WQ0003919_2022 Residual Annual Report_20230228 (2)

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * WQ0003919
Applicant/Permittee City of Kinston
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Washington
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Lysa Finnerty
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
4105376150
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:* WQ0003919
Has Current Existing permit number
Applicant/Permittee Address* 435 Williams Court, Ste 100, Baltimore, MD 21220
Facility Name* City of Kinston Class B Residuals Program
Please provide comments/notes on your current submittal below.
2022 Annual Report for City of Kinston, NC
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Kinston NC 2022 Annual Report FINAL.pdf 14.09MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Alva �Cit'wt%tt,
Submission Date 2/28/2023

435 Williams Court, Suite 100
Baltimore, MD 21220
www.synagro.com
FEBRUARY 28, 2023
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2022 Annual Report for Permit No. WQ0003919
Dear NCDEQ:
SYNAGRO
Synagro is submitting one electronic copy of the above referenced report on behalf of the City
of Kinston, NC.
If you have any questions or comments, please contact Kenneth Stevens at [phone] or
Matthew Carter at [phone].
Sincerely,
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Kenneth Stevens, City of Kinston
Matthew Carter, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

CITY OF KINSTON, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0003919
2022 ANNUAL REPORT

City of Kinston, NC
Residuals Land Application Program
2022 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and Residuals
Analyses
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: WO0003919 County Lenoir Year 2022
Facility Name (as shown on permit) Kinston Regional WRF NPDES No. NC0024236
Land Application Operator S na ro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled,
Part A —Residuals Appl ication Summary:
Total number of application fields in the permit: 51
Total number of fields utilized for land application during the year: 6
Total amount of dry tons applied during the year for all application sites: 311,46
Total number of acres utilized for land application during the year: 107.40
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2022 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water QualityX YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
. Only residuals approved for this permit were applied to the permitted sites.
2. Sol] pH was adjusted as specified in the permit and time was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
44. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T . I 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T . I I i I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
to. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
It. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals fiom the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C .... Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
Kenneth Stevens WRF Superintendent v23
Perm ittee. Name and Title (type or print) Signature ofPermi Date
Signature of Preparer* Date Siba�ofLaiVApplier Date
(if different from Permittee) (if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) 1DCNR FORM ACF (12/2006)

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 1/1/2022 - 12/31/2022
KINSTON, NC
KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE
MONTH/YEAR
April 2022
August 2022
IEel /_1I
Units Key: D - Dry Tons; G — Gallons; W — Wet Tons; Y — Cubic Yards
Report Date: 12/1/2022 9:55:38 AM
AMOUNT
UNIT
DRY TONS
UNIT
DRY METRIC TONS
950.00
Y
137.62
D
124.82
1,200.00
Y
173.84
D
157.67
2,150.00
Y
311.46
D
282.49

SECTION 2

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PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Chris Wynne
Project Name: Kinston WRF
Lot Number:XA13015
Date Completed:01/27/2022
NIM�� Mr�
02/01/2022 9:36 AM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
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'ye I
ANSI NdmlAccre00- Board
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A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: XA13015
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Inorganic Metals
Due to low percent solids, sample -001 has been digested with 3X the normal sample volume. The LOQs
have been adjusted accordingly.
Inorganic Non -Metals
The following sample was diluted due to the nature of the sample matrix for Nitrate and Nitrite: XA13015-
001. The LOQ has been elevated to reflect the dilution.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 7

Client:Synagro Laboratory ID:XA13015-001
Description: Kinston WRF Matrix: Solid
Date Sampled:01/12/2022 1300 % Solids: 17.2 01/18/2022 0045
Date Received:01/13/2022
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 2540G
1 01/18/2022 0045 NBW
28681
1 350.1
(Ammonia - N ) 350.1
20 01/19/2022 2219 DAK
28766
1
(Nitrate - N ) 9056A
10 01/20/2022 2217 AAB
29256
1
(Nitrite - N ) 9056A
10 01/20/2022 2217 AAB
29257
1
(Phosphorus) 365.1
200 01/21/2022 1725 DMA
01/21/2022 1208
29127
1
(Soil pH meas) 9045D
1 01/17/2022 2202 NBW
28677
1 351.4
(TKN) 351.2
10 01/24/2022 1057 DMA
01/21/2022 1404
29104
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
17.2
%
1
Ammonia - N (gas diffusion)
350.1
4500
120
61
mg/kg
1
Nitrate - N (soluble)
9056A
ND
29
5.8
mg/kg
1
Nitrite - N (soluble)
9056A
ND
12
5.8
mg/kg
1
Phosphorus
7723-14-0 365.1
32000
5800
1200
mg/kg
1
Soil pH measured in water @
20.5 ° C
9045D
6.8
su
1
TKN
351.2
41000
2900
1500
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471B
7471B
1 01/21/2022 0554 JAB2
01/21/2022 0141
28437
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471B
0.55
0.47
0.11
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 01/19/2022 1306 JMH
01/19/2022 0051
28436
2 3050B
601OD
5 01/19/2022 1356 JMH
01/19/2022 0051
28436
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
33000
170
63
mg/kg
2
Arsenic
7440-38-2 6010D
5.3
1.3
0.42
mg/kg
1
Cadmium
7440-43-9 6010D
1.8
0.42
0.11
mg/kg
1
Calcium
7440-70-2 6010D
23000
420
52
mg/kg
1
Chromium
7440-47-3 6010D
32
0.83
0.21
mg/kg
1
Copper
7440-50-8 6010D
360
0.83
0.38
mg/kg
1
Iron
7439-89-6 6010D
13000
8.3
3.8
mg/kg
1
Lead
7439-92-1 6010D
28
4.2
1.9
mg/kg
2
Magnesium
7439-95-4 6010D
3400
420
52
mg/kg
1
Manganese
7439-96-5 6010D
200
1.3
0.49
mg/kg
1
Molybdenum
7439-98-7 6010D
6.4
3.3
0.83
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:XA13015-001
Description: Kinston WRF Matrix: Solid
Date Sampled:01/12/2022 1300 % Solids: 17.2 01/18/2022 0045
Date Received:01/13/2022
ICP-AES
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date Batch
1 3050B
6010D 1 01/19/2022 1306 JMH
01/19/2022 0051 28436
2 3050B
6010D 5 01/19/2022 1356 JMH
01/19/2022 0051 28436
CAS Analytical
Parameter
Number Method
Result Q LOQ
DL
Units
Run
Nickel
7440-02-0 6010D
17 3.3
0.88
mg/kg
1
Potassium
7440-09-7 6010D
2800 420
52
mg/kg
1
Selenium
7782-49-2 6010D
7.4 1.7
0.68
mg/kg
1
Sodium
7440-23-5 6010D
3500 420
52
mg/kg
1
Zinc
7440-66-6 6010D
1200 21
5.2
mg/kg
2
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
Sam plesKLeceipt t1w kllst(SRCi iME0018C-1S) :Zevi5ed:9/29/2o2Q
TV AnAyl&V I ss uing Authority: F ace ENV - W COL P4ge 10 1
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6, We,e sani pie ID9 listed on the CJ[7M
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7, Wese scuripie IDs listed on all sample containers?
Yes
E]NQ
S. Wa5 Collection date & cime Iisted on t.10 COS?
Yes
I LJ NO
$, Was culkclion elate & Limo listcd un all sample onnta icrs'?
v' Yes
©No
10. Did al I costa [rear label information (if), date, time) agree with the COC?
d Yes
i N o
11. Were tests to b4 prarfiwmod listed err the C(]t"!
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Yes
7! No
15, Wcrc any samples conminen ruissingl-.Ykcss (circle arc) samples No: listed cn CDC?
Yes
❑No
❑ T+EA
16. For VOA and RSK-175 sariple<e, were It.ihhl�; pr'eserht �"ped�53�e" (1/a"or 6min In di#tmelCrj
in arty al'ibe VOA vials?
Ryes
No
NA
7. Were a'I ORUiiie als}ir,trient salnpJos rezeived a[ a 13H of� 32
LJ Na
AEA
19. Wav aJ cyanide sar:rples received at a pH -� 12 vind sulfide smi pies received at a pH - 0?
Yes
❑No
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residual ch=ovine?
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C0".cIly !-,Intic7lhrr1 frnin !hr. (OC. inl+) Ihr• comment section in LIMS? 1
3'c
' N
1. 14'a9 tnc uom number listed or,1ho container lebe.? If 5 s_ Qaotc 4
.Sampk Prr:sx-.rvntinn (T4 mt br. c:Qm,plrt"I Rr any s#mplf!(.$) lm-ornmtly pmsermd or with Lcadspaoe_)
Samples) 1`116 werereceived iocrr--tictly pre;emed and were adjusted towWirtgy
in sample receit'ing with ''' mL of circle ore: I 121SO4, I IN03, IICI, Na0A using SIZ 4.. `lA
Time of preservation NA If inure than one preservad ve is needed, 71eaw now in the cornme,nis below.
Sample(S) NA -- — — -- - - -- — — - were rec aiml with bubbles mro in diarmctcr,
alq)les(�) ^ were rece ivexl with TRC > O.5 m D'L (4f g 19 k no) and were
a4iir: tcd amoHingly in 5amplc racaivirrg with wdium lba t sulCate (da Da) with Sheaty TD: NA
Sit 'na-errde labels applied by:.13fi2 - ----- Date: 01A302o3z
Comm cats=
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

0p
0
PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Chris Wynne
Project Name: Kinston WRF
Lot Number:XG27051
Date Completed:08/16/2022
NIM�� Mr�
08/16/2022 3:07 PM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: XG27051
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Inorganic Metals
Due to the matrix and low percent solids, the following sample has an initial volume is that 3x greater
than standard procedure: XG27051-001. The LOQ has been adjusted accordingly.
Inorganic Non -Metals
The method blank for prep batch 49397 contained the analyte total phosphate greater than the method
acceptance criteria. The associated samples contained detections for this analyte at concentrations
greater than 1 OX the value found in the method blank; therefore sample results are not impacted. The
data has been reported.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 7

Client: Synagro Laboratory ID: XG27051-001
Description: Kinstin WRF Matrix: Solid
Date Sampled:07/26/2022 1100 % Solids: 15.2 08/07/2022 1403
Date Received:07/27/2022
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 2540G
1 08/07/2022 1403 MJS2
50299
1 350.1
(Ammonia - N ) 350.1
50 08/03/2022 1326 CMM
49861
1
(Nitrate - N ) 353.2
1 07/29/2022 1355 KKP
49563
1
(Nitrite - N ) 353.2
1 07/29/2022 1355 KKP
49565
2
(Phosphorus) 365.1
150 07/30/2022 1629 DMA
07/28/2022 1345 49397
1
(Soil pH meas) 9045D
1 07/28/2022 1909 KKP
49586
1 351.4
(TKN) 351.2
10 07/28/2022 1911 DMA
07/28/2022 1152
49368
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
15.2
%
1
Ammonia - N (gas diffusion)
350.1
5800
330
170
mg/kg
1
Nitrate - N (soluble)
353.2
21
1.3
0.18
mg/kg
1
Nitrite - N (soluble)
353.2
2.3
1.3
0.17
mg/kg
1
Phosphorus
7723-14-0 365.1
42000
4900
990
mg/kg
2
Soil pH measured in water C)
24.2 ° C
9045D
7.1
su
1
TKN
351.2
63000
3300
1600
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 07/28/2022 1622 MRW2
07/28/2022 1449 49353
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471 B
0.076
0.075
0.018
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 08/01/2022 1441 JMH
08/01/2022 0046 49486
2 3050B
601OD
1 08/02/2022 0236 JMH
08/01/2022 0046 49486
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
27000
42
16
mg/kg
1
Arsenic
7440-38-2 6010D
4.4
1.6
0.52
mg/kg
1
Cadmium
7440-43-9 6010D
1.2
0.52
0.13
mg/kg
1
Calcium
7440-70-2 6010D
21000
520
65
mg/kg
1
Chromium
7440-47-3 6010D
31
1.0
0.26
mg/kg
1
Copper
7440-50-8 6010D
250
1.0
0.47
mg/kg
1
Iron
7439-89-6 6010D
14000
10
4.7
mg/kg
1
Lead
7439-92-1 6010D
20
1.0
0.47
mg/kg
1
Magnesium
7439-95-4 6010D
4900
520
65
mg/kg
1
Manganese
7439-96-5 6010D
230
1.6
0.62
mg/kg
1
Molybdenum
7439-98-7 6010D
5.9
4.2
1.0
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range DL - Detection Limit Q - Surrogate failure
ND - Not detected at or above the DL N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% J - Estimated result < LOQ and > DL L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client: Synagro Laboratory ID: XG27051-001
Description: Kinstin WRF Matrix: Solid
Date Sampled:07/26/2022 1100 % Solids: 15.2 08/07/2022 1403
Date Received:07/27/2022
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 08/01/2022 1441 JMH 08/01/2022 0046 49486
2 3050B 6010D 1 08/02/2022 0236 JMH 08/01/2022 0046 49486
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Nickel
7440-02-0
6010D
14
4.2
1.1
mg/kg
1
Potassium
7440-09-7
6010D
4500
520
65
mg/kg
1
Selenium
7782-49-2
6010D
5.3
2.1
0.85
mg/kg
1
Sodium
7440-23-5
6010D
4900
520
65
mg/kg
2
Zinc
7440-66-6
6010D
840
5.2
1.3
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range DL - Detection Limit Q - Surrogate failure
ND - Not detected at or above the DL N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% J - Estimated result < LOQ and > DL L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
5amP195 ixe aerpt ChecldJst t5ttQ {hr E00!LgC-is)
f �t���}'diC�l• Js�uir+ Authol'I RewJrd;'�/�9/��20
Pace ENV- WCO L P2 X of 1
Sample receipt heck[N-t C
c'f;rttr '� Gna] r fns ectad !{late• r
T.w ?,': ]( T Lk
r es v Nn !, Were ous110y seals present an the CDDill - —
Yes Ua " N, 2" If cimbody sep1s were rewen were d ¢matt and tnrbrvken7
S lrip lD' _ Chlorine SfTip M
ettal r�Ijaent eatraraC
1 upon Irocc/ip�t I Nrivil r[�Cr,ereoltd■) temPINMIUre opan reet<ipt %Solid Sup -Cup ]D,
had: Pere '' ° Blank ir�sJt lk3uttl s IR Guth 10;' ll V1.YM1IIL]I
hail of c�anl nr= .lam J Wer Ice � ice, 1D-1 f� ,�,,....... r� _. 1R C��rli Culrcrtlnn Factor_ 0 cc
No
MNA It temperature ot",t,ry cooler xcccded 6,D°C, wqg P1 j4Ct 1+lar�agCr Nolifiad7
Yt3
NV
P�{'n'Toti fir; phpQ� r �m�i] f face.to-Pae� (tiYcic one).
NA d, 19:11te entTimerei.d ooun'y
Yes
No
yg n]ip nttached m tFrie i`OQTrIY
S-, "Perm]UOPer etts[o,dY Micedutea {real uis}Mcclfrecofve falJrnow'�dF
Yes
)~1n
6. 1 'ere saMilk TD.5 lt=d an the ig
Yes
No
7, V4ef"- sarnplc IDS listed on alb sam It cauiltuimus?
i+_+�
NO
0. Wafi colle�ian date & ame Iis0ed on tree Zke4-
YCS
Yes
NU
- 1Vas culJecl{ort ilitta firm listed of atl1.90Mink ooa]talner�?
Yes
INo
No
I .Laid a}� c�rrta2srer ] bel inJ�Drrnali0n �If}, dare, tine} ag„ee u kh the li
11. Were tns#; to be pfor
erttrad listed M JJW
'fas
1 . did eJl samples arriv{s ire Else proper Containers for a
rush testandlor in ga+d cadditian
(urxlxuke�,, IJds an, et,c,)?
Yes
No
13, Was adequate, It valwna avplbblep
a Yes
yes
No
No
14. Were all Lqroplea reccivedwithin hn,9 tarpe Or 49 hOrtrs, wftirhaver tunes First
15, lte'er a vsarrE Pies urlttiner rnissiIrl fe[Coss(circleono}sam leat+Iot]fisted C7C7C7
E� Yes
Ian
[t�A 16• Fax VQA nud RISK.17-9 suripJea, were Ituhhles lxcsent?" pea-siae" (YI"ur 6mnt in 4iarrret� rn UY )
of the VOA VieIRY
Yes
'NO
No
NA 17- V4'ere all D1tCOYM Ls+ryutr'ient ya':Aug reeai at a
NA J anicte Sam Ies reonived
Dye$
D No
ut a H � I2 pnd e �ro les received nt EL PIT > 9^
N�h 19--"'ere � spit cai+le 11� 'cyanid tetly US. ' 6OJl-'I rc n I"
k'e_s o NA 20' ;Vere client +arksll' Vests (i.e, toque dilutiu¢ts, M5{ 81R dcsigtlMicnl8, etc, , , )
oorneody twnscribed from the COC Iwo tha cargtnOM section In LdMS7
No 1, 1Vas the liulc number iisl sd on the eorrCainor]ahci7 if as
Sample Fteserv,rtiole (f4?u�t ba-Mp2etcd for 9ny smupl�(sJ iir4ixrectly preserreorwith hea slxecae.)
5 pie{a) . ,ocitesire- H28G+w, e[tfeNrtt]m3w, HveCdIi,n1ga4r1eulyein rSrRrtl
aweil, ample eceiving with e dd i
NIM oprcsetaliarE Tf mare than ane prescrVative is naedegi l&mt etch in the e
P muttrcm below.
Samplo(s)
_were received with bubblos'6 mm in diarnuter,
Sa�r,lr[cs(s} �� �� ws,•r� djosteQ aecordio2 Y rrre�cved with' � 0.
5 rngIL {f#19 iamlc rw4iving will, 8oaiumthiitsle)fse s nv) and were
(NkS2() J with Shealy ID;
Sit bircode labels apptied by; -y Date-
_ �
CatnmetI
Pace Analytical Services, 1-LC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

0p
0
PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Chris Wynne
Project Name: Kinston WRF
Lot Number:X121026
Date Completed:10/14/2022
NIM�� Mr�
10/17/2022 9:30 AM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: X121026
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
The following samples were classified as biosolids therefore in order to ensure proper digestion they were
initially weighed out at around 3.0-3.5 grams: X121026-001. The LOQ has been adjusted accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 7

Client: Synagro Laboratory ID: X121026-001
Description: Kinston WRF Matrix: Solid
Date Sampled: 09/20/2022 1030 % Solids: 14.5 09/28/2022 2247
)ate Received:09/21/2022
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 2540G
1 09/28/2022 2247 CVR
55585
1 350.1
(Ammonia - N ) 350.1
50 09/28/2022 1342 CMM
55274
1
(Nitrate - N ) 353.2
1 09/29/2022 1735 KKP
55693
1
(Nitrite - N ) 353.2
1 09/29/2022 1735 KKP
55692
1
(Phosphorus) 365.1
200 10/08/2022 1526 DMA
10/07/2022 1400 56358
1
(Soil pH meas) 9045D
1 09/28/2022 1333 KKP
55528
1 351.4
(TKN) 351.2
10 10/07/2022 1808 DMA
10/06/2022 1447
56231
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 2540G
14.5
%
1
Ammonia - N (gas diffusion)
350.1
4600
340
180
mg/kg
1
Nitrate - N (soluble)
353.2
19
1.4
0.18
mg/kg
1
Nitrite - N (soluble)
353.2
0.65 J
1.4
0.18
mg/kg
1
Phosphorus
7723-14-0 365.1
41000
6900
1400
mg/kg
1
Soil pH measured in water C)
12.9 ° C
9045D
7.0
su
1
TKN
351.2
62000
3400
1700
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 09/23/2022 1216 MRW2
09/23/2022 1105 55055
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471 B
0.39 J
0.49
0.12
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601 OD
1 10/06/2022 0143 JMH
09/28/2022 0951
55322
3 3050B
601 OD
3 10/07/2022 2049 JMH
09/28/2022 0951
55322
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 601 OD
28000
40
15
mg/kg
1
Arsenic
7440-38-2 601 OD
4.1
1.5
0.50
mg/kg
1
Cadmium
7440-43-9 601 OD
1.3
0.50
0.13
mg/kg
1
Calcium
7440-70-2 601 OD
23000
500
63
mg/kg
1
Chromium
7440-47-3 601 OD
32
1.0
0.25
mg/kg
1
Copper
7440-50-8 601 OD
290
1.0
0.45
mg/kg
1
Iron
7439-89-6 601 OD
13000
10
4.6
mg/kg
1
Lead
7439-92-1 601 OD
22
1.0
0.45
mg/kg
1
Magnesium
7439-95-4 601 OD
7000
500
63
mg/kg
1
Manganese
7439-96-5 6010D
230
1.5
0.60
mg/kg
1
Molybdenum
7439-98-7 6010D
6.7
4.0
1.0
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range DL - Detection Limit Q - Surrogate failure
ND - Not detected at or above the DL N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% J - Estimated result < LOQ and > DL L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client: Synagro Laboratory ID: X121026-001
Description: Kinston WRF Matrix: Solid
Date Sampled: 09/20/2022 1030 % Solids: 14.5 09/28/2022 2247
Date Received:09/21/2022
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 10/06/2022 0143 JMH 09/28/2022 0951 55322
3 3050B 6010D 3 10/07/2022 2049 JMH 09/28/2022 0951 55322
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Nickel
7440-02-0
601OD
16
4.0
1.1
mg/kg
1
Potassium
7440-09-7
601OD
5000
500
63
mg/kg
1
Selenium
7782-49-2
601OD
4.9
2.0
0.82
mg/kg
1
Sodium
7440-23-5
601OD
5000
500
63
mg/kg
1
Zinc
7440-66-6
601OD
1000
15
3.8
mg/kg
3
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range DL - Detection Limit Q - Surrogate failure
ND - Not detected at or above the DL N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% J - Estimated result < LOQ and > DL L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

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SECTION 4

SUMM111
ENVIRONMENTAL TECHN❑LOMZ3. INC
Arraly0ca1 Laboralorfas
April 28, 2022
Chris Wynne
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL:
FAX:
RE: Kinston WRF
Dear Chris Wynne:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
Order No.: 22041528
Summit Environmental Technologies, Inc. received 1 sample(s) on 4/21/2022 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 2943, Colorado, Connecticut PH-0108, Florida NELAC E87688, Idaho OH00923, Illinois 200061, Indiana C-OH-13, Kansas
E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988, Minnesota 1780279, Nevada OH009232020-1, New
Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP CL0052, Oklahoma
2019-155, Oregon OH2O0001, Pennsylvania 011, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-19-16, Utah OH009232020-12,
Virginia VELAP 10381, West Virginia 9957C
Page 1 of 34

MM' Y Summit Environmental Technologies, Inc. Case Narrative
SU3310 Win St.
ENVIRONMENTAL TEC„HQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 wo#: 22041528
Arralyi9cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com Date: 4/28/2022
CLIENT: Synagro
Project: Kinston WRF
WorkOrder Narrative:
22041528: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
22041528-OOIA TCLP-SVOC-CPEST(8081B): Bracketing CCVs exhibited high recoveries for
Heptachlor and Methoxychlor. Sample is ND for these analytes.
Revision v1
Page 2 of 34

MM summit Environmental Technologies, In Qualifiers and Acronyms
SU3310 Win S
EkiwllOMM@NTALTECHN❑LOG{r,23.INC Cuyahoga Falls, Ohio442� Wo#: 22041528
Arraly0cal Laboralorlas TEL: [phone] FAX.- (330) 253-44E
Wehsite: httn:11www.settek.co Date: 4/28/2022
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
PLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Revision vl
Page 3 of 34

�� 1 � Summit Environmental Technologies, Inc.
SU3310 Win St.
ENVIROMMEWAL YECHNO ijULES. JNG, Cuyahoga Falls, Ohio 44223
Arraly0cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
CLIENT: Synagro
Project: Kinston WRF
Lab SamplelD Client Sample ID
22041528-001 Kinston WRF
Tag No Date Collected
4/20/2022 12:45:00 AM
Workorder
Sample Summary
WO#: 22041528
28 Apr-22
Date Received Matrix
4/21/2022 10:05:00 AM Sludge
Page 4 of 34

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SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arralyt9cal Laboralorfas TEL: [phone] FAX. [phone]
Website: http://n,n-m,.settek.coin
Analytical Report
(base report)
WO#: 22041528
Date Reported: 4/28/2022
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 4/20/2022 12:45:00 AM
Lab ID: 22041528-OOIA
Project: Kinston WRF
Client Sample ID Kinston WRF
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury
ND 0.00200 mg/L
SW7470A SW7470A Analyst: KLC
1 4/25/2022 5:23:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010
SW301OA Analyst: MSK
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
ND
0.500
mg/L
1
4/25/2022 4:26:00 PM
TCLP Barium(Ba)
ND
5.00
mg/L
1
4/25/2022 4:26:00 PM
TCLP Cadmium(Cd)
ND
0.100
mg/L
1
4/25/2022 4:26:00 PM
TCLP Chromium(Cr)
ND
0.200
mg/L
1
4/25/2022 4:26:00 PM
TCLP Lead(Pb)
ND
0.500
mg/L
1
4/25/2022 4:26:00 PM
TCLP Selenium(Se)
ND
0.0500
mg/L
1
4/25/2022 4:26:00 PM
TCLP Silver(Ag)
ND
0.500
mg/L
1
4/25/2022 4:26:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270
SW351OC Analyst: SFG
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
ND
0.200
mg/L
2
4/27/2022 12:18:00 AM
2,4,5-Trichlorophenol
ND
0.500
mg/L
2
4/27/2022 12:18:00 AM
2,4,6-Trichlorophenol
ND
0.500
mg/L
2
4/27/2022 12:18:00 AM
2,4-Dinitrotoluene
ND
0.100
mg/L
2
4/27/2022 12:18:00 AM
Cresols, Total
ND
10.0
mg/L
2
4/27/2022 12:18:00 AM
Hexachloro-1,3-butadiene
ND
0.0400
mg/L
2
4/27/2022 12:18:00 AM
Hexachlorobenzene
ND
0.100
mg/L
2
4/27/2022 12:18:00 AM
Hexachloroethane
ND
0.200
mg/L
2
4/27/2022 12:18:00 AM
Nitrobenzene
ND
0.200
mg/L
2
4/27/2022 12:18:00 AM
Pentachlorophenol
ND
0.500
mg/L
2
4/27/2022 12:18:00 AM
Pyridine
ND
0.500
mg/L
2
4/27/2022 12:18:00 AM
Surr: 2-Fluorophenol
78.4
10 - 157
m %Rec
2
4/27/2022 12:18:00 AM
Surr: Phenol-d6
67.6
10 - 169
%Rec
2
4/27/2022 12:18:00 AM
Surr: Nitrobenzene-d5
71.7
32.1 - 130
%Rec
2
4/27/2022 12:18:00 AM
Surr: 2,4,6-Tribromophenol
80.8
45.4 - 166
%Rec
2
4/27/2022 12:18:00 AM
Surr: 2-Fluorobiphenyl
68.4
35.7 - 130
%Rec
2
4/27/2022 12:18:00 AM
Surr: p-Terphenyl-d14
89.4
70 - 145
%Rec
2
4/27/2022 12:18:00 AM
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H Holding times for preparation or
analysis exceeded
M Manual Integration used to
determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified
compounds
ND Not Detected
OG1
P Second column confirmation exceeds
PL Permit Limit
Revision v1
R RPD outside accepted recovery limits
RL Reporting Detection Limit
Page 6 of 34

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arrafyt9caf Laboralorfas TEL: [phone] FAX. [phone]
Website: http://n,n-m,.settek.coin
Analytical Report
(base report)
WO#: 22041528
Date Reported: 4/28/2022
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 4/20/2022 12:45:00 AM
Lab ID: 22041528-OOIA
Project: Kinston WRF
Client Sample ID Kinston WRF
Analyses
Result
RL
Qual
Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8081
SW351OC Analyst: PGP
TCLP PESTICIDES ANALYSIS
(SW1311/8081)
Chlordane, total
ND
0.0250
mg/L
10
4/26/2022 2:23:00 AM
Toxaphene
ND
0.0500
mg/L
10
4/26/2022 2:23:00 AM
Endrin
ND
0.00500
d
mg/L
10
4/26/2022 2:23:00 AM
gamma-BHC
ND
0.00500
d
mg/L
10
4/26/2022 2:23:00 AM
Heptachlor
ND
0.00500
dQC+
mg/L
10
4/26/2022 2:23:00 AM
Heptachlor epoxide
ND
0.00500
d
mg/L
10
4/26/2022 2:23:00 AM
Methoxychlor
ND
0.00500
d
mg/L
10
4/26/2022 2:23:00 AM
Surr: TCMX
75.7
10 - 119
%Rec
10
4/26/2022 2:23:00 AM
Surr: DCB
91.9
10 - 119
%Rec
10
4/26/2022 2:23:00 AM
TCLP HERBICIDES BY EPA 8321B
SW8321
Analyst: RIS
2,4-D ND
0.500
mg/L
50
4/26/2022 3:42:00 AM
2,4,5-TP ND
0.500
mg/L
50
4/26/2022 3:42:00 AM
Surr: 2,4-Dichlorophenylacetic aci 115
70 - 130
%Rec
50
4/26/2022 3:42:00 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260
SW1311M Analyst: NAW
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene ND
0.250
mg/L
50
4/24/2022 5:37:00 AM
1,2-Dichloroethane ND
0.250
mg/L
50
4/24/2022 5:37:00 AM
MEK ND
5.00
mg/L
50
4/24/2022 5:37:00 AM
Benzene ND
0.250
mg/L
50
4/24/2022 5:37:00 AM
Carbon tetrachloride ND
0.250
mg/L
50
4/24/2022 5:37:00 AM
Chlorobenzene ND
2.50
mg/L
50
4/24/2022 5:37:00 AM
Chloroform ND
0.250
mg/L
50
4/24/2022 5:37:00 AM
Tetrachloroethene ND
0.250
mg/L
50
4/24/2022 5:37:00 AM
Trichloroethene ND
0.250
mg/L
50
4/24/2022 5:37:00 AM
Vinyl chloride ND
0.100
mg/L
50
4/24/2022 5:37:00 AM
Surr: 4-Bromofluorobenzene 91.9
70 - 130
%Rec
50
4/24/2022 5:37:00 AM
Surr: Di brom ofl uorom ethane 96.3
70 - 130
%Rec
50
4/24/2022 5:37:00 AM
Surr: Toluene-d8 105
70 - 130
%Rec
50
4/24/2022 5:37:00 AM
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration used to
determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified
compounds
ND Not Detected
OG1
P Second column confirmation exceeds
PL Permit Limit
Revision v1
R RPD outside accepted recovery limits
RL Reporting Detection Limit
Page 7 of 34

MMIT
Summit Environmental Technologies, Inc. Analytical Report
SU3310 Win St.
ENVIRONMENTAL TECHNOLOGIE-3, IRC Cuyahoga Falls, Ohio 44223 (base report)
Arralyt9cal Laboralorfas TEL: [phone] FAX.- [phone] WO#: 22041528
Website: http://www.settek.com Date Reported: 4/28/2022
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 4/20/2022 12:45:00 AM
Lab ID: 22041528-OOIA
Project: Kinston WRF
Client Sample ID Kinston WRF
Analyses
Result
RL Qual Units
DF
Date Analyzed
RCI
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive
ND
0.490 mg/Kg
1
4/25/2022 10:55:00 AM
IGNITABILITY OF SOLIDS (SW-846: 1030)
SW1030
Analyst: ALT
Ignitability nonflammable
mm/sec
1
4/22/2022 5:58:59 PM
PERCENT SOLIDS BY SM2540MOD
A2540B
Analyst: HDJ
Percent Solids
15.0
%
1
4/25/2022 3:00:00 PM
RCI
SW9045D
Analyst: ALT
PH (SW9045D)
pH
7.5
s.u.@19.5C
1
4/27/2022 12:52:15 PM
RCI
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive
ND
25.0 mg/Kg
1
4/25/2022 10:55:00 AM
Qualifiers: B
Analyte detected in the associated Method Blank
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
OG I
PL Permit Limit Revision vl
RL Reporting Detection Limit
Page 8 of 34

Summit Environmental Technologies, Inc.
Accreditation
Program
fr
3310 Win St.
SUMMIEF
Analv tes Report
n
ENOROMMEWAL IrECHNOL.OG{r,S,
INC Cuyahoga Falls, Ohio 44223
J
Y
Arraly0cal Laboralorlas
TEL: [phone] FAX.- [phone]
Wo#:
22041528
Wehsite: http://www.settek.com
28 Apr-22
Client: Synagro
State: NW
Project: Kinston WRF
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
22041528-OOIA Sludge
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Sludge
Percent Solids by SM2540Mod
Percent Solids
N
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Sludge
TCLP Herbicides by EPA 8321B
2,4,5-TP
A
Sludge
TCLP Herbicides by EPA 8321B
2,4-D
A
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Key
Key
Key
NC WW SCM A Accredited
NC WW SCM N Not Accredited
NC WW SCM U
Unavailabl
Version #2
Page 9 of 34

Summit Environmental Technologies, Inc.
Accreditation
Program
SUMMIEF
fr3310 Win St.
Analv n tes Report
EMOROMMEWAL IrECHHOL.OG{r,S,
INC Cuyahoga Falls, Ohio 44223
J
Y
Arraly0cal Laboralorlas
TEL: [phone] FAX.- [phone]
Wo#:
22041528
Wehsite: http://www.settek.com
28 Apr-22
Client: Synagro
State: NW
Project: Kinston WRF
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
22041528-OOIA Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Sludge
TCLP Volatiles Analysis
1, 1 -Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chloroform
A
Sludge
TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge
TCLP Volatiles Analysis
Trichloroethene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
NC WW SCM A Accredited NC WW SCM N Not Accredited NC WW SCM U Unavailabl
Version #2
Page 10 of 34

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Page 33 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHN❑L4Ga1�S.IfiC Cuyahoga Falls, Ohio44223 Sample Log -In Check List
Arrafocaf Laboralorias TEL: [phone] FAX.- [phone]
Website: http://`h,,",m,.settek.coin
Client Name: SYN-NC-27028 Work Order Number: 22041528 RcptNo: 1
Logged by: Brandon J. Clark 4/21/2022 10:05:00 AM
Completed By: Jennifer Woolf 4/22/2022 8:35:10 AM i?►�
Reviewed By: Christopher Stefan 4/22/2022
Chain of Custody
1. Is Chain of Custody complete? Yes ❑d No ❑ Not Present ❑
2. How was the sample delivered? UPS
Lop In
3. Coolers are present? Yes ❑d No ❑ NA ❑
4. Shipping container/cooler in good condition?
Yes
d❑
No
❑
Custody seals intact on shipping container/cooler?
Yes
❑
No
❑
Not Present V
No. Seal Date:
Signed By:
5. Was an attempt made to cool the samples?
Yes
❑d
No
❑
NA ❑
6. Were all samples received at a temperature of >0° C to 6.0°C
Yes
❑d
No
❑
NA ❑
7. Sample(s) in proper container(s)?
Yes
❑d
No
❑
8. Sufficient sample volume for indicated test(s)?
Yes
❑d
No
❑
g. Are samples (except VOA and ONG) properly preserved?
Yes
❑d
No
❑
10. Was preservative added to bottles?
Yes
❑
No
❑d
NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
❑
No
❑ No VOA Vials ❑�
12. Were any sample containers received broken?
Yes
❑
No
❑d
13. Does paperwork match bottle labels?
Yes
No
❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
❑d
No
❑
15. Is it clear what analyses were requested?
Yes
❑d
No
❑
16. Were all holding times able to be met?
Yes
No
❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
❑
No
❑ NA V
Person Notified: Date:
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Cooler Information
Cooler No
Temp °C
Condition
I Seal Intact
Seal No
Seal Date
Signed By
1
10.3
Goodl
Not Present
Page 34 of 34

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City ofKinston WQ Permit Number: WQ0003919
WWTP Name: Kinston Regional WRF NPDES Number- NCO024236
Monitoring Period: Frein 01/01/22 To 12/31/22
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please Indicate level achieved and alternative performed:
Class A:
Alt. 1/A (timeltemp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Dying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the following monitor€ne data:
Parameter.
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10 to the 61h
MPN
MPN/g
Coliform
power per gram
of total solids
CFU
373000
903000
2170000
CFU/g
0
Annually
Grab
SM9222D
-MF
1000 MPN per gram of
MPNIg
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503,33/15A NCAC 02T.1107) - Please Indicate option/alternative performed:
0ption/Alt. i
Option/Alt, 2
(VS reduction)
(40-day bench)
Option/Alt. 5
Option/Alt. 6
(14-Day Aerobic)
(Alk Stabilization)
Option/Alt. 9
Option/Alt. 10
(injection)
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
Option/Alt. 3
Option/Alt, 4
(30-day bench)
(Spec. 02 uptake) X
Option/Alt, 7
Option/Alt. 8
(Drying — Stable)
(Drying —Unstable)
No vector attraction reduction alternatives were performed
"I certify, under penalty of law, that the pathogen reqquirements in 40 CFR 503,32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33115A NCAC 02T,1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503,32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Kenneth Stevens Wastewater Superintendent
Pre arer Name and Title ( print or type) Land Applier Name and Title (if applicable) (type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 4 FR Part 503.9(r) and 15A NCAC 2T.1 l02 (26)

Cameron Testing Services, Inc. Laboratory Report NC DENR#654
NC PHHS #37799
US EPA #NC01918
Client: Synagro CTS Proj. 2201-0082 DWCert#37799
Project: Kinston WRF Regulatory Yes
Sample Information
Sampled
C. Wynne
Date 01/10/22 Received
J.
Cameron Date
01/10/22
Analyses and Results
Lab ID
Sample ID
p
E
a Analyte .. Result
E
H
d }, :
w E ,�
Std. Methods
2 �
o =
Reference
16- -x -
2201- 01
-01
Sludge Gr Fec. Coliform-S 692000
CFUfg
10 01/10/22 CSC
92220 - MF
-02
1400000
cFurg
10
-03
990000
cFurg
10
-04
373000
CFUlg
10
-05
613000
cFurg
10
-06
2170000
CFUrg
10
-07
1030000
cFurg
10
Geomean 903000
2201- 01
-01
swage Gr TS (%) 15.4
%
001 01 /13/22 KW
2540 G -TS
-02
16.5
0A
0.01
-03
15.1
%
0.01
-04
15.2
%
0.01
-05
15.2
%
0.01
-06
16.2
%
a.01
-07
16.0
%
a.o�
Report
Review
Project Manager
Date
219 S. Steele Str. 919.208-4240
Sanford NC 27330 chris rCi eamerontesting.com

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Specific Oxygen Uptake Rate
SOUR
Facility Name: KRWRF
Biosolids Permit Number: WQ0003919
Date: 3/10/2022
Digester Temperature: 14
Sampling Date/Time: 3/10/22 8:06am
Sampled By: SF
Analysis Date/Time: 3/10/22
Analyzed By: SF
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/1)
9.04
8.22
7.84
7.58
7.35
7.13
6.92
6.69
6.47
6.24
6
5.76
5.52
5.28
5.02
4.78
Slope
I ntercept
Correlation Coefficient
am
300 milliliters
1.9 % Dry Solids
13.1 degrees Celsius
15 degrees Celsius
Oxygen Uptake Rate: mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: mg Oxygen/g/hr
Average Temperature: 14.05 degrees Celsius
Temperature Correction Factor: 1.5
Temperature Corrected Specific Oxygen Uptake Rate: 0.81 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
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Specific Oxygen Uptake Rate
SOUR
Facility Name: KRWRF
Biosolids Permit Number: WQ0003919
Date: 3/10/2022
Digester Temperature: 14
Sampling Date/Time: 3/10/22 8:35am
Sampled By: SF
Analysis Date/Time: 3/10/22
Analyzed By: SF
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/1)
10.1
9.17
8.86
8.65
8.46
8.27
8.07
7.87
7.66
7.45
7.23
7.01
6.76
6.52
6.29
6.04
Slope
I ntercept
Correlation Coefficient
am
300 milliliters
1.9 % Dry Solids
11.8 degrees Celsius
15.3 degrees Celsius
Oxygen Uptake Rate: mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: mg Oxygen/g/hr
Average Temperature: 13.55 degrees Celsius
Temperature Correction Factor: 1.5
Temperature Corrected Specific Oxygen Uptake Rate: 0.77 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
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Specific Oxygen Uptake Rate
SOUR
Facility Name: KRWRF
Biosolids Permit Number: WQ0003919
Date: 3/10/2022
Digester Temperature: 14
Sampling Date/Time: 3/10/22 9:20am
Sampled By: SF
Analysis Date/Time: 3/10/22
Analyzed By: SF
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/1)
10.05
9.6
9.39
9.19
8.99
8.78
8.58
8.38
8.19
7.97
7.75
7.54
7.31
7.09
6.86
6.63
Slope
I ntercept
Correlation Coefficient
am
300 milliliters
1.9 %Dry Solids
12 degrees Celsius
14.4 degrees Celsius
Oxygen Uptake Rate: mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: mg Oxygen/g/hr
Average Temperature: 13.2 degrees Celsius
Temperature Correction Factor: 1.6
Temperature Corrected Specific Oxygen Uptake Rate: 0.80 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
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Specific Oxygen Uptake Rate
SOUR
Facility Name: KRWRF
Biosolids Permit Number: WQ0003919
Date: 3/10/2022
Digester Temperature: 14
Sampling Date/Time: 3/10/22 9:45am
Sampled By: SF
Analysis Date/Time: 3/10/22
Analyzed By: SF
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/1)
9.49
9.1
8.94
8.72
8.51
8.33
8.16
7.91
7.66
7.43
7.21
7.02
6.83
6.6
6.42
6.24
Slope
I ntercept
Correlation Coefficient
am
300 milliliters
1.9 % Dry Solids
11.6 degrees Celsius
13.7 degrees Celsius
Oxygen Uptake Rate: mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: mg Oxygen/g/hr
Average Temperature: 12.65 degrees Celsius
Temperature Correction Factor: 1.6
Temperature Corrected Specific Oxygen Uptake Rate: 0.72 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
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Specific Oxygen Uptake Rate
SOUR
Facility Name: KRWRF
Biosolids Permit Number: WQ0003919
Date: 3/10/2022
Digester Temperature: 14
Sampling Date/Time: 3/10/22 10:12am
Sampled By: SF
Analysis Date/Time: 3/10/22
Analyzed By: SF
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/1)
9.4
8.2
8
7.78
7.67
7.6
7.38
7.18
7.02
6.87
6.73
6.59
6.45
6.32
6.18
6.05
Slope
I ntercept
Correlation Coefficient
300 milliliters
1.9 % Dry Solids
12.1 degrees Celsius
14.5 degrees Celsius
Oxygen Uptake Rate: mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: mg Oxygen/g/hr
Average Temperature: 13.3 degrees Celsius
Temperature Correction Factor: 1.6
Temperature Corrected Specific Oxygen Uptake Rate: 0.49 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
5

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Specific Oxygen Uptake Rate
SOUR
Facility Name: KRWRF
Biosolids Permit Number: WQ0003919
Date: 6/24/2022
Digester Temperature: 22
Sampling Date/Time: 6/24/2022 8:14
Sampled By: SF
Analysis Date/Time: 6/24/
Analyzed By: SF
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/1)
8.91
6.71
6.22
5.74
5.27
4.78
4.33
3.95
3.33
2.93
2.55
2.2
1.89
1.55
1.28
1
Slope
I ntercept
Correlation Coefficient
300 milliliters
2 % Dry Solids
21.9 degrees Celsius
21.5 degrees Celsius
Oxygen Uptake Rate: mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: mg Oxygen/g/hr
Average Temperature: 21.7 degrees Celsius
Temperature Correction Factor: 0.9
Temperature Corrected Specific Oxygen Uptake Rate: 0.27 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
1

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Specific Oxygen Uptake Rate
SOUR
Facility Name: KRWRF
Biosolids Permit Number: WQ0003919
Date: 6/24/2022
Digester Temperature: 22
Sampling Date/Time: 6/24/2022 8:51
Sampled By: SF
Analysis Date/Time: 6/24/
Analyzed By: SF
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/1)
8.04
6.78
6.34
5.9
5.46
5.01
4.59
4.17
3.73
3.28
2.85
2.42
1.98
1.52
1.13
0.67
Slope
I ntercept
Correlation Coefficient
300 milliliters
2 % Dry Solids
21.8 degrees Celsius
21.6 degrees Celsius
Oxygen Uptake Rate: mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: mg Oxygen/g/hr
Average Temperature: 21.7 degrees Celsius
Temperature Correction Factor: 0.9
Temperature Corrected Specific Oxygen Uptake Rate: 0.36 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
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Specific Oxygen Uptake Rate
SOUR
Facility Name: KRWRF
Biosolids Permit Number: WQ0003919
Date: 6/24/2022
Digester Temperature: 22
Sampling Date/Time: 6/24/2022 9:45
Sampled By: SF
Analysis Date/Time: 6/24/
Analyzed By: SF
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/1)
8.45
7.74
7.48
7.25
7.02
6.79
6.59
6.37
6.15
5.93
5.64
5.28
5.06
4.88
4.62
4.4
Slope
I ntercept
Correlation Coefficient
300 milliliters
2 % Dry Solids
22.3 degrees Celsius
22.2 degrees Celsius
Oxygen Uptake Rate: mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: mg Oxygen/g/hr
Average Temperature: 22.2 degrees Celsius
Temperature Correction Factor: 0.9
Temperature Corrected Specific Oxygen Uptake Rate: 0.21 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
3

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Specific Oxygen Uptake Rate
SOUR
Facility Name: KRWRF
Biosolids Permit Number: WQ0003919
Date: 6/24/2022
Digester Temperature: 22
Sampling Date/Time: 6/24/2022 10:13
Sampled By: SF
Analysis Date/Time: 6/24/2
Analyzed By: SF
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/1)
8.72
7.4
6.95
6.51
6.07
5.64
5.2
4.8
4.5
4.22
3.96
3.7
3.44
3.18
2.91
2.64
Slope
I ntercept
Correlation Coefficient
300 milliliters
2 % Dry Solids
22.3 degrees Celsius
22.1 degrees Celsius
Oxygen Uptake Rate: mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: mg Oxygen/g/hr
Average Temperature: 22.2 degrees Celsius
Temperature Correction Factor: 0.9
Temperature Corrected Specific Oxygen Uptake Rate: 0.22 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
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Specific Oxygen Uptake Rate
SOUR
Facility Name: KRWRF
Biosolids Permit Number: WQ0003919
Date: 6/24/2022
Digester Temperature: 22
Sampling Date/Time: 6/24/2022 10:40
Sampled By: SF
Analysis Date/Time: 6/24/2
Analyzed By: SF
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
8.44
1
7.02
2
6.58
3
6.16
4
5.83
5
5.57
6
5.28
7
5
8
4.7
9
4.43
10
4.15
11
3.88
12
3.6
13
3.33
14
3.07
15
2.78
Slope:
I ntercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
300 milliliters
2 % Dry Solids
22.5 degrees Celsius
22.2 degrees Celsius
mg Oxygen/hr
mg Oxygen/g/hr
22.3 degrees Celsius
0.9
Temperature Corrected Specific Oxygen Uptake Rater 0.22 mg Oxygen/g/hr
0.225275
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
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Specific Oxygen Uptake Rate
SOUR
Facility Name: KRWRF
Biosolids Permit Number: WQ0003919
Date: 9/23/2022
Digester Temperature: 20
Sampling Date/Time: 9/23/22 7:53am
Sampled By: SF
Analysis Date/Time: 9/23/22
Analyzed By: SF
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/1)
9.08
8.36
8.12
7.91
7.7
7.5
7.3
7.11
6.92
6.75
6.6
6.5
6.38
6.27
6.16
6.05
Slope
I ntercept
Correlation Coefficient
am
300 milliliters
1.9 % Dry Solids
19.9 degrees Celsius
20.5 degrees Celsius
Oxygen Uptake Rate: mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: mg Oxygen/g/hr
Average Temperature: 20.2 degrees Celsius
Temperature Correction Factor: 1
Temperature Corrected Specific Oxygen Uptake Rate: 0.20 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
1

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Specific Oxygen Uptake Rate
SOUR
Facility Name: KRWRF
Biosolids Permit Number: WQ0003919
Date: 9/23/2022
Digester Temperature: 20
Sampling Date/Time: 9/23/22 8:21am
Sampled By: SF
Analysis Date/Time: 9/23/22
Analyzed By: SF
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/1)
9.03
8.51
8.3
8.12
7.94
7.76
7.58
7.41
7.22
7.04
6.87
6.69
6.51
6.35
6.22
6.11
Slope
I ntercept
Correlation Coefficient
300 milliliters
1.9 % Dry Solids
19.8 degrees Celsius
19.4 degrees Celsius
Oxygen Uptake Rate: mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: mg Oxygen/g/hr
Average Temperature: 19.6 degrees Celsius
Temperature Correction Factor: 1
Temperature Corrected Specific Oxygen Uptake Rate: 0.25 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
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Specific Oxygen Uptake Rate
SOUR
Facility Name: KRWRF
Biosolids Permit Number: WQ0003919
Date: 9/23/2022
Digester Temperature: 20
Sampling Date/Time: 9/23/22 8:51am
Sampled By: SF
Analysis Date/Time: 9/23/22
Analyzed By: SF
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/1)
9.12
8.72
8.55
8.43
8.23
8.1
8.02
7.92
7.83
7.75
7.67
7.58
7.49
7.41
7.34
7.25
Slope
I ntercept
Correlation Coefficient
300 milliliters
1.9 % Dry Solids
19.8 degrees Celsius
20 degrees Celsius
Oxygen Uptake Rate: mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: mg Oxygen/g/hr
Average Temperature: 19.9 degrees Celsius
Temperature Correction Factor: 1
Temperature Corrected Specific Oxygen Uptake Rate: 0.13 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
3

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Specific Oxygen Uptake Rate
SOUR
Facility Name: KRWRF
Biosolids Permit Number: WQ0003919
Date: 9/23/2022
Digester Temperature: 20
Sampling Date/Time: 9/23/22 9:20am
Sampled By: SF
Analysis Date/Time: 9/23/22
Analyzed By: SF
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/1)
8.99
8.52
8.34
8.23
8.12
8.04
7.95
7.85
7.76
7.67
7.59
7.5
7.42
7.32
7.25
7.17
Slope
I ntercept
Correlation Coefficient
300 milliliters
1.9 % Dry Solids
19.7 degrees Celsius
19.5 degrees Celsius
Oxygen Uptake Rate: mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: mg Oxygen/g/hr
Average Temperature: 19.6 degrees Celsius
Temperature Correction Factor: 1
Temperature Corrected Specific Oxygen Uptake Rate: 0.13 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
4

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Specific Oxygen Uptake Rate
SOUR
Facility Name: KRWRF
Biosolids Permit Number: WQ0003919
Date: 9/23/2022
Digester Temperature: 20
Sampling Date/Time: 9/23/22 9:58am
Sampled By: SF
Analysis Date/Time: 9/23/22
Analyzed By: SF
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/1)
9.06
8.75
8.6
8.48
8.37
8.29
8.2
8.11
8.02
7.95
7.86
7.77
7.67
7.61
7.53
7.46
Slope
I ntercept
Correlation Coefficient
300 milliliters
1.9 %Dry Solids
19.5 degrees Celsius
19.8 degrees Celsius
Oxygen Uptake Rate: mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: mg Oxygen/g/hr
Average Temperature: 19.65 degrees Celsius
Temperature Correction Factor: 1
Temperature Corrected Specific Oxygen Uptake Rate: 0.13 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
5

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Specific Oxygen Uptake Rate
SOUR
Facility Name: KRWRF
Biosolids Permit Number: WQ0003919
Date: 11 /23/2
Digester Temperature:
Sampling Date/Time: 11/23/22
Sampled By: SF
Analysis Date/Time: 11/23/22
Analyzed By: SF
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/1)
10.57
10.64
10.36
10.25
10.17
10.1
10.02
9.95
9.86
9.97
9.69
9.6
9.52
9.41
9.32
9.21
Slope
I ntercept
Correlation Coefficient
13
7:5
300 milliliters
1.9 % Dry Solids
10.6 degrees Celsius
13.8 degrees Celsius
Oxygen Uptake Rate: mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: mg Oxygen/g/hr
Average Temperature: 12.2 degrees Celsius
Temperature Correction Factor: 1.72
Temperature Corrected Specific Oxygen Uptake Rate: 0.45 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
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Specific Oxygen Uptake Rate
SOUR
Facility Name: KRWRF
Biosolids Permit Number: WQ0003919
Date: 11 /23/2
Digester Temperature:
Sampling Date/Time: 11/23/22
Sampled By: SF
Analysis Date/Time: 11/23/22
Analyzed By: SF
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/1)
10.58
10.53
10.39
10.28
10.21
10.16
10.09
10.02
9.95
9.87
9.8
9.72
9.63
9.55
9.46
9.37
Slope
I ntercept
Correlation Coefficient
13
8:2
300 milliliters
1.9 % Dry Solids
10.7 degrees Celsius
13.8 degrees Celsius
Oxygen Uptake Rate: mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: mg Oxygen/g/hr
Average Temperature: 12.25 degrees Celsius
Temperature Correction Factor: 1.72
Temperature Corrected Specific Oxygen Uptake Rate: 0.40 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
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Specific Oxygen Uptake Rate
SOUR
Facility Name: KRWRF
Biosolids Permit Number: WQ0003919
Date: 11 /23/2
Digester Temperature:
Sampling Date/Time: 11/23/22
Sampled By: SF
Analysis Date/Time: 11/23/22
Analyzed By: SF
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/1)
10.68
10.45
10.3
10.23
10.17
10.11
10.05
9.99
9.93
9.85
9.78
9.69
9.62
9.53
9.45
9.36
Slope
I ntercept
Correlation Coefficient
13
9:0
300 milliliters
1.9 %Dry Solids
11 degrees Celsius
13.6 degrees Celsius
Oxygen Uptake Rate: mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: mg Oxygen/g/hr
Average Temperature: 12.3 degrees Celsius
Temperature Correction Factor: 1.72
Temperature Corrected Specific Oxygen Uptake Rate: 0.39 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
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Specific Oxygen Uptake Rate
SOUR
Facility Name: KRWRF
Biosolids Permit Number: WQ0003919
Date: 11 /23/2
Digester Temperature:
Sampling Date/Time: 11/23/22
Sampled By: SF
Analysis Date/Time: 11/23/22
Analyzed By: SF
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/1)
10.59
10.52
10.34
10.26
10.2
10.14
10.09
10.03
9.98
9.89
9.83
9.76
9.67
9.59
9.52
9.43
Slope
I ntercept
Correlation Coefficient
13
9:3
300 milliliters
1.9 % Dry Solids
10.6 degrees Celsius
13.4 degrees Celsius
Oxygen Uptake Rate: mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: mg Oxygen/g/hr
Average Temperature: 12 degrees Celsius
Temperature Correction Factor: 1.72
Temperature Corrected Specific Oxygen Uptake Rate: 0.31 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
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SECTION 6

Agricultural Lime Application Log
Year2022
Project Kinston
Fields
Soil
Lime Requirements
Tons/Acre Date
(state -county -site -field)
PH
(from soil analysis)
AAplied Allied
JO-8790-4A
5.6
0.8T
N/A
JO-8790-413
5.6
0.9T
N/A
JO-8790-5
5
1.6T
N/A
JO-8790-6
5.1
1.4T
N/A
JO-8790-7
5.2
1.2T
N/A
JO-8790-11
6.3
OT
N/A
JO-8790-12
6.6
OT
N/A
N/A- Did not apply in 2022
*Lime will be applied when field conditions/cropping pattern permits

SECTION 7

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