Juliet, TN
Wet Chemistry by Method D93/1010A
WG1914763
1
08/23/22 03:12
08/23/22 03:12
WOS
Mt. Juliet, TN
Fn
Mercury by Method 245.1
WG1916974
10
08/27/22 09:08
08/29/2212:43
SRT
Mt. Juliet, TN
Metals (ICP) by Method 200.7
WG1914457
5
08/24/22 22:07
08/26/2215:23
KMG
Mt. Juliet, TN
Fr
Collected by
Collected date/time
Received date/time
WW-3 L1527520-02 Solid
Carrigan Harris
08/18/22 09:00
08/20/22 09:00
Rc
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
Fdate/time
Wet Chemistry by Method 9012 B
WG1918479
60
08/31/22 09:21
08/31/22 22:17
CAT
Mt. Juliet, TN
Wet Chemistry by Method 9034-9030B
WG1933427
1
09/28/2218:30
09/30/22 20:29
AW
Mt. Juliet, TN
F
Wet Chemistry by Method 9056A
WG1921471
1
09/05/22 22:15
09/06/22 00:42
GEB
Mt. Juliet, TN
RC
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Hunt Environmental Associates
L1527520
10/04/22 11:22
3 of 20

CASE NARRATIVE
FP
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
0
Fr
Rc
4�z
F,
Heather J Wagner
[Al
Project Manager
RC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012 B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034-903013.
Sample Delivery Group (SDG) Narrative
The following analysis were performed from an unpreserved, insufficiently or inadequately preserved sample.
Lab Sample ID Project Sample ID Method
L1527520-01 W W-3 350.1
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1527520 10/04/22 11:22 4 of 20

SAMPLE RESULTS - 01
L1527520
WW-3
Collected date/time: 08/18/22 09:00
Wet Chemistry by Method 350.1
Result
Qualifier RDL
Dilution
Analysis
Batch
Analyte mg/I
mg/I
date / time
Ammonia Nitrogen 53.3
12.5
50
08/25/202218:07
WG1916267
Wet Chemistry by Method 351.2
Result
Qualifier RDL
Dilution
Analysis
Batch
Analyte mg/I
mg/I
date / time
Kjeldahl Nitrogen, TKN 194
5.00
20
08/31/2022 00:59
WG1917750
Wet Chemistry by Method 365.4
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date / time
Phosphorus, Total 144 5.00 50 08/30/202217:40 WG1918910
Wet Chemistry by Method 4500H+ B-2011
Result Qualifier Dilution Analysis Batch
Analyte— su date / time
pH 7.19 T8 1 08/29/202218:00 WG1918225
Sample Narrative:
L1527520-01 WG1918225: 7.19 at 22C
Wet Chemistry by Method D93/1010A
Result Qualifier Dilution Analysis Batch
Analyte deg F date/time
Flashpoint DNF at170 1 08/23/2022 03:12 WG1914763
Mercury by Method 245.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date / time
Mercury 0.00843
Metals (ICP) by Method 200.7
Analyte
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
0.00200 10 08/29/202212:43 WG1916974
Result Qualifier RDL Dilution Analysis Batch
mg/I mg/I date / time
0.495
10.0
0.0244
6.04
0.690
ND
0.0922
0.0500
5
08/26/202215:23
WG1914457
0.0250
5
08/26/202215:23
WG1914457
0.0100
5
08/26/202215:23
WG1914457
0.0500
5
08/26/202215:23
WG1914457
0.0250
5
08/26/202215:23
WG1914457
0.0500
5
08/26/202215:23
WG1914457
0.0250
5
08/26/202215:23
WG1914457
— FP
— Fc
FS
-
Fn-
-
Rc
F,
[Al
Rc
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1527520 10/04/22 11:22 5 of 20

SAMPLE RESULTS - 02
L1527520
WW-3
Collected date/time: 08/18/22 09:00
Wet Chemistry by Method 9012 B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Reactive Cyanide ND 15.0 60 08/31/2022 22:17 WG1918479
Sample Narrative:
L1527520-02 WG1918479: Dilution due to matrix.
Wet Chemistry by Method 9034-9030B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Reactive Sulfide 120 T8 75.0 1 09/30/2022 20:29 WG1933427
Wet Chemistry by Method 9056A
Analyte
Nitrate -Nitrite
Result Qualifier RDL Dilution Analysis Batch
mg/kg mg/kg date / time
51.1 20.0 1 09/06/2022 00:42 WG1921471
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1527520 10/04/22 11:22 6 of 20

WG1916267
QUALITY CONTROL SUMMARY
Wet Chemistry by Method 350.1
L1527520-01
Method Blank (MB)
C p
(MB) R3830600-1 03/25/22 1703
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mg/I
TC
I
Ammonia Nitrogen U 0.117 0.250
FS
L1527344-03 Original Sample (OS) • Duplicate (DUP)
[�n]
(OS) L1527344-03 03/25/22 17:29 • (DUP) R3330600-7 03/25/22 17:30
Original Result DUP Result Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
F
Analyte mg/I mg/I
Ammonia Nitrogen ND ND 1 0.000
10
L1527700-01 Original Sample (OS) • Duplicate (DUP)
GI
(OS) L1527700-01 03/25/22 17:45 • (DUP) R3330600-9 03/25/22 17:47
Original Result DUP Result Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
FAI
Analyte mg/I mg/I
Ammonia Nitrogen 3.47 3.50 1 1.03
10
FS
Laboratory Control Sample (LCS)
(LCS) R3830600-2 08/25/22 1705
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
Ammonia Nitrogen 7.50 8.00 107
Rec. Limits LCS Qualifier
90.0-110
L1527556-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1527556-01 03/25/22 17:42 • (MS) R3330600-8 03/25/22 17:44
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/I mg/I mg/I
Ammonia Nitrogen 5.00 0.924 6.66 115 1 90.0-110 J5
L1527344-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1527344-02 03/25/22 17:24 • (MS) R3330600-5 03/25/22 17:26 • (MSD) R3330600-6 03/25/22 17:27
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Ammonia Nitrogen 5.00
ND
5.76
5.86 115 117 1 90.0-110 J5 J5 1.65 10
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1527520 10/04/22 11:22 7 of 20

WG1917750
Wet Chemistry by Method 351.2
Method Blank (MB)
(MB) R3332171-1 03/31/22 00:21
MB Result
Analyte mg/I
Kjeldahl Nitrogen, TKN U
MB Qualifier MB MDL MB RDL
mg/I mg/I
0.140 0.250
L1526657-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1527520-01
(OS) L1526657-01 03/31/22 00:24 • (DUP) R3332171-3 03/31/22 00:25
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I
Kjeldahl Nitrogen, TKN 3.01 3.11 1 3.27 20
L1527098-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1527093-01 03/31/22 00:29 • (DUP) R3332171-6 03/31/22 00:30
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I
Kjeldahl Nitrogen, TKN 1.08 0.910 1 17.1 20
Laboratory Control Sample (LCS)
(LCS) R3832171-2 08/31/22 00:22
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
Kjeldahl Nitrogen, TKN 12.7 12.0 94.5
Rec. Limits LCS Qualifier
75.2-120
L1526657-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1526657-01 03/31/22 00:24 • (MS) R3332171-4 03/31/22 00:26 • (MSD) R3332171-5 03/31/22 00:28
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Kjeldahl Nitrogen, TKN 5.00
3.01
7.49
7.86 89.6 97.0 1 90.0-110 J6 4.82 20
L1527098-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1527093-01 03/31/22 00:29 • (MS) R3332171-7 03/31/22 00:32
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/I mg/I mg/I
Kjeldahl Nitrogen, TKN 5.00 1.08 5.50 88.4 1 90.0-110 J6
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1527520 10/04/22 11:22 3 of 20

WG1918910
QUALITY CONTROL SUMMARY
Wet Chemistry by Method 365.4
L1527520-01
Method Blank (MB)
C p
(MB) R3832125-1 03/30/22 1708
MB Result MB Qualifier MB MDL MB RDL
z
Analyte mg/I mg/I mg/I
TC
Phosphorus, Total U 0.0350 0.100
FSS
L1526657-01 Original Sample (OS) • Duplicate (DUP)
[�n]
(OS) L1526657-01 03/30/22 17:11 • (DUP) R3332125-3 03/30/22 1712
Original Result DUP Result Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
5
Sr
Analyte mg/I mg/I
Phosphorus, Total 4.29 4.18 1 2.60
20
L1527098-01 Original Sample (OS) • Duplicate (DUP)
GI
(OS) L1527093-01 03/30/22 17:16 • (DUP) R3332125-6 03/30/22 1717
Original Result DUP Result Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
FAI
Analyte mg/I mg/I
Phosphorus, Total 0.481 0.419 1 13.8
20
FS
Laboratory Control Sample (LCS)
(LCS) R3832125-2 08/30/22 1709
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
Phosphorus, Total 3.78 3.25 86.0
Rec. Limits LCS Qualifier
83.2-116
L1526657-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1526657-01 03/30/22 17:11 • (MS) R3332125-4 03/30/22 17:13 • (MSD) R3332125-5 03/30/22 1714
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I
Phosphorus, Total 2.50 4.29 5.87 6.28 63.2 79.6 1 90.0-110 E J6 E J6 6.75 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1527520 10/04/22 11:22 9 of 20

WG1918225 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 4500H+ B-2011 L1527520-01
L1527219-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1527219-01 03/29/22 13:00 • (DUP) R3331663-2 03/29/22 13 00
Original Result DUP Result Dilution DUP RPD
Analyte su su
pH 6.90 6.92 1 0.289
Sample Narrative:
OS: 6.9 at20.5C
DUP:6.92 at20.6C
L1527322-01 Original Sample (OS) • Duplicate (DUP)
DUP Qualifier DUP RPD
Limits
(OS) L1527322-01 03/29/22 13:00 • (DUP) R3331663-3 03/29/22 13 00
Original Result DUP Result
Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte su su
pH 7.76 7.76
1 0.000 1
Sample Narrative:
OS: 7.76 at22C
DUP 7.76 at22.1C
Laboratory Control Sample (LCS)
(LCS) R3331663-1 03/29/22 13 00
Spike Amount LCS Result
LCS Rec. Rec. Limits LCS Qualifier
Analyte su su
pH 10.0 9.93
99.3 99.0-101
Sample Narrative:
LCS: 9.93 at 23.4C
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates
L1527520 10/04/22 11:22 10 of 20

WG1918479
QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9012 B
L1527520-02
Method Blank (MB)
C p
(MB) R3332663-1 03/31/22 22:12
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TC
I
Reactive Cyanide U 0.0390 0.250
FS
L1528460-04 Original Sample (OS) • Duplicate (DUP)
[�n]
(OS) L1523460-04 03/31/22 22:29 • (DUP) R3832663-3 03/31/22 22:30
Original Result DUP Result Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
F
Analyte mg/kg mg/kg
Reactive Cyanide ND ND 1 0.000
20
L1528460-08 Original Sample (OS) • Duplicate (DUP)
GI
(OS) L1523460-08 03/31/22 22:38 • (DUP) R3832663-6 03/31/22 22:39
Original Result DUP Result Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
1711
Analyte mg/kg mg/kg
Reactive Cyanide ND ND 1 0.000
20
FSc
Laboratory Control Sample (LCS)
(LCS) R3832663-2 08/31/22 2213
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Reactive Cyanide 2.50 2.43 97.3
Rec. Limits LCS Qualifier
85.0-115
L1528460-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1523460-05 03/31/22 22:31 • (MS) R3832663-4 03/31/22 22:32 • (MSD) R3832663-5 03/31/22 22:33
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 1.66 ND 1.53 1.48 86.9 83.9 1 75.0-125 3.31 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1527520 10/04/22 11:22 11 of 20

WG1933427
Wet Chemistry by Method 9034-9030B
Method Blank (MB)
(MB) R3843547-1 09/30/22 2029
MB Result MB Qualifier MB MDL
Analyte mg/kg mg/kg
Reactive Sulfide U 30.0
Laboratory Control Sample (LCS)
(LCS) R3843547-2 09/30/22 2029
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Reactive Sulfide 100 78.8 78.8
QUALITY CONTROL SUMMARY
L1527520-02
MB RDL
mg/kg
75.0
Rec. Limits LCS Qualifier
53.8-124
L1539225-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1539225-02 09/30/22 20:29 • (MS) R3843547-3 09/30/22 20:29 • (MSD) R3843547-4 09/30/22 20:29
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec.
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Sulfide 100 ND ND ND 0.000 0.000
Sample Narrative:
MS: Matrix spike failure due to matrix interference.
MSD: Matrix spike failure due to matrix interference.
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
1 10.0-136 J6 J6 0.000 20
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1527520 10/04/22 11:22 12 of 20

WG1921471
Wet Chemistry by Method 9056A
Method Blank (MB)
(MB) R3833995-3 09/05/22 2320
MB Result
Analyte mg/kg
Nitrate -Nitrite U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
1.06 20.0
L1530966-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1527520-02
(OS) L1530966-01 09/06/22 03:23 • (DUP) R3833995-5 09/06/22 03:41
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg
Nitrate -Nitrite ND ND 1.04 8.94 15
L1531093-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1531093-02 09/06/22 04:52 • (DUP) R3833995-8 09/06/22 05:10
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg
Nitrate -Nitrite ND ND 1 4.59 15
Laboratory Control Sample (LCS)
(LCS) R3833995-4 09/05/22 23:38
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Nitrate -Nitrite 40.0 39.1 97.9
Rec. Limits LCS Qualifier
80.0-120
L1530966-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1530966-01 09/06/22 03:23 • (MS) R3833995-6 09/06/22 03:59 • (MSD) R3833995-7 09/06/22 0417
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec.
Analyte mg/kg mg/kg mg/kg mg/kg
Nitrate -Nitrite 99.7 ND 97.2 101 95.9 99.4
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
1 80.0-120 3.55 15
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1527520 10/04/22 11:22 13 of 20

WG1914763 QUALITY CONTROL SUMMARY
Wet Chemistry by Method D93/1010A L1527520-01
L1527591-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1527591-01 03/23/22 03:12 • (DUP) R3329035-3 03/23/22 03:12
Original Result DUP Result Dilution DUP RPD
Analyte deg F deg F
Flashpoint DNF at170 DNF at170 1 0.000
L1527817-01 Original Sample (OS) • Duplicate (DUP)
DUP Qualifier DUP RPD
Limits
i
10
(OS) L1527317-01 03/23/22 03:12 • (DUP) R3329035-4 03/23/22 03:12
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte deg F deg F
Flashpoint DNF at200 DNF at200 1 0.000 10
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3329035-1 03/23/22 03:12 • (LCSD) R3329035-2 03/23/22 0312
Spike Amount LCS Result LCSD Result LCS Rec.
LCSD Rec.
Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte deg F deg F deg F
Flashpoint 126 130 128 103
101
96.0-104 1.55 10
ACCOUNT:
PROJECT:
SDG: DATE/TIME: PAGE:
Hunt Environmental Associates
L1527520 10/04/22 11:22 14 of 20

WG1916974
Mercury by Method 245.1
Method Blank (MB)
(MB) R3331531-1 03/29/22 12:20
MB Result MB Qualifier MB MDL
Analyte mg/I mg/I
Mercury U 0.000100
Laboratory Control Sample (LCS)
(LCS) R3831531-2 08/29/22 12:22
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
Mercury 0.00300 0.00302 101
QUALITY CONTROL SUMMARY
L1527520-01
MB RDL
mg/I
0.000200
Rec. Limits LCS Qualifier
85.0-115
L1528759-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1523759-01 03/29/22 12:24 • (MS) R3331531-3 03/29/22 12:27 • (MSD) R3331531-4 03/29/22 12:29
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Mercury 0.00300
ND
0.00304
0.00301 101 100 1 70.0-130 1.05 20
L1529088-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1529033-01 03/29/22 12:36 • (MS) R3331531-5 03/29/22 12:38 • (MSD) R3331531-6 03/29/22 12:41
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I
Mercury 0.00300 ND 0.00290 0.00263 96.6 87.8 1 70.0-130 9.58 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1527520 10/04/22 11:22 15 of 20

WG1914457 QUALITY CONTROL SUMMARY
Metals (ICP) by Method 200.7 L1527520-01
Method Blank (MB)
(MB) R3830988-1 03/26/22 1405
MB Result
MB Qualifier MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
Arsenic U
0.00645
0.0100
Barium U
0.000795
0.00500
Cadmium U
0.000552
0.00200
Chromium U
0.00163
0.0100
Lead U
0.00227
0.00500
Selenium U
0.00616
0.0100
Silver U
0.00131
0.00500
Laboratory Control Sample (LCS)
(LCS) R3830988-2 08/26/22 1407
Spike Amount
LCS Result
Analyte
mg/I
mg/I
Arsenic
1.00
0.966
Barium
1.00
1.00
Cadmium
1.00
0.985
Chromium
1.00
0.972
Lead
1.00
0.998
Selenium
1.00
1.01
Silver
0.200
0.180
LCS Rec. Rec. Limits LCS Qualifier
96.6
100
98.5
97.2
99.8
101
90.1
85.0-115
85.0-115
85.0-115
85.0-115
85.0-115
85.0-115
85.0-115
L1526657-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1526657-01 03/26/22 14:10 • (MS) R3330933-4 03/26/22 1415
Spike Amount
Original Result
MS Result
MS Rec.
Analyte
mg/I
mg/I
mg/I
Arsenic
1.00
ND
0.980
98.0
Barium
1.00
0.0277
1.02
99.1
Cadmium
1.00
ND
0.991
99.1
Chromium
1.00
ND
0.966
95.9
Lead
1.00
ND
0.986
98.6
Selenium
1.00
ND
1.02
102
Silver
0.200
ND
0.182
91.0
Dilution Rec. Limits
1 70.0-130
1 70.0-130
1 70.0-130
1 70.0-130
1 70.0-130
1 70.0-130
1 70.0-130
MS Qualifier
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1527520 10/04/22 11:22 16 of 20

WG1914457 QUALITY CONTROL SUMMARY
Metals (ICP) by Method 200.7 L1527520-01
L1526657-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1526657-01 03/26/22 14:10 • (MS) R3330933-5 03/26/22 1417
Spike Amount
Original Result
MS Result
MS Rec.
Dilution Rec. Limits MS Qualifier
Analyte
mg/I
mg/I
mg/I
Arsenic
1.00
ND
0.997
99.7
1 70.0-130
Barium
1.00
0.0277
1.04
101
1 70.0-130
Cadmium
1.00
ND
1.01
101
1 70.0-130
Chromium
1.00
ND
0.983
97.7
1 70.0-130
Lead
1.00
ND
1.01
101
1 70.0-130
Selenium
1.00
ND
1.04
104
1 70.0-130
Silver
0.200
ND
0.186
92.8
1 70.0-130
L1527353-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1527353-01 03/26/22 14:20 • (MS) R3330933-6 03/26/22 14:23 • (MSD) R3330933-7 03/26/22 14:26
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
mg/I
mg/I
mg/I
mg/I
Arsenic
1.00
0.0229
1.13
1.12
110
110
1 70.0-130
Barium
1.00
0.0489
1.02
1.02
97.5
97.4
1 70.0-130
Cadmium
1.00
ND
1.08
1.08
108
108
1 70.0-130
Chromium
1.00
ND
0.967
0.964
96.7
96.4
1 70.0-130
Lead
1.00
0.00696
1.05
1.05
104
104
1 70.0-130
Selenium
1.00
0.391
1.58
1.57
119
118
1 70.0-130
Silver
0.200
ND
0.204
0.205
102
103
1 70.0-130
MS Qualifier MSD Qualifier RPD
RPD Limits
0.169
20
0.0778
20
0.142
20
0.304
20
0.0124
20
0.428
20
0.518
20
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1527520 10/04/22 11:22 17 of 20

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contactyour project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
u
Fc
Fss]
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
Fn
RDL
Reported Detection Limit.
Rec.
Recovery.
Fr
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
U
Not detected at the Reporting Limit (or MDL where applicable).
Fc
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
F
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
LEI
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
E
The analyte concentration exceeds the upper limit ofthe calibration range ofthe instrument established by the initial
calibration (ICAL).
J5
The sample matrix interfered with the abilityto make any accurate determination, spike value is high.
J6
The sample matrix interfered with the abilityto make any accurate determination, spike value is low.
T8
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates
L1527520 10/04/22 11:22 13 of 20

ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
Nebraska
N E-OS-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TNO02
California
2932
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704 _
Georgia
NELAP
North Carolina 3
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky' 6
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee'"
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas5
LABO152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A2 LA
A2LA— ISO17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1527520 10/04/22 11:22 19 of 20

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lumberton
WWTP Name: City of Lumberton
Monitoring Period: From 7/l/2022 To
WQ Permit Number:
NPDES Number:
9/30/2022
WQ0000672
NCL-024571
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)❑
Alt. C (Prior Testing)❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray 01
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density p
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
1 Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g �
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -pique
M inimu
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
2210000
3120000
4640000
CFU/ g
l
Quarterly
Grab
9222-MF
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 WN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
I Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
I Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
1 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Michael C Hunt, ORC
Preparer Name and Title (type or print)
Signature of Prepare *
Michael C Hunt, ORC
Land Applier Name and Title (if applicable)(type or print)
2/28/2023
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Cameron Testing Services, Inc. Laboratory Report
NC DENR#654
NC PHHS #37799
US EPA #NC01918
Client:
Enviro-Choice Recycling CTS Proj.
2208-0261
DWCert#37799
Project:
City of Lumberton Regulatory
Yes
Sample Information
Sampled
Date 08/26/22 Received
J.
Cameron Bate
08/26/22
Analyses and Results
Lab ID
CL
E L
Sample ID a e9 Analyte Result
'E
Std. Methods
v
c ©
Reference
2208-0261 01
-01 51udgE Gr Fec. Coliform-S 2370000
CFU/g
84800
08/26/22 CSC
9222D - MF
-02 3040000
CFUIg
122000
-03 4640000
GFUlg
119000
-04 3610000
CFU1g
95000
-05 2210000
cFurg
tomoo
-06 3350000
CFUrg
98500
-07 3230000
CFUrg
108000
Geomean 3120000
CFulg
2208-0261 01
-01 Sludge Gr TS (%) 1.04%
0.01
09/01/22 ERP
2540 G -TS
-02 1.16%
0.01
-03 1.17%
0.01
-04 1.39%
0.01
-05 1.33%
0.01
-06 1.34%
0.01
-07 1.16%
0.01
Report
Review
Project Manager Date
219 S. Steele Str. 919-208-4240
Sanford NC 27330 [e-mail]

f
Q
�
' )
;
\§7
I
ƒ
7
§s2
■7$\
�
f
Er
#
t
K
7
z
-
$
, m
z
�f\WS
VOA
�
�
t
§
§
d It
v 2
�
em
m §
.
3
®
/ (
I
•�
�
-
d cog
�z
M
k
§ $
§
d 2U
§
_�
z
Q §
..
2
2
/
f
I*w)�
Ems.
z
§
xgen
�
$
3
I
q` E
/
2
1d$o0
<
.
`�
E
aw±\
■
:
L-C!
•�,
}�)
cc
CL
m
V)
Q co E
7
u
.�
\
Z�
% J

13
ace Analytical ' ANALYTICAL REPORT
November 29, 2022
Hunt Environmental Associates
Sample Delivery Group: L1559561
Samples Received: 11/18/2022
Project Number:
Description: Enviro-Choice Recycling
Report To: Cody Hunt
3330 Saddletree Road
Lumberton, NC 28359
Entire Report Reviewed By: q�"h
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1559561 11/29/22 16:29 1 of 21

TABLE OF CONTENTS
Cp: Cover Page
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
WW-3 L1559561-01
5
Qc: Quality Control Summary
7
Total Solids by Method 2540 G-2011
7
Wet Chemistry by Method 350.1
8
Wet Chemistry by Method 365.4M
10
Wet Chemistry by Method 4500NOrg C-2011
11
Wet Chemistry by Method 9012 B
12
Wet Chemistry by Method 9034-9030B
13
Wet Chemistry by Method 9045D
14
Wet Chemistry by Method 9056A
15
Wet Chemistry by Method D93/1010A
16
Mercury by Method 7471B
17
Metals (ICP) by Method 6010D
18
GI: Glossary of Terms
19
Al: Accreditations & Locations
20
Sc: Sample Chain of Custody
21
ACCOUNT: PROJECT: SDG:
DATE/TIME: PAGE:
Hunt Environmental Associates L1559561
11/29/22 16:29 2 of 21

SAMPLE SUMMARY
Collected by Collected date/time Received date/time
WW-3 L1559561-01 Solid Carrigan Harris 11/17/22 09:35 11/18/22 09:00 , C
P
Method
Batch
Dilution
Preparation
Analysis
Analyst
date/time
date/time
Total Solids by Method 2540 G-2011
WG1962847
1
11/22/2210:20
11/22/22 10:38
CMK
Wet Chemistry by Method 350.1
WG1963217
1
11/28/221118
11/29/22 1136
CAT
Wet Chemistry by Method 365.4M
WG1963223
5
11/27/22 17:30
11/28/2217:18
CAT
Wet Chemistry by Method 4500NOrg C-2011
WG1963220
5
11/27/22 17:29
11/28/2216:10
CAT
Wet Chemistry by Method 9012 B
WG1963212
3
11/24/2216:19
11/28/221109
JCS
Wet Chemistry by Method 9034-9030B
WG1963060
1
11/22/22 09:50
11/24/22 08:31
CAG
Wet Chemistry by Method 9045D
WG1964541
1
11/25/22 09:30
11/25/22 1130
KAD
Wet Chemistry by Method 9056A
WG1963305
1
11/23/2216:45
11/23/22 22:11
LBR
Wet Chemistry by Method D93/1010A
WG1962791
1
11/21/22 03:00
11/21/22 03:00
WOS
Mercury by Method 7471B
WG1962672
1
11/23/22 09:43
11/24/221100
SRT
Metals (ICP) by Method 6010D
WG1963650
1
11/23/2215:02
11/24/2218:37
KMG
Location
FC
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fn
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fr
Mt. Juliet, TN
Mt. Juliet, TN
Rc
Mt. Juliet, TN
F,
SAI
RC
ACCOUNT: PROJECT: SDG: DATE/TIME:
Hunt Environmental Associates L1559561 11/29/22 16:29
PAGE:
3 of 21

CASE NARRATIVE
FP
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
0
Fr
Rc
4�z
F,
Heather J Wagner
[Al
Project Manager
RC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012 B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034-903013.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1559561 11/29/22 16:29 4 of 21

SAMPLE RESULTS - 01
L1559561
WW-3
Collected date/time: 11/17/22 09:35
Total Solids by Method 2540 G-2011
Result
Qualifier Dilution Analysis
Batch
Analyte %
date / time
Total Solids 2.66
1 11/22/202210:38
WG1962847
Wet Chemistry by Method 350.1
Result (dry)
Qualifier RDL (dry) Dilution
Analysis
Analyte mg/kg
mg/kg
date / time
Ammonia Nitrogen 465
376 1
11/29/20221136
Wet Chemistry by Method 365.4M
Batch
WG1963217
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Phosphorus, Total 15300 3760 5 11/28/202217:18 WG1963223
Wet Chemistry by Method 4500NOrg C-2011
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Kjeldahl Nitrogen, TKN 61400 V 3760 5 11/28/202216:10 WG1963220
Wet Chemistry by Method 9012 B
Result Qualifier
RDL
Analyte mg/kg
mg/kg
Reactive Cyanide ND
0.750
Wet Chemistry by Method 9034-9030B
Result Qualifier
RDL
Analyte mg/kg
mg/kg
Reactive Sulfide ND
75.0
Wet Chemistry by Method 9045D
Dilution Analysis Batch
date / time
3 11/28/20221109 WG1963212
Dilution Analysis Batch
date / time
1 11/24/2022 08:31 WG1963060
Result Qualifier
Dilution Analysis
Batch
Analyte su
date / time
pH 7.12 T8
1 11/25/20221130
WG1964541
Sample Narrative:
L1559561-01 WG1964541:7.12 at20.4C
Wet Chemistry by Method 9056A
Result (dry) Qualifier
RDL (dry) Dilution
Analysis
Analyte mg/kg
mg/kg
date / time
Nitrate -Nitrite ND
752 1
11/23/2022 22:11
Wet Chemistry by Method D93/1010A
Batch
WG1963305
Result Qualifier Dilution Analysis Batch
Analyte Deg. F date / time
Ignitability DNI at170 1 11/21/2022 03:00 WG1962791
Mercury by Method 7471B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 1.50 1 11/24/20221100 WG1962672
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1559561 11/29/22 16:29 5 of 21

SAMPLE RESULTS - 01
L1559561
WW-3
Collected date/time: 11/17/22 09:35
Metals (ICP) by Method 6010D
Result (dry)
Analyte
mg/kg
Arsenic
ND
Barium
169
Cadmium
ND
Chromium
136
Lead
ND
Selenium
ND
Silver
ND
Qualifier RDL (dry)
mg/kg
75.2
18.8
18.8
37.6
18.8
75.2
37.6
Dilution Analysis
date / time
1 11/24/202218:37
1 11/24/202218:37
1 11/24/202218:37
1 11/24/202218:37
1 11/24/202218:37
1 11/24/202218:37
1 11/24/202218:37
Batch
WG1963650
WG1963650
WG1963650
WG1963650
WG1963650
WG1963650
WG1963650
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1559561 11/29/22 16:29 6 of 21

WG1962847
Total Solids by Method 2540 G-2011
Method Blank (MB)
(MB) R3364272-1 11/22/22 10:38
MB Result
Analyte
Total Solids 0.00200
MB Qualifier MB MDL MB RDL
L1559657-03 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1559561-01
(OS) L1559657-03 11/22/22 10:38 • (DUP) R3864272-3 11/22/22 10:38
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte % % %_
Total Solids 81.8 81.7 1 0.165 10
Laboratory Control Sample (LCS)
(LCS) R3864272-2 11/22/22 10:38
Spike Amount LCS Result
Analyte
Total Solids 50.0 50.0
LCS Rec. Rec. Limits LCS Qualifier
100 85.0-115
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1559561 11/29/22 16:29 7 of 21

WG1963217 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 350.1 L1559561-01
Method Blank (MB)
(MB) R3366055-1 11/29/22 11:18
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Ammonia Nitrogen U 7.00 10.0
L1559179-17 Original Sample (OS) • Duplicate (DUP)
(OS) L1559179-17 11/29/22 1123 • (DUP) R3366055-3 11/29/22 1125
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
(dry) (dry) Limits
Analyte mg/kg mg/kg
Ammonia Nitrogen ND ND 1 0.000 20
L1559561-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1559561-01 11/29/22 1136 • (DUP) R3366055-6 11/29/22 1137
Original Result DUP Result DUP RPD
Dilution DUP RPD DUP Qualifier
(dry) (dry) Limits
Analyte mg/kg mg/kg
Ammonia Nitrogen 465 464 1 0.269 20
Laboratory Control Sample (LCS)
(LCS) R3866055-2 11/29/22 1120
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg
Ammonia Nitrogen 500 540 108 90.0-110
L1559179-17 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1559179-17 11/29/22 1123 • (MS) R3366055-4 11/29/22 1126 • (MSD) R3366055-5 11/29/22 1127
Spike Amount Original Result MS Result (dry) MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
(dry) (dry) (dry)
Analyte mg/kg mg/kg mg/kg mg/kg
Ammonia Nitrogen 599 ND 616 622 103 104 1 80.0-120 0.922 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1559561 11/29/22 16:29 3 of 21

WG1963217 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 350.1 L1559561-01
L1559561-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1559561-01 11/29/22 1136 • (MS) R3366055-7 11/29/22 1139
Spike Amount Original Result MS Result (dry) MS Rec.
(dry) (dry)
Analyte mg/kg mg/kg mg/kg
Ammonia Nitrogen 18800 465 20600 107
Dilution Rec. Limits MS Qualifier
1 80.0-120
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1559561 11/29/22 16:29 9 of 21

WG1963223 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 365.4M L1559561-01
Method Blank (MB)
(MB) R3365761-1 11/23/22 16:41
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Phosphorus, Total U 5.00 20.0
L1559561-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1559561-01 11/23/22 1718 • (DUP) R3365761-9 11/23/22 1719
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
(dry) (dry) Limits
Analyte mg/kg mg/kg
Phosphorus, Total 15300 14800 5 3.81 25
Laboratory Control Sample (LCS)
(LCS) R3865761-2 11/28/22 16:42
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Phosphorus, Total 151 154 102
Rec. Limits LCS Qualifier
78.9-121
L1559561-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1559561-01 11/23/22 1718 • (MS) R3365761-10 11/23/22 1720 • (MSD) R3365761-11 11/23/22 1722
Spike Amount Original Result
MS Result (dry)
MSD Result MS Rec.
MSD Rec. Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD RPD Limits
(dry) (dry)
(dry)
Analyte mg/kg mg/kg
mg/kg
mg/kg
Phosphorus, Total 7520 15300
21400
20600 80.1
70.2 5 50.0-150
3.57 25
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Hunt Environmental Associates
L1559561
11/29/22 16:29 10 of 21

WG1963220
Wet Chemistry by Method 4500NOrg C-2011
Method Blank (MB)
(MB) R3865731-1 11/23/22 1514
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Kjeldahl Nitrogen, TKN U 4.48 20.0
L1559561-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1559561-01
(OS) L1559561-01 11/23/22 16:10 • (DUP) R3365731-9 11/23/22 16:11
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
(dry) (dry) Limits
Analyte mg/kg mg/kg
Kjeldahl Nitrogen, TKN 61400 62600 5 1.98 20
Laboratory Control Sample (LCS)
(LCS) R3865731-2 11/28/22 15:15
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Kjeldahl Nitrogen, TKN 508 524 103
Rec. Limits LCS Qualifier
75.2-121
L1559561-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1559561-01 11/23/22 16:10 • (MS) R3365731-10 11/23/22 16:13 • (MSD) R3365731-11 11/23/22 16:14
Spike Amount Original Result
MS Result (dry)
MSD Result MS Rec.
MSD Rec. Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD RPD Limits
(dry) (dry)
(dry)
Analyte mg/kg mg/kg
mg/kg
mg/kg
Kjeldahl Nitrogen, TKN 15000 61400
76000
71100 97.0
64.4 5 90.0-110
V 6.67 20
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Hunt Environmental Associates
L1559561
11/29/22 16:29 11 of 21

WG1963212
QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9012 B
L1559561-01
Method Blank (MB)
C p
(MB) R3365736-1 11/23/22 1105
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TC
I
Reactive Cyanide U 0.0390 0.250
FS
L1559700-01 Original Sample (OS) • Duplicate (DUP)
[�n]
(OS) L1559700-01 11/23/22 1110 • (DUP) R3865736-3 11/23/22 1111
Original Result DUP Result Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
F
Analyte mg/kg mg/kg
Reactive Cyanide ND ND 1 27.0
P1 20
L1560754-05 Original Sample (OS) • Duplicate (DUP)
GI
(OS) L1560754-05 11/23/22 1126 • (DUP) R3865736-6 11/23/22 1129
Original Result DUP Result Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
FAI
Analyte mg/kg mg/kg
Reactive Cyanide ND ND 1 0.000
20
FSc
Laboratory Control Sample (LCS)
(LCS) R3865736-2 11/28/22 1106
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Reactive Cyanide 2.50 2.33 93.3
Rec. Limits LCS Qualifier
85.0-115
L1560545-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1560545-02 11/23/22 11:17 • (MS) R3865736-4 11/23/22 1118 • (MSD) R3865736-5 11/23/22 1119
Spike Amount Original Result MS Result
MSD Result MS Rec.
MSD Rec. Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg
mg/kg
Reactive Cyanide 1.67 ND 3.20
3.13 192
188 1 75.0-125
J5 J5 2.24 20
Sample Narrative:
MS: Matrix spike failure due to matrix interference.
MSD: Matrix spike failure due to matrix interference.
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Hunt Environmental Associates
L1559561
11/29/22 16:29 12 of 21

WG1963060
Wet Chemistry by Method 9034-9030B
Method Blank (MB)
(MB) R3364771-1 11/24/22 08:31
MB Result
Analyte mg/kg
Reactive Sulfide U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
30.0 75.0
Laboratory Control Sample (LCS)
(LCS) R3864771-2 11/24/22 08:31
Spike Amount LCS Result
Analyte mg/kg mg/kg
Reactive Sulfide 100 88.2
QUALITY CONTROL SUMMARY
L1559561-01
LCS Rec. Rec. Limits LCS Qualifier
88.2 53.8-124
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1559561 11/29/22 16:29 13 of 21

WG1964541 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9045D L1559561-01
L1558786-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1553736-02 11/25/22 1130 • (DUP) R3364993-2 11/25/22 1130
Original Result DUP Result Dilution DUP RPD
Analyte su su
pH 7.39 7.39 1 0.000
Sample Narrative:
OS: 7.39 at20.8C
DUP: 7.39 at 20.9C
L1560364-11 Original Sample (OS) • Duplicate (DUP)
DUP Qualifier DUP RPD
Limits
(OS) L1560364-11 11/25/22 1130 • (DUP) R3364993-3 11/25/22 1130
Original Result DUP Result
Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte su su
pH 7.67 7.67
1 0.000 1
Sample Narrative:
OS: 7.67 at 20C
DUP 7.67 at19.9C
Laboratory Control Sample (LCS)
(LCS) R3364993-1 11/25/22 1130
Spike Amount LCS Result
LCS Rec. Rec. Limits LCS Qualifier
Analyte su su
pH 10.0 9.91
99.1 99.0-101
Sample Narrative:
LCS: 9.91 at20.7C
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates
L1559561 11/29/22 16:29 14 of 21

WG1963305
Wet Chemistry by Method 9056A
Method Blank (MB)
(MB) R3365039-1 11/23/22 17:43
MB Result
Analyte mg/kg
Nitrate -Nitrite U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
1.06 20.0
L1559181-22 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1559561-01
(OS) L1559131-22 11/23/22 20:56 • (DUP) R3365039-3 11/23/22 2111
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
(dry) (dry) Limits
Analyte mg/kg mg/kg
Nitrate -Nitrite ND ND 1.04 8.27 15
L1559681-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1559631-01 11/23/22 22:25 • (DUP) R3365039-6 11/23/22 22:40
Original Result DUP Result DUP RPD
Dilution DUP RPD DUP Qualifier
(dry) (dry) Limits
Analyte mg/kg mg/kg
Nitrate -Nitrite ND ND 1 0.000 15
Laboratory Control Sample (LCS)
(LCS) R3865039-2 11/23/22 17:57
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Nitrate -Nitrite 40.0 42.2 106
Rec. Limits LCS Qualifier
80.0-120
L1559181-22 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1559131-22 11/23/22 20:56 • (MS) R3365039-4 11/23/22 21:26 • (MSD) R3365039-5 11/23/22 2141
Spike Amount Original Result
MS Result (dry)
MSD Result MS Rec.
MSD Rec. Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD RPD Limits
(dry) (dry)
(dry)
Analyte mg/kg mg/kg
mg/kg
mg/kg
Nitrate -Nitrite 105 ND
118
118 108
109 1.04 80.0-120
0.397 15
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Hunt Environmental Associates
L1559561
11/29/22 16:29 15 of 21

WG1962791 QUALITY CONTROL SUMMARY
Wet Chemistry by Method D93/1010A L1559561-01
L1558094-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1553094-02 11/21/22 03:00 • (DUP) R3363647-3 11/21/22 03:00
Original Result DUP Result Dilution DUP RPD
Analyte Deg. F Deg. F
Ignitability DNI at170 DNI at170 1 0.000
L1558860-01 Original Sample (OS) • Duplicate (DUP)
DUP Qualifier DUP RPD
Limits
i
10
(OS) L1553360-01 11/21/22 03:00 • (DUP) R3363647-4 11/21/22 03:00
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte Deg. F Deg. F
Ignitability DNI at170 DNI at170 1 0.000 10
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3363647-1 11/21/22 03:00 • (LCSD) R3363647-2 11/21/22 03:00
Spike Amount LCS Result LCSD Result LCS Rec.
LCSD Rec.
Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte Deg. F Deg. F Deg. F
Ignitability 126 129 129 103
103
95.6-104 0.000 10
ACCOUNT:
PROJECT:
SDG: DATE/TIME: PAGE:
Hunt Environmental Associates
L1559561 11/29/22 16:29 16 of 21

WG1962672
Mercury by Method 7471B
Method Blank (MB)
(MB) R3364322-1 11/24/22 10:40
MB Result MB Qualifier MB MDL
Analyte mg/kg mg/kg
Mercury U 0.0180
Laboratory Control Sample (LCS)
(LCS) R3864822-2 11/24/22 10:43
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Mercury 0.500 0.480 96.0
QUALITY CONTROL SUMMARY
L1559561-01
MB RDL
mg/kg
0.0400
Rec. Limits LCS Qualifier
80.0-120
L1559883-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1559333-02 11/24/22 10:45 • (MS) R3864822-3 11/24/22 10:48 • (MSD) R3864822-4 11/24/22 10:57
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Mercury 0.500 ND 0.475 0.446 94.9 89.2 1 75.0-125 6.24 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1559561 11/29/22 16:29 17 of 21

WG1963650
Metals (ICP) by Method 6010D
Method Blank (MB)
(MB) R3364334-1 11/24/22 1720
MB Result
MB Qualifier MB MDL
Analyte mg/kg
mg/kg
Arsenic U
0.518
Barium U
0.0852
Cadmium U
0.0471
Chromium U
0.133
Lead U
0.208
Selenium U
0.764
Silver U
0.127
Laboratory Control Sample (LCS)
(LCS) R3864884-2 11/24/22 17:23
Spike Amount
LCS Result
Analyte
mg/kg
mg/kg
Arsenic
100
85.3
Barium
100
88.0
Cadmium
100
86.6
Chromium
100
86.0
Lead
100
89.9
Selenium
100
86.7
Silver
20.0
17.4
LCS Rec.
85.3
88.0
86.6
86.0
89.9
86.7
87.1
QUALITY CONTROL SUMMARY
L1559561-01
MB RDL
mg/kg
2.00
0.500
0.500
1.00
0.500
2.00
1.00
Rec. Limits
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
LCS Qualifier
L1559172-16 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1559172-16 11/24/22 17:26 • (MS) R3864334-5 11/24/22 17:34 • (MSD) R3864334-6 11/24/22 17:36
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
mg/kg
mg/kg
mg/kg
mg/kg
Arsenic
100
ND
91.1
77.0
91.1
77.0
1 75.0-125
Barium
100
12.1
104
89.4
92.1
77.3
1 75.0-125
Cadmium
100
ND
92.7
79.1
92.6
79.0
1 75.0-125
Chromium
100
4.07
94.8
80.0
90.7
76.0
1 75.0-125
Lead
100
24.2
116
102
92.1
77.4
1 75.0-125
Selenium
100
ND
93.4
79.9
93.4
79.9
1 75.0-125
Silver
20.0
ND
18.5
15.8
92.5
78.9
1 75.0-125
MS Qualifier MSD Qualifier RPD
16.8
15.3
15.9
16.9
13.5
15.5
15.9
RPD Limits
20
20
20
20
20
20
20
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1559561 11/29/22 16:29 13 of 21

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contactyour project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
u
Fc
Fss]
(dry)
Results are reported based on the dry weight ofthe sample. [this will only be present on a dry report basis for soils].
MDL
Method Detection Limit.
Fn
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Fr
RDL (dry)
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
Fc
SDG
Sample Delivery Group.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
F
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Rc
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J5
The sample matrix interfered with the ability to make any accurate determination, spike value is high.
P1
RPD value not applicable for sample concentrations less than 5 times the reporting limit.
T8
Sample(s) received past/too close to holding time expiration.
v
The sample concentration is too high to evaluate accurate spike recoveries.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates
L1559561 11/29/22 16:29 19 of 21

ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
Nebraska
N E-OS-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TNO02
California
2932
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704 _
Georgia
NELAP
North Carolina 3
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky' 6
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee'"
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas5
LABO152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A2 LA
A2LA— ISO17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1559561 11/29/22 16:29 20 of 21

„c-panyFp,...� ddiess.
Hunt Environmental Associates
3330 Saddletree Road
Lumberton, NC 28359
RE?pi]r; to
Cody Hunt
Project Description:
Enviro-Choice Recycling -
Phone 910-6I4-S945
Collected by {print).
ected b slgnaturel:
immedl ate
Packed o ce N _ i K
Sample ID
City/State
Collected:
project #
acility ID #
Billing Information
Accounts Payable I Pres
PO Box 390 Chk
Lumberton, NC 28359
tman I 1
1 l�ii�L' I-,Yri� 1Dn y'L
r4
O
Z
4
nor
T
J Please Circle:
A/C- PT MT CT
,x,
O
=
m
Z
-6
O
Z
Lab Project#
HLINTENVLNC-ENVIRQ
N
=
E
_
-
=
OE
QJ
IL
a.
d
a
IL
1 =
vs
.6
P.O.#
Rush? (Lab MUST Be Notified)
Quote ii F
Same Cay
Five Day
!'
_Next bay
_5 Day (Rad only)
Date Results Needed
Two Day _ 10 Day (Rad Only)
Three Day
Comp/Grab
Matrix'
De�pth­D.te
Tame
e€ li- In I T E d
,a ry O E
E z I L an
in w 4-1
_ Ne ( p
Z ~
E
y I =•=
No.
of CL f,l, A U
t3 zLA
Q U lei
:ntrs V7 nt ry a--: L1C Q Q
= O
LL z Z CL a �
7 x x x x I x I x x
Chain of Custody Page_of
/--'P
ace,
a FpetE Fu4cxLlne SCI[iiCF
MT JULIET, TN
11ob5leeanon Rd Mourn lui•eC try 3712i
I Su6m,tnng a sample via th,s ch+in of custody
cor, teWtm ackt Aedg ..and .K.-eFta ..tire
Pace Teems and Cond,tinns found at:
hlms:R,nfo.yaceisbt lmfhubls/pas amed+,d
trvms.pdf
SDG# it 1'5� r 5UI
Tab; C039
kcctnum: HUNENVLNC
PreloRin: P955622
PM: 973 -Heather) Wagner
PB: _ E
5hlpped Via: FedEX Grounin
RemarKS I Sample # Rah only) ,
i Matrix:
i5 Soi} AIR Air F -Filter
iW - Groundwater B - Bioassay
NW - Waste Water
)W - Drinking Water
?T - Other
�iemark Vl J� �J� i V� C 1 Vt� ��� I d
(
(j 1
4L T 1 wtr utn ���—
"'"��'” - ww 111
Samples returned via:
UPS _FedEx Courier Tracking#��a �
+ , ' jam! ��
1 pH _ Temp _
�j�
Y/1 Flow Dther- ��
P-{�
Q �� 1 ��2
! J
R
COC Seal Present/Intact: 1 Y -N
cQC Signed/Accurate: �Y —n
BQttlea arrive intact. ty _
Correct bottles used: !Y N
Sufficient volume sent: �_N
Tf Rot�lica! ie —
V4A Zero Headspace: _�Y _N
Preservation Correct/Checked: N
RAD Screen <0.5 mR/hr:
Hell ishe by: (Sign ue)
l
XT'
Time:
��
Recelvedby- (Signature)y
i�
-
Received by: ;Signature) TemgPdAf
Trip Blank Received: /No
HCL l MeoH
TOR
Relin shed by i n
` }
D e:
Time:
C Bottles Received:
r Z!
- --'-`--�'- "_-
If preservation required by Login: Dail
Relinquish (Signa
D te: Time: _
Received r lab by: {Signature}
-
Date: Time:
Hold:
E
Condition
NCF

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lumberton
WWTP Name: City of Lumberton
Monitoring Period: From 10/1/2022 To
WQ Permit Number:
NPDES Number:
12/31 /2022
WQ0000672
NCL-024571
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)❑
Alt. C (Prior Testing)❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray 01
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density p
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
1 Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g �
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -pique
M inimu
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
2890000
369000
4280000
CFU/ g
l
Quarterly
Grab
9222-MF
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 WN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
I Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
I Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
1 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Michael C Hunt, ORC
Preparer Name and Title (type or print)
Signature of Prepare *
Michael C Hunt, ORC
Land Applier Name and Title (if applicable)(type or print)
2/28/2023
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Cameron Testing Services, Inc. Laboratory Report
NCDENR#654
NC PHHS #37799
US EPA#NC01918
Client;
Enviro-Choice Recyling
CTS Proj.
2212-0141
DW Cert # 37799
Project:
City of Lumberton
Regulatory
Yes
Sample Information
sampled
C. Harris pate 12/12/22
Rece.lvvd-,;
J.
Cameron
Date
12/12/22
Analyses and Results
Lab ID
O
Sample ID m o Analyte
Result
�
d E
T
m � c
Std. Methods
E2
U
Reference
2212-0141
-01 3ludge Gr Fee. Coliform-S
3590000
crulg
6o900
12/13/22 PD
92220 - MF
-02
3790000
CFUrg
80600
-03
4040000
CFUIg
87800
-04
3440000
CFU/g
54600
-05
3970000
CFUrg
90100
-06
2890000
CFUIg
79000
-07
4280000
cFuig
1o90oo
Geomean
3690000
2212-0141
-01 3kudge Gr TS (%)
3.30
%
0.01
12/13/22 PD
2540 G -TS
-02
3.00
%
0.01
-03
2.90
%
0.01
-04
2.80
%
0.01
-05
2.90
%
0.01
-06
3.60
%
0.01
-07
3.10
%
0.01
Report
Review k � h
of �ro5 �� � o�
Project Manager Date
219 S. Steele Stf, 919-208-4240
Sanford NC 27330 [e-mail] camerontesting.com

a
0
� � w
U �
U
u
n. T
ta a © QCL
R
4.0 C Ly �. ❑
Q o
V - � Z c '
xOn
p \'
a C
a
w U z
co E 3
rn {m a ja4}d j
C c }as VOACL
N d l6
CL
a] a
N a G
` d 009
d U
z !
I— 4
o ci �J d ozE
x Z
� � d
(N/A) aol
z 0 xuaevy
c geaJ
dwoo
4 CL
au�ll ,
v .. i — ---�— _— —�—_ s
to
1 q a}ec]
Y
co
� N p
m y c U ++' p N O l C
in rn w
u7 p ai S W m
o a H o :c
N cn a U a w U V
i�
0
a
O.
`o
a
m
cr
2

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY23-SL016594
k5i I"14'4+;4
Client:
Ronald G. Hammonds
Advisor: Michael Hunt
Predictive
1218 Hammonds Rd.
Enviro-Choice Recycling
°± f'
Lumberton, NC 28360
3330 Saddletree Rd
�-
Soil Report Mehlich-3 Extraction
Lumberton, NC 28360
Sampled County : Robeson
_1
Sampled:
Links to Helpful Information
Received: 11/18/2022 Completed: 01/05/2023 Farm:
Client ID:
404031
Advisor ID: 486968
Sample ID: 2003
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S Mn
Zn
Cu B
Information
Lime History:
1- Bermuda hay/past., M 1.3 180-220 0
140
0 0 0
0
0 0
Note: 12
2- Bermuda hay/past., M 0.0 180-220 0
140
0 0 0
0
0 0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I
Mn-All Mn-Al2 Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.81 1.21
10.4 75 2.6 5.4 721 39 60 13
67 168
118 118 1595
1595
895 0.1 1
Sample ID: 2004
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S Mn
Zn
Cu B
Information
Lime History:
1 -Com. Bermuda/Bahia 1.5 100-150 0
90
0 0 0
0
0 0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I
Mn-All Mn-AI2 Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.92 1.28
8.1 69 2.6 5.2 697 23 56 12
72 132
96 1062
1062
700 0.1 1
North Carolina
Tai wLm Truk f and Ctwinlsskm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone:
[phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY23-SL016594
Ronald G. Hammonds
Page 2 of 4
Sample ID: 2006
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Corn, grain
0.0
120 - 160 0
10
0
0
0
0
0 0
Note: 3
2 -
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
1.55 1.13 12.0
87 1.6 6.1
140 73
67 17
66
54
48
205
205
166 0.7
6
Sample ID: 2007
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Corn, grain
0.0
120 - 160 0
0
0
0
0
0
0 0
Note: 3
2 -
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
1.55 1.15 9.2
81 1.7 5.9
214 89
64 12
95
48
46
269
269
221 0.5
5
Sample ID: 2008
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Corn, grain
0.7
120 - 160 0
0
0
0
0
0
0 0
Note: 3
2 -
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
1.49 1.24 10.3
80 2.0 5.7
399 102
60 15
101
75
62
373
373
287 0.3
3

NCDA&CS Agronomic Division Phone:
[phone]
Website: www.ncagr.gov/agronomi/
Report No. FY23-SL016594
Ronald G. Hammonds
Page 3 of 4
Sample ID: 2014
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5 K2O
Mg
S
Mn Zn
Cu B
Information
Lime History:
1 -Corn, grain
0.0
120 - 160 0 0
0
0
0 0
0 0
Note: 3
2 -
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg% S-1 Mn-I
Mn-All
Mn-Al2
Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
1.67 1.22 9.4 82 1.7 5.9
264 91
69 8 111 60
53
329 329
297 0.6 6

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY23-SLO16594
Ronald G. Hammonds
Page 4 of 4
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.pov/apronomi/obpart4.htrntfsfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HW/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability indexM%,
Zn-1
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.pov/agronomi/uyrst.htm

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY23-SL016590
k5i I"14'4+;4
Client:
Patrick Bullard
Advisor:
Michael Hunt
Predictive
4147 Prospect Rd. / PO Box 1262
Enviro-Choice Recycling
°± f'
Pembroke, NC 28372
3330 Saddletree Rd
�- Soil Report Mehlich-3 Extraction
Lumberton, NC 28360
Sampled County : Robeson
_1
Links to Helpful Information
Sampled: Received: 11/18/2022 Completed: 01/05/2023 Farm:
Client ID:
260315
Advisor
ID: 486968
Sample ID: 3904
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S Mn Zn
Cu
B
Information
Lime History:
1- Bermuda hay/past., M 0.8 180-220 0
0
0 0 0 0
0
0
Note: 12
2- Bermuda hay/past., M 0.0 180-220 0
0
0 0 0 0
0
0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I
Mn-All Mn-Al2 Zn-I Zn-AI
Cu-I
Na ESP SS-1 NO3-N
1.37 1.18 10.5 78 2.3 5.7 247 149 55 16
73 93
73 73 406 406
261
0.1 1
Sample ID: 3905
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S Mn Zn
Cu
B
Information
Lime History:
1- Bermuda hay/past., M 0.5 180-220 0
0
0 0 0 0
0
0
Note: 12
2- Bermuda hay/past., M 0.0 180-220 0
0
0 0 0 0
0
0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I
Mn-All Mn-AI2 Zn-I Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.86 1.24 10.5 80 2.1 5.8 264 164 53 19
44 106
81 81 495 495
220
0.1 1
North Carolina
Tai wLm Truk f and Ctwinlsskm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY23-SL016590
Patrick Bullard
Page 2 of 3
Sample ID: 3909
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn Zn
Cu B
Information
Lime History:
1 -Com. Bermuda/Bahia 1.3
100-150 0
110
0
0
0 0
0 0
Note: 12
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-All
Mn-Al2
Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.22 1.25 4.7 53 2.2 5.1 337 16
41 11 47
62
54
271 271
313 0.1 2

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY23-SLO16590
Patrick Bullard
Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.pov/apronomi/obpart4.htrntfsfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
Zn-1
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.pov/agronomi/uyrst.htm

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY23-SL016591
k5i I"14'4+;4
Client: Patrick Bullard
Advisor: Michael Hunt
Predictive
4147 Prospect Rd. / PO Box 1262
Enviro-Choice Recycling
°± f'
Pembroke, NC 28372
3330 Saddletree Rd
�- Soil Report Mehlich-3 Extraction
Lumberton, NC 28360
Sampled County : Robeson
_1
Links to Helpful Information
Sampled: Received: 11/18/2022 Completed: 01/05/2023 Farm:
Client ID: 260315
Advisor ID: 486968
Sample ID: 2802
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O Mg S Mn Zn
Cu B
Information
Lime History:
1 -Corn, grain 0.0 120 - 160 0
0 0 0 0 0
0 0
Note: 3
0.50 tons/acre; 1/2022
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
1.37 1.32 10.1 84 1.6 6.2 480 96 58 21
67 88 66 616 616
432 0.4 4
North Carolina
Tcbwim Truk f and Ctwinlsskm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY23-SLO16591
Patrick Bullard
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.pov/apronomi/obpart4.htrntfsfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
Zn-1
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.pov/agronomi/uyrst.htm

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY23-SL016593
k5i I"14'4+;4
Client:
Ozzell Arrin Baker
Advisor: Michael Hunt
Predictive
2996 Evergreen Church Rd
Enviro-Choice Recycling
°± f'
Pembroke, NC 28372
3330 Saddletree Rd
�- Soil Report Mehlich-3 Extraction
Lumberton, NC 28360
Sampled County : Robeson
_1
Links to Helpful Information
Sampled: Received: 11/18/2022 Completed: 01/05/2023 Farm:
Client ID:
156712
Advisor ID: 486968
Sample ID: 1616
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S Mn Zn
Cu B
Information
Lime History:
1 -Com. Bermuda/Bahia 1.7 100-150 0
80
0 0 0 0
0 0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I
Mn-All Mn-Al2 Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.86 1.13 10.3 67 3.4 5.4 536 30 56 9
87 100
77 958 958
671 0.4 4
Sample ID: 1617
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S Mn Zn
Cu B
Information
Lime History:
1 -Com. Bermuda/Bahia 0.7 100-150 0
90
0 0 0 0
0 0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I
Mn-All Mn-AI2 Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.76 1.09 12.8 79 2.7 5.8 540 26 66 12
87 75
62 889 889
680 0.7 5
North Carolina
Tai wLm Truk f and Ctwinlsskm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY23-SL016593
Ozzell Arrin Baker
Page 2 of 3
Sample ID: 1618
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Com. Bermuda/Bahia 1.9
100-150 0
90
0
0
0
0
0 0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.71 1.13 10.6
67 3.5 5.3 643 25
56 10
96
74
61
818
818
919 0.4
4
Sample ID: 1619
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Com. Bermuda/Bahia 1.1
100-150 0
120
0
0
0
0
0 0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.71 1.23 6.4
68 2.1 5.4 358 12
56 11
63
71
60
385
385
445 0.2
3

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY23-SLO16593
Ozzell Arrin Baker
Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.pov/apronomi/obpart4.htrntfsfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
Zn-1
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.pov/agronomi/uyrst.htm

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY23-SL016592
k5i I"14'4+;4
Client:
Delois/Pete Allen
Advisor: Michael Hunt
Predictive
688 Deep Branch Rd.
Enviro-Choice Recycling
°± f'
Lumberton, NC 28360
3330 Saddletree Rd
�- Soil Report Mehlich-3 Extraction
Lumberton, NC 28360
Sampled County : Robeson
_1
Links to Helpful Information
Sampled: Received: 11/18/2022 Completed: 01/05/2023 Farm:
Client ID:
434958
Advisor ID: 486968
Sample ID: 1701
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S Mn Zn
Cu B
Information
Lime History:
1-Soybean 0.9 0 0
110
0 0 10 0
0 0
Note: 3
0.60 tons/acre; 1/2022
2 - 0.0
0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I
Mn-All Mn-Al2 Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
1.67 1.28 6.8 67 2.2 5.6 98 17 49 17
45 25
25 128 128
100 0.1 1
Sample ID: 1702
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S Mn Zn
Cu B
Information
Lime History:
1-Soybean 1.9 0 0
110
0 0 0 0
0 0
Note: 3
0.60 tons/acre; 1/2022
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I
Mn-All Mn-AI2 Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
1.49 1.26 6.1 52 3.0 5.0 87 17 37 13
69 29
27 103 103
60 0.2 3
North Carolina
Tai wLm Truk f and Ctwinlsskm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone:
[phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY23-SL016592
Delois/Pete Allen
Page 2 of 3
Sample ID: 1703
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1-Soybean
2.1
0 0
100
0
0
0
0
0 0
Note: 3
0.60 tons/acre; 1/2022
2 -
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
1.94 1.25 6.0
46 3.2 4.8
179 22
34 10
93
28
27
210
210
155 0.4
7
Sample ID: 1704
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Soybean
0.0
0 0
100
25
0
$pH
0
0 0
Note: 3 Note: $
0.60 tons/acre; 1/2022
2 -
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
1.19 1.29 7.4
82 1.4 6.2
80 20
75 6
36
21
19
100
100
133 0.1
1

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY23-SLO16592
Delois/Pete Allen
Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.pov/apronomi/obpart4.htrntfsfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
Zn-1
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.pov/agronomi/uyrst.htm

Date & Analyst:
Total Solids
City of Lumberton
Environmental Laboratory
Specific Oxy-gen Uptake Rate (SOUR) Worksheet
2/7/2022 0846 am kcl Dig#1 Day 1
Sample volume used for total solids test: 5 mL
Weight of dish: 111.4064 g
Weight of dish + dried solids: 111.5074 g
Weight of dried solids: 0.1010 g
Total Solids: 20.2 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
12.00
7.47
1
12.00
7.47
2
12.00
7.30
3
12.00
7.21
4
12.00
6.87
5
12.00
6.81
6
12.00
6.74
7
12.00
6.63
8
12.00
6.35
9
12.00
6.20
10
12.00
5.91
11
12.00
5.53
12
12.00
5.29
13
12.00
5.06
14
12.00
4.89
15
12.00
4.60
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
12
0.20 mg/L/minute
0.59 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = 0.87 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 1.01 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 2/8/2022 0750 am kcl Dig#1 Day 2
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 123.1011 g
Weight of dish + dried solids: 123.2032 g
Weight of dried solids: 0.1021 g
Total Solids: 20.42 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
15.00
6.08
1
14.00
6.03
2
13.00
6.00
3
13.00
6.00
4
12.00
5.93
5
12.00
5.73
6
12.00
5.57
7
12.00
5.40
8
12.00
5.25
9
12.00
5.17
10
12.00
5.09
11
12.00
4.91
12
12.00
4.69
13
12.00
4.54
14
13.00
4.36
15
13.00
4.19
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
12.5625
0.13 mg/L/minute
0.39 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = 0.56 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.64 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 2/9/2022 0711am kcl Dig#1 Day 3
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 121.2425 g
Weight of dish + dried solids: 121.3444 g
Weight of dried solids: 0.1019 g
Total Solids: 20.38 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
10.00
7.59
1
10.00
7.38
2
10.00
7.07
3
10.00
6.87
4
11.00
6.87
5
11.00
6.78
6
11.00
6.61
7
11.00
6.49
8
11.00
6.42
9
11.00
6.26
10
11.00
6.17
11
11.00
5.96
12
11.00
5.90
13
11.00
5.78
14
11.00
5.63
15
1 11.00
5.54
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.13 mg/L/minute
0.38 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
oC
10.75
If sewage sludge is > 20°C, SOUR = 0.59 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.70 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 2/10/2022 0712 am kcl Dig#1 Day 4
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 120.9127 g
Weight of dish + dried solids: 121.0019 g
Weight of dried solids: 0.0892 g
Total Solids: 17.84 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
10.00
9.72
1
0.00
9.62
2
10.00
9.44
3
10.00
9.27
4
11.00
9.13
5
11.00
8.89
6
11.00
8.72
7
11.00
8.54
8
11.00
8.26
9
11.00
8.70
10
11.00
8.00
11
11.00
7.76
12
12.00
7.60
13
12.00
7.35
14 1
12.00
7.23
15 1
12.00
7.02
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
10.375
0.18 mg/L/minute
0.61 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = 0.98 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 1.18 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 2/11/2022 0727 am kcl Dig#1 Day 5
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 111.4051 g
Weight of dish + dried solids: 111.5048 g
Weight of dried solids: 0.0997 g
Total Solids: 19.94 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
15.00
6.08
1
13.00
5.51
2
12.00
5.46
3
12.00
5.46
4
12.00
5.39
5
12.00
5.21
6
12.00
5.06
7
13.00
4.86
8
13.00
4.06
9
13.00
4.00
10
13.00
4.37
11
13.00
4.23
12
13.00
4.01
13
13.00
3.85
14
13.00
3.63
15
13.00
3.47
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.16 mg/L/minute
0.49 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
oC
12.8125
If sewage sludge is > 20°C, SOUR = 0.70 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.80 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

Date & Analyst
Total Solids
City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
2/14/2022 0716am kcl Dig#1 Day 6
Sample volume used for total solids test: 5 mL
Weight of dish: 121.2662 g
Weight of dish + dried solids: 121.3413 g
Weight of dried solids: 0.0751 g
Total Solids: 15.02 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
13.00
6.76
1
13.00
6.76
2
13.00
6.59
3
13.00
6.64
4
13.00
6.62
5
13.00
6.57
6
13.00
6.51
7
13.00
6.47
8
13.00
6.27
9
13.00
6.16
10
13.00
5.84
11
14.00
5.64
12
14.00
5.49
13
14.00
5.34
14
14.00
5.17
15
14.00
4.98
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.12 mg/L/minute
0.49 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
13.3125
If sewage sludge is > 20°C, SOUR = 0.68 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.77 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 2/15/2022 0705am kcl Dig#1 Day 7
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 125.4507 g
Weight of dish + dried solids: 125.5582 g
Weight of dried solids: 0.1075 g
Total Solids: 21.5 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
12.00
7.90
1
12.00
7.86
2
12.00
7.68
3
12.00
7.22
4
12.00
6.92
5
11.00
7.80
6
11.00
7.66
7
12.00
7.54
8
12.00
7.38
9
12.00
7.23
10
12.00
7.09
11
12.00
6.90
12
12.00
6.76
13
12.00
6.63
14
12.00
6.45
15
12.00
6.26
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.09 mg/L/minute
0.26 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
11.875
If sewage sludge is > 20°C, SOUR = 0.39 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = i 0.45 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Mon 5/2/22 @ 1058 KCL Day 1
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 121.2441 g
Weight of dish + dried solids: 121.3512 g
Weight of dried solids: 0.1071 g
Total Solids: 21.42 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
21.00
4.33
1
21.00
3.85
2
21.00
2.03
3
21.00
1.38
4
21.00
1.04
5
21.00
0.75
6
21.00
0.61
7
20.00
0.50
8
20.00
0.44
9
20.00
0.40
10
20.00
0.38
11
20.00
0.37
12
21.00
0.36
13
20.00
0.35
14
20.00
0.35
15
20.00
0.34
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
20.5
0.21 mg/L/minute
0.58 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = (mg/g)/hr
If sewage sludge is < 20°C, SOUR = (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Tues 5/3/22 @ 0609 KCL Day 2
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 120.5322 g
Weight of dish + dried solids: 120.6323 g
Weight of dried solids: 0.1001 g
Total Solids: 20.02 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
21.00
4.85
1
21.00
3.13
2
21.00
2.75
3
21.00
1.42
4
21.00
0.65
5
21.00
0.35
6
22.00
0.33
7
.22.00
0.31
8
22.00
0.31
9
22.00
0.31
10
22.00
0.31
11
22.00
0.31
12
22.00
0.31
13
22.00
0.31
14
22.00
0.31
15
22.00
0.31
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.21 mg/L/minute
0.64 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
21.625
If sewage sludge is > 20°C, SOUR = 0.59 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.57 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

Date & Analyst:
Total Solids
City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Wed 5/4122 @ 0618 KCL Day 3
Sample volume used for total solids test: 5 mL
Weight of dish: 111.4069 g
Weight of dish + dried solids: 111.5106 g
Weight of dried solids: 0.1037 g
Total Solids: 20.74 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
22.00
4.92
1
22.00
3.89
2
22.00
1.65
3
22.00
0.75
4
22.00
0.32
5
22.00
0.32
6
22.00
0.30
7
22.00
0.30
8
22.00
0.30
9
22.00
3.00
10
22.00
0.30
11
22.00
0.30
12
22.00
0.30
13
22.00
0.30
14
22.00
0.30
15
22.00
0.30
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.19 mg/L/minute
0.54 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
oC
22
If sewage sludge is > 20°C, SOUR = 0.49 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.47 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Thur 5/5/22 @ 0628 TLS Day 4
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 89.0334 g
Weight of dish + dried solids: 89.1467 g
Weight of dried solids: 0.1133 g
Total Solids: 22.66 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
22.00
2.10
1
22.00
1.19
2
22.00
1.09
3
22.00
0.91
4
22.00
0.82
5
22.00
0.77
6
22.00
0.67
7
22.00
0.62
8
22.00
0.57
9
22.00
0.45
10
22.00
0.41
11
22.00
0.36
12
22.00
0.32
13
22.00
0.32
14
22.00
0.32
15
22.00
0.32
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.08 mg/L/minute
0.22 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
22
If sewage sludge is > 20°C, SOUR = 0.20 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.20 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Fri 516122 @ 0613 KCL Day 5
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 121.2444 g
Weight of dish + dried solids: 121.3445 g
Weight of dried solids: 0.1001 g
Total Solids: 20.02 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
22.00
5.55
1
22.00
2.69
2
22.00
1.40
3
22.00
0.86
4
22.00
0.65
5
22.00
0.51
6
22.00
0.44
7
22.00
0.40
8
22.00
0.39
9
22.00
0.37
10
22.00
0.36
11
22.00
0.36
12
22.00
0.35
13
22.00
0.35
14
22.00
0.35
15
22.00
0.35
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.19 mg/L/minute
0.56 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
22
If sewage sludge is > 20°C, SOUR = 0.51 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.49 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Mon 5/9/22 @ 0624 TLS Day 6
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 111.4071 g
Weight of dish + dried solids: 111.5109 g
Weight of dried solids: 0.1038 g
Total Solids: 20.76 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
20.00
7.12
1
20.00
5.48
2
20.00
2.92
3
20.00
1.26
4
20.00
0.96
5
20.00
0.88
6
20.00
0.79
7
19.00
0.69
8
19.00
0.61
9
19.00
0.58
10
19.00
0.55
11
19.00
0.51
12
19.00
0.48
13
19.00
0.47
14
19.00
0.45
15
19.00
0.42
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.30 mg/L/minute
0.87 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
19.4375
If sewage sludge is > 20°C, SOUR = 0.90 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.91 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Tues 5110/22 @ 0629 TLS Day 7
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 121.2431 g
Weight of dish + dried solids: 121.3492 g
Weight of dried solids: 0.1061 g
Total Solids: 21.22 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
aC
0
21.00
5.28
1
21.00
4.01
2
21.00
3.99
3
21.00
2.07
4
21.00
1.11
5
21.00
0.89
6
21.00
0.71
7
21.00
0.66
8
21.00
0.43
9
21.00
0.39
10
21.00
0.39
11
21.00
0.35
12
21.00
0.35
13
21.00
0.34
14
21.00
0.34
15
21.00
0.34
Oxygen Consumption Rate 0.27 mg/L/minute
SOUR 0.78 (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
21
If sewage sludge is > 20°C, SOUR = 0.74 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.72 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

Date & Analyst
Total Solids
City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Mon 7/11/22 @ 0753 KCL Day 1
Sample volume used for total solids test: 5 mL
Weight of dish: 89.0337 g
Weight of dish + dried solids: 89.1221 g
Weight of dried solids: 0.0884 g
Total Solids: 17.68 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
23.00
5.07
1
23.00
3.26
2
23.00
2.25
3
23.00
1.30
4
23.00
0.36
5
23.00
0.14
6
23.00
0.13
7
23.00
0.13
8
23.00
0.12
9
23.00
0.12
10
23.00
0.12
11
23.00
0.12
12
23.00
0.12
13
23.00
0.12
14
23.00
0.12
15
23.00
0.12
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.22 mg/L/minute
0.75 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
23
If sewage sludge is > 20°C, SOUR = 0.65 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.61 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 1111/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Tues 7/12122 @ 0749 KCL Day 2
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 130.0820 g
Weight of dish + dried solids: 130.1684 g
Weight of dried solids: 0.0864 g
Total Solids: 17.28 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
23.00
4.48
1
23.00
3.38
2
23.00
1.02
3
23.00
0.87
4
23.00
0.58
5
23.00
0.42
6
23.00
0.34
7
23.00
0.26
8
23.00
0.23
9
23.00
0.21
10
23.00
0.19
11
23.00
0.17
12
23.00
0.16
13
23.00
0.16
14
23.00
0.15
15
23.00
0.14
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.19 mg/L/minute
0.65 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
23
If sewage sludge is > 20°C, SOUR = 0.56 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.53 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Wed 7/13/22 @ 0805 KCL Day 3
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 125.4597 g
Weight of dish + dried solids: 125.5452 g
Weight of dried solids: 0.0855 g
Total Solids: 17.1 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
aC
0
24.00
6.84
1
25.00
3.55
2
25.00
2.61
3
25.00
1.17
4
25.00
0.50
5
25.00
0.09
6
25.00
0.07
7
25.00
0.07
8
25.00
0.06
- 9
25.00
0.06
10
25.00
0.06
11
25.00
0.06
12
25.00
0.06
13
25.00
0.06
14
25.00
0.06
15
25.00
0.06
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
24.9375
0.28 mg/L/minute
0.97 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.70 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Thur 7/14/22 @ 0820 KCL Day 4
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 126.9150 g
Weight of dish + dried solids: 127.0045 g
Weight of dried solids: 0.0895 g
Total Solids: 17.9 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
25.00
7.72
1
25.00
7.34
2
25.00
7.14
3
25.00
7.00
4
25.00
6.88
5
25.00
6.75
6
25.00
6.63
7
25.00
6.49
8
25.00
6.35
9
25.00
6.18
10
25.00
6.05
11
25.00
5.90
12
25.00
5.74
13
25.00
5.60
14
25.00
5.43
15
25.00
5.31
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
25
0.15 mg/L/minute
0.50 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = 0.39 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.36 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: fri 7115/22 @ 0735 KCL Day 5
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 121.2454 g
Weight of dish + dried solids: 121.3349 g
Weight of dried solids: 0.0895 g
Total Solids: 17.9 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
24.00
7.94
1
24.00
6.51
2
24.00
6.23
3
24.00
6.02
4
24.00
5.72
5
24.00
5.49
6
24.00
5.27
7
24.00
5.03
8
24.00
4.81
9
24.00
4.58
10
24.00
4.37
11
24.00
4.13
12
24.00
3.91
13
24.00
3.69
14
24.00
3.47
15
24.00
3.25
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.26 mg/L/minute
0.87 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
24
If sewage sludge is > 20°C, SOUR = 0.11 (mg/g)/hr
If sewage sludge is < 20°C, SOUR 40.66 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City ®f Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Mon 7/18/22 @ 0813 KCL Day 6
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 89.0351 g
Weight of dish + dried solids: 89.1225 g
Weight of dried solids: 0.0874 g
Total Solids: 17.48 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
24.00
8.19
1
24.00
7.85
2
24.00
7.59
3
24.00
7.43
4
24.00
7.29
5
24.00
7.09
6
24.00
6.93
7
24.00
6.79
8
24.00
6.61
9
24.00
6.46
10
24.00
6.27
11
24.00
6.14
12
24.00
5.97
13
24.00
5.87
14
24.00
5.74
15
24.00
5.60
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.16 mg/L/minute
0.57 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
24
If sewage sludge is > 20°C, SOUR = 0.47 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.43 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Tues 7/19122 @ 0804 KCL Day 7
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 125.4566 g
Weight of dish + dried solids: 125.5465 g
Weight of dried solids: 0.0899 g
Total Solids: 17.98 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
24.00
7.89
1
24.00
6.81
2
25.00
6.77
3
25.00
6.61
4
25.00
6.45
5
25.00
6.31
6
25.00
6.11
7
25.00
5.99
8
25.00
5.69
9
25.00
5.62
10
25.00
5.47
11
25.00
5.31
12
24.00
5.16
13
24.00
4.99
14
24.00
4.84
15
24.00
4.68
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.18 mg/L/minute
0.59 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
24.625
If sewage sludge is > 20°C, SOUR = 0.47 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.43 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Mon 10/11/22 @ 0725 KGL Day 1
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 130.0825 g
Weight of dish + dried solids: 130.1922 g
Weight of dried solids: 0.1097 g
Total Solids: 21.94 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
19.00
4.89
1
19.00
4.46
2
19.00
3.70
3
19.00
2.97
4
19.00
2.78
5
19.00
2.30
6
19.00
1.90
7
19.00
1.44
8
19.00
0.93
9
19.00
0.35
10
19.00
0.12
11
19.00
0.10
12
19.00
0.10
13
19.00
0.09
14
19.00
0.09
15
19.00
0.09
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
19
0.34 mg/L/minute
0.92 (mg/g)/hr
If sewage sludge is > 20°C, SOUR u(mg/g)/hr
If sewage sludge is < 20°C, SOUR = _1 _ 0:99 „(mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Tues 10/12/22 @ 0616 KCL Day 2
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 121.9548 g
Weight of dish + dried solids: 122.0651 g
Weight of dried solids: 0.1103 g
Total Solids: 22.06 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
aC
0
19.00
7.13
1
18.00
6.82
2
18.00
6.50
3
18.00
6.19
4
18.00
5.87
5
18.00
5.52
6
18.00
5.16
7
19.00
4.78
8
19.00
4.43
9
19.00
4.05
10
19.00
3.68
11
19.00
3.23
12
19.00
2.91
13
19.00
2.52
14
19.00
2.13
15
19.00
1.77
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.36 mg/L/minute
0.98 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
18.625
If sewage sludge is > 20°C, SOUR = 1.05 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 1.08 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11 /1 /11

Date & Analyst:
Total Solids
City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Wed 10/13/22 @ 0602 KCL Day 3
Sample volume used for total solids test: 5mL
Weight of dish: 121.2459 g
Weight of dish + dried solids: 121.3579 g
Weight of dried solids: 0.1120 g
Total Solids: 22.4 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
21.00
6.68
1
21.00
6.36
2
20.00
6.01
3
20.00
5.63
4
20.00
5.25
5
20.00
4.91
6
20.00
4.55
7
20.00
4.16
8
21.00
3.69
9
21.00
3.36
10
21.00
2.97
11
21.00
2.53
12
21.00
2.16
13
21.00
1.72
14
21.00
1.33
15
21.00
0.92
Oxygen Consumption Rate 0.39 mg/L/minute
SOUR 1.04 (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
20.625
If sewage sludge is > 20°C, SOUR = 149 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = (mg/g)/hr
SOUR passes if result is <_ 1.5 (mg/g)hr
Version 11/1/11

Date & Analyst:
Total Solids
City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Fri 10-14-22 @0602 kcl Dig #1 Day 4
Sample volume used for total solids test: 5 mL
Weight of dish: 120.5338 g
Weight of dish + dried solids: 120.6451 g
Weight of dried solids: 0.1113 g
Total Solids: 22.26 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
21.00
5.88
1
21.00
4.93
2
21.00
4.52
3
21.00
4.24
4
21.00
3.83
5
21.00
3.52
6
21.00
3.15
7
21.00
2.79
8
21.00
2.41
9
21.00
1.99
10
21.00
1.50
11
21.00
1.24
12
21.00
0.81
13
21.00
0.46
14
21.00
0.13
15
21.00
0.11
Oxygen Consumption Rate 0.38 mg/L/minute
SOUR 1.02 (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
oC
21
If sewage sludge is > 20°C, SOUR = 0.97 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.95 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Mon 10/17/22 @ 0614 KCL Day 5
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 130.0822 g
Weight of dish + dried solids: 130.1929 g
Weight of dried solids: 0.1107 g
Total Solids: 22.14 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
20.00
6.46
1
20.00
6.13
2
20.00
5.83
3
20.00
5.51
4
20.00
5.21
5
20.00
4.88
6
20.00
4.48
7
20.00
4.16
8
20.00
3.77
9
20.00
3.37
10
20.00
3.08
11
20.00
2.66
12
20.00
2.35
13
20.00
1.98
14
20.00
1.61
15 1
20.00
1.24
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.35 mg/L/minute
0.95 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
20
If sewage sludge is > 20°C, SOUR = 0.95 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.95 (mg/g)/hr
SOUR passes if result is <_ 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Tues 10-18-22 @ 0610 KCL Day6
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 120.5354 g
Weight of dish + dried solids: 120.6546 g
Weight of dried solids: 0.1192 g
Total Solids: 23.84 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
19.00
6.42
1
19.00
5.39
2
18.00
5.02
3
19.00
4.77
4
19.00
4.47
5
19.00
4.20
6
19.00
0.95
7
19.00
3.66
8
19.00
3.42
9
19.00
3.13
10
19.00
2.89
11
19.00
2.61
12
19.00
5.33
13
19.00
2.05
14
19.00
1.76
15
19.00
1.49
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.24 mg/L/minute
0.60 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
oC
18.9375
If sewage sludge is > 20°C, SOUR = 0.63 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.64 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1111

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Wed 10-19-22 @ 0613 KCL Day 7
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 126.9165 g
Weight of dish + dried solids: 127.0286 g
Weight of dried solids: 0.1121 g
Total Solids: 22.42 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
14.00
9.05
1
15.00
8.93
2
15.00
8.80
3
14.00
8.80
4
15.00
8.65
5
15.00
8.54
6
15.00
8.38
7
15.00
8.21
8
15.00
8.14
9
15.00
7.90
10
15.00
7.70
11
15.00
7.67
12
15.00
7.50
13
15.00
7.35
14
16.00
7.13
15
16.00
7.03
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.14 mg/L/minute
0.37 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
oC
15
If sewage sludge is > 20°C, SOUR = 0.47 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.52 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11