WQ0006018_2022 Residual Annual Report_20230227 (2)

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * W00006018
Applicant/Permittee Town of Morehead City
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Wilmington
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Lysa Finnerty
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
4105376150
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation High -Rate Infiltration
Other Wastewater Reclaimed Water
Closed -Loop Recycle Residuals
Single -Family Residence Wastewater Other
Irrigation
Permit Number:* WQ0006018
Has Current Existing permit number
Applicant/Permittee Address* 435 Williams Court, Ste 100, Baltimore, MD 21220
Facility Name* Town of Morehead City Class B Residuals Program
Please provide comments/notes on your current submittal below.
2022 Annual Report for Town of Morehead City, NC
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Morehead City NC 2022 Annual Report FINAL.pdf 7.49MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/27/2023

435 Williams Court, Suite 100
Baltimore, MD 21220
www.synagro.com
FEBRUARY 27, 2023
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2022 Annual Report for Permit No. WQ0006018
Dear NCDEQ:
SYNAGRO
Synagro is submitting one electronic copy of the above referenced report on behalf of the Town
of Morehead City, NC.
If you have any questions or need additional information, please do not hesitate to contact
Daniel Williams at [phone] or Matthew Carter at [phone].
Sincerely,
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Daniel Williams, Town of Morehead City
Matthew Carter, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

TOWN OF MOREHEAD CITY, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0006018
2022 ANNUAL REPORT

Town of Morehead City, NC
Residuals Land Application Program
2022 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and Residuals Analyses
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen Reduction/Vector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00006018 County Carteret Year 2022
Facility Name (as shown on permit) Town of Morehead City WWTP NPDES No. NCO026611
Land Application Operator Svnagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip PartA, and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 7
Total number of fields utilized for land application during the year: 4
Total amount of dry tons applied during the year for all application sites: 81_86
Total number of acres utilized for land application during the year: 49_90
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2022 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T A 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
i l . Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations." —
Daniel Williams, Utilities Director
Pe ttee Name a d Title (type or print) = Signature of . Date
i
3 Perm 2/01/2023
Signature of Preparer* Date S o Lan pplier Date
(if different from Permittee) (if different1from. Pern ittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 1/1/2022 - 12/31/2022
MOREHEAD CITY, NC
MOREHEAD CITY, NC CAKE
MONTH/YEAR
May 2022
TOTAL
Units Key: D - Dry Tons; G — Gallons; W — Wet Tons; Y — Cubic Yards
Report Date: 2/14/2023 4:32:17 PM
AMOUNT UNIT DRY TONS UNIT DRY METRIC TONS
400.00 Y 81.86 D 74.25
400.00 Y 81.86 D 74.25

SECTION 2

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Environmental Chemists,
Inc.
envirochem6602
Windmill
Way, Wilmington, NC 28405 ■ 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
infoeaenvironmentalchemists.com
Town Of Morehead City
Date of Report: Apr 27, 2022
1100 Bridges Street
Customer PO #:
Morehead City NC 28557
Customer ID: 09020011
Attention: Nate Johnson
Report #: 2022-05661
Project ID: Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-13693 Site: Sludge
3/29/2022 10:30 AM Solid/Sludge Nate Johnson
Test
Method
Results Date Analyzed
CCE
AOAC 1.005
1.9 %
04/21/2022
Paint Filter Test
SW 846 Method 9095 A pass
04/21 /2022
Chlordane (TCLP)
SW-846 8081 B
<0.02 mg/L
04/05/2022
Endrin (TCLP)
SW-846 8081 B
<0.0005 mg/L
04/05/2022
Heptachlor (TCLP)
SW-846 8081 B
<0.0005 mg/L
04/05/2022
Heptachlor epoxide (TCLP)
SW-846 8081 B
<0.0005 mg/L
04/05/2022
Lindane (TCLP)
SW-846 8081 B
<0.0005 mg/L
04/05/2022
Methoxychlor (TCLP)
sW-8468081 B
<0.0005mg/L
04/05/2022
Toxaphene (TCLP)
SW-846 8081 B
<0.05 mg/L
04/05/2022
2,4,5-TP (TCLP)
SW-846 8151 A
<0.003 mg/L
04/04/2022
2,4-D (TCLP)
SW-846 8151 A
<0.003 mg/L
04/04/2022
1,4-Dichlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
04/01/2022
2,4,5-Trichlorophenol (TCLP)
SW-8468270E
<0.050mg/L
04/01/2022
2,4,6-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
04/01/2022
2,4-Dinitrotoluene (TCLP)
SW-846 8270 E
<0.050 mg/L
04/01/2022
Cresol (TCLP)
SW-846 8270 E
3.47 mg/L
04/01/2022
Hexachloro-1,3-butadiene (TCLP)
SW-846 8270 E
<0.050 mg/L
04/01/2022
Hexachlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
04/01/2022
Hexachloroethane (TCLP)
SW-846 8270 E
<0.050 mg/L
04/01/2022
m + p-Cresol (TCLP)
SW-846 8270 E
3.47 mg/L
04/01/2022
Nitrobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
04/01/2022
o-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
04/01/2022
Pentachlorophenol (TCLP)
SW-846 8270 E
<0.250 mg/L
04/01/2022
Pyridine (TCLP)
SW-846 8270 E
<0.050 mg/L
04/01/2022
1,1-Dichloroethylene (TCLP)
SW-846 Method 8260D <0.01 mg/L
04/07/2022
1,2-Dichloroethane (TCLP)
SW-846 Method 8260D <0.01 mg/L
04/07/2022
Report #:: 2022-05661
Page 1 of 5

Environmental Chemists,
Inc.
envirochem6602
Windmill Way,
Wilmington, NC 28405 • 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
SM,
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
[e-mail]
Town Of Morehead City
Date of Report: Apr 27, 2022
1100 Bridges Street
Customer PO #:
Morehead City NC 28557
Customer ID: 09020011
Attention: Nate Johnson
Report #: 2022-05661
Project ID: Sludge
Benzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/07/2022
Carbon Tetrachloride (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/07/2022
Chlorobenzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/07/2022
Chloroform (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/07/2022
Methyl ethyl ketone (TCLP)
SW-846 Method 8260D
0.06 mg/L
04/07/2022
Tetrachloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/07/2022
Trichloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/07/2022
Vinyl Chloride (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/07/2022
RCI
Ignitability
EPA 1030
<0.8 mm/sec
04/01/2022
Cyanide
SM 4500 CN D-2016
1.18 mg/kg
04/05/2022
Sulfide
SM 4500 S D
<0.39 mg/kg
04/11/2022
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4, 1994
13600 mg/kg
04/14/2022
Arsenic
EPA 200.7, Rev. 4.4, 1994
7.08 mg/kg
04/14/2022
Cadmium
EPA 200.7, Rev. 4.4, 1994
<3.88 mg/kg
04/14/2022
Calcium
EPA 200.7, Rev. 4.4, 1994
33100 mg/kg
04/14/2022
Chromium
EPA 200.7, Rev. 4.4, 1994
13.7 mg/kg
04/14/2022
Copper
EPA 200.7, Rev. 4.4, 1994
638 mg/kg
04/14/2022
Lead
EPA 200.7, Rev. 4.4,1 994
12.6 mg/kg
04/14/2022
Magnesium
EPA 200.7, Rev. 4.4, 1994
35.4 mg/kg
04/14/2022
Molybdenum
EPA 200.7, Rev. 4.4, 1994
5.18 mg/kg
04/14/2022
Nickel
EPA 200.7, Rev. 4.4, 1994
10.6 mg/kg
04/14/2022
Potassium
EPA 200.7, Rev. 4.4, 1994
3640 mg/kg
04/14/2022
Selenium
EPA 200.7, Rev. 4.4, 1994
<3.88 mg/kg
04/14/2022
Sodium
EPA 200.7, Rev. 4.4, 1994
4150 mg/kg
04/14/2022
Zinc
EPA 200.7, Rev. 4.4, 1994
938 mg/kg
04/14/2022
Nitrate+Nitrite-Nitrogen
EPA353.2
10.5mg/kg
03/30/2022
Total Solids (%)
SM 2540 B
24.3 %
03/30/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
25300 mg/kg
03/30/2022
Report #:: 2022-05661
Page 2 of 5

---77
SM
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 + 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 0 910.347.5843 Lab/Fax
[e-mail]
Town Of Morehead City Date of Report: Apr 27, 2022
1100 Bridges Street Customer PO #:
Morehead City NC 28557 Customer ID: 09020011
Attention: Nate Johnson Report #: 2022-05661
Project ID: Sludge
Total Kjeldahl Nitrogen (TKN) SM 4500 Norg B-2011 66200 mg/kg 03/30/2022
Total Phosphorus SM 4500 P (F-H)-2011 603 mg/kg 04/04/2022
pH SW 846 Method 9045D 8.52 units 04/12/2022
Result estimated. Analyzed out of 15 minutes hold time.
Mercury
SW-846 7471 B
0.941 mg/kg
04/04/2022
TCLP Metals
Arsenic
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
04/05/2022
Barium
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
04/05/2022
Cadmium
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
04/05/2022
Chromium
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
04/05/2022
Lead
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
04/05/2022
Selenium
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
04/05/2022
Silver
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
04/05/2022
Mercury
EPA245.1
<0.0002 mg/L
04/07/2022
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
22-13695 Site: #1
3/29/2022 2:39 PM
Solid/Sludge Nate Johnson
Test
Method
Results Date
Analyzed
Total Solids (%)
SM 2540 B
24.8 %
03/30/2022
Fecal Density
SM 9221C E-2014
622 MPN/g
03/29/2022
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
22-13697 Site: #2
3/29/2022
Solid/Sludge Nate Johnson
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
21.7 %
03/30/2022
Fecal Density
SM 9221C E-2014
2908 MPN/g
03/29/2022
Report #: 2022-05661 Page 3 of 5

Environmental Chemists, Inc.
envirochem6602
Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ■ 910.392.4424 Fax
sM
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
[e-mail]
Town Of Morehead City
Date of Report: Apr 27, 2022
1100 Bridges Street
Customer PO #:
Morehead City NC 28557
Customer ID: 09020011
Attention: Nate Johnson
Report #: 2022-05661
Project ID: Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-13698 Site: #3
3/29/2022 Solid/Sludge Nate Johnson
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 23.2 % 03/30/2022
Fecal Density
SM 9221C E-2014 <8 MPN/g 03/29/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-13699 Site: #4
3/29/2022 Solid/Sludge Nate Johnson
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 22.5 % 03/30/2022
Fecal Density
SM 9221C E-2014 9 MPN/g 03/29/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-13700 Site: #5
3/29/2022 Solid/Sludge Nate Johnson
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 28.5 % 03/30/2022
Fecal Density
SM 9221C E-2014 386 MPN/g 03/29/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-13701 Site: #6
3/29/2022 Solid/Sludge Nate Johnson
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 24.6 % 03/30/2022
Fecal Density
SM 9221C E-2014 >64909 MPN/g 03/29/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-13702 Site: #7
3/29/2022 Solid/Sludge Nate Johnson
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 23.0 % 03/30/2022
Fecal Density
SM 9221C E-2014 <8 MPN/g 03/29/2022
Report #: 2022-05661 Page 4 of 5

,envi ooche]
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
[e-mail]
Town Of Morehead City Date of Report: Apr 27, 2022
1100 Bridges Street Customer PO #:
Morehead City NC 28557 Customer ID: 09020011
Attention: Nate Johnson Report #: 2022-05661
Project ID: Sludge
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
Report #:: 2022-05661 Page 5 of 5

Environmental Chemist, Inc., Wilmington, INC Lab #94
6602 Windmill Way
Wilmington, NC 28405
Sample Receipt Checklist 910.392.0223
Client: �. I�OrP�in P� r, Date: Zq 22 Report Number: _ 2022-
ReceipHEM Pickup Client Delivery ❑ UPS ❑ Fed Ex ❑ Other ❑
Hj44N/A 1. Were custody seals present on the cooler?
N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt —
How temperature taken: ❑ Temperature Blank Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
YES ❑ NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed?
YES ❑
NO
5.
Were sample ID's listed on the COC?
YES
❑
NO
6.
Were samples ID's listed on sample containers?
YES
❑
NO
7.
Were collection date and time listed on the COC?
YES
❑
NO
8.
Were tests to be performed listed on the COC?
YES
❑
NO
9.
Did samples arrive in proper containers for each test?
YES
❑
NO
10. Did samples arrive in good condition for each test?
it YES
❑
NO
11.
Was adequate sam le volum N bl '3'
YES
❑ NO
p eaVC] ia e.
12. Were samples received within proper holding time for requested tests?
❑ YES
❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
❑ NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet
Sample Preservation:
Sample(s)
by adding (circle one):
Time of preservation:
(Must be completed for any sample(s) incorrectly preserved or with headspace)
were received incorrectly preserved and were adjusted accordingly
HNO3 HCI NaOH
If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
tiles Sample(s)
COMMENTS:
H2SO4
were received with headspace
DOC. QA.002 Rev 1
°C

i
aL
I
rk
ion
.. . ........
.. ...
F--j!

SECTION 3

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SECTION 4

F"Wow, -,,"7
Environmental Chemists,
Inc.
envirochem6602
Windmill
Way, Wilmington, NC 28405 ■ 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
infoeaenvironmentalchemists.com
Town Of Morehead City
Date of Report: Apr 27, 2022
1100 Bridges Street
Customer PO #:
Morehead City NC 28557
Customer ID: 09020011
Attention: Nate Johnson
Report #: 2022-05661
Project ID: Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-13693 Site: Sludge
3/29/2022 10:30 AM Solid/Sludge Nate Johnson
Test
Method
Results Date Analyzed
CCE
AOAC 1.005
1.9 %
04/21/2022
Paint Filter Test
SW 846 Method 9095 A pass
04/21 /2022
Chlordane (TCLP)
SW-846 8081 B
<0.02 mg/L
04/05/2022
Endrin (TCLP)
SW-846 8081 B
<0.0005 mg/L
04/05/2022
Heptachlor (TCLP)
SW-846 8081 B
<0.0005 mg/L
04/05/2022
Heptachlor epoxide (TCLP)
SW-846 8081 B
<0.0005 mg/L
04/05/2022
Lindane (TCLP)
SW-846 8081 B
<0.0005 mg/L
04/05/2022
Methoxychlor (TCLP)
sW-8468081 B
<0.0005mg/L
04/05/2022
Toxaphene (TCLP)
SW-846 8081 B
<0.05 mg/L
04/05/2022
2,4,5-TP (TCLP)
SW-846 8151 A
<0.003 mg/L
04/04/2022
2,4-D (TCLP)
SW-846 8151 A
<0.003 mg/L
04/04/2022
1,4-Dichlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
04/01/2022
2,4,5-Trichlorophenol (TCLP)
SW-8468270E
<0.050mg/L
04/01/2022
2,4,6-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
04/01/2022
2,4-Dinitrotoluene (TCLP)
SW-846 8270 E
<0.050 mg/L
04/01/2022
Cresol (TCLP)
SW-846 8270 E
3.47 mg/L
04/01/2022
Hexachloro-1,3-butadiene (TCLP)
SW-846 8270 E
<0.050 mg/L
04/01/2022
Hexachlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
04/01/2022
Hexachloroethane (TCLP)
SW-846 8270 E
<0.050 mg/L
04/01/2022
m + p-Cresol (TCLP)
SW-846 8270 E
3.47 mg/L
04/01/2022
Nitrobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
04/01/2022
o-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
04/01/2022
Pentachlorophenol (TCLP)
SW-846 8270 E
<0.250 mg/L
04/01/2022
Pyridine (TCLP)
SW-846 8270 E
<0.050 mg/L
04/01/2022
1,1-Dichloroethylene (TCLP)
SW-846 Method 8260D <0.01 mg/L
04/07/2022
1,2-Dichloroethane (TCLP)
SW-846 Method 8260D <0.01 mg/L
04/07/2022
Report #:: 2022-05661
Page 1 of 5

Environmental Chemists,
Inc.
envirochem6602
Windmill Way,
Wilmington, NC 28405 • 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
SM,
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
[e-mail]
Town Of Morehead City
Date of Report: Apr 27, 2022
1100 Bridges Street
Customer PO #:
Morehead City NC 28557
Customer ID: 09020011
Attention: Nate Johnson
Report #: 2022-05661
Project ID: Sludge
Benzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/07/2022
Carbon Tetrachloride (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/07/2022
Chlorobenzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/07/2022
Chloroform (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/07/2022
Methyl ethyl ketone (TCLP)
SW-846 Method 8260D
0.06 mg/L
04/07/2022
Tetrachloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/07/2022
Trichloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/07/2022
Vinyl Chloride (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/07/2022
RCI
Ignitability
EPA 1030
<0.8 mm/sec
04/01/2022
Cyanide
SM 4500 CN D-2016
1.18 mg/kg
04/05/2022
Sulfide
SM 4500 S D
<0.39 mg/kg
04/11/2022
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4, 1994
13600 mg/kg
04/14/2022
Arsenic
EPA 200.7, Rev. 4.4, 1994
7.08 mg/kg
04/14/2022
Cadmium
EPA 200.7, Rev. 4.4, 1994
<3.88 mg/kg
04/14/2022
Calcium
EPA 200.7, Rev. 4.4, 1994
33100 mg/kg
04/14/2022
Chromium
EPA 200.7, Rev. 4.4, 1994
13.7 mg/kg
04/14/2022
Copper
EPA 200.7, Rev. 4.4, 1994
638 mg/kg
04/14/2022
Lead
EPA 200.7, Rev. 4.4,1 994
12.6 mg/kg
04/14/2022
Magnesium
EPA 200.7, Rev. 4.4, 1994
35.4 mg/kg
04/14/2022
Molybdenum
EPA 200.7, Rev. 4.4, 1994
5.18 mg/kg
04/14/2022
Nickel
EPA 200.7, Rev. 4.4, 1994
10.6 mg/kg
04/14/2022
Potassium
EPA 200.7, Rev. 4.4, 1994
3640 mg/kg
04/14/2022
Selenium
EPA 200.7, Rev. 4.4, 1994
<3.88 mg/kg
04/14/2022
Sodium
EPA 200.7, Rev. 4.4, 1994
4150 mg/kg
04/14/2022
Zinc
EPA 200.7, Rev. 4.4, 1994
938 mg/kg
04/14/2022
Nitrate+Nitrite-Nitrogen
EPA353.2
10.5mg/kg
03/30/2022
Total Solids (%)
SM 2540 B
24.3 %
03/30/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
25300 mg/kg
03/30/2022
Report #:: 2022-05661
Page 2 of 5

---77
SM
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 + 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 0 910.347.5843 Lab/Fax
[e-mail]
Town Of Morehead City Date of Report: Apr 27, 2022
1100 Bridges Street Customer PO #:
Morehead City NC 28557 Customer ID: 09020011
Attention: Nate Johnson Report #: 2022-05661
Project ID: Sludge
Total Kjeldahl Nitrogen (TKN) SM 4500 Norg B-2011 66200 mg/kg 03/30/2022
Total Phosphorus SM 4500 P (F-H)-2011 603 mg/kg 04/04/2022
pH SW 846 Method 9045D 8.52 units 04/12/2022
Result estimated. Analyzed out of 15 minutes hold time.
Mercury
SW-846 7471 B
0.941 mg/kg
04/04/2022
TCLP Metals
Arsenic
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
04/05/2022
Barium
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
04/05/2022
Cadmium
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
04/05/2022
Chromium
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
04/05/2022
Lead
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
04/05/2022
Selenium
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
04/05/2022
Silver
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
04/05/2022
Mercury
EPA245.1
<0.0002 mg/L
04/07/2022
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
22-13695 Site: #1
3/29/2022 2:39 PM
Solid/Sludge Nate Johnson
Test
Method
Results Date
Analyzed
Total Solids (%)
SM 2540 B
24.8 %
03/30/2022
Fecal Density
SM 9221C E-2014
622 MPN/g
03/29/2022
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
22-13697 Site: #2
3/29/2022
Solid/Sludge Nate Johnson
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
21.7 %
03/30/2022
Fecal Density
SM 9221C E-2014
2908 MPN/g
03/29/2022
Report #: 2022-05661 Page 3 of 5

Environmental Chemists, Inc.
envirochem6602
Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ■ 910.392.4424 Fax
sM
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
[e-mail]
Town Of Morehead City
Date of Report: Apr 27, 2022
1100 Bridges Street
Customer PO #:
Morehead City NC 28557
Customer ID: 09020011
Attention: Nate Johnson
Report #: 2022-05661
Project ID: Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-13698 Site: #3
3/29/2022 Solid/Sludge Nate Johnson
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 23.2 % 03/30/2022
Fecal Density
SM 9221C E-2014 <8 MPN/g 03/29/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-13699 Site: #4
3/29/2022 Solid/Sludge Nate Johnson
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 22.5 % 03/30/2022
Fecal Density
SM 9221C E-2014 9 MPN/g 03/29/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-13700 Site: #5
3/29/2022 Solid/Sludge Nate Johnson
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 28.5 % 03/30/2022
Fecal Density
SM 9221C E-2014 386 MPN/g 03/29/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-13701 Site: #6
3/29/2022 Solid/Sludge Nate Johnson
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 24.6 % 03/30/2022
Fecal Density
SM 9221C E-2014 >64909 MPN/g 03/29/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-13702 Site: #7
3/29/2022 Solid/Sludge Nate Johnson
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 23.0 % 03/30/2022
Fecal Density
SM 9221C E-2014 <8 MPN/g 03/29/2022
Report #: 2022-05661 Page 4 of 5

,envi ooche]
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
[e-mail]
Town Of Morehead City Date of Report: Apr 27, 2022
1100 Bridges Street Customer PO #:
Morehead City NC 28557 Customer ID: 09020011
Attention: Nate Johnson Report #: 2022-05661
Project ID: Sludge
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
Report #:: 2022-05661 Page 5 of 5

Environmental Chemist, Inc., Wilmington, INC Lab #94
6602 Windmill Way
Wilmington, NC 28405
Sample Receipt Checklist 910.392.0223
Client: �. I�OrP�in P� r, Date: Zq 22 Report Number: _ 2022-
ReceipHEM Pickup Client Delivery ❑ UPS ❑ Fed Ex ❑ Other ❑
Hj44N/A 1. Were custody seals present on the cooler?
N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt —
How temperature taken: ❑ Temperature Blank Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
YES ❑ NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed?
YES ❑
NO
5.
Were sample ID's listed on the COC?
YES
❑
NO
6.
Were samples ID's listed on sample containers?
YES
❑
NO
7.
Were collection date and time listed on the COC?
YES
❑
NO
8.
Were tests to be performed listed on the COC?
YES
❑
NO
9.
Did samples arrive in proper containers for each test?
YES
❑
NO
10. Did samples arrive in good condition for each test?
it YES
❑
NO
11.
Was adequate sam le volum N bl '3'
YES
❑ NO
p eaVC] ia e.
12. Were samples received within proper holding time for requested tests?
❑ YES
❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
❑ NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet
Sample Preservation:
Sample(s)
by adding (circle one):
Time of preservation:
(Must be completed for any sample(s) incorrectly preserved or with headspace)
were received incorrectly preserved and were adjusted accordingly
HNO3 HCI NaOH
If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
tiles Sample(s)
COMMENTS:
H2SO4
were received with headspace
DOC. QA.002 Rev 1
°C

i
aL
I
rk
ion
.. . ........
.. ...
F--j!

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Morehead City WQ Permit Number: WQ0006018
WWTP Name: Town of Morehead City WWTP NPDES Number: NCO026611
Monitoring Pcriod: From 01/01/2022 To 12/31/2022
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. I /A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6'
MPN
<3
31
183
CFU/g
0
Annually
Grab
SM92210E
Coliform
power per gram
of total solids
MPN
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) _
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(I4-DayAerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation) X
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
b�p/ii me✓t. I am aware that there are significant penalties for false certification including fine and imprisonment."
T' r Todd Larson Operations Director
Pre arer Name an Title (type or print) Land App ier Name atW T' le (if applicable) type or print)
2/01/2023
ignature of Preparer* Date Signature A Land Applie if applicable) Date
"Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Environmental Chemists, Inc.
envitrochem 6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab . 910.392.4424 Fax
U.
Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info�a'environmentalchemists.com
Town Of Morehead City Date of Report: May 27, 2022
1100 Bridges Street Customer PO #:
Morehead City NC 28557 Customer ID: 09020011
Attention: Nate Johnson Report #: 2022-09519
Project ID: Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-22864 Site: Sludge 1 5/24/2022 11:00 AM Solid/Sludge Nate Johnson
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 56.4 % 05/25/2022
Fecal Density SM 9221C E-2014 59 MPN/g 05/24/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-22865 Site: Sludge 2 5/24/2022 11:01 AM Solid/Sludge Nate Johnson
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 70.8 % 05/25/2022
Fecal Density SM 9221C E-2014 <3 MPN/g 05/24/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-22866 Site: Sludge 3 5/24/2022 11:02 AM Solid/Sludge Nate Johnson
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 66.9 % 05/25/2022
Fecal Density SM 9221C E-2014 35 MPN/g 05/24/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-22867 Site: Sludge 4 5/24/2022 11:03 AM Solid/Sludge Nate Johnson
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 59.3 % 05/25/2022
Fecal Density SM 9221C E-2014 39 MPN/g 05/24/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-22868 Site: Sludge 5 5/24/2022 11:04 AM Solid/Sludge Nate Johnson
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 64.8 % 05/25/2022
Fecal Density SM 9221C E-2014 41 MPN/g 05/24/2022
ReportC 2022-09519 Page 1 of 2

4111111
Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Town Of Morehead City
Date of Report: May 27, 2022
1100 Bridges Street
Customer PO M
Morehead City NC
28557
Customer ID: 09020011
Attention: Nate Johnson
Report M 2022-09519
Project ID: Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-22869 Site: Sludge 6
5/24/2022
11:05 AM Solid/Sludge Nate Johnson
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
60.3 % 05/25/2022
Fecal Density
SM 9221C E-2014
183 MPN/g 05/24/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-22870 Site: Sludge 7
5/24/2022
11:06 AM Solid/Sludge Nate Johnson
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
69.5 % 05/25/2022
Fecal Density
SM 9221C E-2014
16 MPN/g 05/24/2022
Comment: Results reported on a dry weight basis.
Reviewed by:
f
Report #:: 2022-09519 Page 2 of 2

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client:l�l�l�G� (�) Date: Report Number: a s V l 1
Receipt of sample: ECHEM Pickup Client Delivery ❑
JUPS ❑ FeclEx ❑ Other ❑
❑ YES
❑ NO
N/A
1. Were custody seals present on the cooler?
❑ YES
I0 NO
N/A
2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt "C
How temperature taken: ❑ Temperature Blank Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor "C: 0.0
❑ YES
❑ NO
3. If temperature of cooler exceeded 6`C, was Project Mgr./QA notified?
YES
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
fl�l YES
❑ NO
5. Were sample ID's listed on the COC?
YES
❑ NO
6. Were samples ID's listed on sample containers?
YES
❑ NO
7. Were collection date and time listed on the COC?
YES
❑ NO
8. Were tests to be performed listed on the COC?
YES
❑ NO
9. Did samples arrive in proper containers for each test?
YES
❑ NO
10 Did samples arrive in good condition for each test?
YES
❑ NO
11. Was adequate sample volume availableT
YES
❑ NO
12. Were samples received within proper holding time for requested tests?
❑ YES
❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES
❑ YES ill
❑ NO
NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. OA.002 Rev 1

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SECTION 6

Agricultural Lime Application Log
Year 2022
Project Morehead City
Fields
Soil
Lime Requirements
Tons/Acre
Date
(state -county -site-fieldl
PH
(from soil analvsisl
Applied
A liied
CR-01-1
5.6
0.8T
N/A
CR-01-2
5.7
0.3T
N/A
CR-01-3
5.7
0.7T
N/A
ON-1-1
5.7
0.5T
N/A
ON-1-2
5.8
0AT
N/A
ON-1-3
5.8
0AT
N/A
N/A -Did not apply in 2022
*Lime will be applied when field conditions/cropping pattern permits

SECTION 7

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