WQ0030998_2022 Residual Annual Report_20230227

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * WQ0030998
Applicant/Permittee Triple S Farms and Cleaning, Inc.
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Wilmington
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Robert T. Branch
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
3363129007
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0030998
Has Current Existing permit number
Applicant/Permittee Address*
PO Box 709 Beulaville NC 28518
Facility Name*
Triple S Farms and Cleaning Class B Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2022_SSS_AR_COMPLETE.pdf 18.68MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/27/2023

2022 ANNUAL REPORT
TRIPLE S FARMS & CLEANING, INC.
LAND APPLICATION PROGRAM
PERMIT #WQ0030998
Prepared For:
Triple S Farms & Cleaning, Inc.
Post Office Box 709
Beulaville, NC 28518
Prepared By:
Branch Residuals & Soils, LLC
1735 Heckle Blvd. Suite 103-291
Rock Hill, SC 29732
February 2023

BRANCH RESIDUALS & SOILS, LLC
1735 Heckle Blvd, Suite 103-291, Rock Hill, SC 29732
PHONE [phone]
February 27, 2023
North Carolina Department of Environmental Quality
Division of Water Resources
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Reference: 2022 LAND APPLICATION ANNUAL REPORT
Triple S Farms & Cleaning, Inc.
Permit No. WQ0030998
Branch Residuals & Soils Project No. 2007-70
Information Processing Unit:
Branch Residuals & Soils is submitting all monitoring and reporting information as required in the referenced
permit on behalf of the Triple S Farms & Cleaning, Inc. This data includes: 1) Certification Forms and Facility
Information, 2) Annual Residual Sampling Summary Forms, 3) Annual Metals Field Loading Summary Forms,
4) Annual land application Field Summary Forms, 5) Residual Analysis Lab Sheets, 6) TCLP Lab Sheets, 7)
Pathogen & Vector Attraction Forms, 8) Pathogen and Vector Attraction Reduction Documentation, 9) Soils
Lab Data 10) 2022 Application Summary Table, and 11) 2022 Application Condition Summaries.
A total of 6,030,598 gallons and 268.57 wet tons (total of 649.76) of Class B lime -stabilized biosolids or Class
B fecal and injected/incorporated/SOUR tested biosolids were land applied to 139.9 acres in 2022. This
material was divided as follows:
• 253,000 gallons (26.27 dry tons) from Beulaville WWTP,
• 3,251,100 gallons (261.23 dry tons) from Clayton Little Creek WRF,
• 66,000 gallons (2.92 dry tons) from Kenansville WWTP,
• 268.57 wet tons (77.42 dry tons) from Rose Hill WWTP,
• 458,000 gallons (40.11 dry tons) from Warsaw WWTP,
• 24,000 gallons (1.72 dry tons) from Southwest Plantation WWTP
■ 74,000 gallons (1.36 dry tons) from the Town of Bridgeton,
• 110,000 gallons (2.2 dry tons), from the Town of Maysville,
• 300,498 gallons (24.31 dry tons) from Swansboro WWTP, and
• 1,494,000 gallons (162.67.99 dry tons) from the Town of Wallace.
If any further information is required regarding this land application program, please do not hesitate to contact
me at [phone].
Sincerely, r
r
Robert . Branch, L.S.S.
Land Application/Residuals Operator #15676
RTB
Enclosures
cc: Town of Beulaville Town of Kenansville
Town of Rose Hill Town of Warsaw
Southwest Plantation Town of Wallace
Town of Clayton Town of Bridgeton
Town of Maysville Onwasa Swansboro WWTP

TABLE OF CONTENTS
SECTION NO, TITLE
I Certification Forms and Facility Information
II Annual Residual Sampling Summary Forms
III Annual Metals Field Loading Summary Forms
IV Annual Land Application Field Summary Forms
V Residual Analysis Lab Sheets
VI Toxicity Characteristics Leaching Procedure
(TCLP) Analysis Report
VII Pathogen and Vector Attraction Reduction
Forms
VIII Pathogen and Vector Attraction Reduction Documentation
IX Soil Analysis Reports
X 2022 Application Summary Table
XI 2022 Application Condition Summaries

CERTIFICATION FORMS AND FACILITY INFORMATION

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0030998 County: Duplin Year: 2022
Facility Name (as shown on permit): Triple S Farms & Cleaning
Land Application Operator: Triple S Farms & Cleaning Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
El Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Total number of application fields in the pt
Total number of fields utilized for land application during the
Total amount of dry tons applied during the year for all application sites: 600.21
Total number of acres utilizes for land application during the vear 11400
Part B - Annual Comuiance Statement:
Facility was compliant during calendar year 2022 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. p Yes p No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
of Maysville was noncompliant ( explanation follows). Other facilties and the land applier were compliant.
The Town
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T . 1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Mr. Eric R. Smith, Owner
Permittee Name and Title (type or print)
See Attached
�CA'
r-QIa7
Signature of Permittee Date
Signature of Preparer* Date Signature of Land Applier
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
Date
DENR FORM ACF (12/2006)

LAND APPLICATION NONCOMPLIANCE ISSUES
Compliance for Part B Condition 8 — Other Monitoring Performed
This permit had one instance of noncompliance in 2022. This instance involved the Town of
Maysville as noted below.
1. The Town of Maysville had a arsenic concentration for their biosolids sample that
exceeded the ceiling concentration. In discussions with Envirochem, the percent solids of
0.48% probably had significant impact on the labs ability to have lowered detection
limits. The Town of Maysville will collect another sample and that value will be reported
to NCDEQ for confirmation. A sample should have been collected as soon as these
values were reported. I was not given the report until the year had ended.
This permit had one instance of note in 2022. This instance involved the Town of Clayton as
noted below.
1. The Town of Clayton failed to analyze an ammonia nitrogen sample in the fourth quarter.
The collected sample for the fourth quarter was marked correctly on the chain of custody
but not analyzed by the lab. An average of the previous three quarters ammonia value
was used for calculation purposes. This was not listed as a compliance issue and the
Town of Clayton has provided checks and balances to insure proper lab compliance in the
future.

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF BRIDGETON
Part B - Annual Comaiance Statement:
Facility was compliant during calendar year 2022 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. El Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .l 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T. I 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
. f
Signature of Preparer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL LANDS APPLICATION CERTIFICATION FORM
TOWN OF BEULAVILLE
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2022 with all conditions of the Iand application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. C) Yes Cj No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and line was applied (if needed) to achieve a soil pII of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T. 1 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .I l I 1 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the pernit.
1.2) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
.fart C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
w va j
Signature f Prepafer* Date
(if dif ent from Permittee)
Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF CLAYTON
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2022 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. El Yes p No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
(,(J� 2/10/23
Signature of Prepare * Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF IMNAINSVILLE
Pail B - Annual Compiance Statement:
Facility- vas compliant during calendar year 2022 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. El Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites-
2) Soil pH was adjusted as specified in the permit and time was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was perfonned and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T. 1 105(b) (applicable to 40 CFR Par 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .l 1 1 1 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
1 1) Veuetative cover was maintained and proper crop management was perfonned on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
_Part C - Certification:
"I certify, under penalty of la;,-, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Signature' of Preparer" J- Date
(if different fromn Pernnittee)
F'reoarer is defined in 40 CFR Pali 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL LAND APPLICATION GERTIFICATION FORM
TOWN OF MAYSVILLE
P t tial ca miamn%§biment
Facility Was compliant during calendar year 2022 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. Cl Yes El No
If no please, provide m written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Cq-4yresiduals approved for this permit were applied to the permitted sites.
2) Soil pRwas adjusted as specified in the pea nit and lime was applied (if needed) to achieve a soil pll of at least 6.0 or
thelwt spowfied in the permit.
3) Annual soils analysis wereperformed on each site receiving residuals during the past calendar year and three (3) copies
of.laboratory results are attached.
4) Ammsi TCI.P 4talyma (iftcgwred) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accor-lauce with the permit and reported during the year as required and three
(3) copies of certified iaboratoxry, results are attached.
6) The facititlrtliii:uot exceed Aria+ of the Pollutant Concentration Limits in 1 SA NCAC 02T .1105(a) or the Pollutant
Loading Rates- in I SA NCAC ORT .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All :gencral requirements in as specified in the Land Application Pemvt were complied with (applicable to 40 CFR Part
503 =guktied facilities)_
8) All mordtoringand reporitag req*-ements in 13A NCAC 02T .1111 were complied with (applicable to 40 CFR
raft M Vegulatvd i'aeilides).
9) All opwWow and waiateaawr, rcquireme= in the permit were complied with or, in the case of a deviation, prior
vAmization was roc4verl.from the Division of Water Quality.
10) No contravention of Ground `Water Quality Standards ow=rd at a monitoring well or explanations of violations are
aftachc i to inaladri appropriate actions and Actions.
11): Vrsctadve oover was maintained and proper crop management was performed on each site recevng residuals, as
spwi$ed in tbcep=nii.
12) No tlwfl' of residuals from the application sites onto adjacent: property or nmrby surface waters has occurred.
M) All buffer roquircments as specified on the permit w=snaintained daring each application of residuals.
R t atIon.
'Teertify, under penalty of law, that the above information is, to the best of my lsmowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for steipxnitting fa'ise Information, including the
Possibility of fines and imprisonment for knowing violations."
r
S reofPreparer* Date
if different fromPerrnittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 06)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF ROSE HILL
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2022 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. p Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Signature of Preparer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
SWANSBORO WWTP
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2022 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. p Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T . 1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1 111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
2/21 /23
Signature of Preparer* // U Date
(if different from Permittee) (�
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
SOUTHWEST PLANTATION
Part B - Annual Comniance Statement:
Facility was compliant during calendar year 2022 with all conditions of the laud application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. a Yes C] No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 5.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
b) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T. I 111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit,
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete.;ware that there are significant penalties for submitting false information, including the
possibility of f es nd imprisonment for knowing violations."
Signat of r
(if d' erent from Permittee)
* P parer is defined in 410 CFR Part 503.9 (r) and 15A NCAC 02T .l 102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF WALLACE
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2022 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. El Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the pen -nit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
42 ,Z -2023
Si ature ofPreparer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503,9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF WARSAW
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2022 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. El Yes p No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites,
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T A 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1 111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of flues and„imprisonment for knowing violations."
Sinnatfire of
Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

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ANNUAL METALS FIELD LOADING SUMMARY FORMS

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #.
Operator:
Acres Used:
Triple S Farms Total Dry Tons Applied (Annual):
WQ0030998 Cation Exchange Capacity (non 503 only):
Eric Smith Owner: Eric Smith Predominant Soil Series
36 Acres Permitted: 36 Site #: I Field #:
144.05
n/a
NoA
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
C122-054-00122022.00308BL2022.11'_WL2-2022.C222.t294r2ll.t'lo.ira»J91"1Un v_) 113 ue AInie1vvY�Y,.•
Sample
��
orCom-
polite
2122/22
115/22
6121/22
414/22
6/27/22
6,!27/22
9/27/22
7/12/22
1IlIV22
7/6122
I1/7t22
Date
% Solids
1.89
2.71
2.49
2.53
1.64
1.64
2.44
2.52
3.31
1.06
1.93
Arsenic
23.80
30.40
18.90
20.80
29.40
29.40
20.00
25.10
14.70
22.80
20.00
Cadmium
4.76
30.40
18.90
20.80
5.88
5.88
4.00
20.60
14.70
22.80
4.00
Chromium
11.90
44.90
21.30
23.40
16.90
16.90
24.20
25.30
26.60
22.80
23.00
Copper
100.00
987.00
434.00
588.001
170.00
170.00
165.00
632.00
589.00
586.00
142.00
Lead
14.30
42.60
18.90
20.80
1 17.60
17.60
12.00
25.00
28.50
22.80
12.00
Mercury
0.69
0.96
1.31
0.74
8.12
8.12
6.08
0.91
0.73
1.70
6.24
Molyb-
denum
11.90
30.40
18.90
20.80
14.70
14.70
10.00
20.60
14.70
22. 80
10.00
Nickel
11.90
30.40
18.90
20.80
14.70
14.70
11.30
20.60
15.50
22.80
12.60
Selenium
23.80
30.40
18.90
20.80
29AO
29.40
20.00
20.60
14.70
22.80
20.00
Zinc
389.00
1710.00
1330.00
1080.00
700.00
700.001
772.00
1170.001
1050.00
1761.00
652.00
Total
Phos-
24,700
26,400
15,200
26,900
30,100
30,100
25,600
22,000
19,900
16,300
24,600
oruS
Annual heavy Metal Field Loadings (Calculated in lbs/acre):
�e
� o
� �
O
0
0.67
0.32
0.20
0.81
0.03
0.25
0.51
0.70
0.18
0.08
0.24
W
Arsenic
0.03
0.02
0.01
0.03
0.00
0.01
1 0.02
0.04
0.011
0.00
0.01
1
0.18
Cadmium
0.01
0.02
0.01
0.03
0.00
0.00
0.00
0.03
0.01
0.00
0.00
0.11
Ehromium
0.02
0.03
0.01
0.04
0.00
0.01
0.02
0.04
0.01
0.00
0.01
0.19
Copper
0.13
0.63
0.18
0.95
0.01
0.09
0.17
0.89
0.22
0.09
0.07
3.43
Lead
0.02
0.03
0.01
0.03
0.00
0.01
0.01
0.04
0.01
0.00
0.01
0.17
Mercury
0.00
0.00
0.00
0.00
0.00
0.00
0.01
0.00
0.00
0.00
0.00
0.02
Molyb-
denum
0.02
0.02
0.01
0.03
0.00
0.01
0.01
0.03
0.01
0.00
0.00
0.14
Nickel
0.02
0.02
0.01
0.03
0.00
0.01
0.01
0.03
0.01
0.00
0.01
0.14
Selenium
0.03
0.02
0.01
0.03
0.00
0.01
0.02
0.03
0.01
0.00
0.01
0.18
Zinc
0.52
1.10
0.54
1.75
0.05
0.35
0.78
1.64
0.39
0.12
0.31
7.55
Total
Phos-
32.98
16.92
6.23
43.56
2.06
15.06
26.01
30.81
7.32
2.64
11.87
195.46
horus
1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties fqp submitting false information, including the possibili off fin s and imprisonment for knowing violations"
Cp? / j
Signature of Land Applier IDate
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 70.33
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series FoA
Acres Used: 12.6 Acres Permitted: 12.6 Site #: t Field #: 2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
CI 22-054-0012 2-179-W02 MV 2022-10 SWP 2012: BL 2022-1 I C3 22 271-I WL 3 202
Sample
2-l.
C4 22-3124
C4 22-312Ya
or Com-
posite
2122/22
6/27122
6/2/22
2/28/22
6/2 1/22
9/27/22
7112/22
1 I/7l22
1117/22
Date
% Solids
1.89
1.64
0.48
1.72
2.49
2.44
2.52
1.93
1.93
Arsenic
23.80
29.40
1 117.00
29.26-1
18.90
20.00
25.10
20.00
1 20.00
Cadmium
4.76
5.88
38.80
29.20
18.90
4.00
20.60
4.00
4.00
Chromium
11.90
16.90
38.80
29.20
21.30
24.20
25.30
23.00
23.00
Copper
100.00
170.00
842.00
200.00
434.00
165.00
632.00
142.00
142.00
Lead
14.30
17.60
38.80
29.20
18.90
12.00
25.00
12.00
12.00
Mercury
0.68
8.12
3.48
1.03
1.31
6.08
0.91
6.24
6.24
denum
deflum
11.90
14.70
0.00
29.20
18.90
10.00
20.60
10.00
10.00
Nickel
11.90
14.70
38.80
29.20
18.90
11.30
20.60
12.60
12.60
Selenium 1
23.80
29.40
38.80
29.20
18.90
20.00
20.60
20.00
20.00
Zinc
389.00
700.00
1420.00
1050.00
1330.00
772.00
1170.00
652.00
652.00
Total
Phos-
24,700
30,100
647
698
15,200
25,600
22,000
24,600
24,600
horus
A ��.._t
1T__ _ w.r
_a_• r.
_
azeavy iyaetai rieru J oautngs (calculated to
L�
E
0
.>
C `
D
0.37
1.01
0.06
0.07
0.73
1.26
1.40
0.08
0.61
o
FE
V1
Arsenic
0.02
0.06
0.01
0.00
0.03
0.05
0.07
0.00
0.02
0.27
Cadmium
0.00
0.01
0.00
0.00
T 0.03
0.01
0.06
0.00
0.00
0.12
Chromiuir
0.01
0.03
0.00
0.00
0.03
0.06
0.07
0.00
0.03
0.25
Copper
0.07
0.34
0.10
0.03
1 0.63
0.41
1.77
0.02
0.17
3.56
Lead
0.01
0.04
0.00
0.00
0.03
0.03
0.07
0.00
0.01
0.20
Mercury
0.00
0.02
0.00
0.00
0.00
0.02
0.00
0.00
0.01
0.05
Malyb-
denum
0.01
0.03
0.00
0.00
0.03
0.03
0.06
0.00
0.01
0.17
Nickel
0.01
0.03
0.00
0.00
0.03
0.03
0.06
0.00
0.02
0.18
Selenium
0.02
0.06
0.00
0.00
1 0.03
0.05
0.06
0.00
0.02
0.25
Zinc
0.29
1.41
0.17
0.14
1.93
1.94
3.28
0.10
0.80
10.06
Total
Phos-
18.49
60.62
0.08
0.10
22.05
64.37
61.61
3.77
30.15
261.23
horus
for
a ce
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 50.91
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series FoA
Acres Used: 14 Acres Permitted: 14 Site #: I Field #: 3A
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
C122-054-00122022-11184 M22.179.0r127_7na _1or1ene vn ] 1n19 -.
--
Sample
-
-- -- -
or Com-
posite
2/22t22
6/15122
6/27/22
9/27/22
1/4!22
7/12122
1/4/22
Date
%Solids
1.89
2.10
1.64
2.44
0.44
2.52
0.44
Arsenic
23.80
12.30
29.40
20.00
2.50
25.10
2.50
Cadmium
4.76
12.30
5.88
4.00
1.30
20.60
1.30
Chromium
11.90
18.20
16.90
24.20
18.00
25.30
18.00
Copper
100.00
248.00
170.00
165.00
386.00
632.00
1 386.00
Lead
14.30
25.40
17.60
12.00
12.00
25.00
12.00
Mercury
0.68
0.91
8.12
6.08
0.25
0.91
0.25
Molyb-
hum
11.90
15.10
14.70
10.00
5.00
20.60
5.00
Nickel
11.90
12.30
14.70
11.30
12.00
20.60
12.00
Selenium
23.80
12.30
29.40
20.00
5.00
20.60
5.00
Zinc
389.00
681.00
700.00
772.00
2767.00
1170.00
2767.00
Total
Phos-
24,700
11.600
30,100
25,600
15,640
22,000
15,640
horus
heavy ivierat rimy Loathes (Calculated in lWarrel!
K y
n,a
a
0.71
0.26
0.73
1.39
0.02
0.50
0.02
H
m
Arsenic
0.03
0.01
0.04
0.06
0.00
0.02
0.00
0.16
Cadmium
0.01
0.01
0.01
0.01
0.00
0.02
0.00
0.05
Chromium
0.02
0.01
0.02
0.07
0.00
0.03
0.00
0.15
Copper
0.14
0.13
0.25
0.46
0.02
0.63
0.02
1.64
Lead
0.02
0.01
0.03
0.03
0.00
0.02
0.00
0.12
Mercury
0.00
0.00
0.01
0.02
0.00
0.00
0.00
0.03
Molyb-
denum
0.02
0.01
0.02
0.03
0.00
0.02
0.00
0.09
Nickel
0.02
0.01
0.02
0.03
0.00
0.02
0.00
0.10
Selenium
0.03
0.01
0.04
0.06
0.00
0.02
0.00
0.16
Zinc
0.55
0.36
1.02
2.15
0.14
1.16
0.13
5.51
Total
Phos-
34.95
6.09
43.99
71.26
0.78
21.79
0.74
179.61
horus
i cernry, under penalty of taw, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant pe es fo submitting false information, including the possibilityof fi es and imprisonment for knowing violations"
Signature of Land Applier to
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 76.58
Permit M WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series FoA
Acres Used: 19.6 Acres Permitted: 19.6 Site #: I Field #: 345
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
WL 1-2022,00308 2022-11184 C1 22-054-a Ci 2i_0id.( RFr.dene re »_a n t at,n„
Sample
-- '- -
- - -
-
L 44-1
orCom-
posite
1/5/22
6/15/22
V22122
2/22122
1/4122
11/7/22
6/21122
6!2/22
Date
% Solids
2.71
2.10
1.89
1.89
0.44
1.93
2.49
0.48
Arsenic
30.40
12.30
23.80
23.80
2.50
20.00
18.90
117.00
Cadmium
30.40
12.30
4.76
4.76
1.30
4.00
18.90
38.80
Chromium
44.90
18.20
11.90
11.90
18.00
23.00
21.30
38.80
Copper
987.00
248.00
100.00
100.00
386.00
142.00
434.00
842.00
Lead
42.60
25.40
14.30
14.30
12.00
I2.00
18.90
38.80
Mercury
0.96
0.91
0.68
0.68
0.25
6.24
1.31
3.48
Molyb-
denum
30.40
15.10
11.90
11.90
5.00
10.00
18.90
0.00
Nickel
30.40
12.30
11.90
11.90
12.00
12.60
18.90
38.80
Selenium
30.40
12.30
23.80
23.80
5.00
20.00
18.90
38.80
Zinc
1710.00
681.00
389.00
389.00
2767.00
652.00
1330.00
1420.00
Total
Phos-
26,400
11,600
24,700
24,700
15,640
24,600
15,200
647
horus
A-uni navy lvi ai rietn Loaatngs (Calculated in lbs/acre):
;t y
` v
0.87
0.47
0.22
0.39
0.02
1.70
0.21
0.04
o• i
:'
Arsenic
0.05
0.01
0.01
0.02
0.00
0.07
0.01
0.01
1
0.18
Cadmium
0.05
0.01
0.00
0.00
0.00
0.01
0.01
0.00
0.09
Eh-romiurr
0.08
0.02
0.01
0.01
0.00
0.08
0.01
0.00
0.20
Copper
1.71
0.23
0.04
0.08
0.01
0.48
0.18
0.06
F
2.81
Lead
0.07
0.02
0.01
0.01
0.00
0.04
0.01
0.00
0.17
Mercury
0.00
0.00
0.00
0.00
0.00
0.02
0.00
0.00
0.03
Molyb-
denum
0.05
0.01
0.01
0.01
0.00
0.03
0.01
0.00
0.12
Nickel
0.05
0.01
0.01
0.01
0.00
0.04
0.01
0.00
0.13
Selenium
0.05
0.01
0.01
0.02
0.00
0.07
0.01
0.00
0.17
Zinc
2.96
0.65
0.17
0.30
0.10
2.22
0.56
0.10
7.06
Total
Phos-
45.71
10.99
10.70
19.02
0.56
83.62
6.44
0.05
177.08
horus
I cermy, under penalty of taw, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties f submitting false information, including the possibility f fin and imprisonment for knowing violations"
Signature of Land Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 45.65
Permit M W00030998 Cation Exchange Capacity (non 503 only): Na
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series GoA
Acres Used: 17.3 Acres Permitted: 17.3 Site #: 1 Field M 6
Residual Analysis Data (Heavy Metals and Total Phosphorus use mglkg, % Solids use Raw Percent #)•
WS 2022-11194 2072.175F7 re II -'I 171i
ample
- -
or Com-
posite
6115/22
917/22
11/7/22
Date
% Solids
2.10
1.94
1.93
Arsenic
12.30
16.50
20.00
Cadmium
12.30
16.50
4.00
Chromium
18.20
16.50
23.00
Copper
248.00
281.00
142.00
Lead
25.40
16.50
12,00
Mercury
0.91
0.99
6.24
M
15.10
16.50
10.00
um n
um
Nickel
12.30
16.50
12.60
Seleniuml
12.30
16.50
20.00
681.00
3670.00
652.00
L
11,600
15,900
24,600
tlAuual IICav_y lvlcral Field Loannivs ft 111C711atPd in Iha/aural-
o
rr1 E
H
O
0.76
1.41
0.47
Arsenic
0.02
0.05
0.02
0.08
Cadmium
0.02
0.05
0.00
Chromium
0.03
0.05
0.02
0.07
0.10
Copper
0.38
0.79
0.13
Lead
0.04
0.05
0.01
1.30
Mercury
0.00
0.00
0.01
0.10
Molyb-
0.01
denum
0.02
0.05
0.01
0.08
Nickel
0.02
0.05
0.01
Selenium
0.02
0.05
0.02
0 08
0.08
Zinc
1.03
10.31
0.62
Total
11.97
Phos-
17.62
44.68
23.34
horns
85.64
«,...y, uuucr penany vt law, tnat tnts aocument was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
si ific�aat penalties forAdubmittin false information, including the possibility, of fin and imprisonment for knowing violations"
Signature of Land Applier Dat
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 40.62
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series FoA
Acres Used: 11.5 Acres Permitted: 11.5 Site #: I Field #: 7
Residual Analysis Data (Heavy Metals and Total Phosphorus use mglkg, % Solids use Raw Percent #):
CI 22-054-00122022-05935 SWa 2n71A r1 »_uo_j
Sample
- ---- -
--
or Com-
posite
2122/22
414/22
2/28122
6127/22
Date
% Solids
1.89
2.53
1.72
1.64
Arsenic
23.80
20.80
29.20
29.40
Cadmium
4.76
20.80
29.20
.5.88
Chromium
11.90
23.40
29.20
16.90
Copper
100.00
588.00
200.00
170.00
Lead
14.30
20.80
29.20
17.60
Mercury
0.68
0.74
1.03
8.12
Molyb-
denum
11.90
20.80
29.20
14.70
Nickel
11.90
20.80
29.20
14.70
Selenium
23.80
20.80
29.20
29.40
Zinc
389.00
1080.00
1050.00
700.00
Total
Phos-
24,700
26,900
698
30,100
horus
heavy Metal field Loadings (Ca
m Y
ii :0 0
p• f
7 �
0.74
1.16
0.07
1.56
ti:
Arsenic
0.04
0.05
0.00
0.09
Cadmium
0.01
0.05
0.00
0.02
0.18
0.08
Chromium
0.02
0.05
0.00
0.05
Copper
0.15
1.36
0.03
0.53
0.13
Lead
0.02
0.05
0.00
0.05
2.07
Mercury
0.00
0.00
0.00
0.03
0.13
Molyb-
0.03
denum
0.02
0.05
0.00
0.05
0.12
Nickel
0.02
0.05
0.00
0.05
Selenium
0.04
0.05
0.00
0.09
0.12
Zinc
0.57
2,50
0.16
2.19
0.18
Total
5.42
Phos-
36.47
62.26
0.10
94.00
horus
for _
192.83
e
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 139.46
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series GoA
Acres Used: 16.1 Acres Permitted: 16.1 Site #: 1 Field #: 9
Residual Analysis Data (heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
CI 22-054.nn 121w%mim Ru-m-n-m we 7R1, , - ,
--
Sample
-
- ----
or Com-
posite
2122/22
1/5/22
4/29122
6/15/22
7/12/22
Date
% Solids
1.89
2.71
28.83
2.10
2.52
Arsenic
23.80
30.40
7.92
12.30
25.10
Cadmium
4.76
30.40
3.07
12.30
20.60
Chromium
11.90
44.90
52.20
18.20
25.30
.copper
100.00
987.00
313.00
248.00
632.00
Lead
14.30
42.60
30.80
25.40
25.00
Mercury
0.68
0.96
0.55
0.91
0.91
Molyb-
denum
11.90
30.40
3.44
15.10
20.60
Nickel
11.90
30.40
8.20
12.30
20.00
Selenium
23.80
30.40
5.06
I2.30
20.60
Zinc
389.00
1710.00
828.00
681.00
1170.00
Total
Phos-
24,700
26,400
20,600
11,600
22,000
horus
-a. y a.aeaaa ramu i.unuanas n_9acuaarpn an ahe
o
m .ya E
�a
0.79
1.64
4.81
0.87
0.55
�
o
Arsenic
0.04
0.10
0.08
0.02
1 0.03
1
0.26
Cadmium
0.01
0.10
0.03
0.02
0.02
Chromiurr
0.02
0.15
0.50
0.03
0.03
0.18
Copper
0.16
3.25
3.01
0.43
0.69
0.73
Lead
0.02
0.14
0.30
0.04
0.03
7.54
Mercury
0.00
0.00
0.01
0.00
0.00
0.53
Molyb-
0.01
d num
0.02
0.10
0.03
0.03
0.02
0.20
Nickel
0.02
0.10
0.08
0.02
0.02
Selenium
0.04
0.10
0.05
0.02
0.02
0.24
Zinc
0.62
5.62
7.96
1.19
1.28
0.23
16.67
Lh
39.07
86.81
198.13
20.19
24.11368.31
ur
uuuca IMUnaly ul law, tnat inis aocument was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties fo submitting false Information, including the possibility, of fin and imprisonment for knowing violations"
3
Signature of Land Applier Da
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 32.60
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soll Series NoA
Acres Used: 12.8 Acres Permitted: 12.8 Site #: 1 Field #: 10
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent t):
CI 22-054-00122022-10200 BE1440A BL2022-11 BL2022-11
amp er
Com-
posite
Io
2122/22
612122
1/4122
6121122
6121122
Date
% Solids
1.89
0.48
0.44
2.49
2.49
Arsenic
23.80
117.001
2.50
18.90
18.90
Cadmium
4.76
38.80
1.30
18.90
18.90
Chromium
11.90
38.80
18.00
21.30
21.30
-Copper
100.00
842.00
396.00
434.00
434.00
Lead
14.30
38.80
12.00
18.90
18.90
Mercury
0.68
3.48
0.25
1.31
1.31
Molyb-
denum
11.90
0.00
5.00
18.90
18.90
Nickel
11.90
38.80
12.00
18.90
18.90
Selenium
23.80
38.80
5.00
18.90
18.90
Zinc
389.00
1420.00
2767.00
133Q.00
1330.00
Total
Phos-
24,700
647
15,640
15,200
15,200
horus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
3 d
2.03
0.06
0.03
0.10
0.34
Arsenic
0.10
0.01
0.00
0.00
0.01
0.13
Cadmium
0.02
0.00
0.00
0.00
0.01
0.04
Chromium
0.05
0.00
0.00
0.00
0.01
Copper
0.41
0.09
0.02
0.08
0.30
0.07
Lead
0.06
0.00
0.00
0.00
0.01
0.90
Mercury
0.00
0.00
0.00
0.00
0.00
0.08
Molyb-
0.00
denum
0.05
0.00
0.00
0.00
0.01
0.07
Nickel
0.05
0.00
0.00
0.00
0.01
Selenium
0.10
0.00
0.00
0.00
0.01
0.07
Zinc
I.58
0.16
0.14
0.26
1 0.91
0.12
Total
3.04
Phos-
100.14
0.07
0.81
2.96
10.36
114.34
horus
. «. u.y, anger penalty of raw, Mat MIS aocument was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
A ificant pe ]ties r sub 'tting false information, Including the possibilliityp
of tin and Imprisonment for knowing violations"
- oC
Signature of Land Applier Dat
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)

ANNUAL LAND APPLICATION FIELD SUMMARY FORMS

ANNUAL LAND APPLICATION FIELD SUMMARY FORMS LEGEND
All nutrients and metals concentrations listed on the following annual land application field
summary forms are on a pound per acre basis.
The following is a list of symbols and abbreviations used on the field loading rate report:
%TS — Percent Solids
DT/ACRE — Dry Tons Applied per Acre
lb/ac — Pounds per Acre
Metals (lbs/ac)
As —
Arsenic
Cd —
Cadmium
Cr — Chromium
Cu —
Copper
Pb —
Lead
Hg
— Mercury
Mo
— Molybdenum
Ni —
Nickel
Se —
Selenium
Zn —
Zinc
Nutrients (lbs/ac)
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P — Phosphorus
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RESIDUAL ANALYSIS LAB SHEETS

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Town of Bridgeton
Bridgeton WWTP
Havelock, North Carolina
Triple S Farms and Cleaning, Inc.
Wastewater Treatment Plant
BEI-440A
1/4/2022 Type of Stabilization: Lime
1/31/2022
Annual 2022
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
0.440
Nitrogen (TKN)*
6.515
65,150.00
Phosphorus
1.564
15,640.00
Potassium
0.416
4,156.00
Sulfur
Calcium
2.874
28,741.00
Magnesium
0.370
3,698.00
Sodium
1.454
14,544.00
Iron
---
Aluminum
---
3935.00
Manganese
---
Copper
---
386.00
1,500
Zinc
---
2767.00
2,800
Ammonia Nitrogen*
0.013
131.40
Nitrate N / Nitrite N*
---
230.90
Cadmium
---
1.30
39
Chromium
---
18.00
1,200
Nickel
---
12.00
420
Lead
---
12.00
300
Arsenic
---
2.50
41
Mercury
---
0.25
17
Selenium
---
5.00
100
pH
7.100
Calcium Carbonate Eq. (est)
0.00
Organic Nitrogen
6.502
65,018.60
Molybdenum
---
5.00
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Wastewater Treatment Plant
Bridgeton WWTP
Havelock, North Carolina
Triple S Farms and Cleaning, Inc.
Annual 2022
Date Reported: 1/31/2022 Report No: BEI-440A
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
39.604
PAN Inj.
39.736
P
31.280
K
8.312
Lime (estimated)
0.000
Secondary Nutrients
Calcium
57.482
Magnesium
7.396
Sodium
29.088
SAR
1.420
Chloride
0.000
Iron
0.000
Alumium
7.870
Manganese
0.000
Boron
0.000
Sulfur
0.000
Residual Nitrogen Calculation
Year Min Rate PAN #/Acre
% Solids
0.44
pH
7.100
Min Rate
0.300
Metals
Arsenic
0.005
Cadmium
0.003
Chromium
0.036
Copper
0.772
Lead
0.024
Mercury
0.001
Molybdenum
0.010
Nickel
0.024
Seleniun
0.010
Zinc
5.534
2019
2020
2021
2022
0.30
39.01
2023
0.15
13.65
2024
0.08
5.80
2025
0.04
2.68
2026
2027
2028
2029

Environment 1, Incorporated
P.O. BOX 7085,114 OAKMONT DRIVE
GREENVILLE, N.C. 27835-7085
TOWN OF BRIDGETON
HYDRO SERVICES & CONSULTING
MR. KEVIN MULLINEAUX
P.O. BOX 317
HAVELOCK, NC 28532
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), nsg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), nsg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Sodium Adsorption Ratio (calc)
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
7.1
01/05/22
CAW
4500HB-11
3935
01/18/22
LFJ
EPA200.7
< 2.5
01/21/22
MTM
3113B-04
28741
01/18/22
LFJ
EPA200.7
1.3
01/19/22
MTM
3113B-04
386
01/18/22
LFJ
EPA200.7
18
01/18/22
LFJ
EPA200.7
12
01/19/22
MTM
3113B-04
3698
01/18/22
LFJ
EPA200.7
0.25
01/19/22
MTM
EPA7471B
12
01/18/22
LFJ
EPA200.7
4156
01/18/22
LFJ
EPA200.7
< 5.0
01/18/22
MTM
3113B-04
14544
01/18/22
LFJ
EPA200.7
2767
01/18/22
LFJ
EPA200.7
21.5
0.44
01/05/22
JMS
2540G-15
c 65150
01/12/22
TRJ
351.2 112-93
c 131.4
01/10/22
BMD
350.1 112-93
c 15640
01/12/22
BMD
365.4-74
c 230.9
01/10/22
TRJ
353.2 112-93
< 5.0
01/18/22
LFJ
EPA200.7
Drinking water IDi 37715
Wastewater IDe to
PHONE [phone]
FAX [phone]
ID#: 440 A
DATE COLLECTED: 01/04/22
DATE REPORTED : 01/31/22
REVIEW BY / 1)
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Town of Beulaville
Beulaville WWTP
Beulaville, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
BL 2022-11566
6/21/2022
7/12/2022
Annual 2022
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
2.490
Nitrogen (TKN)
4.850
48,500.000
Phosphorus
1.520
15,200.000
Potassium
0.502
5,020.000
Sulfur
0.000
Calcium
2.180
21,800.000
Magnesium
0.198
1,980.000
Sodium
0.502
5,020.000
Iron
---
Aluminum
---
4,980.000
Manganese
---
Copper
---
434.000
1,500
Zinc
---
1,330.000
2,800
Ammonia Nitrogen
0.000
4.020
Nitrate N / Nitrite N
---
15,600.000
Cadmium
---
18.900
85
Chromium
---
21.300
1,200
Nickel
---
18.900
420
Lead
---
18.900
300
Arsenic
---
18.900
75
Mercury
---
1.310
17
Selenium
---
18.900
100
pH
3.670
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
4.850
Molybdenum
---
18.900
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Wastewater Treatment Plant
Beulaville WWTP
Beulaville, North Carolina
Triple S Farms & Cleaning, Inc
Annual 2022
Date Reported: 7/12/2022 Report No: BL 2022-11566
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
60.302
PAN Inj.
60.306
P
30.400
K
10.040
Lime (estimated)
0.000
Secondary Nutrients
Calcium
43.600
Magnesium
3.960
Sodium
10.040
SAR
1.375
Chloride
0.000
Iron
0.000
Alumium
9.960
Manganese
0.000
Boron
0.000
Sulfur
0.000
Physical Characteristics
% Solids
2.49
pH
3.670
Min Rate
0.300
Metals
Arsenic
0.038
Cadmium
0.038
Chromium
0.043
Copper
0.868
Lead
0.038
Mercury
0.003
Molybdenum
0.038
Nickel
0.038
Seleniun
0.038
Zinc
2.660

r I gin'
ANALYTICAL & CONSULTING CHEMISTS
]Environmental Chemists, Inc.
660"''Win6mi i kk`ay, kVihningtmr1, ?4IC'18405 - 9103910223, Lzo Fat
710 boo-1-sertm r1 Rmad, t4anteo, NC 279;-1 b c�
fl, fit: `'t.t-Y1 a�34*, y252.I,1 702',��;�.." i 3t)J},.,, ..'; n
2E" h Wilmington Highway, iiick-50"Vi -!0...
� ,
ifl.f,�i�YEA"ti 3i7t1I11Ciitiil:,�lErllii'IS.CU7?l
Town of Beulaville Date of Report: Jul 12, 2022
PG Box 130 Customer Piz #:
Beulaville NC 28518 Customer ID: 08100015
Attention: Angie Miller Report #: 2022-11566
Project ID: Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-28067 Site: Sludge 6/21/2022 9,00 AM Solid/Sludge Angie Miller
Test Method Results Date Analyzed
Sludge Residuals
Aluminum
EPA 2007.Rev 44 1994
4980mg/kg
07/08/2022
Arsenic
EPA 200 7, Rev 4 4, 1994
<18.g mgikg
07108/2022
Cadmium
EPA 200.7, Rev. 4 4. 1994
<18.9 mglkg
07/08/2022
Calcium
EPA 200,7, Rev 4 4, 1994
21800 mg/kg
07/08/2022
Chromium
EPA 200.7, Rev 4 4, 1994
2 1. 3 mg/kg
07/08/2022
Copper
EPA 200 7, Rev 4 4. 1594
434 mg/kg
07108/2022
Lead
EPA 200 7. Rev 4 4, 1994
< 18.9 mglkg
07l08/2022
Magnesium
EPA 200 :. Rev 1! 4, 1994
1980 mg/kg
07/08/2022
Molybdenum
EPA 200 ',,Rev. 4 4, 1994
<18.9 mg/kg
07108/2022
Nickel
EPA 20U. Rev. 4.4, 1%4
<18.9 mg/kg
07/08/2022
Potassium
EPA 20U.7, Rev_ 4.4, 1994
5020 mg/kq
07/08/2022
Selenium
EFA 200.7, Rev, 4.4, 199R
<18 9 mg/kg
07/08/2022
Sodium
EPA 200.7, Rev, 4.4, 1994
5020 mg/kg
07/08/2022
Zinc
EPA 200.7, Rev. 4A. 1994
1330 mglkg
0710812022
Nitrate+Nitrite-Nitrogen
EPA 353.2
15600 mg/kg
06/23/2022
Total Solids (%)
$M 2540 8
2.49 %
06/24/2022
Ammonia Nitrogen
SIA 4500 NH3 C-2r11
<4.02 matkg
06/2212022
Total Kieldahl Nitrogen (TKN)
SIM 4500 Norg 13-2011
48500 mg/kg
06122/2022
Total Phosphorus
SM 4600 P (F-H)2011
15200 mg/kg
06/28/2022
pH SW 846 Method 9045D
Estimate result is outside calibration range.
3.67 est units
06/2812022
Mercury
sW-046 7471 9
1.31 mg/kg
06/22/2022
Comment: Results, except pH,
reported on a dry weight basis
pl-1 reported on an as received basis.
Reviewed by:

Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill wily
Wilmington, NC 28405
Sample Receipt Checklist 910-392.0223
Date: 40�1 QA_ Report Number:
c4_a _A(5_� �p
Receipt pf so - -pie: ECHEM Pic
0 YES 13 N5— A
13 YES A _INV�J A
Client Deliver
I. Were
2. If cuss
0 1UPS11_ - _Fed `Ex0 _other —[]-
sent on the cooler?
seals were present were the int
uriginzo temperature upon receipt
#
y %-%/ 1.1111JIUKL' Corrected temperature upon receipt.
How temperature taken.
El Temperature blank ir Against Battles
.. . .... . ..... 11.19
IR Gun ID: Thomas Traceable S/N 192511657 :1 R Gun Correction Factor -C. 0.0
—NO
YES7Td_
3. If temperature of—co—olerexcCleded VC, was Project Mgr./QA notified?
_procedures
NO
YES 13 NO
4. Were proper custody (relinquislied/received) followed?
-
S. Were sample ID's listed an tile CAC?
YES Cl NO
6. Were samples 10 s listed on sample containers?
YES S_C7 No
YES
7. Were collection date an d time listed on the Coc?
U NO
8, Were tests to be VEsrtormLd listed on the Coo
YES ii—NO
9. Did samples arrive in - proper containers for each test?
—
�J YES N I &In
10. Did s
­.�
7 RMPIP5 arrivP in Priod condition for each test?
t
----------------
iZ YES_JC3 NO 12. Wert., samples received, wi thi 11 proper holding
yr" M time for requested tests?
YFS
1IVO
W'
13. Were acid preserved samples received at B PH of <21?
14. Were cyanide sample.r. received at a pff
ES
0
NO
N10—
W�ri
I-S. Weresulficle samples received at a pl-I >9?
`­5T
I YES
YES
tj
_�NO
NO
16. Were NH3/TKN/ e t a chlorine re:iduaF;T�0_5 WI-I-L? �**
17. Were 5011717-1-, - —
Ifide/Cyanide received at a chlorine residual of <0.5 m1L5
YFS
13
NO
18. Were orthiophosptate samples pl_s filtered n the field witttln 15 minutes?
*1!',"_/V0l,3tJJPs am pl i checkedat time Of analysis and recorded on the benchrherq.
Bacteria samples are ch;�cked for Chlorine at time of analysis and recorded on the benchshpot,
Preservation;
Must be corn
adding (circle once};H2SO4
p
seals
leted for any samp le(s) incorrectly preserved or with h—e"ad—space)
were received incorrectly preserved and were adjusted accorditigly
HN0j 11110 NaOH
of preservation,.
If more than One Preservative is needed, notate in comments below
Notify customer unrred;atp v for Ircarrectly preserved samples. Obtain a new gI.Mp.e or
the state 1017 if-dwixted to ana yzed - by the customer.Wh) was notified, date and time,
iles Sample(s)
were received with
riqn-trp
COMMENTS:
C. OA-002 Rev 11

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Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms & Cleaning, Inc
Clayton Little Creek WRIT
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
C122-054-0012
2/22/2022
4/13/2022
1st Quarter
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
1.89
Nitrogen (TKN)
6.620
66,200.000
Phosphorus
2.470
24,700.000
Potassium
0.943
9,430.000
Sulfur
0.724
7,240.000
Calcium
0.962
9,620.000
Magnesium
0.449
4,490.000
Sodium
0.409
4,090.000
Iron
---
5.950.000
Aluminum
---
5,050.000
Manganese
---
166.000
Copper
---
100.000
1,500
Zinc
---
389.000
2,800
Ammonia Nitrogen
0.795
7,950.000
Nitrate N / Nitrite N
---
449.000
Cadmium
---
4.760
39
Chromium
---
11.900
1,200
Nickel
---
11.900
420
Lead
---
14.300
300
Arsenic
---
23.800
41
Mercury
---
0.681
17
Selenium
---
23.800
100
pH
6.400
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
5.825
Molybdenum
---
11.900
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340
* average of 7 fecal samples from 2/21/22

Wastewater Treatment Plant
Clayton Little Creek WRF
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
1st Quarter
Date Reported: 4/13/2022 Report No: Cl 22-054-0012
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
43.798
PAN Inj.
51.748
P
49.400
K
18.860
Lime (estimated)
0.000
Secondary Nutrients
Calcium
19.240
Magnesium
8.980
Sodium
8.180
SAR
1.181
Chloride
0.000
Iron
11.900
Alumium
10.100
Manganese
0.332
Boron
0.000
Sulfur
14.480
Residual Nitrogen Calculation
Year Min Rate PAN #/Acre
% Solids
1.89
pH
6.400
Min Rate
0.300
Metals
Arsenic
0.048
Cadmium
0.010
Chromium
0.024
Copper
0.200
Lead
0.029
Mercury
0.001
Molybdenum
0.024
Nickel
0.024
Seleniun
0.048
Zinc
0.778
2019
2020
2021
2022
0.30
34.95
2023
0.15
12.23
2024
0.08
5.20
2025
0.04
2.40
2026
2027
2028
2029

Waypoint
ANALYTICAL
4/4/2022
Town Of Clayton
POB 879
Clayton, NC, 27528
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Ref: Analytical Testing
Report Number: 22-081-0011
Project Description: Holding Tank
Waypoint Analytical Virginia, Inc. received sample(s) on 3/22/2022 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Yawn M t &IC,owr
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
PAIT I of R

(2)
7621 Whitepine Road, Richmond, VA 23237
Waypoint Main 804-743-9401 ° fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 22-081-0011
Client Project Description: Holding Tank
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
57235
Holding
Tank
Solids
57235
Holding
Tank
Solids
57235
Holding
Tank
Solids
57235
Holding
Tank
Solids
57235
Holding
Tank
Solids
57235
Holding
Tank
Solids
57235
Holding
Tank
Solids
03/21/2022
11:00
03/22/2022
03/21/2022
11:00
03/22/2022
03/21/2022
11:00
03/22/2022
03/21/2022
11:00
03/22/2022
03/21/2022
11:00
03/22/2022
03/21/2022
11:00
03/22/2022
03/21/2022
11:00
03/22/2022
SM-4500-NH3C
WP MTN
SM-4500-NH3C-TKN
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SW-7471B
WP MTN
9045D
WP MTN
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
D.-- 7 of 0

0
Waypoint, 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46546
Town Of Clayton Project Holding Tank Original Report Date : 04/04/2022
POg 879 Revised Report Date: 04/13/2022
Information : Received : 03/22/2022
Clayton , NC 27528
Report Number: 22-081-0011
REPORT OFANAL YSIS
Lab No : 57235
Matrix: Solids
Sample ID : Holding Tank
Sampled: 3/21/2022 11:00
Test
Results
Units
MOL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
97.9
%
0.010
1
03/24/2219:00
FMM
SM-2540G
Potassium
9430
mg/Kg - dry
476
1
03/29/22 01:22
EAL
6010D
Sulfur
7240
mg/Kg - dry
476
1
03/25/22 23:34
EAL
6010D
Calcium
9620
mg/Kg - dry
2380
1
03/25/22 23:34
EAL
6010D
Aluminum
5050
mg/Kg - dry
238
1
03/25/22 23:34
EAL
6010D
Manganese
166
mg/Kg - dry
23.8
1
03/25/22 23:34
EAL
6010D
Copper
100
mg/Kg - dry
23.8
1
03/25/22 23:34
EAL
6010D
Nickel
<11.9
mg/Kg - dry
11.9
1
03/25/22 23:34
EAL
6010D
Lead
<14.3
mg/Kg - dry
14.3
1
03/25/22 23:34
EAL
6010D
Arsenic
<23.8
mg/Kg - dry
23.8
1
03/29/22 01:22
EAL
6010D
Silver
<11.9
mg/Kg - dry
11.9
1
03/25/22 23:34
EAL
6010D
Test
Results
Units
MOL
DF
Date / Time
By
Analytical
Analyzed
Method
pH
6.4
s.u.
1
03/29/2215:33
DRS
9045D
Total Solids
2.14
%
0.010
1
03/24/22 19:00
FMM
SM-2540G
Selenium
<23.8
mg/Kg - dry
23.8
1
03/25/22 23:34
EAL
6010D
Sodium
4090
mg/Kg - dry
1190
1
03/25/22 23:34
EAL
6010D
Qualifiers/ DF Dilution Factor
MQL Method Quantitation Limit
Definitions
paaP 3 of R

Waypointo
ANALYTICAL
46546
Town Of Clayton
POB 879
Clayton , NC 27528
Report Number : 22-081-0011
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project Holding Tank
Information :
REPORT Of ANAL YSI'S
Original Report Date : 04/04/2022
Revised Report Date: 04/13/2022
Received : 03/22/2022
Lab No : 57235
Sample ID : Holding Tank
Matrix: Solids
Sampled: 3/21/2022 11:00
Total Kjeldahl Nitrogen
66200
mg/Kg - dry
11900
1
03/29/22 11:00
JPJ ;M-4500-NH3C TKP
Phosphorus
24700
mg/Kg - dry
238
1
03/25/22 23:34
EAL
6010D
Magnesium
4490
mg/Kg - dry
238
1
03/25/22 23:34
EAL
6010D
Iron
5950
mg/Kg - dry
476
1
03/25/22 23:34
EAL
6010D
Zinc
389
mg/Kg - dry
59.5
1
03/25/22 23:34
EAL
6010D
Ammonia Nitrogen
7950
mg/Kg - dry
4760
1
03/29/22 15:00
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
449
mg/Kg - dry
227
1
03/29/22 13:57
ZBD
4500NO3F-2011
Cadmium
<4.76
mg/Kg - dry
4.76
1
03/25/22 23:34
EAL
6010D
Chromium
<11.9
mg/Kg - dry
11.9
1
03/25/22 23:34
EAL
6010D
Mercury
<0.681
mg/Kg - dry
0.681
1
03/30/22 12:19
ZMT
SW-7471B
Molybdenum
<11.9
mg/Kg - dry
11.9
1
03/25/22 23:34
EAL
6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

Waypdlont(2)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 (Fax [phone]
www.waypointanalytical.com
Client: Town Of Clayton CASE NARRATIVE
Project: Holding Tank
Lab Report Number: 22-081-0011
Date: 4/4/2022
Metals Analysis Method 6010D
Sample 76148 (Teanet Field 2)
Analyte: Aluminum
QC Batch No: 1-607591 /L606811
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 76148 (Teanet Field 2)
Analyte: Arsenic
QC Batch No: L607297/1-606811
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 76148 (Teanet Field 2)
Analyte: Iron
QC Batch No: 1-607591/1-606811
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 76148 (Teanet Field 2)
Analyte: Potassium
QC Batch No: 1-607591/1-606811
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 76148 (Teanet Field 2)
Analyte: Magnesium
QC Batch No: L607297/L606811
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 76148 (Teanet Field 2)
Analyte: Manganese
QC Batch No: 1-607591/1-606811
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 76148 (Teanet Field 2)
Analyte: Phosphorus
QC Batch No: 1-607297/1-606811
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 76148 (Teanet Field 2)

Waypoint
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 (Fax [phone]
www.waypointanalytical.com
Analyte: Lead
QC Batch No: L607297/L606811
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 76148 (Teanet Field 2)
Analyte: Selenium
QC Batch No: L607297/1-606811
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.

Waypoint
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46546
Customer Name: Town Of Clayton
Report Number: 22-081-0011
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
UPS 0 Client 0 Courier
Other
Thermometer ID:��
Shipping container/cooler uncompromised?
# Yes
0 No
Number of coolers/boxes received
F 1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
0 Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
Yes
0 No
COC properly completed
Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
High concentration container (48 hr) [_ Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments:
0 Yes * No
Signature: jBrandi Watson Date & Time: b3/22/2022 14:03:38

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Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms & Cleaning, Inc
Clayton Little Creek WRF
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
C2 22-179-0002
6/27/2022
7/7/2022
2nd Quarter
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids *
1.64
Nitrogen (TKN)
8.000
80,000.000
Phosphorus
3.010
30,100.000
Potassium
0.882
8,820.000
Sulfur
0.000
Calcium
1.640
16,400.000
Magnesium
0.574
5,740.000
Sodium
0.512
5,120.000
Iron
---
Aluminum
---
9,760.000
Manganese
---
Copper
---
170.000
1,500
Zinc
---
700.000
2,800
Ammonia Nitrogen
0.647
6,470.000
Nitrate N / Nitrite N
---
576.000
Cadmium
---
5.880
39
Chromium
---
16.900
1,200
Nickel
---
14.700
420
Lead
---
17.600
300
Arsenic
---
29.400
41
Mercury
---
8.120
17
Selenium
---
29.400
100
pH
6.300
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
7.353
Molybdenum
---
14.700
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340
* average of 7 fecal samples from 7/8/22

Wastewater Treatment Plant
Clayton Little Creek WRF
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
2nd Quarter
Date Reported: 7/7/2022 Report No: C2 22-179-0002
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
51.740
PAN Inj.
58.210
P
60.200
K
17.640
Lime (estimated)
0.000
Secondary Nutrients
Calcium
32.800
Magnesium
11.480
Sodium
10.240
SAR
1.117
Chloride
0.000
Iron
0.000
Alumium
19.520
Manganese
0.000
Boron
0.000
Sulfur
0.000
Residual Nitrogen Calculation
Year Min Rate PAN #/Acre
% Solids
1.64
pH
6.300
Min Rate
0.300
Metals
Arsenic
0.059
Cadmium
0.012
Chromium
0.034
Copper
0.340
Lead
0.035
Mercury
0.016
Molybdenum
0.029
Nickel
0.029
Seleniun
0.059
Zinc
1.400
2019
2020
2021
2022
0.30
44.12
2023
0.15
15.44
2024
0.08
6.56
2025
0.04
3.04
2026
2027
2028
2029

WayPAoint_
NALYTICAL
7/7/2022
Town Of Clayton
POB 879
Clayton, NC, 27528
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Ref: Analytical Testing
Report Number: 22-179-0002
Project Description: Town of Clayton
Waypoint Analytical Virginia, Inc. received sample(s) on 6/28/2022 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Tpwi'c M f &10, ry/
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

Waypoint.(D
ANALYTICAL
Report Number: 22-179-0002
Client Project Description: Town of Clayton
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
58403
Holding Tank
Solids
06/27/2022 11:45
06/28/2022
58403
Holding Tank
Solids
06/27/2022 11:45
06/28/2022
SM-4500-NH3C
WP MTN
58403
Holding Tank
Solids
06/27/2022 11:45
06/28/2022
9045D
WP MTN
58403
Holding Tank
Solids
06/27/2022 11:45
06/28/2022
4500NO3F-2011
WP MTN
58403
Holding Tank
Solids
06/27/2022 11:45
06/28/2022
6010D
WP MTN
58403
Holding Tank
Solids
06/27/2022 11:45
06/28/2022
SW-7471B
WP MTN
58403
Holding Tank
Solids
06/27/2022 11:45
06/28/2022
SM-4500-NH3C-TKN
WP MTN
58403
Holding Tank
Solids
06/27/2022 11:45
06/28/2022
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical -TN, Memphis, TN
Page 2 of 7

•
Waypoint.
7621 Whitepine
Road, Richmond,
VA 23237
Main 804-743-9401 ° Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
46546
Town Of Clayton
Project
Town of Clayton
POB 879
Report Date : 07/07/2022
Information :
Received : 06/28/2022
Clayton , NC 27528
T AW#
Pauric Mc Groary Ph.D., CPA
Report Number: 22-179-0002
REPORTOPANALYSIS
Agronomist
Lab No : 58403
Matrix:
Solids
Sample ID : Holding Tank
Sampled:
6/27/2022 11:45
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
98.3
%
0.010
1
07/01/2217:55
ADM
SM-254OG
Total Kjeldahl Nitrogen
80000
mg/Kg - dry
14700
1
07/06/22 11:00
JPJ ')M-4500-NH3C-TKP
Potassium
8820
mg/Kg - dry
588
1
07/05/22 16:43
TJS
6010D
Calcium
16400
mg/Kg - dry
2940
1
07/05/22 16:43
TJS
6010D
Aluminum
9760
mg/Kg - dry
294
1
07/05/22 16:43
TJS
6010D
Copper
170
mg/Kg - dry
29.4
1
07/05/22 16:43
TJS
6010D
Zinc
700
mg/Kg - dry
73.5
1
07/05/22 16:43
TJS
6010D
Nickel
<14.7
mg/Kg - dry
14.7
1
07/05/22 16:43
TJS
6010D
Arsenic
<29.4
mg/Kg - dry
29.4
1
07/05/22 16:43
TJS
6010D
Silver
<14.7
mg/Kg - dry
14.7
1
07/05/22 16:43
TJS
6010D
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Sodium Absorption Ratio
67.1
mg/Kg - dry
58.8
1
07/05/22 16:43
CALCULATION
pH
6.3
S.U.
1
07/06/2215:23
ADM
9045D
Lead
<17.6
mg/Kg - dry
17.6
1
07/05/22 16:43
TJS
6010D
Magnesium
5740
mg/Kg - dry
294
1
07/05/22 16:43
TJS
6010D
Selenium
<29.4
mg/Kg - dry
29.4
1
07/05/22 16:43
TJS
6010D
Qualifiers/ DF Dilution Factor
MQL Method Quantitation Limit
Definitions
Page 3 of 7

0
7621 Whitepine Road, Richmond, VA 23237
Waypoint. Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypoiritanalytical.com
46546
Town Of Clayton Project Town of Clayton
POB 879 Report Date : 07/07/2022
Information : Received : 06/28/2022
Clayton , NC 27528 q
1awc Plc (rrow�/
Report Number: 22-179-0002 REPOR T OF A NA L YSIS Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No : 58403
Sample ID : Holding Tank
Matrix: Solids
Sampled: 6/27/2022 11:45
Total Solids
1.66
%
0.010
1
07/01/22 17:55
ADM
SM-254OG
Phosphorus
30100
mg/Kg - dry
294
1
07/05/22 16:43
TJS
6010D
Sodium
5120
mg/Kg - dry
1470
1
07/05/22 16:43
TJS
6010D
Ammonia Nitrogen
6470
mg/Kg - dry
5880
1
07/06/22 15:30
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
S76
mg/Kg - dry
290
1
07/07/22 14:40
ZBD
4500NO3F-2011
Cadmium
<5.88
mg/Kg - dry
5.88
1
07/05/22 16:43
TJS
6010D
Chromium
16.9
mg/Kg - dry
14.7
1
07/05/22 16:43
TJS
6010D
Mercury
<8.12
mg/Kg - dry
8.12
1
07/05/22 14:36
ZMT
SW-7471B
Molybdenum
<14.7
mg/Kg - dry
14.7
1
07/05/22 16:43
TJS
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 7

Way P 016 nt
ANALYTICAL
Client: Town Of Clayton
Project: Town of Clayton
Lab Report Number: 22-179-0002
Date: 7/7/2022
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 58426
Analyte: Aluminum
QC Batch No: L625343/L624801
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 58426
Analyte: Calcium
QC Batch No: L6252111624801
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 58426
Analyte: Potassium
QC Batch No: L625343/L624801
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 58426
Analyte: Magnesium
QC Batch No: L625211/1-624801
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 58426
Analyte: Molybdenum
QC Batch No: L62521 1 /L624801
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 58426
Analyte: Selenium
QC Batch No: L625211/1-624801
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 5 of 7

(2)
Waypoint
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 1 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46546
Customer Name: Town Of Clayton
Report Number: 22-179-0002
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
Other
Thermometer ID:�
J
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
F 1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
0 Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
# Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
0 N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
# N/A
High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) I Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0) No
Comments:
Signature: IDavid Lennon Date & Time: U6/28/2022 11:20:32
Page 6 of 7

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Page
7
of 7

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms & Cleaning, Inc
Clayton Little Creek WRF
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
C3 22-271-0003
9/27/2022
10/7/2022
3rd Quarter
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids *
2.44
Nitrogen (TKN)
6.000
60,000.000
Phosphorus
2.560
25,600.000
Potassium
0.632
6,320.000
Sulfur
0.000
Calcium
12.000
120,000.000
Magnesium
0.460
4,600.000
Sodium
0.364
3,640.000
Iron
---
Aluminum
---
12.400.000
Manganese
---
Copper
---
165.000
1,500
Zinc
---
772.000
2,800
Ammonia Nitrogen
0.576
5,760.000
Nitrate N / Nitrite N
---
186.000
Cadmium
---
4.000
39
Chromium
---
24.200
1,200
Nickel
---
11.300
420
Lead
---
12.000
300
Arsenic
---
20.000
41
Mercury
---
6.080
17
Selenium
---
20.000
100
pH
11.200
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
5.424
Molybdenum
---
10.000
75
Chloride
---
Boron
Available P205
Specific Gravity
8.340
* average of 7 fecal samples from 9/30/22

Wastewater Treatment Plant
Clayton Little Creek WRF
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
3rd Quarter
Date Reported: 10/7/2022 Report No: C3 22-271-0003
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
38.676
PAN Inj.
44.436
P
51.200
K
12.640
Lime (estimated)
500.000
Secondary Nutrients
Calcium
240.000
Magnesium
9.200
Sodium
7.280
SAR
0.437
Chloride
0.000
Iron
0.000
Alumium
24.800
Manganese
0.000
Boron
0.000
Sulfur
0.000
Residual Nitrogen Calculation
Year Min Rate PAN #/Acre
% Solids
2.44
PH
11.200
Min Rate
0.300
Metals
Arsenic
0.040
Cadmium
0.008
Chromium
0.048
Copper
0.330
Lead
0.024
Mercury
0.012
Molybdenum
0.020
Nickel
0.023
Seleniun
0.040
Zinc
1.544
2019
2020
2021
2022
0.30
32.54
2023
0.15
11.39
2024
0.08
4.84
2025
0.04
2.24
2026
2027
2028
2029

Wayoint
PNALYTICAL
10/7/2022
Town Of Clayton
Salvador Valdiviezo
POB 879
Clayton, NC, 27528
Ref: Analytical Testing
Report Number: 22-271-0003
Project Description: Sludge Disposal
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Salvador Valdiviezo:
Waypoint Analytical Virginia, Inc. received sample(s) on 9/28/2022 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
V­ 1 of 7

Waypoint,(2)
ANALYTICAL
Report Number: 22-271-0003
Client Project Description: Sludge Disposal
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
59521
Holding Tank
Solids
09/27/2022 11:25
09/28/2022
59521
Holding Tank
Solids
09/27/2022 11:25
09/28/2022
SM-4500-NH3C
WP MTN
59521
Holding Tank
Solids
09/27/2022 11:25
09/28/2022
9045D
WP MTN
59521
Holding Tank
Solids
09/27/2022 11:25
09/28/2022
4500NO3F-2011
WP MTN
59521
Holding Tank
Solids
09/27/2022 11:25
09/28/2022
6010D
WP MTN
59521
Holding Tank
Solids
09/27/2022 11:25
09/28/2022
SW-7471B
WP MTN
59521
Holding Tank
Solids
09/27/2022 11:25
09/28/2022
SM-4500-NH3C-TKN
WP MTN
59521
Holding Tank
Solids
09/27/2022 11:25
09/28/2022
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
PanP 9 of 7

0
Waypoint.
7621 Whitepine
Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalocal.com
46546
Town Of Clayton
Project
Sludge Disposal
Salvador Valdiviezo
Report Date : 10/07/2022
POB 879
Information :
Received : 09/28/2022
Clayton , NC 27528
q
Pauric Mc Groary Ph.D., CPA
Report Number : 22-271-0003
REPORT OFANAL YSIS
Agronomist
Lab No : 59521
Matrix:
Solids
Sample ID : Holding Tank
Sampled:
9/27/2022 11:25
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
97.5
%
0.010
1
09/29/2216:06
FMM
SM-2540G
Total Kjeldahl Nitrogen
60000
mg/Kg - dry
10000
1
10/04/22 10:00
JPJ ;M-4500-NH3C-TKP
Potassium
6320
mg/Kg - dry
400
1
10/07/22 05:57
JTR
6010D
Calcium 120000
mg/Kg - dry
2000
1
10/07/22 05:57
JTR
6010D
Aluminum
12400
mg/Kg - dry
200
1
10/07/22 05:57
JTR
6010D
Copper
165
mg/Kg - dry
20.0
1
10/07/22 05:57
JTR
6010D
Zinc
772
mg/Kg - dry
50.0
1
10/07/22 05:57
JTR
6010D
Nickel
11.3
mg/Kg - dry
10.0
1
10/07/22 05:57
JTR
6010D
Arsenic
<20.0
mg/Kg - dry
20.0
1
10/07/22 05:57
JTR
6010D
Silver
<10.0
mg/Kg - dry
10.0
1
10/07/22 05:57
JTR
6010D
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Sodium Absorption Ratio
<40.0
mg/Kg - dry
40.0
1
10/07/22 05:57
CALCULATION
pH
11.2
S.U.
1
10/03/2214:19
SAR
9045D
Lead
<12.0
mg/Kg - dry
12.0
1
10/07/22 05:57
JTR
6010D
Magnesium
4600
mg/Kg - dry
200
1
10/07/22 05:57
JTR
6010D
Selenium
<20.0
mg/Kg - dry
20.0
1
10/07/22 05:57
JTR
6010D
Qualifiers/ DF Dilution Factor
MQL Method Quantitation Limit
Definitions

•
Waypoint. 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46546
Town Of Clayton Project Sludge Disposal
Salvador Valdiviezo Report Date : 10/07/2022
POB 879 Information : Received : 09/28/2022
Clayton , NC 27528
Tack
COO
Report Number: 22-271-0003 REPORT OPANALYSIS Pauric Mc Groary Ph.D., PA
Agronomist
Lab No : 59521
Sample ID : Holding Tank
Matrix: Solids
Sampled: 9/27/2022 11:25
Total Solids
2.49
%
0.010
1
09/29/22 16:06
FMM
SM-2540G
Phosphorus
25600
mg/Kg - dry
200
1
10/07/22 05:57
JTR
6010D
Sodium
3640
mg/Kg - dry
1000
1
10/07/22 05:57
JTR
6010D
Ammonia Nitrogen
5760
mg/Kg - dry
4000
1
10/05/22 13:45
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<186
mg/Kg - dry
186
1
09/30/22 14:55
CLP
4500NO3F-2011
Cadmium
<4.00
mg/Kg - dry
4.00
1
10/07/22 05:57
JTR
6010D
Chromium
24.2
mg/Kg - dry
10.0
1
10/07/22 05:57
JTR
6010D
Mercury
<6.08
mg/Kg - dry
6.08
1
10/04/22 13:11
TJS
SW-7471B
Molybdenum
<10.0
mg/Kg - dry
10.0
1
10/07/22 05:57
JTR
6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

Waypoint
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Client: Town Of Clayton CASE NARRATIVE
Project: Sludge Disposal
Lab Report Number: 22-271-0003
Date: 10/7/2022
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 88911
Analyte: Mercury
QC Batch No: L641201/L640687
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.

Waypoint(2)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 1 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46546
Customer Name: Town Of Clayton
Report Number: 22-271-0003
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other: l y
UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
F-1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
• Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
• Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
Yes
0 No
COC properly completed
Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
# N/A
Trip Blanks received with VOAs
0 Yes
0 No
# N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
High concentration container (48 hr) j Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) I Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes
Comments:
No
Signature: jDavid Lennon Date & Time: 09/28/2022 08:21:04

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Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms & Cleaning, Inc
Clayton Little Creek WRF
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
C4 22-312-0001
11/7/2022
11/16/2022
4th Quarter
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids *
1.93
Nitrogen (TKN)
4.000
40,000.000
Phosphorus
2.460
24,600.000
Potassium
0.636
6,360.000
Sulfur
0.000
Calcium
12.800
128,000.000
Magnesium
0.416
4,160.000
Sodium
0.404
4,040.000
Iron
---
7,680.000
Aluminum
---
11, 800.000
Manganese
---
Copper
---
142.000
1,500
Zinc
---
652.000
2,800
Ammonia Nitrogen**
0.673
6,726.700
Nitrate N / Nitrite N
---
5,280.000
Cadmium
---
4.000
39
Chromium
---
23.000
1,200
Nickel
---
12.600
420
Lead
---
12.000
300
Arsenic
---
20.000
41
Mercury
---
6.240
17
Selenium
---
20.000
100
pH
11.800
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
3.327
Molybdenum
---
10.000
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340
* average of 7 fecal samples from 11/17/22

Wastewater Treatment Plant
Clayton Little Creek WRF
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
4th Quarter
Date Reported: 11/16/2022 Report No:
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
37.251
PAN Inj.
43.977
P
49.200
K
12.720
Lime (estimated)
500.000
Secondary Nutrients
Calcium
256.000
Magnesium
8.320
Sodium
8.080
SAR
0.420
Chloride
0.000
Iron
15.360
Alumium
23.600
Manganese
0.000
Boron
0.000
Sulfur
t 0.000
Residual Nitrogen Calculation
Year Min Rate PAN #/Acre
C4 22-312-0001
Physical Characteristics
% Solids
1.93
PH
11.800
Min Rate
0.300
Metals
Arsenic
0.040
Cadmium
0.008
Chromium
0.046
Copper
0.284
Lead
0.024
Mercury
0.012
Molybdenum
0.020
Nickel
0.025
Seleniun
0.040
Zinc
1.304
2019
2020
2021
2022
0.30
19.96
2023
0.15
6.99
2024
0.08
2.97
2025
0.04
1.37
2026
2027
2028
2029

Waypointe)
ANALYTICAL
11 /16/2022
Town Of Clayton
Salvador Valdiviezo
POB 879
Clayton, NC, 27528
Ref: Analytical Testing
Report Number: 22-312-0001
Project Description: Salvador Valdiviezo
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Salvador Valdiviezo:
Waypoint Analytical Virginia, Inc. received sample(s) on 11/8/2022 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
TaWIT M f &fc'"
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

(2)
•
7621 Whitepine Road, Richmond, VA 23237
Waypoint,Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 22-312-0001
Client Project Description: Salvador Valdiviezo
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
59836
Holding Tank #1
Solids
59836
Holding Tank #1
Solids
59836
Holding Tank #1
Solids
59836
Holding Tank #1
Solids
59836
Holding Tank #1
Solids
59836
Holding Tank #1
Solids
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
11/07/2022
14:40
11/08/2022
11/07/2022
14:40
11/08/2022
11/07/2022
14:40
11/08/2022
11/07/2022
14:40
11/08/2022
11/07/2022
14:40
11/08/2022
11/07/2022
14:40
11/08/2022
SM-4500-NH3C-TKN
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SW-7471B
WP MTN
9045D
WP MTN
SM-2540G
WP MTN
Page 2 of 7

Waypointo
ANALYTICAL
46546
Town Of Clayton
Salvador Valdiviezo
POB 879
Clayton , NC 27528
Report Number: 22-312-0001
Lab No : 59836
Sample ID : Holding Tank #1
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project Salvador Valdiviezo
Information :
REPORT Of ANALYSIS
Report Date : 11/16/2022
Received : 11/08/2022
Taw(c Mt G10T
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 11 / 7/ 2022 14:40
Test
Results
Units
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Moisture
97.5
%
0.010
1
11/10/2216:03
FMM
SM-254OG
Potassium
6360
mg/Kg - dry
400
1
11/14/22 17:17
TJS
6010D
Calcium
128000
mg/Kg - dry
2000
1
11/11/22 18:14
TJS
6010D
Magnesium
4160
mg/Kg - dry
200
1
11/11/22 18:14
TJS
6010D
Sodium
4040
mg/Kg - dry
1000
1
11/11/22 18:14
TJS
6010D
Iron
7680
mg/Kg - dry
400
1
11/11/22 18:14
TJS
6010D
Aluminum
11800
mg/Kg - dry
200
1
11/14/22 17:17
TJS
6010D
Copper
142
mg/Kg - dry
20.0
1
11/11/22 18:14
TJS
6010D
Zinc
652
mg/Kg - dry
50.0
1
11/11/22 18:14
TJS
6010D
Cadmium
<4.00
mg/Kg - dry
4.00
1
11/11/22 18:14
TJS
6010D
Chromium
23.0
mg/Kg - dry
10.0
1
11/11/22 18:14
TJS
6010D
Nickel
12.6
mg/Kg - dry
10.0
1
11/11/22 18:14
TJS
6010D
Lead
<12.0
mg/Kg - dry
12.0
1
11/11/22 18:14
TJS
6010D
Arsenic
<20.0
mg/Kg - dry
20.0
1
11/11/22 18:14
TJS
6010D
Mercury
<6.24
mg/Kg - dry
6.24
1
11/11/22 12:00
JTR
SW-7471B
Selenium
<20.0
mg/Kg - dry
20.0
1
11/11/22 18:14
TJS
6010D
Molybdenum
<10.0
mg/Kg - dry
10.0
1
11/11/22 18:14
TJS
6010D
Silver
<10.0
mg/Kg - dry
10.0
1
11/11/22 18:14
TJS
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 7

0
Waypoint.
7621 Whitepine
Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46546
Town Of Clayton
Project
Salvador Valdiviezo
Salvador Valdiviezo
Report Date : 11/16/2022
POB 879
Information :
Received : 11/08/2022
Clayton , NC 27528
�awrc �� Grow
Pauric Mc Groary Ph.D., CPA
Report Number: 22-312-0001
REPORT
Agronomist
Lab No : 59836
Matrix: Solids
Sample ID : Holding Tank #1
Sampled: 11/7/2022 14:40
Test
Results
Units
MQL
DF Date / Time By Analytical
Analyzed Method
Nitrate+Nitrite-N
5280
mg/Kg - dry
178
1 11/11/22 10:42 ZBD 4500NO3F-2011
pH
11.8
s.u.
1 11/15/2215:06 DRS 9045D
Total Solids
2.47
%
0.010
1 11/10/22 16:03 FMM SM-254OG
Total Kjeldahl Nitrogen
40000
mg/Kg - dry
10000
1 11/15/22 10:30 JPJ >M-4500-NH3C-TKP
Phosphorus
24600
mg/Kg - dry
200
1 11/11/22 18:14 TJS 6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 4 of 7

Waypoint.(2)
ANALYTICAL
Client: Town Of Clayton
Project: Salvador Valdiviezo
Lab Report Number: 22-312-0001
Date: 11/15/2022
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 87938 (Boiler Ash)
Analyte: Aluminum
QC Batch No: 1-648598/1-648207
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 87938 (Boiler Ash)
Analyte: Iron
QC Batch No: 1-648598/1-648207
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 87938 (Boiler Ash)
Analyte: Potassium
QC Batch No: 1-648598/1-648207
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 87938 (Boiler Ash)
Analyte: Magnesium
QC Batch No: 1-648598/1-648207
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 5 of 7

(2)
Waypoint
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
Shipment
Receipt Form
Customer Number: 46546
Customer Name: Town Of Clayton
Report Number: 22-312-0001
Shipping Method
Fed Ex US Postal Lab
Other
• UPS Client Courier
Thermometer ID:
Shipping container/cooler uncompromised?
Yes
No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
Yes
No Not Present
Custody seals intact on sample bottles?
Yes
No • Not Present
Chain of Custody (COC) present?
• Yes
No
COC agrees with sample label(s)?
• Yes
No
COC properly completed
• Yes
No
Samples in proper containers?
6 Yes
No
Sample containers intact?
• Yes
No
Sufficient sample volume for indicated test(s)?
• Yes
No
All samples received within holding time?
• Yes
No
Cooler temperature in compliance?
• Yes
No
Cooler/Samples arrived at the laboratory on ice.
• Yes
No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved
Yes
No • N/A
Water - VOA vials free of headspace
Yes
No • N/A
Trip Blanks received with VOAs
Yes
No 46 N/A
Soil VOA method 5035 — compliance criteria met
Yes
No 16 N/A
High concentration container (48 hr)
Low concentration Encore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
• No
Comments:
Signature: David Lennon Date & Time: 11/08/2022 08:57:19
Page 6 of 7

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Page 7 of 7

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Town of Kenansville
Kenansville WWTP
Kenansville, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
KV 2022-12575
7/6/2022
8/5/2022
Annual 2022
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
1.060
Nitrogen (TKN)
5.400
54,000.000
Phosphorus
1.630
16,300.000
Potassium
0.468
4,680.000
Sulfur
0.000
Calcium
2.100
21,000.000
Magnesium
0.255
2,550.000
Sodium
0.758
7,580.000
Iron
---
Aluminum
---
5,120.000
Manganese
---
Copper
---
586.000
1,500
Zinc
---
761.000
2,800
Ammonia Nitrogen
0.183
1,830.000
Nitrate N / Nitrite N
---
8.560
Cadmium
---
22.800
85
Chromium
---
22.800
1,200
Nickel
---
22.800
420
Lead
---
22.800
300
Arsenic
---
22.800
75
Mercury
---
1.700
17
Selenium
---
22.800
100
pH
7.170
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
5.217
Molybdenum
---
22.800
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Wastewater Treatment Plant
Kenansville WWTP
Kenansville, North Carolina
Triple S Farms & Cleaning, Inc
Annual 2022
Date Reported: 8/5/2022 Report No: KV 2022-12575
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
33.149
PAN Inj.
34.979
P
32.600
K
9.360
Lime (estimated)
0.000
Secondary Nutrients
Calcium
42.000
Magnesium
5.100
Sodium
15.160
SAR
1.350
Chloride
0.000
Iron
0.000
Alumium
10.240
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
1.06
pH
7.170
Min Rate
0.300
Metals
Arsenic
0.046
Cadmium
0.046
Chromium
0.046
Copper
1.172
Lead
0.046
Mercury
0.003
Molybdenum
0.046
Nickel
0.046
Seleniun
0.046
Zinc
1.522

rlp�-. -:-Oqql
s�
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
infota environmentalchemists.com
Town of Kenansville
PO Box 370
Kenansville NC 2B349
Attention: Steve Whitman
Date of Report: Aug 05, 2022
Customer PO #:
Customer ID: 09020018
Report #: 2022-12575
Project ID: Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-30469 Site: sludge
7/6/2022
10:00 AM Solid/Sludge Client
Test
Method
Results
Date Analyzed
Chlordane (TCLP)
SW-B46 8081 B
<0.02 mg/L
07/14/2022
Endrin (TCLP)
SW-846 8081 B
<0.0005 mg/L
07/14/2022
Heptachlor (TCLP)
SW-846 8081 B
<0.0005 mg/L
07/14/2022
Heptachlor epoxide (TCLP)
SW-846 8081 B
<0.0005 mg/L
07/14/2022
Lindane (TCLP)
SW-846 8081 B
<0.0005 mg/L
07/14/2022
Methoxychlor (TCLP)
SW-846 8081 B
<0.0005 mg/L
07/14/2022
Toxaphene (TCLP)
SW-846 8081 B
<0.05 mg/L
07/14/2022
2,4,5-TP (TCLP)
SW-8468151 A
<0.003mg/L
07/14/2022
2,4-D (TCLP)
SW-846 8151 A
<0.003 mg/L
07/14/2022
1,4-Dichlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
07/15/2022
2,4,5-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
07/15/2022
2,4,6-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
07/15/2022
2,4-Dinitrotoluene (TCLP)
SW-846 8270 E
<0.050 mg/L
07/15/2022
Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
07/15/2022
Hexachloro-1,3-butadiene (TCLP)
SW-846 8270 E
<0.050 mg/L
07/15/2022
Hexachlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
07/15/2022
Hexachloroethane (TCLP)
SW-846 8270 E
<0.050 mg/L
07/15/2022
m + p-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
07/15/2022
Nitrobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
07/15/2022
o-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
07/15/2022
Pentachlorophenol (TCLP)
SW-846 8270 E
<0.250 mg/L
07/15/2022
Pyridine (TCLP)
SW-846 8270 E
<0.050 mg/L
07/15/2022
1,1-Dichloroethylene (TCLP)
SW-846 Method8260D
<0.01 mg/L
07/15/2022
1,2-Dichloroethane (TCLP)
SW-846 Method82600
<0.01 mg/L
07/15/2022
Benzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
07/15/2022
Carbon Tetrachloride (TCLP)
SW-846 Method 82600
<0.01 mg/L
07/15/2022
Report tt:: 2022-12575 Page 1 of 3

envirolchem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info(a,environmentalchemists.com
Town of Kenansville
Date of Report: Aug 05, 2022
PO Box 370
Customer PO #:
Kenansville NC
28349
Customer ID: 09020018
Attention: Steve Whitman
Report #: 2022-12575
Project ID: Sludge
Chlorobenzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
07/15/2022
Chloroform (TCLP)
SW-846 Method 8260D
<0.01 mg/L
07/15/2022
Methyl ethyl ketone (TCLP)
SW-846 Method 8260D
<0.05 mg/L
07/15/2022
Tetrachloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
07/15/2022
Trichloroethylene (TCLP)
SW-846 Method82600
<0.01 mg/L
07/15/2022
Vinyl Chloride (TCLP)
SW-846 Method 8260D
<0.01 mg/L
07/15/2022
RCI
Cyanide
SM 4500 CN D-2016
<1.0 mg/kg
07/25/2022
Sulfide
SM 4500 S D
0.22 mg/kg
07/27/2022
Ignitability
SW 846 method 1010
>158 °F
07/19/2022
pH
SW 846 Method 9045D
7.17 units
07/13/2022
Result estimated. Analyzed out
of 15 minutes hold time.
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4, 1994
5120 mg/kg
07/12/2022
Arsenic
EPA 200.7, Rev. 4.4, 1994
<22.8 mg/kg
07/12/2022
Cadmium
EPA 200.7, Rev. 4.4,1994
<22.8 mg/kg
07/12/2022
Calcium
EPA 200.7, Rev. 4.4, 1994
21000 mg/kg
07/12/2022
Chromium
EPA 200.7, Rev. 4.4. 1994
<22.8 mg/kg
07/12/2022
Copper
EPA 200.7, Rev. 4.4, 1994
586 mg/kg
07/12/2022
Lead
EPA 200.7, Rev. 4.4, 1994
<22.8 mg/kg
07/12/2022
Magnesium
EPA 200.7, Rev, 4.4, 1994
2550 mg/kg
07/12/2022
Molybdenum
EPA 200.7, Rev. 4.4, 1994
<22.8 mg/kg
07/12/2022
Nickel
EPA 200.7, Rev. 4.4, 1994
<22.8 mg/kg
07/12/2022
Potassium
EPA 200.7, Rev. 4.4, 1994
4680 mg/kg
07/12/2022
Selenium
EPA 200.7, Rev. 4.4. 1994
<22.8 mg/kg
07/12/2022
Sodium
EPA 200.7, Rev. 4.4,1994
7580 mg/kg
07/12/2022
Zinc
EPA 200.7, Rev. 4.4, 1994
761 mg/kg
07/12/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2
8.56 mg/kg
07/11 /2022
Total Solids (%)
SM 2540 B
1.06 %
07/07/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
1830 mg/kg
07/11 /2022
Report 1f:: 2022.12575
Page 2 of 3

envirochem
su
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 o 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilnngton Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
infot' environmentalchemists.com
Town of Kenansville
Date of Report: Aug 05, 2022
PO Box 370
Customer PO #:
Kenansville NC 28349
Customer ID: 09020018
Attention: Steve Whitman
Report #• 2022-12575
Project ID: Sludge
Total Kjeldahl Nitrogen (TKN) SM 4500 Nora B-2011
54000 mg/kg 07/11 /2022
Total Phosphorus SM 4500 P (F-H)-2011
16300 mg/kg 07/13/2022
Mercury SW-846 7471 B
<1.70 mg/kg 07/08/2022
TCLP Metals
Arsenic
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
07/15/2022
Barium
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
07/15/2022
Cadmium
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
07/15/2022
Chromium
EPA 200.7, Rev. 4.4. 1994
<1.0 mg/L
07/15/2022
Lead
EPA 200.7, Rev. 4.4. 1994
<1.0 mg/L
07/15/2022
Selenium
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
07/15/2022
Silver
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
07/15/2022
Mercury
EPA 245.1
<0.0002 mg/L
07/15/2022
Comment:
Sludge residuals reported on a dry weight basis.
Reviewed by:�-
v
Report #:: 2022-12575 Page 3 of 3

Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
Client:---1 1�%S�% I Ile
Da`_. Report Number:
❑ Receipt YESof sample: E NEM Pickup Client Deiivery ❑ UPS ❑
❑ NO N/A 1. Were custody seals present on the cooler?
❑ YES ❑ NO
N/A 2. If custody seals were
0"
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
FedEx ❑ Oth re ❑
nginal temperature upon receipt 2, present, were they intact/unbroken?
eC Corrected temperature upon receipt_
How temperature taken: ❑ Temperature Blank
IR Gun ID: Thomas Traceable 5/N 192511657 Against Bottles
YES ❑ NO IS Gun Correction Factor °C: 0.0
3. If temperature of cooler exceeded 6°C, was Project Mgr
./qq notified?
YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed?
YES ❑ NO 5. Were sample ID's listed on the COC?
YES ❑ NO 6. Were samples
YES P ID's listed on sample containers?
❑ NO 7. Were collection date and time listed on the
x � IM plr, COC.
yE
l;-caj on the COC?
-- — J - _ - r
r YES ❑ NO r,v. cap, ic;i7
YE 10. Did sample; arr the in good condition for each test?
❑ NO 11. Was ?tlenna-c „ql�
YES ❑ Ni - m- ava'lable?
O 112 AA/
YES
YE5
YES
YES
YES
YES
mples received within proper holding time for reque ted t 13. Were acid presLr.,ed samo'es received at a pH of <2? x
14. Were a '-
d
�
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Wc-re sulfic[E sa:n%ples received at a pH >9?
Were 1,H3/IKN/ Phenol received at a chlorine residual of <0.5 m/L?' Y Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
Were orthophosphate samples filtered in the field within 15 minutcs?
TOC/Volatile; a-e PH checked at tin =
c` ana'jss =nd re_o•ded or; b.2;,chshee,.
** Bacteria 53,,rPfes a"e checked for Ch'o-ine at t�rr e of analysis ald reco,ded on the benchsheet,
m
m
m
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16
17.
18.
Sample Preservation: (Must be completed for any samples) incorrectly
y preserved or with headspace)
were received incorrectly preserved and were adjusted accordingly
by adding (circle one): HZSOz HNO3 HC(
Time of preservation: NaOH
If more than one preservative is needed, notate in comments be(oy,
Vote: iV=`'
'•0`.iiy `^� sia�n ,a_ i= ^ re:Te: -- - - 2• ,-_,�,- .� .'�i?'VQ7 �3-•...`35 0-a• - re, sa , _,e o-
/olatilesSampleO - = r-e_ Jf e : 5 �� ^e ;,as ^a:e all;
were received with hea— d— spare
COMMENTS:
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Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Town of Maysville
Maysville WWTP
Maysville, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
MV 2022-10200
6/2/2022
7/15/2022
Annual 2022
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
0.480
Nitrogen (TKN)
8.610
86,100.000
Phosphorus
0.065
647.000
Potassium
0.902
9,020.000
Sulfur
0.000
Calcium
6.270
62,700.000
Magnesium
0.617
6,170.000
Sodium
1.670
16,700.000
Iron
---
Aluminum
---
8,400.000
Manganese
---
Copper
---
842.000
1,500
Zinc
---
1,420.000
2,800
Ammonia Nitrogen
0.616
6,160.000
Nitrate N / Nitrite N
---
129.000
Cadmium
---
38.800
85
Chromium
---
38.800
1,200
Nickel
---
38.800
420
Lead
---
38.800
300
Arsenic
---
117.000
75
Mercury
---
3.480
17
Selenium
---
38.800
100
pH
7.910
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
7.994
Molybdenum
---
38.800
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Wastewater Treatment Plant
Maysville WWTP
Maysville, North Carolina
Triple S Farms & Cleaning, Inc
Annual 2022
Date Reported: 7/15/2022 Report No: MV 2022-10200
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
54.382
PAN Inj.
60.542
P
1.294
K
18.040
Lime (estimated)
0.000
Secondary Nutrients
Calcium
125.400
Magnesium
12.340
Sodium
33.400
SAR
1.178
Chloride
0.000
Iron
0.000
Alumium
16.800
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
0.48
pH
7.910
Min Rate
0.300
Metals
Arsenic
0.234
Cadmium
0.078
Chromium
0.078
Copper
1.684
Lead
0.078
Mercury
0.007
Molybdenum
0.078
Nickel
0.078
Seleniun
0.078
Zinc
2.840

r
gn:v7irochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
info,ii environmentalchemists.com
Town of Maysville Date of Report: Jul 15, 2022
Post Office Box 265 Customer PO #:
Maysville NC 28555 Customer ID: 17020023
Attention: Schumata Brown Report #: 2022-10200
Project ID: Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-24672 Site: Sludge 6/2/2022 1:14 PM Solid/Sludge Chris Williams
Test Method Results Date Analyzed
Chlordane (TCLP)
SW-846 8081 B
<0.02 mg/L
06/09/2022
Endrin (TCLP)
SW-846 8081 B
<0.0005 mg/L
06/09/2022
Heptachlor (TCLP)
SW-846 8081 B
<0.0005 mg/L
06/09/2022
Heptachlor epoxide (TCLP)
SW-846 8081 B
<0.0005 mg/L
06/09/2022
Lindane (TCLP)
SW-846 8081 B
<0.0005 mg/L
06/09/2022
Methoxychlor (TCLP)
SW-846 8081 B
<0.0005 mg/L
06/09/2022
Toxaphene (TCLP)
SW-846 8061 B
<0.05 mg/L
06/09/2022
2,4,5-TP (TCLP)
SW-846 8151 A
<0.003 mg/L
06/13/2022
2,4-D (TCLP)
SW-846 8151 A
<0.003 mg/L
06/13/2022
1,4-Dichlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
06/08/2022
2,4,5-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
06/08/2022
2,4,6-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
06/08/2022
2,4-Dinitrotoluene (TCLP)
SW-846 8270 E
<0.050 mg/L
06/08/2022
Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
06/08/2022
Hexachloro-1,3-butadiene (TCLP)
SW-846 8270 E
<0.050 mg/L
06/08/2022
Hexachlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
06/08/2022
Hexachloroethane (TCLP)
SW-846 8270 E
<0.050 mg/L
06/08/2022
m + p-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
06/08/2022
Nitrobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
06/08/2022
o-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
06/08/2022
Pentachlorophenol (TCLP)
SW-846 8270 E
<0.250 mg/L
06/08/2022
Pyridine (TCLP)
SW-846 8270 E
<0.050 mg/L
06/08/2022
1,1-Dichloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
06/09/2022
1,2-Dichloroethane (TCLP)
SW-846 Method 8260D
<0.01 mg/L
06/09/2022
Benzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
06/09/2022
Carbon Tetrachloride (TCLP)
SW-846 Method 8260D
<0.01 mg/L
06/09/2022
Report # 2022-10200 Page 1 of 3

[envirochem
ANALYTICAL 8 CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windinill Way, Wilmington, NC 28405 a 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 + 910.347.5843 Lab/Fax
info 4 environmentalchemists.com
Town of Maysville
Date of Report: Jul 15, 2022
Post Office Box 265
Customer PO #:
Maysville NC 28555
Customer ID: 17020023
Attention: Schumata Brown
Report #: 2022-10200
Project ID: Sludge
Chlorobenzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
06/09/2022
Chloroform (TCLP)
SW-846 Method 8260D
<0.01 mg/L
06/09/2022
Methyl ethyl ketone (TCLP)
SW-846 Method 6260D
0.11 mg/L
06/09/2022
Tetrachloroethylene (TCLP)
SW-848 Method 8260D
<0.01 mg/L
06/09/2022
Trichloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
06/09/2022
Vinyl Chloride (TCLP)
SW-846 Method 8260D
<0.01 mg/L
06/09/2022
RCI
Cyanide
SM 4500 CN D-2016
2.75 mg/kg
06/14/2022
Sulfide
SM 4500 S D
12.8 mg/kg
06/13/2022
Ignitability
SW 846 method 1010
>158 °F
06/14/2022
pH
SW 846 Method 9045D
7.91 units
06/28/2022
Result estimated. Analyzed out of 15 minutes hold time.
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4, 1994
8400 mg/kg
06/20/2022
Arsenic
EPA 200.7, Rev. 4.4, 1994
117 mg/kg
06/20/2022
Calcium
EPA 200.7, Rev. 4.4, 1994
62700mg/kg
06/20/2022
Copper
EPA 200.7, Rev. 4.4, 1994
842 mg/kg
06/20/2022
Magnesium
EPA 200.7, Rev. 4.4, 1994
6170 mg/kg
06/20/2022
Potassium
EPA 200.7, Rev. 4.4, 1994
9020 mg/kg
06/28/2022
Sodium
EPA 200.7, Rev. 4.4, 1994
16700 mg/kg
06/20/2022
Zinc
EPA 200.7, Rev. 4.4, 1994
1420 mg/kg
06/20/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2
129 mg/kg
06/08/2022
Total Solids (%)
SM 2540 B
0.48 %
06/03/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
6160 mg/kg
06/06/2022
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
86100 mg/kg
06/06/2022
Total Phosphorus
SM 4500 P (F-H)-2011
647 mg/kg
06/11 /2022
Mercury
SW-846 7471 B
<3.48 mg/kg
06/09/2022
TCLP Metals
Arsenic
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
06/13/2022
Barium
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
06/13/2022
Report # 2022-10200
Page 2 of 3

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, IBC 28405 - 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
sra 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infoC:environmentalchemists.com
Town of Maysville
Post Office Box 265
Maysville NC 28555
Attention: Schumata Brown
Date of Report: Jul 15, 2022
Customer PO #:
Customer ID: 17020023
Report #: 2022-10200
Project ID: Sludge
Cadmium
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
06/13/2022
Chromium
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
06/13/2022
Lead
EPA 200.7, Rev. 4.4, 1994
<1.O mg/L
06/13/2022
Selenium
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
06/13/2022
Silver
EPA 200.7. Rev. 4.4. 1994
<1.0 mg/L
06/13/2022
Mercury
EPA 245.1
<0.0002 mg/L
06/09/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-24672A Site: Sludge
6/2/2022
1:14 PM Solid/Sludge Chris Williams
Test
Method
Results Date Analyzed
Cadmium
EPA 200.7, Rev. 4.4, 1994
<38.8 mg/kg
07/08/2022
Chromium
EPA 2D0.7, Rev. 4.4, 1994
<38.8 mg/kg
07/08/2022
Lead
EPA 200.7, Rev. 4.4,1994
<38.8 mg/kg
07/08/2022
Molybdenum
EPA 200 7, Rev 4 4 1994
<38.8 mg/kg
07/08/2022
Nickel
EPA 200 7, Rev 4 4 1994
<38.8 mg/kg
07/08/2022
Selenium
EPA 200 7, Rev 4 4 1994
<38.8 mg/kg
07/08/2022
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis
Reviewed by:
Report # 2022.10200 Page 3 of 3

Environmental Chemist, Inc., Wilmington, NC Lab ##94 6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client: �l SUS lNt" Date: oQa Report Number: Q a —1() C)O V
Receipt of sample: ECHEM Pickup Client Delivery ❑
UPS ❑ FedEx ❑ Other ❑
❑ YES
10 NO
N/A
1. Were custody seals present on the cooler?
❑ YES
❑ NO
I C&I N/A
2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt °C
How temperature taken: ElTemperature Blank Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
❑ YES
❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
]5 YES
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
AP YES
❑ NO
5. Were sample ID's listed on the COC?
YES
❑ NO
6. Were samples ID's listed on sample containers?
LX YES
❑ NO
7. Were collection date and time listed on the COC?
YES
❑ NO
8. Were tests to be performed listed on the COC?
YES
❑ NO
9. Did samples arrive in proper containers for each test?
104 YES
YES
❑ NO
❑ NO
10. Did samples arrive in good condition for each test?
11. Was adequate sample volume available?'
Ok YES
❑ NO
12. Were samples received within proper holding time for requested tests?
❑ YES
❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
❑ NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pll checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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Facility:
Town of Rose Hill
Source:
Rose Hill WWTP
Location:
Rose Hill, North Carolina
Contractor:
Triple S Farms & Cleaning, Inc
Type of Analysis:
Wastewater Treatment Plant
Report No:
RH-2022-07795
Date Sampled:
4/29/2022 Type of Stabilization: None
Date Reported:
5/11/2022
Reporting Period:
Annual 2022
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
28.829
Nitrogen (TKN)*
3.430
34,300.000
Phosphorus
2.060
20,600.000
Potassium
1.320
13,200.000
Sulfur
0.000
Calcium
2.240
22,400.000
Magnesium
0.111
1,110.000
Sodium
0.043
432.000
Iron
---
Aluminum
---
8,430.000
Manganese
---
Copper
---
313.000
1,500
Zinc
---
828.000
2,800
Ammonia Nitrogen*
0.076
758.000
Nitrate N / Nitrite N*
---
101.000
Cadmium
---
3.070
39
Chromium
---
52.200
1,200
Nickel
---
8.200
420
Lead
---
30.800
300
Arsenic
---
7.920
41
Mercury
---
0.548
17
Selenium
---
5.060
100
pH
6.850
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
3.354
Molybdenum
---
3.440
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Wastewater Treatment Plant
Rose Hill WWTP
Rose Hill, North Carolina
Triple S Farms & Cleaning, Inc
Annual 2022
Date Reported: 5/11/2022 Report No: RH-2022-07795
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
27.794
PAN Inj.
28.552
P
41.200
K
26.400
Lime (estimated)
0.000
Secondary Nutrients
Calcium
44.800
Magnesium
2.220
Sodium
0.864
SAR
0.410
Chloride
0.000
Iron
0.000
Alumium
16.860
Manganese
0.000
Boron
0.000
Sulfur
0.000
Residual Nitrogen Calculation
Year Min Rate PAN #/Acre
% Solids
28.83
pH
6.850
Min Rate
0.400
Metals
Arsenic
0.016
Cadmium
0.006
Chromium
0.104
Copper
0.626
Lead
0.062
Mercury
0.001
Molybdenum
0.007
Nickel
0.016
Seleniun
0.010
Zinc
1.656
2019
2020
2021
2022
0.40
26.83
2023
0.20
8.05
2024
0.10
3.22
2025
0.05
1.45
2026
2027
2028
2029

envirochem
6�h
ANALYTICAL & CONSULTING CHEMISTS
Branch Residuals/Bob Branch
1735 Heckle Blvd Suite 103-291
Rock Hill SC 29732
Attention: Bob Branch
Lab ID Sample ID:
22-18824 Site: Sludge
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
infow environmentalchemists.com
Date of Report: May 11, 2022
Customer PO #:
Customer ID: 15060009
Report #: 2022-07795
Project ID: Rose Hill WWTP
Collect Date/Time Matrix Sampled by
4/29/2022 10:25 AM Solid/Sludge jcb/envirochem
Test
Method
Results
Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4, 1994
8430 mg/kg
05/02/2022
Arsenic
EPA 200.7, Rev. 4.4, 1994
7.92 mg/kg
05/02/2022
Cadmium
EPA 200.7, Rev. 4.4, 1994
<3.07 mg/kg
05/02/2022
Calcium
EPA 200.7, Rev. 4.4, 1994
22400 mg/kg
05/02/2022
Chromium
EPA 200.7, Rev. 4.4, 1994
52.2 mg/kg
05/02/2022
Copper
EPA 200.7, Rev. 4.4, 1994
313 mg/kg
05/02/2022
Lead
EPA 200.7, Rev. 4.4, 1994
30.8 mg/kg
05/02/2022
Magnesium
EPA 200.7, Rev. 4.4, 1994
1110 mg/kg
05/02/2022
Molybdenum
EPA 200.7, Rev. 4.4, 1994
3.44 mg/kg
05/02/2022
Nickel
EPA 200.7, Rev. 4.4, 1994
8.20 mg/kg
05/02/2022
Potassium
EPA 200.7, Rev. 4.4, 1994
1320 mg/kg
05/02/2022
Selenium
EPA 200.7, Rev. 4.4, 1994
5.06 mg/kg
05/02/2022
Sodium
EPA 200.7, Rev. 4.4, 1994
432 mg/kg
05/02/2022
Zinc
EPA 200.7, Rev. 4.4, 1994
828 mg/kg
05/02/2022
Nitrate+Nitrite-Nitrogen
EPA 3532
101 mg/kg
05/03/2022
Total Solids (%)
SM 2540 B
24.5 %
05/03/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
758 mg/kg
05/02/2022
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
34300 mg/kg
05/02/2022
Total Phosphorus
SM 4500 P (F-H)-2011
20600 mg/kg
05/06/2022
pH
SW 846 Method 9045D
6.85 units
05/03/2022
Mercury
SW-846 7471 B
0.548 mg/kg
05/04/2022
Report # 2022-07795 Page 1 of 3

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Renortin2 Period:
Parameter
Solids*
Nitrogen (TKN)*
Phosphorus
Potassium
Sulfur
Calcium
Magnesium
Sodium
Iron
Aluminum
Swansboro WWTP
Swansboro WWTP
Swansboro, NC
Triple S Farms
Wastewater Treatment Plant
SWB E2022-17562
9/7/2022 Type of Stabilization: Lime
9/22/2022
Annual 2022
% PPM
Dry Wei
1.940
3.620
36,200.00
1.590
15,900.00
0.305
3,050.00
0.00
3.080
30,800.00
0.183
1,830.00
0.582
5,820.00
EPA
Monthly Limits
Copper
---
281.000
1,500
Zinc
---
3,670.000
7,500
Ammonia Nitrogen*
0.079
792.000
Nitrate N / Nitrite N*
---
9,050.000
Cadmium
---
16.500
39
Chromium
---
16.500
1,200
Nickel
---
16.500
420
Lead
---
16.500
300
Arsenic
---
16.500
41
Mercury
---
0.985
17
Selenium
---
16.500
100
pH
6.770
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
3.541
Molybdenum
---
16.500
75
Chloride
---
Boron
Available P205
Specific Gravity
8.340

Wastewater Treatment Plant
Swansboro WWTP
Swansboro, NC
Triple S Farms
Annual 2022
Date Reported: 9/22/2022 Report No: SWB E2022-17562
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
40.137
PAN Inj.
40.929
P
31.800
K
6.100
Lime (estimated)
0.000
Secondary Nutrients
Calcium
61.600
Magnesium
3.660
Sodium
11.640
SAR
1.212
Chloride
0.000
Iron
0.000
Alumium
5.180
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
1.94
pH
6.770
Min Rate
0.300
Metals
Arsenic
0.033
Cadmium
0.033
Chromium
0.033
Copper
0.562
Lead
0.033
Mercury
0.002
Molybdenum
0.033
Nickel
0.033
Seleniun
0.033
Zinc
7.340

envirochem
sM
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 Y 910.392.023 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Onslow Water & Sewer Authority Date of Report: Sep 22, 2022
228 Georgetown Road Customer PO #:
Jacksonville NC 28540 Customer ID: 08100092
Attention: Mark Young Report #: 2022-17562
Project ID: Swansboro WRF
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-43084 Site: Sludge 9/7/2022 8:01 AM Solid/Sludge Samantha Howard
Test
Method
Results
Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4, 1994
2590 mg/kg
09/17/2022
Cadmium
EPA 200.7, Rev. 4.4,1994
<16.5 mg/kg
09/17/2022
Calcium
EPA 200.7, Rev. 4.4, 1994
30800 mg/kg
09/17/2022
Chromium
EPA 200.7, Rev. 4.4. 1994
<16.5 mg/kg
09/17/2022
Copper
EPA 200.7, Rev. 4.4, 1994
281 mg/kg
09/17/2022
Lead
EPA 200.7, Rev. 4.4, 1994
<16.5 mg/kg
09/17/2022
Magnesium
EPA 200.7, Rev. 4.4, 1994
1830 mg/kg
09/17/2022
Molybdenum
EPA 200.7, Rev. 4.4, 1994
<16.5 mg/kg
09/17/2022
Nickel
EPA 200.7, Rev. 4.4, 1994
<16.5 mg/kg
09/17/2022
Potassium
EPA 200.7, Rev. 4.4, 1994
3050 mg/kg
09/17/2022
Selenium
EPA 200.7, Rev. 4.4, 1994
<16.5 mg/kg
09/17/2022
Sodium
EPA 200.7, Rev. 4.4, 1994
5820 mg/kg
09/17/2022
Zinc
EPA 200.7, Rev. 4.4, 1994
3670 mg/kg
09/17/2022
Arsenic
EPA 200.8, Rev. 5.4,1994
<16.5 mg/kg
09/20/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2
9050 mg/kg
09/12/2022
Total Solids (%)
SM 2540 B
1.94 %
09/08/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
792 mg/kg
09/08/2022
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
36200 mg/kg
09/09/2022
Total Phosphorus
SM 4500 P (F-H)-2011
15900 mg/kg
09/14/2022
pH
SW 846 Method 9045D
6.77 units
09/12/2022
Mercury
SW-846 7471 B
<0.985 mg/kg
09/17/2022
Report #: 2022.17562 Page 1 of 3

envirochem
SN
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Ine.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255 A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Onslow Water & Sewer Authority Date of Report: Sep 22, 2022
228 Georgetown Road Customer PO #:
Jacksonville NC 28540 Customer ID: 08100092
Attention: Mark Young Report #: 2022-17562
Project ID: Swansboro WRF
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-43085 Site: Sludge 1 9/7/2022 7:47 AM Solid/Sludge Samantha Howard
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221 C E-2014
1.69 % 09/08/2022
544379 MPN/g 09/07/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-43094 Site: Sludge 2 9/7/2022 7:49 AM Solid/Sludge Samantha Howard
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 1.66 % 09/08/2022
Fecal Density SM 9221C E-2014 554217 MPN/g 09/07/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
2243095 Site: Sludge 3 9/7/2022 7:51 AM Solid/Sludge Samantha Howard
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 1.64 % 09/08/2022
Fecal Density SM 9221C E-2014 560976 MPN/g 09/07/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-43096 Site: Sludge 4 9/7/2022 7:53 AM Solid/Sludge Samantha Howard
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 1.82 % 09/08/2022
Fecal Density SM 9221C E-2014 296704 MPN/g 09/07/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-43097 Site: Sludge 5 9/7/2022 7:55 AM Solid/Sludge Samantha Howard
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 1.81 % 09/08/2022
Fecal Density SM 9221C E-2014 193371 MPN/g 09/07/2022
Report #:: 2022.17562 Page 2 of 3

ppow�'—.- —2,oqql
r , r
4.
ANALYTICAL & CONSULTING CHEMISTS
Environmental. Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 r 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Onslow Water & Sewer Authority
Date of Report: Sep 22, 2022
228 Georgetown Road
Customer PO #:
Jacksonville NC 28540
Customer ID: 08100092
Attention: Mark Young
Report #: 2022-17562
Project ID: Swansboro WRF
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-43098 Site: Sludge 6
9/7/2022 7:57 AM Solid/Sludge Samantha Howard
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 1.60 % 09/08/2022
Fecal Density
SM 9221C E-2014 218750 MPN/g 09/07/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-43099 Site: Sludge 7
9/7/2022 7:59 AM Solid/Sludge Samantha Howard
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 1,67 % 09/08/2022
Fecal Density
SM 9221C E-2014 323354 MPN/g 09/07/2022
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
r
Reviewed by:
Report # 2022-17562 Page 3 of 3

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client: W W A 5A Date: T Report Number: _ 2022- ! -7
D I..+ .,F .,1,. rr-i .
=.J—
ck-ncivi PICKUP Client Delivery ❑ SUPS ElFedFx III Other ❑
❑ YES ❑ NO
N/A 1. `Were custody seals present on the cooler?
❑ YES I0 NO
14 N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt °C
How temperature taken:
❑ Temperature Blank 0 Against Bottles
IR Gun ID: Thomas Traceable SIN 192511657 IR Gun Correction Factor °C: 0.0
Cd YES
❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
® YES
❑ NO
5. Were sample ID's listed on the COC?
6a YES
❑ NO
6. Were samples ID's listed on sample containers?
R YES
❑ NO
Were collection date and time listed on the COC?
7T
IN YES
❑ NO
Were tests to be performed listed on the COC?
YES
❑ NO
Did samples arrive in proper containers for each test?
tO YES
❑ NO
Did samples arrive in good condition for each test?
N YES
❑ NO
Was adequate sample volume available?'
f$ YES
❑ NO
_
12. Were samples received within proper holding time for requested tests?
❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ NO
14. Were cyanide samples received at a pH >12?
ED
❑ NO
15. Were sulfide samples received at a pH >9?
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L?❑
NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
❑ NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must
be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s)
were received incorrectly preserved and were adjusted accordingly
by adding (circle one):
H2SO4 HNO3 HCl NaOH
Time of preservation:
If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s)
were received with heacisoarP
COMMENTS:
nnr nn nm on., a

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Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms
Southwest Plantation
Jacksonville, North Carolina
Triple S Farms
Jacksonville WWTP
SWP 2022 3-22
2/28/2022
3/15/2022
Annual 2022
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
1.720
Nitrogen (TKN)
6.150
61,500.000
Phosphorus
0.070
698.000
Potassium
0.634
6,340.000
Sulfur
0.000
Calcium
1.300
13,000.000
Magnesium
0.365
3,650.000
Sodium
1.460
14,600.000
Iron
---
Aluminum
---
2,600.000
Manganese
---
Copper
---
200.000
1,500
Zinc
---
1,050.000
2,800
Ammonia Nitrogen
1.740
17,400.000
Nitrate N / Nitrite N
---
64.700
Cadmium
---
29.200
39
Chromium
---
29.200
1,200
Nickel
---
29.200
420
Lead
---
29.200
300
Arsenic
---
29.200
41
Mercury
---
1.030
17
Selenium
---
29.200
100
pH
7.300
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
4.410
Molybdenum
---
29.200
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Jacksonville WWTP
Southwest Plantation
Jacksonville, North Carolina
Triple S Farms
Annual 2022
Date Reported: 3/15/2022 Report No: SWP 2022 3-22
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
43.989
PAN Inj.
61.389
P
1.396
K
12.680
Lime (estimated)
0.000
Secondary Nutrients
Calcium
26.000
Magnesium
7.300
Sodium
29.200
SAR
3.811
Chloride
0.000
Iron
0.000
Alumium
5.200
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
1.72
pH
7.300
Min Rate
0.300
Metals
Arsenic
0.058
Cadmium
0.058
Chromium
0.058
Copper
0.400
Lead
0.058
Mercury
0.002
Molybdenum
0.058
Nickel
0.058
Seleniun
0.058
Zinc
2.100

:enviroochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Services
PO Box 1054
Jacksonville NC
Attention:
Lab ID Sample ID:
22-08609 Site: Sludge
Envirmumental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
infotJsenvironmentalchemists.com
Date of Report: Mar 15, 2022
Customer PO #:
28541 Customer ID: 14110017
Report #: 2022-03642
Project ID: Bear Trail Golf Course - Sludge
Collect Date/Time Matrix Sampled by
2/28/2022 7:00 AM Solid/Sludge Client
Test
Method
Results
Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4,1994
2600 mg/kg
03/07/2022
Arsenic
EPA 200.7, Rev. 4.4, 1994
<29.2 mg/kg
03/07/2022
Cadmium
EPA 200.7, Rev. 4.4, 1994
<29.2 mg/kg
03/07/2022
Calcium
EPA 200.7, Rev. 4.4, 1994
13000 mg/kg
03/07/2022
Chromium
EPA 200.7, Rev. 4.4, 1994
<29.2 mg/kg
03/07/2022
Copper
EPA 200.7, Rev. 4.4, 1994
200 mg/kg
03/07/2022
Lead
EPA 200.7, Rev. 4.4, 1994
<29.2 mg/kg
03/07/2022
Magnesium
EPA 200.7, Rev. 4.4, 1994
3650 mg/kg
03/07/2022
Molybdenum
EPA 200.7, Rev. 4.4, 1994
<29.2 mg/kg
03/07/2022
Nickel
EPA 200.7, Rev. 4.4, 1994
<29.2 mg/kg
03/07/2022
Potassium
EPA 200.7, Rev. 4.4. 1994
6340 mg/kg
03/07/2022
Selenium
EPA 200.7, Rev. 4.4, 1994
<29.2 mg/kg
03/07/2022
Sodium
EPA 200.7, Rev. 4.4, 1994
14600 mg/kg
03/07/2022
Zinc
EPA 200.7, Rev. 4.4, 1994
1050 mg/kg
03/07/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2
64.7 mg/kg
03/02/2022
Total Solids (%)
SM 2540 B
1,72 %
03/04/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
17400 mg/kg
03/01/2022
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg 8-2011
61500 mg/kg
03/01/2022
Total Phosphorus
SM 4500 P (F-H)-2011
698 mg/kg
03/04/2022
pH
SW 846 Method 9045D
7.30 units
03/14/2022
Result estimated. Analyzed out of
15 minutes hold time.
Mercury SW-846 7471 B <1.03 mg/kg 03/09/2022
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by::
t
Report 9 2022-03642 Page 1 of 1

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910
Sample Receipt Checklist •392.0223
Client:fgU - SvC,, Date
` Report Number: _ 2022- 0 & '
Receipt of sample:
❑ YES ❑ NO
_ ECHEM Pickup Client Delivery ❑ UPS ❑ FedEx ❑ Other
N/A
❑ YES
❑ NO
1. Were custody seals present on the cooler?
N/A
Original temperature
upon
2. If custody seals were present, were they intact/unbroken?
receiptr °C
Corrected temperature upon receipt_
How temperature taken: ❑ Temperature Blank AgainstBoes
IR Gun ID: Thomas Traceable S/N: 210835468 IR Gun Correction
Ct10 0
❑ YES
YES
0 NO
❑ NO
3. If temperature of cooler exceeded 6C, was Project M r, a
YES
❑ NO
4. Were proper custody procedures (relinquished/received) followed?d
5. Were sample ID's listed on the COC?
YES
❑ NO
6. Were samples ID's listed on sample containers?
YES
❑ NO
7. Were collection date and time listed on the COC?
YES
❑ NO
B. Were tests to be performed listed on the COC?
YES
YFS
❑ NO
❑
9. Did samples arrive in proper containers for each test?
�'M Yts
NO
10 NO
in. C;; so,,,a;-, a rioc. i,� good condition for each test? ---'�-
I11 %A'as
YES
❑ NO
adequat9 sam le volume a i,a i-2?
❑ YES
❑ NO
12. Were samples received within proper holding time for requested tests?
❑ YES
❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑
15. Were sulfide samples received at a pH >9?
❑ YES
NO
iO NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/0 *�
❑ YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOr/Volatiles are pH checked at time of anahysi, and recorded on the bench,heet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
is
ample(s) were received incorrectly preserved and were adjusted accordingly
by adding one): HZS04 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed notate in comments below
Note: NotiFf customer service immediately for incorrectly preserved samples obtain a nen sample or
notif�j the state lab if directed to analyzed by the customer. W/ o was notified, date and time:
Volatiles Sample(s) were received with headsoacp
COMMENTS:
'C
DOC. QA.002 Rev 1

0
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Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms
Wallace WWTP
Wallace, North Carolina
Triple S Farms
Wallace WWTP
WL 1-2022-00308
1/5/2022 Type of Stabilization: Non
1/26/2022
1st Quarter 2022
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
2.71
Nitrogen (TKN)*
3.960
39,600.000
Phosphorus
2.640
26,400.000
Potassium
0.604
6,040.000
Sulfur
0.000
Calcium
3.230
32,300.000
Magnesium
0.507
5,070.000
Sodium
0.464
4,640.000
Iron
---
Aluminum
---
14,300.000
Manganese
---
Copper
---
987.000
1,500
Zinc
---
1,710.000
2,800
Ammonia Nitrogen*
0.000
4.440
Nitrate N / Nitrite N*
---
427.000
Cadmium
---
30.400
39
Chromium
---
44.900
1,200
Nickel
---
30.400
420
Lead
---
42.600
300
Arsenic
---
30.400
41
Mercury
---
0.956
17
Selenium
---
30.400
100
pH
6.870
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
3.960
Molybdenum
---
30.400
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Wallace WWTP
Wallace WWTP
Wallace, North Carolina
Triple S Farms
1st Quarter 2022
Date Reported: 1/26/2022 Report No: WL 1-2022-003C
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
24.616
PAN Inj.
24.620
P
52.800
K
12.080
Lime (estimated)
0.000
Secondary Nutrients
Calcium
64.600
Magnesium
10.140
Sodium
9.280
SAR
1.041
Chloride
0.000
Iron
0.000
Alumium
28.600
Manganese
0.000
Boron
0.000
Sulfur
0.000
Residual Nitrogen Calculation
Year Min Rate PAN #/Acre
% Solids
2.71
pH
6.870
Min Rate
0.300
Metals
Arsenic
0.061
Cadmium
0.061
Chromium
0.090
Copper
1.974
Lead
0.085
Mercury
0.002
Molybdenum
0.061
Nickel
0.061
Seleniun
0.061
Zinc
3.420
2019
2020
2021
2022
0.30
23.76
2023
0.15
8.32
2024
0.08
3.53
2025
0.04
1.63
2026
2027
2028
2029

F05,07 41 Environmental Chemists, Inc.
envirochem6602 Windmill Way Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Branch Residuals/Bob Branch
Date of Report: Jan 26, 2022
1735 Heckle Blvd Suite 103-291
Customer PO #:
Rock Hill SC 29732
Customer ID: 15060009
Attention: Bob Branch
Report #: 2022-00308
Project ID: Wallace WWTP
Chlorobenzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/19/2022
Chloroform (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/19/2022
Methyl ethyl ketone (TCLP)
SW-846 Method 8260D
<0.05 mg/L
01/19/2022
Tetrachloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/19/2022
Trichloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/19/2022
Vinyl Chloride (TCLP)
SW-846 Method 82600
<0.01 mg/L
01/19/2022
RCI
Cyanide
SM 4500 CN D
<1.0 mg/kg
01/11/2022
Sulfide
SM 4500 S D
0.26 mg/kg
01/21/2022
Ignitability
SW 846 method 1010
>157 °F
01/10/2022
Sludge Residuals
Aluminum
EPA 2007,Rev 4 4, 1994
14300mg/kg
01/11/2022
Arsenic
EPA 200 7, Rev 4 4, 1994
<30.4 mg/kg
01/11/2022
Cadmium
EPA 200.7, Rev. 4.4, 1994
<30.4 mg/kg
01/11/2022
Calcium
EPA 200.7. Rev. 4.4, 1994
32300mg/kg
01/11/2022
Chromium
EPA 200 7, Rev. 4.4, 1994
44.9 mg/kg
01/11/2022
Copper
EPA 200.7, Rev. 4.4, 1994
987 mg/kg
01/11/2022
Lead
EPA 200.7, Rev. 4.4, 1994
42.6 mg/kg
01/11/2022
Magnesium
EPA 200.7, Rev 4.4, 1994
5070mg/kg
01/11/2022
Molybdenum
EPA 200.7, Rev. 4.4, 1994
<30.4mg/kg
01/11/2022
Nickel
EPA 200.7. Rev. 4.4, 1994
<30.4 mg/kg
01/11/2022
Potassium
EPA 200.7, Rev. 4.4, 1994
6040mg/kg
01/11/2022
Selenium
EPA 200.7,Rev 44 1994
<30.4mg/kg
01/11/2022
Sodium
EPA 200.7, Rev 4 4, 1994
4640 mg/kg
01/11/2022
Zinc
EPA 200.7, Rev 4 4, 1994
1710 mg/kg
01/11/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2
427 mg/kg
01/06/2022
Total Solids (%)
SM 2540 B
2,25 %
01/07/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
<4.44 mg/kg
01/07/2022
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
39600 mg/kg
01/07/2022
Total Phosphorous
SM 4500 P (F-H)-2011
26400 mg/kg
01/11/2022
Report * 2022-00308
Page 2 of 4

nvirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 + 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Branch Residuals/Bob Branch Date of Report: Jan 26, 2022
1735 Heckle Blvd Suite 103-291 Customer PO #:
Rock Hill SC 29732 Customer ID: 15060009
Attention: Bob Branch Report #: 2022-00308
Project ID: Wallace WWTP
pH SW 846 Method 9045D 6.87 units 01 /24/2022
Result estimated Analyzed out of 15 minutes hold time
Mercury
TCLP Metals
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Mercury
Lab ID Sample ID:
22-00777 Site:1
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
22-00778 Site:2
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
22-00779 Site:3
Test
Total Solids (%)
Fecal Density
SW-846 7471 B
EPA 2007 Rev 4.4, 1994
EPA 200 7 Rev 4 4, 1994
EPA 200 7 Rev. 4.4, 1994
EPA 200 7 Rev. 4.4, 1994
EPA 200 7 Rev. 4A, 1994
EPA 200 7 Rev 4.4. 1994
EPA 200 7 Rev 4.4, 1994
EPA 245 1
Collect Date/Time
1 /5/2022 8:50 AM
Method
SM 2540 B
SM 9 221 C E-2014
0.956 mg/kg
<1 mg/L
<1 mg/L
<1 mg/L
<1 mg/L
<1 mg/L
<1 mg/L
<1 mg/L
<n nnn,) mnn
01/14/2022
01/14/2022
01/14/2022
01/14/2022
01/14/2022
01/14/2022
01/14/2022
01/14/2022
01/14/2022
Matrix Sampled by
Solid/Sludge InYoung Sea
Results Date Analyzed
2.78 %
612 MPN/g
Collect DatelTime Matrix Sampled by
1/5/2022 8:50 AM Solid/Sludge InYoung Seo
Method
SM 2540 B
SM 9221 C E-2014
Collect Date/Time
1 /512022 8.50 AM
Method
SM 2540 B
SM 9221C E-2014
01/07/2022
01/05/2022
Results Date Analyzed
2.85 % 01 /07/2022
278 MPN/g 01 /05/2022
Matrix Sampled by
Solid/Sludge InYoung Seo
Results Date Analyzed
2.65 % 01 /07/2022
1057 MPN/g 01 /05/2022
Report $ 2022-00308 Page 3 of 4

Facility:
Triple S Farms
Source:
Wallace WWTP
Location:
Wallace, North Carolina
Contractor:
Triple S Farms
Type of Analysis:
Wallace WWTP
Report No:
WL 2-2022-05935
Date Sampled:
4/4/2022 Type of Stabilization: Non
Date Reported:
4/27/202.2
Reporting Period:
2nd Quarter 2022
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
2.53
Nitrogen (TKN)*
6.370
63,700.000
Phosphorus
2.690
26,900.000
Potassium
0.571
5,710.000
Sulfur
0.000
Calcium
2.360
23,600.000
Magnesium
0.437
4,370.000
Sodium
0.529
5,290.000
Iron
---
Aluminum
---
8,530.000
Manganese
---
Copper
---
588.000
1,500
Zinc
---
1,080.000
2,800
Ammonia Nitrogen*
0.507
5,070.000
Nitrate N / Nitrite N*
---
189.000
Cadmium
---
20.800
39
Chromium
---
23.400
1,200
Nickel
---
20.800
420
Lead
---
20.800
300
Arsenic
---
20.800
41
Mercury
---
0.735
17
Selenium
---
20.800
100
pH
7.290
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
5.863
Molybdenum
---
20.800
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Wallace WWTP
Wallace WWTP
Wallace, North Carolina
Triple S Farms
2nd Quarter 2022
Date Reported: 4/27/2022 Report No: WL 2-2022-0593
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
40.626
PAN Inj.
45.696
P
53.800
K
11.420
Lime (estimated)
0.000
Secondary Nutrients
Calcium
47.200
Magnesium
8.740
Sodium
10.580
SAR
1.317
Chloride
0.000
Iron
0.000
Alumium
17.060
Manganese
0.000
Boron
0.000
Sulfur
0.000
Residual Nitrogen Calculation
Year Min Rate PAN #/Acre
% Solids
2.53
pH
7.290
Min Rate
0.300
Metals
Arsenic
0.042
Cadmium
0.042
Chromium
0.047
Copper
1.176
Lead
0.042
Mercury
0.001
Molybdenum
0.042
Nickel
0.042
Seleniun
0.042
Zinc
2.160
2019
2020
2021
2022
0.30
35.18
2023
0.15
12.31
2024
0.08
5.23
2025
0.04
2.42
2026
2027
2028
2029

Environmental Chemists, Inc.
envirotchhem 6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
,a 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info r, em•ironmentalchemists.com
Branch Residuals/Bob Branch
1735 Heckle Blvd Suite 103-291
Rock Hill SC 29732
Attention:
Date of Report: Apr 27, 2022
Customer PO #:
Customer ID: 15060009
Report #: 2022-05935
Project ID: Sludge -Wallace WWTP
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-14372 Site: Sludge
4/4/2022
7:25 AM Solid/Sludge Sean Pistorino
Test
Method
Results Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7, Rev 4.4, 1994
8530 mg/kg
04/14/2022
Arsenic
EPA 200.7, Rev. 4.4, 1994
<20.8 mg/kg
04/14/2022
Cadmium
EPA 200.7, Rev. 4.4, 1994
<20.8 mg/kg
04/14/2022
Calcium
EPA 200.7, Rev. 4 4, 1994
23600 mg/kg
04/14/2022
Chromium
EPA 200.7, Rev. 4.4, 1994
23.4 mg/kg
04/14/2022
Copper
EPA 200.7, Rev. 4 4, 1994
588 mg/kg
04/14/2022
Lead
EPA 200.7, Rev 4.4. 1994
<20.8 mg/kg
04/14/2022
Magnesium
EPA 200.7, Rev. 4.4, 1994
4370 mg/kg
04/14/2022
Molybdenum
EPA 200.7, Rev. 4.4. 1994
<20.8 mg/kg
04/14/2022
Nickel
EPA 200.7, Rev. 4.4, 1994
<20.8 mg/kg
04/14/2022
Potassium
EPA 200.7, Rev. 4.4, 1994
5710 mg/kg
04/14/2022
Selenium
EPA 200.7, Rev. 4A, 1994
<20.8 mg/kg
04/14/2022
Sodium
EPA 200.7, Rev. 4.4, 1994
5290 mg/kg
04/14/2022
Zinc
EPA 200.7, Rev. 4.4, 1994
1080 mg/kg
04/14/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2
189 mg/kg
04/15/2022
Total Solids (%)
SM 2540 B
2.38 %
04/05/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
5070 mg/kg
04/05/2022
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B•2011
63700 mg/kg
04/05/2022
Total Phosphorus
SM 4800 P (F-H)-2011
26900 mg/kg
04/07/2022
pH
SW 846 Method 9045D
7.29 units
04/12/2022
Result estimated Analyzed out of 15 minutes
hold time.
Mercury
SW-846 7471 B
<0.735 mg/kg
04/25/2022
Repon,, # 2022-05935 Page 1 of 3

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Facility:
Triple S Farms
Source:
Wallace WWTP
Location:
Wallace, North Carolina
Contractor:
Triple S Farms
Type of Analysis:
Wallace WWTP
Report No:
WL 3-2022-13026
Date Sampled:
7/12/2022 Type of Stabilization: Non
Date Reported:
8/5/2022
Reporting Period:
3rd Quarter 2022
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
2.52
Nitrogen (TKN)*
6.880
68,800.000
Phosphorus
2.200
22,000.000
Potassium
0.488
4,880.000
Sulfur
0.000
Calcium
2.490
24,900.000
Magnesium
0.434
4,340.000
Sodium
0.529
5,290.000
Iron
---
Aluminum
---
8,310.000
Manganese
---
Copper
---
632.000
1,500
Zinc
---
1,170.000
2,800
Ammonia Nitrogen*
1.370
13,700.000
Nitrate N / Nitrite N*
---
3.160
Cadmium
---
20.600
39
Chromium
---
25.300
1,200
Nickel
---
20.600
420
Lead
---
25.000 ;
300
Arsenic
---
25.100
41
Mercury
---
0.909
17
Selenium
---
20.600
100
pH
8.190
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
5.510
Molybdenum
---
20.600
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Wallace WWTP
Wallace WWTP
Wallace, North Carolina
Triple S Farms
3rd Quarter 2022
Date Reported: 8/5/2022 Report No: WL 3-2022-1302
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
46.766
PAN Inj.
60.466
P
44.000
K
9.760
Lime (estimated)
0.000
Secondary Nutrients
Calcium
49.800
Magnesium
8.680
Sodium
10.580
SAR
1.288
Chloride
0.000
Iron
0.000
Alumium
16.620
Manganese
0.000
Boron
0.000
Sulfur
0.000
Residual Nitrogen Calculation
Year Min Rate PAN #/Acre
% Solids
2.52
pH
8.190
Min Rate
0.300
Metals
Arsenic
0.050
Cadmium
0.041
Chromium
0.051
Copper
1.264
Lead
0.050
Mercury
0.002
Molybdenum
0.041
Nickel
0.041
Seleniun
j 0.041
Zinc
1 2.340
2019
2020
2021
2022
0.30
33.06
2023
0.15
11.57
2024
0.08
4.92
2025
0.04
2.27
2026
2027
2028
2029

rw-- --qN Environmental Chemists, Inc.
envirochem 6602 Windmill VVay, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392 4424 Fax
710 Bowserto;vn Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A bVilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL 8 CONSULTING CHEMISTS info-u environnientalcheniists.eam
Branch Residuals/Bob Branch
1735 Heckle Blvd Suite 103-291
Rock Hill SC 29732
Attention: Bob Branch
Date of Report: Aug 05, 2022
Customer PO #:
Customer ID: 15060009
Report #: 2022-13026
Project ID: Wallace WWTP
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-31650 Site: Sludge
7/12/2022
10:15 AM Solid/Sludge Sean Pistorino
Test
Method
Results Date
Analyzed
Sludge Residuals
Aluminum
EPA 200.7, Rev, 4.4, 1994
8310 mg/kg
07/19/2022
Arsenic
EPA 200 7, Rev, 4 4, 1994
25.1 mg/kg
07/19/2022
Cadmium
EPA 200 7. Rev. 4.4, 1994
<20.6 mg/kg
07/19/2022
Calcium
EPA 200 7 Rev. 4.4 1994
24900 mg/kg
07/19/2022
Chromium
EPA 200 7, Rev 4 4, 1994
25.3 mg/kg
07/19/2022
Copper
EPA 200.7, Rev. 4 4.1994
632 mg/kg
07/19/2022
Lead
EPA 200 7, Rev. 4 4, 1994
25.0 mg/kg
07/19/2022
Magnesium
EPA 200.7, Rev. 4 4, 1994
4340 mg/kg
07/19/2022
Molybdenum
EPA 200.7, Rev. 4.4, 1994
<20.6 mg/kg
07/19/2022
Nickel
EPA 200.7, Rev. 4 4, 1994
<20.6 mg/kg
07/19/2022
Potassium
EPA 200.7, Rev. 4 4, 1994
4880 mg/kg
07/19/2022
Selenium
EPA 200.7, Rev. 4 4, 1994
<20.6 mg/kg
07/1912022
Sodium
EPA 200.7, Rev. 4 4, 1994
5290 mg/kg
07/19/2022
Zinc
EPA 200.7, Rev. 4.4, 1994
1170 mg/kg
07/19/2022
Nitrate+Nitrite-Nitrogen
EPA353.2
3.16mg/kg
07/19/2022
Total Solids (%)
SM 2540 B
2.42 %
07/14/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
13700 mg/kg
07/14/2022
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
68800 mg/kg
07/15/2022
Total Phosphorus
SM 4500 P (F-H)-2011
22000 mg/kg
07/21/2022
pH
SW 846 Method 9045D
8.19 units
07/29/2022
Result estimated Analyzed out of 15 minutes hold time
Mercury
SW-846 7471 B
0.909 mg/kg
07/18/2022
Report # 2022-13026 Page 1 of 3

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Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms
Wallace WWTP
Wallace, North Carolina
Triple S Farms
Wallace WWTP
WL 4-2022-22651
11/14/2022 Type of Stabilization: Lime
12/16/2022
4th Quarter 2022
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
3.31
Nitrogen (TKN)*
5.430
54,300.000
Phosphorus
1.990
19,900.000
Potassium
0.387
3,870.000
Sulfur
0.000
Calcium
2.210
22,100.000
Magnesium
0.350
3,500.000
Sodium
0.441
4,410.000
Iron
---
Aluminum
---
7,950.000
Manganese
---
Copper
---
589.000
1,500
Zinc
---
1,050.000
2,800
Ammonia Nitrogen*
0.341
3,410.000
Nitrate N / Nitrite N*
---
12.500
Cadmium
---
14.700
39
Chromium
---
26.600
1,200
Nickel
---
15.500
420
Lead
---
28.500
300
Arsenic
---
14.700
41
Mercury
---
0.731
17
Selenium
---
14.700
100
pH
7.540
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
5.089
Molybdenum
---
14.700
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Wallace WWTP
Wallace WWTP
Wallace, North Carolina
Triple S Farms
4th Quarter 2022
Date Reported: 12/16/2022 Report No: WL 4-2022-22651
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
33.969
PAN Inj.
37.379
P
39.800
K
7.740
Lime (estimated)
0.000
Secondary Nutrients
Calcium
44.200
Magnesium
7.000
Sodium
8.820
SAR
1.320
Chloride
0.000
Iron
0.000
Alumium
15.900
Manganese
0.000
Boron
0.000
Sulfur
0.000
Residual Nitrogen Calculation
Year Min Rate PAN #/Acre
Physical Characteristics
% Solids
3.31
pH
7.540
Min Rate
0.300
Metals
Arsenic
0.029
Cadmium
0.029
Chromium
0.053
Copper
1.178
Lead
0.057
Mercury
0.001
Molybdenum
0.029
Nickel
0.031
Seleniun
0.029
Zinc
2.100
2019
2020
2021
2022
0.30
30.53
2023
0.15
10.69
2024
0.08
4.54
2025
0.04
2.10
2026
2027
2028
2029

rn:viroiche6 m
ANALYTICAL & CONSULTING CHEMISTS
Branch Residuals/Bob Branch
1735 Heckle Blvd Suite 103-291
Rock Hill SC 29732
Attention:
Lab ID Sample ID:
22-55615 Site: WWTP
Test
Sludge Residuals
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Nitrate+Nitrite-Nitrogen
Total Solids (%)
Ammonia Nitrogen
Total Kjeldahl Nitrogen (TKN)
Total Phosphorus
Environmental Chemists, Inc.
6602 Windmill Way Wilmington, NC 28405 ' 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
info a env ironmentalchemists. com
Date of Report: Dec 16, 2022
Customer PO #:
Customer ID: 15060009
Report #: 2022-22651
Project ID: Wallace WWTP
Collect Date/Time Matrix
11/14/2022 8:40 AM Solid/Sludge
Method
EPA 200.7, Rev. 4 4, 1994
EPA 200.7, Rev 4 4, 1994
EPA 200.7, Rev. 4 4, 1994
EPA 200.7. Rev 4 4, 1994
EPA 200.7, Rev. 4 4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev 4 4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7. Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 353.2
SM 2540 B
SM 4500 NH3 C-2011
SM 4500 Norg B-2011
SM 4500 P (F-H)-2011
pH SW 846 Method 9045D
Result estimated. Analyzed out of 15 minutes hold time.
Mercury
SW-846 7471 B
Results
Sampled by
Sean Pistorino
Date Ana
7950mg/kg
11/16/2022
<14.7mg/kg
11/16/2022
<14.7 mg/kg
11/16/2022
22100mg/kg
11/16/2022
26.6mg/kg
11/16/2022
589mg/kg
11/16/2022
28.5 mg/kg
11/16/2022
3500 mg/kg
11/16/2022
<14.7 mg/kg
11/16/2022
15.5 mg/kg
11/16/2022
3870 mg/kg
11/16/2022
<14.7mg/kg
11/16/2022
4410 mg/kg
12/08/2022
1050mg/kg
11/16/2022
12.5 mg/kg
11/15/2022
3.31 %
11/15/2022
3410mg/kg
11/15/2022
54300 mg/kg
11/15/2022
19900 mg/kg
11 /23/2022
7.54units
11/30/2022
0.731 mg/kg 12/09/2022
Report p 2022-22651 Page 1 of 3

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Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Town of Warsaw
Warsaw WWTP
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
WS 2022-11184
6/15/2022
7/15/2022
Annual 2022
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
2.100
Nitrogen (TKN)
2.130
21,300.000
Phosphorus
1.160
11,600.000
Potassium
0.367
3,670.000
Sulfur
0.000
Calcium
2.480
24,800.000
Magnesium
0.160
1,600.000
Sodium
0.338
3,380.000
Iron
---
Aluminum
---
7,480.000
Manganese
---
Copper
---
248.000
1,500
Zinc
---
681.000
2,800
Ammonia Nitrogen
0.000
4.760
Nitrate N / Nitrite N
---
1,970.000
Cadmium
---
12.300
85
Chromium
---
18.200
1,200
Nickel
---
12.300
420
Lead
---
25.400
300
Arsenic
---
12.300
75
Mercury
---
0.905
17
Selenium
---
12.300
100
pH
4.330
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
2.130
Molybdenum
---
15.100
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Wastewater Treatment Plant
Warsaw WWTP
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
Annual 2022
Date Reported: 7/15/2022 Report No: WS 2022-11184
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
16.722
PAN Inj.
16.727
P
23.200
K
7.340
Lime (estimated)
0.000
Secondary Nutrients
Calcium
49.600
Magnesium
3.200
Sodium
6.760
SAR
0.813
Chloride
0.000
Iron
0.000
Alumium
14.960
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
2.10
pH
4.330
Min Rate
0.300
Metals
Arsenic
0.025
Cadmium
0.025
Chromium
0.036
Copper
0.496
Lead
0.051
Mercury
0.002
Molybdenum
0.030
Nickel
0.025
Seleniun
0.025
Zinc
1.362

Environmental Chemists,
Inc.
envirochem
6602 Windmill Way,
Wilmington, NC 28405 0 910,392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Pax
255-A Wilmington Highway, Jacksonville, NC 28540 0 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
[e-mail]
Town of Warsaw
Date of Report; Jul 15, 2022
PO Box 464
Customer PO M
Warsaw NC 28398
Customer ID: 09070029
Attention: Greg Hughes
Report M 2022-11184
Project ID: Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-27072 Site: Sludge
6/15/2022
8:00 AM Solid/Sludge Greg Hughes
Test
Method
Results Date Analyzed
Chlordane (TCLP)
sw-e40 60818
<0.02 mg/L
06/23/2022
Endrin (TCLP)
SW-840 6001 B
<0.0005 mg/L
06/23/2022
Heptachlor (TCLP)
Sw-8466081 B
<0.0005mg/L
06/23/2022
Heptachlor epoxide (TCLP)
SW-646 0081 B
<0.0005 mg/L
06/23/2022
Undane (TCLP)
SW-846 8081 B
<0.0005 mg/L
06/23/2022
Methoxychlor (TCLP)
SW-846 60818
<0.0005 mg/L
06/23/2022
Toxaphene (TCLP)
SW-046 00010
<0.05 mg/L
06/23/2022
2,4,5-TP (TCLP)
SW-846 8161 A
<0.003 mg/L
06/29/2022
2,4-D (TCLP)
SW-846 8151 A
<0.003 mg/L
06/29/2022
1,4-Dichlorobenzene (TCLP)
SW-848 8270 E
<0.050 mg/L
06/21/2022
2,4,5-Trichlorophenol (TCLP)
SW-6488270E
<0,050mg/L
06/21/2022
2,4,6-Trichlorophenol (TCLP)
SW-846 6270 E
<0.050 mg/L
06/21/2022
2,4-Dinitrotoluene (TCLP)
SW-e46 8270 E
<0.050 mg/L
06/21/2022
Cresol (TCLP)
SW-046 8270 E
<0.050 mg/L
06/21/2022
Hexachloro-1,3-butadiene (TCLP)
SW-8466270E
<0.050mg/L
06/21/2022
Hexachlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
06/21/2022
Hexachloroethane (TCLP)
SW-846 6270 E
<0.050 mg/L
06/21/2022
m + p-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
06/21/2022
Nitrobenzene (TCLP)
Sw-8468270 E
<0.050 mg/L
06/21/2022
o-Cresol (TCLP)
SW-848 8270 E
<0.050 mg/L
06/21/2022
Pentachlorophenol (TCLP)
SW-846 8270 E
<0.250 mg/L
06/21/2022
Pyridine (TCLP)
SW-846 8270 E
<0.050 mg/L
06/21/2022
1,1-Dichloroethylene (TCLP)
SW-846 Method8260D
<0.01 mg/L
06/23/2022
1,2-Dichloroethane (TCLP)
SW-848 Method8260D
<0.01 mg/L
06/23/2022
Benzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
06/23/2022
Carbon Tetrachloride (TCLP)
SW-846 Method e260D
<0.01 mg/L
06/23/2022
Report #.: 2022-11184
Page 1 of 3

[en7virochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ° 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info(rz cnvironnlentnlchemists.coni
Town of Warsaw
Date of Report: Jul 15, 2022
PO Box 464
Customer PO #:
Warsaw NC
28398
Customer ID: 09070029
Attention: Greg Hughes
Report #: 2022-11184
Project ID: Sludge
Chlorobenzene (TCLP)
SW-846 Method 6260D
<0.01 mg/L
06/23/2022
Chloroform (TCLP)
SW-046 Method 6260D
<0.01 mg/L
06/23/2022
Methyl ethyl ketone (TCLP)
SW846 Method 0260D
<0.05 mglL
06/23/2022
Tetrachloroethylene (TCLP)
SW-846 Method 6280D
<0.01 mg/L
06/23/2022
Trichloroethylene (TCLP)
SW-846 Method 0200D
<0.01 mg/L
06/23/2022
Vinyl Chloride (TCLP)
SW-846 Method 8260D
<0.01 mg/L
06/23/2022
RCI
Cyanide
SM 4500 CN D-2016
<1.0 mg/kg
06/20/2022
Sulfide
SM 4500 S D
0.09 mg/kg
06/24/2022
Ignitability
SW 846 method 1010
>157 °F
06/29/2022
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4, 1994
7480 mg/kg
06/20/2022
Arsenic
EPA 200.7, Rev. 4.4, 1994
<12,3 mg/kg
06/20/2022
Cadmium
EPA 200.7. Rev. 4.4. 1994
<12.3 mg/kg
06/20/2022
Calcium
EPA 200.7, Rev. 4.4, 1094
24800 mg/kg
06/20/2022
Chromium
EPA 200.7, Rev. 4.4, 1904
18.2 mg/kg
06/20/2022
Copper
EPA 200.7, Rev. 4.4, 1094
248 mg/kg
06/20/2022
Lead
EPA 2003, Rev. 4.4, 1994
25.4 mg/kg
06/20/2022
Magnesium
EPA 200.7, Rev. 4.4, 1994
1600 mg/kg
06/20/2022
Molybdenum
EPA 200.7, Rev. 4.4,1904
15.1 mg/kg
06/20/2022
Nickel
EPA 200.7, Rev. 4.4, 1094
<12.3 mg/kg
06/20/2022
Potassium
EPA 200.7, Rev. 4.4, 1994
3670 mg/kg
06/29/2022
Selenium
EPA 200.7, Rev. 4.4, 1994
<12,3 mg/kg
06/20/2022
Sodium
EPA 200.7, Rev. 4.4, 1994
3380 mg/kg
06/20/2022
Zinc
EPA 200.7, Rev. 4.4, 1994
681 mg/kg
06/20/2022
Nitrate+Nitrite-Nitrogen
EPA 363 2
1970 mg/kg
06/28/2022
Total Solids (%)
SM 2640 a
2.10 %
06/16/2022
Ammonia Nitrogen
SM 4600 NH3 C-2011
<4.76 mg/kg
06/20/2022
Total Kjeldahl Nitrogen (TKN)
SM 4600 Norg B-2011
21300 mg/kg
06/20/2022
Total Phosphorus
SM 4600 P (F-H).2011
11600 mg/kg
06/22/2022
Report #:; 2022-11184
Page 2 of 3

;SFA
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab ° 910.392.4424 Fax
710 Rowsertown Road, Manteo, NC 27954 d 252.473.5702 Lab/Fax
255-A Wilmington Highway, jacksonville, NC 28540 V 910.347.5843 Lab/Fax
info(a>environmentnlchemists,com
Town of Warsaw
PO Box 464
Warsaw NC
Attention: Greg Hughes
28398
Date of Report: Jul 15, 2022
Customer PO #:
Customer ID: 09070029
Report #: 2022-11184
Project10: Sludge
pH
SW 846 Method 9045D
4.33 units
06/28/2022
Result estimated. Analyzed
out of 15 minutes hold time.
Mercury
SW-e487471 B
0.905mg/kg
06/17/2022
TCLP Metals
Arsenic
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
06/28/2022
Barium
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
06/28/2022
Cadmium
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
06/28/2022
Chromium
EPA 200.7, Rev. 4.4, 1094
<1.0 mg/L
06/28/2022
Lead
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
06/28/2022
Selenium
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
06/28/2022
Silver
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
06/28/2022
Mercury
EPA 245.1
<0.0002 mg/L
06/28/2022
Comment: Results, except pH, reported on a dry weight basis.
pH reported on an as received basis.
1
Reviewed by:�,�QS�{P
Report #:: 2022.11104 Page 3 of 3

TOXICITY CHARACTERISTICS LEACHING PROCEDURE
(TCLP) ANALYSIS REPORTS

A TCLP ANALYSIS IS REQUIRED FOR THE FOLLOWING FACILITIES:
TOWN OF WALLACE
TOWN OF CLAYTON
TCLP DATA IS REQUIRED ONCE PER PERMIT CYCLE
FOR THE OTHER FACILITIES
TCLP IS REQUIRED FOR NORTHWEST REGIONAL WWTP, BUT THAT FACILITY
WAS NOT LAND APPLIED UNDER THIS PERMIT.

Waypoint'(2)
ANALYTICAL
3/8/2022
Town Of Clayton
POB 879
Clayton, NC, 27528
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Ref: Analytical Testing
Report Number: 22-054-0012
Project Description: Holding Tank #1
Waypoint Analytical Virginia, Inc. received sample(s) on 2/23/2022 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Tawfc Mt &10".
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 10

(2)
Waypoint,7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 22-054-0012
Client Project Description: Holding Tank #1
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
56792
Holding Tank #1
Solids
02/22/2022 11:00
02/23/2022
SW-7.3.3
WP MTN
56792
Holding Tank #1
Solids
02/22/2022 11:00
02/23/2022
SW-9045C
WP MTN
56792
Holding Tank #1
Solids
02/22/2022 11:00
02/23/2022
ASTM D93-80
WP MTN
56792
Holding Tank #1
Solids
02/22/2022 11:00
02/23/2022
SW-7.3.4
WP MTN
56793
Holding Tank #1
TCLP
02/22/2022 11:00
02/23/2022
8270C
WP MTN
56793
Holding Tank #1
TCLP
02/22/2022 11:00
02/23/2022
6010D
WP MTN
56793
Holding Tank #1
TCLP
02/22/2022 11:00
02/23/2022
SW-1311 (ZHE)
WP MTN
56793
Holding Tank #1
TCLP
02/22/2022 11:00
02/23/2022
8151A
WP MTN
56793
Holding Tank #1
TCLP
02/22/2022 11:00
02/23/2022
SW-1311
WP MTN
56793
Holding Tank #1
TCLP
02/22/2022 11:00
02/23/2022
8260B
WP MTN
56793
Holding Tank #1
TCLP
02/22/2022 11:00
02/23/2022
8081A
WP MTN
56793
Holding Tank #1
TCLP
02/22/2022 11:00
02/23/2022
7470A
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 10

•
Waypoint. 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46546
Town Of Clayton Project Holding Tank #1
POB 879 Report Date : 03/08/2022
Information : Received : 02/23/2022
Clayton , NC 27528
Tcuvi c MC 6/00
K/
Report Number: 22-054-0012 REPORTOFANALYSIS Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No : 56792 Matrix: Solids
Sample ID : Holding Tank #1 Sampled: 2/22/2022 11:00
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Sulfide (Reactivity)
<25.0
mg/Kg 25.0
1 03/02/22 11:18
FMM
SW-7.3.4
Cyanide (Reactivity)
<0.125
mg/Kg 0.125
1 03/02/22 11:18
FMM
SW-7.3.3
Ignitability
>96
degrees C
1 03/04/22 09:47
OR
ASTM D93-80
pH
6.5
SM.
1 03/07/2215:40
ADM
SW-9045C
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 10

0
Waypoint.
7621 Whitepine Road, Richmond,
VA 23237
Main 804-743-9401 ° Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
46546
Town Of Clayton
Project
Holding Tank #1
POB 879
Report
Date : 03/08/2022
Information :
Received : 02/23/2022
Clayton , NC 27528
�cuy,c
P1t G/ow�y/
Pauric Mc Groary Ph.D., CPA
Report Number: 22-054-0012
REPORT OFANALYSIS
Agronomist
Lab No : 56793
Matrix:
TCLP
Sample ID : Holding Tank #1
Sampled: 2/22/2022 11:00
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
TCLP Herbicide Extraction
Leachate
1
02/28/22 12:00
PHE
SW-1311
TCLP Metals Extraction
Leachate
1
02/28/22 12:00
PHE
SW-1311
TCLP Pesticide Extraction
Leachate
1
02/28/22 12:00
PHE
SW-1311
TCLP SVOC Extraction
Leachate
1
02/28/22 12:00
PHE
SW-1311
TCLP VOC ZHE Extraction
Leachate
1
02/28/22 12:00
PLD
SW-1311 (ZHE)
Analytical Method: 6010D
Prep Batch(es):
L602415
03/02/22 09:54
Prep Method: 3015A
Test
Results
Units
MOL
DF
Date / Time
By
Analytical
Analyzed
Batch
TCLP Arsenic
<0.250
mg/L
0.250
1
03/02/22 17:21
EAL
L602661
TCLP Barium
<0.250
mg/L
0.250
1
03/02/22 17:21
EAL
L602661
TCLP Cadmium
<0.0500
mg/L
0.0500
1
03/02/22 17:21
EAL
L602661
TCLP Chromium
<0.100
mg/L
0.100
1
03/02/22 17:21
EAL
L602661
TCLP Lead
<0.100
mg/L
0.100
1
03/02/22 17:21
EAL
L602661
TCLP Selenium
<0.500
mg/L
0.500
1
03/02/22 17:21
EAL
L602661
TCLP Silver
<0.0500
mg/L
0.0500
1
03/02/22 17:21
EAL
L602661
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 10

Waypointo
ANALYTICAL
46546
Town Of Clayton
POB 879
Clayton , NC 27528
Report Number:22-054-0012
Lab No : 56793
Sample ID: Holding Tank #1
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project Holding Tank #1
Information :
REPORT OFANAL YSIS
Report Date : 03/08/2022
Received : 02/23/2022
Touy,c t if/owyr
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: TCLP
Sampled: 2/ 22/ 2022 11:00
Analytical Method: 7470A Prep Batch(es): L602120 03/01/22 09:30
Prep Method: 7470A
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
TCLP Mercury
Analytical Method: 8081A
Prep Method: 3510C
Test
TCLP Endrin
TCLP gamma-BHC
TCLP Methoxychlor
TCLP Toxaphene
TCLP Chlordane
TCLP Heptachlor Epoxide
TCLP Heptachlor
Surrogate: Decachlorobiphenyl
Surrogate: Tetrachloro-m-xylene
Analytical Method: 8151A
Prep Method: 8151A
Test
<0.0200 mg/L 0.0200 1 03/01/2215:43 JW2 L602292
Prep Batch(es): L602520 03/02/22 13:45
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
<0.001600
mg/L
0.001600
10
03/04/22
03:33
VIC
L603012
<0.001600
mg/L
0.001600
10
03/04/22
03:33
VIC
L603012
<0.001600
mg/L
0.001600
10
03/04/22
03:33
VIC
L603012
<0.01200
mg/L
0.01200
10
03/04/22
03:33
VIC
L603012
<0.008000
mg/L
0.008000
10
03/04/22
03:33
VIC
L603012
<0.001600
mg/L
0.001600
10
03/04/22
03:33
VIC
L603012
<0.001600
mg/L
0.001600
10
03/04/22
03:33
VIC
L603012
66.00
Limits: 34-116%
10 03/04/22 03:33 VIC
L603012
49.67
Limits: 25-123%
10 03/04/22 03:33 VIC
L603012
Prep Batch(es):
L602317 03/01/22
17:30
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
TCLP 2,4-D <0.0200 mg/L 0.0200 1 03/03/22 01:47 VIC L602760
TCLP 2,4,5-TP (Silvex) <0.0020 mg/L 0.0020 1 03/03/22 01:47 VIC L602760
Surrogate: DCAA 65.20 Limits: 20-120% 1 03/03/22 01:47 VIC L602760
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 5 of 10

Waypointo
ANALYTICAL
46546
Town Of Clayton
POB 879
Clayton , NC 27528
Report Number:22-054-0012
Lab No : 56793
Sample ID : Holding Tank #1
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project Holding Tank #1
Information :
REPORT OFANAL YSIS
Report Date: 03/08/2022
Received : 02/23/2022
TONIC tt1C Gfowyr
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: TCLP
Sampled: 2/ 22/ 2022 11:00
Analytical Method: 8260E
Prep Batch(es):
L602407 03/01/22 08:57
Prep Method: 5030B
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
TCLP Benzene
<0.0100
mg/L
0.0100
1
03/01/22 20:09
MKD
L602473
TCLP Carbon Tetrachloride
<0.0100
mg/L
0.0100
1
03/01/22 20:09
MKD
L602473
TCLP Chlorobenzene
<0.0100
mg/L
0.0100
1
03/01/22 20:09
MKD
L602473
TCLP Chloroform
<0.0100
mg/L
0.0100
1
03/01/22 20:09
MKD
L602473
TCLP 1,4-Dichlorobenzene
<0.0100
mg/L
0.0100
1
03/01/22 20:09
MKD
L602473
TCLP 1,2-Dichloroethane
<0.0100
mg/L
0.0100
1
03/01/22 20:09
MKD
L602473
TCLP 1,1-Dichloroethene
<0.0100
mg/L
0.0100
1
03/01/22 20:09
MKD
L602473
TCLP Methyl Ethyl Ketone (MEK)
<0.200
mg/L
0.200
1
03/01/22 20:09
MKD
L602473
TCLP Tetrachloroethene
<0.0100
mg/L
0.0100
1
03/01/22 20:09
MKD
L602473
TCLP Trichloroethene
<0.0100
mg/L
0.0100
1
03/01/22 20:09
MKD
L602473
TCLP Vinyl Chloride
<0.0100
mg/L
0.0100
1
03/01/22 20:09
MKD
L602473
Surrogate: 4-Bromofluorobenzene
91.2
Limits: 71-137%
1 03/01/22 20:09 MKD
L602473
Surrogate: Dibromofluoromethane
81.8
Limits: 70-128%
1 03/01/22 20:09 MKD
L602473
Surrogate: 1,2-Dichloroethane - d4
88.6
Limits: 63-136%
1 03/01/22 20:09 MKD
L602473
Surrogate: Toluene-d8
91.2
Limits: 70-130%
1 03/01/22 20:09 MKD
L602473
Analytical Method: 8270C
Prep Batch(es):
L602981 03/04/22 09:45
Prep Method: 3510C
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
TCLP 2-Methylphenol
<0.100
mg/L
0.100
5
03/04/22 18:37
VBW
L603155
TCLP 3&4 Methylphenol
<0.200
mg/L
0.200
5
03/04/22 18:37
VBW
L603155
TCLP 2,4-Dinitrotoluene
<0.100
mg/L
0.100
5
03/04/22 18:37
VBW
L603155
Qualifiers/ DF Dilution Factor
MQL
Method Quantitation Limit
Definitions
Page 6 of 10

Waypointo
ANALYTICAL
46546
Town Of Clayton
POB 879
Clayton , NC 27528
Report Number: 22-054-0012
Lab No : 56793
Sample ID : Holding Tank #1
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project Holding Tank #1
Information :
REPORT OPANAL YSIS
Report Date : 03/08/2022
Received : 02/23/2022
low t (to'T
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: TCLP
Sampled: 2/ 22/2022 11:00
Analytical Method: 8270C Prep Batch(es): L602981 03/04/22 09:45
Prep Method: 3510C
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
TCLP Hexachlorobenzene
<0.100
mg/L
0.100
5
03/04/22 18:37 VBW
L603155
TCLP Hexachlorobutadiene
<0.100
mg/L
0.100
5
03/04/22 18:37 VBW
L603155
TCLP Hexachloroethane
<0.100
mg/L
0.100
5
03/04/22 18:37 VBW
L603155
TCLP Nitrobenzene
<0.100
mg/L
0.100
5
03/04/22 18:37 VBW
L603155
TCLP Pentachlorophenol
<0.200
mg/L
0.200
5
03/04/22 18:37 VBW
L603155
TCLP Pyridine
<0.100
mg/L
0.100
5
03/04/22 18:37 VBW
L603155
TCLP 2,4,5-Trichlorophenol
<0.100
mg/L
0.100
5
03/04/22 18:37 VBW
L603155
TCLP 2,4,6 Trichlorophenol
<0.100
mg/L
0.100
5
03/04/22 18:37 VBW
L603155
Surrogate: TCLP 2,4,6 Tribromophenol
46.3
Limits: 42-102%
5 03/04/22 18:37 VBW
L603155
Surrogate: TCLP 2-Fluorobiphenyl
41.8
Limits: 24-86%
5 03/04/22 18:37 VBW
L603155
Surrogate: TCLP 2-Fluorophenol
17.5
Limits: 13-37%
5 03/04/22 18:37 VBW
L603155
Surrogate: TCLP 4-Terphenyl-d14
53.0
Limits: 30-122%
5 03/04/22 18:37 VBW
L603155
Surrogate: TCLP Nitrobenzene-d5
47.3
Limits: 25-78%
5 03/04/22 18:37 VBW
L603155
Surrogate: TCLP Phenol-d6
12.3
Limits: 9-27%
5 03/04/22 18:37 VBW
L603155
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 7 of 10

Waypdlont.(2)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Client: Town Of Clayton CASE NARRATIVE
Project: Holding Tank #1
Lab Report Number: 22-054-0012
Date: 3/7/2022
Flashpoint Method ASTM D93-80
QC Batch No: L603119
The sample analysis was performed using a modified version of the reference method. Due to the sample matrix,
the continual stirring required by the method had to be omitted.
Semivolatile Organic Compounds - GC/MS (TCLP) Method 8270D
Sample 56793 (Holding Tank #1)
QC Batch No: 1-603155/1-602981
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Page 8 of 10

Waypoint(D
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46546
Customer Name: Town Of Clayton
Report Number: 22-054-0012
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F 1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
0 Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) [_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments:
0 Yes 0 No
Signature: iBrandi Watson Date & Time: , 2/23/2022 14:03:23
Page 9 of 10

�J
Page 10 of 10

renvirochem i:;A
6
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Branch Residuals/Bob Branch
Date of Report:
Jan 26, 2022
1735 Heckle Blvd Suite 103-291
Customer PO #:
Rock Hill SC 29732
Customer ID:
15060009
Attention: Bob Branch
Report #:
2022-00308
Project ID: Wallace WWTP
Lab ID Sample ID:
Collect Date/Time Matrix
Sampled by
22-00775 Site: Sludge
1/5/2022 8:50 AM Solid/Sludge
InYoung Seo
Test Method Results Date Analyzed
Chlordane (TCLP)
SW-846 8081 B
<0.02 mg/L
01/12/2022
Endrin (TCLP)
SW-8466081 B
<0.0005mg/L
01/12/2022
Heptachlor (TCLP)
SW-846 8081 8
<0.0005 mg/L
01/12/2022
Heptachlor epoxide (TCLP)
SW-846 8081 B
<0.0005 mg/L
01/12/2022
Lindane (TCLP)
SW-846 8081 B
<0.0005mg/L
01/12/2022
Methoxychlor (TCLP)
SW-846 8081 B
<0.0005mg/L
01/12/2022
Toxaphene (TCLP)
SW-846 8081 B
<0.05mg/L
01/12/2022
2,4,5-TP (TCLP)
SW-846 8151 A
<0.003 mg/L
01/11/2022
2,4-D (TCLP)
SW-846 8151 A
<0.003 mg/L
01/11/2022
1,4-Dichlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
01/11/2022
2,4,5-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
01/11/2022
2,4,6-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
01/11/2022
2,4-Dinitrotoluene (TCLP)
SW-846 8270 E
<0.050 mg/L
01/11/2022
Cresol (TCLP)
SW-8468270E
<0.050mg/L
01/11/2022
Hexachloro-1,3-butadiene (TCLP)
SW-8468270E
<0.050mg/L
01/11/2022
H exachloro benzene (TCLP)
SW-8468270E
<0.050mg/L
01/11/2022
Hexachloroethane (TCLP)
SW-846 8270 E
<0.050 mg/L
01/11/2022
m + p-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
01/11/2022
Nitrobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
01/11/2022
o-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
01/11/2022
Pentachlorophenol (TCLP)
SW-846 8270 E
<0.250 mg/L
01/11/2022
Pyridine (TCLP)
SW-8468270E
<0.050mg/L
01/11/2022
1 1-Dichloroethylene (TCLP)
SW-846 Method82600
<0.01 mg/L
01/19/2022
1,2-Dichloroethane (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/19/2022
Benzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/19/2022
Carbon Tetrachloride (TCLP)
SW-846 Method 82600
<0.01 mg/L
01/19/2022
Report # 2022-00308 Page 1 of 4

r000-.— --� Environmental Chemists, Inc.
11-7
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 + 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Branch Residuals/Bob Branch
Date of Report: Jan 26, 2022
1735 Heckle Blvd Suite 103-291
Customer PO #:
Rock Hill SC 29732
Customer ID: 15060009
Attention: Bob Branch
Report #: 2022-00308
Project ID: Wallace WWTP
Chlorobenzene (TCLP)
SW-846 Method 8250D
<0.01 mg/L
01/19/2022
Chloroform (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/19/2022
Methyl ethyl ketone (TCLP)
SW-846 Method 6260D
<0.05 mg/L
01/19/2022
Tetrachloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/19/2022
Trichloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/19/2022
Vinyl Chloride (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/19/2022
RCI
Cyanide
SM 4500 CN D
<1.0 mg/kg
01 /11/2022
Sulfide
SM 4500 S D
0.26 mg/kg
01 /21/2022
Ignitability
SW 846 method 1010
>157 °F
01/10/2022
Sludge Residuals
Aluminum
EPA 2007,Rev 4 4. 1994
14300mg/kg
01/11/2022
Arsenic
EPA 200 7, Rev 4 4, 1994
<30.4 mg/kg
01/11/2022
Cadmium
EPA 200.7, Rev. 4.4, 1994
<30.4 mg/kg
01/11/2022
Calcium
EPA 200.7, Rev. 4.4, 1994
32300 mg/kg
01/11/2022
Chromium
EPA 200 7, Rev. 4.4, 1994
44.9 mg/kg
01/11/2022
Copper
EPA 200.7, Rev. 4.4, 1994
987 mg/kg
01/11/2022
Lead
EPA 200.7, Rev. 4.4, 1994
42.6 mg/kg
01111 /2022
Magnesium
EPA 200.7, Rev 4.4, 1994
5070 mg/kg
01/11/2022
Molybdenum
EPA 200.7, Rev. 4.4, 1994
<30.4 mg/kg
01/11/2022
Nickel
EPA 200.7, Rev. 4.4, 1994
<30.4 mg/kg
01/11/2022
Potassium
EPA 200.7. Rev. 4.4, 1994
6040 mg/kg
01/11/2022
Selenium
EPA 200.7, Rev 4 4 1994
<30.4 mg/kg
01/11/2022
Sodium
EPA 200.7, Rev 4 4, 1994
4640 mg/kg
01/11/2022
Zinc
EPA 200.7,Rev 4 4. 1994
1710mg/kg
01/11/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2
427 mg/kg
01/06/2022
Total Solids (%)
SM 2540 B
2.25 %
01/07/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
<4.44 mg/kg
01/07/2022
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
39600 mg/kg
01/07/2022
Total Phosphorous
SM 4500 P (F-H)-2011
26400 mg/kg
01/11/2022
Report # 2022-00308
Page 2 or 4

envirochem
6111, L-.�a4
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
infotaemvironmentalchemists.com
Branch Residuals/Bob Branch Date of Report: Jan 26, 2022
1735 Heckle Blvd Suite 103-291 Customer PO #:
Rock Hill SC 29732 Customer ID: 15060009
Attention: Bob Branch Report #: 2022-00308
Project ID: Wallace WWTP
pH SW 846 Method 9045D 6.87 units 01/24/2022
Result estimated Analyzed out of 15 minutes hold time.
Mercury SW-8467471 B 0.956mg/kg 01/14/2022
TCLP Metals
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Mercury
Lab ID Sample ID:
22-00777 Site:1
Test
Total Solids (%
Fecal Density
Lab ID Sample ID:
22-00778 Site:2
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
22-00779 Site:3
Test
Total Solids (%)
Fecal Density
EPA 200 7 Rev. 4.4, 1994
EPA 200 7 Rev 4 4, 1994
EPA 200 7 Rev. 4.4, 1994
EPA 200 7 Rev. 4.4, 1994
EPA 200 7 Rev. 4.4, 1994
EPA 200 7 Rev 4.4, 1994
EPA 200 7 Rev 4.4, 1994
EPA 245 1
<1 mg/L
<1 mg/L
<1 mg/L
<1 mg/L
<1 mg/L
<1 mg/L
<1 mg/L
<0.0002 mg/L
Collect Date/Time Matrix
1/5/2022 8:50 AM Solid/Sludge
Method Results
SM 2540 B
SM 9221C E-2014
Collect Date/Time
1/5/2022 8,50 AM
Method
SM 2540 B
SM 9221C E-2014
Collect DatelTime
1 /512022 8.50 AM
Method
SM 2540 B
SM 9221C E-2014
01 /14/2022
01 /14/2022
01 /14/2022
01 /14/2022
01 /14/2022
01 / 14/2022
01 /14/2022
01 /14/2022
Sampled by
InYoung Seo
Date Analyzed
2 78 % 01 /07/2022
612 MPN/g 01/05/2022
Matrix Sampled by
Solid/Sludge InYoung Seo
Results Date Analyzed
2.85 % 01 /07/2022
278 MPN/g 01 /05/2022
Matrix Sampled by
Solid/Sludge InYoung Seo
Results Date Analyzed
2.65 % 01 /07/2022
1057 MPN/g 01 /05/2022
Report # 2022-00308 Page 3 of 4

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9

PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION
The Town of Beulaville, Town of Kenansville, Town of Warsaw, Town of Bridgeton, Town of
Maysville, Southwest Plantation, Town of Clayton (part of the first and second quarters and all of
the third and fourth quarters) and the Town of Wallace (Part of the third quarter and all of the fourth
quarter) meet pathogen reduction and vector attraction reduction requirements through lime
stabilization. The Town of Clayton (first and second quarters), Town of Rose Hill (only event),
Swansboro WWTP (only event), and Town of Wallace (first, second and part of the third quarter)
met pathogen reduction through fecal density and vector attraction reduction through injection or
incorporation. The Town of Clayton met pathogen reduction and vector attraction reduction
through fecal density and SOUR in one instance by SOUR (January 2022.)
The forms for these facilities are marked appropriately.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Bridgeton WWTP NPDES Number: NCO074837
Monitoring Period: From l/1/2022 To 12/31/2022
Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) _ ❑
Alt 4 (Spec' OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. StabilizationEl
Alt 7 (Drying - Stable) ❑ 1
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (ln'ection) ❑ Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives
were performed ❑
I� IWMWI !4 A TiAI►T 07. ♦ i
v aia�aaa•aa.['�11V1\ 01 L°l1 L'IVIJK 1\ 1 tpiease cneCK the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T 1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
❑ vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
A,1.3 L•W«. MUA4tjvn nas peen mace under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Eric R. Smith
Preparer Name
Signature of Preparer*
(tZpe or print)
Date
Land Applier Name and Title (if applicable)(type or print)
of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Beulaville WWTP NP.DES Number: NCO026018
Monitoring Period: From i/l/2022 To 12/31/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/tem) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) 1 1
Alt(No Prior Test) ❑
Process to Further Reduce Patho en s E t
..........
If applicable to alternative perforted (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑� Heat Treatment ❑ Thermo philic 1
Beta Ray ❑
Gamma R21 ❑
Pasteurization ❑
Class B:
JAIt. (1) Fecal Density []
Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (glass B only) indicate "Process to Significantly Reduce Pathogens":
Y
Lime Stabilization CI
Air Drying ❑
conipostins ❑
Aerobic Digestion ❑
Anaerobic Di estion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
AIlowable Level
in Sludge
Pathogen Density
k y
Number o
Gxcee-
Frequency
of Analysis
Sample
Tenri-zype
na y ica
Tech -
nignp
MinimumGeo.
Mean
MaximumUnits
Fecal Colifonn
2 x 10 to the
6th power
per gram of
total solids
MPN
CPIJ
1000 mpn per grain
of total solid (dry
wei it
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bencli) ❑
JAIL. 4 (Spec. UZ uptake) F
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. StabilizationEl
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) E.
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check ti►e appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
EJ vector attraction reduction requirement in 15A NCAC 02T .11.07 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Stanley Miller, WWTP ORC
Preparer Name and Title (type or print)
Signature Vreparer* Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 27'.1102 (26)
DENR FORM PVRF 02T (12/20061

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Clayton WQ Permit Number: WQ0030998
WWTP Name: Little Creek Water Reclamation Facility NPDES Number: NCO025453
Monitoring Period: From 1/l/2022 To 3/31/2022
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
Alternative 4 ❑
Alternative 5 ❑
Alternative 6 ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment Ll
Thermo hilic ❑
Beta Ra 01
Gatnma Ray ❑
Pasteurization ❑
Class B: I
Alternative 1 El
Alternative 2 El
If applicable to alternative performed Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
Air Drying O 1
Composting ❑
Aerobic Digestion U
Anaerobic Digestion ❑
If applicable to alternative performed Class A or Class B complete the followltil
monitortng data:
Parameter
Allowable Level
in Sludge
t3
Pathogen Density
u r o
Excee-
Frequency
of Analysis
Y
Sample
Type
'ca
Tech-
nintir
inimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
15,000
24,127
58,000
MPN/
Gram
0
Quarterly
Grab
MIS
9221E
CFU
1000 mpn per gram
of total solid (dry
weight)
Satmonel Is bactenna
(in lieu of fecal
coliform
3 per;4 grams
total solid (dry
weiitt
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.1 (VS reduction) 0
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
JAIt. 4 (Spec. O, uptake) El
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization El
1Alt.
Alt 7 (Drying - Stable) ❑
JAIt. 8 (Drying - Unstable) L31
All. 9 (Injection) H1
10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an exalanation why you have not met one or both of the reauirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment"
Mr. William Simpson, WRF ORC Mr. Eric R. Smith, Land Applier ORC
Preparer Name and Title (type or print) LandApplierName and Title (if applicable)(type or print)
2/10/23 J-hU940�, Q
Signature of PrepareDate Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12i2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Clayton WQ Permit Number: WQ0030998
WWTP Name: Little Creek Water Reclamation Facility NPDES Number: NCO025453
Monitoring Period: From 4/l/2022 To 6/30/2022
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Altemadve 1 ❑
Alternative 2 ❑
Alternative 3 ❑
'
Alternative 4 ❑
Alternative 5 ❑ 1
Alternative 6 ❑
If applicable to alternative performed (Class A onl •) indicate "Process to Further Reduce Pathogens":
Compost ❑
at Drying ❑
Heat Treatment
Thermo hilic❑
Beta Ra ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alternative 1 2J
A ternattve 2 0
If applicable to alternative performed Class B only indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El Air in-g ❑ Composting ❑ Aerobic Di estion U
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the llowing monitorin
data:
Parameter
Allowable Level
in Sludge
8
Pathogen Densitynm
01 °
E�cae
Frequency
of Analysis
Y
Sample
TL.ype
uca
Tech-
imutr
Geo. Mean
Maximum
Units
Fecal Coliform
2 s 10 to the
6th power
per gram of
total solids
WN
41,000
117,002
320,000
0
Quarterly
Grab
SM18
9221E
t FU
1000 mprr per grata
of total solid (dry
wei1rhO
Salmonella bacteria
(in lieu of fecal
coliform
3 NEN per 4 grans
total solid (dry
weicffitl
v ector anrAcnon ltetlnMOB M U K ZU3.33 r- rlease indicate ennon nertor hied:
Alt. l (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
JAIL 4 (Spec. Ow uptake) 0
Alt. 5 (14-Day Aerobic) 0
Alt. 6 (Alk. StabilizationEl
Alt 7 (Drying- Stable) O
Alt 8 (Drying - Unstable) ❑
Alt. 9 (Injection) a
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were perforined 0
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalh' of law, that the pathogen requirements In 40 CFR 503.32 and the vector
attraction reduction requirement In 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met" (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the Information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. William Simpson, WRF ORC W. Eric R. Smith, Land Applier ORC
Preparer Name and Title (type or print) Land Applier Nam d �'itle (if applicable)(type or
'nt)
2/10/23 C�.C.t.c till l,�2 3
Signature of Prepare Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Clayton WQ Permit Number: WQ0030998
WWTP Name: Little Creek Water Reclamation Facility NPDES Number: NCO025453
Monitoring Period: From 7/ 112022 TO 9/30/2022
Pathogen Reduction (40 CFR 503.321- Please lndicate level achieved and alternative nerfnrmerl-
Class A:
Alternative 1 ❑
Alternative 2 ❑ Alternative 3❑
Alternative 4❑
Alternative 5 ❑ Alternative 60
If applicable to alternative performed Class A onl indicate `Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermo hilic❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alternative 1 07
Alterative 2 El
If applicable to alternative performed Class B only) Indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
Air Drying Cyj
CompostingCompostiag ❑
Aerobic Digestion
Anaerobic Digestion ❑
If applicable to alternative peirforwed (Class A or Class B) complete the following
monitorin g data:
Parameter
Allo"`able Level
in Sludge
S
Pathogen Density
gun r o
Excee•
Frequency
of Analysis
1
Sample
Type
na ca
Tech-
inimutr
Geo. Mean
aximurt
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
N?N
730
740
750
MPN/
0
Quarterly
Grab
SM18
9221E
CFU
1000 mpn per gram
of total solid (dry
wei ht)
a mane la acteria
(in lieu of fecal
coliform
3 MPN per 4 grans
total solid (dry
��ei ht
vector auracnon itceuucuon t4u (ah'K 503.33) - Yiense indicate option performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
jAlt. 4 (Spec. O_ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk Stabilization El
Alt 7 (Drying - Stable) ❑
lNo
jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement In 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision In accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. William Simpson, WRF ORC Mr. Eric R. Smith, Land Applier ORC
Preparer Name and Title (type or print) Land Applier Namejmd Title (if applicable)(type or print)
U144" 2/10/23 hn.chk-$0L1)-Q,3
Signature of Prepare * Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name. Town of Clayton WQ Permit Number: WQ0030998
WWTP Name: Little Creek Water Reclamation Facility NPDES Number: NCO025453
Monitoring Period: From 10/1/2022 To 12/31/2022
Pathogen Reduction (40 CFR 503.32) - Please Indicate level achieved and alternative (performed:
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 LI
Alternative 4 ❑
Alternative 5 ❑
Alternative 6 ❑
If applicable to alternative erformed Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat P1,
Aug❑
Heat Treatment ❑
Thermo hilic ❑
Beta Ray ❑
Ganuna Ra ❑
Pasteurization ❑
Class B:
Alternative 1 ❑
Alternative 2 El
F
If applicable to alternative performed (Class B onl .) indicate "Process to Slignificantky Reduce Pathogens":
Lime Stabilization El Air D in ❑ Composting ❑ Aerobic Digestion Ll
Anaerobic Di estion ❑
If applicnble to alternative performed (Class A or Class B) complete the followingmonitotin
data:
Parameter
Allowable Level
in Sludge
Pathogen Density
er o
Eacec
Frequency
of
ofAual Analysis
y
Sample
Type
r ica
Tech -
nimu
Geo. Mean
Maximum
Units
Fecal Coliforni
2 x 10 to the
6th power
per gram of
total solids
WN
180,000
336,644
470,000
lWN
Gram
0
Quarterly
Grab
sMla
9221E
CFU
1000 mpn per gram
of total solid (dry
wei ht
Salmonella bacteria
(in lieu of fecal
coliform
3 NVN per 4 grams
total solid (dry
%,.vi ht
V ector Attraction Keduction (4U C'1fK 503.33) - Please indicate option performed:
Alt I (VS reduction) ❑
Alt. 2 (40-day bench) Cl
Alt. 3 (30-day bench) ❑ JAR.
4 (Spec. O, uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization El
Alt 7 (Drying - Stable) ❑
1 Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) CJ
Alt. 10 (Incorporation) ❑
No rector attraction redaction alternatives were performed 1-11
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met"
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met" (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including tine and imprisonment."
Mr. William Simpson, WRF ORC Mr. Eric R. Smith, Land Applier ORC
Preparer Name and Title (type or print) Land Applier Name arld Title (if applicable)(type or 'nt)
c—s �
ae� 2/10/23
Signature of Prep * Date Signature of Land Applier (if applicable) Date
'Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning
WWTP Name: Town of Kenansville WWTP
Monitoring Period: From 1/1/2022
WQ Permit Number: WQ0030998
NPDES Number: NCO036668
To 12/31/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achiever) anal altPrnativP nPrfnrrn.A
Class A:
Alt. A hme/tens p Alt B Alk Treatment ❑
C ) C )
Alt. C (Prior Testing) ❑
.-. ..: .
AIt.D (No Prior Test) ❑ Process to Further Reduce Patho engs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens"
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermo hilic ❑
Beta Ray ❑
Gamma Ra • ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density ❑
I Alt. (2) Process to Significantly Reduce Pathogens El
If applicable to alternative performed Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
Air Drying ❑
Cotnl ostin ❑ Aerobic Digestion p
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
1' y
! um er o
Excee-
Frequency
of Analysis
Sample
Type
Ana lca
Tech -
lllll]nU
Geo. Mean
Maxilnuln
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
a bacteria
Linlieuf fecal
i7-_L_�
-weight)
3 MPN per 4 grams
total solid (dq
weigh[)
r et:wr t%ttL_44;t1U" nUCLUCpOn t1:1A PVI:AC Ulf .11W) - Fie -Me indicate alternative nPrfnrmPrl-
Alt. ] (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. O, uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization p
Alt 7 (Drying -Stable) ❑ I
Alt. 8 (Drying -Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
0 vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if ,you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Gary Harper, WWTP ORC
Prepa: er Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Signature o Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
bENR FORM PVRF 02T (12/20061

VECTOR ATTRACTION REDuc TION FORM (02T Rules)
ANNUAL PATHOGEN AND WQ Permit Number: WQ0030999
Facility Name: Triple S Farms & Cleaning NPDES Number: NCA021482
WWTP Name. Town ofMaysyille WW_rP 11l t2022 12J31J2022
Monitoring Period: From
alteermulaltiv
Pathogen Reduction (15A NCAC 02T.110 0) - I'lci�Se indicate level achievedAla � Prior Testin er1�
Class A: Ait< t timcltent } © Alit t11k Ticatment l7
111t.D No Prior'] cst ❑ I'rciccss to further Reduce Patho en ❑
lfa licable to alternative orfotmcd Class A anl'.,, Wdiratc "t'rogegs to Further Reduce rPathogens"'.
txno i 1 G : ❑
licat t`d� n C7 llcat'T'tcattnt' nt C7
Corn ,st O E3 ..
Beta Rav O ( tarn] i�a� C}_ I'aStt ulii aiii�n t 7
C1a�513: Att. (I? 1'c{ al Ihnsiri d ttlt. 2 Process to if'tcantl Reduce Patha ens CI
jL!PE1!cab1e to aiternatire crfot'med C k%, Bon_ 1 ,} indicate "Process to Si nin ntl Reduce Path ens":
l,in�e Stabiliratinn CI Air ID ,in
❑ Com ostin ❑ Aerobic Lii estion ❑
Anaerobic IJi e�tit}tt
Ifapplicableto alternative erfarmed Class A o_r Class B com lete the followin mopitonln data: ca
Allowable Level Pathogen Density umveroT Frequency Sample Tech -
Parameter in Sludge Minimu Geo. Mean MaximumUnits of Analysis Type
x 10 to the MPN
Gth power
per� of C-FU
.Fecal Coliftarm total solids
1tlt?0 mpn per gram
of total solid (dry
amonena bactena :f MFN per 4 grams
(in lieu offecal I total solid (dry
Vector Attraction Reduction (15A NCAC 02T .11071- Please indicate alternative Derlormed:
Alt .1(NIS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30�day bench) ❑
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 i 14-Day Aerobic) ❑
Alt. 6 (Alk. StabilizationCl
Alt 7 (Drying -Stable) ❑
jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (incorporation) ❑
No vector attraction reduction alternatives
were performed ❑
%_zr% 11.ela...e1I AM \ a l tt xozlvir iN 1 kpiease caecK ine appropriaTe statemenT)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 1SA NCAC 02T .1106 and the
❑ vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in acco ancewith the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment"
Jason Baker WWTP ORC'
zPreparer Name and Title (type or print) Land Applier Name and Title (itapplicable)(type or pr nt)
ture ofPreparer*
Date Signature of Land Applier (if applicable) Dater
*Preparer is defined in Ail OFR Part 503.9(n) and 15A NCAC 2T .1102 (26)
DENR FORM MIRF 02T (12tZp06)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
FacilityName: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Rose Hill WWTP NPDES Number: NCO056863
Monitoring Period: From lilt2022 To 12/31/2022
Pathogen Reduction (15A NCAC 02T .11061- Please indicate 1pvpl arhipvpA and altarnativa nnrfnrmnA.
,---ClassA:
Alt. A time(tem ❑ Aft B (Alk Treatment) ❑ 1 Alt. C (Prior Testin) ❑
A1t.D (No Prior Test) ❑ Process to Further Reduce Patlro$en ❑
If applicable to alternative erfbt7ned (Class A only) indicate "Process to Further Reduce Potho ens":
Com ost ❑
Heat Drying ❑
Heat Treatment ❑
Thermo hilic ❑
Beta Ea ❑
Gamma Ray❑
Pasteurization ❑
Class B.
Alt. l Fecal Density El
Alt. (2) Process to Significatifly Reduce Pathogens ❑
If applicable to alternative performed (Class B oat) indicate "Process to Significantly Reduce Pstho eas":
Lithe Stabilization ❑ Air Drying ❑ composting 0 Aerobic Digestion
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in
in Sludge
Pathogen Density
Excec-
Frequency
Analysis
of Anal
SampleAna
Type
y
Tech -
Miniutut
Geo. Mean
axinnut
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
6285
45190
322808
MPN/
Gram
0
Annuallly
Grab
SM 9221
C E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
11colIform)
3 MPN per 4 grams
total solid (dry
weight
actor Attraction Reduehon (15A NC C 2T .11071 - Plense indicate nitprnativp nprfni-ma .
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 004ay bench) ❑]Alt.
Alt. 4 (Spec. O_ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
All. 6 (Alk. Stabilization ❑
Alt 7 (Drying- Stable) ❑
8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
11". "I"T . we, . •milt- n
All. 10 (Incorporation) El
No vector attraction reduction alternatives were erformed Cl
..�� a ar a —A, av►4 a it es t x.tvsr N 1 tplease check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T 1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
❑ vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
l MAD UUMUItllp S[7utl has oeen mane unaer my alrecaon and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Carl Wheeler, WWTP ORC Mr. Eric R. Smith, Land Applier ORC
Preparer Name and Title (type or print) Land Applier Name d Ti (if applicable)(type or Pilo
Signature of Preparer* Date Signature of Land Applier (if applicable) Pat
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Swansboro WWTP NPDES Number. NCO023261
Monitoring Period: From l/l/2022 To 12/31/2022
Pathogen Reduction (15A NCAC 112T _»nx) - maaaaa rnar....6— rs..-I -1
«—AWT :u ancrunllve perrormea:
Class A: Alt A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testis CJ
A1t.D [No Prior Test ❑ Process to Further Reduce Patlio en s U
If applicableto alternathe performed (Class A only) indicate "Process to Further Reduce Pathogens":
CoinM st ❑ Heat D � ig ❑ Heat Treatment ❑ Thermo hilic U
Beta LaX ❑ Gamma Ray 13 1 Pasteurization ❑
Class B: Alt. (1) Fecal Density El I Alt. (2) Process to Si nifican 1v Reduce Pathogens ❑
If applicable to alternathe performed (Class B onl ) indicate "Process to Si 111conth Reduce Pathogens":
Lime Stabilization ❑ Air D in iJ Com ostin ❑ Aerobic Di estion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) coin late the following monItoring data:
Parameter
Allowable Level
Pathogen Density
"'r' er o
FrequencyLSle
n tca
inim
Geo. Mean
Maximum
Units
in Sludge
Excee-
of Analysise
Tech-
2 x 10 to the MPN
6th power
34.314
57,362
107,624
��/
0
Annually
Grab
SM 9221
per gram of
C E
Fecal Coliform
total solids CFU
1000 mpn per gram
of total solid (dry
wei ht
Salmonella bacteria
3 MPN per 4 grams
(in lieu of fecal
total solid (dry
coliform)
weight
VeCtAI' AttrA�tinn
aarnnlin.. !1 G
A M!� ♦ n
A fT n.,.
r. _ _ _ _
..
_
Alt. t (VS reduction) ❑
- - - --- -- - ---- •
Alt. 2 (40-day bench) ❑
--�......-«.,a..«w waaca uauva CA IViIIICII:
Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization❑
Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) U
Alt. 10 (Incorporation) 13
No vector attraction reduction alternatives were performed ❑
CERT11FIVATrntvcrriWMWuT1..:---_
_a___, — _
---•--'-- - ♦r•—.- ..,,`..a..aav arps WkFA&MlC amcmenrl
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement In 15A NCAC 02T 1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
0 vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
If you check this statement attach an explanation why you have not met one or both of the
---.- . uaa..aa—.a uns ueea maue unaer my atrection and supervision In accor ante w t t e system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Mark Young WWTP ORC Mr. Eric R. Smith, Land Applier ORC
Preparer Name and Title (type or print) Lan plier=Itcable)(typejur p ' t)
2/21 /23�� ,
Signature of Preparer* Date Signature of Land Applier (if applicable) 24)!ate
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
OENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning
WWTP Name: Southwest Plantation WWTP
Monitoring Period: From l/l/2022
To
WQ Permit Number: WQ0030998
NPDES Number: WQ0029601
12/31 /2022
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative aerformed:
Class A:
Alt. A (time/tern) ❑
1 Alt B (Alk Treatment) ❑
Alt. C (Prior Testis ❑
Alt-D (No Prior Test) ❑ Process to further Reduce Patho ens ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat DryiiiE ❑
Heat Treatment ❑
Thenno hilic ❑
Beta Ray ❑
Gamma Ra D
Pasteurization ❑
Class B:
Alt. (1) fecal Density ❑
1 Alt. (2) Process to Significantly Reduce Pathogens El 77
If applicable to alternative perfbiuted (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
Air Drying ❑
CoMpostina ❑
jAerobic Digestion Cl
Anaerobic Digestion LJ
If applicable to alternative performed (Class A or Class B) complete the following
monitoring datst:
Parameter
Allowable Level
in Sludoe
Pathogen Density
um
Excee-
Frequency
of Analysisenceq
Sample
Type
na ice
Tech -
ninne
initnuttGeo.Meau
aximun
Units
Fecal Colifonn
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per grain
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform) I
3 MPN per 4 grams
total solid (dry
Weight)
Vector Attraction Reduction (15A NCAC 02T .1107) -Please indicate alternative nerfortned:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
JAIL 4 (Spec. O, uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization El
Alt 7 (Drying -Stable) ❑
I Alt. 8 (Drying -Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Inco oration) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision to accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties forKalse certification Including fine and imprisonment."
Mr. Sonny S ar' WMTP ORC
Preparer Name d e ( or rint)
C ar ,1 n z n Jr.
Signatur f rer)arer* D e
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
nFNR Ft')RM PVRF n9T ti w,7nnni

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Wallace Regional WWTP NPDES Number: NC0003450
Monitoring Period: From 1/1/2022 To 3/31/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please Indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑ Alt II Alk Treatment ❑ 1 Alt. C (Prior Testis ❑
.
Alt D o Prior Test ❑ Process to Further Reduce Patito en ❑
...........
If applicable to alternative performed jClass A only) Indicate "Process to Farther Reduce Pathogens":
Compost ❑
at Dging ❑
Heat Treat:uent ❑
Thermo hilic ❑
Beta Ray ❑
Gamma Ra ❑
Pasteurization ❑
Class B: JAIL
1 Fecal Density El
Alt. (2) Process to Significantly Reduce Patho ens ❑ ..........
If gppllrmble to alternative performed Class B only) Indicate "Process to Significantly Reduce Pntho ens":
Lime Stabilization ❑ Air Dryina ❑ Cont ostin ❑ Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed Class A or Class B complete the followlnR
monitoring data:
Parameter
Parameter
Allowable Level
in Sludge
Pathogen Density
r4umnerollFrequency
Excee-
of Analysis
Sample
Type
Tech -
'aim
Geo. Mean
MaximumUnits
Fecal Coliform
x 10 to the
6th power
per gram of
total solids
ION
278
721
1,287
WN/
Gram
0
Quarterly
Grab
SM 9221 C
E
C�J
1000 mpn per gran
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
colifogn)
3 WN par4 grams
total solid (dry
Might)
vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-daybench) ❑ Alt. 4 (Spec. Or uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (AIL Stabilization❑
Alt 7 (Dryin - Stable) ❑ JAIt. 8 (Drying - Unstable) ❑
All. 9(Injection) El
All, 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
© "I certify, under penalty of law, that the pathogen requirements In 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
El "I certify, under penalty of law, that the pathogen requirements In 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
If you check this statement attach an explanation why you have not met one or both of the
reauirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment"
Ms. Lisa Cottle, WWTP ORC Mr. Eric R. Smith, Land Applier ORC
Preparer Name and Title (type or print) Land Applier Name and itle (if applicable)(type or
A. �Z lk 2-2 2OZ �« ,
Signature of Preparer* Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (1212006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Wallace Regional WWTP NPDES Number: NC0003450
Monitoring Period: From 4/1/2022 To 6/30/2022
Pathogen Reduction (15A NCAC 02T ,1106) - Please indicate level achieved and alternative nerformede
Class A:
Alt. A timehem ❑ Alt B Alk Treatment) ❑ 1 Alt. C riorTestia ❑
r
AltM (No Prior Test ❑I Process to Further Reduce Mio en ❑
If applicable to alternative erfor med (Class A onl • indicate "Process to Further Reduce Path ens":
Compost ❑
Heat D in ❑
Heat Treatment ❑
Thermo hilic ❑
Beta Ray ❑
Gamma Ra ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density El
JUL 2 Process to Significantly Reduce Patho ens ❑
If applicable to alternativepet-formed Class B o indicate "Process to SIgnIfIcnn!!y Reduce Pathogens" -
Lime Stabilization ❑ Air Rr ing ❑ Cora os ing ❑ JAerobic Digestion [3
Anaerobic Di estion ❑ 4.
If applicable to alternative performed Class A or Class B complete the fo]lowingmonitorin
data:
Parameter
Allowable Level
in Sludge
in
Pathogen Density
or
Excee-
Frequency
of Analysis
Y
Sample
Type
na a
Tech -
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
61h power
per gram of
total solids
MPN
30,860
54,377
362,205
MPN/
0
Quarterly
Grab
SM 9221 C
E
CFU
I NO mpn per gram
of total solid (dry
wei ht
Salmonella bacteria
(in lieu of fecal
coliform) A
3 N214per4 grams
total solid (dry
—!M11110
vector Arrracuon Keoucuon (15A r4t:AL: UZT AIM - Please indicate alternative nerinrmed!
AIL (VS reduction) ❑
Alt. 2 (40-daybench) ❑
All. 3 (30-daybench) [3
JAIL 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic)
Alt, 6 Alk. Stabilization ❑
All 7 in - Stable) ❑
JAIt. 8 (Drying -Unstable) ❑
Alt. 9 Q'ection)El
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performad ❑
%-rurx i w-Lu& i turt a rA x a;tvxxrwv (please cnecic the appropriate statement)
"I certit�, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supery stun in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the Information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment"
Ms. Lisa Cottle, WWTP ORC Mr. Eric R. Smith, Land Applier ORC
Pre arer Name and Title (type or print) Land Applier Name nd Title (if applicable)(type r print)
• 2 Zo2 3� �t IYYj 2
Signature of Preparer* Date Signature of Land Applter tf applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 1 SA NCAC 2T .1102 (26)
DENR FORM PVRF 02T (1212006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Wallace Regional WWTP NPDES Number: NC0003450
Monitoring Period: From 7/1/2022 To 9/30/2022
Pathogen Reduction USA NCAC 02T ,1106) - Please Indicate level achieved and alternative performed:
Class A:
Alt. A tine/tem ❑ 1 Alt B(Alk Treatment) ❑ 1 All. C riot Testis O
AIt.D (No Prior Test) ❑ Process to Further Reduce Pathogen ❑
If a Ii'cable to alternative etformed Class A onl l indicate `Trocess to Further Reduce Pathogens":
Com ost ❑
Heat D in ❑ Heat Treattent tJ
Thermo hilic ❑
Beta Ray 0
Gamins R ❑ Pasteurization ❑
Class B:
]AIt. (1) Fecal Densi 0 Alt. 2 Process to Significantly Reduce Patho ens❑
If applicable to alternative peiformed Class B only) indicate "Process to Sipfficantly Reduce Pathogens".
Lime Stabilization El Air D in ❑ Con sfiu& ❑ JAcrobioDigestion ❑
Anaerobic Di estion ❑
If appBuble to alternative performed Class A or Class B) complete the following
monitorin data:
Parameter
Allowable Level
in
in Sludge
Pathogen Density
Ex era
Frequency
of Analysis:
Y
Sample
Type
ne y -
Tech -
inimu
Gee. Mean
axim
Units
Fecal Coliform
2 x 10 to the
6th power
par gram of
total solids
MPN
72
93
171
MPN/
Gram
0
Quarterly
Grab
SM 922t
C E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform
3 MPN per 4 grams
total solid (dry
weI t
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑
JAIL 3 (30-day bench)
JAIL 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. StabilizationEl
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) El Alt. 10 Inco oration) 13
lNo vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements In 15A NCAC 02T .1106 and the
vector attraction reduction requirement in ISA NCAC 02T .1107 have been met"
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
❑ vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met" (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the Information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment"
Ms. Lisa Cottle, WWTP ORC Mr. Eric R. Smith, Land Applier ORC
Pre arer Name and Tide (type or print) Land Applier Name and itle (if applicable)(type or print)
T
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (1212006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Wallace Regional WWTP NPDES Number: NC0003450
Monitoring Period: From 10/1/2022 To 12/31/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A time/tem 07ARB(ArkTreatrnenty.©
1 Alt. C(Prior Testing) ❑
AIt.D (No Prior Test ❑ Process to Further Reduce Patho en ❑
:.::::..
if a licable to alternntive etd'ormed G9nss A onlyIndicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermo hilic ❑
Hera Ra ❑
Gamma Pa ❑
Pass teurization ❑
Class B:
Alt. 1 Fecal Density ❑
Alt. 2 Process to Si nific nfly Reduce Patho ens O
If applicable to alternative peilbrtned Class B onl indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Cl Air Rgjng ❑ 1 ComRostiaE ❑ jAerobic Digestion D
Anaerobic Di estion ❑
If applicable to alternative performed (Class A or Class complete the followin monitorin
data:
Parameter
Allowable Level
in Sludge
Path en Density
um r o
dimeme Excee-
Frequency
of Analysis
Sample
Type
Tech-
Minunu
Geo. Metui
Maximum
Units
Fecal Coliform
2 x 10 to Ilre
6th power
per gram of
total solids
MPN
77,171
150,614
288,402
MPN/
firaut
0
Quarterly
Grab
SM 9221
C E
CFU
1000 mpn per gram
of total solid (dry
►lei ht
galmonella batten a
(in lieu of fecal
colifotm
3M13N per 4 grams
total solid (dry
► ' t
vecwr anracuott meauenou iitiA NL:Au vi 1- .IXU-1l -Please inOlcate alternative nerformed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) O
JAIL 3 (30-day bench) 0
It. 4 (Spec. Oi]uptake) LlAlt.
5 14-Day Aerobic ❑
Alt. 6 (Alk. Stabilizationls]
Alt7 ing- Stable) D
Alt. 8 'n - stable) ❑
Alt. 9 'ection ❑
Alt. IO co oration ❑
No vector attraction reduction alternatives were tmed ❑
ULK'1'WWA'1'1UN STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met"
❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met" (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision -inn accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment"
Ms. Lisa Cottle, WWTP ORC
Preparer Name and Title (type or print)
,kno.-LAU ? ,Z-2023
Signature of Preparer* Date
Mr. Eric R. Smith, Land Applier ORC
Land Applier Name and Title (if applicablextype orprint
7�/4600
Signature of Land Applier (if applicable) at
*Preparer is defined in 40 CFR Pert 503.9(r) and 15ANCAC 2T .1102 (26)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Warsaw WWTP NPDES Number: WQ0021903
Monitoring Period:
From 1/1/2022 To 12/31/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
A:
Alt. A (time/ten) ❑
AltB (Alkm
❑
Alt. C (Prior Testing) DClass
A1t.D (No Prior Test) Cl
Process to Further Reduce Patho en s ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Beta Ray ❑
Heat Drying ❑
Heat Treatment ❑
Thermo hilic ❑
Gamttia Ray ❑
Pasteurization ❑
Class B:
JAIt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens 17
If applicable to alternative performed (Cinss B only) indicate "Process to Signiflenutly Reduce Pathogens":
Lime Stabilization El T
Air Drying ❑
Couleosting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the followlill
monitoring data:
Parameter
Allowable Level
in Sludge
g
Pathogen Density
Numoer or
Excee-
Frequency
of Analysis
Y
Sample
Type
Ana ica
Tcch-
Minimum
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
wei ht
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
wei ht
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. StabilizationEl
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt, 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements In 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
D "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"-Th s determination has een made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Greg Hugh , WWTP ORC
Prepar Name a d tle (type or print)
Signatu a of P eparer*
Land Applier Name and Title (if applicable)(type or print)
�•�1-23
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T f 12/20063

PATHOGEN AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION

PATHOGEN REDUCTION AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION
The Town of Beulaville, Town of Kenansville, Town of Warsaw, Town of Bridgeton, Town of
Maysville, Southwest Plantation, Town of Clayton (part of the first and second quarters and all of
the third and fourth quarters) and the Town of Wallace (Part of the third quarter and all of the fourth
quarter) meet pathogen reduction and vector attraction reduction requirements through lime
stabilization. The Town of Clayton (first and second quarters), Town of Rose Hill (only event),
Swansboro WWTP (only event), and Town of Wallace (first, second and part of the third quarter)
met pathogen reduction through fecal density and vector attraction reduction through injection or
incorporation. The Town of Clayton met pathogen reduction and vector attraction reduction
through fecal density and SOUR in one instance by SOUR (January 2022.)
Documentation of these activities are found in the following section.

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Town of Clayton
Little Creek Water Reclamation Facility
WQ0023178
Feb-22
Environment 1, Inc.
Lab #
Date Analyzed
Fecal. 0 .. form
per gram
Log
HT-1
2/15/22
17,000
4.230
HT-2
2/15/22
17,000
4.230
HT-3
2/15/22
26,000
4.415
HT-4
2115i22
28,000
4,447
HT-5
2/15/22
58,000
4,763
HT-6
2/15/22
26,000
4.415
HT-7
2/15/22
15,000
4.176
Totall AM
Average 4383 -
Most Probable Number 1 Gram 24,127 Fecal Coliformlgram
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen. and Vector Attraction Reduction Form for this land
application event.

Drinking Water ID: 37715
Wastewater ID 10
ID#: 890 1
MIN OF CLAYTON
MR. BILL SIMPS014
P.O. BOX 879 DATE COLLECTED: 02/15/22
CLAYTON, NC 27528 DATE REPORTED : 02/21/22
REVIEWED BY: — "�`—' "`
Sarziple
Sample
Sample
Sample
Sample
Anul)sis
Method
PARANIFT.RS ul
M2
k3
#4
#5
Date Anahst
Code
Total Residue, mg/l 19200
18867
19167
17700
19100
02/16/22 Jib1S
2540B-15
Fecal Colit'orm (h1PN), ;gram Solids 17000
17000
26000
28000
58000
02/15/22 JN1S
92211,14

Drinking Water ID: 3771E
Wastewater ID- 10
IDS}: 890 I
TOVIN OF CLAYTON
MP.. BILL SIMPSON
P.O. BOX 879 DATE COLLECTED: 02/15/22
CLAYTON, NC 27528 DATE REPORTED : 02/21/22
REVIEWED BY:
Sample Sample Arai}Sis Method
I'ARANIETERS NG #7 Date Analyst Code
Total Residue, mg/I 18567 19367 02/16122 JiNIS 254011-15
Feenl Coliform ('VIPN), /pram Solids 26000 15000 02/15/22 J:1IS 9221E-I1

Town of Clayton
Little Creek Water Reclamation Facility
WQ0023178
Jul-22
Environment 1, Inc.
Lab #
.Date Analyzed
Fecal Coliform
per grain
Log
HT-1
6/30/22
85,000
4.929
HT-2
6/30/22
220,000
5.342
HT-3
6/30/22
320,000
5.505
HT-4
6/30/22
83,000
4.919
HT-5
6/30/22
41,000
4.613
HT-6
6/30/22
67,000
4.826
HT-7
6/30/22
220,000
5.342
Totall 35A77
Averagel 5.069
Most Probable Number / Gram 117,002 1Feca1 Coliform/gram
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

TOWN OF CLAYTON
MR. BILL SIMPSON
P.O. BOX 879
CLAYTON, NC 27528
Sample Sample
PARANIrTF.RS #I #2
Total Residue. mg/I 16.367 16000
Fecal Coliform (.NIPN). Imam Solids 85000 220000
Drinking Water !D: 37715
Wastewater !D: 19
ID#: 890 I
DATE COLLECTED: 06/30/22
DATE REPORTED : 07/08/22
REVIEWED BY: /�� ��• �% _~
Sample
Sample
Sample
Analysis
Method
ii3
#4
#cz
Date Analyst
Code
16733
15733
17200
07/05/22 BI:N'
254013-15
320000
83000
41000
06130/22 I\IS
9221E-14

TOWN OF CLAYTON
MR. BILL SIMPSON
P.O. BOX 879
CLAYTON, NC 27526
Sample Sample
P-kRANTETERS #1 #2
Total Residue. mg/l 16467 16000
Fecal Coliform (NIP,IN). /gram Solids 85000 220000
Drinkir.q Water. ID: 31719
Wastewater ID: 17
ID#: 890 I
DATE COLLECTED: 06/30/22
DATE REPORTED : 07/08/22
REVIEWED BY:
Sample
Sample Sample
Anal }sis Method
#3
#4 #5
Date Analist code
16733
15733 17200
07/05/22 BLN' 254O B-15
320000
83000 41000
06130/22 YNIS 9221E-14

Town of Clayton
Little Creek Water Reclamation Facility
WQ0023178
Sep-22
Environment 1, Inc.
Lab #
Date Analyzed
Fecal Coliform
per gram
Log
HT-1
9/27/22
740
2.869
HT-2
9/27/22
740
2.869
HT-3
9/27/22
730
2.863
HT-4
9/27122
750
2.875
HT-5
9/27/22
740
2.869
HT-6
9/27/22
740
2.869
HT-7
9/27/22
740
2.869
Totall � 20-085
Average ..........::.2.869.. -1
Most Probable Number /Gram
?D Fecal Coliform/gram
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

TOWN OF CLAYTON
MR. BILL SIMPSON
P.O. BOX 879
CLAYTON, NC 27528
Sample Sample
PARADIETERS #1 #2
Total Residue, mg/I 24333 24533
Fecal C'oliform 111P\�, ;gram Solids <740 <740
Drinking Water ID: 37715
Wastewater ID: 10
ID#: 890 I
DATE COLLECTED: 09/27/22
DATE REPORTED : 09/30/22
REVIEWED BY:
Sample
Sample
Sample
Analysis
Method
#3
#4
#5
Date Analyst
Code
24733
23867
24433
09/27/22 JINIS
254013-15
< 730
< 750
< 740
09/27/22 JDJ
9221 E-14

TOWN OF CLAYTON
MR. BILL SIMPSON
P.O. BOX 879
CLAYTON, NC 27528
Sample
PARAMETERS #1
Total Residue, mg/1 24333
Fecal Coliform (ZIP\), /gram Solids <740
Drinking Water ID: 37715
Wastewater ID: 10
ID#: 890 I
DATE COLLECTED: 09/27/22
DATE REPORTED : 09/30/22
REVIEWED BY:
Sample
Sample
Sample Sample
Analysis
Method
#2
#3
#4 #5
Date Analyst Code
24533
24733
23867 24433
09/27./22
JRIS 254013-15
<740
<730
<750 <740
09/27/22
.113,1 9211E-14

Town of Clayton
Little Creek Water Reclamation Facility
WQ0023178
Nov-22
Environment 1, Inc.
Lab #
Date Analyzed
i > eieal` oliform
Log
HT-1
11/10122
190,000
5.279
HT-2
11/10/22
470,000
5.672
HT-3
11/10/22
470,000
5.672
HT-4
11/10/22
300,000
5.477
HT-5
11/10/22
460,000
5.663
HT-6
11/10/22
180,000
5.255
HT-7
11/10/22
470,000
5.672
Total 38.690
Averagel 5.5277
Most Probable Number / Gram 33`t64
,4 lFecal Coliform/gram
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

_._ ......... r . �. Dr3akiag.,Wnter _Il:�•,3r?,T_ 15.
Wastewater ID: 10
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE. N.0 27858 FAX [phone]
ID#: 890 I
TOWN OF CLAYTON
MR. BILL SIMPSON
P.O. BOX 879 DATE COLLECTED: 11/10/22
CLAYTON, NC 27528 DATE REPORTED : 11/17/22
REVIEWED BY_
Sample
Sample
Sample
Sample Sample
Analysis
Method
PARANTETTRS 1l1
#2
#3
tl4 #.;
Date Anahst
Code
Total Residue, mg/l 18400
19433
19367
17833 20233
11/i0122 .J1IS
254OB-15
Fecal Colilbrm (1JPN), /gram Solidi 190000
470000
470000
300000 460000
11/10/22 IINC'.
92211,:-14

E J d'l - -- --
D� n_ iug Wa_ es 2n•
Wastewater ID: 10
114 OAKMONT DRIVE
GREENVILLE. N.0 27858
TOWN OF CLAYTON
MR. BILL SIMPSON
P.O. BOX 879
CLAYTON, NC 27528
Sample Sample
PARA1tETERS N1 #2
Total Residue, mgll 18400 19433
Fecal Coliform (11PN), ;gram Solids 190000 470000
PHONE [phone]
FAX [phone]
ID#: 890 I
DATE COLLECTED: 11/10/22
DATE REPORTED : 11/17/22
REVIEWED BY.
Sample
Sample
Sample
Analysis
Ntctliod
#3
#4
#5
Date Analist
Code
19367
17833
20233
11il0/22 .JNIS
254013-15
470000
300000
460000
11/10/22 BNC
92211-1-14

Town of Clayton
Little Creek Water Reclamation Facility
WQ0023178
Dec-21
pate
SOUR*
In �oxygwg/hr
12/30/2021
0.94
12/30/2021
0.92
12/30/2021
1.04
12/30/2021
0.98
12/30/2021
1.05
12/30/2021
1.05
12/30/2021
0.89
* SOUR = Specific Oxygen Uptake Rate
Average 0.901
SOUR values are less than. 1.5 mg oxygen/gram/hour and meets the 40 CFR Part
503.33 Option 4 for Vector Attraction Reduction.
SOUR values provided by Town of Clayton WRF

Total Solids mg/ =Dill gm x 1000
Sample Vol ml
Date:�b/3o1zJ
Time In: I6
Town of Clayton
Total Solids at 103 - 105' C
SM 2540 B 18th ed.
Tirrfe ouiZ2
%RPD=2(A-B)x100
A + B
i
Dish WET gm
Dish Empty gm
Blank
Z
7 6.q q
Ir.9S,
to %
y390
"7L1.3Sp
1NG
�� / �� O
r'D
ZQ, 2,6g3-
Zz, jI y Z
Sample Vol. ml
0 h,(
Dish Dry.gm
Dish Empty gm
7q, 5 9,
7t1. gj ? Z
7(6, 1—�
mil `i
7 y, 76�'v
71.3
�6.�lor
75:361�
Residual gm
%SOLIDS
% RPD
rdt
�
0. 0
0.9171
Ql <
© g527
Ofv�
Date.
Time In:
Time not
J
Holding tank 1
Opp?
Dish WET gm
aZ-5% 2
Dish Empty gm
2 31
7.S'. 3�
71
Zi1�lel
Sample Vol.ml
Z.Q,6"�1(�
Dish Dry.gm
73 .Zoo
76, 30o Z
-72S�6-?
Dish Empty gm
Residual gm
%SOLIDS
11 11
l
% RPD

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Town
Biosolids Permit Number. WQ C
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids. -
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
1
20.7
12/30/21 0940
112130!21 0940 1
300 milliliters
1.999 %Dry Solids
20.7 degrees Celsius
21 degrees Celsius
0.1
6.7
1.0
5.92 mg Oxygen/hr
0.99 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Sample ID
HT-1
Temperature Corrected Specific Oxygen Uptake Rate: 0.94 mg Oxygen/g/hr
Instructions. Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
Slope.
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate.
Average Temperature.
Temperature Correction Factor:
Town of Clayton
W Q 0023178
12/30/21
20.6
12/30/21 1010
svj cw
12/30/21 1010
svj cw
300
1.981
20.6
21
0.1
8.0
1.0
milliliters
Yo Dry Solids
iegrees Celsius
iegrees Celsius
5.76 mg Oxygen/hr
0.97 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Sample ID
HT-1
Temperature Corrected Specific Oxygen Uptake Rate: 0 92 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
A -I-

IN
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Town
Biosolids Permit Number: WQ C
Digester Temperature:
Sampling Date/Time: 1
Sampled By: s
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
(mgll)
766
7,39
728
7,18
7.08
6.98
6.87
6.77
6.67
6.58
6.47
6.38
6.28
6.18
6.09
5.99
178
20.1
1035
cw
730/21 1035
cw
300 milliliters
1.987 % Dry Solids
20.1 degrees Celsius
20.6 degrees Celsius
Sample ID
HT-1
Slope: 0.1
Intercept: 7.5
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 6.23 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.04 mg Oxygen/g/hr
Average Temperature: 20 degrees Celsius
Temperature Correction Factor: 1
Temperature Corrected Specific Oxygen Uptake Rate: 1.04 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:[12/30/21
of Clayton
Biosol ds Permit Number:023178
Date:0/21
Digester Temperature: 20.
Sampling Date/Time:/21 1055
Sampled By:
Analysis Date/Time: 1055
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
`+U
7.42
7.33
7.24
7.14
7.04
300 Ililiters
1.984 Dry Solids
20.2 degrees Celsius
20.6 d grees Celsius
Sample ID
HT-1
Slope: 0.1
Intercept: 7.9
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 5.86 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.98 mg Oxygen/g/hr
Average Temperature: 20 degrees Celsius
Temperature Correction Factor: 1
Temperature Corrected Specific Oxygen Uptake Rate: �� 0.98 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
'yy

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
riku
6.91
6.67
6.56
6.47
6.36
6.25
6.15
5.6
5.5
5A
73'
5_2
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Town of Clayton
WO 0023178
12/30/2021
19.8
12/30/21 1206
svj cw
12/30/21 1206
svj cw
300
1.976
19.8
20.3
0.1
6.8
1.0
-nilliliters
Yo Dry Solids
Jegrees Celsius
legrees Celsius
6.22 mg Oxygen/hr
1.05 mg Oxygen/g/hr
20 degrees Celsius
1
Sample ID
HT-1
Temperature Corrected Specific Oxygen Uptake Rate: 1.05 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Town of Claytc
Biosol ds Permit Number: WQ 0023178
Date: 12/30/1
Digester Temperature:
Sampling Date/Time. 12/30/21 1225
Sampled By: sv' cw
Analysis Date/Time: 12/30/21 1225
Analyzed By: svj cw
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7.14
7.03
6.93
6.83
6.73
6.63
6.53
6.43
6.33
6.23
6.9
5.85
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
E
1
01
7.4
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
6.25 mg Oxygen/hr
1.05 mg Oxygen/g/hr
20 degrees Celsius
1
Sample ID
HT-1
Temperature Corrected Specific Oxygen Uptake Rate: 1.05 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
,b16

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Town of
Biosolids Permit Number: WQ 002
Date: 12/30/2
Digester Temperature:
Sampling Date/Time: 12/30/21
Sampled By: sv' cw
Analysis Date/Time: 12/30/21
Analyzed By: svj cw
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
mail
7,84
7.73
7.64
7.56
7.44
7.41
7.21
7.17
7.16
6.811
6
Slope -
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
1
300 milliliters
.991 % Dry Solids
20.1 degrees Celsius
20.7 aegrees Celsius
0.1
7.9
1.0
5.33 mg Oxygen/hr
0.89 mg Oxygen/g/hr
20 degrees Celsius
1
Sample ID
HT-1
Temperature Corrected Specific Oxygen Uptake Rate:_ 0.89 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
-t/7

I i C
76
iFi.er Addi(koi
0 f I
1�37-
35
/Z'
7.1
q4
420
Ira.
iZ.g1- /Z'
L ichl"
t Dili

Burnett LiGme Company, Inc. CERTIFIED PUBLIC WEIGHER
0 7095 Hwy 11, Campobello, SC 29322 _.
5200 US Hwy 17 S, Bartow, FL 33830 DELIVERY TICKET NO.
,j 1100 Airport Rd, Eastabega, AL 36260 64810
SHIPMENT DATE
- f
S SHIPMENT WEIGHTS
0 =_
L
T
0
S
H
I
P
T
0
t ,�,i,; x4}.;.' ,r
jrltl� �>t�Lt.LJ' '`%i�l'i 7t3�
CUSTOMER NO. I BLC ORDER LOT NO.
� J I
C7
PROJECT NO.
CUSTOMER PURCHASE ORDER NO.
N t
to
Ln
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-
L9
LU
-
.
BILL FREIGHT CHARGES TO:
BURNETT LIME CONSIGNEE
SHIPPED VIA TERMS
L';
1
1 1 Tanker CAL -FLOG Slurry
DRIVER MUST FIND OPERATOR ON DUTY AT END OF OFF-LOADING
NO DILUTION WATER NEEDED
AUTOMATIC DILUTION METER TURNED "ON"
INITIAL WATER METER READING
FINAL WATER METER READING
� F L�,
..JAL
BEGINNING TANK LEVEL FT ENDING TANK LEVEL FT
SYST E M S SCUFRY
*OPERATOR REQUESTED TO INSPECT SLURRY DILUTION ACCURACY
AND OFF-LOADING AREA CLEANLINESS b_CFg,, CAL-FLO•Slurry
en t Additive
�V` Drinking Water Treatmen
Tested in accordance with
OPERATOR UNABLE TO INSPECT UNLOADING PROCEDURE Standard ANSI/NSF60
Calcium Hydroxide
OPERATOR INITIALS IF DIFFERENT FROM CUSTOMER SIGNATURE tFM �"' 650 mg/L Maximum Use Level
H
w
Z
VIN #
rl ICTnhACD CtcKtATt Mr.

f w'i a ol f €a6 [1)f
� r' P itIIl:ttiotI t•<s
f.i,iil: ^2- � !.fJ.�tlirii:-�i'u,q�anK
fo,o6 X3o,000 �, J
l :3liltli.` I va—'..cd(' .301 415 ttifi t t:L'lf:
am
.l ftei :• dditiolt -
t • = f 2.00 •.1hei tellip.
mp,
Ili-s. after Addition
con-ectloll }
ZQ
I tion f irl if
D?y;31Z11Z 6*3I-_c):3D . _ o�
2 93
133S13/2/,zz' 42.�6 • 2. 7 9 ) z..381
1 13S/3/3Ja1; J2 • `%' . 2 7y lz • zo / ' J� . 9
Date Iime ! f;rlffcI R adia.; IN
I.3�L�L2 _i9b t U-..-_j..._...___I_J03.
f)aie' 7iai: ; I:iilff2t I;�'a+1i11<, ,li} 1

Burnett Dime Company, Inc.
rl 7095 Hwy 11, Campobello, SC 29322
,S200 US Hwy 17 S, Bartow, FL 33830
i100 Airport Rd, Eastaboga, AL 36260
SHIPMENT DATE
S
'My i t
D 0 uX F-
ti
T
0
S
H
I
P
T
0
Li111e C eek VRP
CUSTOMER NO. BLC ORDER LOT NO.
PROJECT NO.
CUSTOMER PURCHASE ORDER NO.
CERTIFIED PUBLIC WEIGHER
DELIVERY TICKET NO.
6508
SHIPMENT WEIGHTS
Ln f.�._
O
K
w
BILL FREIGHT CHARGES TO:
BURNETT LIME CONSIGNEE
SHIPPED VIA TERMS
1 1 1 Tanker CAL—FLO' Slurry
DRIVER MUST FIND OPERATOR ON DUTY AT END OF OFF-LOADING
NO DILUTION WATER NEEDED
AUTOMATIC DILUTION METER TURNED "ON"
INITIAL WATER METER READING
FINAL WATER METER READING
BEGINNING TANK LEVEL FT ENDING TANK LEVEL
*OPERATOR REQUESTED TO INSPECT SLURRY DILUTION ACCURACY
AND OFF-LOADING AREA CLEANLINESS
OPERATOR UNABLE TO INSPECT UNLOADING PROCEDURE
OPERATOR INITIALS IF DIFFERENT FROM CUSTOMER SIGNATURE
FT !�'
ti�
I_,O 8 S L L R R Y
CAL'FLO• Slurry
Drinking Water Treatment Additive
Fc Tested In accordance with
Standard ANSI/NSM
Calcium Hydroxide
„E ' • 650 mg/L Maximum Use Level
.t VIN # '
CUSTOMER SIGNATURE

ItA fle-altior,
1.2 1 0 .:too R .--c '14-i
Hold, k
, � 1 i. 11) li i .' ' v d:
a I.- t ()-I
ltittt3i-7-73
.3o
'I JJ 0 1 tit e i ri i j,
T,,S(-, Hrs. Aft:,
0,
o 3qo
0 11 i f•Ctlon
'14 tics. afierAciditifm
POP
o' zs-
11YO *96t'
?J-0
/Z. 3q 11ol
Dati�' 'Thilf, B Lt I ft,
(7- lit,
21
-
31181.x2 019y'l
3z
frit: QL6
Slope
DrAte" Time Buffer
Reading
My
13// 1/-- azz 70
i �, r�3
- �, g j
— 9'3"x.v'3 %
In - 7,91 99f.10

Burnett Dime Company, Inc. CERTIFIED PUBLIC WEIGHER
0 7095 Hwy 11, Campobello, SC 29322
5200 US Hwy 17 S, Bartow, FL 33830 DELIVERY TICKET NO.
0 1100 Airport Rd, Eastaboga, AL 36260 65264
SHIPMENT DATE
SHIPMENT WEIGHTS
S i1 un v roil # 1 ti"•T: ii-
0IIl[-
L c ties _ ch L.
D
T
O
S Qar -to a Vi' TI-P
I
(.13violl _fib. P._0 0
T
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43)` )I_.
LU
PROJECT NO.
BILL FREIGHT CHARGES TO:
BURNETT LIME CONSIGNEE
CUSTOMER N0.
BLC ORDER LOT NO. CUSTOMER PURCHASE ORDER NO. SHIPPED VIA TERMS
i -
ORDERED
SHIPPED DESCRIPTION-
1
1 Tanker CAL-FLO® Slurry
DRIVER MUST FIND OPERATOR ON DUTY AT END OF OFF-LOADING
NO DILUTION WATER NEEDED
AUTOMATIC DILUTION METER TURNED "ON"
INITIAL WATER METER READING_
FINAL WATER METER READING
C A L ==FLO
BEGINNING TANK LEVEL FT ENDING TANK LEVEL FT
SYSTEM & SLURRY
*OPERATOR REQUESTED TO INSPECT SLURRY DILUTION ACCURACY
AND OFF-LOADING AREA CLEANLINESS o.& r,� CAL-FLD•Slurry
Drinking Water Treatment Additive
F Tested In accordance with
OPERATOR UNABLE TO INSPECT UNLOADING PROCEDURE stziidarNSIlNSF6o
Calcium Hydr6nde
OPERATOR INITIALS IF DIFFERENT FROM CUSTOMER SIGNATURE _`'4e4 65t1 mg/I Maiimum Use Level
1­-
w
z
VIN #
CUSTOMER SIGNATURE
L

"i•S�:Ft`i
3o f m/®iY .-1.f��a Ef � .'li: 1..+ •-LrpT
i ti;[i;lI --
is tti i N;itltri-r:, —
ti�•Q0 nn }
fits. aftci—a=irli icr,In
--
3itt, fi,i• ;t { r,fk.,t l j1:41 1�12r#
o��s/s����zz 78b - •F� �•.. 16-_
G 8z s 141"vz�-1z. 5-Y. -.. -Z V-6
1z.30? 17.3
• lt.l�� lint.
Isttfit2
f:s;'1:iiit�
�Fi
Vyl22
7. o
_
-7.o4
' �•�-
35ah
10.0
fit!1
iit_il:ret--
i r.t :i.l:tir�
z�`I--.
L i
i

Burnett Lime Company, Inc.
7095 Hwy 11, Campobello, SC 29322
?00 US Hwy 17 S, Bartow, FL 33830
Ll i100 Airport Rd, Eastaboga, AL 36260
SHIPMENT DATE •
Skit}+]r lu','•r::
0 Aw rYxt '1JLi:- P-yv al !-
L _
D Ply Pox M--9
LI r1v toli i"'C 27520
T
0
S 0 sytet S L=
27
0
PROJECT NO.
CUSTOMER NO. I BLC ORDER LOT NO. { CUSTOMER PURCHASE ORDER NO.
CERTIFIED PUBLIC WEIGHER
DELIVERY TICKET NO.
65371 j
SHIPMENT WEIGHTS
Ln
O
l9
w
BILL FREIGHT CHARGES TO:
BURNETT LIME CONSIGNEE
SHIPPED VIA TERMS
1 1 Tanker CAL-FL0® Slurry
DRIVER MUST FIND OPERATOR ON DUTY AT END OF OFF-LOADING
NO DILUTION WATER NEEDED
AUTOMATIC DILUTION METER TURNED "ON"
INITIAL WATER METER READING
FINAL WATER METER READING A�,L�
BEGINNING TANK LEVEL FT ENDING TANK LEVEL FT s T s T E n a S: t, R R r
*OPERATOR REQUESTED TO INSPECT SLURRY DILUTION ACCURACY
AND OFF-LOADING AREA CLEANLINESS CAL-FLO•Slurry
Drinking Water Treatment Additive
Tested In accordance with
OPERATOR UNABLE TO INSPECT UNLOADING PROCEDURE `. ' 'f standardnxsi/rvsFw,
J Calcium Hydroxide
OPERATOR INITIALS IF DIFFERENT FROM CUSTOMER SIGNATURE 'yN 're, 65o mgiL Maximum Use level
VIN #
ry
2 ( p
CUSTOMER SIGNATURE

f er R;-'-
u ca o 11
IV/'ZzJv7, 10411
I Sod:
tit,
Fa c i i
0 q
A Re I.
�Iztln-
T
12.0f) ,lfte&
170 L7
q-5-
Z1,
24 Urs. after Addition
44
20.0
Jz
9.5-cl
h't plirej -
ID
J.-JAO-11
-1-3
In t
f. i C. (-"-7
Date. imej
Buffer
Veadill-v
l', r
i C*j'. 0 9
1-15- 0
i 1 .1-15
1 2. -1
1-3-23,3
f n t: '91
S Io p "� �

Burnett Lime Company, Inc.
'-' 7095 Hwy 11, Campobello, SC 29322
5200 US HWY 17 S, Bartow, FL 33830
❑ 1100 Airport Rd, Eastaboga, AL 36260
SHIPMENT DATE •
f
T
O
H Titt1p: ;fi e„ ° kic.F
T
O
PROJECT NO.
CUSTOMER NO•� I BLC ORDER LOT NO. I CUSTOMER PURCHASE ORDER NO.
CERTIFIED PUBLIC WEIGHER
DELIVERY TICKET NO.
6 '1 '2 I
SHIPMENT WEIGHTS
Ln
0
LU
BILL FREIGHT CHARGES TO:
BURNETT LIME CONSIGNEE
SHIPP�D VIA TERMS
1
1 1 Tanker CA' L"FLO® Slurry
DRIVER MUST FIND OPERATOR ON DUTY AT END OF OFF-LOADING
NO DILUTION WATER NEEDED
AUTOMATIC DILUTION METER TURNED "ON"
INITIAL WATER METER READING
FINAL WATER METER READING
BEGINNING TANK LEVEL FT ENDING TANK LEVEL FT��.___
*OPERATOR REQUESTED TO INSPECT SLURRY DILUTION ACCURACY
AND OFF-LOADING AREA CLEANLINESS o kc{ j carFlo=smrry
y'` !Drinktna Waterlteatmer+t Additive
Tested in accordance with
OPERATOR UNABLE TO INSPECT UNLOADING PROCEDURE ° Standard ANSI/NSF/CANED
xide
650 mg/L M u mYum. Use level
OPERATOR INITIALS IF DIFFERENT FROM CUSTOMER SIGNATURE f=Eros`
.I
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VIN #
CUSTOMER SIGNATURE

Rev 4/21/2022
Sludge Stabilization Record
Town of Clayton
Sam's Branch Water Reclamation Facility Permit: NC0025453
Date: 5 /1(r%)a
Location: t-{dC� ni ) lw* .k 1
Volume Treated: 1, 3. ,,,, Alkali Used:
Volume Used: `15.GG� PD5
—
'rime/ Date
Initial ; Correction
Final
Temp
H ' Factor
H
(°C)
Initial C('�1�
/ite%z 7-tL
�, ��
_
- (j• 7_
(�. (nb'
1 fi lc
—
After Addition
(>= 12.00 after temp.
—
',�v�//z L
i L• j
_ 2
Z 3
---
1
correction)
_
Two Urs. After Addition
(>= 12.00 after temp.
M} hz
2• Si
I d
i9 Z
correction)
—
24 Hrs. after Addition
(>= 11.50 after temp.Z�
t
correction)
Preparer:
Date /'rime
Suffer
Rea(
Temp (°C)
11 v _
51NIZZ
4i. 0
41,00_
1-7- 19
/2.q5
2.77
�(5 5
- 32
Int: 5�,yi Slope: -58.37 % Eff: 99 `/b
Date / Time
Buffer
Reading j
rem(,C)
A1v
_
11
q o
q'O
I _ 1', 7
172.9
Air
-7. D
!1
12-260
2 9
Int: SM Slope: -5S 4 1 % Eff: 99 °�

Burnett Lime Company, Inc.
-17095 Hwy 11, Campobello, SC 29322
J 5200 US Hwy 17 S, Bartow, FL 33830il
❑ 1100 Airport Rd, Eastaboga, AL 36260
SHIPMENT DATE tJ
0 :Y.. _q-e
T
O
S "No*
H
P V Y �
T
0
CERTIFIED PUBLIC WEIGHER
DELIVERY TICKET NO.
6747
SHIPMENT WEIGHTS
Ln
Ln
r
LU
.N,
PROJECT NO.
`~.
BILL FREIGHT CHARGES TO:
BURNETT LIME CONSIGNEE
CUSTOMER NO.
BLC ORDER LOT NO. CUSTOMER PURCHASE ORDER NO. SHIPPED VIA TERMS
O. DERED
s
1
1 Tanker CAL—FLO' Slurry
DRIVER MUST FIND OPERATOR ON DUTY AT END OF OFF-LOADING
NO DILUTION WATER NEEDED
AUTOMATIC DILUTION METER TURNED "ON"
INITIAL WATER METER READING
FINAL WATER METER READING
BEGINNING TANK LEVEL FT ENDING TANK LEVEL FT
*OPERATOR REQUESTED TO INSPECT SLURRY DILUTION ACCURACY
AND OFF-LOADING AREA CLEANLINESS ��acFRrR at-rTodat ie�r
Drinking Waterheamieni Additive
w Tested In aaofdance wkh
OPERATOR UNABLE TO INSPECT UNLOADING PROCEDURE ' ° °i StarrdaidAy51/j§F/tAN60
y Calcium Hpdradde
OPERATOR INITIALS IF DIFFERENT FROM CUSTOMER SIGNATURE E" �`' 650mg/1.jviaiimunnUse Lr I
I
VIN #
CUSTOMER SIGNATURE

Rev 1 11i20?1
"'lucire Stabilization I%ecord
7 c n of L lal toil
'+anl's Brand) Ni attr Reclamation I kill(% Vertnit: ; .-1tt}2545.3
Date; -6l31 z oz ?- ----
VolifInc'1I-v;IIed: 3, Allf ali Used: CO
1 olttnic Used:
Time: Date Initid Correcliol;
1Final
Jculp,
lilI
l
%
23.
After Addition
i
!
[ `= 12.00 illtCi ICInp
A�-�-
6
�O
p
2-0� O
correction}
6 1 %Za�2tS�/'j
j -1 tiro III-S. After Addition
'
/03 7
- -
i s>= 12.00 After temp.
t�
' Correction)6t21
Zos.�.
2-1 EIt-s, a!'trr aclditio,I
i: = 11.50 after tcnlll.-----a--
correcdar►} IY ZG'Z-�z f z o 2
i
Pre -parer _
i !?,Ite,iTilli
-:........- — .......
! l3ui'fci
------
-! Readin
_ = I'ctu 'f }
l
Nis -
v
- -
_
- ------ - -- - ----- ---- -- --
Date 'Tillic
! --------- Buffer . _ i Readitlf,
-- ---- _rU . U
Ilit: _ - _ Slope:- Fff: IL96 Pt _—

B rnett Lime
17095 Hwy 11, Campobello, SC 29322
J 5200 US Hwy 17 S, Bartow, FL 33830
Company, Inc.
r
❑ 1100 Airport Rd, Eastaboga, AL 36260
SHIPMENT DATE
•
S {.t l tor; i =1 t. ct,
D
T':
O
CERTIFIED PUBLIC WEIGHER
DELIVERY TICKET NO.
SHIPMENT WEIGHTS
to
Ln
fff
f.1�F
C7
R;e�a
LU
Q
}
2 It fir 6 -�I,c,
PROJECT NO. BILL FREIGHT CHARGES TO:
BURNETT LIME CONSIGNEE
CUSTOMER NO. BLC ORDER LOT NO. CUSTOMER PURCHASE ORDER NO. SHIPPED VIA TERMS
1 1 1 Tanker CAL-FLO' Slurry
DRIVER MUST FIND OPERATOR ON DUTY AT END OF OFF-LOADING
NO DILUTION WATER NEEDED
AUTOMATIC DILUTION METER TURNED "ON"
INITIAL WATER METER READING
FINAL WATER METER READING EE
BEGINNING TANK LEVEL FT ENDINGTANKLEVEL FT
*OPERATOR REQUESTED TO INSPECT SLURRY DILUTION ACCURACY
ce CAL-'FLO• Slurry
AND OFF-LOADING AREA CLEANLINESS y� Drinking Water Treatment Additive
In
OPERATOR UNABLE TO INSPECT UNLOADING PROCEDURE �� of Standard Tedard accordance with
AN51/14$F/CANED
y Calcium Hydrmdde
OPERATOR IN ITLALS IF DIFFERENT FROM CUSTOMER SIGNATURE OeaENOE 6SO mg/L Maximum Use level
VIN #
N
ry
Z
CUSTOMER SIGNATURE

ReN
Town ot, C-LIN hill
Sim's BrAnch Water Reclamation Fiicilit.v Permit: N0,02-5,450"
Date:
Local io I I:
VoI1111w Treated:
3z q,v
'
Volurla. Uwd: goo
Time Dave juilin]
Correctioll
^ I 'illfll Tulip
Factor
pj I
nifial
ARO)''Additioll
12.00 after temp.
Z10
I 4No airs. After Addilion
12.00 arler temp.
Correction)
nftcr Addition [Irs,
I 1 .50 after temp.
z 2.
correctioll)
Prepare,: t111T 4)
BLIMl-
I Readinu
I 11°,D
I
Z.
A-12L
list:
i.R ea (I i n
Date Ti m It" ffer Temp ("C) NIN
--- --------
Int: A�L_ slope: 7 y tC Eff:
<

Burnett Lime Company,
7095 Hwy 11, Campobello, SC 29322
5200 US Hwy 17 S, Bartow, FL 33830
❑ 1100 Airport Rd, Eastaboga, AL 36260
SHIPMENT DATE •
S t.J:; y ii}I'> 11iE'iit.
L PO. )y T%l
T
O
S clay-torl VINVIT ENO+
P clay ri, _ 231,20
T
O
CUSTOMWNO. BLC ORDER L_OT NO.
PROJECT NO.
Inc.
CUSTOMER PURCHASE ORDER NO.
-- J 1 1
CERTIFIED PUBLIC WEIGHER
DELIVERY TICKET NO.
•3QL2
SHIPMENT WEIGHTS
t
O
''►.f�l
l7
LU
E;
f...
...I1,
BILL FREIGHT CHARGES TO:
❑ BURNETT LIME CONSIGNEE
SHIPPED VIA TERMS
• f
1 1 Tanker CAL -FLOG Slurry
DRIVER MUST FIND OPERATOR ON DUTY AT END OF OFF-LOADING
NO DILUTION WATER NEEDED
AUTOMATIC DILUTION METER TURNED "ON"
INITIAL WATER METER READING
FINAL WATER METER READING T
BEGINNING TANK LEVEL FT ENDING TANK LEVEL FT
SYSTEM t SLU R0.Y
*OPERATOR REQUESTED TO INSPECT SLURRY DILUTION ACCURACY
/CAL^fL06Slurry
AND OFF-LOADING AREA CLEANLINESS I^E °'<1 Drinking Water Treatment Additive
ith
OPERATOR UNABLE TO INSPECT UNLOADING PROCEDURE I Tendardsted In accordancevu46
�� Standard ANSI/NSF/CAN6U
i Cildum HVdredde
OPERATOR INITIALS IF DIFFERENT FROM CUSTOMER SIGNATURE 650 mg/l Maximum Use Level
r,
VIN #
! J= W
z
rt e ern E•t r^nt nIrt 113[

Rev?2112N2
Date:
11.0calion:
Sludge Stabilitatiun Record
no n or chl ton
Sarn! fhonch V%Qer Redzirmition hacilil� Permit: N('002-54-53
%Mau Kul:
Volmlic U.Sod: - gr
HI'lle Date F9nititil ! corre Th f emp
iil FactorILI
initial
z 7- - 0
sifter Addition
C— 12.00 after terup. ;Sljp/ZL ?3o 0 - 06 12 -?-'1 ZZ
h'o firs. After addition
12.01) itfter temp. 12 -3o -o.o6 •241
24 tin. wher Addition
Z3 I L50 after lemp.
correction)
2—
Preparer:
It
- ------- 3-L
I tit: tt Slope: Eff-.
Tc- P-f Q vnp
-.--XAO
W: mQ, S I fa p C: - E IF f: Z

Burnett Lime Company, Inc. CERTIFIED PUBLIC WEIGHER
7095 Hwy 11, Campobello, SC 29322
5200 US Hwy 17 S, Bartow, FL 33830 DELIVERY TICKET NO.
❑ 1100 Airport Rd, Eastaboga, AL 36260 L? i
SHIPMENT DATE
_ SHIPMENT WEIGHTS
0
L
D
T
0
5
H
I
P
T
0
CUSTOMER NO. I BLC ORDER LOT NO.
PROJECT NO.
CUSTOMER PURCHASE ORDER NO.
U
BILL FREIGHT CHARGES TO:
BURNETT LIME CONSIGNEE
SHIPPED VIA TERMS
1 1 1 Tanker CAL—A'0_ 6 Slurry
DRIVER MUST FIND OPERATOR ON DUTY AT END OF OFF-LOADING
NO DILUTION WATER NEEDED
AUTOMATIC DILUTION METER TURNED "ON"
INITIAL WATER METER READING
FINAL WATER METER READING _ g
BEGINNING TANK LEVEL FT ENDING TANK LEVEL FT �I L
S Y S i E M S S L U 0. R 7
*OPERATOR REQUESTED TO INSPECT SLURRY DILUTION ACCURACY
AND OFF-LOADING AREA CLEANLINESS Eo "_crt,, Cu'Ft0'slurry
/y OrinldngWaterTreatmentAdditive
w •� n.accotdame with
OPERATOR UNABLE TO INSPECT UNLOADING PROCEDURE ° Standard AN51/MSF%CAN60
91cium Mpdrmid
e
OPERATOR INITIALS IF DIFFERENT FROM CUSTOMER SIGNATURE rx root'` ' 650mQ/L Tested iMtaca Use Level
INSTRUCTIONSSPECIAL CRIVER NAME TANKER NO.
T— �. `y �. _...
VIN #
F-
w
Z
CUSTOMER SIGNATURE

Rev 4llaO22
Shidge Stabilization Recor(j
70"n uf C53mil
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Burnett Lime
Company, Inc,
7095 Hwy 11, Campobello, SC 29322
❑ 5200 US Hwy 17 S, Bartow, FL 33830
❑ 1100 Airport Rd, Eastaboga, AL 36260
SHIPMENT DATE
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SHIPMENT WEIGHTS
L
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BILL FREIGHT CHARGES TO:
❑ BURNETT LIME CONSIGNEE
SHIPPED VIA TERMS
1 1 1 Tanker CAL—FLO' Slurry
DRIVER MUST FIND OPERATOR ON DUTY AT END OF OFF-LOADING
NO DILUTION WATER NEEDED
AUTOMATIC DILUTION METERTURNED "ON"
INITIAL WATER METER READING
FINAL WATER METER READING _
BEGINNING TANK LEVEL FT ENDING TANK LEVEL FT
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t Additive
OPERATOR UNABLE TO INSPECT UNLOADING PROCEDURE ° s�a r'aiuvsi�'sFicso
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Rev 4 Z1,2022
Sludge *Stabilir:uioi] Record
•lovtiI]lit' CJai ton
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Time I Date friitial � C'orrectimi 1'iiial j Tenif)
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Burnett Lima Company, Inc.
77095 Hwy 11, Campobello, SC 29322
j200 US Hwy 17 S, Bartow, FL 33830
❑ 1100 Airport Rd, Eastaboga, AL 36260
SHIPMENT DATE
• 'T I
L PO
(layl D.. X' 27t T
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6907
SHIPMENT WEIGHTS
W
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PROJECT NO.
BILL FREIGHT CHARGES TO:
BURNETT LIME CONSIGNEE
CUSTOMER
BLC ORDER LOT NO. CUSTOMER PURCHASE ORDER NO. SHIPPED VIA TERMS
ORDERED
SHIPPED DESCRIPTION
1
1 - Tanker CAL FLO® Slurry
DRIVER MUST FIND OPERATOR ON DUTY AT END OF OFF-LOADING
NO DILUTION WATER NEEDED
AUTOMATIC DILUTION METER TURNED "ON"
INITIAL WATER METER READING
FINAL WATER METER READING ��•--�yr',,�� � F
{l -^ L
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s
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dhive
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<w '- Tested inaccortlance wfth
_ OPERATOR UNABLE TO INSPECT UNLOADING PROCEDURE Standard AN51/NCAN60
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OPERATOR INITIALS IF DIFFERENT FROM CUSTOMER SIGNATURE y°E 650 mg/l�Miuimum Use level
M
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CUSTOM ER51GNATURE

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Burnett Dime Company, Inc.
7095 Hwy 11, Campobello, SC 29322
u 5200 US Hwy 115, Bartow, FL 33830 r
01100 Airport Rd, Eastaboga, AL 36260
SHIPMENT DATE • r
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24
SHIPMENT WEIGHTS
t0 4 40LE
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CC
I
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BILL FREIGHT CHARGES TO:
BURNETT LIME
SHIPPED VIA
CONSIGNEE
TERMS
1 1 Tanker CAL -FLOG Slurry
DRIVER MUST FIND OPERATOR ON DUTY AT END OF OFF-LOADING
NO DILUTION WATER NEEDED
AUTOMATIC DILUTION METER TURNED "ON"
INITIAL WATER METER READING
FINAL WATER METER READING CAL
L FI��
BEGINNING TANK LEVEL FT ENDING TANK LEVEL FT S Y S T E M & SLURRY
*OPERATOR REQUESTED TO INSPECT SLURRY DILUTION ACCURACY
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AND OFF-LOADING AREA CLEANLINESS �E y Drinking Water Treatment Additive
Tested in accgtdance with
OPERATOR UNABLE TO INSPECT UNLOADING PROCEDURE StandardANSIINSF/caNso
calcium Hydroxide
OPERATOR INITIALS IF DIFFERENT FROM CUSTOMER SIGNATURE �•S �` . 6so mg/L Maximum Use Level
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Town of Rose Hill
Rose Hill WWTP
NPDES Permit # NCO056863
Nov-22
Environmental Chemists, Inc.
Dat A
�-g ... . . . . . . . . ...
...............
............
r:
p ... ........
.....
1
4/29/22
6,285
3.798
1
4/29/22
46,864
4.671
3
4/29/22
322,808
5.509
4
4/29/22
128,866
5.110
5
4/29/22
60,520
4.782
6
4/29/22
12,372
4.092
7
4/29/22
41,950
4.62
Total
Average[:
Most Probable Number / Gram Fecal Cotiform/gram
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4124 Fax
710 Bowsertown Road, Manteo, NC 27954 0 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info n environmentalchemists.com
Branch Residuals/Bob Branch
Date of Report: May 11, 2022
1735 Heckle Blvd Suite 103-291
Customer PO #:
Rock Hill SC 29732
Customer ID: 15060009
Attention: Bob Branch
Report #: 2022-07795
Project ID: Rose Hill WWTP
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-18825 Site: 1
4/29/2022 10:26 AM Solid/Sludge jcb/envirochem
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 6
31.0 % 05/03/2022
Fecal Density
SM 9221C E-2014 6285 MPN/g 04/29/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-18826 Site: 2
4/29/2022 10:26 AM Solid/Sludge jcb/envirochem
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
27.7 % 05/03/2022
Fecal Density
SM 9221C E-2014
46864 MPN/g 04/29/2022
Lab lD Sample ID:
Collect Date/Time Matrix Sampled by
22-18827 Site: 3
4/29/2022 10:27 AM Solid/Sludge jcb/envirochem
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
28.5 % 05/03/2022
Fecal Density
SM 9221C E-2014
322808 MPN/g 04/29/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-18828 Site: 4
4/29/2022 10:27 AM Solid/Sludge jcb/envirochem
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
27.2 % 05/03/2022
Fecal Density
SM 9221C E-2014
128866 MPN/g 04/29/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-18829 Site: 5
4/29/2022 10:28 AM Solid/Sludge jcb/envirochem
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
28.1 % 05/03/2022
Fecal Density
SM 9221C E-2014 60520 MPN/g 04/29/2022
Report # 2022-07795
Page 2 of 3

,e,n.virochem
ANALYTICAL & CONSULTING CHEMISTS
Branch Residuals/Bob Branch
1735 Heckle Blvd Suite 103-291
Rock Hill SC 29732
Attention: Bob Branch
Environmental. Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
into:a` environmentalchemists.coni
Date of Report: May 11, 2022
Customer PO #:
Customer ID: 15060009
Report #: 2022-07795
Project ID: Rose Hill VWVTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-18830 Site: 6 4/29/2022 10:28 AM Solid/Sludge jcb/envirochem
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 28.3 % 05/03/2022
Fecal Density SM 9221C E-2014 12372 MPN/g 04/29/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-18831 Site: 7 4/29/2022 10:29 AM Solid/Sludge jcb/envirochem
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 31.0 % 05/03/2022
Fecal Density SM 9221C E-2014 41950 MPN/g 04/29/2022
Comment: Results, except pH, reported on a dry weight basis, pH reported on an as received basis.
Reviewed by:
Report #. 2022-07795 Page 3 of 3

Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Clientr(,� V 1C� (� ` L '
I �1 Ul C �5 Date: `T 7_9 ZZ Report Number: _ 2022- %%CJ5
Receipt of sample:
ECHEM Pickup Client Delivery ❑
UPS ❑ FedEx ❑ Other ❑
❑ YES ❑ NO
N/A 1. Were custody seals present on the cooler?
❑ YES ❑ NO
N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt 5.0 °C Corrected temperature upon receipt °
How temperature taken:
C
El Temperature Blank N Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
YES ❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES ❑ NO
4. Were proper custody procedures (relinquished/received) followed?
YES ❑ NO
5. Were sample ID's listed on the COC?
YES ❑ NO
6. Were samples ID's listed on sample containers?
YES ❑ NO
7. Were collection date and time listed on the COC?
YES ❑ NO
8. Were tests to be performed listed on the COC?
3Z YES I ❑ NO
9. Did samoles arrive in proper containers for each test?
YES ❑ NO
10. Did samples arrive in good condition for each test?
YES ❑ NO
11. VVas adequate sample volume available?'
YES ❑ NO
12. Were samples received 'th'
❑ YES
❑ NO
wi in proper holding time for requested tests?
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? -_
❑ YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
❑ NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet
Sample Preservation:
Sample(s)
by adding (circle one):
Time of preservation:
(Must be completed for any sample(s) incorrectly preserved or with headspace)
were received incorrectly preserved and were adjusted accordingly
HZS04 HNO3 HCl NaOH
If more than one preservative is needed, notate in cornmpnfc holn,Ar
rvu[e: Koury customer service immed'ately for incorrectly preserved samples Obta'n a new sample or
notify the state lab if directed to a-ia lzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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Onslow Water and Sewer Authority
Swansboro WWTP
Permit # WQ0023261
Nov-22
Environmental Chemists, Inc.
...
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........... .......
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::.:.:.: .:.:.:.:.:...:.:::....:
` Avg
1
I IJ21/22
34,314
4.535
2
11/21/22
107,624
5.032
3
11/21/22
58,202
4.765
4
11/21/22
72,223
4.859
5
11/21/22
64,357
4.809
6
11/21/22
56,702
4.754
7
11/21/22
36,074
4.557
Total 33 310 :::::: ; `
Average4759':`'`:`
Most Probable Number / Gram 5:136 ..:.' : : ; . Fecal Coliform/gram
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

t4l !->
ONWASA
December 13, 2022
Mark Young
Swansboro WRF
199 Williams Road
Swansboro, NC 28584
RE: Swan Solids
ONWASA Laboratory
228 Georgetown Road
Jacksonville NC 28540
[phone]
Enclosed are the results of analyses for samples received by our laboratory on 11/21/2022. If you
have any questions concerning this report, please feel free to contact me.
Sincerely,
Ole
{
,)� 4
Todd A. Roberts For Mark Young
Northwest ORC

��
ONWASA
Swansboro WRF Project: Swan Solids
199 Williams Road Project Number: Reported:
Swansboro, NC 28584 Project Manager: Mark Young 12/13/2022 15:11
Sample Results
Data Analyzed by: Environmental Chemists, Inc.
Sample: Swan Fecal #1 S224803-01 (WW)
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density 34314 MPN/g 11/21/2022 SM 9221C E MPN
24hr 503
Total Solids (%) 2.04 % 11/22/2022 SM 2540 G
Sample Results
Data Analyzed by: Environmental Chemists, Inc.
Sample: Swan Fecal #2 S224803-02 (WW)
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density 107624 MPN/g 11/21/2022 SM 9221C E MPN
24hr 503
Total Solids (%) 2.23 % 11/22/2022 SM 2540 G
Sample Results
Data Analyzed by: Environmental Chemists, Inc.
Sample: Swan Fecal #3 S224803-03 (WW)
Reporting Date Analyst
Analyte Result Qua[ Limit Units Analyzed Initials Method
Fecal Density 58202 MPN/g 11/21/2022 SM 9221C E MPN
24hr 503
Total Solids (%) 1.89 % 11/22/2022 SM 2540 G
Sample Results
Data Analyzed by: Environmental Chemists, Inc.
Sample: Swan Fecal #4 S224803-04 (WW)
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety. Page 2 of 6

ONWASA
Swansboro WRF Project: Swan Solids
199 Williams Road Project Number: Reported:
Swansboro, NC 28584 Project Manager: Mark Young 12/13/2022 15:11
Sample Results
(Continued)
Data Analyzed by: Environmental Chemists, Inc.
Sample: Swan Fecal #4 (Continued) S224803-04 (WW)
Reporting Date Analyst
Analyte Result Qua[ Limit Units Analyzed Initials Method
Fecal Density 72223 MPN/g 11/21/2022 SM 9221C E MPN
24hr 503
Total Solids ("/o) 1.8 % 11/22/2022 SM 2540 G
Sample Results
Data Analyzed by: Environmental Chemists, Inc.
Sample: Swan Fecal #5 S224803-05 (WW)
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density 64357 MPN/g 11/21/2022 SM 9221C E MPN
24hr 503
Total Solids (%) 2.02 % 11/22/2022 SM 2540 G
Sample Results
Data Analyzed by: Environmental Chemists, Inc.
Sample: Swan Fecal #6 S224803-06 (WW)
Reporting Date Analyst
Analyse Result Qual Limit Units Analyzed Initials Method
Fecal Density 56702 MPN/g 11/21/2022 SM 9221C E MPN
24hr 503
Total Solids (%) 1.94 % 11/22/2022 SM 2540 G
Sample Results
Data Analyzed by: Environmental Chemists, Inc.
Sample: Swan Fecal #7 S224803-07 (WW)
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety. Page 3 of 6

4N WASA
Swansboro WRF Project: Swan Solids
199 Williams Road Project Number: Reported:
Swansboro, NC 28584 Project Manager: Mark Young 12/13/2022 15:11
Sample Results
(Continued)
Data Analyzed by: Environmental Chemists, Inc.
Sample: Swan Fecal #7 (Continued) S224803-07 (WW)
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density 36074 MPN/g 11/21/2072
Total Solids (%) 2.19 % 11/22/2022
SM 9221C E MPN
24hr 503
SM 2540 G
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Page 4 of 6

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F"Poo -- --V Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 91.0.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 279544 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS inf6a emrironmentalchemists com
Onslow Water & Sewer Authority
Date of Report: Nov 30, 2022
228 Georgetown Road
Customer PO #:
Jacksonville NC 28540
Customer ID: 08100092
Attention:
Report #: 2022-23233
Project ID: Swansboro
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-57142 Site: 001
11/21/2022 9:50 AM Solid/Sludge Zachary Dail
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
2.04 % 11/22/2022
Fecal Density
SM 9221C E-2014 34314 MPN/g 11/21/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-57144 Site: 002
11/21/2022 9:62 AM Solid/Sludge Zachary Dail
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
2.23 % 11/22/2022
Fecal Density
SM 9221C E-2014 107624 MPN/g 11/21/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-57145 Site: 003
11/21/2022 9:53 AM Solid/Sludge Zachary Dail
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
1.89 % 11/22/2022
Fecal Density
SM 9221C E-2014
58202 MPN/g 11/21/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-57146 Site: 004
11/21/2022 9:54 AM Solid/Sludge Zachary Dail
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
1.80 % 11/22/2022
Fecal Density
SM 9221 C E-2014
72223MPN/g 11/21/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-57147 Site: 005
11/21/2022 9:56 AM Solid/Sludge Zachary Dail
Test
Method
Results Date Analyzed
Total Solids (%) SM 2540 B 2.02 % 11/22/2022
Fecal Density SM 9221C E-2014 64357 MPN/g 11/21/2022
Report #.. 2022-23233 Page 1 of 2

Eenviroche]m
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, ITC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info+Cenvironmentalchemists.com
Onslow Water & Sewer Authority
Date of Report:
Nov 30, 2022
228 Georgetown Road
Customer PO #:
Jacksonville NC 28540
Customer ID:
08100092
Attention:
Report #:
2022-23233
Project ID: Swansboro
Lab ID Sample ID:
Collect DatelTime Matrix
. Sampled by
22-57148 Site: 006
11/21/2022 9:57 AM Solid/Sludge
Zachary Dail
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
22-57149 Site:007
Method
SM 2540 B
SM 9221C E-2014
Results Date Analyzed
1.94 % 11 /22/2022
56702 MPN/g 11/21/2022
Collect Date/Time Matrix Sampled by
11/21/2022 9:58 AM Solid/Sludge Zachary Dail
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E-2014
Comment: Results reported on a dry weight basis.
Reviewed by: ,�(�� P& -
2.19 % 11/22/2022
36074 MPN/g 11/21/2022
Report #:: 2022-23233 Page 2 of 2

Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
6602 Windmill Way
Wilmington, NC 28405
91.0-392.0223
C = nt: �JY�1 vV�h C ' .— -- Date: 121 12L Report Number: 2022-2� ---'9
Ir•:.. rl t,'_ r
�r- yES �J f:G
C�i f:i {=iG;rr)�!i a n[ ). r �u1i « -- -, -- ---
F 7 E3 IJP� Li re:iEr Cl �.
fJ.' ; I1 !{`er_ custod-• 3e31s present on the
Ifcustody s_als:vere present, tivere they intact/unbroken? I
Oribinal temperature upon receipt Z__(�__`C Corrected temperature upon receipt
`J
Ho:�. lernp!rature to :en:
_
❑ Temperature Blank Against Bottles I
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor'C: 0.0 -
YES
D NO
3. If temperature of cooler exceeded 6°C, was Project PVlgr./QA notified?
YES
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
YES
❑ NO
5. Were sample ID's listed on the COC?
NO
6. Were samples ID's listed on sample containers?
NO
7. Were collection date and time listed on the COC?
NO
8 Were tests to be performed listed on the COC?
O
9. Did samples arrive in proper containers for each test?
LYESO
O
10. Did samples arrive in good condition for each test?
O
11. Was adequate sample volume available?' "I
O
O
1.2. Were samples received within proper holding time for requested tests?
13. Were acid preserved samples received at a pH of <2?
O
14. Were cyanide samples received at a pH >12?
❑ YES
D NO
15. Were sulfide samples received at a pH >9?
❑ YES ❑ NO
❑ YES— I❑ NO
1i YES ❑ N0
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/i ?'
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
18. Were orthophosphate samples filtered in the field within 15 minutes?
anai a: onle or ,is and recorded en the i bench-sh=et
"" na_te-ia s=mpl_.S a•e checKed for Chlorine at time of ar,aiysis and recorded on the benchsheet.
Sample Preservation:
Samples)
by adding (circle one)
Time of preservation: _
(Must be completed for any sample(s) incorrectly preserved or with headspace)
— were received incorrectly preserved and were adjusted accordingly
H_50._ HNO; HCI NaOH
if more than one preservative is needed, notate in comments belov.
Voiatiles Samples
were received with headsoace
IVIVMtNrS:
DOC. OA.002 RPj 1

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ENVIRONMENTAL CHEMISTS, INC
P.O. BOX 1037
WRIGHTSVILLE BEACH, NC 28480
Voice: 910-392-0223
Fax: [phone]
E-Mail: [e-mail]
Bill To:
ON WASA
228 GEORGETOWN ROAD
ATTN: DAVID MOHR
JACKSONVILLE, NC 28540
PLEASE USE THE P.O. BOX FOR
ALL REMITTANCES. THANK YOU.
INVOICE NUMBER
202568
Invoice Date:
Dec 8, 2022
Page:
1
Customer ID
Customer PO
Payment Terms
08100092
10859 SWANSBORO FD
Net 30 Days
ENVIROCHEM'S FEDERAL ID #
Ship Date
Due Date
56-18943 79
11 /21 /22
1 /7/23
Quantity
Description
Unit Price
Amount
REPORT #2022-23233
SLUDGE: SWANSBORO WRF
DATE SAMPLED: 11/21/2022
7.00
FECAL DENSITY, TOTAL SOLIDS %
75.00
525.00
1.00
SAMPLE PICKUP FEE: 11/21/2022
15.00
15.00
***** email all invoices with the reports. DO NOT MAIL ANYTHING.
PLEASE REFERENCE INVOICE NUMBER ON ALL
REMITTANCES IN ORDER TO PROPERLY APPLY TO
YOUR ACCOUNT. CALL TERESA WOLFE OR FRAN
GODLEY @ 910-392-0223 FOR QUESTIONS.
Subtotal
Payment/Credit Applied
Total Amount Due $
540.00
540.00

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Town of Wallace
Wallace Wastewater Treatment Plant
NPDES Permit # NCO020702
Jan-22
Enviromnental Chemists, Inc.
Lab #
Date Aaaty ed
Most Probable Number
per gram
Log
1
1/05/2022
612
2.787
2
1/05/2022
278
2.444
3
1/05/2022
1,057
3.024
4
1/05/2022
808
2907
5
1/05/2022
1,041
3.017
6
1/05/2022
519
2.715
7
1/05/2022
1,287
3.110
Total20.404
Average 2.558
Most Probable Number 1 Gram Fecal Coliformlgram
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

nvirochem-
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab * 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 * 910.347.5843 Lab/Fax
infoCenvironmentalchemists.com
Branch Residuals/Bob Branch Date of Report: Jan 26, 2022
1735 Heckle Blvd Suite 103-291 Customer PO #:
Rock Hill SC 29732 Customer ID: 15060009
Attention: Bob Branch Report #: 2022-00308
Project ID: Wallace WWTP
pH SW 846 Method 9045D 6.87 units 01 /24/2022
Result estimated Analyzed out of 15 minutes hold time
Mercury SW-8467471 B 0.956mg/kg 01/14/2022
TCLP Metals
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Mercury
Lab ID Sample ID:
22-00777 Site:1
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
22-00778 Site:2
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
22-00779 Site:3
Test
Total Solids (%)
Fecal Density
EPA 2007 Rev 4 4, 1994
EPA 200 7 Rev 4 4, 1994
EPA 200 7 Rev. 4.4. 1994
EPA 200 7 Rev. 4.4, 1994
EPA 200 7 Rev. 4.4, 1994
EPA 200 7. Rev 4.4, 1994
EPA 200 7 Rev 4 4, 1994
EPA 245 1
<1 mg/L
<1 mg/L
<1 mg/L
<1 mg/L
<1 mg/L
<1 mg/L
<1 mg/L
<0.0002 mg/L
Collect Date/Time Matrix
1/5/2022 8.50 AM Solid/Sludge
Method Results
SM 2540 B
SM 9221C E-2014
2.78 %
612 MPN/g
01/14/2022
01/14/2022
01/14/2022
01/14/2022
01/14/2022
01/14/2022
01/14/2022
01/14/2022
Sampled by
InYoung Seo
Date Analyzed
01 /07/2022
01/05/2022
Collect Date/Time Matrix Sampled by
1/5/2022 8:50 AM Solid/Sludge InYoung Seo
Method Results Date Analyzed
SM 2540 B
SM 9221C E-2014
Collect Date/Time
1/5/2022 8 50 AM
Method
SM 2540 B
SM 9221C E-2014
2.85 %
01 /07/2022
278 MPN/g
01 /05/2022
,
Matrix
Sampled by
Solid/Sludge
InYoung Seo
Results
Date Analyzed
2.65 %
01 /07/2022
1057 MPN/g
01 /05/2022
Report # 2022-00308 Page 3 of 4

envirochem
•r
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 , 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
[e-mail]
Branch Residuals/Bob Branch Date of Report: Jan 26, 2022
1735 Heckle Blvd Suite 103-291 Customer PO #:
Rock Hill SC 29732 Customer ID: 15060009
Attention. Bob Branch Report #: 2022-00308
Project ID: Wallace WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-00780 Site: 4 1/5/2022 8:50 AM Solid/Sludge InYoung Seo
Test w Method Results Date Analyzed
Total Solids (%)
Fecal Density
Lab ID Sample ID:
22-00781 Site:5
Test
Total Solids
Fecal Density
Lab ID Sample ID:
22-00782 Site:6
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
22-00783 Site:7
Test
SM 2540 B
SM 9221C E-2014
Collect Date/Time
1/5/2022 8:50 AM
Method
SM 2540 B
SM 9221C E-2014
Collect Date/Time
1/5/2022 8:50 AM
Method
SM 2540 B
SM 9221C E-2014
Method
Collect DatelTime
1/5/2022 8:50 AM
2.60 % 01/07/2022
808 MPN/g 01/05/2022
Matrix Sampled by
Solid/Sludge InYoung Seo
Results Date Analyzed
2.69 % 01/07/2022
1041 MPN/g 01/05/2022
Matrix Sampled by
Solid/Sludge InYoung Seo
Results Date Analyzed
2.70 % 01/07/2022
519 MPN/g 01/05/2022
Matrix Sampled by
Solid/Sludge InYoung Seo
Results Date Analyzed
Total Solids (%) SM 2540 B 2.72 % 01/07/2022
Fecal Density SM 9221C E-2014 1287 MPN/g 01/05/2022
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:��
Report # 2022-00308 Page 4 of 4

Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Client:_ rGlrCh I")e-S IG`UtnJ5 Date: Report Number: _ 2022- 5)0
Receipt of sample: ECHEM Pickup Client Delivery El
UPS ❑ FedEx ❑ Other ❑
❑ YES
❑ NO
N/A
1. Were custody seals present on the cooler?
❑ YES
10 NO
JW N/A
12. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt Z °C Corrected temperature upon receipt °C
How temperature taken: ❑ Temperature Blank ff Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
❑ YES
❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
IV YES
❑ NO
5. Were sample ID's listed on the COC?
YES
❑ NO
6. Were samples ID's listed on sample containers?
YES
❑ NO
7. Were collection date and time listed on the COC?
YES
❑ NO
8. Were tests to be performed listed on the COC?
YES
❑ NO
9. Did samples arrive in proper containers for each test?
YES
❑ NO
10. Did samples arrive in good condition for each test?
YES
YES
❑ NO
11. Was adequate sample volume availableT
12. Were samples received within proper holding time for requested tests?
❑ NO
❑ YES
❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L?
❑ YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
❑ NO 118.
Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2S01 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new samp!e or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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Town of Wallace
Wallace Wastewater Treatment Plant
NPDES Permit # NCO020702
Apr-22
Environmental Chemists, Inc.
dab #
xlate Aia::t :e
Probable Number
per grate
Log
1
4/04/22
58,033
4.764
2
4/04/22
41,510
4.618
3
4/04/22
30,860
4.489
4
4/04/22
31,103
4.493
5
4/04/22
33,055
4.519
6
4/04/22
50,782
4.706
7
4/04/22
362,205
5.559
Total 331.48. :
Average 4.735
Most Probable Number / Gram 5477 Fecal Coliform
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

77 Environmental Chemists, Inc.
envirochem 6602 Windmill V%laY, Wilmington, NC 28405 • 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, rManteo, NC 27954 • 252.473.5702 Lab/Fax
�4 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info a environnientetrhemists.com
Branch Residuals/Bob Branch
Date of Report: Apr 27, 2022
1735 Heckle Blvd Suite 103-291
Customer PO #:
Rock Hill SC 29732
Customer ID: 15060009
Attention:
Report #: 2022-05935
Project ID: Sludge -Wallace WWTP
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-14373 Site: Sludge 1
4/4/2022 7:25 AM Solid/Sludge Sean Pistorino
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
2.49 % 04/05/2022
Fecal Density
SM 9221C E-2014
58033 MPN/g 04/04/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-14374 Site: Sludge 2
4/4/2022 7:25 AM Solid/Sludge Sean Pistorino
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 a
2.65 % 04/05/2022
Fecal Density
SM 9221C E-2014
41510 MPN/g 04/04/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-14375 Site: Sludge 3
4/4/2022 7:25 AM Solid/Sludge Sean Pistorino
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
2.56 % 04/05/2022
Fecal Density
SM 9221C E-2014
30860 MPN/g 04/04/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-14376 Site: Sludge 4
4/4/2022 7:25 AM Solid/Sludge Sean Pistorino
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
2.54 %
04/05/2022
Fecal Density
SM 9221C E-2014
31103 MPN/g
04/04/2022
Lab ID Sample ID:
Collect DatelTime
Matrix Sampled by
22-14377 Site: Sludge 5
4/4/2022 7:25 AM
Solid/Sludge Sean Pistorino
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
2.39 %
04/05/2022
Fecal Density
SM 9221C E-2014
33055 MPN/g
04/04/2022
Report # 2022-05935 Page 2 of 3

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Branch Residuals/Bob Branch
1735 Heckle Blvd Suite 103-291
Rock Hill SC 29732
Attention:
Environmental Chemists, Inc.
6602 Wiiidmill t4Vay, Wilmington, NC 28405 • 910.392.0213 Lab • 910.392.4424 Fax
710 Bowsertown Road, Mantoo, NC 27954 - 252.473.5702 Lab/Fax
255 A Wilniiilgton lligh%A.,ay, Jacksonville, NC 28540 • 910.347.5843 Lab /Fax
info a environmert3lchemists.com
Date of Report: Apr 27, 2022
Customer PO #:
Customer ID: 15060009
Report #: 2022-05935
Project ID: Sludge -Wallace WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-14378 Site: Sludge 6 4/4/2022 7:25 AM Solid/Sludge Sean Pistorino
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.56 % 04/05/2022
Fecal Density SM 9221C E-2014 50782 MPN/g 04/04/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-14379 Site: Sludge 7 4/4/2022 7:25 AM Solid/Sludge Sean Pistorino
Test
Total Solids (%)
Fecal Density
Method
SM 2540 B
SM 9221C E-2014
Results Date Analyzed
2.54 % 04/05/2022
362205 MPN/g 04/04/2022
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
Report 4: 2022-05935 Page 3 of 3

Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client: &44CI4 Q '` IblLkAt.S Date: Report Number: c a 6Z 9
Receipt of sample: ECHEM Pickup ❑ Client Delivery UPS ❑ FedEx ❑ Other ❑
❑ YES ❑ NO NJ N/A 11. Were custody seals present on the cooler?
❑ YES
❑ NO
11,7 N/A 12.
If custody seals were present, were they intact/unbroken?
Original temperature upon receipt "C Corrected temperature upon receipt 'C
How temperature taken: ❑ Temperature Blank ❑ Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
❑ YES
k ] YES
J�7 YES
❑ NO
❑ NO
❑ NO
3. If temperature of cooler exceeded 6'C, was Project Mgr./QA notified?
4. Were proper custody procedures (relinquished/received) followed?
5. Were sample ID's listed on the COC?
YES
❑ NO
6. Were samples ID's listed on sample containers?
YES
❑ NO
7. Were collection date and time listed on the COC?
YES
❑ NO
8. Were tests to be performed listed on the COC?
YES
❑ NO
9. Did samples arrive in proper containers for each test?
YES
❑ NO
10 Did samples arrive in good condition for each test?
YES
❑ NO
11. Was adequate sample volume available?'
Ck YES
❑ NO.
12. Were samples received within proper holding time for requested tests?
❑ YES
❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14 -Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑ YES
❑ YES
❑ NO
❑ NO
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L?
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO, HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. OA.002 RPv 1

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Town of Wallace
Wallace Wastewater Treatment Plant
NPDES Permit # NCO020702
Jul-22
Environmental Chemists, Inc.
Lob #
Date Analyzed
Most Probable Number
per grave . .
Log
.. .............. .
1
7/12/22
124
2.093
?
7/12/22
81
1.908
3
7/12/22
171
2.233
4
7/12/22
72
1.857
S
7112i22
76
1.881
6
7/12/22
80
1.903
7
7/12/22
82
1.914
Total 13.790
Averagel 1 S70
Most Probable Number 1 Gram 93 Fecal Coliform
Fetal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

poop"". 7 Environmental Chemists, Inc.
envirochem6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
" 255-A Wilmington Highway, iacksom ille, NC 28540 • 91.0.347.5543 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info a environnientalcnemists.coin
Branch Residuals/Bob Branch
Date of Report: Aug 05, 2022
1735 Heckle Blvd Suite 103-291
Customer PO #:
Rock Hill SC 29732
Customer ID: 15060009
Attention: Bob Branch
Report #: 2022-13026
Project ID: Wallace WWTP
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-31651 Site: Sludge 1
7/12/2022 10:15 AM Solid/Sludge Sean Pistorino
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
2.64 % 07/14/2022
Fecal Density
SM 9221C E-2014
124 MPN/g 07/12/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-31652 Site: Sludge 2
7/12/2022 10:15 AM Solid/Sludge Sean Pistorino
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
2.49 % 07/14/2022
Fecal Density
SM 9221C E-2014
81 MPN/g 07/12/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-31653 Site: Sludge 3
7/12/2022 10:15 AM Solid/Sludge Sean Pistorino
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
2.64 % 07/14/2022
Fecal Density
SM 9221C E-2014
171 MPN/g 07/12/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-31656 Site: Sludge 4
7/12/2022 10:15 AM Solid/Sludge Sean Pistorino
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
2.51 % 07/14/2022
Fecal Density
SM 9221C E-2014
<72 MPN/g 07/12/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-31657 Site: Sludge 5
7/12/2022 10:15 AM Solid/Sludge Sean Pistonno
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
2.37 % 07/14/2022
Fecal Density
SM 9221C E-2014 <76 MPN/g 07/12/2022
Report # 2022-13026 Page 2 or 3

Environmental Chemists, Inc.
envirochem6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Tacksom•ille, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info a eavironmentalchemists.com
Branch Residuals/Bob Branch Date of Report: Aug 05, 2022
1735 Heckle Blvd Suite 103-291 Customer PO #:
Rock Hill SC 29732 Customer ID: 15060009
Attention: Bob Branch Report #: 2022-13026
Project ID: Wallace WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-31658 Site: Sludge 6 7/12/2022 10:15 AM Solid/Sludge Sean Pistorino
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.52 % 07/14/2022
Fecal Density SM 9221C E-2014 80 MPN/g 07/12/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-31659 Site: Sludge 7 7/12/2022 10:15 AM Solid/Sludge Sean Pistorino
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.46 % 07/14/2022
Fecal Density SM 9221C E-2014 82 MPN/g 07/12/2022
Comment: Sludge residuals, except pH, reported on a dry we'ght basis. pH reported on an as received basis.
Reviewed by:
Report #:: 2022-13026 Page 3 of 3

Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client: Date: ci, Report Number: oZ a -- oZ (o
Receipt of sample: ECHEM Pickup [ Client Delivery ❑
UPS ❑ FedEx ❑ Other ❑
❑ YES
10 NO
N/A
1. Were custody seals present on the cooler?
❑ YES
111 NO
I CK N/A
12. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt_ 21, - °C Corrected temperature upon receipt_. eC
How temperature taken: ❑ - Temperature Blank Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
❑ YES
❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
I YES
❑ NO
5. Were sample ID's listed on the COC?
YES
❑ NO
6. Were samples ID's listed on sample containers? ^�
YES
❑ NO
7. Were collection date and time listed on the COC? _
YES
❑ NO
8. Were tests to he performed listed on the COC?
9. Did samples arrive in proper containers for each test?
YES
❑ NO
g YES
YtS
Eq YES J11
❑ NO 110.
LJ NO 111.
Did samples arrive in goo_ d condition for each test?
Was adequate samp v -lume availableT
12. Were samples received within proper holding time for requested tests?
NO
❑ YES
❑ NO
❑ -NO
❑ NO
_
13. Were acid preserved samples received at a pH of <2? * — —
14. lilere cyanid=� s�lrnpl?s received at a pH >12?
15. Were sulfide ; received at a pH >9? --- --- --
❑ YES
❑ YES
❑ YES
❑ NO
----)
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L?
❑ YES
❑ NO
17. Were SulfidelC_yanide received at a chlorine residual of <0.5 m/L?
❑ YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes?—`—
" )_ I r ?'at, -aj ,, pit zh-• 1-:1 at turii, of an.i •y , - and rE Cur' -fed n ; tF 6?n h,F r� i
*' Bacteria samp es are checrwd for Ch orin,? at time of arial s;s ard re_crded o- the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace).
Sample(s) _ _ v;ere received incorrectly preserved and were adjusted a_cordingly
by adding (circle one): H2SO, HNO3 HCl NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
dote. -N,) PI customer service °mrred,ate y for ircorre_tly preieNed samples Obta n a ne.,. samo a Cr -^
notify the state lab if d!rected to a-ia.yzed ey the ct.s`.o^ler WhO W3: notlf ed date a ld tmie: _
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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Wallace Regional Wastewater Treatment Plant
NCO003450 Lab Cert #5352
VAR :option 6
Basin ID SHT#1 date time
pH initial, S.0 5.9 9/21/2022 9:00 AM
pH after addition of lime, S 12.3 9/21/2022 11:30 AM
pH after 2 hours,S.0 12.1 9/21/2022 1:30 PM
pH after 24 hours,S.U. 12.2 9/22/2022 11:45 AM
*** Post analysis QC pH 10 did not meet requirement of ±0.1 S.U.
QC pH 10 read 10.18 S.U.
All pH values have had the correction factor applied for temperature.
report reviewed by: Aq ZZ 2�
Lisa Cottle , Lab supervisor

Town of Wallace
Wallace Wastewater Treatment Plant
NPDES Permit # NCO020702
Dec-22
Environmental Chemists, Inc.
Lab #
Date Analyzed
Most Probobk Number
per grate
Log
1
12/16/22
215,977
5.334
2
12/16/22
171,429
5.234
3
12/16/22
288,402
5.460
4
12/16/22
171,429
5.234
5
12/16/22
107,034
5.030
6
12/16/22
116,280
5.066
7
12/16/22
77,171
4.887
Total 36.245
Averagel 5.178
Most Probable Number 1 Gram 15;p,614 Fecal Coliformlgram
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

re7nirochem
6
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ' 910.392.4124 Fax
710 Bowsertown Road, IvIanteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
info a environmentalchemists.com
Branch Residuals/Bob Branch Date of Report: Dec 16, 2022
1735 Heckle Blvd Suite 103-291 Customer PO #:
Rock Hill SC 29732 Customer ID: 15060009
Attention: Report #: 2022-22651
Project ID: Wallace WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-55616 Site: WWTP 11/14/2022 8:40 AM Solid/Sludge Sean Pistorino
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 3.38 % 11/15/2022
Fecal Density SM 9221C E-2014 215977 MPN/g 11/14/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-55617 Site: WWTP 11/14/2022 8:40 AM Solid/Sludge Sean Pistorino
Test Method Results Date Analyzed
Total Solids (%)
SM 2540 8
3.15 % 11/15/2022
Fecal Density
SM 9221C E-2014
171429 MPN/g 11/14/2022
Lab ID Sample ID:
Collect DatelTime
Matrix Sampled by
22-55618 Site: WWTP
11/14/2022 8:40 AM
Solid/Sludge Sean Pistorino
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
3.19 % 11/15/2022
Fecal Density
SM 9221C E-2014
288402 MPN/g 11/14/2022
Lab ID Sample ID:
Collect DatefTime
Matrix Sampled by
22-55619 Site: WWTP
11/14/2022 8:40 AM
Solid/Sludge Sean Pistorino
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
3.15 % 11/15/2022
Fecal Density
SM 9221C E-2014
171429 MPN/g 11/14/2022
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
22-55620 Site: WWTP
11/14/2022 8:40 AM
Solid/Sludge Sean Pistorino
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
3.27 % 11 /15/2022
Fecal Density
SM 9221C E-2014
107034MPN/g 11/14/2022
Report k. 2022-22651 Page 2 of 3

ge:nv7icle-hem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
info a emvironmentalchemists.com
Branch Residuals/Bob Branch
Date of Report:
Dec 16, 2022
1735 Heckle Blvd Suite 103-291
Customer PO #:
Rock Hill SC 29732
Customer ID:
15060009
Attention:
Report #:
2022-22651
Project ID: Wallace WWTP
Lab ID Sample ID:
Collect DatelTime Matrix
Sampled by
22-55621 Site: VW rP
11/14/2022 8:40 AM Solid/Sludge
Sean Pistorino
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
22-55622 Site: WWTP
Test
Total Solids (%)
Fecal Density
Method
Results Date Analyzed
SM 2540 B 3.01 % 11/15/2022
SM 9221C E-2014 116280 MPN/g 11/14/2022
Collect DatelTime Matrix Sampled by
11/14/2022 8:40 AM Solid/Sludge Sean Pistorino
Method
SM 2540 B
SM 9221C E-2014
Results Date Analyzed
3.11 % 11/15/2022
77171 MPN/g 11/14/2022
Comment. Sludge reuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
Report 9 . 2022-22551 Page 3 of 3

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client: ��-i ��1 � date: [.J-(l- R _ Report Number: _ 2022- �—
�Recei t of sample:
❑ YE5 ❑ f40
ECHEM Pickup ❑ Client Delivery ❑ UP5 ❑ Fe_dF>• ❑ Other ❑
f,I/A i. Were custody seals present on the cooler?
❑ YES ❑ NO
( N/A
12. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt °C
How temperature taken:
_
❑ Temperature Blank M Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor `C: 0.0 _ ____—
YES
❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
60 YES
❑ NO
5. Were sample ID's listed on the COC?
ba YES
❑ NO
6. Were samples ID's listed on sample containers?
YES
❑ NO
7_ Were collection date and time listed on the COC? _
8_ Were tests to be performed listed on the COC?
_9. Did samples arrive in proper containers for each test? _
1.0. Did samples arrive in good condition for each test? _
11__:s ad::quate sample volume available?' '^
12. ;,•. _r� samples received within proper holding time fur requ_ � , t
13. bJere acid preserved samples received at a phi of <2?
14. VVerre cyanide samples received at a pH >12?
15. Sulfide samples received at a pH .9?
1E_ '-1r: r. f.N /T1;P�/Phenol received at a chlorine re5idu ! of • 0.', ;W
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5_m/L?
U YES
❑ NO
U YES
❑ NO
YES
❑ NO—
YES
Lk YES
❑ NO
❑ NO
Cl YES
❑ NO _
❑ YES
❑ NO
❑ YES
❑ YES
❑ NO
El N0
❑ YES 10
_
NO
❑ YES
❑ NO
I Were orthophosphate samples filtered in the field within 15 minutes?
* T0C/Vo'ati1r--s are p'i rho- erj at tirre of ar alysi, and recorded on the benchsheet
Bacteria sarnp.o� dr.• ci r c: --.J for t.trurn e at time of analy;i-, anA recorded on th- Lin, h h. t
Sample Preservation:
Sample(s) —_ — _—`
by adding (circle one):
Time of preservation:
(Must be completed for any sample(s) incorrectly preserved or with headspace)
— were received incorrectly preserved and were adjusted accordingly
H2SO, HNOj NCI NaOH
_ _ If more than one preservative is needed, notate in comments belo i
tibte; Not if castamer ==r•: � . —
y ce i ripe j alai; � r P-,rrect:y preser.ed sa * p es. obta n a rev; sa�p:e c r
notify the state lab if d!.: tad to ara! _ed bi the : st me . V,"io was notified, date and tirne:
Volatiles Sample(s)
^_ were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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SOIL ANALYSIS REPORTS

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Location . Grower Farm Field Area Centroid
Dixie Chemical - Beulaville Triple S Farms Triple S Farm Field 1 32.85 acres 34.908716,-78.012548
Sample 2023-01-06 Soil Waters
Date: Lab: NC
Dixie Chemical - Beulaville 01/12/23 07:40 AM
E F C • S Y S T E M Sy 1060 S. NC 41 & 111 Hwy Beulaville, NC 28518 1/1
910-298-3660

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ED-
Location Grower Farm Field Area Centroid
Dixie Chemical - Beulaville Triple S Farms Triple S Farm Field 2 9.06 acres 34.912564,-78.013934
Sample 2023-01-06 Soil Waters
Date: Lab: NC
Dixie Chemical - Beulaville 01/12/23 07:42 AM
F F C •SYSTEMS • 1060 S. NC 41 & 111 Hwy Beulaville, NC 28518 1 /1
910-298-3660

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Dixie Chemical - Beulaville Triple S Farms Triple S Farm Field 3A 14.85 acres 34.911282,-78.015917
Sample 2023-01-06 Soil Waters
Date: Lab: NC
Dixie Chemical - Beulaville 01/12/23 07:43 AM
E F C - S Y S T E M S- 1060 S. NC 41 & 111 Hwy Beulaville, NC 28518 1/1
910-298-3660

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Dixie Chemical - Beulaville Triple S Farms Triple S Farm Field 3B 7.5 acres 34.912407,-78.017559
Sample 2023-01-06 Soil Waters
Date: Lab: NC
Dixie Chemical - Beulaville 01/12/23 07:44 AM
E F C •SYSTEMS • 1060 S. NC 41 & 111 Hwy Beulaville, NC 28518 1 /1
910-298-3660

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Dixie Chemical - Beulaville Triple S Farms Triple S Farm Field 4 5.49 acres 34.913876,-78.019044
Sample 2023-01-06
Date:
Soil Waters
Lab: NC
Dixie Chemical - Beulaville 01 /12/23 07:45 AM
E F C- S Y S T E M S 1060 S. NC 41 & 111 Hwy Beulaville, NC 28518 1 /1
910-298-3660

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Dixie Chemical - Beulaville Triple S Farms Triple S Farm Field 5 13.56 acres 34.91382,-78.016318
Sample 2023-01-06 Soil Waters
Date: Lab: NC
Dixie Chemical - Beulaville 01/12/23 07:46 AM
E F C • S Y S T E M S" 1060 S. NC 41 & 111 Hwy Beulaville, NC 28518 1/1
910-298-3660

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Dixie Chemical - Beulaville
Grower Farm Field Area Centroid
Triple S Farms Triple S Farm new ground 18.07 acres 34.910881,-78.010984
Sample 2023-01-06 Soil Waters
Date: Lab: NC
Dixie Chemical - Beulaville 01 /12/23 07:52 AM
F F C • S Y 5 T E M S • 1060 S. NC 41 & 111 Hwy Beulaville, NC 28518 1 /1
910-298-3660

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Dixie Chemical - Beulaville Triple S Farms Triple S Farm Field 7 20.11 acres 34.906665,-78.013163
Sample 2023-01-06 Soil Waters
Date: Lab: NC
Dixie Chemical - Beulaville 01/12/23 07:49 AM
E F C • S Y S T E M Sy 1060 S. NC 41 & 111 Hwy Beulaville, NC 28518 1/1
910-298-3660

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Location Grower Farm Field Area Centroid
Dixie Chemical - Beulaville Triple S Farms Triple S Farm field 6 18.29 acres 34.904896,-78.010947
Sample 2023-01-06 Soil Waters
Date: Lab: NC
Dixie Chemical - Beulaville 01/12/23 07:47 AM
F F G - S Y S T E M S' 1060 S. NC 41 & 111 Hwy Beulaville, NC 28518 1/1
910-298-3660

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Location Grower Farm Field Area Centroid
Dixie Chemical - Beulaville Triple S Farms Triple S Farm field 8 14.74 acres 34.905695,-78.007975
Sample 2023-01-06 Soil Waters
Date: Lab: NC
Dixie Chemical - Beulaville 01/12/23 07:50 AM
E F C •SYSTEMS • 1060 S. NC 41 & 111 Hwy Beulaville, NC 28518 1 /1
910-298-3660

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2022 APPLICATION SUMMARY TABLE

TRIPLE S FARMS
LAND APPLICATION PROGRAM
PERMIT NO. WQ0030998
2022 APPLICATION SUMMARY
Farmer
'Tract
/Site
......
Fidd::
.......................................
...........
;cYi"s :::Sp�iread:::::
:::Date ::::::::::::::::
lions *
D Tons
r3'
/ Acre
...... ..
... .. ..
................ . . ...
Cxop
....
------- -- ----- -- -- -
Source
PAN
(lbsfac) :
Eric Smith
1
1
36
Oct-22
66,000
0.08
Ryegrass
Kenansville WWTP
171.73
Jan-22
305,700
0.67
Ryegrass
Clayton Little Creek WRF
Feb-22
102,000
0.32
Ryegrass
Wallace WWTP
Apr-22
71,000
0.20
Bermudagrass
Beulaville WWTP
276,000
0.81
Bermudagrass
Wallace WWTP
Apr-22
18,020
0.03
Bermudagrass
Clayton Little Creek WRF
Jun-22
132,000
0.25
Bermudagrass
Clayton Little Creek WRF
Aug-22
180,110
0.51
Bermudagrass
Clayton Little Creek WRF
Sep-22
240,000
0.70
Bermudagrass
Wallace WWTP
Oct-22
48,000
0.18
Bermudagrass
Wallace WWTP
Dec-22
107,980
0.24
Ryegrass
Clayton Little Creek WRF
2
12.6
Jun-22
38,000
0.06
Bermudagrass
Maysville WWTP
284.01
Jan-22
60,000
0.37
Ryegrass
Clayton Little Creek WRF
Apr-22
186,010
1.01
Bermudagrass
Clayton Little Creek WRF
Jul-22
12,000
0.07
Bermudagrass
Southwest Plantation
Jul-22
88,000
0.73
Bermudagrass
Beulaville WWTP
Aug-22
155,990
1.26
Bermudagrass
Clayton Little Creek WRF
Sep-22
168,000
1.40
Bermudagrass
Wallace WWTP
Oct-22
12,000
0.08
Bermudagrass
Clayton Little Creek WRF
Nov-22
95,990
0.61
Ryegrass
Clayton Little Creek WRF
6
17.3
Oct-22
150,000
0.76
Wheat
Warsaw WWTP
87.88
Nov-22
300,498
1.41
Wheat
Swansboro WWTP
Dec-22
102,030
0.47
Wheat
Clayton Little Creek WRF
7
11.5
Jan-22
108,000
0.74
Ryegrass
Clayton Little Creek WRF
169.30
Apr-22
126,000
1.16
Bermudagrass
Wallace WWTP
Apr-22
12,000
0.07
Bermudagrass
Southwest Plantation
May-22
263,250
1.56
Bermudagrass
Clayton Little Creek WRF
9
16.1
Mar-22
161,970
0.79
Bermudagrass
Clayton Little Creek WRF
260.11
Mar-22
234,000
1.64
Bermudagrass
Wallace WWTP
May-22
269
4.81
Bermudagrass
Rose Hill WWTP
Jun-22
160,000
0.87
Bermudagrass
Warsaw WWTP
Sep-22
84,000
0.55
Bermudagrass
Wallace WWTP
10
12.8
Mar-22
36,000
0.06
Fescue
Maysville WWTP
119.28
Nov-22
42,000
0.34
Fescue
Beulaville WWTP
Mar-22
330,050
2.03
Fescue
Clayton Little Creek WRF
Mar-22
18,000
0.03
Fescue
Bridgeton WWTP
Apr-22
12,000
0.10
Fescue
Beulaville WWTP
345
19.6
Nov-22
36,000
0.04
Fescue
Maysville WWTP
137.44
Feb-22
150,000
0.87
Fescue
Wallace WWTP
Feb-22
106,000
0.47
Fescue
Warsaw WWTP
Feb-22
54,000
0.22
Fescue
Clayton Little Creek WRF
Feb-22
96,000
0.39
Fescue
Clayton Little Creek WRF
Jun-22
19,000
0.02
Fescue
Bridgeton WWTP
Nov-22
414,110
1.70
Fescue
Clayton Little Creek WRF
Nov-22
40,000
0.21
Fescue
Beulaville WWTP
3A
14
Jan-22
126,000
0.71
Ryegrass
Clayton Little Creek WRF
163.61
Feb-22
42,000
0.26
Ryegrass
Warsaw WWTP
May-22
150,000
0.73
Bermudagrass
Clayton Little Creek WRF
Aug-22
191,890
1.39
Bermudagrass
Clayton Little Creek WRF
Aug-22
19,000
0.02
Bermudagrass
Bridgeton WWTP
Sep-22
66,000
0.50
Bermudagrass
Wallace WWTP
Dec-22
18,000
0.02
Ryegrass
Bridgeton WWTP
139.9
Total
Town of Beulaville
Town of Clayton Little Creek WRF
Town of Kenansville
Town of Rose Hill
Southwest Plantation
Town of Wallace
Town of Warsaw
Town of Bridgeton
Town of Maysville
Onwasa Swansboro WWTP
6,030,598.00
572.34
NA
253,000.00
26.27
30
39251,100.00
261.23
300
665000.00
2.92
10
268.57
77.42
38
249000.00
1.72
5
194947000.00
162.67
330
4589000.00
40.11
75
749000.00
1.36
5
110,000.00
2.20
15
3009498.00
24.31
110
Total Wet Tons
268.57
77.42
Total Gallons
61030,598
522.79
Total Dry Tons
600.21
Branch Residuals Soils, LLC Confidential 2/10/2023 Page 1

2022 APPLICATION CONDITION SUMMARIES

Town of Bridgeton
Havelock, North Carolina
Triple S Farms and Cleaning, Inc.
WQ0030998
Annual 2022
Bridgeton WWTP
Stabilization Method Lime
Farmer: Eric Smith
Acres: 12.8
Site/Tract: 1
Application Method: Surface
Field: 10
Percent Solids: 0.44
Residual Report No.: BEI-440A
Crop: Fescue
.................
...................................................................... ............... I ...... .
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/29/22
10
18,000.0
Dry
Cool,Clear
0.00
Totat:alldns
18,000_:0

Town of Bridgeton
Havelock, North Carolina
Triple S Farms and Cleaning, Inc.
WQ0030998
Annual 2022
Bridgeton WWTP
Stabilization Method Lime
Farmer: Eric Smith
Acres: 19.6
Site/Tract: 1
Application Method: Surface
Field: 345
Percent Solids: 0.44
Residual Report No.: BEI-440A
Crop: Fescue
.......................................................
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/11/22
345
19,000.0
Dry
warm,Clear
0.00
Total Gallons
19;00:0;0

Town of Bridgeton
Havelock, North Carolina
Triple S Farms and Cleaning, Inc.
WQ0030998
Annual 2022
Bridgeton WWTP
Stabilization Method Lime
Farmer: Eric Smith
Acres: 14
Site/Tract: 1
Application Method: Surface
Field: 3A
Percent Solids: 0.44
Residual Report No.: BEI-440A
Crop: Bermudagrass
....................... .......
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
8/29/22
3A
19,000.0
Dry
Hot,Ciear
0.00
Tot 1 Gallons
�—i
19-1000.0

Town of Bridgeton
Havelock, North Carolina
Triple S Farms and Cleaning, Inc.
WQ0030998
Annual 2022
Bridgeton WWTP
Stabilization Method Lime
Farmer: Eric Smith
Acres: 14
Site/Tract: 1
Application Method: Surface
Field: 3A
Percent Solids: 0.44
Residual Report No.: BEI-440A
Crop: Ryegrass
..................................
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
12/31/22
3A
18,000.0
Dry
warm,Clear
0.00
Total Gallons
-48;000.0

Town of Beulaville
Beulaville, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2022
Beulaville WWTP
Farmer: Eric Smith
Acres: 36
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 2.49
Residual Report No.: BL 2022-11566
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
4/4/22
1
71,000.0
Dry
warm,Clear
0.00
Total Gallons
71,000.0

Town of Beulaville
Beulaville, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2022
Beulaville WWTP
Farmer: Eric Smith Acres: 12.6
Site/Tract: 1 Application Method: Surface
Field: 2 Percent Solids: 2.49
Residual Report No.: BL 2022-11566 Crop: Bermudagrass
........... ...............
............
..................... ...... ............. ....... ......
................
Soil Weather Prev. 24 Hour
Date Field No. Subfield Gallons
Conditions Conditions Rainfall
7/29/22 2 88,000.0 Dry Hot,Clear 0.00
fid:G

Town of Beulaville
Beulaville, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2022
Beulaville WWTP
Farmer: Eric Smith
Acres: 19.6
Site/Tract: 1
Application Method: Surface
Field: 345
Percent Solids: 2.49
Residual Report No.: BL 2022-11566
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/10/22
345
40,000.0
Dry
Cool,Clear
0.00
T6ta1 GaU+�ns
40,000.0

Town of Beulaville
Beulaville, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2022
Beulaville WWTP
Farmer: Eric Smith
Acres: 12.8
Site/Tract: I
Application Method: Surface
Field: 10
Percent Solids: 2.49
Residual Report No.: BL 2022-11566
Crop: Fescue
....
..........
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
4/4/22
10
12,000.0
Dry
Warm,Clear
0.00
Total Gallons
11. 1.0.00.0

Town of Beulaville
Beulaville, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2022
Beulaville WWTP
Farmer: Eric Smith
Acres: 12.8
Site/Tract: 1
Application Method: Surface
Field: 10
Percent Solids: 2.49
Residual Report No.: BL 2022-11566
Crop: Fescue
......... ............................. ................ . ... ...... .
................. ..
................. ... ... ..
................
.................
................
.................
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/9/22
10
42,000.0
Dry
Cool,Clear
0.00
Total Gallons
42,.000.0

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
1st Quarter
Clayton Little Creek WRIT
Farmer: Eric Smith
Acres: 36.00
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 1.89
Residual Report No.: C 1 22-054-0012
Crop: Ryegrass
.... ...........
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
1/14/22
1
36,000.0
Dry
Cool,Clear
0.00
1/20/22
1
42,000.0
Dry
Cool,Clear
0.00
1/26/22
1
47,700.0
Dry
Cool,Clear
0.00
1/27/22
1
30,000.0
Dry
Cool,Clear
0.00
1/28/22
1
36,000.0
Dry
Cool,Clear
0.00
1/31/22
1
54,000.0
Dry
Cool,Clear
0.00
2/1/22
1
60,000.0
Dry
Cool,Clear
0.00
::Tofal:Gallons
305,700,0

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
1st Quarter
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 12.80
Site/Tract: 1
Application Method: Surface
Field: 10
Percent Solids: 1.89
Residual Report No.: C1 22-054-0012
Crop: Fescue
...... ....... ... .. .... .......... ..
....... .................. .... ... ........... ..
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/4/22
10
18,000.0
Dry
Wann,Clear
0.00
3/7/22
10
18,000.0
Dry
Wann,Clear
0.00
3/8/22
10
36,000.0
Dry
Cool,Clear
0.00
3/9/22
10
30,000.0
Dry
Warm,Cloudy
0.43
3/10/22
10
36,000.0
Moist
Cool,cloudy
0.26
3/14/22
10
36,000.0
Moist
Wann,Clear
0.00
3/28/22
10
36,000.0
Dry
Cool,Clear
0.00
3/29/22
10
30,000.0
Dry
Cool,Clear
0.00
3/30/22
10
48,050.0
Dry
Cool,Clear
0.00
3/31 /22
10
42,000.0
Dry
Wann.Clear
0.00
Total Gallons
330,050,0

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
1st Quarter
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 12.60
Site/Tract: 1
Application Method: Surface
Field: 2
Percent Solids: 1.89
Residual Report No.: C1 22-054-0012
Crop: Ryegrass
............ . ................
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
1/5/22
2
36,000.0
Dry
Cool,Cloudy
0.05
1/6/22
2
24,000.0
Dry
Cool,Cloudy
0.01
Total Gallons
60,000.6

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
1st Quarter
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 11.50
Site/Tract: I
Application Method: Surface
Field: 7
Percent Solids: 1.89
Residual Report No.: C 1 22-054-0012 1
Crop: Ryegrass
Date
Field No.
Su6field
Gallons
Conditions
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
117122
7
36,000.0
Dry
COOLCIcu
0.00
1 /10/22
7
48,000.0
Dry
Cool.Cloudy
0.49
1/ 11 /22
7
24,000.0
Moist
Cnol,Ciear
0.00
Total Gallons
108,000.0

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
1st Quarter
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 19.60
Site/Tract: 1
Application Method: Injected
Field: 345
Percent Solids: 1.89
Residual Report No.: Cl 22-054-0012
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
2/28/22
345
42,000.0
Dry
Coo►,Cloudy
0.29
3/1/22
345
54,000.0
Moist
Cool,Clear
0.00
Total Gallons
96100.0.0

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
1st Quarter
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 19.60
Site/Tract: 1
Application Method: Surface
Field: 345
Percent Solids: 1.89
Residual Report No.: C1 22-054-0012
Crop: Fescue
.... ... .. ..... .
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
2/16/22
345
18,000.0
Dry
Cool,Clear
0.00
2/21/22
345
6,000.0
Dry
Cool,Clear
0.00
2/22/22
345
12,000.0
Dry
Wann,Clear
0.00
2/23/22
345
18,000.0
Dry
Wann,Clear
0.00
Total Gallons
54,000.0

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
1st Quarter
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 14.00
Site/Tract: 1
Application Method: Surface
Field: 3A
Percent Solids: 1.89
Residual Report No.: C1 22-054-0012
Crop: Ryegrass
... ............
.............
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
1/12/22
3A
60,000.0
Dry
Cool,Clear
0.00
1/13/22
3A
66,000.0
Dry
Cool,Clear
0.00
Total Gallons
126,000.0

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
1st Quarter
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 16.10
Site/Tract: 1
Application Method: Surface
Field: 9
Percent Solids: 1.89
Residual Report No.: C1 22-054-0012
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/ 15/22
9
53,970.0
Dry
Cool,Clear
0.00
3/21/22
9
42,000.0
Dry
Cool,Clear
0.00
3/22/22
9
24,000.0
Dry
Cool,Clear
0.00
3/23/22
9
42,000.0
Dry
warm,Clear
0.00
Total Gallons
161,970.0

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
2nd Quarter
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 36.00
Site/Tract: 1
Application Method: Injected
Field: 1
Percent Solids: 1.64
Residual Report No.: C2 22-179-0002
Crop: Bermudagrass
...............
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
4/13/22
1
18,020.0
Dry
warm,Clear
0.00
Total Gallons
181020.0

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
2nd Quarter
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 36.00
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 1.64
Residual Report No.: C2 22-179-0002
Crop: Bermudagrass
....................... ..
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/14/22
1
60,000.0
Dry
Hot,Cloudy
0.14
6/15/22
1
66,000.0
Dry
Hoc,Clear
0.00
6/16/22
1
6,000.0
Dry
Hoc,Clear
0.00
Total Gallons
1321000.0

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
2nd Quarter
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 12.60
Site/Tract: 1
Application Method: Injected
Field: 2
Percent Solids: 1.64
Residual Report No.: C2 22-179-0002
Crop: Bermudagrass
............................ .
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
4/27/22
2
18,000.0
Dry
warm,Cloudy
0.14
4/28/22
2
18,000.0
Dry
warm,Clear
0.00
4/29/22
2
24,010.0
Dry
warm,Clear
0.00
5/2/22
2
66,000.0
Dry
warm,Cloudy
0.15
5/3/22
2
60,000.0
Dry
warm,Clear
0.00
Total Gallons
186,010.0

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
2nd Quarter
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 11.50
Site/Tract: 1
Application Method: Surface
Field: 7
Percent Solids: 1.64
Residual Report No.: C2 22-179-0002
Crop: Bertnudagrass
.. . ........
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
5/25/22
7
36,080.0
Moist
Wartn,Clear
0.00
5/26/22
7
35,100.0
Dry
Warm,Clear
0.00
5/27/22
7
12,000.0
Dry
Warm,C►ear
0.00
6/1/22
7
18,040.0
Dry
Hot,Clear
0.00
6/6/22
7
54,040.0
Dry
Wann,Clear
0.00
6/7/22
7
60,000.0
Dry
Wann,Clear
0.00
6/8/22
7
36,000.0
Dry
Hot,Clear
0.00
6/13/22
7
11,990.0
Moist
Hot,Clear
0.00
Total Gallons
263,250.0

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
2nd Quarter
Clayton Little Creek WRY
Farmer: Eric Smith
Acres: 14.00
Site/Tract: 1
Application Method: Injected
Field: 3A
Percent Solids: 1.64
Residual Report No.: C2 22-179-0002
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
5/4/22
3A
54,000.0
Dry
Warm,Cloudy
0.46
5/5/22
3A
60,000.0
Moist
Warm,Cloudy
0.23
5/6/22
3A
36,000.0
Moist
Wann,Clear
0.00
Total Gallons
150,000.0

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
3rd Quarter
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 36.00
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 2.44
Residual Report No.: C3 22-271-0003
Crop: Bermudagrass
.............. . ........ . ............ ..
... . . ..... . ..
. .............
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
8/29/22
1
36,000.0
Dry
Hot,Clear
0.00
8/30/22
1
36,010.0
Dry
wann,Clear
0.00
8/31/22
1
36,030.0
Dry
warm,Clear
0.00
9/1/22
1
24,000.0
Dry
Hot,Clear
0.00
9/6/22
1
12,060.0
Dry
wann,Cloudy
0.02
9/7/22
1
24,010.0
Dry
Hot,Clear
0.00
9/8/22
1
12,000.0
Dry
warm,Cloudy
0.17
Total Gallons
180,1104

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
3rd Quarter
Clayton Little Creek WRIT
Farmer: Eric Smith
Acres: 12.60
Site/Tract: 1
Application Method: Surface
Field: 2
Percent Solids: 2.44
Residual Report No.: 0 22-271-0003
Crop: Bermudagrass
.....
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
8/9/22
2
24,000.0
Dry
Hot,Clear
0.00
8/ 10/22
2
66,000.0
Dry
Hot,Clear
0.00
8/ 11 /22
2
65,990.0
Dry
Hot,Clear
0.00
Total Gallons
155,990.0

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
3rd Quarter
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 14.00
Site/Tract: 1
Application Method: Surface
Field: 3A
Percent Solids: 2.44
Residual Report No.: C3 22-271-0003
Crop: Bermudagrass
... . ..... ........
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
8/12/22
3A
42,000.0
Dry
Hot,Clear
0.00
8/15/22
3A
60,090.0
Dry
Warm,Cloudy
0.02
8/18/22
3A
11,970.0
Dry
Wann,Clear
0.00
8/22/22
3A
36,000.0
Dry
Wann,Cloudy
0.43
8/23/22
3A
11,820.0
Moist
Wann,Cloudy
0.02
8/25/22
3A
18,000.0
Dry
Wann,Clear
0.00
8/26/22
3A
12,010.0
Dry
Wann,Cloudy
0.36
Total Gallons
191,890.0

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
4th Quarter
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 36.00
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 1.93
Residual Report No.: C4 22-312-0001
Crop: Ryegrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
12/12/22
1
36,000.0
Dry
Cool,Clear
0.00
12/13/22
1
35,990.0
Dry
Cool,Clear
0.00
12/14/22
1
35,990.0
Dry
Cool,Clear
0.00
Total Gallons
107,980.0

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
4th Quarter
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 12.60
Site/Tract: 1
Application Method: Surface
Field: 2
Percent Solids: 1.93
Residual Report No.: C4 22-312-0001
Crop: Bermudagrass
......
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10'6:'22
2
12,000.0
Dry
warm,Clear
0.00
Total Gallons
12100.0.0

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
4th Quarter
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 12.60
Site/Tract: 1
Application Method: Surface
Field: 2
Percent Solids: 1.93
Residual Report No.: C4 22-312-0001
Crop: Ryegrass
..... ...... .... .. .. ....... . .... .. .. .
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/29/22
2
35,990.0
Dry
Cool,Cloudy
0.12
11/30/22
2
36,000.0
Dry
Cool,Cloudy
0.44
12/1/22
2
12,000.0
Moist
Cool,Cloudy
0.08
12/2/22
2
12,000.0
Dry
Cool,Clear
0.00
Total Gallons
95,990.0

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
4th Quarter
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 19.60
Site/Tract: 1
Application Method: Surface
Field: 345
Percent Solids: 1.93
Residual Report No.: C4 22-312-0001
Crop: Fescue
.............
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/7/22
345
29,960.0
Dry
Wann,Clear
0.00
11/8/22
345
36,010.0
Dry
Wann,Clcar
0.00
11/9/22
345
30,000.0
Dry
Cool,Clear
0.00
11/10/22
345
29,990.0
Dry
Cool,Clear
0.00
11/14/22
345
59,990.0
Dry
Cool,Clear
0.00
11/15/22
345
36,020.0
Dry
Cool,Clear
0.00
11/16/22
345
30,010.0
Dry
Cool,Clear
0.00
11/18/22
345
24,000.0
Dry
Cool,Clear
0.00
11 /21 /22
345
48,110.0
Dry
Cool,Clear
0.00
11/22/22
345
54,000.0
Dry
Cool,Clcar
0.00
11/28/22
345
36,020.0
Dry
Warm,Cloudy
0.05
Total Gallons
414,110.0

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
4th Quarter
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 17.30
Site/Tract: 1
Application Method: Surface
Field: 6
Percent Solids: 1.93
Residual Report No.: C4 22-312-0001
Crop: Wheat
............
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
12/5/22
6
36,000.0
Dry
Cool,Clear
0.00
12/6/22
6
36,000.0
Dry
Cool,Clear
0.00
12/7/22
6
30,030.0
Dry
Cool,Cloudy
0.01
Total Gallons
;: `102,030.0

Town of Kenansville
Kenansville, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2022
Kenansville WWTP
Farmer: Eric Smith
Acres: 36
Site/Tract: I
Application Method: Surface
Field: I
Percent Solids: 1.06
Residual Report No.: KV 2022-12575
Crop: Ryegrass
......................
.....................
......................
- ----- ......................
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10/21/22
1
48,000.0
Dry
Cool,Clear
0.00
10/24/22
1
18,000.0
Dry
Warm,Clear
0.00
Total Gallons
661,000.0

Town of Maysville
Maysville, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2022
Maysville WWTP
Farmer: Eric Smith
Acres: 12.6
Site/Tract: 1
Application Method: Surface
Field: 2
Percent Solids: 0.48
Residual Report No.: MV 2022-10200
Crop: Bermudagrass
Date
FieldNo.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/29/22
2
18,000.0
Dry
Warm,Cloudy
0.02
6/30/22
2
20,000.0
Dry
Warm,Cloudy
0.08
Total Gallons
38,000.0

Town of Maysville
Maysville, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2022
Maysville WWTP
Farmer: Eric Smith
Acres: 12.8
Site/Tract: I
Application Method: Surface
Field: 10
Percent Solids: 0.48
Residual Report No.: MV 2022-10200
Crop: Fescue
...........
......................... ............. .. ................... ......... ......
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/28/22
10
12,000.0
Dry
Cool,Clear
0.00
3/29/22
10
24,000.0
Dry
Cool,Clear
0.00
...............
............
.

Town of Maysville
Maysville, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2022
Maysville WWTP
Farmer: Eric Smith
Acres: 19.6
Site/Tract: 1
Application Method: Surface
Field: 345
Percent Solids: 0.48
Residual Report No.: MV 2022-10200
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/18/22
345
36,000.0
Dry
Cool,Clear
0.00
Total Gallons4
36,000.0

Town of Rose Hill
Rose Hill, North Carolina
Triple S Farms & Cleaning, Inc
WQ00030998
Annual 2022
Rose Hill WWTP
Farmer: Eric Smith
Acres: 16.1
Site/Tract: I
Application Method: Incorporated
Field: 9
Percent Solids: 28.83
Residual Report No.: RH-2022-07795
Crop: Bermudagrass
...................... . ..............
Date
Field No.
Subfield
Wet Tons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
5/10/22
9
143
Dry
Cool,Clear
0.00
5/11/22
9
125
Dry
Warm,Clear
0.00
Total. Gallons
':: 269

Swansboro WWTP
Swansboro, NC
Triple S Farms
WQ0030998
Annual 2022
Swansboro WWTP
Stabilization Method None
Farmer: Eric Smith
Acres: 17.3
Site/Tract: I
Application Method: Injected
Field: 6
Percent Solids: 1.94
Residual Report No.: SWB E2022-17562
Crop: Wheat
............ .............
............
..............................
..... ......... ..........................
................. I ..............
Date
Field No.
fi
Subeld
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/28/22
6
30,498.0
Dry
Wann,Cloudy
0.05
11/29/22
6
36,000.0
Dry
Cool,Cloudy
0.12
12/2/22
6
30,000.0
Dry
Cool,Clear
0.00
12/5/22
6
36,000.0
Dry
Cool,Clear
0.00
12/6/22
6
54,000.0
Dry
Cool,Clear
0.00
12/7/22
6
54,000.0
Dry
Cool,Cloudy
0.01
12/8/22
6
60,000.0
Dry
Wann,Cioudy
0.18
Otal:c ........
............
- 9180

Triple S Farms
Jacksonville, North Carolina
Triple S Farms
WQ00030998
Annual 2022
Southwest Plantation
Farmer: Eric Smith
Acres: 11.5
Site/Tract: 1
Application Method: Surface
Field: 7
Percent Solids: 1.72
Residual Report No.: SWP 2022 3-22
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
4/15/22
7
12,000.0
Dry
warm,Clear
0.00
Total Gallons
12;000:0

Triple S Farms
Jacksonville, North Carolina
Triple S Farms
WQ00030998
Annual 2022
Southwest Plantation
Farmer: Eric Smith
Acres: 12.6
Site/Tract: 1
Application Method: Surface
Field: 2
Percent Solids: 1.72
Residual Report No.: SWP 2022 3-22
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
7/1/22
2
12,000.0
Dry
Warm,Clear
0.00
Total Gallons
12,000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ00030998
1st Quarter 2022
Wallace WWTP
Stabilization Method None
Farmer: Eric Smith
Acres: 36.00
Site/Tract: 1
Application Method: Injected
Field: 1
Percent Solids: 2.71
Residual Report No.: WL 1-2022-00308
Crop: Ryegrass
..... ....... .
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
2/14/22
1
24,000.0
Dry
Cool,Clear
0.00
3/22/22
1
60,000.0
Dry
Cool,Clear
0.00
3/23/22
1
18,000.0
Dry
wann,Clear
0.00
Total Gallons-
102,00-0.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ00030998
1st Quarter 2022
Wallace WWTP
Stabilization Method None
Farmer: Eric Smith
Acres: 19.60
Site/Tract: I
Application Method: Incorporated
Field: 345
Percent Solids: 2.71
Residual Report No.: WL 1-2022-00308
Crop: Fescue
...... ..... . ...... ........ ...................
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
2/2/22
345
42,000.0
Dry
Cool,Clear
0.00
2/3/22
345
36,000.0
Dry
Cool,Clear
0.00
2/7/22
345
36,000.0
Dry
Cool,Cloud)
0.04
2/17/22
345
36,000.0
Dry
Cool,Clear
0.00
. ... .. . .....

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ00030998
1st Quarter 2022
Wallace WWTP
Stabilization Method None
Farmer: Eric Smith
Acres: 16.10
Site/Tract: 1
Application Method: Injected
Field: 9
Percent Solids: 2.71
Residual Report No.: WL 1-2022-00308
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 2411our
Rainfall
3/16/22
9
78,000.0
Dry
warm,Clcar
0.00
3/17/22
9
36,000.0
Dry
wann,Cloudy
0.45
3/18/22
9
54,000.0
Moist
Warm,Clear
0.00
3/21 /22
9
66,000.0
Dry
Cooi.Clear
0.00
Total Gallons
234,000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ00030998
2nd Quarter 2022
Wallace WWTP
Stabilization Method None
Farmer: Eric Smith
Acres: 36.00
Site/Tract: 1
Application Method: Injection
Field: 1
Percent Solids: 2.53
Residual Report No.: WL 2-2022-05935
Crop: Bennudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
4/4/22
1
42,000.0
Dry
Wann,Clear
0.00
4/5/22
1
96,000.0
Dry
Cool,Clear
0.00
4/6/22
1
18,000.0
Dry
Wann,Cloudy
0.38
4/11/22
1
42,000.0
Dry
Cool,Clear
0.00
4/12/22
1
36,000.0
Dry
Wann,Clear
0.00
4/13/22
1
24,000.0
Dry
Wann,Clear
0.00
4/14/22
1
18,000.0
Dry
Wann,Clear
0.00
Total Gallons
276,000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ00030998
2nd Quarter 2022
Wallace WWTP
Stabilization Method None
Farmer: Eric Smith
Acres: 11.50
Site/Tract: 1
Application Method: Injection
Field: 7
Percent Solids: 2.53
Residual Report No.: WL 2-2022-05935
Crop: Bennudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
4/14/22
7
54,000.0
Dry
wann,C►ear
0.00
4/20/22
7
42,000.0
Moist
Cool,Clear
0.00
4/21/22
7
30,000.0
Dry
Wann,Clear
0.00
.... ................

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ00030998
3rd Quarter 2022
Wallace WWTP
Stabilization Method Lime
Farmer: Eric Smith
Acres: 36.00
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 2.52
Residual Report No.: WL 3-2022-13026
Crop: Bennudagrass
........... ..
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/26/22
1
72,000.0
Dry
Wann,Clear
0.00
9/27/22
1
78,000.0
Dry
Wann,Clear
0.00
9/28/22
1
90,000.0
Dry
Wann,Clear
0.00
Total Gallons
1 240,000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ00030998
3rd Quarter 2022
Wallace WWTP
Stabilization Method None
Farmer: Eric Smith
Acres: 12.60
Site/Tract: 1
Application Method: Injection
Field: 2
Percent Solids: 2.52
Residual Report No.: WL 3-2022-13026
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/19/22
2
30,000.0
Dry
warm,Clear
0.00
9/20/22
2
72,000.0
Dry
wann,Clear
0.00
9/21/22
2
66,000.0
Dry
warm,Clear
0.00
Total Gallons
1 168,000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ00030998
3rd Quarter 2022
Wallace WWTP
Stabilization Method None
Farmer: Eric Smith
Acres: 16.10
Site/Tract: 1
Application Method: Injection
Field: 9
Percent Solids: 2.52
Residual Report No.: WL 3-2022-13026
Crop: Bermudagrass
.............
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/22/22
9
84.000.0
Dry
Hot,Clear
0.00
Total Gallons
84,000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ00030998
3rd Quarter 2022
Wallace WWTP
Stabilization Method None
Farmer: Eric Smith
Acres: 14.00
Site/Tract: 1
Application Method: Injection
Field: 3A
Percent Solids: 2.52
Residual Report No.: WL 3-2022-13026
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/23/22
3A
42,000.0
Dry
Hot,Clear
0.00
9/26/22
3A
24,000.0
Dry
wann,Clear
0.00
Total Gallons
66,00.0.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ00030998
4th Quarter 2022
Wallace WWTP
Stabilization Method Lime
Farmer: Eric Smith
Acres: 36.00
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 3.31
Residual Report No.: WL 4-2022-22651
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10/3/22
1
30,000.0
Dry
Cool,Clear
0.00
10/4/22
1
18,000.0
Dry
Cool,Clear
0.00
Total Gallons
48,000.0

Town of Warsaw
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2022
Warsaw WWTP
Farmer: Eric Smith
Acres: 14
Site/Tract: 1
Application Method: Surface
Field: 3A
Percent Solids: 2.10
Residual Report No.: WS 2022-11184
Crop: Ryegrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
2/14/22
3A
42,000.0
Dry
Cool,Clear
0.00
Total Gallons
42,000.0

Town of Warsaw
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2022
Warsaw WWTP
Farmer: Eric Smith
Acres: 19.6
Site/Tract: 1
Application Method: Surface
Field: 345
Percent Solids: 2.10
Residual Report No.: WS 2022-11184
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
2/15/22
345
80,000.0
Dry
Cool,Clear
0.00
2/16/22
345
26,000.0
Dry
Cool,Clear
0.00
Total Gallons
: 06.1000.0

Town of Warsaw
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2022
Warsaw WWTP
Farmer: Eric Smith
Acres: 16.1
Site/Tract: I
Application Method: Surface
Field: 9
Percent Solids: 2.10
Residual Report No.: WS 2022-11184
Crop: Bermudagrass
............ ..... .....
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/20/22
9
60,000.0
Dry
Warm,Clear
0.00
6/21/22
9
60,000.0
Dry
Warm,Clear
0.00
6/22/22
9
40,000.0
Dry
Warm,Clear
0.00
Total Gallons
1160,00.0.0

Town of Warsaw
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2022
Warsaw WWTP
Farmer: Eric Smith
Acres: 17.3
Site/Tract: 1
Application Method: Surface
Field: 6
Percent Solids: 2.10
Residual Report No.: WS 2022-11184
Crop: Wheat
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10/26/22
6
12,000.0
Dry
Warm,Clear
0.00
10/27/22
6
120,000.0
Dry
Warm,Clear
0.00
10/31/22
6
18,000.0
Dry
Cool,Clear
0.00
Total -Gallons
150;000.0