WQ0002883_2022 Residual Annual Report_20230227 (2)

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * WQ0002883
Applicant/Permittee City of Elizabeth City
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Washington
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Stephen Cummings
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
2524897317
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0002883
Has Current Existing permit number
Applicant/Permittee Address*
410 Pritchard Street, Elizabeth City, NC 27909
Facility Name*
City of Elizabeth City Class B Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Annaul Report ECity.pdf 7.08MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/27/2023

City of Elizabeth City
2022 ANNUAL LAND APPLICATION OF RESIDUAL BIOSOLIDS REPORT
CLASS B PROGRAM
WQ0002883
Submitted by:
Atlantic OBX, INC.
PO Box 2560
Kitty Hawk, NC, 27949
2/27/23

noAir
- ; 0
;0
AO
P.O. Box 2560
KITTY HAWK, NC 27949
[phone]
S TEPHENkATLANUC SE WAGE. COM
2/27/23
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Re: 2022 LAND APPLICATION ANNUAL REPORT
Elizabeth City "Class B Program"
NC Permit No.: WQ0002883
Information Processing Unit:
Atlantic OBX, Inc. is submitting all monitoring and reporting requirements as specified in the above
referenced permit for the City of Elizabeth City. Atlantic OBX has compiled this report using data gathered
during the compliance year. This data includes (1) the annual certification Form, (2) residual sampling. (3)
field loading calculations, (4) pathogen and vector attraction reduction documentation, & (5) soil fertility
nutrient analysis.
The City of Elizabeth City conducted application events on permitted fields in Pasquotank County during
2022. A total of 564.79 dry tons or 3,374,000 gallons of permitted residual biosolids were generated by the
City of Elizabeth City's WWTP in 2022. A total of 340.087 dry tons or 1,624,000 gallons from the City's
WWTP were land applied to permitted fields in WQ0002883. An additional 224.70 dry tons or 1,750,000
gallons were land applied under Atlantic OBX's Class B permit WQ0000974.
A total of 1,073.86 dry tons or 3,241,000 gallons of permitted residual biosolids were generated from the City
of Elizabeth City's WTP in 2022. A total of 564.986 dry tons or 1,652,000 gallons from the City's WTP were
land applied as a Class B product to permitted fields in WQ0002883. An additional 508.88 dry tons or
1,589,000 gallons of WTP residuals were distributed as a Class A product under permit WQ0040622.
Soil Samples for permitted fields WB 1-106 were sampled by WB Bateman & Sons. A reference page has
been implemented in the soil sample section of this report along with associated maps for those samples.
If there is any further information required or questions regarding this annual report, please do not hesitate to
contact me or Elizabeth City (252-337-6626) for further assistance.
Regards,
Stephen Cummings, Atlantic OBX, Inc.
Montre Freeman, City of Elizabeth City

City of Elizabeth City 2022 Land Application of Residual
Biosolids Report
WQ0002883
Elizabeth City, NC
INDEX
Annual Certification Form
• Source Summary
• Field Loading Summary
Residual Sampling Summary Forms
• Elizabeth City WWTP
• Elizabeth City WTP
Field Summary Forms
Pathogen & Vector Reduction Forms
• Elizabeth City WWTP
Soil Samples

City of Elizabeth City
2022 Class B Annual Report
WQ0002883
Annual Certification Form
Source Summary
Field Loading Summary

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0002883 County: Pasquotank Year: 2022
Facility Name (as shown on permit):
Land Application Operator:
City of Elizabeth City
Atlantic OBX Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
d Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in the permit:
162
Total number of fields utilized for land application during the year:
17
Total amount of dry tons applied during the year for all application sites:
905.073
Total number of acres utilizes for land application during the year:
241.84
Part B - Annual Comr fiance Statement:
Facility was compliant during calendar year 2!0')? with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. E Yes ❑ No
If no please, provide a ✓r itten description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was perfonned in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits -in 15A NCAC 02T .1 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T. I 1 I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
1 1) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations." ' /
i
an p— Aug--- ZIU2 2
Permittee Name and Title (type or print) Si ature of Permittee Date
2/23/23 2/23/23
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in - O CFR Part 503.9 (r) and 15A NCAC 02T. 1102 (26)
DENR FORM ACF (12/2006)

E7
Source Summary Report
WWTPI Volume Applied I Measurement I Total Dry Tons
Elizabeth City WWTP 1,624,000 Gallons 340.087
Elizabeth City WTP 1,652,000 Gallons 564.986
Total 3,276,000 905.073

2022 Field Loading Summary
Crops Used and Volume Applied
Permitted Crops and Loading Rates
Crop 1 Crop 2
Acres
Volume
PAN Pan
Total P
Crop 1
% PAN 1
Crop 2
% PAN 2
Field
Used
Applied
Total DT
Ibs/Ac. Ibs/Ac.
Ibs/Ac.
Crop 1 Name
PAN
Used
Crop 2 Name
PAN
Used
26
6.92
119,000
31.972
40.712
63.407
Corn (Grain)
169
24.1%
Site # WB
27
8.88
161,000
39.876
41.122
63.229
Corn (Grain)
169
24.3%
28
9.60
266,000
63.433
97.010
148.495
Corn (Grain)
169
57.4%
Wheat, Grain
50
0.0%
29
10.53
238,000
58.508
62.333 10.498
121.214
Corn (Grain)
169
36.9%
Wheat, Grain
50
21.0%
30
11.34
168,000
45.046
61.713
96.019
Soybeans - Full Season
177
34.9%
31
11.79
210,000
53.873
78.970
122.215
Soybeans - Full Season
177
44.6%
82
11.53
168,000
57.577
2.173
6.008
Soybeans - Full Season
174
1.2%
83
11.59
161,000
48.922
2.309
4.918
Soybeans - Full Season
174
1.3%
84
11.47
133,000
38.399
2.005
3.841
Soybeans - Full Season
174
1.2%
30
15.7
182,000
54.480
39.817
62.687
Corn (Grain)
117
34.0%
Site # LL
31
18.55
196,000
57.423
37.863
59.423
Corn (Grain)
117
32.4%
32
12.79
224,000
43.619
53.141
84.218
Corn (Grain)
117
45.4%
33
22.37
238,000
71.466
21.198
0.027
32.640
Corn (Grain)
147
14.4%
Wheat, Grain
50
0.1%
34
19.88
238,000
73.080
36.901
0.031
57.118
Corn (Grain)
147
25.1%
Wheat, Grain
50
0.1%
35
20.26
259,000
92.229
27.044
0.029
43.369
Corn (Grain)
147
18.4%
Wheat, Grain
50
0.1%
36
20.31
189,000
44.953
38.021
0.006
58.304
Corn (Grain)
147
25.9%
Wheat, Grain
50
0.0%
37
18.33
126,000
30.217
27.383
0.005
42.002
Corn (Grain)
147
18.6%
Wheat, Grain
50
0.0%
Total 3,276,000 905.073

City of Elizabeth City
2022 Class B Annual Report
WQ0002883
Residual Summary Form
Elizabeth City WWTP
Elizabeth City WTP
Field Loading Calculations
2022 Analytical & TCLP

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
WQ Permit No. WQ0002883 Facility Name City of Elizabeth City Source Permit No. NC0025011 Source Name Elizabeth City W WTP
Laboratory 1
Laboratory 2
Sample or Composite Date
Parameter (mg/Kg) Class A Class B
Environmental
Chemists, Inc.
Environmental
Chemists, Inc.
Environmental
Chemists, Inc.
Environmental
Chemists, Inc.
3/30/2022
6/8/2022
8/3/2022
11/9/2022
Aluminum
N/A
N/A
12,600
11,300
4,220
9,420
Ammonia
N/A
N/A
1,150
8,120
9,050
4,270
Arsenic
41
75
9•32
13.10
25.10
24.00
Cadmium
39
85
9•32
13.10
25.10
12.00
Calcium
N/A
N/A
125,000
137,000
133,000
165,000
Copper
1,500
4,300
156
206
84
273
Lead
Magnesium
300
840
9.32
13.10
25.10
15.80
N/A
N/A
4,920
5,420
3,840
5,760
Mercury
17
57
0.36
0.347
0.91
0.446
Molybdenum
N/A
75
9•32
13.10
42.60
12.00
Nickel
420
420
9•32
13.10
25.10
13.20
Nitrate -Nitrite
Nitrogen
N/A
N/A
26.10
8.10
17.30
35.50
Percent Solids
N/A
N/A
5.02
5.04
1.84
3.99
pH (no units)
N/A
N/A
11.18
11.19
11.03
12.01
Phosphorus
N/A
N/A
13,800
20,100
9,880
28,600
Potassium
N/A
N/A
4,560
6,330
13,700
5,410
PAN (Inj./Inc.)
N/A
N/A
13,701
17,182
20,092
13,975
PAN (Surface)
N/A
N/A
13,126
13,122
15,567
11,840
Selenium
100
100
3.46
13.10
25.10
12.00
Sodium
N/A
N/A
1,480
1,970
5,520
3,180
SAR
N/A
N/A
0.25
0.32
0.55
0.42
TKN
N/A
N/A
42,900
38,300
45,800
36500
Zinc
2,800
7,500
709
1 871
1 370
1 1,060
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2/21/23
Sig- of p.p- * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

Facility
Sampling Date
% Solids
Mineralization Rate
Gallons Per DT
pH
Elizabeth City WW IP
3/30/2022
5.02
0.3
4777.05
11.18
Field Loading Estimate
SAR 0.25 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
SAR Calculation
Value From source Meq/L
Na 1480 3.23026087
Ca 125,000 313.75
Mg 4920 20.582
I Nitrogen Application Nutrient Application
TKN (mg/Kg)
Ammonia Nitrogen (mg/Kg)
Nitrate -Nitrite (mg/Kg)
42900
lbs./1000 gal
17.935
1150
lbs./1000 gal
0.481
26.1
lbs./1000 gal
0.011
Plant Available Nitrogen Surface Applied
PAN (mg/Kg) 13126.1 (lbs./1000 gal) 5.488
Plant Available Nitrogen Injected/Incorporated Applied
PAN (mg/Kg) 13701.1 (lbs./1000 gal) 5.728
Volatilization Rate= .5 Surface Application
1.0 Injection/ Incorporation
EPA Metal Limits
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
Arsenic
Cadmium
Copper
Lead
Mercury
Nickel
Selenium
Zinc
Metal Concentration
9.32
9.32
156
9.32
0.355
9.32
9.32
709
Residual Nitrogen Calculation
Potassium
Phosphorus
Calcium
Magnesium
Molybdenum
Chromium
(mg/Kg)
4660
13800
125,000
4920
9.32
13.7
Metal
Arsenic
Cadmium
Copper
Lead
Mercury
Nickel
Selenium
Zinc
(lbs./1000 gal)
1.9482
5.7692
52.2576
2.0569
0.0039
0.0057
Jbs./1000
0.0039
0.0039
0.0652
0.0039
0.0001
0.0039
0.0039
0.2964
TKN
Surface (S)
PAN (S)
lbs/DT
Organic N
TKN
Subsurface
(INJ)
(INJ)
Organic N
1st Year
42900
13126
26.25
29774
42900
13701
27.40
29199
2nd Year
29774
4466
8.93
25308
29199
4380
8.76
24819
3rd Year
25308
1898
3.80
23410
24819
1861
3.72
22958
4th Year
23410
878
1.76
22532
22958
861
1.72
22097
5th Year
22532
422
0.84
22109
22097
414
0.83
21682
Total
20791
41.58
Total
21218
42.44
Equations
1st Yr. PAN (mg/Kg)-(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)- 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)- 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)- 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)- 5th Yr. TKN x (MR/16)

Environmental Chemists,
Inc.
6602 Windmill Way,
Wilmington, NC 28405 ' 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown
Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
sM7
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
[e-mail]
Atlantic OBX
Date of Report: May 02, 2022
PO Box 2560
Customer PO #:
Kitty Hawk NC 27949
Customer ID: 18120006
Attention:
Report #: 2022-05793
Project ID: Elizabeth City WWTP
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-14040 Site: Sludge
3/30/2022
11:30 AM Solid/Sludge Client
Test
Method
Results Date Analyzed
Chlordane (TCLP)
SW-846 8081 B
<0.02 mg/L
04/15/2022
Endrin (TCLP)
SW-846 8081 B
<0.0005 mg/L
04/15/2022
Heptachlor (TCLP)
SW-846 8081 B
<0.0005 mg/L
04/15/2022
Heptachlor epoxide (TCLP)
SW-846 8081 B
<0.0005 mg/L
04/15/2022
Lindane (TCLP)
SW-846 8081 B
<0.0005 mg/L
04/15/2022
Methoxychlor (TCLP)
SW-846 8081 B
<0.0005 mg/L
04/15/2022
Toxaphene (TCLP)
SW-846 8081 B
<0.05 mg/L
04/15/2022
2,4,5-TP (TCLP)
SW-846 8151 A
<0.003 mg/L
04/18/2022
2,4-D (TCLP)
SW-846 8151 A
<0.003 mg/L
04/18/2022
1,4-Dichlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
04/14/2022
2,4,5-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
04/14/2022
2,4,6-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
04/14/2022
2,4-Dinitrotoluene (TCLP)
SW-846 8270 E
<0.050 mg/L
04/14/2022
Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
04/14/2022
Hexachloro-1,3-butadiene (TCLP)
SW-846 8270 E
<0.050 mg/L
04/14/2022
Hexachlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
04/14/2022
Hexachloroethane (TCLP)
SW-846 8270 E
<0.050 mg/L
04/14/2022
m + p-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
04/14/2022
Nitrobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
04/14/2022
o-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
04/14/2022
Pentachlorophenol (TCLP)
SW-846 8270 E
<0.250 mg/L
04/14/2022
Pyridine (TCLP)
SW-846 8270 E
<0.050 mg/L
04/14/2022
1, 1 -Dichloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/07/2022
1,2-Dichloroethane (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/07/2022
Benzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/07/2022
Carbon Tetrachloride (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/07/2022
Report #:: 2022-05793
Page 1 of 3

jenvirochie]m
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
[e-mail]
Atlantic OBX
Date of Report: May 02, 2022
PO Box 2560
Customer PO #:
Kitty Hawk NC
27949
Customer ID: 18120006
Attention:
Report #: 2022-05793
Project ID: Elizabeth City WWTP
Chlorobenzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/07/2022
Chloroform (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/07/2022
Methyl ethyl ketone (TCLP)
SW-846 Method 8260D
<0.05 mg/L
04/07/2022
Tetrachloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/07/2022
Trichloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/07/2022
Vinyl Chloride (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/07/2022
:1«]I
Cyanide
SM 4500 CN D-2016
<1.0 mg/kg
04/05/2022
Sulfide
SM 4500 S D
0.27 mg/kg
04/11/2022
Ignitability
SW 846 method 1010
>156 OF
04/12/2022
pH
SW 846 Method 9045D
11.18 units
04/12/2022
Result estimated. Analyzed out
of 15 minutes hold time.
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4,1994
12600 mg/kg
04/14/2022
Arsenic
EPA 200.7, Rev. 4.4,1994
<9.32 mg/kg
04/14/2022
Cadmium
EPA 200.7, Rev. 4.4,1994
<9.32 mg/kg
04/14/2022
Calcium
EPA 200.7, Rev. 4.4,1994
125000 mg/kg
04/14/2022
Chromium
EPA 200.7, Rev. 4.4,1994
13.7 mg/kg
04/14/2022
Copper
EPA 200.7, Rev. 4.4,1994
156 mg/kg
04/14/2022
Lead
EPA 200.7, Rev. 4.4,1994
<9.32 mg/kg
04/14/2022
Magnesium
EPA 200.7, Rev. 4.4,1994
4920 mg/kg
04/14/2022
Molybdenum
EPA 200.7, Rev. 4.4,1994
<9.32 mg/kg
04/14/2022
Nickel
EPA 200.7, Rev. 4.4,1994
<9.32 mg/kg
04/14/2022
Potassium
EPA 200.7, Rev. 4.4,1994
4660 mg/kg
04/14/2022
Selenium
EPA 200.7, Rev. 4.4,1994
<9.32 mg/kg
04/14/2022
Sodium
EPA 200.7, Rev. 4.4,1994
1480 mg/kg
04/14/2022
Zinc
EPA 200.7, Rev. 4.4,1994
709 mg/kg
04/14/2022
Nitrate+Nitrite-Nitrogen
EPA353.2
26.1 mg/kg
04/01/2022
Total Solids (%)
SM 2540 B
5.02 %
04/01/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
1150 mg/kg
04/01/2022
Report #:: 2022-05793
Page 2 of 3

-- —1 �"7
Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Atlantic OBX
Date of Report: May 02, 2022
PO Box 2560
Customer PO #:
Kitty Hawk NC 27949
Customer ID: 18120006
Attention:
Report #: 2022-05793
Project ID: Elizabeth City WWTP
Total Kjeldahl Nitrogen (TKN) SM 4500 Norg B-2011
42900 mg/kg 04/01/2022
Total Phosphorus SM 4500 P (F-H)-2011
13800 mg/kg 04/06/2022
Mercury SW-e467471 B
<0.355mg/kg 04/04/2022
TCLP Metals
Arsenic
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
04/27/2022
Barium
EPA 200.7, Rev. 4.4,1994
<1 mg/L
04/20/2022
Cadmium
EPA 200.7, Rev. 4.4,1994
<1 mg/L
04/20/2022
Chromium
EPA 200.7, Rev. 4.4,1994
<1 mg/L
04/20/2022
Lead
EPA 200.7, Rev. 4.4,1994
<1 mg/L
04/20/2022
Selenium
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
04/27/2022
Silver
EPA 200.7, Rev. 4.4,1994
<1 mg/L
04/20/2022
Mercury
EPA 245.1
<0.0002 mg/L
04/22/2022
Comment:
Sludge residuals reported o dry weight basis.
Reviewed by:
Report #:: 2022-05793 Page 3 of 3

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client: ��nh O(�jx Date: ( 2-Z Report Number: _ 2022- t)-4-q3
Receipt of sample: ECHEM Pickup ❑ Client Delivery ❑ UPS FeclEx ❑ Other ❑
❑ YES]EDZI
N/A 1. Were custody seals present on the cooler?
❑ YESN/A2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt °C
How temperature taken: ❑ Temperature Blank N 'Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
YES ❑ NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed?
YES
I
❑
NO
5. Were sample ID's listed on the COC?
YES
❑
NO
6. Were samples ID's listed on sample containers?
YES
❑
NO
7. Were collection date and time listed on the COC?
YES
❑
NO
8. Were tests to be performed listed on the COC?
YES
❑
NO
9. Did samples arrive in proper containers for each test?
YES
❑
NO
10. Did samples arrive in good condition for each test?
Fr YES
❑
NO
11. Was adequate sam le v 1 �'
YES
❑ NO
p m o ue av3 able.
12. Were samples received within proper holding time for requested tests?
❑ YES
❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
O NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet
Sample Preservation:
Sample(s)
by adding (circle one):
me of preservation:
(Must be completed for any sample(s) incorrectly preserved or with headspace)
were received incorrectly preserved and were adjusted accordingly
H2SO4 HNO3 HCI NaOH
If more than one preservative is needed, notate in commiI hoinu,
rvute: rvutny customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

M
*
ib R b
r-
n
� fD
it
M.
tzI
C�
LA13ID b
I I ] ] J.
. G
NU1V3F.R
11
Sample
Type
G1AC�'A4�AC1nC�
A4�c�G��G�
c�4�c�G�
n
Composite H
r,
or
Grab
N
Container
G) 3
r
1*
(P or
W
f
ChlOrine O
VrJ-
NONE
t�
IRCL
b 11
HaSO,
E
O
RNOs
NaO$
g
a
z
MO
OTHER
d
�
�
d
e�
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d
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N
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N
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Facility
Sampling Date
% Solids
Mineralization Rate
Gallons Per DT
pH
Elizabeth City WW IP
6/8/2022
5.04
0.3
4758.10
11.19
Field Loading Estimate
SAR 0.32 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
SAR Calculation
Value From source Meq/L
Na 1970 4.316869565
Ca 137,000 345.24
Mg 5420 22.764
I Nitrogen Application Nutrient Application
TKN (mg/Kg)
Ammonia Nitrogen (mg/Kg)
Nitrate -Nitrite (mg/Kg)
38300
lbs./1000 gal
16.076
8120
lbs./1000 gal
3.408
8.1
lbs./1000 gal
0.003
Plant Available Nitrogen Surface Applied
PAN (mg/Kg) 13122.1 (lbs./1000 gal) 5.508
Plant Available Nitrogen Injected/Incorporated Applied
PAN (mg/Kg) 17182.1 (lbs./1000 gal) 7.212
Volatilization Rate= .5 Surface Application
1.0 Injection/ Incorporation
EPA Metal Limits
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
Arsenic
Cadmium
Copper
Lead
Mercury
Nickel
Selenium
Zinc
Metal Concentration
13.1
13.1
206
13.1
0.347
13.1
13.1
871
Residual Nitrogen Calculation
Potassium
Phosphorus
Calcium
Magnesium
Molybdenum
Chromium
(mg/ Kg)
6330
20100
137,000
5420
13.1
18.7
Metal
Arsenic
Cadmium
Copper
Lead
Mercury
Nickel
Selenium
Zinc
(lbs./1000 gal)
2.6569
8.4365
57.5025
2.2749
0.0055
0.0078
Jbs./1000
0.0055
0.0055
0.0865
0.0055
0.0001
0.0055
0.0055
0.3656
TKN
Surface (S)
PAN (S)
lbs/DT
Organic N
TKN
Subsurface
(INJ)
(INJ)
Organic N
1st Year
38300
13122
26.24
25178
38300
17182
34.36
21118
2nd Year
25178
3777
7.55
21401
21118
3168
6.34
17950
3rd Year
21401
1605
3.21
19796
17950
1346
2.69
16604
4th Year
19796
742
1.48
19054
16604
623
1.25
15981
5th Year
19054
357
0.71
18697
15981
300
0.60
15682
Total
19603
39.21
Total
22618
45.24
Equations
1st Yr. PAN (mg/Kg)-(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)- 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)- 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)- 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)- 5th Yr. TKN x (MR/16)

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
s 255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Atlantic OBX Date of Report: Jun 30, 2022
PO Box 2560 Customer PO #:
Kitty Hawk NC 27949 Customer ID: 18120006
Attention: Report #: 2022-10659
Project ID: Elizabeth City WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-25826 Site: Sludge 6/8/2022 12:20 PM Solid/Sludge Stephen Cummings
Test Method Results Date Analyzed
Sludge Residuals
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
Zinc
EPA 200.7, Rev. 4.4, 1994
Nitrate+N itrite-N itrogen
EPA 353.2
Total Solids (%)
SM 2540 B
Ammonia Nitrogen
SM 4500 NH3 C-2011
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
Total Phosphorus
SM 4500 P (F-H)-2011
pH
SW 846 Method 9045D
Result estimated. Analyzed out of
15 minutes hold time.
Mercury
SW-846 7471 B
11300 mg/kg
<13.1 mg/kg
<13.1 mg/kg
137000 mg/kg
18.7 mg/kg
206 mg/kg
<13.1 mg/kg
5420 mg/kg
<13.1 mg/kg
13.1 mg/kg
6330 mg/kg
<13.1 mg/kg
1970 mg/kg
871 mg/kg
8.10 mg/kg
5.04 %
8120 mg/kg
38300 mg/kg
20100 mg/kg
11.19 units
<0.347 mg/kg
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: 0, �J'Qla2
06/20/2022
06/20/2022
06/20/2022
06/20/2022
06/20/2022
06/20/2022
06/20/2022
06/20/2022
06/20/2022
06/20/2022
06/28/2022
06/20/2022
06/20/2022
06/20/2022
06/15/2022
06/14/2022
06/13/2022
06/13/2022
06/20/2022
06/28/2022
06/17/2022
Report #:: 2022-10659 Page 1 of 1

Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client: n RQn-h c C)6X Date: ZZ Report Number: _ 2022- 1065
Receipt of sample: ECHEM Pickup ❑ Client Delivery ❑ UPS FedEx ❑ Other ❑
❑ YES ❑ NO�EOI
N/A 1. Were custody seals present on the cooler?
❑ YES ❑ NON/A 2. If custody seals were present wer th
e ey intact/unbroken?
Original temperature upon receipt `j• °C Corrected temperature upon receipt_
How temperature taken:
❑ Temperature Blank Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
YES
❑
NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
❑
NO
4. Were proper custody procedures (relinquished/received) followed?
91
YES
❑
NO
5. Were sample ID's listed on the COC?
YES
❑
NO
6. Were samples ID's listed on sample containers?
9'
YES
❑
NO
7. Were collection date and time listed on the COC?
it
YES
❑
NO
8. Were tests to be performed listed on the COC?
YES
Lj
❑
NO
10. Did samples arrive in good condition for each test?
YES
❑
NO
ll. Was adequate sample volume available?'
YES
❑
NO
12 Were ram les
p "Co VC wit in proper holding time for requested tests?
❑ YES ❑ NO 113. Were acid preserved samples received at a pH of <2?
❑ YES ❑ NO 14. Were cyanide samples received at a pH >12?
❑ YES ❑ NO 15. Were sulfide samples received at a pH >9?
❑ YES ❑ jNO
t17.
Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L?
❑ YES ❑ EWere
ulfide/Cyanide received at a chlorine residual of <0.YES ❑ rthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCl NaOH
me of preservation:
If more than one preservative is needed, notate in comments below
Vote: Notify customer seniice imm ied�ately for incorrectly preserved samples. Obtain a new sample or
loti y the state_ lab if directed to alalyzed by the customer. Who was notified, dare and t;me:
Volatiles Sample(s)
COMMENTS:
were received with headspace
'C
DOC. QA.002 Re , 1

is
n
n
t9
`L7
r�
G
n0n0
r)0n4o
0
AG7A A
Composite
or
Grab
` _
N
F�'
"A ►ry
"n }d
�1 ►d
"r1 }d
r� �i
"r] �e!
'C] ►sy
"A
►d 'A b �l
r
P
...
�t
or�G
)
f
&
C
Cblorine
mg(L
L
NONE
i
HCL
'
H3504
HNo,
NROH
O .
I
�
�
TMO
OTHEF2
a.
M
m.
9
rt
wwZ�
m
o �Nn
Ns
a W,A
O
Ul

Facility
Sampling Date
% Solids
Mineralization Rate
Gallons Per DT
pH
Elizabeth City WW IP
8/3/2022
1.84
0.3
13033.05
11.19
Field Loading Estimate
SAR 0.55 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
SAR Calculation
Value From source Meq/L
Na 5520 4.416
Ca 133,000 122.36
Mg 3840 5.888
I Nitrogen Application Nutrient Application
TKN (mg/Kg) 45800 lbs./1000 gal 7.018
Ammonia Nitrogen (mg/Kg) 9050 lbs./1000 gal 1.387
Nitrate -Nitrite (mg/Kg) 17.3 lbs./1000 gal 0.003
Plant Available Nitrogen Surface Applied
PAN (mg/Kg) 15567.3 (lbs./1000 gal) 2.385
Plant Available Nitrogen Injected/Incorporated Applied
PAN (mg/Kg) 20092.3 (lbs./1000 gal) 3.079
Volatilization Rate= .5 Surface Application
1.0 Injection/ Incorporation
EPA Metal Limits
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
Metal Concentration
Arsenic
25.1
Cadmium
25.1
Copper
84
Lead
25.1
Mercury
0.91
Nickel
25.1
Selenium
25.1
Zinc
370
Residual Nitrogen Calculation
Potassium
Phosphorus
Calcium
Magnesium
Molybdenum
Chromium
(mg/ Kg)
13700
9880
133,000
3840
42.6
25.1
Metal
Arsenic
Cadmium
Copper
Lead
Mercury
Nickel
Selenium
Zinc
(lbs./1000 gal)
2.0993
1.5139
20.3801
0.5884
0.0065
0.0038
Jbs./1000
0.0038
0.0038
0.0129
0.0038
0.0001
0.0038
0.0038
0.0567
TKN
Surface (S)
PAN (S)
lbs/DT
Organic N
TKN
Subsurface
(INJ)
(INJ)
Organic N
1st Year
45800
15567
31.13
30233
45800
20092
40.18
25708
2nd Year
30233
4535
9.07
25698
25708
3856
7.71
21852
3rd Year
25698
1927
3.85
23770
21852
1639
3.28
20213
4th Year
23770
891
1.78
22879
20213
758
1.52
19455
5th Year
22879
429
0.86
22450
19455
365
0.73
19090
Total
23350
46.70
Total
26710
53.42
Equations
1st Yr. PAN (mg/Kg)-(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)- 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)- 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)- 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)- 5th Yr. TKN x (MR/16)

SM
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 0 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
[e-mail]
Atlantic OBX Revised Report: Aug 30, 2022
PO Box 2560 Original Report Date: Aug 26, 2022
Kitty Hawk NC 27949 Report #: 2022-14875
Attention: Customer ID: 18120006
Project ID: Elizabeth City WWTP
Lab ID Sample ID:
22-36286 Site: Sludge
Test
Sludge Residuals
Aluminum
Calcium
Magnesium
Arsenic
Cadmium
Chromium
Copper
Lead
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Collect Date/Time Matrix Sampled by
8/3/2022 12:22 PM Solid/Sludge Stephen Cummings
Method Results Date Analyzed
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.8, Rev. 5.4, 1994
EPA 200.8, Rev. 5.4, 1994
EPA 200.8, Rev. 5.4, 1994
EPA 200.8, Rev. 5.4, 1994
EPA 200.8, Rev. 5.4, 1994
EPA 200.8, Rev. 5.4, 1994
EPA 200.8, Rev. 5.4, 1994
EPA 200.8, Rev. 5.4, 1994
EPA 200.8, Rev. 5.4, 1994
EPA 200.8, Rev. 5.4, 1994
EPA 200.8, Rev. 5.4, 1994
Nitrate+Nitrite-Nitrogen
EPA 353.2
Total Solids (%)
SM 2540 B
Ammonia Nitrogen
SM 4500 NH3 C-2011
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
Total Phosphorus
SM 4500 P (F-H)-2011
pH
Sw 846 Method 9045D
Result estimated. Analyzed out of
15 minutes hold time.
Mercury
Comment:
Reviewed by:
SW-846 7471 B
4220 mg/kg
133000 mg/kg
3840 mg/kg
<25.1 mg/kg
<25.1 mg/kg
<25.1 mg/kg
84.0 mg/kg
<25.1 mg/kg
42.6 mg/kg
<25.1 mg/kg
13700 mg/kg
<25.1 mg/kg
5520 mg/kg
370 mg/kg
17.3 mg/kg
1.84 %
9050 mg/kg
45800 mg/kg
9880 mg/kg
11.03 units
<0.91 mg/kg
08/23/2022
08/23/2022
08/23/2022
08/16/2022
08/16/2022
08/16/2022
08/16/2022
08/16/2022
08/16/2022
08/16/2022
08/17/2022
08/16/2022
08/17/2022
08/16/2022
08/08/2022
08/05/2022
08/08/2022
08/05/2022
08/17/2022
08/16/2022
08/16/2022
Amended 8/30/2022 to correct project id. Results, except pH, reported on a dry weight basis. pH
reported on an as received basis,
0
Report #: 2022-14875
Page 1 of 1

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
Sample Receipt Checklist 910.392.0223
Hai: rri. (� z 2Z
-- i-��
Report f%:urnber. 2022_ I
Receiptofsample: ECHEM Pickup❑
YES p NO Client DelLLa—
ivery[] �p
fJ/A 1, Were custody seals.preseiiL on the cooler? FedEx ❑ Other ❑
❑ 1`E5 ❑ NO - -
fJ/4 2. If custody seals were present, t;�e` 6 they intact/unbroken?
Original temperature upon receipt _
Hoty temperature taken- �C Corrected temperature upon receipt
IR Gun ID: Thomas Traceable S/N19251 65, tare Blank oC
Against Bottles
YES ❑ NO IP, Gun Correction Factor `C; 0.0
3. If ternpErawre of cooler exceeded 6'C, was Project M r.
YES ❑ NO 4. r�Jefe Prep=r cusrady procedures (relinquished/received/ a); QA n1oQn-o�
" YES ❑ NO
5. Vlere s:rr;;;;e ID listed on the ) G-'�d?
YES ❑ NO 6. kVe - - - COC?
YESr='- : 1'0's listed on sample containers?
'3C YES --- I '0 'r ----- - -- 2nd, time listed on the COC?
YES I❑ i-- - _____ - -=,:�' `----_, •---' r
f'o
= i =oo i f ----- --- '
4'ES ❑ C condition ror each test? _
fJ0 I .. i„ - - _ .
-- y,E� �❑ f`in Imo----:_ _ .'(T 21ai)�hlc?' — -----—
I!� YES I❑ r -- :-- -cl�':ithinprGperhol:iin� ---
f.0 I1 J r',/e,.: _ _ o time for reuucs`_
❑ YES I❑ NO - _ - _ -- e� _a nill= receives at a pH of <2? -- �
I' YES I❑ NO1.5re'cei:=_d at a p,1 >1?? _
- b', e
)=r YESI❑ NO I = at a P.'>9?
�❑ }ES If�- received z't a chlorine residua I
i40 �17. ��;`ere S_ =id=�i _: �a 1 or
❑ YES �❑ iJ0 Q �� -J , -� -_ r=sewed at a chlGrine residual o; <
I �. erE C: i^op'�0sr-- -Te r 0.5
�_�C sampres filtered in _ the field with;
53TGIe3 2-E the:k= r: n - C i t c. �= ch5hE2t.
- • '�`= =•�d record=d on the _ ,
- nc„sh
Sample Preservation: � t
St be co-nPlet_d fo
Sample!;) (r�r'Jr an,; sample(s) incorrectly Presor✓ec or ;t
h headsp==a)
.•=,C received inco-
re,u3y preen�ed and ;v2rebyaddin� (circle one): 5o,
n HC,Js:e� c=CC`"'0Hs
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- -
N'^ r` - L
COMM—EN I S:

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Sample
19
Type
Composite
A or
Grab
Container
(PorG)
Chlorine
mg/L
11
0
NONE
C/]
HCL
�r
fi V CO,
1�
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Facility
Sampling Date
% Solids
Mineralization Rate
Gallons Per DT
pH
Elizabeth City WWTP
11/9/2022
3.99
0.3
6010.23
Field Loading Estimate
SAR 0.42 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
SAR Calculation
Value From source Meq/L
Na 3180 5.516608696
Ca 165,000 329.175
Mg 5760 19.152
I Nitrogen Application Nutrient Application
TKN (mg/Kg) 36500 lbs./1000 gal 12.161
(mg/Kg)
Ammonia Nitrogen (mg/Kg) 4270 lbs./1000 gal 1.423
Potassium
5410
Nitrate -Nitrite (mg/Kg) 35.5 lbs./1000 gal 0.012
Phosphorus
28600
Calcium
165,000
Plant Available Nitrogen Surface Applied
Magnesium
5760
PAN (mg/Kg) 11839.5 (lbs./1000 gal) 3.945
Molybdenum
12.0
Chromium
22.3
Plant Available Nitrogen Injected/Incorporated Applied
PAN (mg/Kg) 13974.5 (lbs./1000 gal) 4.656
Volatilization Rate= .5 Surface Application
1.0 In ection /Incorporation
(lbs./1000 gal)
1.8024
9.5285
54.9722
EPA Metal
Limits
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
Heavy Metal Concentration (mg/Kg)
Heavy Metal Loading (lbs./1000
Arsenic
24.0
Arsenic
0.0080
41
75
39
85
Cadmium
12.0
Cadmium
0.0040
1,500
4,300
Copper
273.0
Copper
0.0910
300
840
Lead
15.8
Lead
0.0053
17
57
Mercury
0.446
Mercury
0.0001
420
420
Nickel
13.2
Nickel
0.0044
100
100
Selenium
12.0
Selenium
0.0040
2,800
7,500
Zinc
1060
Zinc
0.3532
Residual Nitrogen Calculation
1.9190
0.0040
0.0074
Remaing
PAN
Remaing
PAN (S)
Subsurface
TKN
Surface (S)
Organic N
TKN
(INJ)
Organic N
lbs/DT
(INJ)
(S)
lbs/DT
(INJ)
1 st Year
36500
11840
23.68
24661
36500
13975
27.95
22526
2nd Year
24661
3699
7.40
20961
22526
3379
6.76
19147
3rd Year
20961
1572
3.14
19389
19147
1436
2.87
17711
4th Year
19389
727
1.45
18662
17711
664
1.33
17047
5th Year
18662
350
0.70
18312
17047
320
0.64
16727
Totall
18188
36.38
1 Total
19773
39.55
Equations
1st Yr. PAN (1ng/hg)=(b1R x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)- 2nd Yr. TKN x (b7R/2)
3rd Yr PAN (mg/Kg)- 3rd Yr. TKN x (b7R/4)
4di Yr PAN (mg/Kg)- 4di Yr. TKN x (b7R/8)
5di Yr PAN (mg/Kg)- 5di Yr. TKN x (b7R/16)

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
(sMi 255-A Wilmington Highway, Jacksonville, NC 28540 e 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Atlantic OBX Revised Report: Dec 20, 2022
PO Box 2560 Original Report Date: Dec 16, 2022
Kitty Hawk NC 27949 Report #: 2022-22494
Attention: Customer ID: 18120006
Project ID: Elizabeth City WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-55150A Site: Sludge 11/9/2022 11:00 AM Solid/Sludge Stephen Cummings
Test
Method
Results
Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4,1994
9420 mg/kg
11/16/2022
Arsenic
EPA 200.7, Rev. 4.4,1994
<24.0 mg/kg
12/08/2022
Cadmium
EPA 200.7, Rev.4.4, 1994
<12.0 mg/kg
11/16/2022
Calcium
EPA 200.7, Rev. 4.4,1994
165000 mg/kg
11/16/2022
Chromium
EPA 200.7, Rev. 4.4,1994
22.3 mg/kg
11/16/2022
Copper
EPA 200.7, Rev. 4.4,1994
273 mg/kg
11/16/2022
Lead
EPA 200.7, Rev. 4.4,1994
15.8 mg/kg
11/16/2022
Magnesium
EPA 200.7, Rev. 4.4,1994
5760 mg/kg
11/16/2022
Molybdenum
EPA 200.7, Rev. 4.4,1994
<12.0 mg/kg
11/16/2022
Nickel
EPA 200.7, Rev. 4.4,1994
13.2 mg/kg
11/16/2022
Potassium
EPA 200.7, Rev. 4.4, 1994
5410 mg/kg
11/16/2022
Selenium
EPA 200.7, Rev. 4.4,1994
<12.0 mg/kg
11/16/2022
Sodium
EPA 200.7, Rev. 4.4,1994
3180 mg/kg
12/08/9202
Zinc
EPA 200.7, Rev. 4.4,1994
1060 mg/kg
11/16/2022
Nitrate+Nitrite-Nitrogen
EPA353.2
35.5mg/kg
11/14/2022
Total Solids (%)
SM 2540 B
3.99 %
12/15/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
4270 mg/kg
11/21/2022
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
36500 mg/kg
11/21/2022
Total Phosphorus
SM 4500 P (F-H)-2011
28600 mg/kg
11/22/2022
pH
SW 846 Method 9045D
12.01 units
11/29/2022
Result estimated. Analyzed out of
15 minutes hold time.
Mercury SW-846 7471 B <0.446 mg/kg 11/14/2022
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Revised to amend project ID and collection time. -.,
Reviewed by:
Report #:: 2022-22494 Page 1 of 1

Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client:��"��_O� _Date: I �%�� Report Number: _ 2022-90
Receipt of sample: ECHEM Pinkun ❑ rro„r noc„ar., r"l I inclIffr,
❑ YES ❑ NO
�L Icl
Ip N/A 1. Were custody seals present on the cooler?
❑ YES 10 NO
N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt °C
How temperature taken: ❑ Temperature Blank Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
Ig YES
❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
kT YES
10 NO
4. Were proper custody procedures (relinquished/received) followed?
❑ NO
5. Were sample ID's listed on the COC?
RYES
YES
Vr G vc
❑ NO
t1 nin
6. Were samples ID's listed on sample containers?
, ,.,-_- _
--
YES
— . --
❑ NO
I �VIIUV.uull UOIC 011U LIIIIt! ilSteu on [ne t..ULf
B. Were tests to be performed listed on the COC?
YES
O NO
9. Did samples arrive in proper containers for each test?
YES
❑ NO
10. Did samples arrive in good condition for each test?
YES
❑ NO
11. Was adequate sample volume available?'
YES 10
NO 112.
Were samples received within proper holding time for requested tests?
❑ YES
❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑ YES
❑ YES
❑ NO
❑ NO
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCl NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time: _
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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ANNUAL RESIDUAL SAMPLING SUMMARY FORM
WQ Permit No. WQ0002883 Facility Name City of Elizabeth City Source Permit No. 04-70-010 Source Name Elizabeth City WTP
Laboratory 1
Laboratory 2
Sample or Composite Date
Parameter (mg/Kg) Class A Class B
Environmental
Chemists, Inc.
Environmental
Chemists, Inc.
Environmental
Chemists, Inc.
Environmental
Chemists, Inc.
Environmental
Chemists, Inc.
Environmental
Chemists, Inc.
2/28/22
3/30/2022
6/8/2022
7/12/2022
9/8/2022
11/9/2022
Aluminum
N/A
N/A
6,580
13,800
14,300
13,200
8,610
9,250
Ammonia
N/A
N/A
38.5
233
1,230
1.57
1.32
0.747
Arsenic
41
75
43.10
4.70
9.58
6.74
3.46
3.05
Cadmium
39
85
0.112
4.70
9.58
6.74
3.46
3.05
Calcium
N/A
N/A
130,000
342,000
274,000
458,000
207,000
235,000
Copper
1,500
4,300
43.10
4.70
9.58
6.74
3.46
3.05
Lead
Magnesium
300
840
43.10
4.70
9.58
10.10
3.46
3.05
N/A
N/A
11,800
129,000
13,400
13,800
8,570
9,870
Mercury
17
57
5.81
0.157
0.414
0.282
0.249
0.141
Molybdenum
N/A
75
43.10
4.70
9.58
6.74
3.46
3.05
Nickel
420
420
43.10
4.70
9.58
6.74
3.46
3.05
Nitrate -Nitrite
Nitrogen
N/A
N/A
101
2.69
11.30
7.05
3.31
8.26
Percent Solids
N/A
N/A
0.26
10.60
4.25
6.38
7.60
13.40
pH (no units)
N/A
N/A
8.27
8.24
7.63
7.68
9.08
9.40
Phosphorus
N/A
N/A
444
636
463
294
97.9
182
Potassium
N/A
N/A
2,146
235
478
337
176
152
PAN (Inj./Inc.)
N/A
N/A
140
236
1,241
9.00
5.00
9.00
PAN (Surface)
N/A
N/A
120
119
626
8.00
4.00
8.60
Selenium
100
100
43.10
4.70
9.58
8.15
3.46
3.05
Sodium
N/A
N/A
15,300
689
1,320
1,000
755
527
SAR
N/A
N/A
0.55
0.10
0.14
0.10
0.12
0.11
TKN
N/A
N/A
5,450
537
1,920
7.80
317
294
Zinc
2,800
7,500
1 43.10
1 4.70
1 9.58
1 6.74
1 3.46
1 3.05
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2/21/23
Sig- of p.p- * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

Facility
Sampling Date
% Solids
Mineralization Rate
Gallons Per DT
pH
Elizabeth City WTP
2/28/2022
0.26
0
92233.91
8.27
Field Loading Estimate
SAR 0.55 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
SAR Calculation
Value From source Meq/L
Na 15300 1.729565217
Ca 130,000 16.9
Mg 11800 2.556666667
I Nitrogen Application Nutrient Application
TKN (mg/Kg)
5450
lbs./1000 gal 0.118
(mg/Kg)
Ammonia Nitrogen (mg/Kg)
38.5
lbs./1000 gal 0.001
Potassium
2146
Nitrate -Nitrite (mg/Kg)
101
lbs./1000 gal 0.002
Phosphorus
444
Calcium
130,000
Plant Available Nitrogen Surface Applied
Magnesium
11800
PAN (mg/Kg) 120.25
(lbs./1000 gal)
0.003
Molybdenum
43.1
Chromium
43.1
Plant Available Nitrogen Injected/Incorporated Applied
PAN (mg/Kg) 139.5 (lb s./1000 gal) 0.003
Volatilization Rate= .5 Surface Application
1.0 Injection/ Incorporation
(lbs./1000 gal)
0.0465
0.0096
2.8148
0.2555
0.0009
0.0009
EPA Metal
Limits
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
Heavy Metal Concentration (mg/Kg)
Heavy Metal Loading (lbs./1000
Arsenic
43.1
Arsenic
0.0009
41
75
39
85
Cadmium
0.112
Cadmium
0.0000
1,500
4,300
Copper
43.1
Copper
0.0009
300
840
Lead
43.1
Lead
0.0009
17
57
Mercury
5.81
Mercury
0.0001
420
420
Nickel
43.1
Nickel
0.0009
100
100
Selenium
43.1
Selenium
0.0009
2,800
7,500
Zinc
43.1
Zinc
0.0009
Residual Nitrogen Calculation
TKN
Surface (S)
PAN (S)
lbs/DT
Ing Organic N
TKN
Subsurface
(INJ)
(INJ)
Organic N
1 st Year
5450
120
0.24
5330
5450
140
0.28
5311
2nd Year
5330
0
0.00
5330
5311
0
0.00
5311
3rd Year
5330
0
0.00
5330
5311
0
0.00
5311
4th Year
5330
0
0.00
5330
5311
0
0.00
5311
5th Year
5330
0
0.00
5330
5311
0
0.00
5311
Total
120
0.24
Total
140
0.28
Equations
1st Yr. PAN (mg/Kg)-(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)- 2nd Yr. TKN x (MR/2)
3id Yr PAN (mg/Kg)- 3id Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)- 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)- 5th Yr. TKN x (MR/16)

Environmental Chemists, Inc.
envirochem
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infoCenvironmentalchemists.com
Atlantic OBX Revised Report: May 03, 2022
PO Box 2560 Original Report Date: Mar 18, 2022
Kitty Hawk NC 27949 Report #: 2022-03659
Attention: Customer ID: 18120006
Project ID: Elizabeth City WTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-08652 Site: Sludge 2/28/2022 11:45 AM Solid/Sludge Stephen Cummings
Test Method Results Date Analyzed
Chlordane (TCLP)
SW-846 8081 B
<0.02 mg/L
03/08/2022
Endrin (TCLP)
SW-846 8081 B
<0.0005 mg/L
03/08/2022
Heptachlor (TCLP)
SW-846 8081 B
<0.0005mg/L
03/08/2022
Heptachlor epoxide (TCLP)
SW-846 8081 B
<0.0005 mg/L
03/08/2022
Lindane (TCLP)
SW-846 8081 B
<0.0005 mg/L
03/08/2022
Methoxychlor (TCLP)
SW-846 8081 B
<0.0005 mg/L
03/08/2022
Toxaphene (TCLP)
SW-846 8081 B
<0.05 mg/L
03/08/2022
2,4,5-TP (TCLP)
SW-846 8151 A
<0.003 mg/L
03/08/2022
2,4-D (TCLP)
SW-846 8151 A
<0.003 mg/L
03/08/2022
1,4-Dichlorobenzene (TCLP)
SW-848 8270 E
<0.050 mg/L
03/10/2022
2,4,5-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
03/10/2022
2,4,6-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
03/10/2022
2,4-Dinitrotoluene (TCLP)
SW-846 8270 E
<0.050 mg/L
03/10/2022
Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
03/10/2022
Hexachloro-1,3-butadiene (TCLP)
SW-846 8270 E
<0.050 mg/L
03/10/2022
Hexachlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
03/10/2022
Hexachloroethane (TCLP)
SW-846 8270 E
<0.050 mg/L
03/10/2022
m + p-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
03/10/2022
Nitrobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
03/10/2022
o-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
03/10/2022
Pentachlorophenol (TCLP)
SW-846 8270 E
<0.250 mg/L
03/10/2022
Pyridine (TCLP)
SW-846 8270 E
<0.050 mg/L
03/10/2022
1,1-Dichloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
03/08/2022
1,2-Dichloroethane (TCLP)
SW-846 Method 8260D
<0.01 mg/L
03/08/2022
Benzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
03/08/2022
Carbon Tetrachloride (TCLP)
SW-846 Method 8260D
<0.01 mg/L
03/08/2022
Report#:: 2022-03659
Page 1 of 3

Environmental Chemists, Inc.
envitrochem 6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Atlantic OBX
Revised Report:
May 03, 2022
PO Box 2560
Original Report Date: Mar 18, 2022
Kitty Hawk NC
27949
Report #:
2022-03659
Attention:
Customer ID:
18120006
Project ID:
Elizabeth City WTP
Chlorobenzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
03/08/2022
Chloroform (TCLP)
SW-846 Method 8260D
<0.01 mg/L
03/08/2022
Methyl ethyl ketone (TCLP)
SW-846 Method 8260D
<0.05 mg/L
03/08/2022
Tetrachloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
03/08/2022
Trichloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
03/08/2022
Vinyl Chloride (TCLP)
SW-846 Method 8260D
<0.01 mg/L
03/08/2022
RCI
Cyanide
SM 4500 CN D-2016
<1.0 mg/kg
03/01 /2022
Sulfide
SM 4500 S D
< 1.00 mg/kg
03/03/2022
Ignitability
SW 846 method 1010
>159 °F
03/08/2022
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4 4,1994
6580 mg/kg
03/07/2022
Arsenic
EPA 200.7, Rev. 4.4, 1994
<43.1 mg/kg
03/07/2022
Cadmium
EPA 200.7, Rev. 4.4,1994
<0.112 mg/kg
03/07/2022
Calcium
EPA 200.7, Rev. 4.4,1994
130000 mg/kg
03/07/2022
Chromium
EPA 200.7, Rev. 4.4,1994
<43.1 mg/kg
03/07/2022
Copper
EPA 200.7, Rev. 4.4,1994
<43.1 mg/kg
03/07/2022
Lead
EPA 200.7, Rev. 4.4,1994
<43.1 mg/kg
03/07/2022
Magnesium
EPA 200.7, Rev. 4.4,1994
11800 mg/kg
03/07/2022
Molybdenum
EPA 200.7, Rev. 4.4,1994
<43.1 mg/kg
03/07/2022
Nickel
EPA 200.7, Rev. 4.4, 1994
<43.1 mg/kg
03/07/2022
Potassium
EPA 200.7, Rev. 4.4,1994
<2146 mg/kg
03/07/2022
Selenium
EPA 200.7, Rev. 4.4,1994
<43.1 mg/kg
03/07/2022
Sodium
EPA 200.7, Rev. 4.4,1994
15300 mg/kg
03/07/2022
Zinc
EPA 200.7, Rev. 4.4,1994
<43.1 mg/kg
03/07/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2
101 mg/kg
03/02/2022
Total Solids (%)
SM 2540 B
0.26 %
03/04/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
<38.5 mg/kg
03/02/2022
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
5450 mg/kg
03/03/2022
Report #:: 2022-03659 Page 2 of 3

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
srn 255-A Wilmington Highway, Jacksonville, NC 28540 e 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Atlantic OBX
PO Box 2560
Kitty Hawk
Attention:
NC 27949
Revised Report: May 03, 2022
Original Report Date: Mar 18, 2022
Report #: 2022-03659
Customer ID: 18120006
Project ID: Elizabeth City WTP
Total Phosphorus
SM 4500 P (F-H)-2011
444 mg/kg
03/04/2022
pH
SW 846 Method 9045D
8.27 units
03/14/2022
Result estimated.
Analyzed out of 15 minutes hold time.
Mercury
SW-846 7471 B
<5.81 mg/kg
03/09/2022
TCLP Metals
Arsenic
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
03/07/2022
Barium
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
03/07/2022
Cadmium
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
03/07/2022
Chromium
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
03/07/2022
Lead
EPA 200.7, Rev. 4 4,1994
<1.0 mg/L
03/07/2022
Selenium
EPA 200.7, Rev. 4A, 1994
<1.0 mg/L
03/07/2022
Silver
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
03/07/2022
Mercury
EPA 245.1
<0.0002 mg/L
03/09/2022
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
AMENDED 05/03/2022 to correct project name.
Reviewed by:
`=EQ�,yt,,�� Z�4��
Report #:: 2022-03659 Page 3 of 3

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
Sample Receipt Checklist 910.392.0223
ClientA60HC BX Ik"i (.c �^.o "t
Date: 2 Z Report Number: _ 2022_
Receipt of sample:
P E HEM Pickup ❑ Client Delivery ❑ UPS
El YES El NO FedEx ❑ Other N/A ❑
1. Were custody seals present on the cooler?
❑ YES ❑ NO N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C
How temperature taken: ❑ Temperature Blank Corrected temperature upon receipt
°C
IR Gun ID: Thomas Traceable S/N: 210835468 IR Gun Ces
orrecti n lactorr Ct10.0
❑ YES ❑ NO 3. If temperature of cooler exceeded 6°C, was Project M r.
YES El 4. Were proper custody� g /QA notified?
procedures (relinquished/received) followed?
YES ❑ NO 5. Were sample ID's listed on the COL?
YES ❑ NO 6. Were samples ID's listed on sample containers?
YES ❑ NO 7. Were collection date and time listed on the COC?
YES ❑ NO 8. Were tests to be performed listed on the COC?
YES ❑ NO 9. Did samples arrive in proper containers for each test?
_ Y=5 ❑ f10 110. Did sdniples arrive in good condition for each test? 14+11 Yr� IU NO ill IA a rin i Rta /_5 a-._q.l_,_ ca�tnlo volumes available?'^
MElmr,
O 12. Were samples received within proper holding time for requested tests?
O .1 Were acid preserved samples received at a pH of <2?
O 14. Were cyanide samples received at a pH >12?
O 15. Were sulfide samples received at a pH >9?
16. bVere NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ' f
17. %AVere Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiies are pH checked at time of analysis and recorded on the benchsheet.
t(circle
ia samples are checked for Chlorine at time of analysisand recorded on the benchshe2t.
eservation: (Must be completed for an+ / samples) incorrectly preserved or with headspace)
were received incorrectly preserved and were adjusted accordingly
(circle one): HSO HNO3 HCI NaOH
eservation: If more than one resrvative is needed, notate in comments below
JStOR12f 5?iVlCe immed
iately / for If
preserved samples. obtain a new sa-n le
loti5/ the sate lab if directej to ana'� zed by the P _ or
/ / custorr,er. Who was notified, date and time:
Volatiles Sample(s)
were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

ep
�+ C L
6-1 i
v,
rAR ID
eCL e,
e.
t
c
r� c�
a'
Sample
A
Type
G�n0n0nOno nOno o non
n
=osite
a o
ty
�II1--,11Grab
?
C� 'd Ca ►o hi C] �d 0 ' 4' M G] ►e ,n b ro �] ►�
Caawner
r w
S
(PorG)
n
Cblorine Q
a
mg/L
c
NONE G'
[A
y,y
HCL II
%g. j C
C�
h rn
to
CZ
Do
Z
p
nuo
Lirr
oT'HER
a
n
�
N
�
�
�
d
n

Facility
Sampling Date
% Solids
Mineralization Rate
Gallons Per DT
pH
SAR
SAR Calculation
Value From source
Na
Ca
Mg
Field Loading Estimate
Elizabeth City WTP
3/30/2022
10.6
0
2262.34
8.24
0.10 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Meq/L
689 3.175391304
342,000 1812.6
12900 113.95
I Nitrogen Application Nutrient Application
TKN (mg/Kg)
537
lbs./1000 gal 0.474
(mg/Kg)
Ammonia Nitrogen (mg/Kg)
233
lbs./1000 gal 0.206
Potassium
235
Nitrate -Nitrite (mg/Kg)
2.69
lbs./1000 gal 0.002
Phosphorus
636
Calcium
342,000
Plant Available Nitrogen Surface Applied
Magnesium
12900
PAN (mg/Kg) 119.19
(lbs./1000 gal)
0.105
Molybdenum
4.7
Chromium
4.7
Plant Available Nitrogen Injected/Incorporated Applied
PAN (mg/Kg) 235.69 (lb s./1000 gal) 0.208
Volatilization Rate= .5 Surface Application
1.0 Injection/ Incorporation
(lbs./1000 gal)
0.2074
0.5614
301.9033
11.3876
0.0041
0.0041
EPA Metal
Limits
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
Heavy Metal Concentration (mg/Kg)
Heavy Metal Loading (lbs./1000
Arsenic
4.7
Arsenic
0.0041
41
75
39
85
Cadmium
4.7
Cadmium
0.0041
1,500
4,300
Copper
4.7
Copper
0.0041
300
840
Lead
4.7
Lead
0.0041
17
57
Mercury
0.157
Mercury
0.0001
420
420
Nickel
4.7
Nickel
0.0041
100
100
Selenium
4.7
Selenium
0.0041
2,800
7,500
Zinc
4.7
Zinc
0.0041
Residual Nitrogen Calculation
TKN
Surface (S)
PAN (S)
lbs/DT
Ing Organic N
TKN
Subsurface
(INJ)
(INJ)
Organic N
1 st Year
537
119
0.24
418
537
236
0.47
301
2nd Year
418
0
0.00
418
301
0
0.00
301
3rd Year
418
0
0.00
418
301
0
0.00
301
4th Year
418
0
0.00
418
301
0
0.00
301
5th Year
418
0
0.00
418
301
0
0.00
301
Total
119
0.24
Total
236
0.47
Equations
1st Yr. PAN (mg/Kg)-(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)- 2nd Yr. TKN x (MR/2)
3id Yr PAN (mg/Kg)- 3id Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)- 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)- 5th Yr. TKN x (MR/16)

F-7 -0 0 Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
SMl
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
[e-mail]
Atlantic OBX
Revised Report: May 03, 2022
PO Box 2560
Original Report Date: Apr 27, 2022
Kitty Hawk NC 27949
Report #: 2022-05795
Attention:
Customer ID: 18120006
Project ID: Elizabeth City WTP
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-14044 Site: Sludge
3/30/2022
11:10 AM Solid/Sludge Client
Test
Method
Results
Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4, 1994
13800 mg/kg
04/14/2022
Arsenic
EPA 200.7, Rev. 4.4, 1994
<4.70 mg/kg
04/14/2022
Cadmium
EPA 200.7, Rev. 4.4,1994
<4.70 mg/kg
04/14/2022
Calcium
EPA 200.7, Rev. 4.4, 1994
342000 mg/kg
04/20/2022
Chromium
EPA 200.7, Rev. 4.4,1994
<4.70 mg/kg
04/14/2022
Copper
EPA 200.7, Rev. 4.4,1994
<4.70 mg/kg
04/14/2022
Lead
EPA 200.7, Rev. 4.4, 1994
<4.70 mg/kg
04/14/2022
Magnesium
EPA 200.7, Rev. 4.4, 1994
12900 mg/kg
04/14/2022
Molybdenum
EPA 200.7, Rev. 4.4, 1994
<4.70 mg/kg
04/14/2022
Nickel
EPA 200.7, Rev. 4.4, 1994
<4.70 mg/kg
04/14/2022
Potassium
EPA 200.7, Rev. 4.4, 1994
<235 mg/kg
04/14/2022
Selenium
EPA 200.7, Rev. 4.4, 1994
<4.70 mg/kg
04/14/2022
Sodium
EPA 200.7, Rev. 4.4,1994
689 mg/kg
04/14/2022
Zinc
EPA 200.7, Rev. 4.4, 1994
<4.70 mg/kg
04/14/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2
2.69 mg/kg
04/01/2022
Total Solids (%)
SM 2540 B
10.6 %
04/01/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
233 mg/kg
04/01/2022
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
537 mg/kg
04/01/2022
Total Phosphorus
SM 4500 P (F-H)-2011
636 mg/kg
04/06/2022
pH
SW 846 Method 9045D
8.24 units
04/12/2022
Result estimated. Analyzed out of 15 minutes hold time.
Mercury
SW-846 7471 B
<0.157 mg/kg
04/04/2022
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
AMENDED 05/03/2022 to correct project name
Reviewed by:
Report #:: 2022-05795 Page 1 of 1

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
Sample Receipt Checklist 910.392.0223
Client:_ N 1,G Vn�i Q e) y 3 3 I 2.2 Date: �_ Report Number: _ 2022- t:57c:�'15
Receipt of sample:
❑ YES ❑ NO
HEM Pickup ElClientClient Delivery❑ UPS FedEx Other ❑
O
N/A
O YES
❑ NO
N/A
1. Were custody seals present on the cooler?
Original temperature
upo
r ceipt---`C
2. If custody seals were present, were they intact/unbroken?
Corrected temperature upon receipt__
How temperature taken: ❑ Temperature Blank
Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor'C: 0.0
YES
YES
❑ NO
❑
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
NO
❑
4. Were proper custody procedures (relinquished/received) followed?
NO
5. Were sample ID's listed on the COC?
YES
❑ NO
6. Were samples ID's listed on sample containers?
YES
❑ NO
7. Were collection date and time listed on the COC?
YES
❑ NO
8. Were tests to be performed listed on the COC?
YES
YES
❑ NO
❑
9. Did samples arrive in proper containers for each test?
NO
10. Did samples arrive in good condition for each test?
YES
❑ NO
11. Was adequate sample volume available?'
YES
❑
❑ NO
12. Were samples received within proper holding time for requested tests?
YES
❑
❑ NO
13. Were acid preserved samples received at a pH of <2?
YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑ YES
❑ NO
❑
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L?
❑ YES
NO
❑
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
;ample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
;ample(s) were received incorrectly preserved and were adjusted accordingly
iy adding (circle one): H2504 HNO3 HCl NaOH
'ime of preservation: If more than one preservative is needed, notate in comments below
ote: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
3tify the state lab if directed to analyzed by the customer. Who was notified, date and time:
olatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1
'C

N ~
a
U
a
e
2
G
rt
N
o
en
�
N
LAB ID
A
NUMBER
eD
W
C
�
ttA
a
o
n
q
21
II
Sample
2.
Type
y
Compositeor
Grab
Z
G)co
5
(P or
m
Q
Chlorine
—_I
Mgt
0
NOM
C
�
�
b
NmOH
O
::
"no
OTHER
7,
k
r.
A
�D
,
u

Facility
Sampling Date
% Solids
Mineralization Rate
Gallons Per DT
pH
Elizabeth City WTP
6/8/2022
4.25
0
5642.54
7.63
Field Loading Estimate
SAR 0.14 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
SAR Calculation
Value From source Meq/L
Na 1320 2.439130435
Ca 274,000 582.25
Mg 13400 47.45833333
I Nitrogen Application Nutrient Application
TKN (mg/Kg)
1920
lbs./1000 gal 0.680
(mg/Kg)
Ammonia Nitrogen (mg/Kg)
1230
lbs./1000 gal 0.435
Potassium
478
Nitrate -Nitrite (mg/Kg)
11.3
lbs./1000 gal 0.004
Phosphorus
463
Calcium
274,000
Plant Available Nitrogen Surface Applied
Magnesium
13400
PAN (mg/Kg) 626.3
(lbs./1000 gal)
0.222
Molybdenum
9.58
Chromium
9.58
Plant Available Nitrogen Injected/Incorporated Applied
PAN (mg/Kg) 1241.3 (lb s./1000 gal) 0.439
Volatilization Rate= .5 Surface Application
1.0 Injection/ Incorporation
(lbs./1000 gal)
0.1692
0.1639
96.9785
4.7427
0.0034
0.0034
EPA Metal
Limits
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
Heavy Metal Concentration (mg/Kg)
Heavy Metal Loading (lbs./1000
Arsenic
9.58
Arsenic
0.0034
41
75
39
85
Cadmium
9.58
Cadmium
0.0034
1,500
4,300
Copper
9.58
Copper
0.0034
300
840
Lead
9.58
Lead
0.0034
17
57
Mercury
0.414
Mercury
0.0001
420
420
Nickel
9.58
Nickel
0.0034
100
100
Selenium
9.58
Selenium
0.0034
2,800
7,500
Zinc
9.58
Zinc
0.0034
Residual Nitrogen Calculation
TKN
Surface (S)
PAN (S)
lbs/DT
Ing Organic N
TKN
Subsurface
(INJ)
(INJ)
Organic N
1 st Year
1920
626
1.25
1294
1920
1241
2.48
679
2nd Year
1294
0
0.00
1294
679
0
0.00
679
3rd Year
1294
0
0.00
1294
679
0
0.00
679
4th Year
1294
0
0.00
1294
679
0
0.00
679
5th Year
1294
0
0.00
1294
679
0
0.00
679
Total
626
1.25
Total
1241
2.48
Equations
1st Yr. PAN (mg/Kg)-(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)- 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)- 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)- 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)- 5th Yr. TKN x (MR/16)

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
info(aDenvironmentalchemists.com
Atlantic OBX
Date of Report: Jun 30, 2022
PO Box 2560
Customer PO #:
Kitty Hawk NC 27949
Customer ID: 18120006
Attention:
Report #: 2022-10660
Project ID: Elizabeth City WTP
Lab ID Sample ID:
22-25827 Site: Sludge
Collect Date/Time Matrix Sampled by
6/8/2022 11:35 AM Solid/Sludge Stephen Cummings
Test
Method
Results
Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4,1994
14300 mg/kg
06/20/2022
Arsenic
EPA 200.7, Rev. 4.4,1994
<9.58 mg/kg
06/20/2022
Cadmium
EPA 200.7, Rev. 4.4,1994
<9.58 mg/kg
06/20/2022
Calcium
EPA 200.7, Rev. 4.4,1994
274000 mg/kg
06/28/2022
Chromium
EPA 200.7, Rev. 4.4,1994
<9.58 mg/kg
06/20/2022
Copper
EPA 200.7, Rev. 4.4,1994
<9.58 mg/kg
06/20/2022
Lead
EPA 200.7, Rev. 4.4,1994
<9.58 mg/kg
06/20/2022
Magnesium
EPA 200.7, Rev. 4.4,1994
13400 mg/kg
06/20/2022
Molybdenum
EPA 200.7, Rev. 4.4,1994
<9.58 mg/kg
06/20/2022
Nickel
EPA 200.7, Rev. 4.4,1994
<9.58 mg/kg
06/20/2022
Potassium
EPA 200.7, Rev. 4.4,1994
<478 mg/kg
06/28/2022
Selenium
EPA 200.7, Rev. 4.4, 1994
<9.58 mg/kg
06/20/2022
Sodium
EPA 200.7, Rev. 4.4,1994
1320 mg/kg
06/20/2022
Zinc
EPA 200.7, Rev. 4.4,1994
<9.58 mg/kg
06/20/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2
11.3 mg/kg
06/15/2022
Total Solids (%)
SM 2540 B
4.25 %
06/14/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
1230 mg/kg
06/13/2022
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
1920 mg/kg
06/13/2022
Total Phosphorus
SM 4500 P (F-H)-2011
463 mg/kg
06/20/2022
pH
SW 846 Method 9045D
7.63 units
06/28/2022
Result estimated. Analyzed out of 15 minutes hold time.
Mercury
SW-846 7471 B
<0.414 mg/kg
06/17/2022
Comment: Results, except pH, reported on a dry weight basis. pH
reported on an as received basis.
Reviewed by: ��_
au" X
Report #:: 2022-10660 Page 1 of 1

Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client: P4A Cn�iC Date: 1 22
Report Number: _ 2022-1 o(,C,(,_,D
Receipt of sample:
ECHEM Pickup ❑ Client Delivery ❑
UPS FedEx El Other ❑
❑ YES
❑
NO
N/A
1. Were custody seals present on the cooler?
❑ YES
❑
NO
N/A
2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt
°C Corrected temperature upon receipt °C
How temperature taken:
❑ Temperature Blank IX Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
YES
❑
NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
❑
NO
4. Were proper custody procedures (relinquished/received) followed?
YES
❑
NO
5. Were sample ID's listed on the COC?
YES
❑
NO
6. Were samples ID's listed on sample containers?
YES
❑
NO
7. Were collection date and time listed on the COC?
YES
❑
NO
8. Were tests to be performed listed on the COC?
YES
I—
❑
NO
1r. Er -.,.i"aiii ars [Ij, Ea CI-1 LE—I—I•1'L—
10.
Did samples arrive in good condition for each test? -
YES
❑
NO
11. Was adeg!iat-_ sample vo!ume availableT
YES
❑
NO
12. Were samples received within proper holding time for requested tests?
❑ YES
❑
NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑
NO
114. Were cyanide samples received at a pH >12?
❑ YES
❑
NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑
NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? xx
❑ YES
❑
NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
❑
NO 118.
Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. obtain a new sample or
notify the state lab if directed to analyzed by the customer. who was notified, date and t'me:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

f,
i
NONE
i
'
HCL
!
H2SO4 _
HNO3 C
a
�
NadH 9
'
THIO
a�
Z
d
�
d
sm

Facility
Sampling Date
% Solids
Mineralization Rate
Gallons Per DT
pH
Elizabeth City WTP
7/12/2022
6.38
0
3758.75
7.98
Field Loading Estimate
SAR 0.10 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
SAR Calculation
Value From source Meq/L
Na 1000 2.773913043
Ca 458,000 1461.02
Mg 13800 73.37
I Nitrogen Application Nutrient Application
TKN (mg/Kg)
7.8
lbs./1000 gal 0.004
(mg/Kg)
Ammonia Nitrogen (mg/Kg)
1.57
lbs./1000 gal 0.001
Potassium
337
Nitrate -Nitrite (mg/Kg)
7.05
lbs./1000 gal 0.004
Phosphorus
294
Calcium
458,000
Plant Available Nitrogen Surface Applied
Magnesium
13800
PAN (mg/Kg) 7.835
(lbs./1000 gal)
0.004
Molybdenum
6.74
Chromium
6.74
Plant Available Nitrogen Injected/Incorporated Applied
PAN (mg/Kg) 8.62 (lb s./1000 gal) 0.005
Volatilization Rate= .5 Surface Application
1.0 Injection/Incorporation
(lbs./1000 gal)
0.1791
0.1562
243.3448
7.3322
0.0036
0.0036
EPA Metal
Limits
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
Heavy Metal Concentration (mg/Kg)
Heavy Metal Loading (lbs./1000
Arsenic
6.74
Arsenic
0.0036
41
75
39
85
Cadmium
6.74
Cadmium
0.0036
1,500
4,300
Copper
6.74
Copper
0.0036
300
840
Lead
10.1
Lead
0.0054
17
57
Mercury
0.282
Mercury
0.0001
420
420
Nickel
6.74
Nickel
0.0036
100
100
Selenium
8.15
Selenium
0.0043
2,800
7,500
Zinc
6.74
Zinc
0.0036
Residual Nitrogen Calculation
TKN
Surface (S)
PAN (S)
lbs/DT
Ing Organic N
TKN
Subsurface
(INJ)
(INJ)
Organic N
1 st Year
7.8
8
0.02
0
7.8
9
0.02
0
2nd Year
0
0
0.00
0
0
0
0.00
0
3rd Year
0
0
0.00
0
0
0
0.00
0
4th Year
0
0
0.00
0
0
0
0.00
0
5th Year
0
0
0.00
0
0
0
0.00
0
Total
8
0.02
Total
9
0.02
Equations
1st Yr. PAN (mg/Kg)-(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)- 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)- 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)- 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)- 5th Yr. TKN x (MR/16)

F7 0 077
Cnviroche]m
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Atlantic OBX
Date of Report: Aug 16, 2022
PO Box 2560
Customer PO #:
Kitty Hawk NC
27949
Customer ID: 18120006
Attention:
Report #: 2022-13266
Project ID: Elizabeth City WWTP
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-32227 Site: Sludge
7/12/2022
12:00 PM Solid/Sludge Stephen Cummings
Test
Method
Results Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4, 1994
13200 mg/kg
07/19/2022
Arsenic
EPA 200.7, Rev. 4.4, 1994
<6.74 mg/kg
07/19/2022
Cadmium
EPA 200.7, Rev. 4.4, 1994
<6.74 mg/kg
07/19/2022
Calcium
EPA 200.7, Rev. 4.4, 1994
458000 mg/kg
07/22/2022
Chromium
EPA 200.7, Rev. 4.4, 1994
<6.74 mg/kg
07/19/2022
Copper
EPA 200.7, Rev. 4.4, 1994
<6.74 mg/kg
07/19/2022
Lead
EPA 200.7, Rev. 4.4, 1994
10.1 mg/kg
07/19/2022
Magnesium
EPA 200.7, Rev. 4.4, 1994
13800 mg/kg
07/19/2022
Molybdenum
EPA 200.7. Rev. 4.4,1994
<6.74 mg/kg
07/19/2022
Nickel
EPA 200.7, Rev. 4.4, 1994
<6.74 mg/kg
07/19/2022
Potassium
EPA 200.7, Rev. 4.4, 1994
<337 mg/kg
07/19/2022
Selenium
EPA 200.7, Rev. 4.4, 1994
8.15 mg/kg
07/19/2022
Sodium
EPA 200 7, Rev 4.4, 1994
1000 mg/kg
07/19/2022
Zinc
EPA 2007, Rev. 4.4, 1994
<6.74 mg/kg
07/19/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2
7.05 mg/kg
07/20/2022
Total Solids (%)
SM 2540 B
6.38 %
07/15/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
<1.57 mg/kg
07/20/2022
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
<7.8 mg/kg
08/09/2022
Total Phosphorus
SM 4500 P (F-H)-2011
294 mg/kg
07/22/2022
pH
SW 846 Method 9045D
7.98 units
07/29/2022
Result estimated. Analyzed out of 15 minutes hold time.
Mercury
SW-8467471 B
<0.282mg/kg
07/18/2022
Comment: Sludge resiudals,
except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
Report #!! 2022-13266 Page 1 of 1

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
Sample Receipt Checklist 910-392.0223
Client: c _ �jj�u.
Date' Report NurnbEr: _ 2022- 1-32JO6
❑ Receipt YESofsample: ECHEM Pickup ❑ Client Delivery i 2Z ❑ UPS
❑ NO N/A 1. Were custod s - I FedEx ❑ Other ❑
Li YES Li NO y ea s-present on the cooler?
N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt 'C
How temperature taken: Corrected temperature upon receipt
O Temperature Blank
IR Gun ID: Thomas Traceable 5/N 192511657 Against Bottles
IR Gun Correction Factor'C: 0.0
YES ❑ NO 3. If temperature of cooler exceeded 6°C was Project M r.
YES El NO 4. Were proper custody procedures (relinquished/received) oAlowelded?
YES ❑ NO 5. Were sample ID's listed on the COC?
' YES ❑ NO 6. Were samples ID's listed on sample containers?
YES ❑ NO ,7. Were collection date and time listed on the COC?
x YES I D, PIS-
- iisted on the COC? -
( YES
YES 10, Did samples arri..,e in good condition for each test? - -
❑ N0 adequato ca 710 I
YES - `" l-,me available?'
❑ NO I12. Were samples rec- ive-+ within
YES p ` - U within proper holding time for requested tests?
YES 1❑ NO 13. Were aci:i preser.,ad sa„iples received at a pH of <ze x
0 NO 114. Were cyanide samples re
YES ceived at a pH >12?
❑ NO 115. Were sulfide YES i ❑ NO sam;,!es received at a pH >9?
i F u/� „T,,.. -
- „� , .r:� nenoi received at a chlorine residual of <0.5 m/L? xY
YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0,5 m/�?
YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volataes are pH checked at tL„e
c v' an�I'yS'j a"ld recorded on the benchsheet.
Bacteria SamFies are checked for Ch!o-ine at tirre 0` analysis and recorded On the benChsheet,
Sample Preservation: (Must be completed for any sampfe(s) incorrect) Samples) y preserved or with headspace)
were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H S0�
z HNO; HCI NaOH
Time of presentation:
If"more than one preservative is needed, notate in comments beloy,
Vase:
10:y fat = ec-,e -, ,_ a n 2
Volatiles Samp'e(s}
were received with headspa=e
COMMENTS:
oC

H
�5

Facility
Sampling Date
% Solids
Mineralization Rate
Gallons Per DT
pH
Elizabeth City WTP
9/8/2022
7.6
0
3155.37
9.08
Field Loading Estimate
SAR 0.12 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
SAR Calculation
Value From source Meq/L
Na 755 2.494782609
Ca 207,000 786.6
Mg 8570 54.27666667
I Nitrogen Application Nutrient Application
TKN (mg/Kg)
317
lbs./1000 gal 0.201
(mg/Kg)
Ammonia Nitrogen (mg/Kg)
1.32
lbs./1000 gal 0.001
Potassium
176
Nitrate -Nitrite (mg/Kg)
3.31
lbs./1000 gal 0.002
Phosphorus
97.9
Calcium
207,000
Plant Available Nitrogen Surface Applied
Magnesium
8570
PAN (mg/Kg) 3.97
(lbs./1000 gal)
0.003
Molybdenum
3.46
Chromium
3.46
Plant Available Nitrogen Injected/Incorporated Applied
PAN (mg/Kg) 4.63 (lb s./1000 gal) 0.003
Volatilization Rate= .5 Surface Application
1.0 Injection/Incorporation
(lbs./1000 gal)
0.1114
0.0620
131.0146
5.4241
0.0022
0.0022
EPA Metal
Limits
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
Heavy Metal Concentration (mg/Kg)
Heavy Metal Loading (lbs./1000
Arsenic
3.46
Arsenic
0.0022
41
75
39
85
Cadmium
3.46
Cadmium
0.0022
1,500
4,300
Copper
3.46
Copper
0.0022
300
840
Lead
3.46
Lead
0.0022
17
57
Mercury
0.249
Mercury
0.0002
420
420
Nickel
3.46
Nickel
0.0022
100
100
Selenium
3.46
Selenium
0.0022
2,800
7,500
Zinc
3.46
Zinc
0.0022
Residual Nitrogen Calculation
TKN
Surface (S)
PAN (S)
lbs/DT
Ing Organic N
TKN
Subsurface
(INJ)
(INJ)
Organic N
1 st Year
317
4
0.01
313
317
5
0.01
312
2nd Year
313
0
0.00
313
312
0
0.00
312
3rd Year
313
0
0.00
313
312
0
0.00
312
4th Year
313
0
0.00
313
312
0
0.00
312
5th Year
313
0
0.00
313
312
0
0.00
312
Total
4
0.01
Total
5
0.01
Equations
1st Yr. PAN (mg/Kg)-(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)- 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)- 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)- 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)- 5th Yr. TKN x (MR/16)

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
J 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Atlantic OBX Date of Report: Oct 14, 2022
PO Box 2560 Customer PO #:
Kitty Hawk NC 27949 Customer ID: 18120006
Attention: Report #: 2022-17740
Project ID: Elizabeth City WTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-43496 Site: Sludge 9/8/2022 12:25 PM Solid/Sludge Stephen Cummings
Test Method Results Date Analyzed
Sludge Residuals
Aluminum EPA 200.7, Rev. 4.4,1994 8610 mg/kg 09/17/2022
Cadmium EPA 200.7, Rev. 4.4,1994 <3.46 mg/kg 09/17/2022
Calcium EPA 200.7, Rev. 4.4,1994 207000 mg/kg 09/19/2022
Chromium EPA 200.7, Rev. 4.4,1994 <3.46 mg/kg 09/17/2022
Copper EPA 200.7, Rev. 4.4,1994 <3.46 mg/kg 09/17/2022
Lead EPA 200.7, Rev. 4.4,1994 <3.46 mg/kg 09/17/2022
Magnesium EPA 200.7, Rev. 4.4,1994 8570 mg/kg 09/17/2022
Molybdenum EPA 200.7, Rev. 4.4,1994 <3.46 mg/kg 09/17/2022
Nickel EPA 200.7, Rev. 4.4,1994 <3.46 mg/kg 09/17/2022
Potassium EPA 200.7, Rev. 4.4,1994 176 mg/kg 09/17/2022
Selenium EPA 200.7, Rev. 4.4,1994 <3.46 mg/kg 09/17/2022
Sodium EPA 200.7, Rev. 4.4,1994 755 mg/kg 09/17/2022
Zinc EPA 200.7, Rev. 4.4,1994 <3.46 mg/kg 09/17/2022
Arsenic EPA 200.8, Rev. 5.4,1994 <3.46 mg/kg 09/20/2022
Nitrate+Nitrite-Nitrogen EPA 353.2 3.31 mg/kg 09/12/2022
Total Solids (%) SM 2540 B 7.60 % 09/15/2022
Ammonia Nitrogen SM 4500 NH3 C-2011 <1.32 mg/kg 09/13/2022
Total Kjeldahl Nitrogen (TKN) SM 4500 Norg B-2011 317 mg/kg 09/13/2022
Total Phosphorus SM 4500 P (F-H)-2011 97.9 mg/kg 09/19/2022
pH SW 846 Method 9045D 9.08 units 09/12/2022
Mercury SW-846 7471 B <0.249 mg/kg 09/17/2022
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
Report #:: 2022-17740 Page 1 of 1

n
0
c�
0
rn
rt
C.
m
Chloe
mg/L
NONE
I
i
HUI
�•
ILSO.,
f�D
HNO, C C
xaaH ;
td
�
..
z
TMO
oT=
�Z
v
i
0
ri
N�
N W
A
Ln

Facility
Sampling Date
% Solids
Mineralization Rate
Gallons Per DT
pH
Elizabeth City WTP
11/9/2022
13.4
0
1789.61
Field Loading Estimate
SAR 0.11 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
SAR Calculation
Value From source Meq/L
Na 527 3.070347826
Ca 235,000 1574.5
Mg 9870 110.215
I Nitrogen Application Nutrient Application
TKN (mg/Kg) 294 lbs./1000 gal 0.329
(mg/Kg)
Ammonia Nitrogen (mg/Kg) 0.747 lbs./1000 gal 0.001
Potassium
152
Nitrate -Nitrite (mg/Kg) 8.26 lbs./1000 gal 0.009
Phosphorus
182
Calcium
235,000
Plant Available Nitrogen Surface Applied
Magnesium
9870
PAN (mg/Kg) 8.6335 (lbs./1000 gal) 0.010
Molybdenum
3.05
Chromium
3.05
Plant Available Nitrogen Injected/Incorporated Applied
PAN (mg/Kg) 9.007 (lbs./1000 gal) 0.010
Volatilization Rate= .5 Surface Application
1.0 In ection /Incorporation
(lbs./1000 gal)
0.1701
0.2036
262.9415
11.0435
0.0034
0.0034
EPA Metal
Limits
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
Heavy Metal Concentration (mg/Kg)
Heavy Metal Loading (lbs./1000
Arsenic
3.05
Arsenic
0.0034
41
75
39
85
Cadmium
3.05
Cadmium
0.0034
1,500
4,300
Copper
3.05
Copper
0.0034
300
840
Lead
3.05
Lead
0.0034
17
57
Mercury
0.14
Mercury
0.0002
420
420
Nickel
3.05
Nickel
0.0034
100
100
Selenium
3.05
Selenium
0.0034
2,800
7,500
Zinc
3.05
Zinc
0.0034
Residual Nitrogen Calculation
Remaing
PAN
Remaing
PAN (S)
Subsurface
TKN
Surface (S)
Organic N
TKN
(INJ)
Organic N
lbs/DT
(INJ)
(S)
lbs/DT
(INJ)
1 st Year
294
9
0.02
285
294
9
0.02
285
2nd Year
285
0
0.00
285
285
0
0.00
285
3rd Year
285
0
0.00
285
285
0
0.00
285
4th Year
285
0
0.00
285
285
0
0.00
285
5th Year
285
0
0.00
285
285
0
0.00
285
Totall
9
0.02
1 Total
9
0.02
Equations
1st Yr. PAN (1ng/hg)=(b1R x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)- 2nd Yr. TKN x (b7R/2)
3rd Yr PAN (mg/Kg)- 3rd Yr. TKN x (b7R/4)
4di Yr PAN (mg/Kg)- 4di Yr. TKN x (b7R/8)
5di Yr PAN (mg/Kg)- 5di Yr. TKN x (b7R/16)

F""" -- Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
SM
255-A Wilmington Highway, Jacksonville, NC 28540 e 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Atlantic OBX
Revised Report: Dec 20, 2022
PO Box 2560
Original Report Date: Dec 13, 2022
Kitty Hawk NC
27949
Report #: 2022-22500
Attention:
Customer ID: 18120006
Project ID: Elizabeth City WTP
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-55158 Site: Sludge
11/9/2022
10:35 AM Solid/Sludge Stephen Cummings
Test
Method
Results
Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4,1994
9250 mg/kg
11/16/2022
Arsenic
EPA 200.7, Rev. 4.4,1994
<3.05 mg/kg
11/16/2022
Cadmium
EPA 200.7, Rev. 4.4,1994
<3.05 mg/kg
11/16/2022
Calcium
EPA 200.7, Rev. 4.4,1994
235000 mg/kg
12/08/2022
Chromium
EPA 200.7, Rev. 4.4,1994
<3.05 mg/kg
11/16/2022
Copper
EPA 200.7, Rev. 4.4,1994
<3.05 mg/kg
11 /1612022
Lead
EPA 200.7, Rev. 4.4,1994
<3.05 mg/kg
11/16/2022
Magnesium
EPA 200.7, Rev. 4.4,1994
9870 mg/kg
11/16/2022
Molybdenum
EPA 200.7, Rev. 4.4,1994
<3.05 mg/kg
11/16/2022
Nickel
EPA 200.7, Rev. 4.4,1994
<3.05 mg/kg
11/16/2022
Potassium
EPA 200.7, Rev. 4.4,1994
<152 mg/kg
11/16/2022
Selenium
EPA 200.7, Rev. 4.4,1994
<3.05 mg/kg
11/16/2022
Sodium
EPA 200.7, Rev. 4.4, 1994
527 mg/kg
12/08/2022
Zinc
EPA 200.7, Rev. 4.4,1994
<3.05 mg/kg
11/16/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2
8.26 mg/kg
11/14/2022
Total Solids (%)
SM 2540 B
13.4 %
11/11/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
<0.747 mg/kg
11/11/2022
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
294 mg/kg
11/11/2022
Total Phosphorus
SM 4500 P (F-H)-2011
182 mg/kg
11/22/2022
pH
SW 846 Method 9045D
9.40 units
11/14/2022
Result estimated. Analyzed out of 15 minutes hold time.
Mercury
SW-8467471 B
<0.141 mg/kg
11/14/2022
Comment: Sludge residuals,
except pH, reported on a dry weight basis. pH reported on an as received basis.
Revised to amend collection time.
Reviewed by:
����
Report #:: 2022-22500 Page 1 of 1

Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client: Qom,/%' Date: Report Number: _ 2022- (�W
Receipt of sample:
❑
ECHEM Pickup ❑ Client Delivery ❑ UPS FedEx ❑ Other ❑
YES
❑
NO
N/A 1. Were custody seals present on the cooler?
❑ YES
El
NO
N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt
How temperature taken:
❑ Temperature Blank A Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
YES
ID
NO
1 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
I ❑
NO
4. Were proper custody procedures (relinquished/received) followed?
YES
❑
NO
5. Were sample ID's listed on the COC?
YES
❑
NO
6. Were samples ID's listed on sample containers?
YES
❑
NO
7. Were collection date and time listed on the COC?
YES
❑
NO
8. Were tests to be performed listed on the COC?
YES
❑
NO
9. Did samples arrive in proper containers for each test?
YES
❑
NO
10. Did samples arrive in good condition for each test?
YES
❑
NO
11. Was adequate sample volume available?'
YES
❑
NO
12. Were samples received within proper holding time for requested tests?
❑ YES
O
NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑
NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑
NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑
NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES
❑
NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
❑
NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Samples) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): HzSOa HNO3 HCl NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspacp
COMMENTS:
DOC. QA.002 Rev 1
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City of Elizabeth City
2022 Class B Annual Report
WQ0002883
Land Application Field Summary Forms

Permit Numner WQ0002883
Facility Name City of Elizabeth City
Land Owner Lawrence Larabee
Annual Land Application Field Summary Form
Site # LL
Field Name 30
Acres Permitted 15.70
County Pasquotank
Soil Series GrA
Soil Abbreviation Gertie
Crop 1 Corn (Grain)
Crop 1 PAN 117
Crop 2
Crop 2 PAN
Date Measurement
Volume
Applied
% Solids
Acres Used
DT/Ac.
Dry Tons
Source
Soil Condition
Precip.
Application
Method
P (Ibs/1000 g)
Total P
Volatilization
Mineralization
TKN
Ammonia
Nitrate-
Nitrite
Crop 1 Pan
(Ibs/Ac)
Crop 2 Pan
(Ibs/Ac)
Crop
3/9/2022 Gallons
70000
10.60%
15.70
1.971
30.941
Elizabeth City WTP
Moist
0
Surface
0.561
2.503
0.5
0
537
233
2.69
0.470
Crop 1
5/2/2022 Gallons
70000
5.04%
15.70
0.937
14.712
Elizabeth City WWTP
Moist
0
Surface
8.437
37.615
0.5
0.3
38300
8120
8.1
24.592
Crop 1
6/23/2022 Gallons
42000
5.04%
15.70
0.562
8.827
Elizabeth City WWTP
Dry
0
Surface
8.437
22.569
0.5
0.3
38300
8120
8.1
14.755
Crop 1
Total Volume Applied
182000
Total Dry Tons
54.480
Sum Total P
62.687
Crop 1 Total
39.817
0.000
Crop 2
Reported in Gallons
PAN
Total PAN
(Ibs./Ac.)
(Ibs./Ac.)
Arsenic
Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Current Year
0.058
0.058
0.635
0.074
0.058
0.002
0.058
0.058
0.058
2.626
Prior Year
0.024
0.004
0.617
0.045
0.083
0.001
0.018
0.025
0.018
1.633
Cumulative Total
0.0817
0.0617
1.2523
0.1195
0.1407
0.0027
0.0757
0.0827
0.0757
4.2595
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2/27/23
Signature of Land Applier Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.51 Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

Permit Numner WQ0002883
Facility Name City of Elizabeth City
Land Owner Lawrence Larabee
Annual Land Application Field Summary Form
Site # LL
Field Name 31
Acres Permitted 18.55
County Pasquotank
Soil Series GrA
Soil Abbreviation Gertie
Crop 1 Corn (Grain)
Crop 1 PAN 117
Crop 2
Crop 2 PAN
Date Measurement
Volume
Applied
% Solids
Acres Used
DT/Ac.
Dry Tons
Source
Soil Condition
Precip.
Application
Method
P (Ibs/1000 g)
Total P
Volatilization
Mineralization
TKN
Ammonia
Nitrate-
Nitrite
Crop 1 Pan
(Ibs/Ac)
Crop 2 Pan
(Ibs/Ac)
Crop
4/22/2022 Gallons
70000
10.60%
18.55
1.668
30.941
Elizabeth City WTP
Moist
0
Surface
0.561
2.118
0.5
0
537
233
2.69
0.398
Crop 1
5/3/2022 Gallons
84000
5.04%
18.55
0.952
17.654
Elizabeth City WWTP
Moist
0
Surface
8.437
38.203
0.5
0.3
38300
8120
8.1
24.977
Crop 1
6/20/2022 Gallons
42000
5.04%
18.55
0.476
8.827
Elizabeth City WWTP
Dry
0
Surface
8.437
19.102
0.5
0.3
38300
8120
8.1
12.488
Crop 1
Total Volume Applied
196000
Total Dry Tons
57.423
Sum Total P
59.423
Crop 1 Total
37.863
0.000
Crop 2
Reported in Gallons
PAN
Total PAN
(Ibs./Ac.)
(Ibs./Ac.)
Arsenic
Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Current Year
0.053
0.053
0.603
0.069
0.053
0.002
0.053
0.053
0.053
2.499
Prior Year
0.024
0.004
0.617
0.045
0.083
0.001
0.018
0.025
0.018
1.633
Cumulative Total
0.0770
0.0570
1.2200
0.1140
0.1360
0.0025
0.0710
0.0780
0.0710
4.1319
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2/27/23
Signature of Land Applier Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.51 Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

Permit Numner WQ0002883
Facility Name City of Elizabeth City
Land Owner Lawrence Larabee
Annual Land Application Field Summary Form
Site # LL
Field Name 32
Acres Permitted 12.79
County Pasquotank
Soil Series GrA
Soil Abbreviation Gertie
Crop 1 Corn (Grain)
Crop 1 PAN 117
Crop 2
Crop 2 PAN
Date Measurement
Volume
Applied
% Solids
Acres Used
DT/Ac.
Dry Tons
Source
Soil Condition
Precip.
Application
Method
P (Ibs/1000 g)
Total P
Volatilization
Mineralization
TKN
Ammonia
Nitrate-
Nitrite
Crop 1 Pan
(Ibs/Ac)
Crop 2 Pan
(Ibs/Ac)
Crop
5/4/2022 Gallons
84000
5.04%
12.79
1.380
17.654
Elizabeth City WWTP
Moist
0
Surface
8.437
55.408
0.5
0.3
38300
8120
8.1
36.225
Crop 1
5/19/2022 Gallons
49000
4.25%
12.79
0.679
8.684
Elizabeth City WTP
Moist
0
Surface
0.164
0.628
0.5
0
1920
1230
11.3
0.850
Crop 1
5/29/2022 Gallons
56000
4.25%
12.79
0.776
9.925
Elizabeth City WTP
Moist
0
Surface
1.164
5.096
0.5
0
1920
1230
11.3
0.972
Crop 1
6/22/2022 Gallons
35000
5.04%
12.79
0.575
7.356
Elizabeth City WWTP
Dry
0
Surface
8.437
23.087
0.5
0.3
38300
8120
8.1
15.094
Crop 1
Total Volume Applied
224000
Total Dry Tons
43.619
Sum Total P
84.218
Crop 1 Total
53.141
0.000
Crop 2
Reported in Gallons
PAN
Total PAN
(Ibs./Ac.)
(Ibs./Ac.)
Arsenic
Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Current Year
0.079
0.079
0.832
0.101
0.079
0.003
0.079
0.079
0.079
3.429
Prior Year
0.024
0.004
0.617
0.045
0.083
0.001
0.018
0.025
0.018
1.633
Cumulative Total
0.1030
0.0830
1.4493
0.1459
0.1620
0.0036
0.0970
0.1040
0.0970
5.0623
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2/27/23
Signature of Land Applier Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

Permit Numner WQ0002883
Facility Name City of Elizabeth City
Land Owner Lawrence Larabee
Annual Land Application Field Summary Form
Site # LL
Field Name 33
Acres Permitted 22.37
County Pasquotank
Soil Series PgA
Soil Abbreviation Pettigrew
Crop 1 Corn (Grain)
Crop 1 PAN 147
Crop 2 Wheat
Crop 2 PAN 50
Date Measurement
Volume
Applied
% Solids
Acres Used
DT/Ac.
Dry Tons
Source
Soil Condition
Precip.
Application
Method
P (Ibs/1000 g)
Total P
Volatilization
Mineralization
TKN
Ammonia
Nitrate-
Nitrite
Crop 1 Pan
(Ibs/Ac)
Crop 2 Pan
(Ibs/Ac)
Crop
5/5/2022 Gallons
42000
5.04%
22.37
0.395
8.827
Elizabeth City WWTP
Moist
0
Surface
8.437
15.840
0.5
0.3
38300
8120
8.1
10.356
Crop 1
5/19/2022 Gallons
49000
4.25%
22.37
0.388
8.684
Elizabeth City WTP
Moist
0
Surface
0.164
0.359
0.5
0
1920
1230
11.3
0.486
Crop 1
5/25/2022 Gallons
42000
5.04%
22.37
0.395
8.827
Elizabeth City WWTP
Moist
0
Surface
8.437
15.840
0.5
0.3
38300
8120
8.1
10.356
Crop 1
10/17/2022 Gallons
56000
7.60%
22.37
0.793
17.748
Elizabeth City WTP
Moist
0
Surface
0.062
0.155
0.5
0
317
1.32
3.31
0.006
Crop 2
11/21/2022 Gallons
49000
13.40%
22.37
1.224
27.380
Elizabeth City WTP
Moist
0
Surface
0.204
0.446
0.5
0
294
0.747
8.26
0.021
Crop 2
Total Volume Applied
238000
Total Dry Tons
71.466
Sum Total P
32.640
Crop 1 Total
21.198
0.027
Crop 2
Reported in Gallons
PAN
Total PAN
(Ibs./Ac.)
(Ibs./Ac.)
Arsenic
Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Current Year
0.028
0.028
0.332
0.037
0.028
0.001
0.028
0.028
0.028
1.380
Prior Year
0.128
0.023
2.597
0.067
0.284
0.005
0.095
0.158
0.113
8.127
Cumulative Total
0.1561
0.0511
2.9291
0.1039
0.3121
0.0059
0.1231
0.1861
0.1411
9.5072
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2/27/23
Signature of Land Applier Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.51 Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

Permit Numner WQ0002883
Facility Name City of Elizabeth City
Land Owner Lawrence Larabee
Annual Land Application Field Summary Form
Site # LL
Field Name 34
Acres Permitted 19.88
County Pasquotank
Soil Series PgA
Soil Abbreviation Pettigrew
Crop 1 Corn (Grain)
Crop 1 PAN 147
Crop 2 Wheat
Crop 2 PAN 50
Date Measurement
Volume
Applied
% Solids
Acres Used
DT/Ac.
Dry Tons
Source
Soil Condition
Precip.
Application
Method
P (Ibs/1000 g)
Total P
Volatilization
Mineralization
TKN
Ammonia
Nitrate-
Nitrite
Crop 1 Pan
(Ibs/Ac)
Crop 2 Pan
(Ibs/Ac)
Crop
5/6/2022 Gallons
35000
5.04%
19.88
0.370
7.356
Elizabeth City WWTP
Dry
0
Surface
8.437
14.853
0.5
0.3
38300
8120
8.1
9.711
Crop 1
5/23/2022 Gallons
35000
5.04%
19.88
0.370
7.356
Elizabeth City WWTP
Dry
0
Surface
8.437
14.853
0.5
0.3
38300
8120
8.1
9.711
Crop 1
6/13/2022 Gallons
63000
5.04%
19.88
0.666
13.241
Elizabeth City WWTP
Dry
0
Surface
8.437
26.735
0.5
0.3
38300
8120
8.1
17.479
Crop 1
10/18/2022 Gallons
56000
7.60%
19.88
0.893
17.748
Elizabeth City WTP
Moist
0
Surface
0.062
0.175
0.5
0
317
1.32
3.31
0.007
Crop 2
11/22/2022 Gallons
49000
13.40%
19.88
1.377
27.380
Elizabeth City WTP
Moist
0
Surface
0.204
0.502
0.5
0
294
0.747
8.26
0.024
Crop 2
Total Volume Applied
238000
Total Dry Tons
73.080
Sum Total P
57.118
Crop 1 Total
36.901
0.031
Crop 2
Reported in Gallons
PAN
Total PAN
(Ibs./Ac.)
(Ibs./Ac.)
Arsenic
Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Current Year
0.051
0.051
0.593
0.067
0.051
0.002
0.051
0.051
0.051
2.460
Prior Year
0.140
0.025
2.697
0.104
0.296
0.006
0.101
0.172
0.125
8.436
Cumulative Total
0.1914
0.0764
3.2900
0.1711
0.3474
0.0078
0.1524
0.2234
0.1764
10.8964
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2/27/23
Signature of Land Applier Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

Permit Numner WQ0002883
Facility Name City of Elizabeth City
Land Owner Lawrence Larabee
Annual Land Application Field Summary Form
Site # LL
Field Name 35
Acres Permitted 20.26
County Pasquotank
Soil Series PgA
Soil Abbreviation Pettigrew
Crop 1 Corn (Grain)
Crop 1 PAN 147
Crop 2 Wheat
Crop 2 PAN 50
Date Measurement
Volume
Applied
% Solids
Acres Used
DT/Ac.
Dry Tons
Source
Soil Condition
Precip.
Application
Method
P (Ibs/1000 g)
Total P
Volatilization
Mineralization
TKN
Ammonia
Nitrate-
Nitrite
Crop 1 Pan
(Ibs/Ac)
Crop 2 Pan
(Ibs/Ac)
Crop
3/11/2022 Gallons
70000
10.60%
20.26
1.527
30.941
Elizabeth City WTP
Moist
0
Surface
0.561
1.940
0.5
0
537
233
2.69
0.364
Crop 1
5/9/2022 Gallons
56000
5.04%
20.26
0.581
11.769
Elizabeth City WWTP
Dry
0
Surface
8.437
23.319
0.5
0.3
38300
8120
8.1
15.246
Crop 1
6/14/2022 Gallons
42000
5.04%
20.26
0.436
8.827
Elizabeth City WWTP
Dry
0
Surface
8.437
17.489
0.5
0.3
38300
8120
8.1
11.434
Crop 1
10/19/2022 Gallons
42000
7.60%
20.26
0.657
13.311
Elizabeth City WTP
Moist
0
Surface
0.062
0.129
0.5
0
317
1.32
3.31
0.005
Crop 2
11/23/2022 Gallons
49000
13.40%
20.26
1.351
27.380
Elizabeth City WTP
Moist
0
Surface
0.204
0.492
0.5
0
294
0.747
8.26
0.023
Crop 2
Total Volume Applied
259000
Total Dry Tons
92.229
Sum Total P
43.369
Crop 1 Total
27.044
0.029
Crop 2
Reported in Gallons
PAN
Total PAN
(Ibs./Ac.)
(Ibs./Ac.)
Arsenic
Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Current Year
0.054
0.054
0.445
0.065
0.054
0.002
0.054
0.054
0.054
1.795
Prior Year
0.131
0.025
2.872
0.108
0.303
0.006
0.096
0.166
0.115
9.026
Cumulative Total
0.1847
0.0787
3.3174
0.1731
0.3567
0.0079
0.1497
0.2197
0.1687
10.8215
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2/27/23
Signature of Land Applier Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

Permit Numner WQ0002883
Facility Name City of Elizabeth City
Land Owner Lawrence Larabee
Annual Land Application Field Summary Form
Site # LL
Field Name 36
Acres Permitted 20.31
County Pasquotank
Soil Series PgA
Soil Abbreviation Pettigrew
Crop 1 Corn (Grain)
Crop 1 PAN 147
Crop 2 Wheat
Crop 2 PAN 50
Date Measurement
Volume
Applied
% Solids
Acres Used
DT/Ac.
Dry Tons
Source
Soil Condition
Precip.
Application
Method
P (Ibs/1000 g)
Total P
Volatilization
Mineralization
TKN
Ammonia
Nitrate-
Nitrite
Crop 1 Pan
(Ibs/Ac)
Crop 2 Pan
(Ibs/Ac)
Crop
5/10/2022 Gallons
42000
5.04%
20.31
0.435
8.827
Elizabeth City WWTP
Dry
0
Surface
8.437
17.446
0.5
0.3
38300
8120
8.1
11.406
Crop 1
5/13/2022 Gallons
35000
5.04%
20.31
0.362
7.356
Elizabeth City WWTP
Dry
0
Surface
8.437
14.539
0.5
0.3
38300
8120
8.1
9.505
Crop 1
5/24/2022 Gallons
21000
5.04%
20.31
0.217
4.414
Elizabeth City WWTP
Dry
0
Surface
8.437
8.723
0.5
0.3
38300
8120
8.1
5.703
Crop 1
6/21/2022 Gallons
42000
5.04%
20.31
0.435
8.827
Elizabeth City WWTP
Dry
0
Surface
8.437
17.446
0.5
0.3
38300
8120
8.1
11.406
Crop 1
10/27/2022 Gallons
49000
7.60%
20.31
0.765
15.529
Elizabeth City WTP
Moist
0
Surface
0.062
0.150
0.5
0
317
1.32
3.31
0.006
Crop 2
Total Volume Applied
189000
Total Dry Tons
44.953
Sum Total P
58.304
Crop 1 Total
38.021
0.006
Crop 2
Reported in Gallons
PAN
Total PAN
(Ibs./Ac.)
(Ibs./Ac.)
Arsenic
Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Current Year
0.043
0.043
0.601
0.059
0.043
0.001
0.043
0.043
0.043
2.525
Prior Year
0.121
0.025
3.169
0.12
0.318
0.006
0.091
0.161
0.103
10.025
Cumulative Total
0.1642
0.0682
3.7703
0.1794
0.3612
0.0074
0.1342
0.2042
0.1462
12.5503
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
112!12 jaw
2/27/23
Signature of Land Applier Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

Permit Numner WQ0002883
Facility Name City of Elizabeth City
Land Owner Lawrence Larabee
Annual Land Application Field Summary Form
Site # LL
Field Name 37
Acres Permitted 18.33
County Pasquotank
Soil Series PgA
Soil Abbreviation Pettigrew
Crop 1 Corn (Grain)
Crop 1 PAN 147
Crop 2 Wheat
Crop 2 PAN 50
Date Measurement
Volume
Applied
% Solids
Acres Used
DT/Ac.
Dry Tons
Source
Soil Condition
Precip.
Application
Method
P (Ibs/1000 g)
Total P
Volatilization
Mineralization
TKN
Ammonia
Nitrate-
Nitrite
Crop 1 Pan
(Ibs/Ac)
Crop 2 Pan
(Ibs/Ac)
Crop
5/11/2022 Gallons
21000
5.04%
18.33
0.241
4.414
Elizabeth City WWTP
Dry
0
Surface
8.437
9.665
0.5
0.3
38300
8120
8.1
6.319
Crop 1
5/12/2022 Gallons
42000
5.04%
18.33
0.482
8.827
Elizabeth City WWTP
Dry
0
Surface
8.437
19.331
0.5
0.3
38300
8120
8.1
12.638
Crop 1
6/24/2022 Gallons
28000
5.04%
18.33
0.321
5.885
Elizabeth City WWTP
Dry
0
Surface
8.437
12.887
0.5
0.3
38300
8120
8.1
8.425
Crop 1
10/20/2022 Gallons
35000
7.60%
18.33
0.605
11.092
Elizabeth City WTP
Moist
0
Surface
0.062
0.118
0.5
0
317
1.32
3.31
0.005
Crop 2
Total Volume Applied
126000
Total Dry Tons
30.217
Sum Total P
42.002
Crop 1 Total
27.383
0.005
Crop 2
Reported in Gallons
PAN
Total PAN
(Ibs./Ac.)
(Ibs./Ac.)
Arsenic
Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Current Year
0.031
0.031
0.433
0.043
0.031
0.001
0.031
0.031
0.031
1.819
Prior Year
0.119
0.025
3.085
0.113
0.312
0.006
0.900
0.157
0.101
9.750
Cumulative Total
0.1505
0.0565
3.5184
0.1561
0.3435
0.0070
0.9315
0.1885
0.1325
11.5691
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2/27/23
Signature of Land Applier Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

Permit Numner
WQ0002883
Facility Name
City of Elizabeth City
Land Owner
W.B. Bateman
Annual Land Application Field Summary Form
Site # W B
Field Name 26
Acres Permitted 6.92
County Pasquotank
Soil Series Hyde
Soil Abbreviation HyA
Crop 1 Corn (Grain)
Crop 1 PAN 169
Crop 2
Crop 2 PAN
Date Measurement
Volume
Applied
% Solids
Acres Used
DT/Ac.
Dry Tons
Source
Soil Condition
Precip.
Application
Method
P (Ibs/1000 g)
Total P
Volatilization
Mineralization
TKN
Ammonia
Nitrate-
Nitrite
Crop 1 Pan
(Ibs/Ac)
Crop 2 Pan
(Ibs/Ac)
Crop
3/18/2022 Gallons
35000
10.60%
6.92
2.236
15.471
Elizabeth City WTP
Moist
0
Surface
0.561
2.839
0.5
0
537
233
2.69
0.533
Crop 1
4/12/2022 Gallons
49000
5.04%
6.92
1.488
10.298
Elizabeth City WWTP
Moist
0
Surface
8.437
59.738
0.5
0.3
38300
8120
8.1
39.056
Crop 1
5/17/2022 Gallons
35000
4.25%
6.92
0.896
6.203
Elizabeth City WTP
Moist
0
Surface
0.164
0.829
0.5
0
1920
1230
11.3
1.123
Crop 1
Total Volume Applied
119000
Total Dry Tons
31.972
Sum Total P
63.407
Crop 1 Total
40.712
0.000
Crop 2
Reported in Gallons
PAN
Total PAN
(Ibs./Ac.)
(Ibs./Ac.)
Arsenic
Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Current Year
0.077
0.077
0.650
0.094
0.077
0.002
0.077
0.077
0.077
2.627
Prior Year
0.050
0.015
2.668
0.125
0.327
0.011
0.093
0.105
0.065
5.928
Cumulative Total
0.1271
0.0921
3.3184
0.2187
0.4041
0.0135
0.1701
0.1821
0.1421
8.5548
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2/27/23
Signature of Land Applier Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

Permit Numner WQ0002883
Facility Name City of Elizabeth City
Land Owner W.B. Bateman
Annual Land Application Field Summary Form
Site # W B
Field Name 27
Acres Permitted 8.88
County Pasquotank
Soil Series Hyde
Soil Abbreviation HyA
Crop 1 Corn (Grain)
Crop 1 PAN 169
Crop 2
Crop 2 PAN
Date Measurement
Volume
Applied
% Solids
Acres Used
DT/Ac.
Dry Tons
Source
Soil Condition
Precip.
Application
Method
P (Ibs/1000 g)
Total P
Volatilization
Mineralization
TKN
Ammonia
Nitrate-
Nitrite
Crop 1 Pan
(Ibs/Ac)
Crop 2 Pan
(Ibs/Ac)
Crop
3/17/2022 Gallons
35000
10.60%
8.88
1.742
15.471
Elizabeth City WTP
Moist
0
Surface
0.561
2.213
0.5
0
537
233
2.69
0.415
Crop 1
4/11/2022 Gallons
35000
5.04%
8.88
0.828
7.356
Elizabeth City WWTP
Moist
0
Surface
8.437
33.252
0.5
0.3
38300
8120
8.1
21.740
Crop 1
5/16/2022 Gallons
63000
4.25%
8.88
1.257
11.165
Elizabeth City WTP
Moist
0
Surface
0.164
1.163
0.5
0
1920
1230
11.3
1.575
Crop 1
6/9/2022 Gallons
28000
5.04%
8.88
0.663
5.885
Elizabeth City WWTP
Dry
0
Surface
8.437
26.602
0.5
0.3
38300
8120
8.1
17.392
Crop 1
Total Volume Applied
161000
Total Dry Tons
39.876
Sum Total P
63.229
Crop 1 Total
41.122
0.000
Crop 2
Reported in Gallons
PAN
Total PAN
(Ibs./Ac.)
(Ibs./Ac.)
Arsenic
Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Current Year
0.079
0.079
0.654
0.096
0.079
0.003
0.079
0.079
0.079
2.634
Prior Year
0.050
0.015
2.668
0.125
0.327
0.011
0.093
0.105
0.065
5.928
Cumulative Total
0.1294
0.0944
3.3218
0.2211
0.4064
0.0136
0.1724
0.1844
0.1444
8.5621
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2/27/23
Signature of Land Applier Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

Permit Numner WQ0002883
Facility Name City of Elizabeth City
Land Owner W.B. Bateman
Annual Land Application Field Summary Form
Site # W B
Field Name 28
Acres Permitted 9.60
County Pasquotank
Soil Series Hyde
Soil Abbreviation HyA
Crop 1 Corn (Grain)
Crop 1 PAN 169
Crop 2 Wheat
Crop 2 PAN 50
Date Measurement
Volume
Applied
% Solids
Acres Used
DT/Ac.
Dry Tons
Source
Soil Condition
Precip.
Application
Method
P (Ibs/1000 g)
Total P
Volatilization
Mineralization
TKN
Ammonia
Nitrate-
Nitrite
Crop 1 Pan
(Ibs/Ac)
Crop 2 Pan
(Ibs/Ac)
Crop
4/8/2022 Gallons
35000
5.04%
9.60
0.766
7.356
Elizabeth City WWTP
Moist
0
Surface
8.437
30.758
0.5
0.3
38300
8120
8.1
20.109
Crop 1
4/25/2022 Gallons
42000
5.04%
9.60
0.919
8.827
Elizabeth City WWTP
Moist
0
Surface
8.437
36.910
0.5
0.3
38300
8120
8.1
24.131
Crop 1
5/11/2022 Gallons
21000
4.25%
9.60
0.388
3.722
Elizabeth City WTP
Moist
0
Surface
0.164
0.359
0.5
0
1920
1230
11.3
0.486
Crop 1
6/8/2022 Gallons
91000
5.04%
9.60
1.992
19.125
Elizabeth City WWTP
Dry
0
Surface
8.437
79.971
0.5
0.3
38300
8120
8.1
52.284
Crop 1
10/14/2022 Gallons
42000
7.60%
9.60
1.387
13.311
Elizabeth City WTP
Moist
0
Surface
0.062
0.271
0.5
0
317
1.32
3.31
0.011
Crop 2
10/25/2022 Gallons
35000
7.60%
9.60
1.155
11.092
Elizabeth City WTP
Moist
0
Surface
0.062
0.226
0.5
0
317
1.32
3.31
0.009
Crop 2
Total Volume Applied
266000
Total Dry Tons
63.433
Sum Total P
148.495
Crop 1 Total
97.010
0.020
Crop 2
Reported in Gallons
PAN
Total PAN
(Ibs./Ac.)
(Ibs./Ac.)
Arsenic
Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Current Year
0.121
0.121
1.538
0.162
0.121
0.004
0.121
0.121
0.121
6.423
Prior Year
0.050
0.015
2.668
0.125
0.327
0.011
0.093
0.105
0.065
5.928
Cumulative Total
0.1712
0.1362
4.2061
0.2873
0.4482
0.0151
0.2142
0.2262
0.1862
12.3507
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2/27/23
Signature of Land Applier Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

Permit Numner WQ0002883
Facility Name City of Elizabeth City
Land Owner W.B. Bateman
Annual Land Application Field Summary Form
Site # W B
Field Name 29
Acres Permitted 10.53
County Pasquotank
Soil Series Hyde
Soil Abbreviation HyA
Crop 1 Corn (Grain)
Crop 1 PAN 169
Crop 2 Wheat
Crop 2 PAN 50
Date Measurement
Volume
Applied
% Solids
Acres Used
DT/Ac.
Dry Tons
Source
Soil Condition
Precip.
Application
Method
P (Ibs/1000 g)
Total P
Volatilization
Mineralization
TKN
Ammonia
Nitrate-
Nitrite
Crop 1 Pan
(Ibs/Ac)
Crop 2 Pan
(Ibs/Ac)
Crop
4/7/2022 Gallons
35000
5.04%
10.53
0.699
7.356
Elizabeth City WWTP
Moist
0
Surface
8.437
28.042
0.5
0.3
38300
8120
8.1
18.333
Crop 1
4/18/2022 Gallons
35000
5.04%
10.53
0.699
7.356
Elizabeth City WWTP
Moist
0
Surface
8.437
28.042
0.5
0.3
38300
8120
8.1
18.333
Crop 1
6/7/2022 Gallons
49000
5.04%
10.53
0.978
10.298
Elizabeth City WWTP
Dry
0
Surface
8.437
39.258
0.5
0.3
38300
8120
8.1
25.667
Crop 1
10/12/2022 Gallons
28000
3.990%
10.53
0.442
4.659
Elizabeth City WWTP
Moist
0
Surface
9.529
25.337
0.5
0.3
36500
4270
35.5
10.476
Crop 2
10/13/2022 Gallons
42000
7.60%
10.53
1.264
13.311
Elizabeth City WTP
Moist
0
Surface
0.062
0.247
0.5
0
317
1.32
3.31
0.010
Crop 2
10/24/2022 Gallons
49000
7.60%
10.53
1.475
15.529
Elizabeth City WTP
Moist
0
Surface
0.062
0.289
0.5
0
317
1.32
3.31
0.012
Crop 2
Total Volume Applied
238000
Total Dry Tons
58.508
Sum Total P
121.214
Crop 1 Total
62.333
10.498
Crop 2
Reported in Gallons
PAN
Total PAN
(Ibs./Ac.)
(Ibs./Ac.)
Arsenic
Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Current Year
0.102
0.092
1.238
0.127
0.095
0.003
0.092
0.093
0.092
5.089
Prior Year
0.050
0.015
2.668
0.125
0.327
0.011
0.093
0.105
0.065
5.928
Cumulative Total
0.1523
0.1067
3.9059
0.2524
0.4221
0.0144
0.1847
0.1978
0.1567
11.0174
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2/27/23
Signature of Land Applier Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

Permit Numner WQ0002883
Facility Name City of Elizabeth City
Land Owner W.B. Bateman
Annual Land Application Field Summary Form
Site # W B
Field Name 30
Acres Permitted 11.34
County Pasquotank
Soil Series Cape Lookout
Soil Abbreviation CfA
Crop 1 Soybeans Full Season Crop 2
Crop 1 PAN 177 Crop 2 PAN
Date Measurement
Volume
Applied
% Solids
Acres Used
DT/Ac.
Dry Tons
Source
Soil Condition
Precip.
Application
Method
P (Ibs/1000 g)
Total P
Volatilization
Mineralization
TKN
Ammonia
Nitrate-
Nitrite
Crop 1 Pan
(Ibs/Ac)
Crop 2 Pan
(Ibs/Ac)
Crop
3/8/2022 Gallons
42000
10.60%
10.34
1.795
18.565
Elizabeth City WTP
Moist
0
Surface
0.561
2.280
0.5
0
537
233
2.69
0.428
Crop 1
4/5/2022 Gallons
28000
5.04%
11.34
0.519
5.885
Elizabeth City WWTP
Moist
0
Surface
8.437
20.831
0.5
0.3
38300
8120
8.1
13.619
Crop 1
4/15/2022 Gallons
28000
5.04%
11.34
0.519
5.885
Elizabeth City WWTP
Moist
0
Surface
8.437
20.831
0.5
0.3
38300
8120
8.1
13.619
Crop 1
4/27/2022 Gallons
42000
5.04%
11.34
0.778
8.827
Elizabeth City WWTP
Moist
0
Surface
8.437
31.246
0.5
0.3
38300
8120
8.1
20.428
Crop 1
5/27/2022 Gallons
28000
5.04%
11.34
0.519
5.885
Elizabeth City WWTP
Dry
0
Surface
8.437
20.831
0.5
0.3
38300
8120
8.1
13.619
Crop 1
Total Volume Applied
168000
Total Dry Tons
45.046
Sum Total P
96.019
Crop 1 Total
61.713
0.000
Crop 2
Reported in Gallons
PAN
Total PAN
(Ibs./Ac.)
(Ibs./Ac.)
Arsenic
Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Current Year
0.076
0.076
0.976
0.103
0.076
0.002
0.076
0.076
0.076
4.077
Prior Year
0.050
0.015
2.668
0.125
0.327
0.011
0.093
0.105
0.065
5.928
Cumulative Total
0.1265
0.0915
3.6441
0.2276
0.4035
0.0131
0.1695
0.1815
0.1415
10.0054
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2/27/23
Signature of Land Applier Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

Permit Numner WQ0002883
Facility Name City of Elizabeth City
Land Owner W.B. Bateman
Annual Land Application Field Summary Form
Site # W B
Field Name 31
Acres Permitted 11.79
County Pasquotank
Soil Series Cape Lookout
Soil Abbreviation CfA
Crop 1 Soybeans Full Season Crop 2
Crop 1 PAN 177 Crop 2 PAN
Date Measurement
Volume
Applied
% Solids
Acres Used
DT/Ac.
Dry Tons
Source
Soil Condition
Precip.
Application
Method
P (Ibs/1000 g)
Total P
Volatilization
Mineralization
TKN
Ammonia
Nitrate-
Nitrite
Crop 1 Pan
(Ibs/Ac)
Crop 2 Pan
(Ibs/Ac)
Crop
3/7/2022 Gallons
42000
10.60%
11.79
1.575
18.565
Elizabeth City WTP
Moist
0
Surface
0.561
2.000
0.5
0
537
233
2.69
0.375
Crop 1
4/4/2022 Galons
42000
5.04%
11.79
0.749
8.827
Elizabeth City WWTP
Moist
0
Surface
8.437
30.054
0.5
0.3
38300
8120
8.1
19.649
Crop 1
4/14/2022 Gallons
42000
5.04%
11.79
0.749
8.827
Elizabeth City WWTP
Moist
0
Surface
8.437
30.054
0.5
0.3
38300
8120
8.1
19.649
Crop 1
4/26/2022 Gallons
42000
5.04%
11.79
0.749
8.827
Elizabeth City WWTP
Moist
0
Surface
8.437
30.054
0.5
0.3
38300
8120
8.1
19.649
Crop 1
5/26/2022 Gallons
42000
5.04%
11.79
0.749
8.827
Elizabeth City WWTP
Dry
0
Surface
8.437
30.054
0.5
0.3
38300
8120
8.1
19.649
Crop 1
Total Volume Applied
210000
Total Dry Tons
53.873
Sum Total P
122.215
Crop 1 Total
78.970
0.000
Crop 2
Reported in Gallons
PAN
Total PAN
(Ibs./Ac.)
(Ibs./Ac.)
Arsenic
Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Current Year
0.093
0.093
1.247
0.127
0.093
0.003
0.093
0.093
0.093
5.224
Prior Year
0.050
0.015
2.668
0.125
0.327
0.011
0.093
0.105
0.065
5.928
Cumulative Total
0.1431
0.1081
3.9148
0.2516
0.4201
0.0136
0.1861
0.1981
0.1581
11.1521
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2/27/23
Signature of Land Applier Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

Permit Numner WQ0002883
Facility Name City of Elizabeth City
Land Owner W.B. Bateman
Annual Land Application Field Summary Form
Site # W B
Field Name 82
Acres Permitted 11.53
County Pasquotank
Soil Series Wasda-Conaby Complex
Soil Abbreviation WcA
Crop 1 Soybeans Full Season Crop 2
Crop 1 PAN 174 Crop 2 PAN
Date Measurement
Volume
Applied
% Solids
Acres Used
DT/Ac.
Dry Tons
Source
Soil Condition
Precip.
Application
Method
P (Ibs/1000 g)
Total P
Volatilization
Mineralization
TKN
Ammonia
Nitrate-
Nitrite
Crop 1 Pan
(Ibs/Ac)
Crop 2 Pan
(Ibs/Ac)
Crop
4/11/2022 Gallons
70000
10.60%
11.53
2.684
30.941
Elizabeth City WTP
Moist
0
Surface
0.561
3.408
0.5
0
537
233
2.69
0.640
Crop 1
4/19/2022 Gallons
35000
10.60%
11.53
1.342
15.471
Elizabeth City WTP
Moist
0
Surface
0.561
1.704
0.5
0
537
233
2.69
0.320
Crop 1
5/17/2022 Gallons
63000
4.25%
11.53
0.968
11.165
Elizabeth City WTP
Moist
0
Surface
0.164
0.896
0.5
0
1920
1230
11.3
1.213
Crop 1
Total Volume Applied
168000
Total Dry Tons
57.577
Sum Total P
6.008
Crop 1 Total
2.173
0.000
Crop 2
Reported in Gallons
PAN
Total PAN
(Ibs./Ac.)
(Ibs./Ac.)
Arsenic
Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Current Year
0.056
0.056
0.056
0.056
0.056
0.002
0.056
0.056
0.056
0.056
Prior Year
0.115
0.06
4.41
0.234
0.767
0.013
0.207
0.223
0.178
10.302
Cumulative Total
0.1713
0.1163
4.4663
0.2903
0.8233
0.0151
0.2633
0.2793
0.2343
10.3583
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2/27/23
Signature of Land Applier Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

Permit Numner WQ0002883
Facility Name City of Elizabeth City
Land Owner W.B. Bateman
Annual Land Application Field Summary Form
Site # W B
Field Name 83
Acres Permitted 11.59
County Pasquotank
Soil Series Wasda-Conaby Complex
Soil Abbreviation WcA
Crop 1 Soybeans Full Season Crop 2
Crop 1 PAN 174 Crop 2 PAN
Date Measurement
Volume
Applied
% Solids
Acres Used
DT/Ac.
Dry Tons
Source
Soil Condition
Precip.
Application
Method
P (Ibs/1000 g)
Total P Volatilization Mineralization TKN
Nitrate-
Ammonia Nitrite
Crop 1 Pan
(Ibs/Ac)
Crop 2 Pan
(Ibs/Ac)
Crop
4/20/2022 Gallons
77000
10.60%
11.59
2.937
34.036
Elizabeth City WTP
Moist
0
Surface
0.561
3.730 0.5 0 537
233 2.69
0.700
Crop 1
5/18/2022 Gallons
84000
4.25%
11.59
1.284
14.887
Elizabeth City WTP
Moist
0
Surface
0.164
1.188 0.5 0 1920
1230 11.3
1.609
Crop 1
Total Volume Applied
161000
Total Dry Tons
48.922
Sum Total P
4.918
Crop 1 Total
2.309
0.000
Crop 2
Reported in Gallons
PAN
Total PAN
(Ibs./Ac.)
(Ibs./Ac.)
Arsenic
Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Current Year
0.052
0.052
0.052
0.052
0.052
0.002
0.052
0.052
0.052
0.052
Prior Year
0.115
0.06
4.41
0.234
0.767
0.013
0.207
0.223
0.178
10.302
Cumulative Total
0.1671
0.1121
4.4621
0.2861
0.8191
0.0150
0.2591
0.2751
0.2301
10.3541
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2/27/23
Signature of Land Applier Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

Permit Numner WQ0002883
Facility Name City of Elizabeth City
Land Owner W.B. Bateman
Annual Land Application Field Summary Form
Site # W B
Field Name 84
Acres Permitted 11.47
County Pasquotank
Soil Series Wasda-Conaby Complex
Soil Abbreviation WcA
Crop 1 Soybeans Full Season Crop 2
Crop 1 PAN 174 Crop 2 PAN
Date Measurement
Volume
Applied
% Solids
Acres Used
DT/Ac.
Dry Tons
Source
Soil Condition
Precip.
Application
Method
P (Ibs/1000 g)
Total P
Volatilization
Mineralization
TKN
Ammonia
Nitrate-
Nitrite
Crop 1 Pan
(Ibs/Ac)
Crop 2 Pan
(Ibs/Ac)
Crop
4/13/2022 Gallons
28000
10.60%
11.47
1.079
12.377
Elizabeth City WTP
Moist
0
Surface
0.561
1.370
0.5
0
537
233
2.69
0.257
Crop 1
4/21/2022 Gallons
28000
10.60%
11.47
1.079
12.377
Elizabeth City WTP
Moist
0
Surface
0.561
1.370
0.5
0
537
233
2.69
0.257
Crop 1
5/20/2022 Gallons
77000
4.25%
11.47
1.190
13.646
Elizabeth City WTP
Moist
0
Surface
0.164
1.100
0.5
0
1920
1230
11.3
1.490
Crop 1
Total Volume Applied
133000
Total Dry Tons
38.399
Sum Total P
3.841
Crop 1 Total
2.005
0.000
Crop 2
Reported in Gallons
PAN
Total PAN
(Ibs./Ac.)
(Ibs./Ac.)
Arsenic
Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Current Year
0.043
0.043
0.043
0.043
0.043
0.002
0.043
0.043
0.043
0.043
Prior Year
0.115
0.06
4.41
0.234
0.767
0.013
0.207
0.223
0.178
10.302
Cumulative Total
0.1580
0.1030
4.4530
0.2770
0.8100
0.0147
0.2500
0.2660
0.2210
10.3450
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2/27/23
Signature of Land Applier Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

City of Elizabeth City
2022 Class B Annual Report
WQ0002883
Pathogen & Vector Reduction Forms
Elizabeth City WWTP - Lime
Stabilization Sheets

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Elizabeth City
WWTP Name: Elizabeth City WWTP
WQ Permit Number: WQ0002883
NPDES Number: NCO025011
Monitoring Period: From l/l/2022 To 3/31/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) L,
I Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑ I
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density ❑
I Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
I Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in
in Sludge
Pathogen Density
Number of
Excee-
dences
Frequency
of Analysis
y
Sample
Type
a ytri
Tech -
ni ue
Minimum
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC
02T .1107)- Please indicate alternative
Derformed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) J Alt. 4 (Spec. Oz uptake)
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization 0
Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable)
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please nott:
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
,,:bjk,eA2 &LA —�.- , f i h `,r,,,0e J- J. Bryan Smith, President
Preparer Name and Title (type or rint) Land Applier Name and Title (if applicable)(type or print
2/23/23
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

City of Elizabeth City W WTP I
I
I
I
I
City of Elizabeth City W WTP
Monitoring Sheet for Lime Stabilization
I
Monitoring Sheet for Lime Stabilization
Alternative 2 PSRP
NPDES Permit # NCO025011
NPDES Permit # NCO025011
Class B Biosolids
Residuals Permit # WQ0002883
Residuals Permit # WQ0002883
Dates: 01/1/2022
thru: 01/31/2022
40 CFR Part 503 Subpart D 503.30-503.33
40 CFR Part 503 Subpart D 503.30-503.33
Initial pH
pH After 2 Hours
pH After 24 Hours
Tank
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp ("
c)
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp ("
c)
Shipped
to SST
#lor2
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp ("
c)
Stabilization
Amount
(Gallons)
Sheet Total (Gallons):
0

City of Elizabeth City WWiP I
I
I
I
I
City of Elizabeth City WWiP
Monitoring Sheet for Lime Stabilization
I
Monitoring Sheet for Lime Stabilization
Alternative 2 PSRP
NPDES Permit# NCO025011
NPDES Permit# NCO025011
Class B Biosolids
Residuals Permit # WQ0002883
Residuals Permit # WQ0002883
Dates:
01 2022
thru:
2/28/20
2
40 CFR Part 503 Subpart D 503.30-503.33
40 CFR Part 503 Subpart D 503.30-503.33
Initial pH
pH After 2 Hours
pH After 24 Hours
Tank
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Shipped
to SST
#1or2
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Stabilization
Amount
(Gallons)
Sheet Total (Gallons):
0

City of Elizabeth City W WTP I
I
I
I
I
City of Elizabeth City W WTP
Monitoring Sheet for Lime Stabilization
I
Monitoring Sheet for Lime Stabilization
Alternative 2 PSRP
NPDES Permit# NCO025011
NPDES Permit # NCO025011
Class B Biosolids
Residuals Permit# WQ0002883
Residuals Permit# WQ0002883
Dates: 3/1/22
thru: 3/31/22
40 CFR Part 503 Subpart D 503.30-503.33
40 CFR Part 503 Subpart D 503.30-503.33
Initial pH
pH After 2 Hours
pH After 24 Hours
Tank
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Analyst
Date
Time
pH (s u)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Shipped
to SST
#1or2
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Stabilization
Amount
(Gallons)
2
JR
3/1/2022
1039
12.84
-0.21
12.81
18.3
JR
3/1/2022
1256
12.78
-0.21
12.57
18.1
1
JR
3/2/2022
1058
12.54
-0.18
12.36
19.1
20000
1
MR
3/1/2022
2132
12.67
-0.21
12.46
18.0
MR
3/1/2022
2332
12.64
-0.21
12.43
18.3
1
MR
3/2/2022
2135
12.63
-0.24
12.39
17.3
20000
2
MR
3/2/2022
2130
12.28
-0.24
12.04
16.8
MR
3/2/2022
2330
12.38
-0.24
12.14
17.2
1
DR
3/3/2022
2135
12.45
-0.21
12.24
18.91
20000
1
QS
3/3/2022
1845
12.62
-0.24
12.38
17.2
DR
3/2/20221
2045
12.53
-0.24
12.291
17.3
1
QS
3/4/2022
1925
12.49
-0.24
12.25
16.8
20000
2
QS
3/4/2022
1940
12.50
-0.27
12.23
16.4
QS
3/4/2022
2147
12.40
-0.27
12.13
16.3
1
QS
3/5/2022
1950
12.14
-0.21
11.93
18.7
20000
2
RT
1 3/7/2022
1740
12.42
-0.18
12.241
19.5
QS
3/7/2022
1940
12.38
-0.18
12.20
19.21
1
QS
1 3/8/2022
17451
12.28
-0.24
12.04
17.4
20000
1
QS
3/8/2022
0430
12.42
-0.18
12.24
19.0
QS
3/8/2022
0630
12.36
-0.21
12.15
18.3
1
DR
3/9/2022
0445
12.13
-0.18
11.95
19.2
20000
1
DR
3/10/2022
1915
12.60
-0.24
12.36
17.2
DR
3/10/2022
2115
12.62
-0.27
12.35
16.0
1
DR
3/11/2022
1915
12.53
-0.21
12.32
18.0
20000
2
DR
3/11/2022
2000
12.68
-0.27
12.41
16.4
DR
3/11/2022
2200
12.64
-0.24
12.41
17.1
1
QS
3/12/2022
2000
12.65
-0.33
12.32
14.6
20000
2
QS
3/14/2022
2230
12.65
-0.27
12.38
15.9
QS
3/15/2022
0030
12.67
-0.30
12.37
15.4
1
DR
3/15/2022
2230
12.55
-0.24
12.31
17.4
20000
1
QS
3/15/2022
0300
12.63
-0.27
12.36
15.9
QS
3/15/20221
0500
12.61
-0.27
12.34
16.1
2
DR
3/16/2022
0300
12.49
-0.24
12.25
17.7
20000
1
AE
3/17/2022
943
12.38
-0.15
12.23
20.0
SC
3/17/20221
1145
12.39
-0.12
12.27
20.8
2
RT
3/18/2022
943
12.33
-0.15
12.18
20.5
20000
2
AE
3/17/2022
0946
12.44
-0.15
12.29
19.51
SC
3/17/2022
1148
12.35
-0.12
12.23
20.8
2
RT
3/18/2022
0946
12.36
-0.12
12.24
21.11
20000
1
RT
3/20/2022
900
12.51
-0.21
12.30
18.9
RT
3/20/2022
1100
12.49
-0.18
12.31
19.3
2
RT
3/21/2022
900
12.42
-0.15
12.28
20.0
20000
2
RT
3/20/2022
900
12.52
-0.21
12.31
18.5
RT
3/20/2022
1100
12.46
-0.15
12.31
20.0
2
RT
3/21/2022
900
12.13
-0.12
12.01
21.1
20000
1
QS
3/22/2022
0700
12.11
-0.21
11.90
18.2
JR
3/22/2022
0900
12.08
-0.181
11.88
19.0
2
JR
3/22/2022
0739
11.85
-0.24
11.61
16.9
20000
2
SC
3/22/2022
730
12.66
-0.24
12.42
17.2
JR
3/22/2022
9301
12.56
-0.15
12.41
19.8
2
JR
3/22/2022
744
12.45
-0.12
12.33
16.8
20000
1
QS
3/27/2022
0050
12.51
-0.18
12.33
19.4
QS
3/27/2022
0250
12.50
-0.24
12.26
19.6
2
QS
3/28/2022
0100
12.58
-0.27
12.31
16.4
20000
2
QS
3/27/2022
100
12.42
-0.12
12.30
21.2
QS
3/27/2022
300
12.46
-0.12
12.34
20.91
2
QS
3/28/2022
130
12.47
-0.15
12.32
19.8
20000
2
QS
3/29/2022
2001
12.63
-0.24
12.39
17.0
QS
3/29/2022
400
12.63
-0.24
12.39
16.8
2
DR
3/30/2022
200
12.54
-0.21
12.33
18.4
20000
1
QS
3/29/2022
310
12.69
-0.27
12.42
16.0
QS
3/29/2022
510
12.64
-0.27
12.37
16.0
2
DR
3/30/2022
300
12.58
-0.27
12.311
16.9
20000
Sheet Total (Gallons):
420000

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Elizabeth City
WWTP Name: Elizabeth City WWTP
WQ Permit Number: WQ0002883
NPDES Number: NCO025011
Monitoring Period: From
4/l/2022 To 6/30/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑ I
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
I Process to Further Reduce Patho ens ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑ Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density ❑
I Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative
performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
I Air Drying ❑
I Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
g
Pathogen Density
Number of
Excee-
deuces
Frequency
of Analysis
y
Sample
Type
a ytr
Tech
niqut
Minimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
colifonn)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC
02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) ❑ jAlt.
2 (40-day bench) ❑
jAlt. 3 (30-day bench) ❑
lAlt. 4 (Spec. OZ uptake)
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization
jAlt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable)
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation)
INo vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please not(
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
,eke' ZjL-4�5
Preparer Name and Title (type br print)
Signature of Preparer* Date
J. Bryan Smith, President
Land Applier Name and Title (if applicable)(type or print
2/23/23
Signature of Land Applier (if applicable) Dat(
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

City of Elizabeth City W WTP I
I
I
City of Elizabeth City W WTP
Monitoring Sheet for Lime Stabilization
Monitoring Sheet for Lime Stabilization
Alternative 2 PSRP
NPDES Permit # NCO025011
NPDES Permit # NCO025011
Class B Biosolids
Residuals Permit # WQ0002883
Residuals Permit # WQ0002883
Dates: 4/1/2022
thru: 4/30/2022
40 CFR Part 503 Subpart D 503.30-503.33
40 CFR Part 503 Subpart D 503.30-503.33
Initial pH
pH After 2 Hours
pH After 24 Hours
Tank
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Shipped
to SST
#1or2
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Stabilization
Amount
(Gallons)
1
DR
4/1/2022
0030
12.52
-0.15
12.37
20.1
DR
4/1/2022
0230
12.52
0.15
12.37
20.1
1
JR
4/1/2022
0048
12.47
-0.15
12.32
19.6
20,000
2
DR
4/1/2022
100
12.53
-0.15
12.38
20.1
DR
4/1/2022
0300
12.52
-0.15
12.37
20.2
2
JR
4/1/2022
0048
12.38
-0.12
12.26
20.9
20,000
1
RT
4/4/2022
1000
12.59
-0.18
12.41
19.1
RT
4/4/2022
1200
12.56
-0.21
12.35
18.9
2
QS
4/5/2022
1000
12.28
-0.06
12.22
22.6
20,000
2
RT
4/4/2022
1000
12.61
-0.181
12.43
19.1
RT
4/4/20221
1200
12.53
-0.28
12.351
19.7
1
QS
4/5/2022
1200
12.35
-0.12
12.231
20.4
20,000
2
QS
4/6/2022
0905
12.49
-0.12
12.39
20.5
QS
4/6/2022
1105
12.39
-0.09
12.30
22.3
1
QS
4/7/2022
0905
12.21
-0.12
12.09
21.4
20,000
1
QS
4/6/2022
1150
12.42
-0.12
12.35
21.0
QS
4/6/2022
1350
12.46
-0.12
12.34
21.21
1
QS
4/7/2022
1150
12.46
-0.06
12.40
23.3
20,000
1
JS
4/11/2022
1153
12.61
-0.09
12.52
22.2
JS
4/11/2022
1353
12.56
-0.09
12.57
22.0
1
QS
4/12/2022
1245
12.41
-0.03
12.38
24.3
20,000
2
JS
4/11/2022
1328
12.51
-0.09
12.42
22.2
RT
4/11/2022
1528
12.44
-0.06
12.38
23.6
1
JS
4/12/2022
1340
12.20
-0.12
12.32
21.8
20,000
2
QS
4/13/2022
1350
12.45
-0.06
12.39
22.5
QS
4/13/2022
1450
12.40
-0.06
12.34
23.4
2
JS
4/14/2022
1250
12.18
0.00
12.18
24.61
20,000
1
QS
4/13/2022
1355
12.39
-0.06
12.33
23.0
QS
4/13/2022
1555
12.35
-0.06
12.29
23.3
1
JS
4/14/2022
1350
12.16
0.00
12.16
24.7
20,000
1
JS
4/15/2022
1145
12.59
-0.12
12.47
21.8
JS
4/15/2022
1345
12.55
-0.06
12.49
23.0
1
RT
4/16/2022
1145
12.51
-0.09
12.42
22.2
20,000
2
JS
4/15/2022
1142
12.55
-0.09
12.46
22.0
RT
4/15/2022
1642
12.47
-0.12
12.35
22.1
1
RT
4/16/2022
1442
12.34
-0.03
12.31
23.6
20,000
1
JR
4/18/2022
2137
12.50
-0.18
12.32
19.41
JR
4/19/2022
1228
12.49
-0.18
12.31
19.2
1
DR
4/20/2022
2130
12.51
-0.21
12.30
18.3
20,000
2
JR
4/18/2022
2139
12.54
-0.15
12.33
19.7
JR
4/19/2022
1225
12.35
-0.18
12.37
19.0
2
DR
4/20/2022
2130
12.50
-0.21
12.29
18.4
20,000
2
QS
4/21/2022
0905
12.48
-0.15
12.33
20.1
QS
4/21/2022
1105
12.45
-0.12
12.33
20.8
2
QS
4/22/2022
0905
12.36
-0.06
12.30
22.6
20,000
1
QS
4/21/2022
1055
12.47
-0.12
12.35
20.8
QS
4/21/2022
1255
12.36
-0.12
12.24
21.2
1
QS
4/22/2022
1100
12.04
-0.12
11.82
21.71
20,000
1
RT
4/23/2022
1015
12.37
-0.09
12.28
21.5
RT
4/23/2022
1215
12.31
-0.09
12.22
21.8
1
RT
4/24/2022
10151
12.13
-0.06
12.07
23.2
20,000
2
RT
4/23/2022
1015
12.37
-0.061
12.31
20.1
RT
4/23/2022
1215
12.36
-0.06
12.30
23.0
2
RT
4/24/2022
1015
12.17
0.03
12.20
25.5
20,000
2
JS
4/27/2022
0430
12.57
-0.08
12.48
22.0
JS
4/27/2022
0540
12.55
-0.09
12.46
22.41
2
JS
4/28/2022
0345
12.46
-0.09
12.37
22.1
20,000
1
JS
4/27/2022
0415
12.54
-0.09
12.43
22.21
JS
4/27/2022
0615
12.56
-0.09
12.47
22.1
1
JS
4/28/2022
0445
12.47
-0.12
12.35
21.2
20,000
2
JS
4/29/2022
0506
12.45
-0.15
12.30
20.1
QS
4/29/2022
0709
12.42
-0.12
12.30
21.2
2
JR
4/30/2022
0510
12.32
-0.03
12.29
23.5
20,000
1
JS
4/29/2022
0849
12.47
-0.15
12.32
20.0
QS
4/29/2022
0800
12.45
-0.12
12.33
20.8
1
JR
4/30/2022
0557
12.37
-0.12
12.29
21.4
20,000
Sheet Total (Gallons):
440000

City of Elizabeth City W WTP I
I
I
I
City of Elizabeth City W WiP
Monitoring Sheet for Lime Stabilization
I
Monitoring Sheet for Lime Stabilization
Alternative 2 PSRP
NPDES Permit # NCO025011
NPDES Permit # NCO025011
Class B Biosolids
Residuals Permit # WQ0002883
Residuals Permit # WQ0002883
Dates:
5/1/2022
thru:
5/31/202
40 CFR Part 503 Subpart D 503.30-503.33
40 CFR Part 503 Subpart D 503.30-503.33
Initial pH
pH After 2 Hours
pH After 24 Hours
Tank
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Shipped
to SST
#1or2
Analyst
Date
Time
pH (s u)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Stabilization
Amount
(Gallons)
1
QS
5/1/2022
805
12.50
-0.12
12.38
21.2
QS
5/1/2022
1005
12.43
-0.09
12.34
21.8
2
RT
5/2/2022
0855
12.84
-0.03
12.81
23.1
20,000
2
QS
5/2/2022
805
12.51
-0.09
12.42
21.6
QS
5/2/2022
1015
12.47
-0.09
12.38
22.2
1
RT
5/2/2022
928
12.37
-0.03
12.34
23.4
20,000
1
QS
5/4/2022
715
12.39
-0.06
12.33
23.4
QS
5/4/2022
0915
12.35
-0.03
12.32
23.9
1
JS
5/5/2022
1056
12.28
0.00
12.28
25.0
20,000
2
QS
5/4/2022
715
12.40
-0.06
12.34
23.41
QS
5/4/20221
0915
12.34
-0.03
12.31
24.2
2
JS
5/5/2022
1059
12.30
0.00
12.301
25.01
20,000
1
JS
5/6/2022
0148
12.30
-0.03
12.27
24.0
JS
5/6/2022
1300
12.33
-0.03
12.30
24.2
2
QS
5/7/2022
0950
12.35
0.00
12.35
24.6
20,000
2
JS
1 5/6/2022
1481
12.37
-0.061
12.31
23.2
JS
5/6/2022
1300
12.38
-0.03
12.351
24.1
2
1 QS
5/7/2022
955
12.33
0.00
12.33
25.3
20,000
1
JS
5/13/2022
1040
12.30
-0.03
12.27
24.0
JS
5/13/2022
1305
12.21
-0.06
12.23
23.0
1
JS
5/16/2022
1046
12.22
-0.06
12.16
23.3
20,000
2
JS
5/13/2022
1042
12.22
-0.03
12.17
26.0
JS
5/13/2022
1305
12.21
-0.09
12.12
22.0
2
JS
5/16/2022
1047
12.18
-0.06
12.12
23.0
20,000
2
QS
5/16/2022
1230
12.34
-0.03
12.31
24.3
QS
5/16/2022
1430
12.31
0.00
12.31
24.9
2
QS
5/17/2022
1230
12.19
0.00
12.19
25.0
20,000
1
DR
5/16/2022
1650
12.18
-0.03
12.15
24.6
DR
5/16/2022
1850
12.08
-0.06
12.02
23.6
2
DR
5/17/2022
1650
11.83
0.06
11.89
27.2
20,000
2
JER
5/19/2022
0709
12.48
-0.06
12.42
22.51
QS
5/19/2022
0910
12.22
-0.06
12.16
23.3
2
QS
5/20/2022
0720
12.24
0.00
12.24
25.01
20,000
1
QS
5/19/2022
950
12.26
-0.03
12.23
23.8
QS
5/19/2022
1150
12.24
-0.03
12.21
24.1
2
QS
5/20/2022
950
12.01
0.00
12.01
24.5
20,000
2
JS
5/21/2022
1300
12.20
0.03
12.23
26.7
JS
5/21/2022
1500
12.28
0.03
12.31
26.5
2
RT
5/22/2022
1300
12.02
0.09
12.11
27.5
20,000
1
JS
5/21/2022
1500
12.31
0.03
12.34
26.4
DR
5/21/2022
1700
12.05
0.09
12.14
28.7
2
RT
5/22/2022
1500
12.17
-0.09
12.26
27.7
20,000
2
QS
5/24/2022
855
12.32
-0.03
12.29
24.1
QS
5/24/2022
1055
12.21
-0.03
12.18
24.0
2
QS
5/25/2022
850
12.17
-0.03
12.14
23.6
20,000
1
QS
5/24/2022
1440
12.29
0.00
12.29
24.9
DR
5/24/2022
1640
12.11
-0.06
12.05
23.2
2
QS
5/25/2022
1400
12.03
-0.06
11.92
23.1
20,000
2
QS
5/26/2022
745
12.43
-0.03
12.40
23.6
QS
5/26/20221
945
12.21
-0.03
12.18
23.7
2
QS
5/27/2022
745
12.14
0.03
12.17
25.7
20,000
1
QS
5/26/2022
0825
12.53
-0.03
12.50
24.31
DR
5/26/2022
1525
12.53
0.00
12.53
25.7
1
QS
5/27/2022
1305
12.47
0.03
12.501
25.71
20,000
2
JS
5/29/2022
1111
12.13
-0.03
12.21
26.0
JS
5/29/2022
1320
12.18
0.03
12.16
26.5
1
RT
5/30/2022
1100
12.40
0.06
12.46
27.4
20,000
1
JS
5/29/2022
12051
12.14
0.00
12.14
26.6
JS
5/29/2022
1431
12.08
0.03
12.11
26.0
1
RT
5/30/2022
1105
12.37
0.09
12.46
28.4
20,000
Sheet Total (Gallons):
400000

City of Elizabeth City WWTP I
I
I
I
I
City of Elizabeth City W WTP
Monitoring Sheet for Lime Stabilization
I
Monitoring Sheet for Lime Stabilization
Alternative 2 PSRP
NPDES Permit # NCO025011
NPDES Permit # NCO025011
Class B Biosolids
Residuals Permit # WQ0002883
Residuals Permit # WQ0002883
Dates:
6-1-2022
thru:
6-30-202
40 CFR Part 503 Subpart D 503.30-503.33
40 CFR Part 503 Subpart D 503.30-503.33
Initial pH
pH After 2 Hours
pH After 24 Hours
Tank
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Shipped
to SST
#1or2
Analyst
Date
Time
pH (s u)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Stabilization
Amount
(Gallons)
1
QS
6/3/2022
1455
12.34
0.09
12.43
27.9
QS
6/3/2022
1655
12.31
0.09
12.40
28.0
1
QS
6/4/2022
1458
12.20
0.15
12.35
29.6
20,000
2
QS
6/3/2022
1500
12.31
0.12
12.43
28.8
QS
6/3/2022
1705
12.32
0.12
12.44
28.7
2
QS
6/4/2022
1505
12.30
0.12
12.42
29.0
20,000
1
DR
6-8-22
1230
12.04
0.03
12.07
26.7
DR
6/8/2022
1930
12.19
0.03
12.22
26.4
1
DR
6/9/2022
1730
11.92
0.09
12.01
28.51
20,000
2
DR
6/8/2022
12301
12.13
0.06
12.19
27.41
DR
6/8/2022
1930
12.241
0.03
12.27
26.3
2
DR
6/9/2022
1730
12.12
0.06
12.18
27.3
20,000
2
QS
6/11/2022
0755
12.32
0.03
12.35
25.7
QS
6/11/2022
1010
12.01
0.03
12.04
26.3
2
QS
6/12/2022
0800
11.43
0.06
11.49
27.3
20,000
1
QS
6/11/2022
905
12.07
0.06
12.13
26.5
QS
6/11/2022
1105
12.20
0.03
12.23
26.51
1
QS
6/12/2022
905
11.52
0.06
11.58
27.1
20,000
2
JS
6/13/2022
0300
12.23
0.03
12.26
25.6
JS
6/13/2022
0500
12.16
0.03
12.19
26.0
2
JS
6/14/2022
0301
12.03
0.09
12.12
28.2
20,000
1
JS
6/13/2022
0630
12.12
0.03
12.15
26.4
QS
6/13/2022
0840
12.00
0.06
12.06
26.6
1
QS
6/14/2022
0800
11.79
0.09
11.88
27.5
20,000
2
JS
6/15/2022
0545
12.14
0.03
12.17
26.2
RT
6/15/2022
0745
12.11
0.06
12.17
27.1
2
JS
6/16/2022
0847
12.20
0.09
12.29
27.5
20,000
1
RT
6/15/2022
1000
12.14
0.09
12.23
27.7
RT
6/15/2022
1200
12.12
0.09
12.21
28.1
1
QS
6/16/2022
1000
12.10
0.00
12.10
25.01
20,000
2
QS
6/21/2022
1805
12.03
0.06
12.09
27.41
JS
6/21/2022
2042
12.01
0.06
12.07
27.0
2
QS
6/23/2022
0030
12.04
0.06
12.10
27.0
20,000
1
JS
6/21/2022
2044
12.07
0.06
12.13
26.8
JS
6/21/2022
2300
12.00
0.06
12.06
26.8
1
QS
6/23/2022
140
12.04
0.06
12.10
27.2
20,000
1
DR
6/25/2022
1800
12.42
0.06
12.48
27.2
DR
6/25/2022
2000
12.14
0.03
12.17
26.2
1
SNC
6/26/2022
1800
12.12
0.06
12.18
26.9
20,000
2
DR
6/25/2022
1800
12.21
0.06
12.27
27.3
DR
6/25/2022
2000
12.21
0.00
12.21
25.8
2
SNC
6/26/2022
1800
12.18
0.06
12.24
27.0
20,000
1
SNC
6/29/2022
1130
12.41
0.06
12.47
27.0
SNC
6/29/2022
1330
12.38
0.06
12.44
27.0
1
JCS
6/30/2022
1338
12.30
0.09
12.34
28.3
20,000
2
SNC
6/29/2022
1130
12.07
0.06
12.13
27.0
SNC
6/29/2022
1330
12.05
0.06
12.11
27.2
2
JCS
6/30/2022
1338
12.09
0.12
12.21
28.9
20,000
Sheet Total (Gallons):
320000

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Elizabeth City WQ Permit Number: WQ0002883
WWTP Name: Elizabeth City WWTP
Monitoring Period: From 7/l/2022 To
NPDES Number: NCO025011
9/30/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A: Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑ Alt. C (Prior Testing)
A1t.D (No Prior Test) ElProcess
to Further Reduce Pathogengs
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic
Beta Ray ❑
Gamma Ray ❑
Pasteurization L-1
Class B:
jAlt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative
performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization 0 I
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number of'
Excee-
Excee-
Frequency
of Analysis
Sample
Type
a yt''
Tech
Tighe
Minimum
Geo. Mean
Maximum!
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC
02T .1107) - Please indicate alternative
performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench)
Alt. 3 (30-day bench)
Alt. 4 (Spec. OZ uptake)
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization El
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable)
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) _
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please not(
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
A41e.'o LCA AJ,L+ J. Bryan Smith, President
Preparer Name and Title (typb or print) Land Applier Name and Title (if applicable)(type or print
�� 2/23/23
Signature of Preparer* Date Signature of Land Applier (if applicable) Datf
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

City of Elizabeth City WWTP
Monitoring Sheet for Lime Stabilization
Alternative 2 PSRP
Class B Biosolids
Dates: 7-1-2022 thru: 7-31-2022
NPDES Permit # NCO025011
Residuals Permit # WQ0002883
40 CFR Part 503 Subpart D 503.30-503.33
City of Elizabeth City WWTP
Monitoring Sheet for Lime Stabilization
NPDES Permit # NCO025011
Residuals Permit # WQ0002883
40 CFR Part 503 Subpart D 503.30-503.33
Initial pH
pH After 2 Hours
pH After 24 Hours
Tank
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Shipped
to SST
#1or2
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Stabilization
Amount
(Gallons)
1
QS
7/3/2022
1140
12,34
0.09
12.43
28.2
CIS
7/3/2022
1345
12.29
0.12
12.41
28.9
2
CIS
7/4/2022
0749
12.28
0.12
12.40
28.6
20000
2
QS
7/3/2022
0618
12,48
0.06
12.54
26.8
CIS
7/3/2022
0818
12.43
0.06
12.49
27.1
2
CIS
7/4/2022
1140
12.23
0.12
12.35
28.4
20000
1
1S
7/6/2022
1714
12.36
0.12
12.49
28.5
1S
7/6/2022
1423
12.10
0.09
12.09
28.5
1
1S
7/7/2022
1731
12.03
0.12
12.15
28.7
20000
2
1S
7/6/2022
1714
12.04
0.12
12.16
28.6
1S
7/6/2022
1425
12.10
0.12
12.22
29.4
2
1S
7/7/2022
1733
12.08
0.12
12.20
28.71
20000
2
QS
7/13/2022
1415
12.39
0.09
12.48
22.9
CIS
7/13/2022
1615
12.53
0.06
12.59
27.8
2
CIS
7/14/2022
1415
12.35
0.09
12.44
28.0
20000
1
1R
7/14/2022
0651
12.33
0.09
12.42
27.6
1R
7/14/2022
0830
12.07
0.08
12.16
28.0
1
DR
7/20/2022
0630
12.27
0.09
12.36
28.4
20000
1
DR
7/19/2022
2045
12.271
0.00
12.27
25.2
DR
7/19/2022
2213
12.21
0.09
12.30
28.6
2
CIS
7/21/2022
2013
11.96
0.15
12.11
30.1
20000
2
QS
7/20/2022
1230
12.11
0.21
12.32
31.6
CIS
7/20/2022
1430
12.10
0.18
12.28
30.4
1
1S
7/23/2022
1230
11.91
0.24
12.15
32.6
20000
1
1S
7/22/2022
1915
12.01
0.15
12.16
30.5
1S
7/22/2022
2116
12.12
0.12
12.24
30.0
2
1S
7/24/2922
2120
11.95
0.18
12.13
31.5
20000
2
1S
7/22/2022
2117
12.19
0.12
12.31
29.2
1S
7/22/2022
0241
12.13
0.06
12.19
26.9
2
1R
7/25/2022
0036
12.24
0.15
12.39
30.2
20000
2
DR
7/25/2022
1716
12.23
0.15
12.38
30.7
DR
7/25/2022
1916
12.24
0.15
12.39
30.0
1
DR
7.25/2022
1716
12.24
0.12
12.36
29.71
20000
1
DR
7/25/2022
2000
11.92
0.15
12.07
30.5
DR
7/25/2022
2200
12.24
0.12
12.36
29.6
1
DR
7/30.2022
1718
12.19
0.12
12.31
29.2
20000
1
RT
7/29/2022
1123
12.20
0.18
12.38
31.2
RT
7/29/2022
1323
12.16
0.21
12.37
31.5
2
RT
7/30/2022
1109
11.63
0.21
11.84
32.3
20000
Sheet Total (Gallons):
260000

City of Elizabeth City WWTP I
I
I
I
I City of Elizabeth City WWTP
Monitoring Sheet for Lime Stabilization
I
Monitoring Sheet for Lime Stabilization
Alternative 2 PSRP
NPDES Permit # NCO025011
NPDES Permit # NCO025011
Class B Biosolids
Residuals Permit # WQ0002883
Residuals Permit # WQ0002883
Dates:
8/01/20
2
thru:
8/31/20
2
40 CFR Part 503 Subpart D 503.30-503.33
40 CFR Part 503 Subpart D 503.30-503.33
Initial pH
pH After 2 Hours
pH After 24 Hours
Tank
Analyst
Date
Time
pH (s u)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Analyst
Date
Time
pH (s u)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Shipped
to SST
#1or2
Analyst
Date
Time
pH (s u)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Stabilization
Amount
(Gallons)
2
JS
8/2/2022
0950
12.42
0.12
12.54
29.5
SNC
8/2/2022
12.25
12.34
0.15
12.49
30.7
2
AE
8/3/2022
1124
12.14
0.21
12.35
31.9
20000
1
JS
8/2/2022
1431
12.25
0.18
12.43
31.0
DR
8/2/2022
16.31
12.12
0.18
12.36
31.4
2
RT
8/3/2022
1431
12.09
0.21
12.30
31.6
20000
2
QS
8/6/2022
1400
12.40
0.18
12.66
29.8
DR
8/6/2022
16.00
12.44
0.15
12.59
30.3
2
QS
8/7/2022
1400
12.16
0.21
12.37
31.0
20000
1
DR
8/6/2022
1530
12.39
0.12
12.31
29.1
DR
8/6/2022
17.36
12.15
0.15
12.40
30.1
1
JS
8/7/2022
1540
12.27
0.18
12.45
31.6
20000
2
QS
8/12/2022
1155
12.35
0.09
12.44
28.4
QS
8/12/2022
13.55
12.46
0.06
12.52
26.7
2
QS
8/13/2022
1155
12.29
0.15
12.44
30.3
20000
1
DR
8/12/2022
1415
12.36
0.06
12.42
27.4
DR
8/12/2022
21.15
12.46
0.06
12.46
27.0
1
DR
8/13/2022
1915
12.28
0.06
12.34
27.9
20000
2
JS
8/17/2022
1041
12.34
0.12
12.46
28.71
JS
8/17/2022
14.18
12.33
0.12
12.45
28.81
2
JS
8/18/2022
1038
12.31
0.12
12.43
29.6
20000
1
JS
8/18/2022
1325
12.23
0.12
12.35
29.6
DR
8/18/2022
16.18
12.36
0.12
12.42
25.1
1
QS
8/19/2022
1015
12.10
0.12
12.22
28.7
20000
1
QS
8/19/2022
0915
12.21
0.09
12.30
27.9
QS
8/19/2022
11.15
12.17
0.12
12.39
28.8
2
QS
8/20/2022
1015
11.66
0.09
11.75
28.2
20000
2
QS
8/19/2022
0915
12.21
0.03
12.24
26.4
QS
8/19/2022
11.15
12.34
0.09
12.43
28.7
2
JS
8/20/2022
1015
12.20
0.15
12.35
30.8
20000
2
JS
8/25/2022
1028
12.26
0.12
12.38
28.8
JS
8/25/2022
12.30
12.31
0.12
12.43
29.3
2
DR
8/26/2022
1020
12.26
0.09
12.35
28.2
20000
1
DR
8/25/2022
1800
12.27
0.12
12.39
29.0
DR
8/25/2022
20.00
12.40
0.06
12.46
27.3
1
QS
8/26/2022
1800
11.50
0.12
11.62
30.8
20000
2
JS
8/28/2022
0029
12.26
0.12
12.38
29.0
JS
8/28/2022
3040
12.39
0.06
12.461
27.4
1
QS
8/29/2022
1045
12.29
0.12
12.35
28.21
20000
1
JS
8/28/2022
613
12.28
0.09
12.37
28.1
QS
8/28/2022
825
12.28
0.09
12.37
29.1
1
js
8/29/2022
1100
12.29
0.06
12.35
26.5
20000
Sheet Total (Gallons):
280000

City of Elizabeth City WWTP
Monitoring Sheet for Lime Stabilization
Alternative 2 PSRP
Class B Biosolids
Dates: 9/01/2022 thru: a/-An/7n77
NPDES Permit # NCO025011
Residuals Permit# WQ0002883
40 CFR Part 503 Subpart D 503.30-503.33
City of Elizabeth City WWTP
Monitoring Sheet for Lime Stabilization
NPDES Permit # NCO025011
Residuals Permit# WQ0002883
40 CFR Part 503 Subpart D 503.30-503.33
Initial pH
pH After 2 Hours
pH After 24 Hours
Tank
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Shipped
to SST
#1or2
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Stabilization
Amount
(Gallons)
2
CIS
9/1/2022
1010
12.25
0.09
12.34
28.3
CIS
9/1/2022
1210
12.12
0.15
12.27
30.0
2
1S
9/2/2022
1010
11.98
0.15
12.13
30.6
20000
1
1S
9/1/2022
1101
12.08
0.27
12.35
34.2
1S
9/1/2022
1810
12.13
0.15
12.28
30.0
1
DR
9/2/2022
1801
12.16
0.18
12.28
30.6
20000
2
DR
9/7/2022
1200
12.30
0.12
12.42
29.6
DR
9/6/2022
1900
12.24
0.12
12.36
27.0
1
CIS
9/8/2022
0722
12.13
0.12
12.25
30.6
20000
1
1R
9/7/2022
0028
12.46
0.09
12.55
27.8
CIS
9/7/2022
0837
12.30
0.12
12.42
29.1
1
CIS
9/8/2022
0730
12.21
0.12
12.33
30.6
20000
2
CIS
9/13/2022
0815
12.16
0.09
12.25
27.8
CIS
9/13/2022
1015
12.19
0.12
12.31
28.6
1
CIS
9/15/2022
0820
12.14
0.09
12.23
30.6
20000
1
CIS
9/13/2022
820
12.28
0.09
12.37
27.8
CIS
9/13/2022
1020
12.31
0.09
12.40
28.1
1
CIS
9/15/2022
825
12.21
0.09
12.30
30.6
20000
1
1S
9/17/2022
1700
12.24
0.09
12.33
28.3
1S
9/17/2022
1226
12.16
0.06
12.17
27.0
1
AE
9/19/2022
1010
11.67
0.12
11.79
30.6
20000
2
CIS
9/28/2022
1445
12.17
0.15
12.32
30.1
DR
9/28/2022
1245
12.27
0.09
12.36
28.0
2
CIS
9/29/2022
1315
12.17
0.09
12.26
30.6
20000
1
1S
9/29/2022
0040
12.20
-0.06
12.14
23.0
1S
9/29/2022
0038
12.10
-0.09
12.01
22.0
1
1S
9/30/2022
0020
11.75
-0.03
11.72
30.6
20000
Sheet Total (Gallons):
180000

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Elizabeth City
WWTP Name: Elizabeth City WWTP
WQ Permit Number: WQ0002883
NPDES Number: NCO025011
Monitoring Period: From 10/1/2022 To 12/31/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) u
A1t.D (No Prior Test) I
Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ]
1 Heat Drying ❑
Heat Treatment ❑ Thermophilic C
Beta Ray 0
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens 0
If applicable to alternative
performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization 0
Air Drying ❑
Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
ginimum
in SludgeJMPN
Pathogen Density
Number of
Excee-
deuces
Frequency
of Analysis
y
Sample
Type
a yti
Tech
nique
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
colifonn)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC
02T .1107) - Please indicate alternative nerformed:
Alt.l (VS reduction) ❑
jAlt. 2 (40-day bench) ❑
jAlt. 3 (30-day bench) ❑Alt.
4 (Spec. Oz uptake)
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization r❑
jAlt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable)
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
INo vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Awtz� e�—Ao�j J. Bryan Smith, President
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print
Signature of Preparer* Date
2/23/23
Signature of Land Applier (if applicable) Datf
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

City of Elizabeth City WWTP
Monitoring Sheet for Lime Stabilization
Alternative 2 PSRP
Class B Biosolids
Dates: In/nl/7n77 thru: 10/31/2022
NPDES Permit # NCO025011
Residuals Permit# WQ0002883
40 CFR Part 503 Subpart D 503.30-503.33
City of Elizabeth City WWTP
Monitoring Sheet for Lime Stabilization
NPDES Permit # NCO025011
Residuals Permit # WQ0002883
40 CFR Part 503 Subpart D 503.30-503.33
Initial pH
pH After 2 Hours
pH After 24 Hours
Tank
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Shipped
to SST
#1or2
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Stabilization
Amount
(Gallons)
2
1S
10/5/2022
0858
12.12
-0.09
12.03
21.8
1S
10/5/2022
1252
12.33
-0.12
12.21
21.3
1
CIS
10/7/2022
0909
12.17
0.00
12.17
24.8
20000
1
CIS
10/6/2022
0905
12.16
-0.03
12.13
23.9
CIS
10/5/2022
1105
12.31
0.00
12.31
24.7
1
CIS
10/7/2022
0110
12.18
0.00
12.18
25.4
20000
1
1R
10/11/2022
0410
12.56
-0.09
12.47
22.0
1R
10/11/2022
0621
12.49
-0.06
12.43
22.9
1
1R
10/12/2022
0625
12.42
-0.06
12.36
23.21
20000
2
RT
10/11/2022
0841
12.26
-0.03
12.23
22.01
RT
10/11/2022
1041
12.32
0.00
12.32
24.7
1
AE
10/13/2022
0727
12.18
0.00
12.18
25.0
20000
2
CIS
10/15/2022
0810
12.25
-0.06
12.19
23.3
CIS
10/15/2022
1010
12.20
0.00
12.20
24.7
1
CIS
10/16/2022
1030
12.17
0.00
12.17
25.3
20000
1
CIS
10/15/2022
1430
12.34
0.00
12.34
25.1
DR
10/15/2022
1630
12.30
0.00
12.30
25.7
1
CIS
10/16/2022
1430
12.13
0.09
12.22
27.7
20000
2
CIS
10/19/2022
0805
12.22
-0.09
12.13
21.7
CIS
10/19/2022
1005
12.44
-0.09
12.35
22.2
1
RT
10/20/2022
0810
12.13
-0.09
12.04
21.7
20000
1
CIS
10/19/2022
1175
12.59
-0.15
12.44
20.4
CIS
10/19/2022
1315
12.46
-0.09
12.37
22.1
1
RT
10/20/2022
1130
12.26
-0.09
12.17
21.8
20000
2
CIS
10/26/2022
1455
12.39
0.00
12.39
24.5
CIS
10/26/2022
1655
12.33
-0.03
12.32
24.3
1
1S
10/27/2022
1604
12.31
-0.03
12.28
28.5
20000
1
1R
10/27/2022
0538
12.16
-0.03
12.43
23.7
CIS
10/27/2022
0250
12.31
-0.06
12.28
23.5
1
1R
10/28/2022
0634
12.45
-0.03
12.42
24.11
20000
Sheet Total (Gallons):
200000

City of Elizabeth City WWTP
Monitoring Sheet for Lime Stabilization
Alternative 2 PSRP
Class B Biosolids
Dates: 11/ni/7n77 thru: 11/30/2022
NPDES Permit # NCO025011
Residuals Permit # WQ0002883
40 CFR Part 503 Subpart D 503.30-503.33
City of Elizabeth City WWTP
Monitoring Sheet for Lime Stabilization
NPDES Permit # NCO025011
Residuals Permit # WQ0002883
40 CFR Part 503 Subpart D 503.30-503.33
Initial pH
pH After 2 Hours
pH After 24 Hours
Tank
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Shipped
to SST
#1or2
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Stabilization
Amount
(Gallons)
2
CIS
11/1/2022
1335
12.32
-0.03
12.36
24.4
DR
11/1/2022
1535
12.57
0.00
12.57
25.0
2
AE
11/2/2022
1339
12.18
0.00
12.18
24.5
20000
1
CIS
11/2/2022
830
12.16
-0.03
12.13
24.3
CIS
11/2/2022
1030
12.20
0.00
12.28
24.8
2
CIS
11/3/2022
0830
12.11
-0.03
12.08
24.2
20000
2
DR
11/2/2022
1430
12.30
-0.4
12.39
24.7
DR
11/3/2022
1630
12.28
0.09
12.37
22.2
2
RT
11/4/2022
0230
12.20
-0.09
12.11
22.91
20000
1
1S
11/3/2022
1833
12.33
-0.06
12.27
23.3
1S
11/3/2022
2044
12.28
-0.06
12.22
23.2
1
1S
11/6/2022
1801
12.25
0.00
12.25
25.0
20000
2
1S
11/4/2022
1726
12.33
-0.03
12.30
24.5
1S
11/4/2022
1936
12.47
-0.03
12.44
26.0
2
DR
11/6/2022
1226
12.25
0.06
12.31
23.7
20000
1
CIS
11/4/2022
710
12.37
-0.06
12.31
23.1
CIS
11/4/2022
0910
12.48
-0.06
12.42
23.2
1
CIS
11/12/2022
0930
12.18
0.00
12.18
24.8
20000
2
CIS
11/11/2022
0740
12.3
-0.06
12.24
23.0
CIS
11/11/2022
1000
12.40
-0.06
12.34
23.4
1
1S
11/12/2022
1700
12.29
0.03
12.26
24.3
20000
1
1S
11/11/2022
1651
12.27
-0.06
12.26
23.4
1S
11/11/2022
1905
12.43
-0.06
12.37
23.6
2
DR
11/14/2022
2136
12.13
0.21
12.34
19.6
20000
2
DR
11/13/2022
2132
11.54
-0.12
12.66
21.2
1R
11/14/2022
0005
12.53
-0.05
12.38
20.0
1
DR
11/15/2022
1636
12.10
0.15
12.35
20.3
20000
1
DR
11/14/2022
1630
12.36
-0.21
12.57
18.2
DR
11/14/2022
1830
12.22
0.21
12.43
15.71
1
CIS
11/19/2022
1230
12.27
-0.03
12.24
24.41
20000
2
CIS
11/18/2022
1230
12.52
-0.15
12.37
19.9
CIS
11/18/2022
1430
12.58
-0.15
12.43
20.3
1
1S
11/19/2022
2115
12.29
-0.24
12.05
17.1
20000
1
DR
11/18/2022
2130
12.65
-0.14
12.51
17.6
1R
11/19/2022
0028
12.63
-0.18
12.45
19.0
1
DR
11/21/2022
2100
12.27
-0.27
12.00
16.8
20000
1
1S
11/20/2022
2115
12.76
-0.21
12.55
17.9
1R
11/21/2022
0008
12.22
-0.18
12.34
18.3
1
DR
11/21/2022
2100
12.24
-0.24
12.00
17.6
20000
2
1S
11/20/2022
2116
12.6
-0.21
12.39
17.9
1R
11/21/2022
0010
12.63
-0.22
12.36
18.6
1
CIS
11/24/2022
1000
12.28
-0.12
12.16
21.1
20000
2
1R
11/23/2022
652
12.71
-0.18
12.53
19.3
CIS
11/23/2022
0852
12.37
-0.15
12.22
17.8
1
CIS
11/24/2022
1000
12.40
-0.12
12.28
20.5
20000
1
1R
11/23/2022
0912
12.51
-0.15
12.36
20.3
CIS
11/23/2022
1112
12.59
-0.15
12.45
20.1
1
RT
11/28/2022
0840
12.18
-0.12
12.06
20.6
20000
2
CIS
11/27/2022
840
12.47
-0.15
12.32
19.8
CIS
11/27/2022
1040
12.47
-0.15
12.32
19.91
1
1S
11/28/2022
0730
12.25
-0.15
12.10
20.21
20000
1,
CIS
11/27/2022
1440
12.48
-0.12
12.36
20.7
1S
11/27/2022
1640
12.44
-0.12
12.37
20.8
1
1S
11/30/2022
1441
12.40
-0.12
12.28
20.5
20000
Sheet Total (Gallons):
360000

City of Elizabeth City WWTP I
I
I
I
I
I
I City of Elizabeth City WWTP
Monitoring Sheet for Lime Stabilization
I
I
Monitoring Sheet for Lime Stabilization
Alternative 2 PSRP
NPDES Permit # NCO025011
NPDES Permit # NCO025011
Class B Biosolids
Residuals Permit # WQ0002883
Residuals Permit # WQ0002883
Dates:
12 01 2
22
thru:
12/31/2
22
40 CFR Part 503 Subpart D 503.30-503.33
40 CFR Part 503 Subpart D 503.30-503.33
Initial pH
pH After 2 Hours
pH After 24 Hours
Tank
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Analyst
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Shipped
to SST
#1or2
Analyst
I
Date
Time
pH (su)
Correction
Factor
pH (su)
after
Correction
Temp (°
c)
Stabilization
Amount
(Gallons)
1
RT
12/2/2022
1040
12.65
-0.15
12.50
19.7
RT
12/2/2022
1340
12.53
-0.15
12.30
19.6
1
CIS
12/3/2022
1040
12.51
-0.12
12.39
20.8
20000
2
RT
12/2/2022
1110
12.67
-0.15
12.52
20.0
RT
12/2/2022
1400
12.59
-0.15
12.44
20.4
1
CIS
12/3/2022
1110
12.48
-0.15
12.33
20.2
20000
2
1S
12/5/2022
1822
12.30
-0.21
12.09
17.6
1S
12/5/2022
2044
12.48
-0.21
12.27
17.6
1
1S
12/6/2022
1830
12.32
-0.18
12.14
19.3
20000
1
CIS
12/6/2022
1340
12.37
-0.15
12.22
20.0
1S
12/6/2022
1542
12.06
-0.21
11.91
19.8
1
1S
12/7/2022
1342
11.81
-0.12
11.69
20.9
20000
1
1S
12/10/2022
0000
12.44
-0.18
12.26
18.7
1S
12/10/2022
0205
12.36
-0.21
12.15
18.1
1
1S
12/11/2022
0010
12.24
-0.21
12.03
17.9
20000
2
CIS
12/10/2022
1350
12.54
-0.18
12.39
19.8
DR
12/10/2022
1550
12.34
-0.15
12.14
19.3
1
CIS
12/11/2022
1350
12.52
-0.15
12.37
19.6
20000
1
1S
12/21/2022
1604
12.62
-0.15
12.47
14.8
1S
12/21/2022
1930
12.80
-0.33
12.47
14.1
1
1S
12/22/2022
1630
12.73
-0.27
12.46
16.5
20000
2
RT
12/22/2022
1035
12.49
-0.15
12.25
17.2
RT
12/22/2022
1335
12.52
-0.27
12.30
16.2
1
1S
12/23/2022
1040
12.40
-0.27
12.13
16.4
20000
Sheet Total (Gallons):
160000

City of Elizabeth City
2022 Class B Annual Report
WQ0002883
Soil Samples

Soil Sample References
WB & Sons Desert Shelter/Shop
Soil Sample DS-18
= Permitted Field WB-31
Soil Sample DS-19
= Permitted Field WB-30
Soil Sample DS-20
= Permitted Field WB-29
Soil Sample DS-21=
Permitted Field WB-28
Soil Sample DS-22
= Permitted Field WB-27
Soil Sample DS-23
= Permitted Field WB-26
WB & Sons Desert 400 Acre Block
Soil Sample D423 = Permitted Field WB-84
Soil Sample D424 = Permitted Field WB-83
Soil Sample D425 = Permitted Field WB-82

Farm 2734
USDA United States
Department of Agriculture Pasquotank County, North Carolina
-
Tract 1990
2019 Program Year
CLU
Acres
HEL
Crop
1
17.35
UHEL
2
15.23
UHEL
3
15.93
UHEL
4
15.72
UHEL
5
114.12
1 UHEL
6
15.51
UHEL
7
14.63
UHEL
8
15.38
UHEL
9
15.49
UHEL
10
15.74
UHEL
11
14.89
UHEL
12
15.19
UHEL
13
15.49
UHEL
14
15.1
UHEL
15
9.7
UHEL
17
15.69
UHEL
18
15.12
UHEL
19
14.9
UHEL
20
13.61
UHEL
21
12.54
UHEL
22
11.49
UHEL
23
9.74
UHEL
24
6.71
UHEL
25
8.3
UHEL
26
7.45
UHEL
27
6.24
UHEL
28
5.5
UHEL
29
4.26
UHEL
30
5.0
UHEL
31
14.81
UHEL
I Noncropland
PagwQrapiatnd ZOW:2EM102 acres
Base Image Layer flown in 2018
Common Land Unit
Cropland
Non -Cropland
QTract Boundary
Wetland Determination Identifiers
•
Restricted Use
V
Limited Restrictions
Exempt from Conservation
El
Compliance Provisions
USDA FSA maps are for FSA Program administration only. This map does not represent a legal survey or reflect actual ownership; rather it depicts the information provided directly from the producer and/or the NAIP imagery. The producer
accepts the data 'as is' and assumes all risks associated with its use. The USDA Farm Service Agency assumes no responsibility for actual or consequential damage incurred as a result of any user's reliance on this data outside FSA Programs.
Wetland identifiers do not represent the size, shape, or specific determination of the area. Refer to your original determination (CPA-026 and attached maps) for exact boundaries and determinations or contact NRCS.

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY23-SL000614
WB Bateman
Page 2 of 13
Sample ID: DS18
Recommendations.
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1-Soybean
0.3
0 0
0
0
0
0
0
0
0
Note: 3
2 -Corn, grain
0.0
120 - 160 0
0
0
0
0
0
0
0
Note: 3
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/drr?]:
Soil Class:
Mineral -Organic
HM% WN CEC BS% Ac pH
P-1 K-I
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn4
Zn-AI
Cu-I
Na
ESP
SS-1 NO3-N
4.32 0.89 13.7
76 3.2 5.4
206 169
54 16
126
46
45
52
48
60
129
0.1
1
Sample ID: DS19
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1- Soybean
0.0
0 0
0
0
0
0
0
0
0
Note: 3
2- Corn, grain
0.0
120 - 160 0
0
0
0
0
0
0
0
Note: 3
Test Results [units - WN in g/crrt?; CEC and Na in meq/100 cm3; NO3-N in mg/dd]:
Soil Class:
Mineral -Organic
HM% WN CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS-1 NO3-N
3.67 0.89 13.4
77 3.1 5.5
188 198
52 18
157
42
43
50
35
44
69
0.1
1
Sample ID: J04A
Recommendations:
Lime
Nu
More
Cr
(tons/acre)
N
20
Mg
S
Mn
Zn
Cu
B
In o tion
Lime History:
1-Soybean
5
0
0
0
0
0
0
0
0
Note: 3
2 - Corn, grain
0.0
60 0
0
0
0
0
0
0
0
Note: 3
Test Results [units - WN in glcm3; nd Na in meq/100 cm3; NO3-N in mgldm3]:
Soil Class:
Mineral
HM% WN CEC
% Ac pH
P-1 K-I
Ca% Mg%
S-I
Mn-1
-AI1
Mn-Al2
Zn-I
Zn-AI
Cu-1
Na
ESP
SS-1 NO3-N
0.46 1. 8.4
82 1.5 5.7
251 110
55 21
164
141
95
102
102
101
0.1
1
O�.

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY23-SL008899
WB Bateman
Page 18 of 25
Sample ID: DS20
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P205
K20
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Corn, grain
0.8
120 - 160 0
0
0
0
0
0
0 0
Note: 3
2 -
0.0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
3.01 0.96 12.5
81 2.4 5.7
160 165
57 17
44
32
36
42
42
69 0.1
1
Sample ID: DS21
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P205
K20
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Corn, grain
0.6
120 - 160 0
0
0
0
0
0
0 0
Note: 3
2 -
0.0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N
in mg/dm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
3.28 0.93 13.6
83 2.3 5.8
164 142
60 18
36
33
37
42
42
88 0.1
1
Sample ID: DS22
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P205
K20
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Corn, grain
0.3
120 - 160 0
0
0
0
0
0
0 0
Note: 3
2 -
0.0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
2.22 1.06 12.5
83 2.1 5.9
169 127
62 16
38
39
40
38
38
108 0.1
1

NCDA&CS Agronomic Division Phone:
[phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY23-SL008899
WB Bateman
Page 19 of 25
Sample ID: DS23
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Corn, grain
0.6
120 - 160 0
0
0
0
0
0
0 0
Note: 3
2 -
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
2.60 1.03 13.3
84 2.2 5.8
203 173
63 14
30
41
42
60
60
94 0.1
1
Sample ID: DS24
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Corn, grain
0.0
120 - 160 0
0
0
0
0
0
0 0
Note: 3
2 -
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
2.29 1.04 14.4
88 1.7 6.1
235 166
66 17
28
52
46
65
65
120 0.1
1
Sample ID: DS25
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Corn, grain
0.0
120 - 160 0
0
0
0
pH$
0
0 0
Note: 3 Note: $
2 -
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
2.01 1.05 15.9
92 1.2 6.6
191 138
70 18
27
50
37
60
60
135 0.1
1

Farm 2734
USDA United States
Depart
Agrricult fetof Pasquotank County, North Carolina
Pasquotank NC139 T1987 Al
�F
r
i
I
1:3
1� 1�
N
0 370 740 1,4
.. s Fe
Tract 1987
2019 Program Year
CLU
Acres
HEL
Crop
1
16.34
UHEL
2
14.99
UHEL
3
15.71
UHEL
4
15.45
UHEL
5
15.68
UHEL
6
15.6
UHEL
7
16.43
UHEL
8
15.57
UHEL
9
15.15
UHEL
10
15.58
UHEL
11
15.25
UHEL
12
15.19
UHEL
13
15.31
UHEL
14
15.16
UHEL
15
15.38
UHEL
16
15.17
UHEL
17
15.47
UHEL
18
14.94
UHEL
19
14.77
UHEL
20
14.75
UHEL
21
14.31
UHEL
22
16.3
UHEL
23
15.29
UHEL
24
15.96
UHEL
25
14.24
UHEL
26
16.21
UHEL
Page Cropland Total: 400.2 acres
Map Created March 18, 2019
Base Image Layer flown in 2018
Common Land Unit
Cropland
Tract Boundary
Wetland Determination
6 Restricted Use
n Limited Restrictions
E Exempt from Conservation
Compliance Provisions
USDA FSA maps are for FSA Program administration only. This map does not represent a legal survey or reflect actual ownership; rather it depicts the information provided directly from the producer and/or the NAIP imagery. The producer
accepts the data 'as is' and assumes all risks associated with its use. The USDA Farm Service Agency assumes no responsibility for actual or consequential damage incurred as a result of any user's reliance on this data outside FSA Programs.
Wetland identifiers do not represent the size, shape, or specific determination of the area. Refer to your original determination (CPA-026 and attached maps) for exact boundaries and determinations or contact NRCS.

h -q co ac-
NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY23-SL000614
WB Bateman
Page 8 of 13
Sample ID: D421
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P205
K20
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1-Soybean
0.0
0 0
0
0
0
0
0
0
0
Note: 3
2 -Corn, grain
0.0
120 - 160 0
0
0
0
0
0
0
0
Note: 3
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Organic
HM% W/V CEC BS% Ac pH
P-1 K-I
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2 Zn-I
Zn-AI
Cu-I
Na ESP
SS -I NO3-N
7.70 0.80 18.1
71 5.2 5.0
244 101
54 14
116
89
79
86
141
234
47
0.1
1
Sample ID: D422
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P205
K20
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1-Soybean
0.0
0 0
0
0
0
0
0
0
0
Note: 3
2- Corn, grain
0.0
120 - 160 0
0
0
0
0
0
0
0
Note: 3
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Organic
HM% WN CEC BS% Ac pH
P-1 K-I
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP
SS -I NO3-N
8.54 0.81 19.3
73 5.2 5.1
243 109
58 12
110
83
74
81
137
227
47
0.1
1
Sample ID: D423
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P205
K20
Mg
S
Mn
Zn
Cu
B
information
Lime History:
1- Soybean
0.0
0 0
0
0
0
0
0
0
0
Note: 3
2- Corn, grain
0.0
120 - 160 0
0
0
0
0
0
0
0
Note: 3
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Organic
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP
SS-1 NO3-N
7.96 0.82 22.1
79 4.6 5.4
250 148
65 11
156
72
63
70
135
224
51
0.2
1

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No,
FY23-SL000614
WB Bateman
Page 9 of 13
Sample ID: D424
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P205
K20
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1- Soybean
0.0
0 0
0
0
0
0
0
0
0
Note: 3
2 -Corn, grain
0.0
120 - 160 0
0
0
0
0
0
0
0
Note: 3
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Organic
HM% WN CEC BS% Ac pH
P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-All
Mn-Al2 Zn-I
Zn•AI
Cu-I
Na
ESP
SS-1 NO3-N
7.45 0.85 23.0
83 4.0 5.6
256 126
69 11 114
59
52
59
120
199
53
0.1
0
Sample ID: D425
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P205
K20
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1-Soybean
0.0
0 0
0
0
0
0
0
0
0
Note: 3
2- Corn, grain
0.0
120 - 160 0
0
0
0
0
0
0
0
Note: 3
Test Results [units - WN in
g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Organic
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn•AI
Cu-I
Na
ESP
SS-1 NO3-N
7.70 0.83 21.2
78 4.6 5.3
251 124
64 12 133
76
66
73
123
204
67
0.1
0
Sample ID: D426
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P205
K20
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1- Soybean
0.0
0 0
0
0
0
0
0
0
0
Note: 3
2- Corn, grain
0.0
120 - 160 0
0
0
0
0
0
0
0
Note: 3
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dd]:
Soil Class:
Organic
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS-1 NO3-N
&20 0.80 26.9
89 3.0 6.0
253 172
75 10 122
47
38
45
99
164
62
0.1
0

Form AD-1 (April2015) SOIL SAMPLE INFORMATION — N.C. Soil Only
ROUTINE/PREDICTIVE SAMPLES
April — Thanksgiving: no fee
December —March: $4 / sample
Check online for exact dates.
SAMPLE INFORMATION PAYMENT
NCDA&CS Agronomic Division Soil Testing Section
Mailing Address: 1040 Mail Service Center, Raleigh NC 27699-1040
Physical Address (UPS/FedEx): 4300 Reedy Creek Road, Raleigh NC 27607
Phone: [phone] Website: www.ncagr.gov/agronomi
For laboratory results, go to www.neagr.gov/agronomi/pals.
GROWER INFORMATION (please print legibly) CONSULTANT/OTHER RECIPIENT
FARM ID (optional)
FEE TOTAL
LAST NAME
FIRST NAME
LAST NAME
FIRST NAME
Larabee
METHOD OF PAYMENT
ESCROW ACCOUNT ONLY
(write account name below)
Atlantic OBX, Inc.
Cummings
Stephen
ADDRESS (in N.C. where samples were collected)
ADDRESS
SAMPLE DATE (optional)
9/15/2022
P.O. Box 2560
P.O. Box 2560
CITY
Kitty Hawk
STATE ZIP
NC 27949
CITY
Kitty Hawk
STATE ZIP
NC 27949
NC COUNTY (where collected)
PaS Uotank
q
Reminders
Use NCDA&CS sample
boxes only. Fill to red
E-MAILADDRESS
E-MAILADDRESS
NUMBER OF SAMPLES
line. Bags not accepted.
[e-mail]
10
Select crop code(s) from
on back of form.
PHONE
252-255-2030
PA LS #--
(if known) ------
PHONE
252-489-7317
PALS itlist
(if known) -----
By submitting this form to the NCDA&CS Agronomic Division, I attest that the accompanying samples were collected in North Carolina.
LIME APPLIED WITHIN
You must specify a crop CODE to receive a recommendation (see reverse side of form)
LAB NUMBER
SAMPLE
PAST 12 MONTHS
(Leave blank)
IDENTIFICATION
FIRST CROP
CODE
SECOND CROP
CODE
Tons/Acre Month Year
2 8
Corn
001
Soybean Double Cropped
018
2
2 1 9
Corn
001
Soybean Double Cropped
018
s
3 1 0
Corn
001
Soybean Double Cropped
018
a
3 1
Corn
001
Soybean Double Cropped
018
5
3 1 2
Corn
001
Soybean Double Cropped
018
s
3 1 3
Corn
001
Soybean Double Cropped
018
3 1 4
Corn
001
Soybean Double Cropped
018
$
3 1 5
Corn
001
Soybean Double Cropped
018
s
3 1 6
Corn
001
Soybean Double Cropped
018
10
I I I 3 1 7
1
Com
001
Soybean Double Cropped
01,
Thank you for using agronomic services to manage nutrients and safeguard environmental quality. — Steve1'roxler, Commissioner of Agriculture

Taking a Soil Sample
-A 201 test is 011P,y M good M tie 201 SUTAP d
Use iron or stainless steel tools. Sample dry soil
in areas of 10 acres or fewer. Avoid combining
soils of different types and/or treatment histories.
Avoid fertilizer bands and corners or end -turn
areas. For each sample, collect 15-20 cores at the
appropriate depth (0-8" for plowed soils; 0-4"
for no -till, sod & lawns). Mix cores in a plastic
bucket, then fill the sample box.
DO NOT PUT SOIL IN PLASTIC BAGS.
REQUIRED INFORMATION
The lab MUST have this information.
Filling out the Sample Information Form
LIME APPLIED WITHIN
LAB NUMBER
SAMPLE
PAST 12 MONTHS
FIRST CROP
CODE
SECOND CROP
CODE
(Leave blank)
IDENTIFICATION
Tons/Acre Month Year
1
J 1
1
9
2012
Cony
001
(nxwK
004
2
IS1
2
9
2012
NoLYen / Gnass, M
050
NoLYen / Gnass, M
050
3
s 2
0
F_
043
Benw�uda Ala , Nl
044
SAMPLE & GROWER INFORMATION — Provide as much information as possible. Print neatly.
CONSULTANT/OTHER RECIPIENT — List name & contact information for anyone else who needs to know about the report.
SAMPLE IDENTIFICATION — Print an identifier (use numbers and/or letters) for each sample on a separate line. The identifier should
help remind you where the sample came from (Example: J 1, S 1). Make sure the sample identifers on the boxes and on the information
form are the same. Use pencil or waterproof markers.
FIRST CROP — List the crop for which you want lime and fertilizer recommendations. Be sure to include the appropriate CODE from
the list below (e.g., Bermuda hay or pasture establishment, 043).
A. Use Lawn (code 026) for all lawn grasses except Centipede. Use one of the Fine Turf codes only for golf and athletic field turf.
B. Use Shrubs (code 029) for all shrubs, except azalea, camellia, rhododendron and mountain laurel.
C. For all home garden vegetables, use code 024.
LIME APPLIED WITHIN PAST 12 MONTHS — Provide the amount of lime applied in tons/acre, as well as the year and month of the last
DESIRABLE INFORMATION application, if made during the past 12 months. (50M = 50 lb/1000 ft', which is equivalent to one ton per acre.)
The lab can make better suggestions SECOND CROP — List the name of the crop that will follow the one listed as FIRST CROP. Include its CODE from the list below. This
if this information is provided. will enable us to make suggestions for this crop, assuming that the field is treated as suggested the first year. List the second crop even if
it will be grown the same year as FIRST CROP.
CROP CODES
E = establishment (1st year)
M = maintenance
SG = small grain
Field Crops
001 Corn, grain
002 Corn, silage
003 Cotton
004 Small Grain
005 Millet, pearl
006 Milo (Grain Sorghum)
007 Peanut
008 Rice
009 Sorghum, syrup
010 Soybean
011 Sunflower
012 Tobacco, burley
013 Tobacco, flue -cured
014 Tobacco, greenhouse
015 SG silage/ Soybean
016 SG silage/ Corn silage
017 Kenaf, fiber
018 SG/ Soybean (double crop)
Home Lawn & Garden
020 Azalea/ Camellia
022 Lawn, centipede
023 Flower garden
024 Vegetable garden
025 Mtn. Laurel/ Rhodod.
026 Lawn (not centipede)
028 Rose
029 Shrubs
030 Berries/Fruit/Nuts
031 Tree, shade
032 Blueberries, home
Christmas Trees
034 Leyland Cypress
035 Line-out/ Seed beds
036 Fir/N. Spruce/Hem, E
037 Fir/N. Spruce/Hem, M
038 Pine, white or Va.
039 BI. Spruce/Red Cedar
Forage & Pasture
040 Alfalfa, E
041 Alfalfa, M
042 Corn. Bermuda/Bahia
Forage & Pasture (cont.)
043 Bermuda hay/past., E
044 Bermuda hay/past., M
047 Bluegrass pasture
048 Bluegrass/Wh. Clover
049 Clover/Grass, E
050 Clover/Grass, M
051 Gamagrass
053 Legumes, misc.
054 Fescue/OGrass/Tim, E
055 Fescue/OGrass/Tim, M
056 Prairiegrass
057 Switchgrass
059 Sudan/Sorghum past.
060 Sudan/Sorghum silage
Roadside Areas
061 Critical area
062 Grass, roadside, E
063 Grass, roadside, M
Wildlife Areas / Food Plots
066 Deer/Turkey
067 Upland Game
068 Waterfowl
069 Fish Pond
Commercial Hort Crops ONLY
[024 = all Home Vegetables]
070 Asparagus, E
071 Asparagus, M
072 Beans/Peas
073 Beans, pole
074 Beet
075 Blueberry, E
076 Blueberry, M
077 Brocc/ BSprout/Caulif
079 Cabbage
080 Cantaloupe/Melons
084 Corn, sweet
085 Cucumber
088 Grape, E
089 Grape, M
090 Kale/ Mustard/ Spinach
093 Okra
095 Pea, southern
096 Pepper/Sage
097 Plant bed, vegetable
098 Potato, Irish
099 Sweetpotato
100 Radish
101 Canola/Rape
Commercial Hort Crops (cont.)
102 Black/Raspberry, E
103 Black/Raspberry, M
107 Squash/Pumpkin
108 Strawberry, E
109 Strawberry, M
110 Tomato
111 Tomato, greenhouse
115 Turnip
116 Vegetables, other
118 Strawberry, plastic
119 Hops
175 Grape - vinifera
Commercial Nursery & Flowers
120 Dahlia
121 Gladiolus
122 Greenhouse
123 Gypsophila (baby's breath)
124 Flower, bulbs
125 Flower, roots
126 Container nursery
132 Rhod/Ginseng/Natives
136 Tree nursery
Orchard. Fruit & Nut
130 Apple, E
131 Apple, M
138 Peach, E
139 Peach, M
140 Pecan, E
141 Pecan. M
Forest Trees & Seed
133 Hardwood, E
134 Hardwood, M
137 Pine nursery
142 Pine, E
143 Pine, M
144 Hardwood, seed
145 Fir/Spruce, seed
146 Pine, seed
Fine Turf
150 Fairway/Athl. turf
151 Tee
152 Greens
Stormwater
200 Bioretention cell

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY23-SL005604
k5i I"14'4+;4
Client:
Atlantic Sewage Control
Advisor:
Predictive
PO Box 2560
°± f'
Kitty Hawk, NC 27949
�- Soil Report Mehlich-3 Extraction
Sampled County : Pasquotank
_1
Links to Helpful Information
Sampled: 09/15/2022 Received: 09/23/2022 Completed: 10/04/2022 Farm: Larabee
Client ID:
216556
Advisor ID:
Sample ID: 28
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, grain 1.3 120 - 160 0
0
0 0
0
0
0
0
Note: 3
2-SG/Soybean(DC) 0.0 80-100 0
0
0 0
0
0
0
0
Note:3
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg%
S-1 Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I Na
ESP
SS-1 NO3-N
3.28 1.10 11.5 75 2.8 5.5 178 80 57 14
83 75
62 55
88
88
76 0.1
1
Sample ID: 29
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, grain 1.5 120 - 160 0
10
0 0
0
0
0
0
Note: 3
2-SG/Soybean(DC) 0.0 80-100 0
0
0 0
0
0
0
0
Note:3
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg%
S-1 Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na
ESP
SS-1 NO3-N
3.47 1.10 11.5 75 2.9 5.4 179 78 57 14
80 74
61 54
89
89
76 0.1
1
North Carolina
Tai wLv Truk f and Ctwinlsskm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY23-SL005604
Page 2 of 5
Sample ID: 30
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, grain
0.0
120 - 160 0
10
0
0
pH$
0
0
0
Note: 3 Note: $
2 -SG/Soybean (DC)
0.0
80-100 0
0
0
0
pH$
0
0
0
Note: 3 Note: $
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS-1 NO3-N
2.76 1.04 24.8
95 1.2 6.6
208 72
88 6
97
72
52
45
93
93
74
0.1
0
Sample ID: 31
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, grain
0.0
120 - 160 0
0
0
0
pH$
0
0
0
Note: 3 Note: $
2 -SG/Soybean (DC)
0.0
80-100 0
0
0
0
pH$
0
0
0
Note: 3 Note: $
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS-1 NO3-N
2.52 1.02 21.1
94 1.2 6.5
255 90
84 8
97
69
50
43
102
102
71
0.1
0
Sample ID: 32
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, grain
0.5
120 - 160 0
20
0
0
0
0
0
0
Note: 3
2-SG/Soybean(DC)
0.0
80-100 0
30
0
0
0
0
0
0
Note:3
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS-1 NO3-N
2.68 1.12 14.5
85 2.1 5.8
265 63
75 9
87
57
51
44
85
85
56
0.1
1

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY23-SL005604
Page 3 of 5
Sample ID: 33
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, grain
1.0
120 - 160 0
0
0
0
0
0
0
0
Note: 3
2-SG/Soybean(DC)
0.0
80-100 0
0
0
0
0
0
0
0
Note:3
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS-1 NO3-N
2.84 1.12 13.4
81 2.5 5.6
241 80
68 11
100
70
59
52
107
107
67
0.2
1
Sample ID: 34
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, grain
1.1
120 - 160 0
0
0
0
0
0
0
0
Note: 3
2-SG/Soybean(DC)
0.0
80-100 0
0
0
0
0
0
0
0
Note:3
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS-1 NO3-N
2.84 1.07 11.5
79 2.4 5.5
206 81
62 13
91
70
59
52
83
83
70
0.1
1
Sample ID: 35
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, grain
1.4
120 - 160 0
0
0
0
0
0
0
0
Note: 3
2-SG/Soybean(DC)
0.0
80-100 0
0
0
0
0
0
0
0
Note:3
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS-1 NO3-N
3.19 1.10 12.0
77 2.8 5.4
187 79
59 15
89
72
60
53
87
87
69
0.1
1

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY23-SL005604
Page 4 of 5
Sample ID: 36
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, grain
1.5
120 - 160 0
0
0
0
0
0
0
0
Note: 3
2-SG/Soybean(DC)
0.0
80-100 0
0
0
0
0
0
0
0
Note:3
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS-1 NO3-N
3.47 1.09 11.6
75 2.9 5.4
182 84
56 15
85
75
62
55
90
90
75
0.1
1
Sample ID: 37
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, grain
0.0
120 - 160 0
0
0
0
0
0
0
0
Note: 3
2-SG/Soybean(DC)
0.0
80-100 0
0
0
0
0
0
0
0
Note:3
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral -Organic
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS-1 NO3-N
3.57 1.08 11.7
75 2.9 5.4
184 79
57 15
82
75
70
63
91
114
78
0.1
1

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY23-SL005604
Page 5 of 5
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.pov/apronomi/obpart4.htrntfsfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
Zn-1
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.pov/agronomi/uyrst.htm