WQ0001026_2022 Residual Annual Report_20230228 (2)

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * WQ0001026
Applicant/Permittee City of Washington
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Washington
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Brent Collins
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
336-399-3646
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation High -Rate Infiltration
Other Wastewater Reclaimed Water
Closed -Loop Recycle Residuals
Single -Family Residence Wastewater Other
Irrigation
Permit Number:* WQ0001026
Has Current Existing permit number
Applicant/Permittee Address* PO Box 1988, Washington, NC 27889
Facility Name* City of Washington Class B Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2022 Washington Annual Report - WQ0001026.pdf 6.26MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/28/2023

February 28, 2023
DENR/Water Quality Section
Non -Discharge Compliance Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2022 Annual Report - Washington
Treatment and Land Application of Residuals
Permit No. WQ0001026
Dear Sir or Madam:
Enclosed is the 2022 Annual Report for the above referenced land application permit.
During 2022 EMA Resources, Inc. land applied 232.37 dry tons of wastewater residuals
to 105.38 acres of private farmland. Please contact Brent Collins - Director of Technical
Services if you have any further questions regarding this report.
Sincerely,
Z.-e4:241-
Brent Collins
Director of Technical Services
brent.collins&emaresourcesinc.com
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

--Resources, Inc.
City of Washington
2022 Annual Report
Residuals Land Application
Permit No. WQ0001026
Prepared By:
EMA Resources, Inc.
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0001026 County: Beaufort County, NC Year:
2022
Facility Name (as shown on permit):
Land Application Operator:
City of Washington
EMA Resources Inc. Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
El Yes 0 No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in thepermit:
54
Total number of fields utilized for land application during the year:
3
Total amount of dry tons applied during the year for all application sites:
232.37
Total number of acres utilizes for land application during the year:
105.38
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2022 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. R1 Yes 0 No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and time was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Hope Woolard - Public Works Director
h`DdG �710DIaj-Gf Feb 7, 2023
Ho�lard (Feb 7, 2023 08:02 EST)
Permittee Name and Title (type or print) Signature of Permittee Date
ZeynPi I;Vm0w471- Feb 1 2023Z�fz Lonnie I Woolard Jr (Feb 1, 202314:31 EST) 1 /3 1 /2023
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0001026 Laboratory: 1)
Facility Name: City of Washington 2)
Residual Source WQ # or NCO020648 3)
NPDES #: 4)
WWTP Name: Washington WWTP 5)
Recidnal AnAvcic Data
Waypoint Analytical
Parameter
(mg/kg)(mg/kg
Conc.
Limit
a
Sample or Composite Date
4/6/22
4/20/22
Spring
Average
10/19/22
10/27/22
Fall
Average
Percent Solids (%)
NA
2.87
3.32
3.10
3.72
3.7
3.71
Arsenic
75
17.2
7.27
12.2
6.7
7.38
7.04
Cadmium
85
3.45
0.706
2.1
0.611
0.806
0.71
Copper
4,300
272
345
308.5
308
344
326.00
Chromium
NA
29.8
23
26.4
22.7
26.2
24.45
Lead
840
23.3
31.8
27.6
26.1
30
28.05
Mercury
57
0.572
0.864
0.7
0.868
0.283
0.58
Molybdenum
75
8.62
5.48
7.1
6.22
5.91
6.07
Nickel
420
14
16.4
15.2
17.6
18
17.80
Selenium
100
17.2
9.7
13.5
9.41
9.41
9.41
Zinc
7,500
683
852
767.5
827
941
884.00
Total Phosphorus
NA
33500
36400
34950
38100
38200
38150
TKN
NA
67900
51200
59550
47600
55000
51300
Ammonia -Nitrogen
NA
7860
8360
8110.0
12000
10100
11050
Nitrate and Nitrite
NA
366
273
319.5
147
143
145
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Zoeel /7` Feb 1 2023
Lonnie I Woolard Jr (Feb 1, 2023 14:31 EST) 7
Signature of Preparer *
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number:
WQ0001026
Facility Name: City of Washington
Residual Source
NPDES # or WQ#:
WWTP Name:
Residual Analvsis Data
NCO020648
Washington WWTP
Laboratory: 1) Waypoint Analytical
2)
3)
4)
5)
Parameter
(mg/kg)
Sample or Composite Date
4/6/22
4/20/22
Average
10/19/22
10/27/22
A erage
Aluminum
39700
38500
39100
40300
44100
42200
Calcium
21800
34200
28000
27600
30300
28950
Magnesium
3190
3580
3385
3110
3470
3290
pH
6.8
6.7
6.75
7
7
7
Potassium
3690
3390
3540
2660
2860
2760
Sodium
4100
3360
3730
3490
1 4000
3745
PAN
22308
17305
19807
16827
18663
17745
SAR
1.16
0.84
1.02
1.11
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
LOIm`U21;Vy1wG�47/-
Lonnie I Woolard Jr (Feb 1, 202314:31 EST)
Signature of Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Feb 1, 2023
Date
DENR FORM RSSF - B (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Washington Total Dry Tons Applied (Annual): 125.67
Permit #: WQ0001026 Cation Exchange Capacity (non 503 only):
Operator: Hunter Roost Farms Owner: Hunter Roost Farms Predominant Soil Series: GoA
Acres Used: 64.02 Acres Permitted: 64.02 Site #: BF210 Field #: 4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phorus
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total
11
21
3
4
5j
6j
7j
81
9
10
ill
12
DT/Ac./
App.
.fir
Event
1.96
Arsenic
0.028
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.028
Cadmium
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Copper
1.280
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.280
Chromium
0.096
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.096
Lead
0.110
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.110
Mercury
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molyb-
0.024
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.024
denum
Nickel
0.070
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.070
Selenium
0.037
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.037
Zinc
3.471
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.471
Total
Phos-
149.777
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
149.777
horus
1
1
1
1
"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
1/31/2023
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Washington
Hunter Roost Farms
Operator: Hunter Roost Farms
Crop 1 Name: Rye - Grain
WQ Permit #: WQ0001026 Field #:
Annual Dry Tons Applied: 125.67 Site #:
Predominant Soil Series: GoA
Crop 1 Max. PAN:
136 Crop 2 Name:
4
BF210
Acres Utilized:
Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
64.02
64.02
0
N
Q
Volume applied
enter one Solids/
( )
Liquid
Cu_ Yds Gallons
o
/o
Solids
Volume
Applied per
pp p
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(may'
Wet,
Moist)
precip.
Past 24
Ms.
inches
a
F ,'tea
c�
w
*o•
o
,•d
�,
#
w •,
* N
*�
TKN
mg/kg
Z
•;
o
M o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
10/22
71500
3.71
0.173
Washington
D
<.5"
S
0.5
0.3
51300
11050
145
6.132
NA
Rye
10/23
52000
3.71
0.126
Washington
D
<.5"
S
0.5
0.3
51300
11050
145
4.460
NA
Rye
10/24
32500
3.71
0.079
Washington
D
<.5"
S
0.5
0.3
51300
11050
145
2.787
NA
Rye
10/25
195000
3.71
0.471
Washington
D
<.5"
S
0.5
0.3
51300
11050
145
16.724
NA
Rye
10/26
1
234000
3.71
0.565
Washington
D
<.5"
S
0.5
0.3
51300
1 11050
145
20.069
NA
Rye
10/27
227500
3.71
0.550
Washington
D
<.5"
S
0.5
0.3
51300
11050
145
19.511
NA
Rye
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
1 0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
01
812500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
7-1-69-6821
0.000
Lime Applied
Annuallbs/acre
0.028
0.003
1.280
0.096
0.110
0.002
0.024
0.070
0.037
3.471
149.7771
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.263
0.07
8.958
1.173
1.049
0.047
0.227
0.706
0.231
23.247
Current Cumulative lbs/ac
0.291
1 0.073
10.238
1.269
1.159
0.049
0.251
0.776
0.268
26.718
Permitted C. P. L. R.****
1 36
1 34
1 1338
1
1 267
1 15
1
1 374
1 89
1 2498
Permit PAN Limit lst/2nd Crop
136
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/31/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Washington Total Dry Tons Applied (Annual): 42.01
Permit #: WQ0001026 Cation Exchange Capacity (non 503 only):
Operator: Hunter Roost Farms Owner: Hunter Roost Farms Predominant Soil Series: Ra
Acres Used: 15.92 Acres Permitted: 15.92 Site #: BF210 Field #: 5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
... 0107115
Com-
posite
Date
E
Molon
on
OEM
EMBEEM
MEMO
Total
Phos-
phorus
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total
11
2 1
3
4
5j
6j
7
8
9
10
11
12
DT/Ac./
App.
.fir
Event
2.64
Arsenic
0.065
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.065
Cadmium
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Copper
1.631
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.631
Chromium
0.139
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.139
Lead
0.145
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.145
Mercury
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Molyb-
0.037
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.037
denum
Nickel
0.080
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
1 0.000
0.080
Selenium
0.071
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.071
Zinc
4.054
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.054
Total
Phos-
184.466
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
184.466
horus
1
1
1
1
1
"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
1/31/2023
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Washington
Hunter Roost Farms
Operator: Hunter Roost Farms
Crop 1 Name: Soybeans
WQ Permit #: WQ0001026 Field #:
Annual Dry Tons Applied: 42.01 Site #:
Predominant Soil Series: Ra
Crop 1 Max. PAN:
170
Crop 2 Name:
Acres Utilized:
BF210 Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
15.92
15.92
0
N
Q
Volume applied
enter one Solids/
)
Liquid
Cu_ Yds Gallons
o
/o
Solids
Volume
Applied per
pp p
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
( y'
Wet,
Moist)
Precip.
Past 24
Ms.
inches
a
F ,'tea
c�
w
*o•
o
,•d
�,
#
4
w •,
* N
*�
TKN
mg/kg
Z
o
8
oa o
�•
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/13
273000
3.1
2.217
Washington
D
<.5"
S
0.5
1 0.3
59550
8110
320
87.814
NA
Beans
4/14
52000
3.1
0.422
Washington
D
<.5"
S
0.5
0.3
59550
8110
320
16.727
NA
Beans
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4-0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
01
325000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
104,54
00.000
Lime Applied
Annuallbs/acre
0.065
0.011
1.631
0.139
0.145
0.004
0.037
0.080
0.071
4.054
184.466
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.078
0.02
2.937
0.446
0.37
0.015
0.062
0.261
0.094
7.517
Current Cumulative lbs/ac
0.143
0.031
4.568
0.585
0.515
0.019
0.099
0.341
0.165
11.571
Permitted C. P. L. R.****1
36
1 34
1 1338
1
1 267
1 15
1
1 374
1 89
1 2498
Permit PAN Limit lst/2nd Crop
1 170
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/31/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Washington Total Dry Tons Applied (Annual): 64.69
Permit #: WQ0001026 Cation Exchange Capacity (non 503 only):
Operator: Hunter Roost Farms Owner: Hunter Roost Farms Predominant Soil Series: CrA
Acres Used: 25.44 Acres Permitted: 25.44 Site #: BF210 Field #: 16
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
... 0107115
Com-
posite
Date
E
Molon
on
OEM
EMBEEM
MEMO
Total
Phos-
phorus
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total
11
2 1
3
4
5j
6j
7
8
9
10
11
12
DT/Ac./
App.
.fir
Event
2.54
Arsenic
0.062
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.062
Cadmium
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Copper
1.572
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.572
Chromium
0.134
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.134
Lead
0.140
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.140
Mercury
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Molyb-
0.036
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.036
denum
Nickel
0.077
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
1 0.000
0.077
Selenium
0.068
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.068
Zinc
3.906
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.906
Total
Phos-
177.756
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
177.756
horus
1
1
1
1
1
"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
1/31/2023
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Washington
Hunter Roost Farms
Operator: Hunter Roost Farms
Crop 1 Name: Soybeans
WQ Permit #: WQ0001026 Field #:
Annual Dry Tons Applied: 64.69 Site #:
Predominant Soil Series: CrA
Crop 1 Max. PAN:
154 Crop 2 Name:
16
Acres Utilized:
BF210 Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
25.44
25.44
0
N
Q
Volume applied
enter one Solids/
)
Liquid
Cu_ Yds Gallons
o
/o
Solids
Volume
Applied per
pp p
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
( y'
Wet,
Moist)
Precip.
Past 24
Ms.
inches
a
F ,'tea
c�
w
*o•
o
,•d
�,
#
4
w •,
* N
*�
TKN
mg/kg
Z
8
o
oa o
�•
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/10
52000
3.1
0.264
Washington
D
<.5"
S
0.5
0.3
59550
8110
1 320
10.467
NA
Beans
4/11
227500
3.1
1.156
Washington
D
<.5"
S
0.5
0.3
59550
8110
320
45.794
NA
Beans
4/12
221000
3.1
1.123
Washington
D
<.5"
S
0.5
0.3
59550
8110
320
44.486
NA
Beans
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
01
500500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
100.7471
0.000
Lime Applied
Annuallbs/acre
0.062
0.011
1.572
0.134
0.140
0.004
0.036
0.077
0.068
3.906
177.756
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.176
0.032
6.86
0.752
0.708
0.04
0.13
0.428
0.182
16.729
Current Cumulative lbs/ac
0.238
0.043
8.432
0.886
0.848
0.044
0.166
0.505
0.250
20.635
Permitted C. P. L. R.****
36
34
1 1338
1
1 267
1 15
374
1 89
1 2498
Permit PAN Limit lst/2nd Crop
154
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/31/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Waypointo
ANALYTICAL
4/15/2022
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 22-097-0048
Client Project Description: Washington, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 4/7/2022 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 9

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2023
Arkansas
State Program
88-0650
02/07/2023
California
State Program
2904
06/30/2022
Florida
State Program
- NELAP
E871157
06/30/2022
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2022
Illinois
State Program
- NELAP
200078
10/10/2022
Kentucky
State Program
80215
06/30/2022
Kentucky
State Program
KY90047
12/31/2022
Louisiana
State Program
- NELAP
LA037
12/31/2022
Louisiana
State Program
- NELAP
04015
06/30/2022
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
415
12/31/2022
Pennsylvania
State Program
- NELAP
68-03195
05/31/2022
South Carolina
State Program
84002
06/30/2022
South Carolina
State Program
84002
06/30/2022
Tennessee
State Program
02027
02/11/2023
Texas
State Program
- NELAP
T104704180
09/30/2022
Virginia
State Program
00106
06/30/2022
Virginia
State Program
- NELAP
460181
09/14/2022
Page 1 of 1 00001/22-097-0048
Page 2 of 9

Waypoint
ANALYTICAL
Report Number: 22-097-0048
Client Project Description: Washington, NC
Lab No Client Sample ID
89660 Washington
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Matrix Date Collected Date Received
Solids 04/06/2022 06:00 04/07/2022
Page 3 of 9

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Washington, NC
Lab Report Number: 22-097-0048
Date: 4/15/2022
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 99495 (SS-1)
Analyte: Arsenic
QC Batch No: 1-610642/1-609727
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 99495 (SS-1)
Analyte: Calcium
QC Batch No: 1-610642/1-609727
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99495 (SS-1)
Analyte: Iron
QC Batch No: 1-610642/1-609727
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99495 (SS-1)
Analyte: Potassium
QC Batch No: 1-610642/1-609727
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99495 (SS-1)
Analyte: Magnesium
QC Batch No: 1-610642/1-609727
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99495 (SS-1)
Analyte: Manganese
QC Batch No: 1-610642/1-609727
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99495 (SS-1)
Analyte: Phosphorus
QC Batch No: 1-610642/1-609727
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99495 (SS-1)
Page 4 of 9

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 fax [phone]
www.waypointanalytical.com
Analyte: Lead
QC Batch No: 1-610642/1-609727
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 91031 (NE Cake)
Analyte: Mercury
QC Batch No: 1-611054/1-610645
The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control
acceptance ranges. Matrix interference is suspected
Page 5 of 9

Waypointo
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Washington, NC
Information :
Report Date : 04/15/2022
nReceived : 04/07/2022
C-�*�-� =
Connie Cook
Report Number : 22-097-0048
REPORT OFANALYSIS
Project
Manager
Lab No : 89660
Matrix:
Solids
Sample ID : Washington
Sampled:
4/6/2022
6:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
97.1
%
1
04/07/22 16:58
FMM
SW-DRYWT
Ammonia Nitrogen
7860
mg/Kg -
dry
552
3450
1
04/15/22 10:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
366
mg/Kg -
dry
172
172
1
04/14/22 15:36
ZBD
4500NO3F-2016
Organic N
60070
mg/Kg -
dry
551.7
3448
1
04/14/22 09:30
CALCULATION
pH
6.8
S.U.
1
04/14/2216:03
DRS
9045D
Total Solids
2.87
%
0.010
0.010
1
04/07/22 16:58
FMM
2540G-2011
Total Volatile Solids
64.9
%
0.010
0.010
1
04/07/22 16:58
FMM
2540G-2011
Total Kjeldahl Nitrogen
67900
mg/Kg -
dry
345
8620
1
04/14/22 09:30
JPJ ;M-4500-NH3C-TKI`
Phosphorus
33500
mg/Kg -
dry
95.2
172
1
04/12/22 23:47
TJS
6010D
Aluminum
39700
mg/Kg -
dry
159
172
1
04/13/22 13:55
TJS
6010D
Arsenic
<17.2
mg/Kg -
dry
8.28
17.2
1
04/12/22 23:47
TJS
6010D
Cadmium
<3.45
mg/Kg -
dry
0.690
3.45
1
04/12/22 23:47
TJS
6010D
Calcium
21800
mg/Kg -
dry
1330
1720
1
04/12/22 23:47
TJS
6010D
Chromium
29.8
mg/Kg -
dry
8.14
8.62
1
04/12/22 23:47
TJS
6010D
Copper
272
mg/Kg -
dry
10.7
17.2
1
04/12/22 23:47
TJS
6010D
Iron
16600
mg/Kg -
dry
294
345
1
04/12/22 23:47
TJS
6010D
Lead
23.3
mg/Kg -
dry
6.21
10.3
1
04/12/22 23:47
TJS
6010D
Magnesium
3190
mg/Kg -
dry
89.0
172
1
04/12/22 23:47
TJS
6010D
Manganese
514
mg/Kg -
dry
11.2
17.2
1
04/12/22 23:47
TJS
6010D
Mercury
0.572
mg/Kg -
dry
0.216
0.497
1
04/14/22 15:13
ZMT
7471A
Molybdenum
<8.62
mg/Kg -
dry
4.66
8.62
1
04/12/22 23:47
TJS
6010D
Nickel
14.0
mg/Kg -
dry
4.14
8.62
1
04/12/22 23:47
TJS
6010D
Potassium
3690
mg/Kg -
dry
213
345
1
04/12/22 23:47
TJS
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 6 of 9

•
Waypoint
27090 Whitten
Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
ANALYTICAL
www.waypointanalyiical.com
46245
EMA Resources Inc
Project
Washington,
NC
Mr. Brent Collins
Report Date : 04/15/2022
755 Yadkinville Rd
Information :
Received : 04/07/2022
Mocksville , NC 27028
Connie Cook
Report Number : 22-097-0048
REPORT OFANALYSIS
Project Manager
Lab No : 89660
Matrix: Solids
Sample ID : Washington
Sampled: 4/6/2022 6:00
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Selenium
<17.2
mg/Kg - dry
11.0
17.2 1 04/12/22 23:47 TJS 6010D
Sodium
4100
mg/Kg - dry
448
862 1 04/12/22 23:47 TJS 6010D
Zinc
683
mg/Kg - dry
27.9
43.1 1 04/12/22 23:47 TJS 6010D
Sulfur
11300
mg/Kg - dry
179
345 1 04/13/22 13:55 TJS 6010D
Sodium Absorption Ratio
1.16
Ratio
0.01
0.01 1 04/12/22 23:47 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 7 of 9

s
WayPAoi nt ..(2) �79p Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 901.213.240fl °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 22-097-0048
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
IT102
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IMakayla Weaver Date & Time: 04/07/2022 10:52:39
Page 8 of 9

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4/6/2022
mg/kg
mg/L
Equiv Weight Milli Equiv
Sodium
4100
117.67
23 5.116087
Calcium
21800
625.66
20 31.283
Magnesium
3190
91.553
12 7.629417
Percent Solids
2.87
SAR
1.16
SAR =
Na+
a (Ca2+ + M;42+ )
5.11609
0.5( 31.283 2 + 7.62942 2 )

Waypointo
ANALYTICAL
5/4/2022
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 22-111-0009
Client Project Description: Washington, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 4/21/2022 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 9

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2023
Arkansas
State Program
88-0650
02/07/2023
California
State Program
2904
06/30/2022
Florida
State Program
- NELAP
E871157
06/30/2022
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2022
Illinois
State Program
- NELAP
200078
10/10/2022
Kentucky
State Program
80215
06/30/2022
Kentucky
State Program
KY90047
12/31/2022
Louisiana
State Program
- NELAP
LA037
12/31/2022
Louisiana
State Program
- NELAP
04015
06/30/2022
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
415
12/31/2022
Pennsylvania
State Program
- NELAP
68-03195
05/31/2022
South Carolina
State Program
84002
06/30/2022
South Carolina
State Program
84002
06/30/2022
Tennessee
State Program
02027
02/11/2023
Texas
State Program
- NELAP
T104704180
09/30/2022
Virginia
State Program
00106
06/30/2022
Virginia
State Program
- NELAP
460181
09/14/2022
Page 1 of 1 00001/22-111-0009
Page 2 of 9

Waypoint
ANALYTICAL
Report Number: 22-111-0009
Client Project Description: Washington, NC
Lab No Client Sample ID
95442 Washington
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Matrix Date Collected Date Received
Solids 04/20/2022 06:30 04/21/2022
Page 3 of 9

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Washington, NC
Lab Report Number: 22-111-0009
Date: 5/4/2022
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 95889
Analyte: Aluminum
QC Batch No: 1-613308/1-612535
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 95889
Analyte: Arsenic
QC Batch No: 1-613308/1-612535
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 95889
Analyte: Iron
QC Batch No: 1-613308/1-612535
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 95889
Analyte: Potassium
QC Batch No: 1-613308/1-612535
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Sample 95889
Analyte: Manganese
QC Batch No: 1-613308/1-612535
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 95889
Analyte: Molybdenum
QC Batch No: 1-613308/1-612535
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 95889
Analyte: Lead
QC Batch No: 1-613308/1-612535
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 95889
Page 4 of 9

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 fax [phone]
www.waypointanalytical.com
Analyte: Selenium
QC Batch No: 1-613308/1-612535
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 95943 (Little Patuxent Class A)
Analyte: Mercury
QC Batch No: 1-613427/1-612896
The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control
acceptance ranges. Matrix interference is suspected
Page 5 of 9

Waypointo
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Washington, NC
Information :
Report Date : 05/04/2022
nReceived : 04/21/2022
C-�*�-� =
Connie Cook
Report Number : 22-111-0009
REPORT OFANALYSIS
Project
Manager
Lab No : 95442
Matrix:
Solids
Sample ID : Washington
Sampled:
4/20/2022
6:30
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
96.7
%
1
04/25/22 17:36
FMM
SW-DRYWT
Ammonia Nitrogen
8360
mg/Kg -
dry
485
3030
1
05/04/22 10:45
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
273
mg/Kg -
dry
142
142
1
04/25/22 14:38
ZBD
4500NO3F-2016
Organic N
42850
mg/Kg -
dry
484.8
3030
1
05/01/22 13:00
CALCULATION
pH
6.7
S.U.
1
04/28/2215:20
DRS
9045D
Total Solids
3.32
%
0.010
0.010
1
04/25/22 17:36
FMM
2540G-2011
Total Volatile Solids
63.8
%
0.010
0.010
1
04/25/22 17:36
FMM
2540G-2011
Total Kjeldahl Nitrogen
51200
mg/Kg -
dry
303
7580
1
05/01/22 13:00
JPJ ;M-4500-NH3C-TKI`
Phosphorus
36400
mg/Kg -
dry
83.6
152
1
04/27/22 02:36
JTR
6010D
Aluminum
38500
mg/Kg -
dry
140
152
1
04/27/22 02:36
JTR
6010D
Arsenic
<7.27
mg/Kg -
dry
7.27
15.2
1
04/27/22 18:54
JTR
6010D
Cadmium
0.7063
mg/Kg -
dry
0.606
3.03
1
04/27/22 02:36
JTR
6010D
Calcium
34200
mg/Kg -
dry
1170
1520
1
04/27/22 02:36
JTR
6010D
Chromium
23.0
mg/Kg -
dry
7.15
7.58
1
04/27/22 02:36
JTR
6010D
Copper
345
mg/Kg -
dry
9.39
15.2
1
04/27/22 02:36
JTR
6010D
Iron
19700
mg/Kg -
dry
258
303
1
04/27/22 02:36
JTR
6010D
Lead
31.8
mg/Kg -
dry
5.45
9.09
1
04/27/22 02:36
JTR
6010D
Magnesium
3580
mg/Kg -
dry
78.2
152
1
04/27/22 02:36
JTR
6010D
Manganese
542
mg/Kg -
dry
9.85
15.2
1
04/27/22 02:36
JTR
6010D
Mercury
0.8643
mg/Kg -
dry
0.189
4.33
1
04/27/22 13:55
JTR
7471A
Molybdenum
5.483
mg/Kg -
dry
4.09
7.58
1
04/27/22 02:36
JTR
6010D
Nickel
16.4
mg/Kg -
dry
3.64
7.58
1
04/27/22 02:36
JTR
6010D
Potassium
3390
mg/Kg -
dry
187
303
1
04/27/22 02:36
JTR
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 6 of 9

•
Waypoint
27090 Whitten
Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
ANALYTICAL
www.waypointanalyiical.com
46245
EMA Resources Inc
Project
Washington,
NC
Mr. Brent Collins
Report Date : 05/04/2022
755 Yadkinville Rd
Information :
Received : 04/21/2022
Mocksville , NC 27028
Connie Cook
Report Number : 22-111-0009
REPORT OFANALYSIS
Project Manager
Lab No : 95442
Matrix: Solids
Sample ID : Washington
Sampled: 4/20/2022 6:30
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Selenium
<9.70
mg/Kg - dry
9.70
15.2 1 04/27/22 18:54 JTR 6010D
Sodium
3360
mg/Kg - dry
394
758 1 04/27/22 02:36 JTR 6010D
Zinc
852
mg/Kg - dry
24.5
37.9 1 04/27/22 02:36 JTR 6010D
Sulfur
12000
mg/Kg - dry
157
303 1 04/27/22 02:36 JTR 6010D
Sodium Absorption Ratio
0.83
Ratio
0.01
0.01 1 04/27/22 02:36 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 7 of 9

s
WayPAoi nt ..(2) �79p Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 901.213.240fl °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 22-111-0009
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
IT102
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IMakayla Weaver Date & Time: 04/21/2022 10:01:27
Page 8 of 9

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Page 9 of 9

4/20/2022
mg/kg mg/L Equiv Weight Milli Equiv
Sodium 3360 111.552 23 4.850087
Calcium 34200 1135.44 20 56.772
Magnesium 3580 118.856 12 9.904667
Percent Solids 3.32
SAR 0.84
SAR — Na
2 (Ca2+ + Mg2- )
4.85009
0.5( 56.772 2 + 9.90467 2 )

Waypointo
ANALYTICAL
10/31 /2022
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 22-294-0040
Client Project Description: Washington, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 10/21/2022 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2023
Arkansas
State Program
88-0650
02/07/2023
California
State Program
2904
06/30/2023
Florida
State Program
- NELAP
E871157
06/30/2023
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2023
Illinois
State Program
- NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2022
Louisiana
State Program
- NELAP
LA037
12/31/2022
Louisiana
State Program
- NELAP
04015
06/30/2023
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2022
Pennsylvania
State Program
- NELAP
68-03195
05/31/2023
South Carolina
State Program
84002
06/30/2022
Tennessee
State Program
02027
02/11/2023
Texas
State Program
- NELAP
T104704180
09/30/2022
Virginia
State Program
00106
06/30/2023
Virginia
State Program
- NELAP
460181
09/14/2023
Page 1 of 1 00001/22-294-0040
Page 2 of 8

Waypoint
ANALYTICAL
Report Number: 22-294-0040
Client Project Description: Washington, NC
Lab No Client Sample ID
81014 Washington
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Matrix Date Collected Date Received
Solids 10/19/2022 11:30 10/21/2022
Page 3 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Washington, NC
Lab Report Number: 22-294-0040
Date: 10/28/2022
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 82664 (SB-4)
Analyte: Aluminum
QC Batch No: 1-645566/1-645192
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 82664 (SB-4)
Analyte: Iron
QC Batch No: 1-645824/1-645192
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 82664 (SB-4)
Analyte: Potassium
QC Batch No: 1-645566/1-645192
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 82664 (SB-4)
Analyte: Manganese
QC Batch No: 1-645824/1-645192
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 82664 (SB-4)
Analyte: Selenium
QC Batch No: 1-645824/1-645192
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 4 of 8

Waypointo
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Washington, NC
Information :
Report Date : 10/31/2022
Received : 10/21/2022
" l.�—
Connie Cook
Report Number : 22-294-0040
REPORT OFANALYSIS
Project
Manager
Lab No : 81014
Matrix:
Solids
Sample ID : Washington
Sampled:
10/19/2022
11:30
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
96.3
%
1
10/24/22 17:20
FMM
SW-DRYWT
Ammonia Nitrogen
12000
mg/Kg -
dry
432
2700
1
10/27/22 15:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
147
mg/Kg -
dry
132
132
1
10/25/22 14:32
ZBD
4500NO3F-2016
Organic N
35570
mg/Kg -
dry
432.4
2703
1
10/27/22 10:30
DH
CALCULATION
pH
7.0
S.U.
1
10/28/2214:02
SAR
9045D
Total Solids
3.72
%
0.010
0.010
1
10/24/22 17:20
FMM
2540G-2011
Total Volatile Solids
58.8
%
0.010
0.010
1
10/24/22 17:20
FMM
2540G-2011
Total Kjeldahl Nitrogen
47600
mg/Kg -
dry
270
6760
1
10/27/22 10:30
JPJ ;M-4500-NH3C-TKI`
Phosphorus
38100
mg/Kg -
dry
74.6
135
1
10/26/22 18:49
EAL
6010D
Aluminum
40300
mg/Kg -
dry
125
135
1
10/26/22 18:49
6010D
Arsenic
6.703
mg/Kg -
dry
6.49
13.5
1
10/26/22 18:49
EAL
6010D
Cadmium
0.6113
mg/Kg -
dry
0.541
2.70
1
10/26/22 18:49
EAL
6010D
Calcium
27600
mg/Kg -
dry
1050
1350
1
10/26/22 18:49
EAL
6010D
Chromium
22.7
mg/Kg -
dry
6.38
6.76
1
10/26/22 18:49
EAL
6010D
Copper
308
mg/Kg -
dry
8.38
13.5
1
10/26/22 18:49
EAL
6010D
Iron
18100
mg/Kg -
dry
230
270
1
10/26/22 18:49
EAL
6010D
Lead
26.1
mg/Kg -
dry
4.86
8.11
1
10/26/22 18:49
EAL
6010D
Magnesium
3110
mg/Kg -
dry
69.7
135
1
10/26/22 18:49
EAL
6010D
Manganese
673
mg/Kg -
dry
8.78
13.5
1
10/26/22 18:49
EAL
6010D
Mercury
0.8683
mg/Kg -
dry
0.180
4.14
1
10/26/22 11:44
TJS
7471A
Molybdenum
6.223
mg/Kg -
dry
3.65
6.76
1
10/26/22 18:49
EAL
6010D
Nickel
17.6
mg/Kg -
dry
3.24
6.76
1
10/26/22 18:49
EAL
6010D
Potassium
2660
mg/Kg -
dry
167
270
1
10/26/22 18:49
EAL
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 5 of 8

•
Waypoint
27090 Whitten
Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
ANALYTICAL
www.waypointanalyiical.com
46245
EMA Resources Inc
Project
Washington,
NC
Mr. Brent Collins
Report Date : 10/31/2022
755 Yadkinville Rd
Information :
Received : 10/21/2022
Mocksville , NC 27028
n
Connie Cook
Report Number : 22-294-0040
REPORT OFANALYSIS
Project Manager
Lab No : 81014
Matrix: Solids
Sample ID : Washington
Sampled: 10/19/2022 11:30
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Selenium
9.413
mg/Kg - dry
8.65
13.5 1 10/26/22 18:49 EAL 6010D
Sodium
3490
mg/Kg - dry
351
676 1 10/26/22 18:49 EAL 6010D
Zinc
827
mg/Kg - dry
21.9
33.8 1 10/26/22 18:49 EAL 6010D
Sulfur
11400
mg/Kg - dry
140
270 1 10/26/22 18:49 EAL 6010D
Sodium Absorption Ratio
1.02
Ratio
0.01
0.01 1 10/26/22 18:49 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 6 of 8

s
WayPAoi nt ..(2) �79p Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 901.213.240fl °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 22-294-0040
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
IT136
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IMallory Earle Date & Time: 10/21/2022 10:23:30
Page 7 of 8

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Page 8 of 8

10/19/2022
mg/kg
mg/L
Equiv Weight Milli Equiv
Sodium
3490
129.828
23 5.644696
Calcium
27600
1026.72
20 51.336
Magnesium
3110
115.692
12 9.641
Percent Solids
3.72
SAR
1.02
SAR =
Na+
a (Ca2+ + M;42+ )
5.64470
0.5( 51.336 2 + 9.64100 2 )

Waypointo
ANALYTICAL
11 /7/2022
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 22-301-0014
Client Project Description: Washington, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 10/28/2022 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2023
Arkansas
State Program
88-0650
02/07/2023
California
State Program
2904
06/30/2023
Florida
State Program
- NELAP
E871157
06/30/2023
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2023
Illinois
State Program
- NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2022
Louisiana
State Program
- NELAP
LA037
12/31/2022
Louisiana
State Program
- NELAP
04015
06/30/2023
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2022
Pennsylvania
State Program
- NELAP
68-03195
05/31/2023
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
02/11/2023
Texas
State Program
- NELAP
T104704180
09/30/2022
Virginia
State Program
00106
06/30/2023
Virginia
State Program
- NELAP
460181
09/14/2023
Page 1 of 1 00001/22-301-0014
Page 2 of 8

Waypoint
ANALYTICAL
Report Number: 22-301-0014
Client Project Description: Washington, NC
Lab No Client Sample ID
84162 Washington
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Matrix Date Collected Date Received
Solids 10/27/2022 09:00 10/28/2022
Page 3 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Washington, NC
Lab Report Number: 22-301-0014
Date: 11 /7/2022
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 84143 (JK-2-1)
Analyte: Aluminum
QC Batch No: 1-647142/1-646104
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 84143 (JK-2-1)
Analyte: Iron
QC Batch No: 1-647142/1-646104
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 84143 (JK-2-1)
Analyte: Potassium
QC Batch No: 1-647142/1-646104
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 84143 (JK-2-1)
Analyte: Molybdenum
QC Batch No: 1-646946/1-646104
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 4 of 8

Waypointo
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Road
Mocksville , NC 27028
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Washington, NC
Information :
Report Date : 11/07/2022
nReceived : 10/28/2022
C-�*�-� =
Connie Cook
Report Number : 22-301-0014
REPORT OFANALYSIS
Project
Manager
Lab No : 84162
Matrix:
Solids
Sample ID : Washington
Sampled:
10/27/2022
9:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
96.6
%
1
10/28/22 16:09
FMM
SW-DRYWT
Ammonia Nitrogen
10100
mg/Kg -
dry
471
2940
1
11/04/22 16:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<143
mg/Kg -
dry
143
143
1
11/02/22 14:07
ZBD
4500NO3F-2016
Organic N
44910
mg/Kg -
dry
470.6
2941
1
11/04/22 12:45
CALCULATION
pH
7.0
S.U.
1
11/04/2216:20
DRS
9045D
Total Solids
3.70
%
0.010
0.010
1
10/28/22 16:09
FMM
2540G-2011
Total Volatile Solids
58.6
%
0.010
0.010
1
10/28/22 16:09
FMM
2540G-2011
Total Kjeldahl Nitrogen
55000
mg/Kg -
dry
294
7350
1
11/04/22 12:45
JPJ ;M-4500-NH3C-TKI`
Phosphorus
38200
mg/Kg -
dry
81.2
147
1
11/02/22 01:15
JTR
6010D
Aluminum
44100
mg/Kg -
dry
136
147
1
11/04/22 20:45
EAL
6010D
Arsenic
7.383
mg/Kg -
dry
7.06
14.7
1
11/04/22 20:45
EAL
6010D
Cadmium
0.8063
mg/Kg -
dry
0.588
2.94
1
11/02/22 01:15
JTR
6010D
Calcium
30300
mg/Kg -
dry
1140
1470
1
11/02/22 01:15
JTR
6010D
Chromium
26.2
mg/Kg -
dry
6.94
7.35
1
11/02/22 01:15
JTR
6010D
Copper
344
mg/Kg -
dry
9.12
14.7
1
11/04/22 20:45
EAL
6010D
Iron
19600
mg/Kg -
dry
251
294
1
11/02/22 01:15
JTR
6010D
Lead
30.0
mg/Kg -
dry
5.29
8.82
1
11/02/22 01:15
JTR
6010D
Magnesium
3470
mg/Kg -
dry
75.9
147
1
11/04/22 20:45
EAL
6010D
Manganese
765
mg/Kg -
dry
9.56
14.7
1
11/02/22 01:15
JTR
6010D
Mercury
0.2833
mg/Kg -
dry
0.181
4.15
1
11/01/22 15:03
JTR
7471A
Molybdenum
5.913
mg/Kg -
dry
3.97
7.35
1
11/02/22 01:15
JTR
6010D
Nickel
18.0
mg/Kg -
dry
3.53
7.35
1
11/02/22 01:15
JTR
6010D
Potassium
2860
mg/Kg -
dry
182
294
1
11/04/22 20:45
EAL
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 5 of 8

•
Waypoint
27090 Whitten
Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
ANALYTICAL
www.waypointanalyiical.com
46245
EMA Resources Inc
Project
Washington,
NC
Mr. Brent Collins
Report Date : 11/07/2022
755 Yadkinville Road
Information :
Received : 10/28/2022
Mocksville , NC 27028
Connie Cook
Report Number : 22-301-0014
REPORT OFANALYSIS
Project Manager
Lab No : 84162
Matrix: Solids
Sample ID : Washington
Sampled: 10/27/2022 9:00
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Selenium
<9.41
mg/Kg - dry
9.41
14.7 1 11/04/22 20:45 EAL 6010D
Sodium
4000
mg/Kg - dry
382
735 1 11/04/22 20:45 EAL 6010D
Zinc
941
mg/Kg - dry
23.8
36.8 1 11/02/22 01:15 JTR 6010D
Sulfur
12100
mg/Kg - dry
152
294 1 11/02/22 01:15 JTR 6010D
Sodium Absorption Ratio
1.06
Ratio
0.01
0.01 1 11/02/22 01:15 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 6 of 8

s
WayPAoi nt ..(2) �79p Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 901.213.240fl °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 22-301-0014
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
IT135
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: lEmily M. Peterson Date & Time: 10/28/2022 09:31:30
Page 7 of 8

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Page 8 of 8

10/27/2022
mg/kg mg/L Equiv Weight Milli Equiv
Sodium 4000 148 23 6.434783
Calcium 30300 1121.1 20 56.055
Magnesium 3470 128.39 12 10.69917
Percent Solids 3.7
SAR 1.11
SAR — Na
2 (Ca2+ + Mg2- )
6.43478
0.5( 56.055 2 + 10.69917 2 )

13
ace Analytical ' ANALYTICAL REPORT
April 26, 2022
EMA Resources
Sample Delivery Group: L147982O
Samples Received: 04/07/2022
Project Number:
Description: Sludge
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By: z � ��
Cassandra Foster
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy ofthe information provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1479320 04/26/22 07:10 1 of 20

TABLE OF CONTENTS
Cp: Cover Page
u
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
Fss]
WASHINGTON L1479820-01
5
Fn
Qc: Quality Control Summary
7
Wet Chemistry by Method 9012 B
7
Fr
Wet Chemistry by Method 9034-9030B
8
Wet Chemistry by Method 9045D
9
Rc
Wet Chemistry by Method D93/1010A
10
F
Mercury by Method 7470A
11
Metals (ICP) by Method 6010D
12
[Al
Volatile Organic Compounds (GC/MS) by Method 8260D
13
Chlorinated Acid Herbicides (GC) by Method 8151A
14
RC
Pesticides (GC) by Method 8081B
15
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
16
GI: Glossary of Terms
18
al: Accreditations & Locations
19
Sc: Sample Chain of Custody
20
ACCOUNT: PROJECT: SDG:
DATE/TIME:
PAGE:
EMA Resources L1479320
04/26/22 07:10
2 of 20

WASHINGTON L1479820-01 Waste
Method
Preparation by Method 1311
Preparation by Method 1311
Wet Chemistry by Method 9012 B
Wet Chemistry by Method 9034-9030B
Wet Chemistry by Method 9045D
Wet Chemistry by Method D93/1010A
Mercury by Method 7470A
Metals (ICP) by Method 6010D
Volatile Organic Compounds (GC/MS) by Method 8260D
Chlorinated Acid Herbicides (GC) by Method 8151A
Pesticides (GC) by Method 8081B
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
SAMPLE SUMMARY
Collected by
Brent Collins
Batch
WG1849584
WG1849631
WG1845372
WG1846335
WG1845900
WG1847388
WG1852287
WG1852357
WG1851052
WG1851431
WG1852709
WG1852705
Dilution Preparation
date/time
1 04/20/22 07:52
1 04/17/22 1114
1 04/12/22 0107
1 04/11/22 08:00
1 04/09/2210:00
1 04/13/22 04:23
1 04/21/2213:20
1 04/21/2214:47
2 04/19/22 22:40
1 04/22/22 08:30
1 04/22/2217:27
1 04/22/2217:47
Collected date/time Received date/time
04/06/22 09:00 04/07/22 09:00 C
P
Analysis
date/time
04/20/22 07:52
04/17/221114
04/12/2212:12
04/11/2217:00
04/11/2212:03
04/13/22 04:23
04/23/2216:04
04/22/22 09:41
04/19/22 22:40
04/25/2218:15
04/23/22 00:53
04/23/2212:35
Analyst
JAV
JAV
LDT
VRP
PSN
WOS
ABL
CCE
BMB
JMB
HLJ
AGW
Location
FC
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fn
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fr
Mt. Juliet, TN
Mt. Juliet, TN
Rc
Mt. Juliet, TN
Mt. Juliet, TN
GI
SAI
RC
ACCOUNT: PROJECT: SDG:
EMA Resources L1479320
DATE/TIME: PAGE:
04/26/22 07:10 3 of 20

CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the FP
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data. 0
Fr
FQ-cl
GI
Cassandra Foster
Project Manager
RC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012 B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034-903013.
Pyridine is reporting with critically low recovery in the laboratory control sample(s). This compound is a method defined poor
performer. Results are estimated.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1479320 04/26/22 07:10 4 of 20

SAMPLE RESULTS - 01
L1479820
WASHINGTON
Collected date/time: 04/06/22 09:00
Preparation by Method 1311
Result Qualifier Prep
Batch
Analyte
date / time
TCLP Extraction
4/20/2022 7:52:34 AM
WG1849584
TCLP ZHE Extraction
- 4/17/20221114:41 AM
WG1849631
Fluid
1 4/20/2022 7:52:34 AM
WG1849584
Initial pH
7.21 4/20/2022 7:52:34 AM
WG1849584
Final pH
4.83 4/20/2022 7:52:34 AM
WG1849584
Wet Chemistry by Method 9012 B
Result Qualifier RDL
Analyte mg/kg mg/kg
Reactive Cyanide ND 0.250
Wet Chemistry by Method 9034-9030B
Result Qualifier RDL
Analyte mg/kg mg/kg
Reactive Sulfide ND 75.0
Wet Chemistry by Method 9045D
Dilution Analysis Batch
date / time
1 04/12/202212:12 WG1845372
Dilution Analysis Batch
date / time
1 04/11/202217:00 WG1846335
Result Qualifier Dilution Analysis Batch
Analyte su date / time
Corrosivity by pH 7.41 T8 1 04/11/202212:03 WG1845900
Sample Narrative:
L1479820-01 WG1845900: 7.41 at24.3C
Wet Chemistry by Method D93/1010A
Result
Analyte Deg. F
Ignitability DNI at170
Mercury by Method 7470A
Qualifier Dilution Analysis Batch
date / time
1 04/13/2022 04:23 WG1847388
Result Qualifier RDL Limit
Analyte mg/I mg/I mg/I
Mercury ND 0.0100 0.20
Metals (ICP) by Method 6010D
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Arsenic
ND
0.100
5
Barium
ND
0.100
100
Cadmium
ND
0.100
1
Chromium
0.187
0.100
5
Lead
ND
0.100
5
Selenium
ND
0.100
1
Silver
ND
0.100
5
Volatile Organic
Compounds (GC/MS) by Method
8260D
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Benzene
ND
0.100
0.50
Carbon tetrachloride
ND
0.100
0.50
Chlorobenzene
ND
0.100
100
Chloroform
ND
0.500
6
ACCOUNT:
PROJECT:
EMA Resources
Dilution Analysis Batch
date / time
1 04/23/202216:04 WG1852287
Dilution Analysis
Batch
date / time
1 04/22/2022 0941
WG1852357
1 04/22/2022 0941
WG1852357
1 04/22/2022 0941
WG1852357
1 04/22/2022 0941
WG1852357
1 04/22/2022 0941
WG1852357
1 04/22/2022 0941
WG1852357
1 04/22/2022 0941
WG1852357
Dilution
Analysis
Batch
date / time
2
04/19/2022 22:40
WG1851052
2
04/19/2022 22:40
WG1851052
2
04/19/2022 22:40
WG1851052
2
04/19/2022 22:40
WG1851052
SDG:
DATE/TIME: PAGE:
L1479320
04/26/22 07:10 5 of 20

WASHINGTON
SAMPLE RESULTS
- 01
Collected date/time: 04/06/22 09:00
L1479820
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
F
Analyte
mg/I
mg/I
mg/I
date/time
1,2-Dichloroethane
ND
0.100
0.50
2
04/19/2022 22:40
WG1851052
Fc
1,1-Dichloroethene
ND
0.100
0.70
2
04/19/2022 22:40
WG1851052
2-Butanone (MEK)
ND
1.00
200
2
04/19/2022 22:40
WG1851052
Tetrachloroethene
ND
0.100
0.70
2
04/19/2022 22:40
WG1851052
SS
F
Trichloroethene
ND
0.100
0.50
2
04/19/2022 22:40
WG1851052
Vinyl chloride
ND
J4 0.100
0.20
2
04/19/2022 22:40
WG1851052
Fn
(S) Toluene-dH
112
80.0-120
041191202222.40
WG1851052
(S) 4-Bromofluorobenzene
92.4
77.0-126
0411912022 22.40
WG1851052
(S) 1,2-Dichloroethane-d4
103
70.0-130
041191202222.40
WG1851052
Sample Narrative:
Rc
L1479820-01 WG1851052: Non -target
compounds too high
to run at a lower dilution.
Chlorinated Acid Herbicides (GC) by Method 8151A
,
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
e
AI
2,4,5-TP (Silvex)
ND
0.00200
1
1
04/25/202218:15
WG1851431
2,4-D
ND
0.00200
10
1
04/25/202218:15
WG1851431
F
(S)2,4-DichlorophenylAcetic Acid
65.0
14.0-158
041251202218.15
WG1851431
Pesticides (GC) by Method 8081B
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
Chlordane
ND
0.00500
0.03
1
04/23/2022 0053
WG1852709
Endrin
ND
0.00500
0.02
1
04/23/2022 0053
WG1852709
Heptachlor
ND
0.00500
0.0080
1
04/23/2022 0053
WG1852709
Heptachlor epoxide
ND
0.00500
0.0080
1
04/23/2022 0053
WG1852709
Lindane
ND
0.00500
0.40
1
04/23/2022 0053
WG1852709
Methoxychlor
ND
0.00500
10
1
04/23/2022 0053
WG1852709
Toxaphene
ND
0.0100
0.50
1
04/23/2022 0053
WG1852709
(S) Decochlorobiphenyl
96.2
10.0-128
0412312022 00.53
WG1852709
(S) Tetrochloro-m-xylene
76.0
10.0-127
0412312022 00.53
WG1852709
Semi Volatile Organic Compounds
(GC/MS) by Method
8270E
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
1,4-Dichlorobenzene
ND
0.100
7.50
1
04/23/202212:35
WG1852705
2,4-Dinitrotoluene
ND
0.100
0.13
1
04/23/202212:35
WG1852705
Hexachlorobenzene
ND
0.100
0.13
1
04/23/202212:35
WG1852705
Hexachloro-1,3-butadiene
ND
0.100
0.50
1
04/23/202212:35
WG1852705
Hexachloroethane
ND
0.100
3
1
04/23/202212:35
WG1852705
Nitrobenzene
ND
0.100
2
1
04/23/202212:35
WG1852705
Pyridine
ND
J4 0.100
5
1
04/23/202212:35
WG1852705
3&4-Methyl Phenol
ND
0.100
400
1
04/23/2022 12:35
WG1852705
2-Methylphenol
ND
0.100
200
1
04/23/202212:35
WG1852705
Pentachlorophenol
ND
0.100
100
1
04/23/202212:35
WG1852705
2,4,5-Trichlorophenol
ND
0.100
400
1
04/23/202212:35
WG1852705
2,4,6-Trichlorophenol
ND
0.100
2
1
04/23/202212:35
WG1852705
(S) 2-Fluorophenol
35.1
10.0-120
0412312022 12.35
WG1852705
(S) Phenol-d5
21.5
10.0-120
0412312022 12.35
WG1852705
(S) Nitrobenzene-d5
60.3
10.0-127
0412312022 12.35
WG1852705
(S) 2-Fluorobiphenyl
64.9
10.0-130
0412312022 12.35
WG1852705
(S)2,4,6-Tribromophenol
80.5
10.0-155
041231202212.35
WG1852705
(S) p-Terphenyl-d14
68.9
10.0-128
0412312022 12.35
WG1852705
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
L1479320
04/26/22 07:10
6 of 20

WG1845372
Wet Chemistry by Method 9012 B
Method Blank (MB)
(MB) R3730122-1 04/12/22 1158
MB Result
Analyte mg/kg
Reactive Cyanide U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
0.0390 0.250
L1479671-16 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1479820-01
(OS) L1479671-16 04/12/22 12:04 • (DUP) R3730122-3 04/12/22 12:05
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %_
Reactive Cyanide 0.322 0.323 1 0.517 20
L1480170-05 Original Sample (OS) • Duplicate (DUP)
(OS) L1430170-05 04/12/22 12:25 • (DUP) R3730122-6 04/12/22 12:26
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg
Reactive Cyanide ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3780122-2 04/12/22 1159
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Reactive Cyanide 2.50 2.45 98.0
Rec. Limits LCS Qualifier
85.0-115
L1479671-16 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1479671-16 04/12/22 12:04 • (MS) R3730122-4 04/12/22 12:06 • (MSD) R3730122-5 04/12/22 12:07
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 1.67 0.322 0.581 0.950 15.6 37.7 1 75.0-125 J6 J3 J6 48.2 20
L1480170-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1430170-05 04/12/22 12:25 • (MS) R3730122-7 04/12/22 12:27 • (MSD) R3730122-8 04/12/22 12:28
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 1.67 ND 1.41 1.53 84.5 91.5 1 75.0-125 8.03 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1479320 04/26/22 07:10 7 of 20

WG1846335
Wet Chemistry by Method 9034-9030B
Method Blank (MB)
(MB) R3780511-1 04/11/22 1700
MB Result MB Qualifier MB MDL
Analyte mg/kg mg/kg
Reactive Sulfide U 30.0
Laboratory Control Sample (LCS)
(LCS) R3780511-2 04/11/22 17:00
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Reactive Sulfide 100 86.8 86.8
QUALITY CONTROL SUMMARY
L1479820-01
MB RDL
mg/kg
75.0
Rec. Limits LCS Qualifier
53.8-124
L1480091-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1430091-04 04/11/22 17:00 • (MS) R3730511-3 04/11/22 17:00 • (MSD) R3730511-4 04/11/22 17:00
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Sulfide 100 ND ND ND 32.8 31.0 1 10.0-136 0.000 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1479320 04/26/22 07:10 3 of 20

WG1845900 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9045D L1479820-01
L1480378-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1430373-02 04/11/22 12:03 • (DUP) R3779677-3 04/11/22 12:03
Original Result DUP Result Dilution DUP RPD
Analyte su su
Corrosivity by pH 8.16 8.16 1 0.000
Sample Narrative:
OS: 8.16 at 23.6C
DUP: 8.16 at23.4C
Laboratory Control Sample (LCS)
DUP Qualifier DUP RPD
Limits
(LCS) R3779677-1 04/11/22 12:03
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte su su
Corrosivity by pH 10.0 9.95 99.5 99.0-101
Sample Narrative:
LCS: 9.95 at 23.2C
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1479320 04/26/22 07:10 9 of 20

WG1847388 QUALITY CONTROL SUMMARY
Wet Chemistry by Method D93/1010A L1479820-01
L1478062-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1473062-02 04/13/22 04:23 • (DUP) R3730327-3 04/13/22 04:23
Original Result DUP Result Dilution DUP RPD
Analyte Deg. F Deg. F
Ignitability DNI at170 DNI at170 1 0.000
L1479923-01 Original Sample (OS) • Duplicate (DUP)
DUP Qualifier DUP RPD
Limits
i
10
(OS) L1479923-01 04/13/22 04:23 • (DUP) R3730327-4 04/13/22 04:23
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte Deg. F Deg. F
Ignitability DNI at170 DNI at170 1 0.000 10
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3730327-1 04/13/22 04:23 • (LCSD) R3730327-2 04/13/22 04:23
Spike Amount LCS Result LCSD Result LCS Rec.
LCSD Rec.
Rec. Limits LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyte Deg. F Deg. F Deg. F
Ignitability 126 124 130 98.3
103
95.6-104 4.73
10
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
EMA Resources
L1479320
04/26/22 07:10 10 of 20

WG1852287 QUALITY CONTROL SUMMARY
Mercury by Method 7470A L1479820-01
Method Blank (MB)
(MB) R3784374-1 04/23/22 1513
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mg/I
Mercury U 0.00330 0.0100
Laboratory Control Sample (LCS)
(LCS) R3784374-2 04/23/22 1515
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
Mercury 0.0300 0.0336 112
Rec. Limits LCS Qualifier
80.0-120
L1479188-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1479133-01 04/23/22 15:17 • (MS) R3784374-3 04/23/22 15:19 • (MSD) R3784374-4 04/23/22 15:21
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Mercury 0.0300
ND
0.0311
0.0302 104 101 1 75.0-125 3.10 20
L1479864-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1479364-01 04/23/22 15:23 • (MS) R3784374-5 04/23/22 15:25 • (MSD) R3784374-6 04/23/22 15:27
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Mercury 0.0300
ND
0.0317
0.0311 106 104 1 75.0-125 1.62 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1479320 04/26/22 07:10 11 of 20

WG1852357
Metals (ICP) by Method 6010D
Method Blank (MB)
(MB) R3734123-1 04/22/22 08:24
MB Result
MB Qualifier MB MDL
Analyte mg/I
mg/I
Arsenic U
0.0333
Barium U
0.0333
Cadmium U
0.0333
Chromium U
0.0333
Lead U
0.0333
Selenium 0.0472
J 0.0333
Silver U
0.0333
Laboratory Control Sample (LCS)
(LCS) R3784128-2 04/22/22 08:27
Spike Amount
LCS Result
LCS Rec.
Analyte mg/I
mg/I
Arsenic 10.0
9.79
97.9
Barium 10.0
9.71
97.1
Cadmium 10.0
9.67
96.7
Chromium 10.0
9.44
94.4
Lead 10.0
9.63
96.3
Selenium 10.0
10.4
104
Silver 2.00
1.86
93.1
QUALITY CONTROL SUMMARY
L1479820-01
MB RDL
mg/I
0.100
0.100
0.100
0.100
0.100
0.100
0.100
Rec. Limits
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
LCS Qualifier
L1479595-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1479595-02 04/22/22 08:41 • (MS) R3734123-6 04/22/22 08:44 • (MSD) R3734123-7 04/22/22 08:47
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
Arsenic
10.0
ND
9.72
9.86
97.2
98.6
Barium
10.0
0.101
9.79
9.89
96.9
97.9
Cadmium
10.0
ND
9.64
9.75
96.4
97.5
Chromium
10.0
ND
9.67
9.52
95.8
94.4
Lead
10.0
ND
9.60
9.69
96.0
96.9
Selenium
10.0
ND
10.3
10.5
103
105
Silver
2.00
ND
1.88
1.88
94.0
94.1
Dilution Rec. Limits
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
MS Qualifier MSD Qualifier RPD
1.38
0.986
1.16
1.47
0.899
2.05
0.0815
RPD Limits
20
20
20
20
20
20
20
ACCOUNT: PROJECT: SDG:
EMA Resources L1479320
DATE/TIME:
04/26/22 07:10
PAGE:
12 of 20

WG1851052 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1479820-01
Method Blank (MB)
(MB) R3732911-3 04/19/22 18:22
MB Result
Analyte
mg/I
Benzene
U
Carbon tetrachloride
U
Chlorobenzene
U
Chloroform
U
1,2-Dichloroethane
U
1,1-Dichloroethene
U
2-Butanone (MEK)
U
Tetrachloroethene
U
Trichloroethene
U
Vinyl chloride
U
(S) Toluene-dH ill
(S) 4-Bromofluorobenzene 91.5
(S) 1,2-Dichloroethane-d4 100
MB Qualifier MB MDL
mg/I
MB RDL
mg/I
0.0167
0.0500
0.0167
0.0500
0.0167
0.0500
0.0833
0.250
0.0167
0.0500
0.0167
0.0500
0.167
0.500
0.0167
0.0500
0.0167
0.0500
0.0167
0.0500
80.0-120
77.0-126
70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3782911-1 04/19/22 15:24 • (LCSD) R3782911-2 04/19/22 15:46
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mg/I
mg/I
mg/I
Benzene
0.250
0.269
0.263
108
105
70.0-123
Carbon tetrachloride
0.250
0.259
0.273
104
109
68.0-126
Chlorobenzene
0.250
0.298
0.288
119
115
80.0-121
Chloroform
0.250
0.255
0.255
102
102
73.0-120
1,2-Dichloroethane
0.250
0.246
0.244
98.4
97.6
70.0-128
1,1-Dichloroethene
0.250
0.291
0.288
116
115
71.0-124
2-Butanone (MEK)
1.25
1.36
1.34
109
107
44.0-160
Tetrachloroethene
0.250
0.263
0.254
105
102
72.0-132
Trichloroethene
0.250
0.274
0.274
110
110
78.0-124
Vinyl chloride
0.250
0.331
0.316
132
126
67.0-131
(S) Toluene-dH
112
109
80.0-120
(S) 4-Bromofluorobenzene
92.9
90.2
77.0-126
(S) 1,2-Dichloroethane-d4
99.1
97.8
70.0-130
LCS Qualifier
J4
LCSD Qualifier RPD
2.26
5.26
3.41
0.000
0.816
1.04
1.48
3.48
0.000
4.64
RPD Limits
20
20
20
20
20
20
20
20
20
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1479320 04/26/22 07:10 13 of 20

WG1851431
QUALITY CONTROL SUMMARY
Chlorinated Acid Herbicides (GC) by Method 8151A
L1479820-01
Method Blank (MB)
(MB) R3734902-1 04/25/22 1716
MB Result MB Qualifier
MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
2,4,5-TP (Silvex) U
0.000667
0.00200
2,4-D U
0.000667
0.00200
(S) Z4-Dichlorophenyl Acetic 67.6
14.0-158
Acid
Laboratory Control Sample (LCS)
(LCS) R3784902-2 04/25/22 1731
Spike Amount LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I mg/I
2,4,5-TP (Silvex) 0.0500 0.0278
55.6
50.0-125 P
2,4-D 0.0500 0.0273
54.6
50.0-120 P
(S) Z4-Dichlorophenyl Acetic
44.2
14. 0-158
Acid
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1479320 04/26/22 07:10 14 of 20

WG1852709
Pesticides (GC) by Method 8081B
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1479820-01
(MB) R3734346-1 04/22/22 23:47
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Chlordane
U
0.00167
0.00500
Endrin
U
0.00167
0.00500
Heptachlor
U
0.00167
0.00500
Heptachlor epoxide
U
0.00167
0.00500
Gamma BHC
U
0.00167
0.00500
Methoxychlor
U
0.00167
0.00500
Toxaphene
U
0.00333
0.0100
(S) Decachlorobiphenyl
87.7
10.0-128
(S) Tetrochloro-m-xylene
70.3
10.0-127
Laboratory Control Sample (LCS)
(LCS) R3784346-2 04/22/22 23:56
Spike Amount
LCS Result
Analyte
mg/I
mg/I
Endrin
0.0100
0.00756
Heptachlor
0.0100
0.00836
Heptachlor epoxide
0.0100
0.00782
Gamma BHC
0.0100
0.00802
Methoxychlor
0.0100
0.00802
(S) Decachlorobiphenyl
(S) Tetrochloro-m-xylene
LCS Rec. Rec. Limits LCS Qualifier
75.6
83.6
78.2
80.2
80.2
70.3
62.7
57.0-134
27.0-132
57.0-130
55.0-129
54.0-155
10.0-128
10.0-127
L1479253-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1479253-01 04/23/22 00:15 • (MS) R3784346-3 04/23/22 00:25 • (MSD) R3784346-4 04/23/22 00:34
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
Endrin
0.0100
ND
0.00870
0.00592
87.0
59.2
Heptachlor
0.0100
ND
0.00833
0.00603
83.3
60.3
Heptachlor epoxide
0.0100
ND
0.00721
ND
72.1
49.1
Gamma BHC
0.0100
ND
0.00955
0.00617
95.5
61.7
Methoxychlor
0.0100
ND
0.00887
0.00653
88.7
65.3
(S) Decachlorobiphenyl
71.5
46.9
(S) Tetrochloro-m-xylene
60.9
39.8
Dilution Rec. Limits
1 10.0-160
1 16.0-136
1 10.0-160
1 14.0-141
1 10.0-160
10.0-128
10.0-127
MS Qualifier MSD Qualifier RPD RPD Limits
38.0 39
32.0 40
J3 38.0 36
J3 43.0 40
30.4 34
ACCOUNT: PROJECT: SDG:
EMA Resources L1479320
DATE/TIME:
04/26/22 07:10
PAGE:
15 of 20

WG1852705
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
QUALITY CONTROL SUMMARY
L1479820-01
Method Blank (MB)
(MB) R3784452-2 04/23/22 1023
MB Result
Analyte
mg/I
1,4-Dichlorobenzene
U
2,4-Dinitrotoluene
U
Hexachlorobenzene
U
Hexachloro-1,3-butadiene
U
Hexachloroethane
U
Nitrobenzene
U
Pyridine
U
3&4-Methyl Phenol
U
2-Methylphenol
U
Pentachlorophenol
U
2,4,5-Trichlorophenol
U
2,4,6-Trichlorophenol
U
(S) 2-Fluorophenol
36.0
(S) Phenol-d5
22.2
(S) Nitrobenzene-d5
64.9
(S) 2-Fluorobiphenyl
74.8
(S) Z4, 6-Tribromophenol
82.0
(S) p-Terphenyl-d14
78.3
MB Qualifier
Laboratory Control Sample (LCS)
MB MDL
mg/I
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
MB RDL
mg/I
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
10.0-120
10.0-120
10.0-127
10.0-130
10.0-155
10.0-128
(LCS) R3784452-1 04/23/22 10:01
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/I
mg/I
1,4-Dichlorobenzene
0.500
0.331
66.2
18.0-120
2,4-Dinitrotoluene
0.500
0.447
89.4
49.0-124
Hexachlorobenzene
0.500
0.387
77.4
44.0-120
Hexachloro-1,3-butadiene
0.500
0.296
59.2
19.0-120
Hexachloroethane
0.500
0.340
68.0
15.0-120
Nitrobenzene
0.500
0.327
65.4
27.0-120
Pyridine
0.500
0.0247
4.94
10.0-120 J4
3&4-Methyl Phenol
0.500
0.275
55.0
31.0-120
2-Methylphenol
0.500
0.271
54.2
28.0-120
Pentachlorophenol
0.500
0.403
80.6
23.0-120
2,4,5-Trichlorophenol
0.500
0.401
80.2
44.0-120
2,4,6-Trichlorophenol
0.500
0.394
78.8
42.0-120
(S) 2-Fluorophenol
37.4
10.0-120
(S) Phenol-d5
23.2
10.0-120
(S) Nitrobenzene-d5
54.4
10.0-127
ACCOUNT:
PROJECT:
EMA Resources
SDG: DATE/TIME: PAGE:
L1479320 04/26/22 07:10 16 of 20

WG1852705 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1479820-01
Laboratory Control Sample (LCS)
(LCS) R3784452-1 04/23/22 10:01
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
(S) 2-Fluorobiphenyl 74.3 10.0-130
(S) 2,4, 6-Tribromophenol 88.5 10. 0-155
(S) p-Terphenyl-d14 73.7 10.0-128
L1479188-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1479188-01 04/23/22 10:45 • (MS) R3784452-3 04/23/22 11:07 • (MSD) R3784452-4 04/23/22 1129
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec. Dilution
Rec. Limits
Analyte
mg/I
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
0.500
ND
0.314
0.289
62.8
57.8 1
17.0-120
2,4-Dinitrotoluene
0.500
ND
0.429
0.393
85.8
78.6 1
39.0-125
Hexachlorobenzene
0.500
ND
0.304
0.329
60.8
65.8 1
35.0-122
HexachIaro-1,3-butadiene
0.500
ND
0.270
0.273
54.0
54.6 1
12.0-120
Hexachloroethane
0.500
ND
0.319
0.299
63.8
59.8 1
10.0-120
Nitrobenzene
0.500
ND
0.313
0.292
62.6
58.4 1
12.0-120
Pyridine
0.500
ND
ND
ND
0.000
0.000 1
10.0-120
3&4-Methyl Phenol
0.500
ND
0.267
0.257
53.4
51.4 1
10.0-120
2-Methylphenol
0.500
ND
0.248
0.244
49.6
48.8 1
10.0-120
Pentachlorophenol
0.500
ND
0.363
0.384
72.6
76.8 1
10.0-128
2,4,5-Trichlorophenol
0.500
ND
0.341
0.358
68.2
71.6 1
33.0-120
2,4,6-Trichlorophenol
0.500
ND
0.347
0.363
69.4
72.6 1
26.0-120
(S) 2-Fluorophenol
33.5
31.6
10.0-120
(S) Phenol-d5
24.2
21.9
10.0-120
(S) Nitrobenzene-d5
53.7
50.4
10.0-127
(S) 2-Fluorobiphenyl
69.7
64.1
10.0-130
(S)2,4,6-Tribromophenol
79.5
81.0
10.0-155
(S) p-Terphenyl-d14
58.3
68.4
10.0-128
MS Qualifier MSD Qualifier RPD RPD Limits
J6 J6
8.29 40
8.76 25
7.90 24
1.10 34
6.47 40
6.94 30
0.000 37
3.82 36
1.63 30
5.62 37
4.86 31
4.51 31
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1479320 04/26/22 07:10 17 of 20

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contactyour project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
u
Fc
Fss]
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
Fn
RDL
Reported Detection Limit.
Rec.
Recovery.
Fr
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
F
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
F
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Rc
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J
The identification ofthe analyte is acceptable, the reported value is an estimate.
J3
The associated batch QC was outside the established quality control range for precision.
J4
The associated batch QC was outside the established quality control range for accuracy.
J6
The sample matrix interfered with the ability to make any accurate determination, spike value is low.
P
RPD between the primary and confirmatory analysis exceeded 40%.
T8
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1479320 04/26/22 07:10 13 of 20

ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
Nebraska
N E-OS-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TNO02
California
2932
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704 _
Georgia
NELAP
North Carolina 3
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky' 6
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee'"
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas5
LABO152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A2 LA
A2LA— ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME:
EMA Resources L1479320 04/26/22 07:10
PAGE:
19 of 20

Company Name/Address:
Billing Information: � ! or rprvativp
EMA Resources
Mr. Brent Collins LChk'
755 Yadkinville Road
755 Yadkinville Road
Macksvijle, NC 27028
Mocksville, NC 27028
Report to:
Email T-
Mr. Brent Collins
[e-mail];roy.whitak
Project Description:
Sludge
Phone: [phone]
Collected by (print):
&Yn+ Co ui nS
Collected by (signature):
Immediately
Packed on Ice N y
1 Sample ID
City/State Please Circle:
Collected: WGS�iiv ,'i7q �NG PT MT CT ET
Client Project # Lab Project #
Site/Facility ID #
Rush? (Lab MUST Be Notified)
Same Day Five Day
Next Day _ 5 Day (Rad Only)
Two Day 10 Day {Rad Only)
_Three Day
Comp/Grab
Matrix'
Depth
G
Ss
3
a
z°
ote #
O
w
�
J
Date Results Needed
No.
U
Date Time ntrs
N
CL
d
U
Yl�lz2
9r'00
2
x
X
Chain of Custody Page_ of
ace*
PEOPIE Rl>vMNCING SCrtXCE
MT JULIET, TN
12065 Lebanon Rd Mi Juliet, TN 37122
Subm,m a Sami thif chain of c44tpdy
canstdutes acknowledgment and acceptance of the
Pace Terms and conditions found at
http,flinfo, pacelits.com/hubft/pas-sta,d,,d.
terms.pdf
SDG# •{�gzfl
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4cctnum: EMARES
remplate:TI1413
Prelogin: P916841
PM: 807 - Justin Carr
PB:
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shipped Via: Fed EX Standard
Remarks Sample Of (lab only)
* Matrix:
SS - Soil AIR - Air F - Filter
GW- Groundwater B- Bioassay
ema►ks:
pH
Temp
Sample Receipt Checkii
COC Seal Present/Intact: -�iill_Y N
COC Signed/Accurate: _eV�N
WW - Wastewater
OT Drinking Water
OT -Other
Flow
Other
Bottles arrive intact: /Y N
Correct bottles used: /5[ N
sufficient volume sent: 1¢ �
If Aoolicable
VOA Zero Headspace: Y --X
Preservation Correct/Checked: Y —N
RAD Screen a0.5 mR/hr: � �l
Samples returned via:
—UPS FedEx Courier
Tracking#
Relinquished by: (Signature)
✓J ��
Date:
y/�/ZZ
Time:
+�'
Received by: (Signature)
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HCL / MeoH
TBR
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4 y : (Si nature
Date:
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Date: J Time:
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Hold: Conditi(y+ti
NCF

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Washington WQ Permit Number: WQ0001026
WWTP Name:
Washington WWTP
NPDES Number: NCO020648
Monitoring Period: From l/l/2022 To 12/31/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
1 Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
I Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
I Heat Drying ❑
1 Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
1 Gamma Ray ❑
1 Pasteurization ❑
Class B:
I Alt. (1) Fecal Density 0
I Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Cl. 2021
Parameter
Allowable Level
in Sludge
Pathogen Density
g �
Number o
Excee-
ences
Frequency
of Analysis
Sample
Type
Analytical
Tech -pique
Minimum
Geo. Mean
Maximurr
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
4500
14143
42500
MPN/g
0
Quarterly
G
SM92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt. I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable)
jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
❑`' "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Lonnie Woolard - NPDES ORC Brent Collins; Director of Technical Services
Preparer Name
/ ,and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
LMIIIr�i /!'I/��L�1'//l 4/� Feb 1, 2023
Lonnie I Woolard Jr (Feb 1, 202314:31 EST 1/3 1 /2023
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Date: 10/27/2022
Location #
1
2
3
4
5
6
7
Summary Sheet
Fecal Coliforms
Pathogen Reduction
MPN/g
10000
42500
11250
4500
11250
17000
27500
Log
4.0000
4.6284
4.0512
3.6532
4.0512
4.2304
4.4393
14143
Geometric Means/g
Total Dry Solids
/2�U�71) .
Signature

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Average Percent Volume of Sludge
Weight Volatile/Weight Dry x 100
January 2022 Average
R.S. 1 & 2 R.S. 3 R.S. 4
73.32% 73.05% 66.84%
February 2022 Average
R.S. 1 & 2 R.S. 3 R.S. 4
76.03% 75.53% 72.96%
March 2022 Average
R.S. 1 & 2 R.S. 3 R.S. 4
81.67% 75.92% 73.30%
April 2022 Average
R.S. 1 & 2 R.S. 3 R.S. 4
74.18% 74.37% 72.83%
May 2022 Average
R.S. 1 & 2 R.S. 3 R.S. 4
75.43% 73.61% 70.73%
June 2022 Average
R.S. 1 & 2 R.S. 3 R.S. 4
72.14% 71.07% 68.39%
July 2022 Average
R.S. 1 & 21 R.S. 3 R.S. 4
69.15% 1 73.85% 68.71%
August 2022 Average
R.S. 1 & 21 R.S. 3 R.S. 4
71.27% 1 69.60% 69.35%
September 2022 Average
R.S. 1 & 21 R.S. 3 R.S. 4
73.22% 1 70.80% 71.73%
October 2022 Average
R.S. 1 & 21 R.S. 3 R.S. 4
72.15% 1 73.13% 70.47%
November 2022 Average
R.S. 1 & 21 R.S. 3 R.S. 4
77.21% 1 79.28% 70.78%
December 2022 Average
R.S. 1 & 21 R.S. 3 R.S. 4
74.72% 1 76.08% 72.78%

January 2022 Average AVG.
R.S. 1 & 2 1 R.S. 3 R.S. 4
73.32% 1 73.05% 1 66.84% 71.07%
February 2022 Average
R.S. 1 & 21 R.S. 3 R.S. 4
76.03% 1 75.53% 1 72.96% 74.84%
March 2022 Average
R.S. 1 & 21 R.S. 3 R.S. 4
81.67% 1 75.92% 1 73.30% 76.96%
April 2022 Average
R.S. 1 & 21 R.S. 3 R.S. 4
74.18% 1 74.37% 1 72.83% 73.79%
May 2022 Average
R.S. 1 & 21 R.S. 3 R.S. 4
75.43% 1 73.61% 1 70.73% 73.26%
June 2022 Average
R.S. 1 & 21 R.S. 3 R.S. 4
72.14% 1 71.07% 1 68.39% 70.53%
July 2022 Average
R.S. 1 & 21 R.S. 3 R.S. 4
69.15% 1 73.85% 1 68.71% 70.57%
August 2022 Average
R.S. 1 & 21 R.S. 3 R.S. 4
71.27% 1 69.60% 1 69.35% 70.07%
September 2022 Average
R.S. 1 & 21 R.S. 3 R.S. 4
73.22% 1 70.80% 1 71.73% 71.92%
October 2022 Average
R.S. 1 & 21 R.S. 3 R.S. 4
72.15% 1 73.13% 1 70.47% 71.92%
November 2022 Average
R.S. 1 & 21 R.S. 3 R.S. 4
77.21% 1 79.28% 1 70.78% 75.76%
December 2022 Average
R.S. 1 & 21 R.S. 3 R.S. 4
74.72% 1 76.08% 1 72.78% 74.53%
2022 Average
10/19/22 Sample
VS in 0.7293
VS out 0.588
VSFR= 47.03
72.93%

Page 1 of 1
Report No: 23-003-0521
Account No: 46245
Advisor: EMA Resources Inc
755 Yadkinville Road
Mocksville NC 27028
Waypo'10 t
ANALYTICAL
Client: Hunters Roost Farms
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm: BF210
Date Received:01/03/2023
Date of Report: 01/04/2023
Lab No Field ID
Sample ID
Soil Class
HM% W/V
pH
Ac
P-1
K-1
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
CEC
BS %
Ca %
Mg %
ESP
Na
23662
04
MIN
1.3
5.3
1.8
9
20
29
588
0 0
75
75
65
5.8
68
47
19
0.8
0
23663
05
MIN
1.4
6.1
1.0
29
88
27
600
0 0
213
213
105
7.3
86
55
23
1.5
0.1
Comment:
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/V in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY22-SL033173
kSi l"14'4+;4,
Client: Harvey Williamson
Advisor: Brent Collins
Predictive
Hunters Roost Farm Septic Service
EMA Resources Inc
°± f'
5365 US Hwy 17 N
755 Yadkinville Rd
Soil Report Mehlich-3 Extraction
Washington, NC 27889
Mocksville, NC 27028
Links to Helpful Information
Sampled: Received: 05/03/2022 Completed: 05/10/2022 Farm: BF210
Sampled County : Beaufort
Client ID: 282102
Advisor ID: 405413
Sample ID: 16
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O Mg S Mn Zn
Cu B
Information
Lime History:
1-Soybean 0.0 0 0
70 0 0 0 0
0 0
Note: 3
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.36 1.34 5.0 78 1.1 5.9 384 36 57 17
31 77 56 180 180
222 0.1 2
North Carolina
Tcbwiv Truk f and Ct wmisskm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

Signature Page
Final Audit Report
Created: 2023-02-06
By: Brent Collins ([e-mail])
Status: Signed
Transaction ID: CBJCHBCAABAABPIjG7VCL3Gak2CxgfrdAcXJg7jNpmNb
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