WQ0039552_2022 Residual Annual Report_20230228 (2)

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * WQ0039552
Applicant/Permittee Town of Mocksville
Email Notifications
Does this need review by the hydrogeologist? * Yes U No
Regional Office Winston-Salem
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Brent Collins
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
336-399-3646
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0039552
Has Current Existing permit number
Applicant/Permittee Address*
171 Clement Street, Mocksville, NC 27028
Facility Name*
Town of Mocksville Class A Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2022 Mocksville WTP Annual Report - WQ0039552.pdf 8.93MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/28/2023

February 28, 2023
DENR/Water Quality Section
Non -Discharge Compliance Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2022 Annual Report — Mocksville WTP
Treatment and Land Application of Residuals
Permit No. WQ0039552
Dear Sir or Madam:
Enclosed is the 2022 Annual Report for the above referenced land application permit.
During 2022 EMA Resources, Inc. land applied 114.93 dry tons of wastewater residuals
to 18.2 acres of private farmland. Please contact Brent Collins - Director of Technical
Services if you have any further questions regarding this report.
Sincerely,
Brent Collins
Director of Technical Services
brent.collins&emaresourcesinc.com
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

t
esources, Inc.
Town of Mocksville WTP
2022 Annual Report
Residuals Land Application
Permit No. WQ0039552
Prepared By:
EMA Resources, Inc.
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT 4: WQ0039552 FACILITY NAME:
PHONE:
COUNTY: Davie
Town of Mocksville - Water Treatment Plant
OPERATOR:
Town of Mocksville
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
2 Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes ! 1 No ❑ —► If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES 4 if applicable)
Volume (dry tons)
Recipient information
Amendment/ Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
(January
February
(March
I
April
I
IMay
I
1June
y
j
(July
I
(August
(September
JOctober
lNovember
December
Total from FORM DMSDF (sup)
0
114.93
1 14.93
114.93
Totals:
Annual (dry tons):
0
114.93
114.93
114.93
Amendment(s) used:
Bulking A ent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)):
Part C:
Total Number of Form DMSDF (Supp)l 0 1
Facility was compliant during the past calendar year with all conditions of the land application permit L9 Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: ❑ No --► If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
XlzlieezLh w GawXg
Kenneth W. Gamble (Feb 23, 202312:00 EST)
Signature of Permittee
Feb 23, 2023
Date
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Signature of Preparer**
(if different from Permittee)
A7-22-2 3
Date
DENR FORM DMSDF (12/2006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0039552 FACILITY NAME:
PHONE:
Supplemental Information
COUNTY: Davie
Town of Mocksville - Water Treatment Plant
OPERATOR: Town of Mocksville
FACILITY TYPE (please check one): © Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
Distribution and Marketing (complete Parts A, and B)
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
March
Town of Mocksville WTP
114.93
114.93
Roger Spillman
114.93
Soil Amendment
Totals:
Annual (dry tons):
0
114.93
114.93 114.93
Amendment(s) used: I Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)l 1
DENR FORM DMSDF (Supp) (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0039552 Laboratory:
Facility Name: Town of Mocksville - WTP
Residual Source WQ # or
NPD1 S #:
WWTP Name:
Residual Analysis Data
NCO230010
Mocksville WTP
1) Waypoint Analytical
2)
3)
4)
5)
Parameter
(mg/kg)
Conc.
Limit
(mg/kg)
Sample or Composite Date
1/24/22
Percent Solids (°/a)
NA
5.3
Arsenic
75
7.58
Cadmium
85
0.377
Copper
4,300
37.2
Cliromium
NA
71.5
Lead
840
28.5
Mercury
57
0.124
Molybdenum
75
2.55
_
420
28.1
^` _
_Nickel _
Selenium
100
6.04
Zinc
7,500
86.4
Total Phosphorus
TKN
Ammonia -Nitro en
Nitrate and Nitrite
NA
NA
NA
NA
1580
14600
2090
93.4
_
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathergd and evaluated the information submitted. I am aware that there are significant
penaly. es for submitting false information, including the possibility of fines and imprisonment for knowing violations."
of Preparer *
-,23-23
Date
*Preparer is defined in 40 CFR Part 5039(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number:
WQ0039552
Facility Name:
Town of Mocksville - WTP
Residual Source
NCO230010
NPDES # or WQ#:
WWTP Name:
Mocksville WTP
Residual Analvsis Data
Laboratory: 1) Waypoint Analytical
2)
3)
4)
5)
Parameter
(mg/kg)
Sample or Composite Date
1 /24/22
Aluminum
89100
Calcium
1690
Magnesium
3960
pH
6.5
Potassium
Sodium
PAN
SAR
2960
289
2389
0.2
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
,Z.23—
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF - B (1212006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Mocksville-WTP Total Dry Tons Applied (Annual):
WQ0039552 Cation Exchange Capacity (non 503 only):
Roger Spillman Owner: Roger Spillman Predominant Soil Series:
18.2 Acres Permitted: 18.2 Site #: NC-DVO08 Field #:
128.13
MrB2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
WTP
1/24/22
2 j
WWTP
10/6/22
3
4
5
6
7
8
9
10
11
12
% Solids
5.3
1.09
Arsenic
1 7.58
21.8
Cadmium
0.377
1.82
Copper
37.2
380
Chromium
71.5
31.1
Lead
28.5
22.8
Mercury
0.124
0.606
Molyb-
denum
2.55
12.3
Nickel
28.1
21.2
Selenium
6.04
29.1
Zinc
86.4
819
Total
Phos-
horus
1580
28900
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
8
Total
m
mD
-EventNEW
Monosson
1 1••
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
®
1 1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1•
®
1 •1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1•
®
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 1
®�
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1:•
®
1 1 •
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
®
1 •
::
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
Phos-
• •
•1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
• :•1
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/3/2023
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Town of Mocksville-WTP WQ Permit #: WQ0039552 Field #: 8 Acres Utilized:
Roger Spillman Annual Dry Tons Applied: 128.13 Site #: NC-DVO08 Acres Permitted:
Roger Spillman
Crop 1 Name: Fescue -Pasture
Predominant Soil Series:
Crop 1 Max. PAN: 141
MrB2
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
18.2
18.2
a� o
c�
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
.
(Dry,
Wet,
Moist)
Precip.
Past 24
Hrs.
inches
a
4 �
co
0 w
o
o
-
N
=
= _-
7y
D N
� w
o,
TKN
mg/kg
Z a
I �
o
o
CD
�
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
3/15/22
182000
5.3
2.210
Mocksville WTP
Dry
<.5"
S
0.5
0
14600
1 2090
93.4
5.032
NA
Fescue
3/16/22
104000
5.3
1.263
Mocksville WTP
Dry
<.5"
S
0.5
0
14600
2090
93.4
2.875
NA
Fescue
3/21/22
123500
5.3
1.500
Mocksville WTP
Dry
<.5"
S
0.5
0
14600
2090
93.4
3.415
NA
Fescue
3/22/22
110500
5.3
1.342
Mocksville WTP
Dry
<.5"
S
0.5
0
14600
2090
93.4
3.055
NA
Fescue
10/18/221
143000
1.09
0.357
Dutchman's Creek
Dry
<.5"
1 S
0.5
0.3
1 85600
6080
1 7920
24.868
1 NA
Fescue
10/19/22
84500
1 1.09
0.211
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
85600
6080
7920
14.695
NA
Fescue
12/28/23
18000
1.09
0.045
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
85600
6080
7920
3.130
NA
Fescue
12/29/23
45000
1.09
0.112
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
85600
6080
7920
7.826
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM
FSF supp
to this form):
TOTALS:
01
810500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
64.895
0.000
Lime Applied
Annuallbs/acre
0.127
0.007
1.021
0.948
0.393
0.002
0.050
0.386
0.118
2.279
61.860 1
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.419
0.173
16.654
4.708
3.914
0.087
0.662
2.214
0.432
66.771
Current Cumulative lbs/ac
0.546
0.180
17.675
5.656
4.307
0.089
0.712
2.600
0.550
69.050
Permitted C. P. L. R.****
36
1 34
1 1338
1
1 267
1 15
1
1 374
1 89
1 2498
Pennit PAN Limit 1 st/2nd Crop
1 141
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/3/2023 **Volatilization Rate: Surface - 0.5, injection/incorporation -1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Waypointo
ANALYTICAL
2/2/2022
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 22-025-0020
Client Project Description: Mocksville, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 1 /25/2022 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a' -'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 9

0%
Wayp�int.
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2022
Arkansas
State Program
88-0650
02/07/2022
California
State Program
2904
06/30/2022
Florida
State Program
- NELAP
E871157
06/30/2022
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2022
Illinois
State Program
- NELAP
200078
10/10/2022
Kentucky
State Program
80215
06/30/2022
Kentucky
State Program
KY90047
12/31/2022
Louisiana
State Program
- NELAP
LA037
12/31/2022
Louisiana
State Program
- NELAP
04015
06/30/2022
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
415
12/31/2022
Pennsylvania
State Program
- NELAP
68-03195
05/31/2022
South Carolina
State Program
84002
06/30/2022
South Carolina
State Program
84002
06/30/2022
Tennessee
State Program
02027
02/11/2023
Texas
State Program
- NELAP
T104704180
09/30/2022
Virginia
State Program
00106
06/30/2022
Virginia
State Program
- NELAP
460181
09/14/2022
Page 1 of 1 00001/22-025-0020
Page 2 of 9

•
Waypoint 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 22-025-0020
Client Project Description: Mocksville, NC
Lab No Client Sample ID Matrix Date Collected Date Received
91577 Mocksville WTP Solids 01/24/2022 09:00 01/25/2022
Page 3 of 9

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Mocksville, NC
Lab Report Number: 22-025-0020
Date: 2/1 /2022
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 99187
Analyte: Aluminum
QC Batch No: L596771 /L596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Analyte: Calcium
QC Batch No: L597088/L596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Analyte: Copper
QC Batch No: L596771 /L596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Analyte: Iron
QC Batch No: L596771 /L596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Analyte: Potassium
QC Batch No: L597000/L596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 99187
Analyte: Magnesium
QC Batch No: L597000/L596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Analyte: Manganese
QC Batch No: L596771 /L596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Page 4 of 9

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Analyte: Phosphorus
QC Batch No: 1-597000/1-596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Analyte: Lead
QC Batch No: 1-596771 /L596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Analyte: Sulfur
QC Batch No: 1-597000/1-596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Analyte: Zinc
QC Batch No: 1-596771 /L596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 5 of 9

Waypointo
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 22-025-0020
Lab No : 91577
Sample ID : Mocksville WTP
Project Mocksville, NC
Information :
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° fax [phone]
www.waypointanalytical.com
REPORT OFANALYSIS
Report Date : 02/02/2022
Received : 01/25/2022
00 �&':� w-a
Danyale Love
Project Manager
Matrix: Solids
Sampled: 1/24/2022 9:00
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Moisture
94.7
%
0.010
1
01/26/2216:41
FMM
SW-DRYWT
Ammonia Nitrogen
2090
mg/Kg - dry
302
1890
1
02/01/22 14:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<93.4
mg/Kg - dry
93.4
93.4
1
02/01/22 14:46
ZBD
4500NO3F-2011
Organic N
12550
mg/Kg - dry
301.9
1887
1
01/31/22 10:00
CALCULATION
pH
6.5
S.U.
1
01/31/2215:39
DRS
9045D
Total Solids
5.30
%
0.010
0.010
1
01/26/22 16:41
FMM
2540G-2011
Total Kjeldahl Nitrogen
14600
mg/Kg - dry
189
4720
1
01/31/22 10:00
JPJ
;M-4500-NH3C-TKP
Phosphorus
1580
mg/Kg - dry
52.1
94.3
1
01/28/22 05:34
EAL
6010D
Aluminum
89100
mg/Kg - dry
87.2
94.3
1
01/28/22 05:34
EAL
6010D
Arsenic
7.583
mg/Kg - dry
4.53
9.43
1
01/28/22 05:34
EAL
6010D
Cadmium
<0.377
mg/Kg - dry
0.377
1.89
1
01/28/22 05:34
EAL
6010D
Calcium
1690
mg/Kg - dry
730
943
1
01/28/22 05:34
EAL
6010D
Chromium
71.5
mg/Kg - dry
4.45
4.72
1
01/28/22 05:34
EAL
6010D
Copper
37.2
mg/Kg - dry
5.85
9.43
1
01/28/22 05:34
EAL
6010D
Iron
42300
mg/Kg - dry
161
189
1
01/28/22 05:34
EAL
6010D
Lead
28.5
mg/Kg - dry
3.40
5.66
1
01/28/22 05:34
EAL
6010D
Magnesium
3960
mg/Kg - dry
48.7
94.3
1
01/28/22 05:34
EAL
6010D
Manganese
1000
mg/Kg - dry
6.13
9.43
1
01/28/22 05:34
EAL
6010D
Mercury
<0.124
mg/Kg - dry
0.124
0.285
1
01/26/22 17:15
JW2
7471A
Molybdenum
<2.55
mg/Kg - dry
2.55
4.72
1
01/28/22 05:34
EAL
6010D
Nickel
28.1
mg/Kg - dry
2.26
4.72
1
01/28/22 05:34
EAL
6010D
Potassium
2960
mg/Kg - dry
117
189
1
01/28/22 21:48
EAL
6010D
Selenium
<6.04
mg/Kg - dry
6.04
9.43
1
01/28/22 21:48
EAL
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 6 of 9

•
Waypoint.
27090 Whitten
Road, Memphis, TN 38133
Main 901.213.2400 ° fax [phone]
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Project
Mocksville, NC
Mr. Brent Collins
Report Date : 02/02/2022
755 Yadkinville Rd
Information :
Received : 01/25/2022
Mocksville , NC 27028
Danyale Love
Report Number :22-025-0020
REPORT OFANAL
YSIS
Project Manager
Lab No : 91577
Matrix: Solids
Sample ID : Mocksville WTP
Sampled: 1/24/2022 9:00
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Sodium
289 J
mg/Kg - dry
245
472 1 01/28/22 05:34 EAL 6010D
Zinc
86.4
mg/Kg - dry
15.3
23.6 1 01/28/22 05:34 EAL 6010D
Sulfur
1340
mg/Kg - dry
97.7
189 1 01/28/22 05:34 EAL 6010D
Sodium Absorption Ratio
0.20 J
Ratio
0.01
0.01 1 01/28/22 05:34 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
J Estimated value
Page 7 of 9

Wayj�oi279D Whitten Road, Memphis, TN 38133
Main 901,213.2400 ° Fax [phone]
N A LYT I C A L www.waypointanalyrical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 22-025-0020
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
T137
Shipping container/cooler uncompromised?
# Yes
0 No
Number of coolers/boxes received
F_ 1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
Yes
0 No
COC properly completed
Yes
0 No
Samples in proper containers?
Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
Water - VOA vials free of headspace
Trip Blanks received with VOAs
Soil VOA method 5035 — compliance criteria met
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Special precautions or instructions included?
Comments:
DYes
0No
ON/A
0 Yes
0 No
0 N/A
DYes
0No
ON/A
0 Yes
0 No
0 N/A
Low concentration EnCore samplers (48 hr)
F_ Low conc
pre -weighed
vials (Sod Bis -14 d)
DYes ONo
Signature: Imakayla Weaver Date & Time: 01 /25/2022 09:00:55
Page 8 of 9

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1 /24/2022
mg/kg mg/L Equiv Weight Milli Equiv
Sodium 289 15.317 23 0.665957
Calcium 1690 89.57 20 4.4785
Magnesium 3960 209.88 12 17.49
Percent Solids 5.3
SAR 0.20
SAR = Na'
(C a2-i + Mg2+ )
0.66596
0.5( 4.4785 2 + 17.49000 2 )

(:�;a'cmnalXical"' ANALYTICAL REPORT
February 07, 2022
EMA Resources
Sample Delivery Group: L1454554
Samples Received: 01/25/2022
Project Number:
Description: Sludge
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By:
Justin Carr
' Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
4
a
11
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
rMA Resources L1454554 02/07/22 16:05 1 of 21

TABLE OF CONTENTS
Cp: Cover Page
Tc: Table of Contents
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
MOCKSVILLE WTP L1454554-01
5
Qc: Quality Control Summary
7
Wet Chemistry by Method 9012 B
7
Wet Chemistry by Method 9034-9030B
8
Wet Chemistry by Method 9045D
9
Wet Chemistry by Method D93/1010A
10
Mercury by Method 7470A
11
Metals (ICP) by Method 6010D
12
Volatile Organic Compounds (GC/MS) by Method 8260D
13
Chlorinated Acid Herbicides (GC) by Method 8151A
15
Pesticides (GC) by Method 8081B
16
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
17
GI: Glossary of Terms
19
Al: Accreditations & Locations
20
Sc: Sample Chain of Custody
21
ACCOUNT: PROJECT: SDG:
DATE/TIME: PAGE:
EMA Resources L1454554
02/07/22 16:05 2 of 21

MOCKSVILLE WTP L1454554-01 Waste
Collected by
Brent Collins
Collected date/time
01/24/22 09:00
Received date/time
01/25/22 09:15
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
date/time
date/time
Preparation by Method 1311
WG1808840
1 01/27/2210:39
01/27/2210:39
JWS
Mt. Juliet, TN
Preparation by Method 1311
WG1809554
1 01/28/2212:49
01/28/2212:49
CJW
Mt. Juliet, TN
Wet Chemistry by Method 9012 B
WG1808566
1 01/30/2211:27
02/01/2214:39
LDT
Mt. Juliet, TN
Wet Chemistry by Method 9034-9030B
WG1809680
1 01/31/2216:00
02/01/22 22:00
SAC
Mt. Juliet, TN
Wet Chemistry by Method 9045D
WG1808419
1 01/26/2214:00
01/27/22 09:00
GI
Mt. Juliet, TN
Wet Chemistry by Method D93/1010A
WG1812928
1 02/04/22 01:08
02/04/22 01:08
WOS
Mt. Juliet, TN
Mercury by Method 7470A
WG1810317
1 01/30/22 09:32
01/31/22 09:41
MRW
Mt. Juliet, TN
Metals (ICP) by Method 6010D
WG1810384
1 02/01/22 00:24
02/01/22 23:50
CCE
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1810127
1 01/29/2216:27
01/29/2216:27
JAH
Mt. Juliet, TN
Chlorinated Acid Herbicides (GC) by Method 8151A
WG1811223
1 02/02/22 08:09
02/03/2211:59
AO
Mt. Juliet, TN
Pesticides (GC) by Method 8081B
WG1809205
1 02/03/22 06:33
02/03/2215:56
AO
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG1809535
1 01/30/2216:30
01/31/22 06:11
JNJ
Mt. Juliet, TN
ACCOUNT:
PROJECT:
S DG:
DATE /TIME:
PAGE:
LMA Resources
L1454554
02/07/22
16:05
3 of 21

CASE NARRATIVE
Cp
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
17C
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
ISS]
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
Sr
I
5
QC
GI
Justin Carr
CAI
Project Manager
I _SC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012 B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034-9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1454554 02/07/2216:05 4 of21

SAMPLE RESULTS - 01
L1454554
MOCKSVILLE WTP
Collected date/time: 01/24/22 09:00
Preparation by Method 1311
Result Qualifier
Prep
Batch
Analyte
date / time
TCLP Extraction
1/27/202210:39:54 AM
WG1208840
TCLP ZHE Extraction -
1/28/202212:49:36 PM
WG1309554
Fluid 1
1/27/202210:39:54 AM
WG1308840
Initial pH 6.60
1/27/202210:39:54 AM
WG1308840
Final pH 4.98
1/27/202210:39:54 AM
WG1308840
Wet Chemistry by Method 9012 B
Result Qualifier
RDL Dilution
Analysis Batch
Analyte mg/kg
mg/kg
date / time
Reactive Cyanide ND
0.250 1
02/01/202214:39 WG1808566
Wet Chemistry by Method 9034-9030B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Reactive Sulfide ND
Wet Chemistry by Method 9045D
Analyte
25.0 1 02/01/2022 22:00 WG1809680
Result Qualifier Dilution Analysis Batch
su date/time
Corrosivity by pH 6.64 T8
Sample Narrative:
L1454554-01 WG1808419:6.64 at18C
Wet Chemistry by Method D93/1010A
1 01/27/2022 09:00 WG1808419
Result Qualifier Dilution Analysis Batch
Analyte Deg. F date / time
Ignitability DNI at 200 1 02/04/2022 01:08 WG1812928
Mercury by Method 7470A
Result Qualifier RDL Limit
Analyte mg/I mg/I mg/I
Mercury ND 0.0100 0.20
Metals (ICP) by Method 6010D
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Arsenic
ND
0.100
5
Barium
ND
0.100
100
Cadmium
ND
0.100
1
Chromium
ND
0.100
5
Lead
ND
0.100
5
Selenium
ND
0.100
1
Silver
ND
0.100
5
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Benzene
ND
0.0500
0.50
Carbon tetrachloride
ND
0.0500
0.50
Chlorobenzene
ND
0.0500
100
Chloroform
ND
0.250
6
ACCOUNT:
LIMA Resources
PROJECT:
Dilution Analysis Batch
date / time
1 01/31/2022 09:41 WG1810317
Dilution Analysis
Batch
date / time
1 02/01/2022 23:50
WG1810384
1 02/01/2022 23:50
WG1810384
1 02/01/2022 23:50
WG1810384
1 02/01/2022 23:50
WG1810384
1 02/01/2022 23:50
WG1810384
1 02/01/2022 23:50
WG1810384
1 02/01/2022 23:50
WG1810384
Dilution Analysis
Batch
date / time
1 01/29/202216:27
WG1810127
1 01/29/202216:27
WG1810127
1 01/29/202216:27
WG1810127
1 01/29/202216:27
WG1810127
SDG:
DATE/TIME:
L1454554
02/07/22 16:05
PAGE:
5of21

MOCKSVILLE WTP
SAMPLE RESULTS
- 01
Collected date/time: 01/24/22 09:00
L1454554
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
Analyte
mg/l
mg/l
mg/1
date/time
1,2-Dichloroethane
ND
0.0500
0.50
1
01/29/2022 16:27
WG1810127
1,1-Dichloroethene
ND
0.0500
0.70
1
01/29/2022 16:27
WG1810127
2-Butanone (MEK)
ND
0.500
200
1
01/29/2022 16:27
WG1810127
Tetra chloroethene
ND
0.0500
0.70
1
01/29/2022 16:27
WG1810127
Trichloroethene
ND
0.0500
0.50
1
01/29/2022 16:27
WG1810127
Vinyl chloride
ND
0.0500
0.20
1
01/29/2022 16:27
WG1810127
(S) Toluene-d8
93.6
80.0-120
011291202216:27
WG1810127
(S)4-Bromofluorobenzene
102
77.0-126
011291202216:27
WG1810127
(S)1,2-Dichloroethane-d4
90.6
70.0-130
011291202216:27
WG1810127
Chlorinated Acid Herbicides (GC) by
Method 8151A
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
Analyte
mg/l
mg/l
mg/1
date/time
2,4,5-TP (Silvex)
ND
0.00200
1
1
02/03/202211:59
WG1811223
2,4-D
ND
0.00200
10
1
02/03/202211:59
WG1811223
(S) 2,4-Dichlorophenyl Acetic Acid
77.8
14.0-158
021031202211:59
WG1811223
Pesticides (GC) by Method 8081B
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
Analyte
mg/l
mg/l
mg/1
date/time
Chlordane
ND
0.00500
0.03
1
02/03/202215:56
WG1809205
Endrin
ND
0.00500
0.02
1
02/03/202215:56
WG1809205
Heptachlor
ND
0.00500
0.0080
1
02/03/202215:56
WG1809205
Heptachlor epoxide
ND
0.00500
0.0080
1
02/03/202215:56
WG1809205
Lindane
ND
0.00500
0.40
1
02/03/202215:56
WG1809205
Methoxychlor
ND
0.00500
10
1
02/03/202215:56
WG1809205
Toxaphene
ND
0.0100
0.50
1
02/03/202215:56
WG1809205
(S) Decochlorobiphenyl
93.8
10.0-128
021031202215:55
WG1809205
(S) Tetrochloro-m-xylene
93.0
10.0-127
021031202215:55
WG1809205
Semi Volatile Organic Compounds
(GC/MS) by Method 8270E
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
Analyte
mg/l
mg/l
mg/1
date/time
1,4-Dichlorobenzene
ND
0.100
7.50
1
01/31/2022 0611
WG1809535
2,4-Dinitrotoluene
ND
0.100
0.13
1
01/31/2022 0611
WG1809535
Hexachlorobenzene
ND
0.100
0.13
1
01/31/2022 0611
WG1809535
Hexachloro-1,3-butadiene
ND
0.100
0.50
1
01/31/2022 0611
WG1809535
Hexachloroethane
ND
0.100
3
1
01/31/2022 0611
WG1809535
Nitrobenzene
ND
0.100
2
1
01/31/2022 0611
WG1809535
Pyridine
ND
0.100
5
1
01/31/2022 06:11
WG1809535
3&4-Methyl Phenol
ND
0.100
400
1
01/31/2022 0611
WG1809535
2-Methylphenol
ND
0.100
200
1
01/31/2022 0611
WG1809535
Pentachlorophenol
ND
0.100
100
1
01/31/2022 0611
WG1809535
2,4,5-Trichlorophenol
ND
0.100
400
1
01/31/2022 0611
WG1809535
2,4,6-Trichlorophenol
ND
0.100
2
1
01/31/2022 0611
WG1809535
(S) 2-Fluorophenol
52.0
10.0-120
0113112022 06:11
WG1809535
(S) Phenol-d5
31.0
10.0-120
0113112022 06:11
WG1809535
(S) Nitrobenzene-d5
78.0
10.0-127
0113112022 06:11
WG1809535
(S) 2-Fluorobiphenyl
72.3
10.0430
0113112022 06:11
WG1809535
(S) 2,4,6-Tribromophenol
74.0
10.0455
0113112022 06:11
WG1809535
(S) p-Terphenyl-d14
85.9
10.0-128
0113112022 06:11
WG1809535
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
EMA Resources
L1454554
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
Intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
u
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J3
The associated batch QC was outside the established quality control range for precision.
J5
The sample matrix Interfered with the ability to make any accurate determination; spike value is high.
J6
The sample matrix Interfered with the ability to make any accurate determination; spike value is low.
T8
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1454554 02/07/22 16:05 19 of 21

ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
Nebraska
NE-05-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TNO02
California
2932
New Mexico
_
TN00003 _
Colorado _
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolina'
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
_ Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky's
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
AI30792
Tennessee
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas'
LAB0152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-305
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A2LA
A2LA — 150 17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A21-A — ISO 17025'
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks ' Aquatic Toxicity 4 Chemical/Microbiological ' Mold ' Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
ACCOUNT: PROJECT: SDG: DATE/TIME:
LMA Resources L1454554 02/07/2216:05
PAGE:
20 of 21

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2022 Mocksville WTP Annual Report -
WQ0039552
Final Audit Report
Created: 2023-02-23
By: Brent Collins ([e-mail])
Status: Signed
Transaction ID: CBJCHBCAABAAwHGNhryl5VXpODUyLIChf-mwY5lB81 DI
2023-02-23
"2022 Mocksville WTP Annual Report - WQ0039552" History
Document created by Brent Collins ([e-mail])
2023-02-23 - 4:50:34 PM GMT- IP address: 206.85.202.26
Document emailed to [e-mail] for signature
2023-02-23 - 4:51:10 PM GMT
Email viewed by [e-mail]
2023-02-23 - 4:59:03 PM GMT- IP address: 67.213.52.2
Signer [e-mail] entered name at signing as Kenneth W. Gamble
2023-02-23 - 5:00:10 PM GMT- IP address: 67.213.52.2
00 Document e-signed by Kenneth W. Gamble ([e-mail])
Signature Date: 2023-02-23 - 5:00:12 PM GMT - Time Source: server- IP address: 67.213.52.2
Agreement completed.
2023-02-23 - 5:00:12 PM GMT
a Adobe Acrobat Sign