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HomeMy WebLinkAboutWQ0037135_2022 Residual Annual Report_20230227Initial Review Reviewer Nathaniel.Thornburg Is this submittal an application? (Excluding additional information.) * Yes No If not an application what is the submittal type?* Annual Report Residual Annual Report Additional Information Other Annual Report Year* 2022 Permit Number (IR)* WQ0037135 Applicant/Permittee U.S. Biosolids, Inc. Email Notifications Does this need review by the hydrogeologist? * Yes U No Regional Office Winston-Salem CO Reviewer Admin Reviewer Submittal Form Project Contact Information Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence. ..................................................................................................................................................................................................................................................................................... ... ... ... ... ... .. ... ... ... ... .. Name* Zach Key Email Address* zachkey@usbiosolids.com Project Information ......................... Application/Document Type* New (Fee Required) Modification - Major (Fee Required) Renewal with Major Modification (Fee Required) Annual Report Additional Information Other Phone Number* 3367776909 Modification - Minor Renewal GW-59, NDMR, NDMLR, NDAR-1, N DAR-2 Residual Annual Report Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* Wastewater Irrigation High -Rate Infiltration Other Wastewater Reclaimed Water Closed -Loop Recycle Residuals Single -Family Residence Wastewater Other Irrigation Permit Number:* WQ0037135 Has Current Existing permit number Applicant/Permittee Address* PO BOX 146 RONDA, NC 28670 Facility Name* U.S. Biosolids Class B Residuals Program Please provide comments/notes on your current submittal below. Land Application Annual Report for U.S. Biosolids, Inc. Permit No. WQ0037135 At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here. (Application Form, Engineering Plans, Specifications, Calculations, Etc.) 2022 Annual Report WQ0037135.pdf 8.35MB Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger than upload limit. * By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Submission Date 2/27/2023 County:Year: Land Application Operator:Phone: Land application of residuals as allowed by the permit occurred during the past calendar year? No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summary: Part B - Annual Compiance Statement: Facility was compliant during calendar year 2022 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Resources.Yes No 1) 2) 3) 4) 5) 6) 7) 8) 9) 10) 11) 12) 13) Part C - Certification: Permittee Name and Title (type or print)Signature of Permittee Signature of Preparer*Signature of Land Applier (if different from Permittee)(if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. Date 16 Total amount of dry tons applied during the year for all application sites: All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. Date Only residuals approved for this permit were applied to the permitted sites. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. Total number of acres utilizes for land application during the year: Yes Facility Name (as shown on permit):U.S. Biosolids, Inc. U.S. Biosolids, Inc. Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. All buffer requirements as specified on the permit were maintained during each application of residuals. 486.84 182.74 Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. Date ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#:WQ0037135 Wilkes 2022 All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). Total number of application fields in the permit:49 Total number of fields utilized for land application during the year: 336-777-6909 DENR FORM ACF (12/2006) 2-24-2023 2-24-2023 2-24-2023 Zach Key U.S. Biosolids, Inc. WQ Permit Number:1) Facility Name: 2) 3) 4) WWTP Name:5) Residual Analysis Data Parameter (mg/kg)3-14-22 Percent Solids (%)NA 2.95 Arsenic 75 16.7 Cadmium 85 3.33 Copper 4,300 205 Chromium NA 24.4 Lead 840 17.7 Mercury 57 2.91 Molybdenum 75 8.33 Nickel 420 17.7 Selenium 100 16.7 Zinc 7,500 517 Total Phosphorus NA 31100 TKN NA 43000 Ammonia-Nitrogen NA 5170 Nitrate and Nitrite NA 159 *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Signature of Preparer *Date Yadkin Valley Sewer Authority Sample or Composite Date ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ0037135 U.S. Biosolids, Inc. Residual Source WQ # or NPDES #:NC0020567 Waypoint AnalyticalLaboratory: “I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.” a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. Conc. Limit (mg/kg)a DENR FORM RSSF (12/2006) 2-24-2023 WQ Permit Number:1) Facility Name: 2) 3) 4) WWTP Name:5) Residual Analysis Data Parameter (mg/kg)3-14-22 pH 6 Aluminum 59700 Calcium 7670 Iron 20500 Manganese 483 Magnesium 3170 Potassium 5400 Sodium 2170 PAN 14093 SAR 0.97 *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Residual Source NPDES # or WQ#: WQ0037135 U.S. Biosolids, Inc. NC0020567 Signature of Preparer *Date Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. Yadkin Valley Sewer Authority Laboratory: Sample or Composite Date “I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.” Waypoint Analytical DENR FORM RSSF - B (12/2006) 2-24-2023 ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may, contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B NVQ Permit Number: WQ00371 35 Laboratory: 1) Facility Name: ToNn of North Wilkesboro 2) Residual Source WQ # or N00020761 3) NPDFS #: ;) WN'TP Name: Thurmond Street W Wl P 5) Residual Analvsis Data Cone. Sample or Composite Date Parameter Limit 5-1 3_22 Percent Solids (0/0 NA 1.65 Arsenic 75 29.4 Cadmium 85 5.88 Copper 4,100 71-4 Chromium \A 88.2 Lead 840 61.8 Mercun 57 8 Mokbdenurn 75 14.7 Nickel 420 3)6.2 Selenium lo0 29.4 /111c 7.500 1960 Total Phosphorus NA 10000 Ili\ \A 67000 Antinonin-Nitrogen \A 11700 Nitrate and Nitrite \A 283 For surface di}posal facihlics the ceiling concentration limits listed in this form are nut applicable Reference the mdwdual permit for metals lunits "1 certify, under penalty of lm, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ignahtre of Preparer * Date *Preparer is defined in 40 CFR Part 503 9(r) and 15A NCAC'_T 1101 (26) DENR FORM RSSF (1212006) ANNEAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were anal zed for over the past calendar year. Use additional forms as needed. WQ Permit Number: WQOU)71 ;5 Facility Name: Residual Source NPI)ES # or WQ#: WWTP Name: Residual Analvsis Data I Parameter 'fo�wn ol'North Wilkesboro NC0020761 l'hurmond Street WWTP Laboratory: I ) 2) 3) 4) Sample or Composite Date Waypoint Analytical Potassium 6590 Sulltln- 14'_U(1 Calcium 19;00 Magne,nim 45811 Sodnum i01O Iron 2840U ma�'anese 441 Organic \ 5394t) p11 7.2 I Aluminum 57800 SA1t I a64 I I 1 PAS I I I I I I I I I I I "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance w ith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of tines and imprisonment for knowing violations." p&�/Z-e D�-/0-.2 Si_nature of Preparer * Date *Prepares is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26) DENR FORM RSSF - B (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: W000+7105 Facility Name: Residual Source WQ # or N'PDES 9: WWTP Name: Residual Anatvsis Data Forest City W\VTP NCO025994 Forest Cite W W7 P Cone. Parameter Limit (mg/kg) (mg/kg)° 3- 14- " Percent Solids (%) NA 14.5 Arsenic 75 4.08 Cadmium 85 1.88 Copper 4,300 321 Chromium NA 37 Lead 840 52.3 Mercury 57 0.537 MoINbdenUm 75 6.75 Nickel 420 13.2 Selenium )00 9.1 Zinc 7,500 1260 Total Phosphorus NA 22300 TKN I NA i 52500 Ammonia -Nitrogen NA I 690 Nitrate, Nitrite NA 46.6 For surface disposal facilities the ceiling concentration limits fisted in this form are n Laboratory: 1) 2) 3) 4) 5) Sample or Composite Date WaNpoint Analytical )t applicable. Reference the individual permit for metals limits. "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly, gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of eparer * Date *Preparer is defined in 40 CFR Part 503.9(1 ) and I5A \CAC 2T .1102 (26) DENR FORM RSSF (12/2006) ANNEAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling anal sis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: W00037105 Facility Name: Residual Source NPDES # or WQ#: WWTP Name: Residual Analvsis Data Parameter (mg/kg) 3-11-22 Organic N 52480 pH 5.4 Aluminum 22900 Calcium 9240 iron 13400 Maganese 172 Magnesium 2900 Potassium 4390 Sulfur 8550 PAS 17520.6 SAR 0.63 Forest City W WTP NC0025984 Forest City W WTP Laboratory: I ) 2) 3) 4) 5) Sample or Composite Date Waypoint Analytical "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." //� 1-)3-J) Sinanue of Preparer * / L� Date *Preparer is defined tf 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF - B (12/2006) WQ Permit Number:1) Facility Name: 2) 3) 4) WWTP Name:5) Residual Analysis Data Parameter (mg/kg)3-4-22 Percent Solids (%)NA 3.39 Arsenic 75 14.7 Cadmium 85 2.94 Copper 4,300 335 Chromium NA 65.3 Lead 840 22.3 Mercury 57 1.08 Molybdenum 75 7.35 Nickel 420 21.7 Selenium 100 14.7 Zinc 7,500 1960 Total Phosphorus NA 27400 TKN NA 3100 Ammonia-Nitrogen NA 2940 Nitrate and Nitrite NA 721 *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Laboratory: “I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.” a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. Conc. Limit (mg/kg)a ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ0037135 U.S. Biosolids, Inc. Residual Source WQ # or NPDES #:NC0021181 Waypoint Analytical Signature of Preparer *Date Belmont WWTP Sample or Composite Date DENR FORM RSSF (12/2006) 2-24-2023 WQ Permit Number:1) Facility Name: 2) 3) 4) WWTP Name:5) Residual Analysis Data Parameter (mg/kg)3-14-22 Potassium 3240 Sulfur 9470 Calcium 16000 Magnesium 3470 Sodium 7820 Iron 28300 Aluminum 51200 Manganese 1160 Organic N 32060 PAN 10939 SAR 2.677 pH 5.9 *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Sample or Composite Date “I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.” Waypoint Analytical Signature of Preparer *Date Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. Belmont WWTP Laboratory: ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Residual Source NPDES # or WQ#: WQ0037135 U.S. Biosolids, Inc. NC0021181 DENR FORM RSSF - B (12/2006) 2-24-2023 WQ Permit Number:1) Facility Name: 2) 3) 4) WWTP Name:5) Residual Analysis Data Parameter (mg/kg)4-26-22 Percent Solids (%)NA 1.57 Arsenic 75 31.3 Cadmium 85 6.25 Copper 4,300 306 Chromium NA 18.9 Lead 840 19.3 Mercury 57 8.94 Molybdenum 75 15.6 Nickel 420 15.6 Selenium 100 31.3 Zinc 7,500 1460 Total Phosphorus NA 29800 TKN NA 114000 Ammonia-Nitrogen NA 8310 Nitrate and Nitrite NA 287 *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Laboratory: “I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.” a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. Conc. Limit (mg/kg)a ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ0037135 U.S. Biosolids, Inc. Residual Source WQ # or NPDES #:NC0025861 Waypoint Analytical Signature of Preparer *Date Lowell WWTP Sample or Composite Date DENR FORM RSSF (12/2006) 2-24-2023 WQ Permit Number:1) Facility Name: 2) 3) 4) WWTP Name:5) Residual Analysis Data Parameter (mg/kg)4-26-22 Sulfur 10400 Calcium 14200 Aluminum 8000 Manganese 1000 Organic N 105400 Potassium 7500 Magnesium 4060 Sodium 5010 Iron 42400 pH 6.7 SAR 1.19 PAN 36149 *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Sample or Composite Date “I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.” Waypoint Analytical Signature of Preparer *Date Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. Lowell WWTP Laboratory: ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Residual Source NPDES # or WQ#: WQ0037135 U.S. Biosolids, Inc. NC0025861 DENR FORM RSSF - B (12/2006) 2-24-2023 Owner:Predominant Soil Series: Site #:Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): % Solids 2.95 Arsenic 16.7 Cadmium 3.33 Copper 205 Chromium 24.4 Lead 17.7 Mercury 2091 Molyb- denum 8.33 Nickel 17.7 Selenium 16.7 Zinc 517 Total Phos- phorus 31100 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 5.00 To t a l s : Arsenic 0.167 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.167 Cadmium 0.033 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.033 Copper 2.049 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.049 Chromium 0.244 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.244 Lead 0.177 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.177 Mercury 20.902 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 20.902 Molyb- denum 0.083 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.083 Nickel 0.177 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.177 Selenium 0.167 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.167 Zinc 5.168 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 5.168 Total Phos- phorus 310.876 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 310.876 Signature of Land Applier 1 Date __________________________________________________________ Sample or Com- posite Date ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name:U.S. Biosolids, Inc.55.18Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Acres Permitted: WQ0037135 11.04 11.04 NC-WK-BP FcB2William PorterWilliam Porter "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Permit #: Operator: Acres Used: 3/14/22 1 2 3 4 5 6 7 8 9 11 12 1 2 3 4 5 6 7 8 9 10 11 12 10 DENR FORM MFLSF (12/2006) 2-24-2023 Facility Name:WQ Permit #:Field #:Acres Utilized: Land Owner:Annual Dry Tons Applied:Site #:Acres Permitted: Operator:Predominant Soil Series:Cation Exchange Capacity (non 503): Crop 1 Name:Crop 1 Max. PAN:Crop 2 Name:Crop 2 Max. PAN: Volume Applied per Acre Precip. Past 24 Hrs. TKN Am m o n i a Ni t r o g e n Nitrate and Nitrite Cu. Yds Gallons (Dry Tons/Ac)inches mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 3-2022 299000 2.95 3.332 dry 0 s 0.5 0.3 43000 5170 159 93.906 NA Corn 11-2022 149500 2.95 1.666 dry 0 s 0.5 0.3 43000 5170 159 46.953 NA Corn 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 TOTALS:0 448500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 140.859 0.000 Annual lbs/acre 0.167 0.033 2.049 0.244 0.177 20.902 0.083 0.177 0.167 5.168 310.876 Date lbs/ac Prior Years Cumulative lbs/ac 0.169 0.039 9.672 1.847 0.872 0.03 0.16 2.103 0.121 24.672 12-22 1000 Current Cumulative lbs/ac 0.336 0.072 11.721 2.091 1.049 20.932 0.243 2.280 0.288 29.840 Permitted C. P. L. R.****36 34 1338 NA 267 15 NA 374 89 2498 Permit PAN Limit 1st/2nd Crop 207 *Application Method: S - Surface, IN - Injection, INC - Incorporation Date ****C.P.L.R.: Cumulative Pollutant Loading Rate 207Corn PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. “I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.” PAN Applied ( lbs/acre) Signature of Land Applier Lime Applied **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 Da t e o r Mo n t h % Solids Volume applied (enter one) Solids/ Liquid Mi n e r a l i z a t i o n Ra t e * * * Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Vo l a t i l i z a t i o n Ra t e * * Ap p l i c a t i o n Me t h o d * U.S. Biosoilds Inc. William Porter William Porter WQ0037135 55.1722 FcB2 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): NC-WK-BP 1 11.04 11.04 Name of Crop Type Receiving Residual Application NC00205967 NC00205967 DENR FORM FSF (12/2006) 2-24-2023 Owner:Predominant Soil Series: Site #:Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): % Solids 1.65 2.95 Arsenic 29.4 16.7 Cadmium 5.88 3.33 Copper 724 205 Chromium 88.2 24.4 Lead 61.8 17.7 Mercury 8 2.91 Molyb- denum 14.7 8.33 Nickel 36.2 17.7 Selenium 29.4 16.7 Zinc 1960 517 Total Phos- phorus 30600 31100 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 2.17 0.42 To t a l s : Arsenic 0.128 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.142 Cadmium 0.026 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 Copper 3.141 0.173 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.313 Chromium 0.383 0.021 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.403 Lead 0.268 0.015 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.283 Mercury 0.035 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.037 Molyb- denum 0.064 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.071 Nickel 0.157 0.015 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.172 Selenium 0.128 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.142 Zinc 8.502 0.435 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 8.938 Total Phos- phorus 132.743 26.186 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 158.929 Signature of Land Applier "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Permit #: Operator: Acres Used: 5/13/22 3/14/22 WQ0037135 26.6 26.6 NC-WK-BP FcB2William PorterWillaim Porter Sample or Com- posite Date ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name:U.S. Biosolids, Inc.68.89Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Acres Permitted:4 Date __________________________________________________________ 1 2 3 4 5 6 7 8 9 11 12 1 2 3 4 5 6 7 8 9 10 11 12 10 DENR FORM MFLSF (12/2006) 2-24-2023 Facility Name:WQ Permit #:Field #:Acres Utilized: Land Owner:Annual Dry Tons Applied:Site #:Acres Permitted: Operator:Predominant Soil Series:Cation Exchange Capacity (non 503): Crop 1 Name:Crop 1 Max. PAN:Crop 2 Name:Crop 2 Max. PAN: Volume Applied per Acre Precip. Past 24 Hrs. TKN Am m o n i a Ni t r o g e n Nitrate and Nitrite Cu. Yds Gallons (Dry Tons/Ac)inches mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 5-2022 838500 1.65 2.169 dry 0 s 0.5 0.3 67600 13700 283 101.084 NA Corn 11-202 91000 2.95 0.421 dry 0 s 0.5 0.3 43000 5170 159 11.862 NA Corn 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 TOTALS:0 929500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 112.946 0.000 Annual lbs/acre 0.142 0.028 3.313 0.403 0.283 0.037 0.071 0.172 0.142 8.938 158.929 Date lbs/ac Prior Years Cumulative lbs/ac 0.237 0.045 9.98 1.853 0.864 0.033 0.157 3.428 0.146 20.477 12-2022 1000 Current Cumulative lbs/ac 0.379 0.073 13.293 2.256 1.147 0.070 0.228 3.600 0.288 29.415 Permitted C. P. L. R.****36 34 1338 NA 67 15 NA 374 89 2498 Permit PAN Limit 1st/2nd Crop 207 *Application Method: S - Surface, IN - Injection, INC - Incorporation Date ****C.P.L.R.: Cumulative Pollutant Loading Rate Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): NC-WK-BP 4 26.6 26.6 Name of Crop Type Receiving Residual Application NC0020567 NC0020761 U.S. Biosolids. Inc. William Porter William Porter WQ0037135 68.8874 FcB2 Da t e o r Mo n t h % Solids Volume applied (enter one) Solids/ Liquid Mi n e r a l i z a t i o n Ra t e * * * Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Vo l a t i l i z a t i o n Ra t e * * Ap p l i c a t i o n Me t h o d * Signature of Land Applier Lime Applied **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. “I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.” PAN Applied ( lbs/acre) 207Corn DENR FORM FSF (12/2006) 2-24-2023 Owner:Predominant Soil Series: Site #:Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): % Solids 2.95 Arsenic 16.7 Cadmium 3.33 Copper 205 Chromium 24.4 Lead 17.7 Mercury 2091 Molyb- denum 8.33 Nickel 17.7 Selenium 16.7 Zinc 517 Total Phos- phorus 31100 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1.16 To t a l s : Arsenic 0.039 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.039 Cadmium 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 Copper 0.475 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.475 Chromium 0.057 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.057 Lead 0.041 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.041 Mercury 4.847 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.847 Molyb- denum 0.019 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.019 Nickel 0.041 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.041 Selenium 0.039 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.039 Zinc 1.198 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.198 Total Phos- phorus 72.090 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 72.090 Signature of Land Applier "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Permit #: Operator: Acres Used: 3/14/22 WQ0037135 3.45 3.45 NC-WK-CM FcB2Carolyn McCannCarolyn McCann Sample or Com- posite Date ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name:U.S. Biosolids, Inc.4.00Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Acres Permitted:1 Date __________________________________________________________ 1 2 3 4 5 6 7 8 9 11 12 1 2 3 4 5 6 7 8 9 10 11 12 10 DENR FORM MFLSF (12/2006) 2-24-2023 Facility Name:WQ Permit #:Field #:Acres Utilized: Land Owner:Annual Dry Tons Applied:Site #:Acres Permitted: Operator:Predominant Soil Series:Cation Exchange Capacity (non 503): Crop 1 Name:Crop 1 Max. PAN:Crop 2 Name:Crop 2 Max. PAN: Volume Applied per Acre Precip. Past 24 Hrs. TKN Am m o n i a Ni t r o g e n Nitrate and Nitrite Cu. Yds Gallons (Dry Tons/Ac)inches mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 9-2022 32500 2.95 1.159 dry 0 s 0.5 0.3 43000 5170 159 32.663 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 TOTALS:0 32500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 32.663 0.000 Annual lbs/acre 0.039 0.008 0.475 0.057 0.041 4.847 0.019 0.041 0.039 1.198 72.090 Date lbs/ac Prior Years Cumulative lbs/ac 0 0 0 0 0 0 0 0 0 0 12-22 2000 Current Cumulative lbs/ac 0.039 0.008 0.475 0.057 0.041 4.847 0.019 0.041 0.039 1.198 Permitted C. P. L. R.****36 34 1338 NA 267 15 NA 374 89 2498 Permit PAN Limit 1st/2nd Crop 188 *Application Method: S - Surface, IN - Injection, INC - Incorporation Date ****C.P.L.R.: Cumulative Pollutant Loading Rate Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): NC-WK-CM 1 3.45 3.45 Name of Crop Type Receiving Residual Application NC0020567 U.S. Biosolids, Inc. Carolyn McCann Carolyn McCann WQ0037135 3.9980 FcB2 Da t e o r Mo n t h % Solids Volume applied (enter one) Solids/ Liquid Mi n e r a l i z a t i o n Ra t e * * * Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Vo l a t i l i z a t i o n Ra t e * * Ap p l i c a t i o n Me t h o d * Signature of Land Applier Lime Applied **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. “I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.” PAN Applied ( lbs/acre) 188Fescue DENR FORM FSF (12/2006) 2-24-2023 Owner:Predominant Soil Series: Site #:Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): % Solids 14.5 Arsenic 4.08 Cadmium 1.88 Copper 321 Chromium 37 Lead 52.3 Mercury 0.537 Molyb- denum 6.75 Nickel 132 Selenium 9.1 Zinc 1260 Total Phos- phorus 22300 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 4.40 To t a l s : Arsenic 0.036 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.036 Cadmium 0.017 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.017 Copper 2.822 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.822 Chromium 0.325 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.325 Lead 0.460 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.460 Mercury 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Molyb- denum 0.059 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.059 Nickel 1.161 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.161 Selenium 0.080 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.080 Zinc 11.078 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 11.078 Total Phos- phorus 196.062 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 196.062 Signature of Land Applier "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Permit #: Operator: Acres Used: 3/14/22 WQ0037135 5.5 5.5 NC-RU-FC PbB2Forest CaltonForest Calton Sample or Com- posite Date ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name:U.S. Biosolids, Inc.24.18Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Acres Permitted:2 Date __________________________________________________________ 1 2 3 4 5 6 7 8 9 11 12 1 2 3 4 5 6 7 8 9 10 11 12 10 DENR FORM MFLSF (12/2006) 2-24-2023 Facility Name:WQ Permit #:Field #:Acres Utilized: Land Owner:Annual Dry Tons Applied:Site #:Acres Permitted: Operator:Predominant Soil Series:Cation Exchange Capacity (non 503): Crop 1 Name:Crop 1 Max. PAN:Crop 2 Name:Crop 2 Max. PAN: Volume Applied per Acre Precip. Past 24 Hrs. TKN Am m o n i a Ni t r o g e n Nitrate and Nitrite Cu. Yds Gallons (Dry Tons/Ac)inches mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 3-2022 88 14.5 1.954 dry 0 s 0.5 0.3 52500 690 46.6 62.267 NA Fescue 7-2022 110 14.5 2.442 dry 0 s 0.5 0.3 52500 690 46.6 77.834 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 TOTALS:198 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 140.102 0.000 Annual lbs/acre 0.036 0.017 2.822 0.325 0.460 0.005 0.059 1.161 0.080 11.078 196.062 Date lbs/ac Prior Years Cumulative lbs/ac 0.069 0.053 4.123 0.598 1.154 0.2 0.122 0.262 0.418 16.01 0 Current Cumulative lbs/ac 0.105 0.070 6.945 0.923 1.614 0.205 0.181 1.423 0.498 27.088 Permitted C. P. L. R.****36 34 1338 NA 267 15 NA 374 89 2498 Permit PAN Limit 1st/2nd Crop 178 *Application Method: S - Surface, IN - Injection, INC - Incorporation Date ****C.P.L.R.: Cumulative Pollutant Loading Rate Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): NC-RU-FC 2 5.5 5.5 Name of Crop Type Receiving Residual Application NC0025984 NC0025984 U.S. Biosolids, Inc. Forest Calton Forest Calton WQ0037135 24.1788 PbB2 Da t e o r Mo n t h % Solids Volume applied (enter one) Solids/ Liquid Mi n e r a l i z a t i o n Ra t e * * * Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Vo l a t i l i z a t i o n Ra t e * * Ap p l i c a t i o n Me t h o d * Signature of Land Applier Lime Applied **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. “I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.” PAN Applied ( lbs/acre) 178Fescue DENR FORM FSF (12/2006) 2-24-2023 Owner:Predominant Soil Series: Site #:Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): % Solids 14.5 Arsenic 4.08 Cadmium 1.88 Copper 321 Chromium 37 Lead 52.3 Mercury 0.537 Molyb- denum 6.75 Nickel 13.2 Selenium 9.1 Zinc 1260 Total Phos- phorus 22300 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 2.81 To t a l s : Arsenic 0.023 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023 Cadmium 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Copper 1.805 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.805 Chromium 0.208 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.208 Lead 0.294 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.294 Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- denum 0.038 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.038 Nickel 0.074 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.074 Selenium 0.051 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.051 Zinc 7.086 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 7.086 Total Phos- phorus 125.415 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 125.415 Signature of Land Applier 3 Date __________________________________________________________ Sample or Com- posite Date ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name:U.S. Biosolids, Inc. 24.18Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Acres Permitted: WQ0037135 8.6 8.6 NC-RU-FC PbB2Forest CaltonForest Calton "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Permit #: Operator: Acres Used: 3/14/22 1 2 3 4 5 6 7 8 9 11 12 1 2 3 4 5 6 7 8 9 10 11 12 10 DENR FORM MFLSF (12/2006) 2-24-2023 Facility Name:WQ Permit #:Field #:Acres Utilized: Land Owner:Annual Dry Tons Applied:Site #:Acres Permitted: Operator:Predominant Soil Series:Cation Exchange Capacity (non 503): Crop 1 Name:Crop 1 Max. PAN:Crop 2 Name:Crop 2 Max. PAN: Volume Applied per Acre Precip. Past 24 Hrs. TKN Am m o n i a Ni t r o g e n Nitrate and Nitrite Cu. Yds Gallons (Dry Tons/Ac)inches mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 3-2022 44 14.5 0.625 dry 0 s 0.5 0.3 52500 690 46.6 19.911 NA Fescue 8-2022 154 14.5 2.187 dry 0 s 0.5 0.3 52500 690 46.6 69.689 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 TOTALS:198 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 89.600 0.000 Annual lbs/acre 0.023 0.011 1.805 0.208 0.294 0.003 0.038 0.074 0.051 7.086 125.415 Date lbs/ac Prior Years Cumulative lbs/ac 0.065 0.052 3.843 0.551 1.086 0.016 0.115 0.248 0.415 14.86 0 Current Cumulative lbs/ac 0.088 0.063 5.648 0.759 1.380 0.019 0.153 0.322 0.466 21.946 Permitted C. P. L. R.****36 34 1338 NA 267 15 NA 374 89 2498 Permit PAN Limit 1st/2nd Crop 178 *Application Method: S - Surface, IN - Injection, INC - Incorporation Date ****C.P.L.R.: Cumulative Pollutant Loading Rate 178Fescue PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. “I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.” PAN Applied ( lbs/acre) Signature of Land Applier Lime Applied **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 Da t e o r Mo n t h % Solids Volume applied (enter one) Solids/ Liquid Mi n e r a l i z a t i o n Ra t e * * * Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Vo l a t i l i z a t i o n Ra t e * * Ap p l i c a t i o n Me t h o d * U.S. Biosolids, Inc. Forest Calton Forest Calton WQ0037135 24.1788 PbB2 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): NC-RU-FC 3 8.6 8.6 Name of Crop Type Receiving Residual Application NC0025984 NC0025984 DENR FORM FSF (12/2006) 2-24-2023 Owner:Predominant Soil Series: Site #:Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): % Solids 14.5 Arsenic 4.08 Cadmium 1.88 Copper 321 Chromium 37 Lead 52.3 Mercury 0.537 Molyb- denum 6.75 Nickel 13 Selenium 9.1 Zinc 1260 Total Phos- phorus 22300 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 2.58 To t a l s : Arsenic 0.021 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.021 Cadmium 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.010 Copper 1.653 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.653 Chromium 0.191 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.191 Lead 0.269 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.269 Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- denum 0.035 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.035 Nickel 0.067 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.067 Selenium 0.047 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.047 Zinc 6.489 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 6.489 Total Phos- phorus 114.845 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 114.845 Signature of Land Applier 2 Date __________________________________________________________ Sample or Com- posite Date ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name:U.S. Biosolids, Inc, 43.00Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Acres Permitted: WQ0037135 16.7 16.7 NC-RU-FLB PbB2Frank LawsonFrank Lawson "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Permit #: Operator: Acres Used: 3/14/22 1 2 3 4 5 6 7 8 9 11 12 1 2 3 4 5 6 7 8 9 10 11 12 10 DENR FORM MFLSF (12/2006) 2-24-2023 Facility Name:WQ Permit #:Field #:Acres Utilized: Land Owner:Annual Dry Tons Applied:Site #:Acres Permitted: Operator:Predominant Soil Series:Cation Exchange Capacity (non 503): Crop 1 Name:Crop 1 Max. PAN:Crop 2 Name:Crop 2 Max. PAN: Volume Applied per Acre Precip. Past 24 Hrs. TKN Am m o n i a Ni t r o g e n Nitrate and Nitrite Cu. Yds Gallons (Dry Tons/Ac)inches mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 2-2022 66 14.5 0.483 dry 0 s 0.5 0.3 52500 690 46.6 15.380 NA Fescue 3-2022 121 14.5 0.885 dry 0 s 0.5 0.3 52500 690 46.6 28.197 NA Fescue 5-2022 99 14.5 0.724 dry 0 s 0.5 0.3 52500 690 46.6 23.071 NA Fescue 7-2022 44 14.5 0.322 dry 0 s 0.5 0.3 52500 690 46.6 10.254 NA Fescue 9-2022 22 14.5 0.161 dry 0 s 0.5 0.3 52500 690 46.6 5.127 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 TOTALS:352 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 82.029 0.000 Annual lbs/acre 0.021 0.010 1.653 0.191 0.269 0.003 0.035 0.067 0.047 6.489 114.845 Date lbs/ac Prior Years Cumulative lbs/ac 0.068 0.039 3.976 0.45 1.085 0.011 0.099 0.203 0.383 15.949 12-22 2000 Current Cumulative lbs/ac 0.089 0.049 5.629 0.641 1.354 0.014 0.134 0.270 0.430 22.438 Permitted C. P. L. R.****36 34 1338 NA 267 15 NA 374 89 2498 Permit PAN Limit 1st/2nd Crop 178 *Application Method: S - Surface, IN - Injection, INC - Incorporation Date ****C.P.L.R.: Cumulative Pollutant Loading Rate 178Fescue NC0025984 NC0025984 PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. “I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.” PAN Applied ( lbs/acre) Signature of Land Applier Lime Applied **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 Da t e o r Mo n t h % Solids Volume applied (enter one) Solids/ Liquid Mi n e r a l i z a t i o n Ra t e * * * Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Vo l a t i l i z a t i o n Ra t e * * Ap p l i c a t i o n Me t h o d * U.S. Biosolids,Inc. Frank Lawson Frank Lawson WQ0037135 42.9845 PbB2 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): NC-RU-FLB 2 16.7 16.7 Name of Crop Type Receiving Residual Application NC0025984 NC0025984 NC0025984 DENR FORM FSF (12/2006) 2-24-2023 Owner:Predominant Soil Series: Site #:Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): % Solids 14.5 Arsenic 4.08 Cadmium 1.88 Copper 321 Chromium 37 Lead 52.3 Mercury 0.537 Molyb- denum 6.75 Nickel 13.2 Selenium 9.1 Zinc 1260 Total Phos- phorus 22300 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 3.36 To t a l s : Arsenic 0.027 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.027 Cadmium 0.013 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013 Copper 2.156 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.156 Chromium 0.248 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.248 Lead 0.351 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.351 Mercury 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- denum 0.045 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.045 Nickel 0.089 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.089 Selenium 0.061 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.061 Zinc 8.462 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 8.462 Total Phos- phorus 149.767 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 149.767 Signature of Land Applier 1 Date __________________________________________________________ Sample or Com- posite Date ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name:U.S. Biosolids, Inc.26.86Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Acres Permitted: WQ0037135 8 8 NC-RU-LB PbB2Larry BaileyLarry Bailey "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Permit #: Operator: Acres Used: 3/14/22 1 2 3 4 5 6 7 8 9 11 12 1 2 3 4 5 6 7 8 9 10 11 12 10 DENR FORM MFLSF (12/2006) 2-24-2023 Facility Name:WQ Permit #:Field #:Acres Utilized: Land Owner:Annual Dry Tons Applied:Site #:Acres Permitted: Operator:Predominant Soil Series:Cation Exchange Capacity (non 503): Crop 1 Name:Crop 1 Max. PAN:Crop 2 Name:Crop 2 Max. PAN: Volume Applied per Acre Precip. Past 24 Hrs. TKN Am m o n i a Ni t r o g e n Nitrate and Nitrite Cu. Yds Gallons (Dry Tons/Ac)inches mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 1-2022 77 14.5 1.175 dry 0 s 0.5 0.3 52500 690 46.6 37.458 NA Fescue 3-2022 110 14.5 1.679 dry 0 s 0.5 0.3 52500 690 46.6 53.511 NA Fescue 5-2022 33 14.5 0.504 dry 0 s 0.5 0.3 52500 690 46.6 16.053 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 TOTALS:220 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 107.022 0.000 Annual lbs/acre 0.027 0.013 2.156 0.248 0.351 0.004 0.045 0.089 0.061 8.462 149.767 Date lbs/ac Prior Years Cumulative lbs/ac 0.11 0.082 6.823 0.801 1.744 0.027 0.18 0.371 0.487 28.306 0 Current Cumulative lbs/ac 0.137 0.095 8.979 1.049 2.095 0.031 0.225 0.460 0.548 36.768 Permitted C. P. L. R.****36 34 1338 NA 267 15 NA 374 89 2498 Permit PAN Limit 1st/2nd Crop 178 *Application Method: S - Surface, IN - Injection, INC - Incorporation Date ****C.P.L.R.: Cumulative Pollutant Loading Rate 178Fescue PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. “I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.” PAN Applied ( lbs/acre) Signature of Land Applier Lime Applied **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 Da t e o r Mo n t h % Solids Volume applied (enter one) Solids/ Liquid Mi n e r a l i z a t i o n Ra t e * * * Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Vo l a t i l i z a t i o n Ra t e * * Ap p l i c a t i o n Me t h o d * U.S. Biosolids, Inc. Larry Bailey Larry Bailey WQ0037135 26.8653 PbB2 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): NC-RU-LB 1 8 8 Name of Crop Type Receiving Residual Application NC0025984 NC0025984 NC0025984 DENR FORM FSF (12/2006) 2-24-2023 Owner:Predominant Soil Series: Site #:Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): % Solids 14.5 Arsenic 4.08 Cadmium 1.88 Copper 321 Chromium 37 Lead 52.3 Mercury 0.537 Molyb- denum 6.75 Nickel 13.2 Selenium 9.1 Zinc 1260 Total Phos- phorus 22300 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 3.76 To t a l s : Arsenic 0.031 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.031 Cadmium 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 Copper 2.412 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.412 Chromium 0.278 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.278 Lead 0.393 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.393 Mercury 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- denum 0.051 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.051 Nickel 0.099 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.099 Selenium 0.068 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.068 Zinc 9.468 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 9.468 Total Phos- phorus 167.562 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 167.562 Signature of Land Applier 2 Date __________________________________________________________ Sample or Com- posite Date ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name:U.S. Biosolids, Inc. 43.96Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Acres Permitted: WQ0037135 11.7 11.7 NC-RU-LB PbB2Larry BaileyLarry Bailey "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Permit #: Operator: Acres Used: 3/14/22 1 2 3 4 5 6 7 8 9 11 12 1 2 3 4 5 6 7 8 9 10 11 12 10 DENR FORM MFLSF (12/2006) 2-24-2023 Facility Name:WQ Permit #:Field #:Acres Utilized: Land Owner:Annual Dry Tons Applied:Site #:Acres Permitted: Operator:Predominant Soil Series:Cation Exchange Capacity (non 503): Crop 1 Name:Crop 1 Max. PAN:Crop 2 Name:Crop 2 Max. PAN: Volume Applied per Acre Precip. Past 24 Hrs. TKN Am m o n i a Ni t r o g e n Nitrate and Nitrite Cu. Yds Gallons (Dry Tons/Ac)inches mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 2-2022 132 14.5 1.378 dry 0 s 0.5 0.3 52500 690 46.6 43.906 NA Fescue 5-2022 88 14.5 0.918 dry 0 s 0.5 0.3 52500 690 46.6 29.271 NA Fescue 9-2022 84 14.5 0.877 dry 0 s 0.5 0.3 52500 690 46.6 27.940 NA Fescue 10-2022 56 14.5 0.584 dry 0 s 0.5 0.3 52500 690 46.6 18.627 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 TOTALS:360 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 119.745 0.000 Annual lbs/acre 0.031 0.014 2.412 0.278 0.393 0.004 0.051 0.099 0.068 9.468 167.562 Date lbs/ac Prior Years Cumulative lbs/ac 0.099 0.08 5.912 0.595 1.494 0.012 0.157 0.316 0.452 24.968 0 Current Cumulative lbs/ac 0.130 0.094 8.324 0.873 1.887 0.016 0.208 0.415 0.520 34.436 Permitted C. P. L. R.****36 34 1338 NA 267 15 NA 374 89 2498 Permit PAN Limit 1st/2nd Crop 178 *Application Method: S - Surface, IN - Injection, INC - Incorporation Date ****C.P.L.R.: Cumulative Pollutant Loading Rate 178Fescue NC0025984 PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. “I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.” PAN Applied ( lbs/acre) Signature of Land Applier Lime Applied **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 Da t e o r Mo n t h % Solids Volume applied (enter one) Solids/ Liquid Mi n e r a l i z a t i o n Ra t e * * * Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Vo l a t i l i z a t i o n Ra t e * * Ap p l i c a t i o n Me t h o d * U.S. Biosolids, Inc. Larry Bailey Larry Bailey WQ0037135 43.9614 PbB2 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): NC-RU-LB 2 11.7 11.7 Name of Crop Type Receiving Residual Application NC0025984 NC0025984 NC0025984 DENR FORM FSF (12/2006) 2-24-2023 Owner:Predominant Soil Series: Site #:Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): % Solids 14.5 Arsenic 4.08 Cadmium 1.88 Copper 321 Chromium 37 Lead 52.3 Mercury 0.537 Molyb- denum 6.75 Nickel 132 Selenium 9.1 Zinc 1260 Total Phos- phorus 22300 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 4.81 To t a l s : Arsenic 0.039 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.039 Cadmium 0.018 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.018 Copper 3.085 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.085 Chromium 0.356 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.356 Lead 0.503 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.503 Mercury 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Molyb- denum 0.065 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.065 Nickel 1.269 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.269 Selenium 0.087 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.087 Zinc 12.111 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 12.111 Total Phos- phorus 214.348 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 214.348 Signature of Land Applier 3 Date __________________________________________________________ Sample or Com- posite Date ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name:U.S. Biosolids, Inc.14.90Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Acres Permitted: WQ0037135 3.1 3.1 NC-RU-LB PbB2Larry BaileyLarry Bailey "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Permit #: Operator: Acres Used: 3/14/22 1 2 3 4 5 6 7 8 9 11 12 1 2 3 4 5 6 7 8 9 10 11 12 10 DENR FORM MFLSF (12/2006) 2-24-2023 Facility Name:WQ Permit #:Field #:Acres Utilized: Land Owner:Annual Dry Tons Applied:Site #:Acres Permitted: Operator:Predominant Soil Series:Cation Exchange Capacity (non 503): Crop 1 Name:Crop 1 Max. PAN:Crop 2 Name:Crop 2 Max. PAN: Volume Applied per Acre Precip. Past 24 Hrs. TKN Am m o n i a Ni t r o g e n Nitrate and Nitrite Cu. Yds Gallons (Dry Tons/Ac)inches mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 2-2022 66 14.5 2.600 dry 0 s 0.5 0.3 52500 690 46.6 82.856 NA Fescue 11-2022 56 14.5 2.206 dry 0 s 0.5 0.3 52500 690 46.6 70.302 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 TOTALS:122 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 153.158 0.000 Annual lbs/acre 0.039 0.018 3.085 0.356 0.503 0.005 0.065 1.269 0.087 12.111 214.348 Date lbs/ac Prior Years Cumulative lbs/ac 0.064 0.046 3.725 0.398 0.895 0.006 0.09 0.172 0.221 16.147 0 Current Cumulative lbs/ac 0.103 0.064 6.810 0.754 1.398 0.011 0.155 1.441 0.308 28.258 Permitted C. P. L. R.****36 34 1338 NA 267 15 NA 374 89 2498 Permit PAN Limit 1st/2nd Crop 178 *Application Method: S - Surface, IN - Injection, INC - Incorporation Date ****C.P.L.R.: Cumulative Pollutant Loading Rate 178Fescue PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. “I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.” PAN Applied ( lbs/acre) Signature of Land Applier Lime Applied **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 Da t e o r Mo n t h % Solids Volume applied (enter one) Solids/ Liquid Mi n e r a l i z a t i o n Ra t e * * * Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Vo l a t i l i z a t i o n Ra t e * * Ap p l i c a t i o n Me t h o d * U.S Bisolids, Inc. Larry Bailey Larry Bailey WQ0037135 14.8980 PbB2 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): NC-RU-LB 3 3.1 3.1 Name of Crop Type Receiving Residual Application NC0025984 NC0025984 DENR FORM FSF (12/2006) 2-24-2023 Owner:Predominant Soil Series: Site #:Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): % Solids 14.5 Arsenic 4.08 Cadmium 1.88 Copper 321 Chromium 37 Lead 52.3 Mercury 0.537 Molyb- denum 6.75 Nickel 132 Selenium 9.1 Zinc 1260 Total Phos- phorus 22300 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 4.27 To t a l s : Arsenic 0.035 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.035 Cadmium 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.016 Copper 2.743 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.743 Chromium 0.316 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.316 Lead 0.447 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.447 Mercury 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Molyb- denum 0.058 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.058 Nickel 1.128 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.128 Selenium 0.078 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.078 Zinc 10.768 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 10.768 Total Phos- phorus 190.576 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 190.576 Signature of Land Applier 4 Date __________________________________________________________ Sample or Com- posite Date ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name:U.S. Biosolids, Inc. 23.07Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Acres Permitted: WQ0037135 5.4 5.4 NC_RU-LB PbB2Larry BaileyLarry Bailey "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Permit #: Operator: Acres Used: 3/14/22 1 2 3 4 5 6 7 8 9 11 12 1 2 3 4 5 6 7 8 9 10 11 12 10 DENR FORM MFLSF (12/2006) 2-24-2023 Facility Name:WQ Permit #:Field #:Acres Utilized: Land Owner:Annual Dry Tons Applied:Site #:Acres Permitted: Operator:Predominant Soil Series:Cation Exchange Capacity (non 503): Crop 1 Name:Crop 1 Max. PAN:Crop 2 Name:Crop 2 Max. PAN: Volume Applied per Acre Precip. Past 24 Hrs. TKN Am m o n i a Ni t r o g e n Nitrate and Nitrite Cu. Yds Gallons (Dry Tons/Ac)inches mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 1-2022 77 14.5 1.741 dry 0 s 0.5 0.3 52500 690 46.6 55.493 NA Fescue 8-2022 56 14.5 1.266 dry 0 s 0.5 0.3 52500 690 46.6 40.358 NA Fescue 11-2022 56 14.5 1.266 dry 0 s 0.5 0.3 52500 690 46.6 40.358 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 TOTALS:189 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 136.210 0.000 Annual lbs/acre 0.035 0.016 2.743 0.316 0.447 0.005 0.058 1.128 0.078 10.768 190.576 Date lbs/ac Prior Years Cumulative lbs/ac 0.076 0.056 4.498 0.419 1.059 0.006 0.108 0.204 0.241 19.779 0 Current Cumulative lbs/ac 0.111 0.072 7.241 0.735 1.506 0.011 0.166 1.332 0.319 30.547 Permitted C. P. L. R.****36 34 1338 NA 267 15 NA 374 89 2498 Permit PAN Limit 1st/2nd Crop 178 *Application Method: S - Surface, IN - Injection, INC - Incorporation Date ****C.P.L.R.: Cumulative Pollutant Loading Rate 178Fescue PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. “I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.” PAN Applied ( lbs/acre) Signature of Land Applier Lime Applied **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 Da t e o r Mo n t h % Solids Volume applied (enter one) Solids/ Liquid Mi n e r a l i z a t i o n Ra t e * * * Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Vo l a t i l i z a t i o n Ra t e * * Ap p l i c a t i o n Me t h o d * U.S. Biosolids, Inc. Larry Bailey Larry Bailey WQ0037135 23.0798 PbB2 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): NC-RU-LB 4 5.4 5.4 Name of Crop Type Receiving Residual Application NC0025984 NC0025984 NC0025984 DENR FORM FSF (12/2006) 2-24-2023 Owner:Predominant Soil Series: Site #:Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): % Solids 2.95 Arsenic 16.7 Cadmium 3.33 Copper 205 Chromium 24.4 Lead 17.7 Mercury 2091 Molyb- denum 8.33 Nickel 17.7 Selenium 16.7 Zinc 517 Total Phos- phorus 31100 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 0.74 To t a l s : Arsenic 0.025 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.025 Cadmium 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Copper 0.303 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.303 Chromium 0.036 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.036 Lead 0.026 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.026 Mercury 3.095 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.095 Molyb- denum 0.012 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.012 Nickel 0.026 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.026 Selenium 0.025 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.025 Zinc 0.765 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.765 Total Phos- phorus 46.028 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 46.028 Signature of Land Applier 1 Date __________________________________________________________ Sample or Com- posite Date ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name:U.S. Biosolid, Inc.10.40Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Acres Permitted: WQ0037135 14.05 14.05 NC-WK-LW FcB2Lee WalkerLee Walker "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Permit #: Operator: Acres Used: 3/14/22 1 2 3 4 5 6 7 8 9 11 12 1 2 3 4 5 6 7 8 9 10 11 12 10 DENR FORM MFLSF (12/2006) 2-24-2023 Facility Name:WQ Permit #:Field #:Acres Utilized: Land Owner:Annual Dry Tons Applied:Site #:Acres Permitted: Operator:Predominant Soil Series:Cation Exchange Capacity (non 503): Crop 1 Name:Crop 1 Max. PAN:Crop 2 Name:Crop 2 Max. PAN: Volume Applied per Acre Precip. Past 24 Hrs. TKN Am m o n i a Ni t r o g e n Nitrate and Nitrite Cu. Yds Gallons (Dry Tons/Ac)inches mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 6-2022 84500 2.95 0.740 dry 0 s 0.5 0.3 43000 5170 159 20.853 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 TOTALS:0 84500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 20.853 0.000 Annual lbs/acre 0.025 0.005 0.303 0.036 0.026 3.095 0.012 0.026 0.025 0.765 46.028 Date lbs/ac Prior Years Cumulative lbs/ac 0.138 0.03 6.039 1.023 0.52 0.02 0.111 0.384 0.135 16.074 0 Current Cumulative lbs/ac 0.163 0.035 6.342 1.059 0.546 3.115 0.123 0.410 0.160 16.839 Permitted C. P. L. R.****36 34 1338 NA 267 15 NA 374 89 2498 Permit PAN Limit 1st/2nd Crop 188 *Application Method: S - Surface, IN - Injection, INC - Incorporation Date ****C.P.L.R.: Cumulative Pollutant Loading Rate 188Fescue PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. “I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.” PAN Applied ( lbs/acre) Signature of Land Applier Lime Applied **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 Da t e o r Mo n t h % Solids Volume applied (enter one) Solids/ Liquid Mi n e r a l i z a t i o n Ra t e * * * Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Vo l a t i l i z a t i o n Ra t e * * Ap p l i c a t i o n Me t h o d * U.S. Biosolids,Inc. Lee Walker Lee Walker WQ00037135 10.3948 FcB2 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): NC-WK-LW 1 14.05 14.05 Name of Crop Type Receiving Residual Application NC0020567 DENR FORM FSF (12/2006) 2-24-2023 Owner:Predominant Soil Series: Site #:Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): % Solids 3.39 Arsenic 14.7 Cadmium 2.94 Copper 335 Chromium 65.3 Lead 22.3 Mercury 1.08 Molyb- denum 7.35 Nickel 21.7 Selenium 14.7 Zinc 1960 Total Phos- phorus 27400 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 4.06 To t a l s : Arsenic 0.119 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.119 Cadmium 0.024 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.024 Copper 2.720 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.720 Chromium 0.530 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.530 Lead 0.181 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.181 Mercury 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009 Molyb- denum 0.060 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.060 Nickel 0.176 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.176 Selenium 0.119 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.119 Zinc 15.915 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 15.915 Total Phos- phorus 222.488 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 222.488 Signature of Land Applier 4 Date __________________________________________________________ Sample or Com- posite Date ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name:U.S. Biosolids, Inc. 17.46Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Acres Permitted: WQ0037135 4.3 4.3 NC-GA-MH-2 CeB2Charles KillianCharles Killain "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Permit #: Operator: Acres Used: 3/14/22 1 2 3 4 5 6 7 8 9 11 12 1 2 3 4 5 6 7 8 9 10 11 12 10 DENR FORM MFLSF (12/2006) 2-24-2023 Facility Name:WQ Permit #:Field #:Acres Utilized: Land Owner:Annual Dry Tons Applied:Site #:Acres Permitted: Operator:Predominant Soil Series:Cation Exchange Capacity (non 503): Crop 1 Name:Crop 1 Max. PAN:Crop 2 Name:Crop 2 Max. PAN: Volume Applied per Acre Precip. Past 24 Hrs. TKN Am m o n i a Ni t r o g e n Nitrate and Nitrite Cu. Yds Gallons (Dry Tons/Ac)inches mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 4-2022 65000 3.39 2.137 dry 0 s 0.5 0.3 32100 2940 721 46.751 NA Fescue 6-2022 58500 3.39 1.923 dry 0 s 0.5 0.3 32100 2940 721 42.076 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 TOTALS:0 123500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 88.826 0.000 Annual lbs/acre 0.119 0.024 2.720 0.530 0.181 0.009 0.060 0.176 0.119 15.915 222.488 Date lbs/ac Prior Years Cumulative lbs/ac 0.133 0.03 5.695 2.021 0.411 0.013 0.115 0.357 0.143 20.361 12-22 2000 Current Cumulative lbs/ac 0.252 0.054 8.415 2.551 0.592 0.022 0.175 0.533 0.262 36.276 Permitted C. P. L. R.****36 34 1338 NA 267 15 NA 74 89 2498 Permit PAN Limit 1st/2nd Crop 209 *Application Method: S - Surface, IN - Injection, INC - Incorporation Date ****C.P.L.R.: Cumulative Pollutant Loading Rate 209Fescue PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. “I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.” PAN Applied ( lbs/acre) Signature of Land Applier Lime Applied **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 Da t e o r Mo n t h % Solids Volume applied (enter one) Solids/ Liquid Mi n e r a l i z a t i o n Ra t e * * * Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Vo l a t i l i z a t i o n Ra t e * * Ap p l i c a t i o n Me t h o d * U.S. Biosolids, Inc. Charles Killian Charles Killian WQ0037135 17.4583 CeB2 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): NC-GA-MH-2 4 4.3 4.3 Name of Crop Type Receiving Residual Application NC0021181 NC0021181 DENR FORM FSF (12/2006) 2-24-2023 Owner:Predominant Soil Series: Site #:Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): % Solids 3.39 1.57 Arsenic 14.7 31.3 Cadmium 2.94 6.25 Copper 335 306 Chromium 65.3 18.9 Lead 22.3 19.3 Mercury 1.08 8.94 Molyb- denum 7.35 15.6 Nickel 21.7 15.6 Selenium 14.7 31.3 Zinc 1960 1460 Total Phos- phorus 27400 29800 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 2.32 0.38 To t a l s : Arsenic 0.068 0.024 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.092 Cadmium 0.014 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.018 Copper 1.552 0.232 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.784 Chromium 0.302 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.317 Lead 0.103 0.015 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.118 Mercury 0.005 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.012 Molyb- denum 0.034 0.012 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.046 Nickel 0.101 0.012 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.112 Selenium 0.068 0.024 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.092 Zinc 9.079 1.107 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 10.185 Total Phos- phorus 126.917 22.588 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 149.505 Signature of Land Applier 5 Date __________________________________________________________ Sample or Com- posite Date ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name:U.S. Biosolids, Inc. 66.30Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Acres Permitted: WQ0037135 24.6 24.6 NC-GA-MH-2 CeB2Charles KillianCharles Killian "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Permit #: Operator: Acres Used: 3/14/22 4/26/22 1 2 3 4 5 6 7 8 9 11 12 1 2 3 4 5 6 7 8 9 10 11 12 10 DENR FORM MFLSF (12/2006) 2-24-2023 Facility Name:WQ Permit #:Field #:Acres Utilized: Land Owner:Annual Dry Tons Applied:Site #:Acres Permitted: Operator:Predominant Soil Series:Cation Exchange Capacity (non 503): Crop 1 Name:Crop 1 Max. PAN:Crop 2 Name:Crop 2 Max. PAN: Volume Applied per Acre Precip. Past 24 Hrs. TKN Am m o n i a Ni t r o g e n Nitrate and Nitrite Cu. Yds Gallons (Dry Tons/Ac)inches mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 3-2022 175500 3.39 1.009 dry 0 s 0.5 0.3 32100 2940 721 22.064 NA Fescue 4-2022 39000 3.39 0.224 dry 0 s 0.5 0.3 32100 2940 721 4.903 NA Fescue 6-2022 188500 3.39 1.083 dry 0 s 0.5 0.3 32100 2940 721 23.698 NA Fescue 9-2022 142500 1.57 0.379 dry 0 s 0.5 0.3 114000 8310 287 27.418 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 TOTALS:0 545500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 78.084 0.000 Annual lbs/acre 0.092 0.018 1.784 0.317 0.118 0.012 0.046 0.112 0.092 10.185 149.505 Date lbs/ac Prior Years Cumulative lbs/ac 1.452 0.175 26.055 7.543 3.354 0.117 0.673 15.335 0.252 75.825 12-22 2000 Current Cumulative lbs/ac 1.544 0.193 27.839 7.860 3.472 0.129 0.719 15.447 0.344 86.010 Permitted C. P. L. R.****36 34 1338 NA 267 15 NA 374 89 2498 Permit PAN Limit 1st/2nd Crop 209 *Application Method: S - Surface, IN - Injection, INC - Incorporation Date ****C.P.L.R.: Cumulative Pollutant Loading Rate 209Fescue NC0025861 PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. “I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.” PAN Applied ( lbs/acre) Signature of Land Applier Lime Applied **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 Da t e o r Mo n t h % Solids Volume applied (enter one) Solids/ Liquid Mi n e r a l i z a t i o n Ra t e * * * Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Vo l a t i l i z a t i o n Ra t e * * Ap p l i c a t i o n Me t h o d * U.S. Biosolids, Inc. Charles Killian Charles Killian WQ0037135 66.2986 CeB2 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): NC-GA-MH-2 5 24.6 24.6 Name of Crop Type Receiving Residual Application NC0021181 NC0021181 NC0021181 DENR FORM FSF (12/2006) 2-24-2023 Owner:Predominant Soil Series: Site #:Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): % Solids 14.5 Arsenic 4.08 Cadmium 1.88 Copper 321 Chromium 37 Lead 52.3 Mercury 0.537 Molyb- denum 6.75 Nickel 13.2 Selenium 9.1 Zinc 1260 Total Phos- phorus 22300 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 3.90 To t a l s : Arsenic 0.032 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.032 Cadmium 0.015 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.015 Copper 2.504 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.504 Chromium 0.289 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.289 Lead 0.408 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.408 Mercury 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- denum 0.053 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.053 Nickel 0.103 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.103 Selenium 0.071 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.071 Zinc 9.828 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 9.828 Total Phos- phorus 173.940 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 173.940 Signature of Land Applier 1 Date __________________________________________________________ Sample or Com- posite Date ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name:U.S. Biosolids, Inc 24.18Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Acres Permitted: WQ0037135 6.2 6.2 NC-RU-NM PbB2Norman McDanielNorman McDaniel "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Permit #: Operator: Acres Used: 3/14/22 1 2 3 4 5 6 7 8 9 11 12 1 2 3 4 5 6 7 8 9 10 11 12 10 DENR FORM MFLSF (12/2006) 2-24-2023 Facility Name:WQ Permit #:Field #:Acres Utilized: Land Owner:Annual Dry Tons Applied:Site #:Acres Permitted: Operator:Predominant Soil Series:Cation Exchange Capacity (non 503): Crop 1 Name:Crop 1 Max. PAN:Crop 2 Name:Crop 2 Max. PAN: Volume Applied per Acre Precip. Past 24 Hrs. TKN Am m o n i a Ni t r o g e n Nitrate and Nitrite Cu. Yds Gallons (Dry Tons/Ac)inches mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 4-2022 132 14.5 2.600 dry 0 s 0.5 0.3 52500 690 46.6 82.856 NA Fescue 6-2022 66 14.5 1.300 dry 0 s 0.5 0.3 52500 690 46.6 41.428 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 TOTALS:198 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 124.284 0.000 Annual lbs/acre 0.032 0.015 2.504 0.289 0.408 0.004 0.053 0.103 0.071 9.828 173.940 Date lbs/ac Prior Years Cumulative lbs/ac 0.076 0.072 5.522 0.64 1.429 0.018 0.15 0.308 0.442 22.844 12-22 1000 Current Cumulative lbs/ac 0.108 0.087 8.026 0.929 1.837 0.022 0.203 0.411 0.513 32.672 Permitted C. P. L. R.****36 34 1338 NA 267 15 NA 374 89 2498 Permit PAN Limit 1st/2nd Crop 178 *Application Method: S - Surface, IN - Injection, INC - Incorporation Date ****C.P.L.R.: Cumulative Pollutant Loading Rate 178Fescue PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. “I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.” PAN Applied ( lbs/acre) Signature of Land Applier Lime Applied **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 Da t e o r Mo n t h % Solids Volume applied (enter one) Solids/ Liquid Mi n e r a l i z a t i o n Ra t e * * * Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Vo l a t i l i z a t i o n Ra t e * * Ap p l i c a t i o n Me t h o d * U.S. Biosolids, Inc. Norman McDaniel Norman McDaniel WQ0037135 24.1788 PbB2 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): NC-RU-NM 1 6.2 6.2 Name of Crop Type Receiving Residual Application NC0025984 NC0025984 DENR FORM FSF (12/2006) 2-24-2023 Owner:Predominant Soil Series: Site #:Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): % Solids 14.5 Arsenic 4.08 Cadmium 1.88 Copper 321 Chromium 37 Lead 52.3 Mercury 0.537 Molyb- denum 6.75 Nickel 13.2 Selenium 9.1 Zinc 1260 Total Phos- phorus 22300 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1.92 To t a l s : Arsenic 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.016 Cadmium 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007 Copper 1.232 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.232 Chromium 0.142 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.142 Lead 0.201 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.201 Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- denum 0.026 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.026 Nickel 0.051 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.051 Selenium 0.035 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.035 Zinc 4.836 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.836 Total Phos- phorus 85.587 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 85.587 Signature of Land Applier 2 Date __________________________________________________________ Sample or Com- posite Date ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name:U.S. Biosolids, Inc.8.06Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Acres Permitted: WQ0037135 4.2 4.2 NC-RU-NM PaC2Norman McDanielNorman McDaniel "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Permit #: Operator: Acres Used: 3/14/22 1 2 3 4 5 6 7 8 9 11 12 1 2 3 4 5 6 7 8 9 10 11 12 10 DENR FORM MFLSF (12/2006) 2-24-2023 Facility Name:WQ Permit #:Field #:Acres Utilized: Land Owner:Annual Dry Tons Applied:Site #:Acres Permitted: Operator:Predominant Soil Series:Cation Exchange Capacity (non 503): Crop 1 Name:Crop 1 Max. PAN:Crop 2 Name:Crop 2 Max. PAN: Volume Applied per Acre Precip. Past 24 Hrs. TKN Am m o n i a Ni t r o g e n Nitrate and Nitrite Cu. Yds Gallons (Dry Tons/Ac)inches mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 2-2022 66 14.5 1.919 dry 0 s 0.5 0.3 52500 690 46.6 61.155 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 TOTALS:66 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 61.155 0.000 Annual lbs/acre 0.016 0.007 1.232 0.142 0.201 0.002 0.026 0.051 0.035 4.836 85.587 Date lbs/ac Prior Years Cumulative lbs/ac 0.127 0.101 7.544 0.829 1.944 0.02 0.204 0.417 0.609 31.344 0 Current Cumulative lbs/ac 0.143 0.108 8.776 0.971 2.145 0.022 0.230 0.468 0.644 36.180 Permitted C. P. L. R.****36 34 1338 NA 267 15 NA 374 89 2498 Permit PAN Limit 1st/2nd Crop 158 *Application Method: S - Surface, IN - Injection, INC - Incorporation Date ****C.P.L.R.: Cumulative Pollutant Loading Rate 158Fescue PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. “I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.” PAN Applied ( lbs/acre) Signature of Land Applier Lime Applied **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 Da t e o r Mo n t h % Solids Volume applied (enter one) Solids/ Liquid Mi n e r a l i z a t i o n Ra t e * * * Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Vo l a t i l i z a t i o n Ra t e * * Ap p l i c a t i o n Me t h o d * U.S. Biosolids, Inc. Norman McDaniel Norman McDaniel WQ0037135 8.0596 PaC2 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): NC-RU-NM 2 4.2 4.2 Name of Crop Type Receiving Residual Application NC0025984 DENR FORM FSF (12/2006) 2-24-2023 Owner:Predominant Soil Series: Site #:Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): % Solids 14.5 Arsenic 4.08 Cadmium 1.88 Copper 321 Chromium 37 Lead 52.3 Mercury 0.537 Molyb- denum 6.75 Nickel 13.2 Selenium 9.1 Zinc 1260 Total Phos- phorus 22300 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1.10 To t a l s : Arsenic 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009 Cadmium 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Copper 0.707 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.707 Chromium 0.081 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.081 Lead 0.115 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.115 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- denum 0.015 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.015 Nickel 0.029 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.029 Selenium 0.020 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 Zinc 2.775 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.775 Total Phos- phorus 49.105 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 49.105 Signature of Land Applier 1B Date __________________________________________________________ Sample or Com- posite Date ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name:U.S. Biosolids, Inc. 32.26Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Acres Permitted: WQ0037135 29.3 29.3 NC-RU-RD CaB2Evelyn DavisNorman McDaniel "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Permit #: Operator: Acres Used: 3/14/22 1 2 3 4 5 6 7 8 9 11 12 1 2 3 4 5 6 7 8 9 10 11 12 10 DENR FORM MFLSF (12/2006) 2-24-2023 Facility Name:WQ Permit #:Field #:Acres Utilized: Land Owner:Annual Dry Tons Applied:Site #:Acres Permitted: Operator:Predominant Soil Series:Cation Exchange Capacity (non 503): Crop 1 Name:Crop 1 Max. PAN:Crop 2 Name:Crop 2 Max. PAN: Volume Applied per Acre Precip. Past 24 Hrs. TKN Am m o n i a Ni t r o g e n Nitrate and Nitrite Cu. Yds Gallons (Dry Tons/Ac)inches mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 2-2022 77 14.5 0.321 dry 0 s 0.5 0.3 52500 690 46.6 10.227 NA Fescue 3-2022 88 14.5 0.367 dry 0 s 0.5 0.3 52500 690 46.6 11.688 NA Fescue 11-2022 99 14.5 0.413 dry 0 s 0.5 0.3 52500 690 46.6 13.149 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 TOTALS:264 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 35.065 0.000 Annual lbs/acre 0.009 0.004 0.707 0.081 0.115 0.001 0.015 0.029 0.020 2.775 49.105 Date lbs/ac Prior Years Cumulative lbs/ac 0.066 0.026 0.965 0.092 0.087 0.004 0.064 0.067 0.058 1.773 0 Current Cumulative lbs/ac 0.075 0.030 1.672 0.173 0.202 0.005 0.079 0.096 0.078 4.548 Permitted C. P. L. R.****36 34 1338 NA 267 15 NA 374 89 2498 Permit PAN Limit 1st/2nd Crop 209 *Application Method: S - Surface, IN - Injection, INC - Incorporation Date ****C.P.L.R.: Cumulative Pollutant Loading Rate 209Fescue PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. “I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.” PAN Applied ( lbs/acre) Signature of Land Applier Lime Applied **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 Da t e o r Mo n t h % Solids Volume applied (enter one) Solids/ Liquid Mi n e r a l i z a t i o n Ra t e * * * Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Vo l a t i l i z a t i o n Ra t e * * Ap p l i c a t i o n Me t h o d * U.S. Biosolids, Inc. Evelyn Davis Norman McDaniel WQ0037135 32.2384 CaB2 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): NC-RU-RD 1B 29.3 29.3 Name of Crop Type Receiving Residual Application NC0025984 NC0025984 NC0025984 DENR FORM FSF (12/2006) 2-24-2023 WQ Permit Number: NPDES Number: To Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: If applicable to alternative performed (Class A only) indicate “Process to Further Reduce Pathogens”: If applicable to alternative performed (Class B only) indicate “Process to Significantly Reduce Pathogens”: If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Minimum Geo. Mean Maximum Units MPN 16340 42978 162338 MPN/G 0 7 grab sm9221 CFU CERTIFICATION STATEMENT (please check the appropriate statement) Preparer Name and Title (type or print)Land Applier Name and Title (if applicable)(type or print) _______________ Signature of Preparer*Date Signature of Land Applier (if applicable)Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) “I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met.” Allowable Level in Sludge Alt. 8 (Drying - Unstable) 2 x 10 to the 6th power per gram of total solids Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt. 6 (Alk. Stabilization Alt. 10 (Incorporation) Alt 7 (Drying - Stable) Facility Name: WWTP Name: 1/1/2022 Class A: Aerobic Digestion Pathogen Density Number of Excee- dences Analytical Tech- nique Beta Ray Pasteurization Zach Key U.S. Biosolids, Inc. Heat Treatment Thermophilic Frequency of Analysis Sample Type Alt.D (No Prior Test)Process to Further Reduce Pathogengs Alt. (2) Process to Significantly Reduce Pathogens 1000 mpn per gram of total solid (dry weight) “I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met.” (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) 12/31/2022Monitoring Period: From Alt. A (time/temp) U.S. Biosolids, Inc. Yadkin Valley Sewer Authority Alt B (Alk Treatment)Alt. C (Prior Testing) WQ0037135 NC020567 ___________________________________ Zach Key U.S. Biosolids, Inc. Alt. (1) Fecal Density 3 MPN per 4 grams total solid (dry weight) Fecal Coliform Salmonella bacteria (in lieu of fecal coliform) Parameter Lime Stabilization “This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment.” ______________________________________ Gamma Ray Class B: Compost Heat Drying Anaerobic Digestion Air Drying Composting No vector attraction reduction alternatives were performed Alt.1 (VS reduction)Alt. 2 (40-day bench)Alt. 3 (30-day bench)Alt. 4 (Spec. O2 uptake) Alt. 5 (14-Day Aerobic) Alt. 9 (Injection) DENR FORM PVRF 02T (12/2006) 2-24-20232-24-2023 ANNUAL PATFIOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: to„n ot'North Wilkesboro WQ Permit Number: WQ0037135 WWTP Name: Thurmond Street W WIT NPDFS Number: N00020761 Monitoring Period: From 1/1/2022 To 12/331,2_022 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt A (tnnc temp) Alt R IAlk'I'rcaunent) I Alt. C (Prior IcStmg)' Alt D (No Pi or 1 r,t) I Pnrcetis to 1 ur[hcr Reduce PathOgengs �If applicable to alternative performed (( lass 4 ont) indicate "Process to Further Reduce Pathogens": Compost _ heat I )ry1 I teat l rratincat I hcnnophilic IBcta Ray G;unma Ray ._, Pasteurvatun Class 13: IAII ( I ) I ecal Densuv Alt. (2) Proccs� to Slgm icantl\' Reduce Pathogen, Ilf applicable to alternative performed (( lass 13 onh) indicate ^Process to SignificantIN Reduce Pathogens": II imeStahiliration Ji Au DiNumg I CumpOtiling IAetobic Di`acsthon ..i jAnacrohic Diuestior IIf applicable to alternative performed (Class A or Class 11) complete the following monitoring data: Allov,ahle I c,el Palho`uen Dcr[sit, (Number of Analytical hicyuenq Sample ParameterTech- ill Sludge Mlnm lllnlM l GCO. Mean aSimUn llli its ol'Anabsts l'vpe dencr, - nimic 2s10tofile MPN 1176 158i 4849 MPN/e 0 7 grah sm9221 6th po,rcr per gram of 1'ecal Colilbrm total.olids Cl tI 1000 n,pn per gran, of total solid (lh"\ „eight) Salmonella bactei is 3 MPN per I grams (in lieu of tccal total Solid Idp coliform) ��ci;;ht) Vector Attraction Reduction (15A NCAC 62T .1107) - Please indicate alternative performed: JAIL) (VS reduction) Alt '_ ( 10-da\ hench) Alt. ; 130-cim hench) V7 Alr I (Spec.0, uptake) 1 JAIt.5(11-DavAcruhic) %It.0(Alk.SlehIlVeLIOn Ah7(Dr\ing-',tablet Ah.B(Drine-Unstable) I JAlt. 9 (Injection) _ Alt, 10 ( Incorporation) No oector attraction reduction alternati\es „ere performed CERTIFICATION STATEMENT (please check the appropriate statement) y "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .11(17 have not been met." (Please note if you check this statement attach an explanation vvhy you have not met one or both of the requirements.) "This determination has been matte under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." J,* PerYt, rlanf oRr_ ZRCh Ke/� V.S. )3:ossUr,TAC. Preparer Name 4nd I itle (t\ pc or print) Land Applier Ntrfnc and I itle (if applicable)(lype or print) Si,nattu'e of Prepar Date Sign we of La \pplicr (if applicable) Date *Preparer is defined in 10 CFR Part 503 9(r) and I �A NCAC' 2'1 .I 102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Forest City W W l P WQ Permit Number: W00037105 W WTP Name: Forest City W WTP NPDES Number: N00025984 Monitoring Period: From 1/1/2022 To 12/31/2022 Pathogen Reduction (15A NCAC 021' .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (timrtemp) J I Alt 13 (Alk hreatntcnt) -J I Alt C (Prior 'I esting).1 Alt D (No Prior Tcst) (_: I Process to Further Reduce Pathogens Ll ilf applicable to alternative performed (Class A onh') indicate "Process to Further Reduce Pathogens Compost C7 Heat Drying --i heat Treatment _i I'liernlophtlic I13eta Ray Gaumta Ray Pasteuri/atton i `I Class B: jAll (1) Fecal Dcnsu�, vj :11t. (2) Process to Significantly' Reduce Pathogens CI Ilf applicable to alternative performed (( lass B ono') indicate "Process to Significant] Reduce Pathogens": Lime Stabilization _I I 'fir Drying I Composting ....I IAcrobic Digestion U Anaerobic Digestior b., If applicable to ;Ilernative performed (Class A or Class B) complete the following monitoring data: Nf Anal ocal Alloy+able Level Pathogen Density Frcuntncr oqucncy Sample } Parameter races- I ech- m Sludge Minimum 600. Mcan Maximum (Mils of Analysis Type niaue dcnccs 2 s 10 to the MPN 15.385 22533 I 1 1888 MPN/g 0 7 grab sm9221 6th power per gram of Fecal Cohibrm total solids CFU 1000 mpn per gram oftotalsolid (dry %%eight) Salmonella bacteria 3 MPN per 1 ,rams (in lieu of fecal total solid (dry colitbrnt) weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate a ternative performed: JAIt.1 (VS reduction) :._} I Alt. 2 ( 10-day bench) _! Alt. 3 (30-day bench) Alt. 9 (Spec. O, uptake) ! IAlt. 5 ( l !-Day Aerobic) _.I Alt. 6 (AIL. Stabilization Alt 7 (Drying Stable) Alt. 8 (Dry ing - Unstable) 1 , Alt. 9 (Injection) AIL 10 ( Incorporation) _ No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." J4«� drJ92 ORC Dennis Key U.S. Hiosolids. Inc. Preparer Name and Tille (type or print) Land Applicr Name and Title (ifapplicable)(typc or print) SignatuH)IPrarer Date Signatuye of Land Applier (if applicable) Date *Preparer is defined in d0 CFR Part 503 9(r) and 15A NCAC 21'.I 102 (26) DENR FORM PVRF 02T (12/2006) WQ Permit Number: NPDES Number: To Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: If applicable to alternative performed (Class A only) indicate “Process to Further Reduce Pathogens”: If applicable to alternative performed (Class B only) indicate “Process to Significantly Reduce Pathogens”: If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Minimum Geo. Mean Maximum Units MPN 3406 8270 25478 MPN/g 0 7 grab sm921 CFU CERTIFICATION STATEMENT (please check the appropriate statement) Preparer Name and Title (type or print)Land Applier Name and Title (if applicable)(type or print) _______________ Signature of Preparer*Date Signature of Land Applier (if applicable)Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Composting No vector attraction reduction alternatives were performed Alt.1 (VS reduction)Alt. 2 (40-day bench)Alt. 3 (30-day bench)Alt. 4 (Spec. O2 uptake) Alt. 5 (14-Day Aerobic) Alt. 9 (Injection) Gamma Ray Class B: Compost Heat Drying Anaerobic Digestion Air Drying ___________________________________ Zach Key U.S. Biosolids, Inc. Alt. (1) Fecal Density 3 MPN per 4 grams total solid (dry weight) Fecal Coliform Salmonella bacteria (in lieu of fecal coliform) Parameter Lime Stabilization “This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment.” ______________________________________ ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) 12/31/2022Monitoring Period: From Alt. A (time/temp) U.S. Biosolids, Inc. Belmont WWTP Alt B (Alk Treatment)Alt. C (Prior Testing) WQ0037135 NC0021181 Zach Key U.S. Biosolids, Inc. Heat Treatment Thermophilic Frequency of Analysis Sample Type Alt.D (No Prior Test)Process to Further Reduce Pathogengs Alt. (2) Process to Significantly Reduce Pathogens 1000 mpn per gram of total solid (dry weight) “I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met.” (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) Facility Name: WWTP Name: 1/1/2022 Class A: Aerobic Digestion Pathogen Density Number of Excee- dences Analytical Tech- nique Beta Ray Pasteurization “I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met.” Allowable Level in Sludge Alt. 8 (Drying - Unstable) 2 x 10 to the 6th power per gram of total solids Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt. 6 (Alk. Stabilization Alt. 10 (Incorporation) Alt 7 (Drying - Stable) DENR FORM PVRF 02T (12/2006) 2-24-2023 2-24-2023 WQ Permit Number: NPDES Number: To Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: If applicable to alternative performed (Class A only) indicate “Process to Further Reduce Pathogens”: If applicable to alternative performed (Class B only) indicate “Process to Significantly Reduce Pathogens”: If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Minimum Geo. Mean Maximum Units MPN 7386 17725 40462 MPN/g 0 7 grab sm9221 CFU CERTIFICATION STATEMENT (please check the appropriate statement) Preparer Name and Title (type or print)Land Applier Name and Title (if applicable)(type or print) _______________ Signature of Preparer*Date Signature of Land Applier (if applicable)Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Composting No vector attraction reduction alternatives were performed Alt.1 (VS reduction)Alt. 2 (40-day bench)Alt. 3 (30-day bench)Alt. 4 (Spec. O2 uptake) Alt. 5 (14-Day Aerobic) Alt. 9 (Injection) Gamma Ray Class B: Compost Heat Drying Anaerobic Digestion Air Drying ___________________________________ Alt. (1) Fecal Density 3 MPN per 4 grams total solid (dry weight) Fecal Coliform Salmonella bacteria (in lieu of fecal coliform) Parameter Lime Stabilization “This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment.” ______________________________________ ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) 12/31/2022Monitoring Period: From Alt. A (time/temp) U.S. Biosolids, Inc. Lowell WWTP Alt B (Alk Treatment)Alt. C (Prior Testing) WQ0037135 NC0025861 Zach Key U.S. Biosolids, Inc. Heat Treatment Thermophilic Frequency of Analysis Sample Type Alt.D (No Prior Test)Process to Further Reduce Pathogengs Alt. (2) Process to Significantly Reduce Pathogens 1000 mpn per gram of total solid (dry weight) “I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met.” (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) Facility Name: WWTP Name: 1/1/2022 Class A: Aerobic Digestion Pathogen Density Number of Excee- dences Analytical Tech- nique Beta Ray Pasteurization “I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met.” Allowable Level in Sludge Alt. 8 (Drying - Unstable) 2 x 10 to the 6th power per gram of total solids Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt. 6 (Alk. Stabilization Alt. 10 (Incorporation) Alt 7 (Drying - Stable) DENR FORM PVRF 02T (12/2006) 2-24-2023 2-24-2023 Zach Key U.S. Biosolids, Inc. NORTH WILKESBORO NC0020761 Waypoint. ANALYTICAL 46381 US Biosolids Inc Dennis Key 958 Hoots Road Roaring River , NC 28669 Report Number : 22-136-0004 Lab No: 57884 Sample ID : N. Wilkesboro 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Project N. Wilkesboro Information : REPORT OFANAL YSIS Report Date : 05/25/2022 Received : 05/16/2022 a Pauric Mc Groary Ph.D., CPA Agronomist Matrix: Solids Sampled: 5 / 13/ 2022 13:30 Test Results Units MQL DF Date/Time By Analytical Analyzed Method Total Solids 1.65 % 0.010 1 05/18/22 16:00 FMM SM-254OG Total Kjeldahl Nitrogen 67600 mg/Kg - dry 14700 1 05/24/22 11:00 JPJ eM-4500-NH3C-TKt Phosphorus 30600 mg/Kg - dry 294 1 05/19/22 23:01 iJS 6010D Potassium 6590 mg/Kg - dry 588 1 05/19/22 23:01 TJS 6010D Sulfur 14200 mg/Kg - dry 588 1 05/19/22 23:01 TJS 6010D Calcium 19300 mg/Kg - dry 2940 1 05/20/22 16.20 EAL 6010D Magnesium 4580 mg/Kg - dry 294 1 05/19/22 23:01 TJS 6010D Sodium 3010 mg/Kg - dry 1470 1 05/19/22 23:01 TJS 6010D Iron 28400 mg/Kg - dry 588 1 05/19/22 23:01 TJS 6010D Manganese 443 mg/Kg - dry 29.4 1 05/19/22 23:01 TJS 6010D Copper 724 mg/Kg - dry 29.4 1 05/19/22 23:01 TJS 6010D Zinc 1960 mg/Kg - dry 73.5 1 05/19/22 23.01 TJS 6010D Organic N 53940 mg/Kg - dry 14710 1 05/24/22 11:00 CALCULATION Nitrate+Nitnte-N <283 mg/Kg - dry 283 1 05/23/22 15:27 ZBD 4500NO3F-2011 Nickel 36.2 mg/Kg - dry 14.7 1 05/19/22 23:01 iJS 6010D Mercury <8.00 mg/Kg - dry 8.00 1 05/20/22 13:12 ZMT SW-74718 Selenium <29.4 mg/Kg ' dry 29.4 1 05/19/22 23:01 TJS 6010D pH 7.2 S.u. 1 05/23/2215:34 DRS 9045D Qualifiers/ OF Dilution Factor Definitions MQL Method Quantrtation Limit Page 3 of 9 Waypoint. ANALYTICAL 16381 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanaWcal.com US Biosolids Inc Project N. Wilkesboro Dennis Key 958 Hoots Road Information Roaring River , NC 28669 Report Number : 22-136-0004 Lab No: 57884 Sample ID . N. Wilkesboro Test Ammonia Nitrogen Aluminum Arsenic Cadmium Chromium Lead Molybdenum Analytical Method: SM-254OG Test Moisture Qualifiers/ DF Dilution Factor Definitions 0"dd3lr7yrlGL4FYE7 Results Units 13700 mg/Kg - dry 57800 mg/Kg - dry <29.4 mg/Kg - dry <5.88 mg/Kg - dry 88.2 mg/Kg - dry 61.8 mg/Kg - dry <14.7 mg/Kg - dry MQL 5880 294 29.4 5.88 14.7 17.6 14.7 Results Units MQL 98.3 % 0 010 Report Date : 05/25/2022 Received: 05/ 16/2022 P Paunc Mc Groary Ph.D., CPA Agronomist Matrix: Solids Sampled: 5 / 13 / 2022 13:30 DF Date / Time By Analytical Analyzed Method 1 05/25/2210:00 JPJ SM-+500-NH3C 1 05/19/22 23:01 TJS 6010D 1 05/19/22 23:01 TJS 6010D 1 05/19/22 23:01 TJS 6010D 1 OS/19/22 23:01 TJS 6010D 1 05/19/22 23:01 TJS 6010D 1 05/19/22 23:01 TJS 6010D DF Date / Time By Analytical Analyzed Batch 1 05/18/22 16.00 FMM L616978 MQL Method Quantitation Limit Page 4 of 9 z a I j co a O O O N ON m 2 m Z x E 9 E : O II II II II N 0 C O N p N O X -q N O O a0 d O x x X Z + m Y m Y s p E O z O 0 a z + O y M _ Z Z + _ N c u) _ 4 + I0 + + M m= N _ A � m Z Z £0)0 Z Z d o O F F V Of cr A N Z O — — Z m Z d — — L a L C A pas ` o CDu uo 0 ZIN a 2•=°a °a =°mat m�vx N N N _aa_a_ N W N a_a_a N aN N d ac a M O Or 0 M a Ip i p i Z cv) Z IT p co p m V -- c O -- C. u d fZ� I 7 0 Y C Y a m a cma E a E _ _ rn 0 mP9 C. O N 0 0 O O M O W Z a N d Z a N a N M N M N Op d d A CIO 00 N 0 N y C SAR Sodium Absorption Ratio Na(Mq/L) Ca(Mq/L1 M M /L Na Sodium (Mg/L) Equivalent weight 23 49 665 31845 7557 Ca Calcium (Mg/L) Equivalent weight 20 Mg Magnesium (Mg/L) Equivalent weight 12 Na (ME) CaiME) Mg(ME, 2.159348 15.9225 6.2975 Milli Equivalent = Mg/L / Equivalent weight The amour amount of SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0 5 power Permitting SAR = 0 647837 (From Mg/L entered above) SAR= 0 649056'(From ME entered below) Na (ME) Ca (ME) Mg (ME) 216 1 15.92 1 623 U.S. Biosolids Inc 958 Hoots Road Roaring River, NC 28669 Receive Date: Reported: For: Comments: Analytical Results O5/05/2022 05/06/2022 N Wilkesboro Sample Number parameter Sample ID Result Unit Method Analyzed Analyst 220505-21-01 Fecal Coliforms NWt <1176 MPN/g SM92210E 2006 05/05/2022 MD 220505-21-01 Percent Solids NW1 1.70 % sWWB-211 05105/2022 MD 220505-21-02 Fecal Coliforms NW2 <1220 MPN/g SM92210E-2006 05/05/2022 MD 220505-21-02 Percent Solids NW2 1 64 % SM25406-2011 05/05/2022 MD 220505-21-03 Fecal Coliforms NW3 1250 MPN/g SM92210E-2006 05/05/2022 MD 220505-21-03 Percent Solids NW3 1.60 % SM254oe-21 1 05/05/2022 MD 220505-21-04 Fecal Coliforms NW4 2454 MPN/g SM92210E-2006 05/05/2022 MD 220505-21-04 Percent Solids NW4 1.63 % SM2549B 2011 05/05/2022 MD 220505-21-05 Fecal Coliforms NW5 4849 MPN/g SM9221ce-2oo6 05/05/2022 MD 220505-21-05 Percent Solids NW5 1 65 % SM2s40e@011 05/05/2022 MD 220505-21-06 Fecal Coliforms NW6 1197 MPN/g SM92210E-2006 05/05/2022 MD 220505-21-06 Percent Solids NW6 0.67 % SM254oB-2011 05/05/2022 MD 220505-21-07 Fecal Coliforms NW7 1205 MPN/g SM92210E-2006 05/05/2022 MD 220505-21-07 Percent Solids NW7 1.66 % SM25466-2011 05/05/2022 MD Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 4 Analytical Results U.S. Biosolids Inc 958 Hoots Road Roaring River, NC 28669 Receive Date: 05/05/2022 Reported: 06/20/2022 For: N WILKESBORO Comments: Sample Number Parameter Sample ID Result 220505-26-01 TCLP N See Attached WILKESBORO Respectfully submitted, Melissa Myers NC Cent #440, NCDW Cen #37755, EPA #NC00909 Unit Method Analyzed Analyst n Nosed 05/06/2022 PACE PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 36 Pace Analytical Servlcet, LLC 9800 Key Ave SuitsaceAnaiytica( Huitervilte NC28078 W+e.Ncalabenn (704)875-9092 ANALYTICAL RESULTS Project NVALKESBORO US BID Pace Project No 92603541 Sample- 220505-2"1 lab ID 92603541001 Collected 05105/22 08 30 Received 05/06/22 13 23 Matrix Solid Results reported on a -dry wepW basis and are adjusted for percent moisture, sample arse and any dilutions Parameters Results Units Report Limit OF Prepared Analyzed CAS No Oual 8081 TCLP Pesticides RVE Analytical Method EPA8081B Preparation Method EPA3510C Leachate Method(Date EPA 1311 051121221504 Initial pH 5 8 Final pH 5 Pace Analytical Services Charlotte gamma-BHC (Latdane) NO ug1L 0 50 1 05/16122 1314 05/17/2213 38 58-89-9 Chlordane(Technical) ND ug/L 30 1 05116122 13 14 05/171221338 57-74-9 Endnn ND ugiL 050 1 05116122 13 14 D5/171221338 72-20-8 Heplachlor NO ug/L 050 1 05/161221314 05117221338 7644-8 Heplachlor epoxide NO ug/L 050 1 05116/221314 05/17/22 13 38 1024-57-3 Melhoxy&lor ND ugiL 1000 1 051161221314 05/17122 13 38 72-43-5 Toxaphene NO ugiL 30 1 05116221314 011171221338 8001-35-2 Surrogates Decachlarobtphemyl (S) 99 10-200 1 0516122 13 14 05117/22 13 38 2051-24-3 Telrachlom-m-xylene(S) 83 % 10-182 1 05116/22 13 14 061171221338 877-09-8 8082 TCLP PCBs RVE Analytical Method EPA 8082A Preparation Method EPA 3510C Leachate Method/Date EPA 1311, 05/1 2/22 15 D4 Initial pH 58. Final pH.5 Pace Analytical Services - Gardens PCB-1016(Anclor 1016) NO ug/L 1000 1 05116221315 05118/22 03 20 12674-11-2 PCB-1221(Aroctor 1221) NO ug/L 1000 1 0511&22 13 16 05118/22 03 20 11104-28-2 PCB 1232 (Amdor 1232) NO ug/L 1000 1 05116/221315 05!18I2203 20 11141-16-5 PCB-1242(Aroclor 1242) NO ugiL 1000 1 05116122 13 15 05118!220320 53469-21-9 PCB-1248(Arodor 1248) NO u9IL 1000 1 05116122 13 15 05118122 03 20 1267229-6 PCB-1254(Arodo, 1254) ND u9IL 1000 1 0511&221315 05/18/220320 11097-69-1 PCB-1260 (Article, 1260) NO u9I1- 1000 1 05111 1315 05.r1822 D3 20 11096-82-5 Surrogates Decachlorobiphenyl(S) 87 'b 10-181 1 05/161221315 05118122 03 20 2051-24-3 6010 MET ICP. TCLP Analytical Method EPA 6010D Preparation Method EPA 3010A Leachate Model ate EPA 1311, 05/12122 15 04 initial pH 5 8, Final pH 2 Pace Analytical Services - Ashevile Arsenic NO mg,iL 0050 1 05114/220014 05/26/221659 7440-36-2 Banum 0.28 mg!L 025 1 051141220014 05261221659 7440-39-3 Geri NO pi 00050 1 05)14)220014 05/26i221659 7440-43-9 Chromium NO mg1L 0050 1 05114122 00 14 05126i221659 7440-47-3 Lead ND mglL 0025 1 051141220014 051261221659 7439-92.1 Selenmm ND mg/L 010 1 05/14/2200'14 05126/221659 7782-49-2 Silver NO mg/L 0025 1 051141220014 05261221659 7440-22-4 7470 Mercury, TCLP Analytical Method EPA 7470A Preparation Method EPA 7470A Leachate MethodlDate EPA 1311, 05112122 15 D4 Initial pH 5 8. Final pH- 2 Pace Analytical Services - Asheville Mercury ND mqA- 000020 1 05114122 17 22 05117122 14 11 7439-97.6 REPORT OF LABORATORY ANALYSIS This report shall not be repoacuced, e,cept in full Dale 06I03/2022 05 52 PM without the written consent W Pace Analytical Services LLC Page 4 of 33 PO Box 228 a Statesville, NC 28687 a 704/872/4697 Page 7 of 36 PaceAnalytical rwraeWeN con ANALYTICAL RESULTS Project NWILKESBORO US BID Pace Project No 92603541 Sample- 220505-26-01 Lab ID: 92603541001 Collected D5/05/22 08 30 Received 05/06/22 13 23 Resufts reported on a -dry —ii basis and are adjusted forpe2eof morafune, sample size and any r/7lutrons Parameters Results Units Report Limit DIP Prepared Analyzed Pace Anali Services, LL6 9800 Kincey Ave Sue. 100 HiIn1e11WIt NC 2BO78 170418IS9092 Matrix Solid GAS No Owl 8270E TCLP FIVE Analytical Method EPA 8270E Preparation Method EPA 351 OC Leachate Method/Date EPA 1311, 05112122 15 04 Initial pH 58 Final pH 5 Pace Analytical Services - Charlotte I4-D,chlombenzene NO ug1L 500 1 05116122 11 09 05117122 13 51 106-46.7 2.4-Dlnarotoluene NO u9IL 500 1 05116122 11 09 05117221351 121-14-2 Hexachloral 3-butadlene NO ugrL 500 1 05116/22 11 09 05117122 13 51 87-58-3 Hexachlorobenzene NO u9I1- 500 1 051161221109 05117/221351 118-74-1 Hexachloroethane NO ugll. 500 1 05116122 11 09 051171221351 67-72.1 240amylperido-Crasol) NO ug/L 500 1 051161221109 05/17122 13 51 95-48-7 384-Methylphenol(mBp Cresoll NO ugiL 500 1 05116/221109 OS/171221351 15831-10-4 Nitrobenzene NO ugrL 500 1 05116122 11 09 05117/22 13 51 98-95-3 Pentachlorophenol NO u9IL 100 1 051161221109 05/171221351 87-86-5 Pyndme ND ug1L 500 1 05116122 11 09 05/1 P22 13 51 110.86-1 0 245-TrioNorophenoj ND u9IL Soo 1 05116/221109 D5/171221351 95-95-0 24,6-Trlchlorophenol NO ugh- 500 1 05116,22 11 09 05117/22 13 51 88-0&2 Surrogates Nltrobenzeri IS) 84 % 10-144 1 05116122 11 09 0511 T1221351 4165-60-0 2-Puoromphenyt IS) 67 10-130 1 05/16/221109 05/17/221351 321-60-8 Terpheny)-d14(S) 73 % 34-163 1 0506221109 05117/221351 1718.51-0 Phenobd6(S) 43 % 10-130 1 05116122 11 09 051171221351 13127-88-3 2-Ffuorophenol IS) 57 10-130 1 05116/22 11 09 05117/221351 367-124 24,6-Tnbromophenol (S) B2 °y 10-144 1 05116122 11 09 05117/22 13 51 118-791 8260D MSV TCLP Analytical Method EPA 8260D Leachate MethodlDale EPA 1311, 05/11122 13 38 Pace Analytical Semces - Charlotte Benzene ND ugli- 100 2D 05113)221948 71-43-2 2-Bulanone(MEK) NO ugiL 2DO 20 051131221948 78-93-3 Carbon tetrachloride ND ugh- 100 20 051131221948 56-23-5 Chlorobenzene NO u911 100 20 05,131221948 108.90-7 Chloroform NO ugiL 1DO 20 05113/221948 6766-3 14-Dmtijombenzene NO ugrL 100 20 051131221948 106-46-7 1,2-Dtchloroethane NO ugiL 100 20 051131221948 107-06-2 Q 11-Dlchloroethene NO ugrL 100 20 05(13,221948 75-35-4 Telrachlornethene HD ugiL 100 20 05113/221948 127-184 Tnchloroelmme ND ug1L 100 20 05!13)221948 79-01-6 Vrnyl chloride NO liVL 100 2D 051131221948 75-01-4 Surrogates 1,2-Dichloroethane-d4(S) 95 1/1 70-130 20 051131221948 17060-07-0 Toluene-d81S) 101 % 6T-135 20 05113,221948 2037-26-5 4-Brom0Oumobenzene IS) 99 % 70130 2D 051131221948 460-00-4 Percent Moisture Analytical Method SW-846 Pace Analytical Servloes - Charlotte Percent Moisture 99.0 % 010 1 D5110I221659 N2 REPORT OF LABORATORY ANALYSIS This report Shall not be reproduced except in toll Date 0610312022 05 52 PM otli the wmen consent of Pace Analylmal Services LLC Page 5 of 33 PO Box 228 e Statesville, NC 28687 a 704/872/4697 Page 8 of 36 Pace Analytical services, LLC aceAnalyticalA 9800 Johney Ave Suite IGO Hnnleraallle NC 20078 awwands, sn p04J875-9092 ANALYTICAL RESULTS Protect NWILKESBORO US 810 Pace Protect No 92603W Sample- 220505-26-01 Lab ID: 92603541001 Collected D5105/22 08 30 Received 05106/22 13 23 Mabu Solid Results reported on a -dry weioW basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DP Prepared Analyzed CAS No Coal 1010 Flashpoint,Closed Cup Analytical Method EPA 10108 Pace Analytical Services - Asheville Flashppmt s200 deg F 700 1 05116/22 14 26 9045 pH Sell Analytical Method EPA 90450 Pace Analytical Services - Asheville pH at 25 Degrees C 6.9 Sod Units 0 10 1 05n3122 10 21 H3 9095 Palm Fitter Liquid Test Analytical Method EPA 90958 Pace Analytical Services - Asheville Free Liquids FAIL 1 0 1 05116/22 12 14 733C S Reactive Cyanide Analytical Method SW-846 7 3 3 2 Preparation Method SW-846 7 3 3 2 Pace Analillboal Services - New Orleans Cyanide Reactive NO mg/kg 250 1 051191221519 05!19221832 733C S Reactive Cyanide Analytical Method EPA 9014 Preparation Method SW-846 7 3 3 2 Pace Analytical Services - Greensburg Cyanitle, Reactive NO mi 100 1 05116!22 13 50 05116122 14 47 734S Reactive Sulfide Analytical Method SM 4500,S2-F-2011 Preparation Method SW-846 7 3 4 2 Pace Analytical Services - Greensburg Sulfide. Reactive ND roi 1000 1 05n61221350 05/161221359 Ht,H2 REPORT OF LABORATORY ANALYSIS This reVon shall not be repoxI a reyt in full Date 06/0312022 05-52 PM without the written consent of Pace Analytical Selvicee LLC Page 6 of 33 PO Box 228 a Statesville, NC 28687 a 704/872/4697 Page 9 of 36 Analytical EnNironniental Services, Inc Uate: In-bfey-_'_ II Client: Pace Ana1)1,nA lien ¢cw le, Client Sample ID: 2H1505-26-III 1'mjeet dame: 9260:531 Collection Date. 5'S 2022 9 30 00 ANI Lab ID: 2205B84-001 blavia; S.W \nahaca Rrsnll Reporting Qual lmis BatehlD Dilution Date \nal)reA \nalust Limii Factor CHLORINNrED HERBICIDES SR8I51A (S\535500 ♦ 4 4.1 BRI 1,50WI rrg Le+L. 116114 1 11, 12 20" " Iq Kit 24.5-TP (Slhex) Bolt 6q)00 mng.L` 3:e 114 1 05 1 1,10]"1I4 Kit 2 4-1) BILL M"(10 rrp 1 p-arr W1114 1 UI 12 20" 2214 KH 2 4-D13 BRI I I01100 up hp It., 116114 1 "1 1_ 102_ 2_1 W Kit Dalapon BRL oAulon ug Ng4, 11,114 1 051_'20122L4 Kit D¢emba BRL na000 u_hg.M1. 311114 1 1F 12.2II2222114 Kit D eehlnrplop BRL 65MU uy hr-a11 136114 1 651"1121"W Kit Dmoseb HRI 170000 rrg Kp do :LH IJ I 1,1112112220.1 Kit WP4 BRI n<IHOW, ut tS.6v :'PIIJ Ili 11 2204 All \IC PP BRI 1"(100009 u, hg Jn 11e114 1 ON 1"n""W Kit S,,rr D('AA 4-1 419-110 '.An 111'1 IJ 1 Oa 12 22 W Kit PERCENT NtO1S'IDRE D2216 Poeoui""tule R485AI4 1 IK 112022110 W IR ou'..on \eluevv.vv, I. n I.. I I r....ul n I I I I I I a I I'II v v l 1 1.rr 1- lv.rlxv ahnv vl• I,II rur I...,II IM "III. I'I ♦ \lut Pevir�rr rev vv6lrrn.r. vlr.e u.,n urr. 11 Ilvlvlrnv rrni.v rv.r ervl.nrau..u.x runlv.i.va. :.I:.i \vrr ♦vv .....rnr ui 1 1nvl�ry mn \Il i(vvn.rr..l 1 anilr �..l ri rM1vlrlv..luvl•I.vv.. error rr.niv iryv nv'rinxl M \n.rlvly avr.vlvrl in rM1v r..v�r uv.l rrn'IluuiFu r! I..v ur.n Ilv •rlrv:uv rrr�.rr,r!IoIR—.1 nl.,, 1 "I 1A1, d r 11 iv rnr,. r,.r Mry..r e.p-„I I 11 page 29 of 33 Page 3 of 7 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 32 of 36 U.S. Biosolids Inc 958 Hoots Road Roaring River, NC 28669 Receive Date: Reported: For: Comments: Analytical Results 05/05/2022 06/10/2022 N WILKESBORO Sample Number Parameter Sample ID Result 220505-23-01 30 Day Benchscale N. 15.5 WILKESBORO Respectfully submitted, 5�P. J. ';` Melissa Myers NC Cert #440, NCDW Cart #37755, EPA #NC00909 Unit Method EPA625-R-92M S STATESVILLE ANALYTICAL Analyzed Analyst 05/05/2022 MD PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page i of 6 30 Day Bench Worksheet Sample ID # 220505-23-01 WEEK 1 Date: 5/6/22 10:45 Samples Total Solids Volatile Solids % Volatile Fraction I 1 1.13 0.71 2 I 1.13 0.70 3 I 1.16 0.72 I Average: I 1.14 0.71 0.6228 WEEK 2 Date: 5/12/22 15:00 Samples Total Solids Volatile Solids % Volatile Fraction 1 1.11 0.68 2 1.12 0.68 1 I 3 1.10 0.67 i Average:1 1.11 0.68 _ 0.6126 WEEK 3 Date: 5/18/22 16:00 Samples Total Solids Volatile Solids I % Volatile Fraction 1 1.08 0.64 1 2 1.07 0.64 3 1.07 0.64 I 1 Average: 1.07 0.64 1 0.5981 WEEK 4 Date: 5/24/22 16:00 Samples Total Solids Volatile Solids % Volatile Fraction 1 1.02 0.58 I 2 1.03 I 0.58 I 3 1.04 I 0.60 Average: 1.03 I 0.59 0,5728 WEEK 5 Date: 5/31122 16:00 I Samples Total Solids Volatile Solids % Volatile Fraction 1 I 1 1.06 0.62 2 1.04 0.60 3 1.03 0.60 Average: 1.04 0.61 0.5865 WEEK 6 Date: 6/6/22 15:00 Samples Total Solids Volatile Solids % Volatile Fraction 1 1.04 0.61 I 2 1.02 0.59 3 1.04 0.61 Average: 1.03 0.60 0.5825 Van Kleeck Reduction: 0.6228 - 0.5825 X 100 = 15.5 % 0.6228 - ( 0.6228 X 0.5825) Final Result: 15.5% PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 5 YADKIN VALLEY SEWER AUTHORITY NC0020567 0Waypoint 7621 -7 Road, Richmond, Main 804-743-9401 0Fax ain 80 27 -6446 804-271-6446 ANALYTICAL www.waypointanalytical.com 46381 US Biosohds Inc Project Yusa Dennis Key Report Date : 03/23/2022 958 Hoots Road Information Received : 03/15/2022 Roaring River , NC 28669 �oavr �1/ Grvor� Paunc Mc Groary Ph.D., CPA Report Number : 22-074-0003 REPORT OFANA2 YSIS Agronomist Lab No : 57146 Matrix: Solids Sample ID : Yusa Sampled: 3/14/2022 13:00 Test Results Units MOL OF Date / Time By Analytical Analyzed Method Moisture 97.0 % 0.010 1 03/16/2216:04 FMM SM-254OG Sulfur 6630 mg/Kg - dry 333 1 03/19/22 11:13 EAL 6010D Calcium 7670 mg/Kg - dry 1670 1 03/19/22 11:13 EAL 6010D Aluminum 59700 mg/Kg - dry 167 1 03/19/22 11:13 EAL 6010D Manganese 483 mg/Kg - dry 16.7 1 03/22/22 04.00 EAL 6010D Organic N 37830 mg/Kg - dry 8333 1 03/21/22 11:30 CALCULATION Nickel 17.7 mg/Kg - dry 8.33 1 03/19/22 11:13 EAL 6010D Lead 17.7 mg/Kg - dry 10.0 1 03/19/22 11:13 EAL 6010D Arsenic <16.7 mg/Kg - dry 16.7 1 03/19/22 11:13 EAL 6010D Selenium <16.7 mg/Kg - dry 16.7 t 03/19/22 11:13 EAL 6010D Test Results Units MOL OF Date / Time By Analytical Analyzed Method Total Solids 2.95 % 0.010 1 03/16/22 16:04 FMM SM-2590G Phosphorus 31100 mg/Kg - dry 167 1 03/19/22 11:13 EAL 6010D Copper 205 mg/Kg - dry 16.7 1 03/19/22 11:13 EAL 6010D Total Kjeldahl Nitrogen 43000 mg/Kg - dry 8330 1 03/21/22 11:30 JPJ fM-4500-NH3C-TKr Qualifiers/ OF Dilution Factor MQL Method Quantitation Limit Definitions Waypoint. ANALYTICAL 46381 US Biosolids Inc Dennis Key 958 Hoots Road Roaring River , NC 28669 Report Number : 22-074-0003 Lab No : 57146 Sample ID : Yusa 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-94010Fax 804.271-6446 www.waypoititanalytical.com Project Yusa Information : REPORT OF ANAL YSIS Report Date: 03/23/2022 Received : 03/15/2022 Taus p11 &cowr Paunc Mc Groary Ph.D., CPA Agronomist Matrix: Solids Sampled: 3/ 14/2022 13:00 Potassium 5400 mg/Kg - dry 333 1 03/19/22 11:13 EAL 6010D Magnesium 3170 mg/Kg - dry 167 1 03/19/22 11:13 EAL 6010D Sodium 2170 mg/Kg - dry 833 1 03/19/22 11:13 EAL 6010D Iron 20500 mg/Kg - dry 333 1 03/22/22 04:00 EAL 6010D Zinc 517 mg/Kg - dry 41.7 1 03/19/22 11:13 EAL 6010D Ammonia Nitrogen 5170 mg/Kg - dry 3330 1 03/22/22 09:30 JP3 SM-4500-NH3C Nitrate+Nitrite-N <159 mg/Kg - dry 159 1 03/22/22 14:29 ZBD 4500NO3F-2011 Cadmium <3.33 mg/Kg - dry 3.33 1 03/19/22 11:13 EAL 6010D Chromium 24.4 mg/Kg - dry 8.33 1 03/19/22 11:13 EAL 6010D Mercury 2.91 mg/Kg - dry 0.473 1 03/21/22 14:45 ZMT SW-7471B PH 6.0 S.U. 1 03/22/22 15:S5 DRS 9045D Molybdenum <833 mg/Kg - dry 8.33 1 03/19/22 11:13 EAL 6010D Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions SAR Sodium Absorption Ratio Na: Sodium (Mg/L) Equivalent weight 23 Ca - Calcium (Mg/L) Equivalent weight. 20 Mg : Magnesium (Mg/L) Equivalent weight 12 Milli Equivalent = Mg/L / Equivalent weight Na M /L Ca(Mq/L) Mg(Mq/L) 64.015 1226.265 I 64.015 Na _(ME) I Ca (ME) I Mg�MEZ 2.783261 11.31325 15 334583 SAR= Na Milli Equivalent/[0 5 X (Ca Milli Equivalent + Mg Milli equivalent)]0 5 power SAR = 0.964695'(From Mg/L entered above) SAR= 0.971894 (From ME entered below) Na (ME) Ca (ME) Mg (ME) 28 1 11 3 1 5.3 The amour amount of Permitting c O c O m N 01 Vl E II 2 II E II D 11 C O O N Co O _ Q X X N Z + m Y N rn Y Q Q Cl)O Z + E + Cl) O = Z O> + w C to = ♦ w + Z M C] A rn Z z tf p D o Y Y F- v N � > N 2 O Z m Z d Q ` Q ` rn Z 0 IL Zto _a _a a_ aMU) aco coo coo M CDM O xI Z aD > N p M > M N--c�_ O Z) o O � 0 d F MM 7 co y � Y V aE a aE o. c O M eo co m O 0 0 0 z a _ pN O O M Z Q N �L) T p to Analytical Results U.S. Biosolids Inc 958 Hoots Road Roaring River, NC 28669 Receive Date: 09/22/2022 Reported: 10/31/2022 For: YVSA Comments: Sample Number Parameter Sample ID 220922-28-01 30 Day Benchscale YVSA Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cart #37755, EPA #NC00909 Result Unit Method 5.4 % EPA625-R-92/6 STATESVILLE ANALYTICAL Analyzed Analyst 09/22/2022 MD PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 5 30 Day Bench Worksheet Sample ID # 220922-28-01 WEEK I Samples Total Solids Volatile Solids I % Volatile Fraction I 1 1.07 0.58 2 1.07 0.58 3 1.07 0.57 Average: 1.07 0.58 0.5421 I WEEK 2 I Samples Total Solids Volatile Solids % Volatile Fraction I 1 1.10 0.59 I 2 1.08 0.58 3 I 1.06 0.57 I Average: I 1.08 0.58 0.5370 WEEK 3 Samples ( 1 I 2 I 3 Average: WEEK 4 Samples I 1 I 2 I 3 Average: Total Solids Volatile Solids % Volatile Fraction I 1.08 0.58 I 1.08 0.58 I 1.07 0.57 I 1.08 0.58 0.5370 I Total Solids 1.08 1.05 1.08 1.07 WEEK 5 Samples I Total Solids 1 1.12 2 1.12 3 1.12 Average: 1.12 Volatile Solids % Volatile Fraction 0.58 I 0.57 I 0.58 0.58 0.5421 Volatile Solids I % Volatile Fraction 0.60 0.60 0.60 0.60 0.5357 WEEK 6 1 Samples Total Solids Volatile Solids % Volatile Fraction 1 1.05 0.55 2 1.06 0.57 I 3 1.06 0.57 Average: 1.06 0.56 0.5283 Van Kleeck Reduction: 0.5421 - 0.5283 X 100 = 5.40 % 0.5421 - ( 0.5421 X 0.5283) Final Result: 5.4% PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 5 Analytical Results U.S. Biosolids Inc 958 Hoots Road Roaring River, NC 28669 Receive Date: 03/03/2022 Reported: 03/07/2022 For: YVSA Comments: Geometric Mean: 42,978 MPNIg (Most probable number) STATESVILLE ANALYTICAL Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 220303-21-01 Fecal Coliforms 1 162338 MPWg SM92210E-2006 031032022 MD 220303-21-01 Percent Solids 1 3.08 % SM25408-2011 03/03/2022 MD 220303-21-02 Fecal Coliforms 2 115512 MPN/g SM92210E-2006 03/03/2022 MD 220303-21-02 Percent Solids 2 3.03 ova SM2 08-2011 03/03/2022 MD 220303-21-03 Fecal Coliforms 3 34810 MPN/g SM92210E-2006 03/03/2022 MD 220303-21-03 Percent Solids 3 3.16 % SM2640a-2011 03/03/2022 MD 220303-21-04 Fecal Coliforms 4 26490 MPN/g SM9zzlcE�2ws 03/03/2022 MD 220303-21-04 Percent Solids 4 3.02 % SM2WB-2011 03/03/2022 MD 220303-21-05 Fecal Coliforms 5 26667 MPN/g SM92210E-2006 03I03/2022 MD 220303-21-05 Percent Solids 5 3.00 % SM2WB-2011 03/03/2022 MD 220303-21-06 Fecal Coliforms 6 16340 MPN/g SM92210E-2006 03/03/2022 MD 220303-21-06 Percent Solids 6 3.06 % SM26496-2011 03/032022 MD 220303-21-07 Fecal Coliforms 7 35948 MPNIg SM92210E-2M 03103/2022 MD 220303-21-07 Percent Solids 7 3.06 % sWWB-2011 03/03/2022 MD Respectfully submitted, Melissa Myers NC Cart #440, NCDW Cert #37755, EPA #NG00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 4 aceAnaVicala asle.leeaetaaaa ANALYTICAL RESULTS Project: US BIOSOLIDS YVSA Pace Project No.: 92591527 Sample: US BIOSOLIDS NSA Lab ID: 92591527001 Collected: 03/03/2208:15 Received: 03/0412210:15 Results reported on a 'dry wefl;W basis and aft adjusted forpement moisture, sample size and any dilue'ons. Parameters Results Units Report Limit OF Prepared Analyzed Pau Analytical Seni LLC 9800 kinoy Ave. Suite 100 Henteovllb. NC 28078 (704)B75.9092 Matrix: Solid CAS No. Oual 8081 TCLP Pesticides FIVE Analytical Method: SPA8081B Preparation Method: EPA3510C Leachate Method/Date: EPA 1311; 03I07/22 14:30 Initial pH: &48; Final PH: 5 Pace Analytical Services - Charlotte gamma-8HC (Undane) NO ug/L 0.50 1 03/110/2212:29 03/112214:47 5949-9 Chlordene(Technlce0 ND ug/L 3.0 1 03/10/22 12:29 03/11/22 14:47 57-74-9 Endnn ND ug/L 0.50 1 03/102212:29 03/112214,47 72-205 Heptachlor ND ug)L 0.50 1 0&101P212:29 OVIII2214:47 764" Heptachlor epoxide ND ug/L 0.50 1 03/10122 12:29 0311112214:47 1024.57-3 Methoxychlor ND ug/L 1000 1 0311012212:29 03111/2214:47 72-435 Toxaphene ND ug1L 3.0 1 03/1012212:29 0311112214:47 8001.352 Surrogates Decachloroblphanyl(S) 102 % 1D-154 1 031102212:29 03/11/2214:47 2051-24-3 Tetrachloro-m-xylene (S) 83 % 10.184 1 0311012212:29 03/112214:47 87759-8 8082 OCS PCB Analytical Method: EPA 8082A Preparation Method: EPA 3546 Pace Ane"cal Services - Chanotte PCB-1016 (Aroclor 1016) NO ug/kg 66700 1 03/09/22 16:24 03/10/22 10:43 12674-11-2 PCB-1221 (Aroclor 1221) NO ug/kg 66700 1 0310921 16:24 03/10I22 10:43 11104-28.2 PCB-1232 (Aroclor 1232) ND ugtkg 66700 1 03/0922 16:24 0311022 10:43 11141-16-5 PCB-1242 (Aroclor 1242) ND u9/110 66700 1 03/0922 1&24 0&10122 1043 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/kg 66700 1 03/09122 16:24 03/10/22 10:43 12672-29.6 PCB-1254 (Arodor 1254) NO ug/kg 66700 1 0310922 16:24 OW1022 10:43 11097-69.1 PCB-1260 (Aroclor 1260) ND ug/kg 66700 1 031092216:24 0311012210:43 1109852-5 Surrogates Decachlorobiphenyl(S) 21 % 10-160 1 03109122 16:24 113110122 t0:43 2051.24-3 8052 TCLP PCBs RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C Leachate Method/Date: EPA 1311; 0310722 14:30 Initial pH: 5.46; Final pH: 5 Pace Analytical Services - Charlotte PCB-1016 (Arodor 1016) NO ug/L 1000 1 03/1012212:29 03/11/2217:06 12674-11.2 PCB-1221(Aroclor 1221) ND ug/L 1000 1 03/1012212:29 031112217:06 11104-28-2 PCB-1232 (Arodor 1232) ND ug/L 1000 1 03/10/22 12:29 0311112217:06 11141-165 PCB-1242 (Aroclor 1242) NO ug/L 1000 1 03/101221229 03/11/22 17:06 53469-21.9 PCB-1248 (Aroctor 1248) NO ug/L 1000 1 0311022 1229 031112217:08 12672-29-8 PCB-1254 (Aroclor 1264) NO ug/L 1000 1 03110/22 12:29 03/11/22 17:06 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 1000 1 0311GO 12:29 03/1112217:06 11096-82-5 Sunogetes Decachloroblphenyl(S) 94 % 10-181 1 0311022 12:29 03/11/22 17:06 2051-24-3 6010D ATL ICP, TCLP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Leachate Method(Date: EPA 1311; 03/14122 15:00 Initial pH: 8.24; Final pH: 5A1 Pace Analytical Services - Peachtree Comers, GA Arsenic ND mg/L 0.30 1 03/1522 15:3D 0311622 00:31 7440-3&2 Barium ND mg/L 0.50 1 031152215:30 03/16/2200:31 7440-39.3 Cadmium ND mg/L 0.10 1 03/152215:30 03/1612200:31 744043.9 Chromium ND mg0. 0.10 1 031152216:30 03/16M D0:31 744047-3 Lead ND mg/L 0.25 1 0311512215:30 03/162200:31 7439-92-1 REPORT OF LABORATORY ANALYSIS This capon shall not be repraduced, escapt in full, Date: 03/18)2022 04:5S PM vAhow the wrinen consent of Pace Analytical Services, LLC. Page 5 o133 PO Box 228 a Statesville, NC 28687 a 704/872/4F Page 9 of ' 8CeAnaVical e •arslssshbsms ANALYTICAL RESULTS Pau Analytical Sarvicea, LLC 980010ncay Ave. Suite100 Huntar rylb, NC 28078 (704)075.9092 Project: US BIOSOUDS YVSA Pace Project No.: 92591527 Sample: US BIOSOLIDS TVSA Lab ID: 92591527001 Collected: 03103/22 08:15 Received: 031D4/22 10:15 Matrix: Solid Results reported on a -dry weight- oasis and are adjusted for percent moisture, aample size and any dilutions. Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual 60100 ATL ICP, TCLP Analytical Method: EPA 60100 Preparation Method: EPA 3010A Leschate Method/Date: EPA 1311; OW142215:00 Initial pH: 8.24; Final pH: 5.41 Pace Analytical Services - Peachtree Comers, GA Selenium ND mg/L 0.40 1 0311512216:30 03/162200:31 7782-49-2 Silver NO mg/L 0.10 1 03/152215:30 03/162200:31 7440.22-4 7470 Mercury, TCLP Analytical Method: EPA 7470A Preparation Method: EPA 7470A Leachate Method/Date: EPA 1311; 03/14/22 15:00 Initial pH: 8.24; Final pH: 5A1 Pace Analytical Services - Peachtree Comers, GA Mercury ND mglL 0.0050 1 0311612207:45 031162213:09 7439-97-6 M1 8270E TCLP RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Leachale Mathod/Date: EPA 1311; 03/0722 14:30 Initial pH: 5A6; Final pH: 5 Pace Analytical Services - Charlotte 'IA-Dichlombenzene ND ug/L 50.0 1 03/09/22 16:34 03/10/22 12:03 10646-7 2,4-Dinitrotoluene ND ug/L 50.0 1 03/09/22 16:34 03/10/22 12:03 121-14-2 Hexechloro-1,3-butediene NO uglL 50.0 1 0311192216:34 03/102212:03 87418.3 Hexechlorobenzene ND ug/L 50.0 1 031092216:34 03/10/22 12:03 118-74-1 Hexachloroelhane ND ug/L 50.0 1 03I0922 16:34 0311022 12:03 67-72-1 2-MethNphenol(o-Cresol) ND ug/L 50.0 1 031092216:34 031102212:03 9548-7 384-Methylphenol(milp Cresol) ND ug/L 50.0 1 031092216:34 031102212:03 IN31-104 Nitrobenzene ND uglL 50.0 1 03/09/22 16:34 03110/2212:03 98-95.3 Pentachlomphenol ND ug/L 100 1 0310912216:34 0311=212:03 87-0" Pyridine ND ug/L 50.0 1 03109/22 16:34 0311022 12:03 110-86-1 2,4,5-Trichlorophenol ND ug/L 50.0 1 0310922 16:34 03/10/22 12:03 95-954 2,4,6-Trichlorophenol ND uglL 50.0 1 03/0922 16:34 03110/22 12:03 88-06-2 Surnwates Nitrobenzene-d5 (S) 92 % 10-144 1 03/092216:34 03/102212.03 416MO-0 2-Fluombiphenyl(S) B4 % 10-130 1 03/09/22 16:34 0311022 12:03 3214M-8 TerphenylE14(S) 150 % 34-163 1 03/0912216:34 03/102212:03 1718.51-0 Pheno1-16 (S) 57 % 10.130 1 031092216:34 03/102212:03 13127-88-3 2-Fluorophend (S) 75 % 10-130 1 0310922 16:34 031102212:03 367-124 2,4,6-Tribromophanol(S) 96 % 10-144 1 03/0922 16:34 03/10122 12:03 118-79-6 8260D MSV TCLP Analytical Method: EPA 82600 Leachale Method/Date: EPA 1311; 03M9/22 1325 Paco Analytical Services - Charlotte Benzene ND ug/L 100 20 03/10/2214:39 71-43-2 2-Butanons (MEK) NO ug/L 200 20 031102214:39 78.93-3 Carbon tetrachloride ND ug/L 100 20 031102214:39 56.235 Chlorobenzene ND uglL 100 20 031102214:39 106-90-7 Chloroform NO ug/L 100 20 0311012214:39 67-66.3 1A.Dichlorooenzene ND ug/L 100 20 03/102214:39 106-46-7 12-Dichloroethane ND ug/L 100 20 0311022 14:39 107-06.2 1,1-Dichlomethene ND ug/L 100 20 03/102214:39 76-36-4 Telrachlomethene ND u911- 100 20 03110/2214:39 127-184 Trichloroethene NO ug/L 100 20 0&10/2214:39 79-01-5 REPORT OF LABORATORY ANALYSIS This repon shall not be Wimduca4. except In full, Date: 03/1812022 04:55 PM Wilicut the written consent of Pace Analytical Services. LLC- Page 6 of 33 PO Box 228 a Statesville, NC 28687 a 704/872/4697 Page 10 of 39 Pace Analytical SaMus. LL0 17 2eAmlyficalo 9800 KIncey Ave. Suite 100 Huntersville. NC 28078 trw.weWbasa (704)875.9092 ANALYTICAL RESULTS Project US BIOSOUDS YVSA Pace Project No.: 92591527 Sample: US BIOSOLIDS TVSA Lab ID: 92SO1527001 Collected: 03/03/2208:15 Received: 031D4/2210:15 Matrix: Solid Results reported on a 'dry weight' basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual 8260D MSV TCLP Analytical Method: EPA 8260D Leachate Method/Dale: EPA 1311; 03/09/22 13:25 Pace Analytical Services - Charlene Vinyl chloride ND ug/L 100 20 03/10/22 14:39 75-01-4 Surrogates 1,2-Dichioroethaned4(S) 95 % 70-130 20 03110/2214:39 17060-07-0 Toluene-d8 (S) 102 % 67-135 20 03/10/22 14:39 2037-26.5 4-8romo8uorubamene(S) 100 % 70-130 20 03110/2214:39 480-004 Percent Moisture Analytical Method: SW-846 Paw Analytical Services - Charlotte Paimm Moisture 97.0 % 0.10 1 03/08/22 16:19 N2 1010 Flashpolnt.Closed Cup Analytical Method: EPA 1010E Paw Analytical Services -Asheville Flashpoint >200 dog F 70.0 1 03/1712213:05 904S pH Soil Analytical Method: EPA 9045D Paw Analytical Services - Asheville pH at 25 Degrees C 6.8 Std. Units 0.10 1 03/07/22 14:48 H3 9095 Paint Filter Liquid Test Analytical Method: EPA 9095E Paw Analytical Services - Asheville Free Liquids FAIL 1.0 1 03108M 09:42 Percent Moisture Analytical Method: Moisture Pace Analytical Services - New Orleans Percent Moisture 97.1 % 0.50 1 03/15/22 11:16 733C S Reactive Cyanide Analytical Method: SW-846 7.3.32 Preparation Method: SW-846 7.3.32 Paw Analytical Services - New Orleans Cyanide, Reactive ND mg/kg 25.0 1 03117/2209:34 03/1812208:52 734S Reactive Sulfide Analytical Method: SM 4500S2.F-2011 Preparation Method: SW-848 7.3.4.2 Pace Analytical Services - Greensburg Sulfide, Reactive ND mg/kg 338 1 03/10/22 19:38 0311CV2219:59 REPORT OF LABORATORY ANALYSIS This revert shall not be reproduced. except in cal. Date: 03/18/2022 04:55 PM without the written consent of Pace Analy0m Services. LLC. Page 7 of 33 PO Box 228 a Statesville, NC 28687 a 704/872/4697 Page 11 of 39 Analytical Environmental Services, Inc Date: 14-Mar-22 Client: Pace Analytical Client Sample lD: US BIOSOLIDS TVSA Project Name: 92591527 Collection Date: 3/3/2022 8.15 OOAM Lab ID: 2203A21-001 Matrix: Solid Reporting Dilution Analyses Result Qual Units BatchlD DateAnalyzed Analyst Limit Factor BERBICIDES,TCLP SW1311/8151A (SW3510C) 2,4,5-TP(Silvex) BRL 0.20 myL 332444 1 03111/1022 17 50 KH 2,4-D BRL 020 mg/L 332444 1 03/11/2022 17 50 KH Surr: DCAA 666 501-120 %Rec 332444 1 03A 1/2022 17 50 KH panm,m ....el BRL Below rtOomnF limn S Spike Reemery ouladc limit, dne mmatm H Holtlm, nm-mr przpaeveon or mulsie eeeeeded Nvrt So, cn. naretwe N Anal,.,—NFLAC c,mr,d F Anely,ed in the lA x hwh,, a d—wim, mom ilo—thud H Amlvp dan¢d m th—w v-mel method blmk < Le., lhav Be,.], crem,r:n.n xe:mr.ane / Emmaea.ame dammed below Retiring t mel Page 30 of 33 Page 3 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 34 of 39 FOREST CITY NC0025984 0Waypoint, 7621 -7 Road, Richmond, Main 804-743-9401°Fax ain 80 27 -6446 804-271-6446 ANALYTICAL www.waypoiiitanalytical.com 46381 US Biosolids Inc Project Forest City Dennis Key Report Date : 03/23/2022 958 Hoots Road Information . Received : 03/15/2022 Roaring River , NC 28669 Tp 'r Mt 610wr Report Number : 22-074-0002 REPORT OFANAL YSIS Pauric Mc Groary Ph.D., PA C Agronomist Lab No : 57145 Matrix: Solids Sample ID : Forest City Sampled: 3/14/2022 9:30 Test Results Units MCL DF Date / Time By Analytical Analyzed Method Moisture 85.5 070 0.010 1 03/16/2216:04 FMM SM-254OG Sulfur 8550 mg/Kg - dry 69.0 1 03/19/22 11:08 EAL 6010D Caloum 9240 mg/Kg - dry 345 1 03/19/22 11:08 EAL 6010D Aluminum 22900 mg/Kg - dry 34.5 1 03/19/22 11:08 EAL 6010D Manganese 172 mg/Kg - dry 3.45 1 03/22/22 03:45 EAL 6010D Organic N 52480 mg/Kg - dry 1724 1 03/21/22 11:30 CALCULATION Nickel 13.2 mg/Kg - dry 1.72 1 03/19/22 11:08 EAL 6010D Lead 52.3 mg/Kg - dry 2.07 1 03/19/22 11:08 EAL 6010D Arsenic 4.08 mg/Kg - dry 3.4S 1 03/19/22 11:08 EAL 6010D Selenium 9.10 mg/Kg - dry 3.45 1 03/19/22 11:08 EAL 6010D Test Results Units MCL DF Date / Time By Analytical Analyzed Method Total Solids 14.5 % 0.010 1 03/16/22 16:04 FMM SM-254OG Phosphorus 22300 mg/Kg - dry 34.5 1 03/19/22 11:08 EAL 6010D Copper 321 mg/Kg - dry 3.45 1 03/19/22 11:08 EAL 6010D Total Kleldahl Nitrogen 52500 mg/Kg - dry 1720 t 03/21/22 11:30 JPl ;M-4500-NH3C-TKP Qualifiers/ DF Dilution Factor MQL Method Quanhtation Limit Definitions Waypoint. ANALYTICAL 46381 US Biosolids Inc Pro]ect Forest City Dennis Key 958 Hoots Road Information Roaring River , NC 28669 Report Number:22-074-0002 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401°Fax 804-271-6446 www.waypointanalytical.com REPORT OF ANAL PSIS Report Date : 03/23/2022 Received : 03/15/2022 Tr is (4t Groat/ Pauric Mc Groary Ph.D., CPA Agronomist Lab No: 57145 Matrix: Solids Sample ID : Forest City Sampled: 3/14/2022 9:30 Potassium 4390 mg/Kg - dry 69.0 1 03/19/22 11:08 EAL 6010D Magnesium 2900 mg/Kg - dry 34.5 1 03/19/22 11:08 EAL 6010D Sodium 717 mg/Kg - dry 172 1 03/19/22 11:08 EAL 6010D Iron 13400 mg/Kg - dry 69.0 1 03/22/22 03:45 EAL 6010D Zinc 1260 mg/Kg - dry 8.62 1 03/19/22 11:08 EAL 6010D Ammonia Nitrogen <690 mg/Kg - dry 690 1 03/22/22 09:30 ]P] SM4500-NH3C Ndrate+Nitrite-N 46.6 mg/Kg - dry 34.5 1 03/22/22 14:27 ZBD 4500NO3F-2011 Cadmium 1.88 mg/Kg - dry 0.690 1 03/19/22 11:08 EAL 6010D Chromium 37.0 mg/Kg - dry 1.72 1 03/19/22 11:08 EAL 6010D Mercury 0.537 mg/Kg - dry 0.106 1 03/21/22 14:43 ZMT SW-7471B PH 5.4 S.U. 1 03/22/2215:55 DRS 9045D Molybdenum 6.75 mg/Kg - dry 1.72 1 03/19/22 11:08 EAL 6010D Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions N Cl)y v 3 D (D Z m A)O Old 01 G CD N O .� V W s N M Z m Z O p O N •�i. OAf O Ot O 0 O O N O 0/ 07 7 zo F Z Z n 10 c m o Z o � � A O W N C N NN m . 91 N N N ff% ?Acn m 6 N Q .mi m m m m D M D z O Z < a 0 < 0 z d z d 0 0 0 D 0 D 3 m Z m Z IZ O 0) 3 m N e CL m m o z z z A 0 3 S 2 N CL W W N + + Z 0 W Z N a Z a: ID 2 O W + Z (n + D O O O + I0 N x Z _ 00 X X O ' O oN O N 0 X N O n p u u N_ u Ip N N 00 O O O O n m c SAR Sodium Absorption Ratio Na(Mq/L) Ca(Mq/L) Ma(_Mg/L) Na Sodium (Mg/L) Equivalent weight. 23 103.965 1339 8 420.5 Ca. Calcium (Mg/L) Equivalent weight 20 Mg Magnesium (Mg/L) Equivalent weight 12 Na (ME) Ca (ME) MgIME 4.520217 66 99 35.04167 Milli Equivalent = Mg/L / Equivalent weight The amour amount of SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0 5 power Permitting SAR = 0.632859'(From Mg/L entered above) SAR= 0 630126 (From ME entered below) Na (ME) Ca (ME) Mg (ME) 4.5 1 67 1 35 . PaceilnalXical nne.iai d.b ra. ANALYTICAL RESULTS Project FOREST CITY FULL TCLP Pace Project No 92593152 Sample220310-26.01 Liable 92593152001 Collected 0311012208, 45 Received 03111122 10 27 Results trepanation a "dry weigsW basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed Pace Analytical Services, LLC 9800 Kmcwy Ave Sude 100 Hvnterscile NC 28078 VO4)875 9092 Matnx Solid CAS No Coal $081 TCLP Pesticides RVE Analytical Method EPA 80818 Preparation Method EPA 3510C Leachate Method/Date EPA 1311 03/15/22 15 08 initial pH 4 65, Final pH 5 Pace Analytical Services - Charlotte gamma-BHC (Lindane) NO i lL 050 1 03116/22 17 21 03117/22 07 37 58-89-9 Chlordane (Technical) ND ug1L 30 1 03/16/22 1721 03117122 07 37 57-74-9 Endrm NO ug/L 050 1 03/16/22 1721 03/17/22 07 37 72-20-8 Heptachlor ND ug/L 050 1 03116/22 1721 03/17/22 07 37 76.44-8 Heptachlor epoxide ND ug/L 050 1 03/16r22 1721 03117/22 07 37 1024-57-3 Methoxychlor ND ug/L 1000 1 0311622 1721 03117/22 07 37 72-43.5 Toxaphene NO ul 30 1 03/16221721 03117122 07 37 8001-35-2 Surrogates Decachlorobiphenyl (S) 103 % 10-154 1 03/16/22 1721 03/17122 07 37 2051-24-3 Tetrachloro-onaylene(5) 89 1/. 10-184 1 031161221721 0117122 07 37 877-09-8 8082 GCS PC8 Analytical Method EPA 8082A Preparation Method EPA 3546 Pace Analytical Services - Charlotte PCB-1016 (Aroclor 1016) No uglkg 234 1 03/14/22 22 24 03/15122 16 16 12674-11-2 PCB-1221 (Aroclor 1221) ND uglkg 234 1 03/14/22 22 24 03/15/22 16 16 11104-28-2 PC8-1232 Aroclor 1232) ND uglkg 234 1 03/14/22 22 24 03/15122 16 16 11141-16-5 PCB-1242 (Aroclor 1242) ND uglkg 234 1 03/14/22 22.24 03/15/22 16 16 53469-21-9 PCB-1248 (Aroclor 1248) ND uglkg 234 1 03114122 22 24 03/15122 16 16 12672-29-6 PCB-1254(Arodor 1254) ND uglkg 234 1 03/14122 22 24 03115/221616 11097-69-1 PCB-1260 (Aroclor 1260) ND i lkg 234 1 03/14/22 22 24 03/15/22 16 16 11096-82-5 Surrogates Decachlorobiphenyl(S) 46 % 10-160 1 03114/22 22 24 03/15/22 16 16 2051-24-3 8082 TCLP PC8s RVE Analytical Method EPA 8082A Preparation Method EPA 3510C Leachate Method/Date EPA 1311; 03115122 15 08 Initial pH 4 65, Final pH 5 Pace Analytical Services - Charlotte PCB-1016 (Aroclor 1016) NO ug1L 1000 1 03/16/22 1721 03117/22 1939 12674.11-2 PCB-1221 (Annear 1221) NO tl 1000 1 03116/22 1721 03117/22 19 39 11104-28-2 PCB-1232 (Aroclor 1232) NO ill 1000 1 03/16/22 17 21 G3117/22 1939 11141.16.5 PCB-1242 (Aroclor 1242) NO ti 1000 1 03116i22 17 21 03117122 1939 53469-21-9 PCB-1248 (Aroclor 1248) ND ug.4 1000 1 03116/22 1721 03117122 1939 12672-29-6 PCB-1254 (Al 1254) ND ug1L 1000 1 03M622 1721 03117'22 19 39 11097-69-1 PCB-1260 (Aroclor 1260) ND ug1L 1000 1 03/16/22 1721 03117122 1939 11096-82-5 Surrogates Decachlorobiphenyl(S) 99 % 10-181 1 03/16/22 1721 03117122 19 39 2051-24-3 6010D ATL ICP, TCLP Analytical Method EPA 6010D Preparation Method EPA 3010A Leachate Method/Dale EPA 1311, 03/30122 13 40 Initial pH 9, Final pH 5 15 Pace Analytical Services - Peachtree Corners GA Arsenic ND ri 030 1 03/31/22 15 03 04/01/22 20 01 7440-38-2 Sanum NO mg/L 050 1 03/31/22 15 03 04101122 20 01 7440-39-3 Cadmwm ND o l 010 1 03131/221503 04el!222001 7440-43-9 Chromium 0.16 hi a10 1 03131/22 15 03 04/01122 20 01 7440-473 Lead NO mg/L 025 1 03/31122 15 03 04101 /22 20 01 7439-92.1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in lull Date 04/04/2022 04 54 PM without the written consent of Pace Analytical Selmces LLC R1 R1 Ri Page 5 of 33 PO Box 228 a Statesville, NC 28687 e 704/872/4697 Page 8 of 38 PaceAnalytical s^ay.NtMalesom ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave Suite 100 HuniersW e, NC 28078 (7041875-9092 Project FOREST CITY FULL TCLP Pace Project No 92593152 Sample: 220310-26-01 Lab ID: 92593152001 Collected 03/10/220845 Received 03111/22 10 27 Matrix Solid Results reported on a -dry weight- basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit OF Prepared Analyzed CAS No oust 6010D ATL ICP, TCLP Analytical Method EPA 6010D Preparation Method EPA 3010A Leachate Method/Date EPA 1311, 03130/22 13 40 Initial pH 9, Final pH 5 15 Pace Analytical Services - Peachtree Comers GA Selenium NO mg1L 040 1 03/31/22 15 03 0410V222001 7782-49-2 Silver ND mg1L 010 1 03131/22 15 03 04/01/22 20 01 7440-22-4 7470 Mercury, TCLP Analytical Method EPA 7470A Preparation Method EPA 7470A Leachate MethodlDate EPA 1311. 03/30122 13 40 Initial pH 9, Final pH 5 15 Pace Analytical Services - Peachtree Corners, GA Mercury 0.011 mgfi 00050 1 03131122 15 10 041011220928 7439-97-6 8270E TCLP RVE Analytmal Method EPA 8270E Preparation Method EPA 3510C Leachate MethodlDate EPA 1311 03/15/22 15 08 Initial pH 4 65 Final pH 5 Pace Analytical Services - Charlotte 1.4-Dichlorobenzene ND ug/L 500 1 03116/22 1728 03117122 1238 106.46-7 2.4-0mdrotnluene NO u91L 500 1 03116/221728 03/17/2212.38 121-14-2 Hexachloro 1,3-butadiene NO ug/L 500 1 03/161221728 03/171221238 87-68-3 Hexachlorobenzene ND ug/L 500 1 03/16/22 17 28 03/17122 1238 118-74-1 Hexachloroethane ND ug/L 500 1 03116/22 1728 03/17/22 1238 67-72-1 2-Methylphenol(o-Cresol) NO ug/L 500 1 03/16122 17 28 03/171221238 95-48-7 3&4-Methylphenol(m&p Cresol) NO ug/L 500 1 031161221728 03117122 12 38 15831-10-4 Ndrabenzene ND ug/L 500 1 03/161221728 03117122 12 38 98.95-3 Pentachlomphenol ND ug/L 100 1 03/16122 17 28 03/17122 1238 87.86-5 Pyridine NO ug/L 500 1 03/16122 1728 03/17122 1238 110-86-1 2 4 5-Trichlorophenol NO ug1L 500 1 03116/22 1728 03117122 1238 95-95-4 24,6-Trichlorophenol ND uglL 500 1 031161221728 03117122 12 38 86-06-2 Surrogates Nitrobenzene-d5(S) 73 % 10-144 1 031161221728 03117122 12 38 4165-60.0 2-Fluorobiphenyl(S) 64 10-130 1 03116/22 1728 03/17/22 12 38 321-60-8 Terpher l-d14(S) 103 34.163 1 03/16/221728 0117122 12 38 1718-51-0 Phenoltl6(B) 47 % 10-130 1 03116/22 17 28 03117122 1238 13127-88-3 2-Fluorophenol (S) 60 % 10-130 1 03116/22 1728 03/17/22 1238 367-12-4 2,4 6-Tnbromophenoi (S) 103 % 10-144 1 03116122 1728 03/17/22 1238 118-79-6 8260D MSV TCLP Analytical Method EPA 8260D Leachate Method/Date EPA 1311, 03116122 13 08 Pace Analytical Services - Charlotte Benzene NO ug/L 100 20 03/171221232 71-43-2 2-eutanone (MEK) NO ug/L 200 20 03/17/22 12 32 78-93-3 Carbon tetrachloride NO ug/L 100 20 03/17122 1232 56 23-5 Chlorobenzene ND ug/L 100 20 03117122 1232 108-90-7 Chloroform ND ug/L 100 20 03/17/22 12 32 67-66-3 1.4-Dichlorobenzeae ND ug/L 100 20 03/17122 1232 1013 46-7 1.243ichioroethane ND ug/L 100 20 03/17122 1232 107-06-2 11-13chiomemene ND ug/L 100 20 031171221232 75-35-4 Tebachlomemene NO ug1L 100 20 03117/221232 127-18-4 Tnchloroethene NO 1 100 20 03/17/22 1232 79-01-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date. 04104/2022 04 54 PM without the carmen consent of Pace Analyecal Sernces, LLC Page 6 of 33 PO Box 228 a Statesville, NC 28687 a 704/872/4697 Page 9 of 38 Pace Analytical Services. Li ~ 9800 Kincay Ave Suite 100 n ace Analyhcal Huntersvdle, INC 28078 ainciacM.n.o. (704)875-9092 ANALYTICAL RESULTS Project FOREST CITY FULL TCLP Pace Project No 92593152 Sample: 220310-26-01 Lab ID: 92593152001 Collected 031101220845 Received 03/11122 10 27 Matrix Solid Results reported on a -dry weight- basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit OF Prepared Analyzed CAS No Oual 8260D MSV TCLP Analytical Method EPA 8260D Leachate Methodl0ate EPA 1311, 03/16/22 13 08 Pace Analytical Services - Charlotte Vinyl chloride NO ug/L 100 20 03/17122 1232 75-01-4 Surrogates 1,2-Dichloroethane-d4 (S) 91 % 70-130 20 03;17/22 1232 17060-07-0 Toluene-d8(S) 108 % 67-135 20 03/171221232 2037-26-5 4-8romonuorobenzene (S) 99 % 70-130 20 03117i22 1232 460-00-4 Percent Moisture Analytical Method SW-846 Pace Analytical Services - Charlotte Percent Moisture 85.7 %, 010 1 03/141221625 N2 1010 Flashpolnt,Closed Cup Analyhcal Method EPA 1010E Pace Analytical Services - Asheville Flashpoint >200 deg F 700 1 0312302 12 39 9045 pH Soil Analytical Method EPA 9645D Pace Analytical Services -Asheville pH at 25 Degrees C 5.8 Std Units 010 1 03/16/22 18 04 H3 9095 Paint Filter Liquid Test Analytical Method. EPA 9095E Pace Analytical Services Asheville Free Liquids PASS 1 0 1 03M8/22 15.56 Percent Moisture Analytical Method Moisture Pace Analytical Services - New Orleans Percent Moisture 85.6 % 050 1 03124122 12 04 733C S Reactive Cyanide Analytical Method SW-846 7 3 3 2 Preparation Method SW-846 7 3 3 2 Pace Analytical Services - New Orleans Cyanide Reactive ND mgAg 250 1 03/251220745 03125/22 13 14 734S Reactive Sulfide Analytical Method SM 4500-S2-F-2011 Preparation Method SW-846 7 3 4 2 Pace Analytical Services - Greensburg Sulfide Reactive NO mgi 704 1 031161222045 031l6'222048 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date 04/04/2022 04 54 PM wMoul the came, consent of Paoe Analyhcal Services LLC Page 7 of 33 PO Box 228 a Statesville, NC 28687 e 704/872/4697 Page 10 of 38 Analytical Environmental Services, Inc Client: PJic Analy I,c4l Project Name: 92591152 Lab ID: 2203174-001 Analyses HERBICIDES,TCLP SWI311/8151A 4.sAP(Sdces) 4-D Surr DC'AA Hkl I4'Irrn i:rrr'r�ti lrrnrr H IIv.IJrnu rr.n�. n Mtl arvrr�.n.r,�nnl..r•�,....e.� � .lr�ehrt nr�\'ll ii .cnrir..l 11 4n.I.t..M,.�eJ rn rl�-.r..r.. r.i«J rnenx•J I.IJn4 - Inur�.r Jrnn a..�rlr ..rlu. note: 22-Mar-22 Client sample ID: 2203111-26-01 Collection pate: 3,10,2022 9 4i GRAM Mama: Sohd Reporting Dilution Result Qual Units Balch!) Date .Anah'rM Analyst Limit Pastor (SN'351BC) BRI 920 rnsrl 112811, 1 WIF 21122 11 49 Kit 14RI 010 nrel t3791n 1 ()11h 111217 4a Kit 64-1 ku1-1111 ^.KII tt_t]N 1 W Is,_202217U Kit F I. m.n.Jn nn, ay. n, rrvn r,.rr 1 S �fr,. v. rn•n ..rrnnit lrnrrr. Ju. r.•rnnrrr, 1 trr.rI,11. H1 r.r""I'.lrn r J.v r.nrr.i. lr..rr. rl. rn,xlr.vl Lrrr..r.a1.11r11.l.r.• nlli'l.. ky,.l Page 30 of 33 Page 3 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 33 of 38 Analytical Results U.S. Biosolids Inc 958 Hoots Road Roaring River, NC 28669 Receive Date: 03/10/2022 Reported: 03/11/2022 For: Forest City Comments: GEOMETRIC MEAN: 22,533 MPN/g STATESVILLE ANALYTICAL Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 220310-23-01 Fecal Coliforms FC-1 15385 MPN/g SM92210E-2005 03/10/2022 MD 220310-23-01 Percent Solids FC-1 14.3 % SM2640B-2011 03/10/2022 MD 220310-23-02 Fecal Coliforms FC-2 20548 MPN/g SM92210E-2006 03/10/2022 MD 220310-23-02 Percent Solids FC-2 14.6 % sWMM-2011 03/10/2022 MD 220310-23-03 Fecal Coliforms FC-3 89696 MPN/g SM92210E-2006 03/10/2022 MD 220310-23-03 Percent Solids FC-3 14.5 % SM2540a-2011 03/10/2022 MD 220310-23-04 Fecal Coliforms FC-4 21277 MPN/g SM92210E-2006 03/10/2022 MD 220310-23-04 Percent Solids FC-4 14.1 % SM25409-2011 03/10/2022 MD 220310-23-05 Fecal Coliforms FC-5 20833 MPN/g SM92210E-2006 03/10/2022 MD 220310-23-05 Percent Solids FC-5 14A % SM254OB-2011 03/10/2022 MD 220310-23-06 Fecal Coliforms FC-6 20979 MPN/g SM92210E-2006 03/10/2022 MD 220310-23-06 Percent Solids FC-6 14.3 % SM2540a-2011 03/10/2022 MD 220310-23-07 Fecal Coliforms FC-7 111888 MPN/g SM92210E-2006 03/10/2022 MD 220310-23-07 Percent Solids FC-7 14.3 % SM26406-2011 03/10/2022 MD Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 4 PARPROMPT-AGCURATE:RELIABLE LABORATORIES,INC WWW.PARLABS.COM REPORT OF ANALYSES Attn:ZACH KEY U.S.BIOSOLIDS,INC.PROJECT NAME:AUG 22 PO BOX 146 DATE:09/29/22 RONDA,NC 28670‑ SAMPLE NUMBER-145109 SAMPLE ID-FOREST CITY WWTP SAMPLE MATRIX-WW DATE SAMPLED-08/16/22 TIME SAMPLED-1115 DATE RECEIVED-08/16/22 SAMPLER-ZK RECEIVED BY-DJ TIME RECEIVED-1410 DELIVERED BY-ZK TYPE SAMPLE-Grab Page 1 of 1 ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS 30 DAY BENCH SCALE TEST VAR 08/16/22 1600 RE 9.28 % LABORATORY DIRECTOR te ae 2217 Graham Park Drive ¢Charlotte,NC 28273 Phone:(704)588-8333 ¢Fax:(704)588-8335 PROMPT ACCURATE:RELIABLE LABORATORIES,INC WWW.PARLABS.COM 0.0149011|0.0135152 x Mass Fraction of Fixed Solids in Liquid Sludge |0.0039022|0.0051871 CLIENT NAME: SAMPLE ID: SAMPLE #:|145109, START DATE: END DATE: Start:End: IFSVR(MassBalance)CC‐i‘iRSSCdT9.31% IFSVR(VanKleeck)Ci‘8.28 %_ IFSVR (Mass Balance)<15%||YESS SVR (Van Kleeck)<15%|Yes | P.O.Box 411483 @Charlotte,NC 28241-1483 Phone:(704)588-8333 @Fax:(704)588-8335 (ere:2>CERT #20;SCCERT #99003 PROMPT ACCURATE RELIABLE LABORATORIES,INC WWW.PARLABS.COM 30 Day Bench Scale Extended Aeration Test VAR Option 3,Percent Volatile Solids Reduction CLIENT NAME: SAMPLE ID: SURE tsstoo START DATE: END DATE: As Received Day 0 Day 7 Day 14 Day 21 Day 28 Collected 08/16/22 08/18/22 08/25/22 09/01/22 09/08/22 09/15/22 DO.|nes |tor |att |Sts |50” Crucible |xs |eS]xe S|Sts |xa]ts Tare Wt (g)16.2957 25.0661 17.1077 22.6925 17.1730 23.1855 Tare Wt (g)39.3214 35.5217 37.2411 42.5536 29.1438 40.5363 (g)23.0257 10.4556 20.1334 19.8611 11.9708 17.3508 Oven Temp °C 16 |tos,S|Sts S|Sts Date/Time In [08/16/22 16:00 |08/18/22 09:10 |08/25/22 08:45 }09/01/22 09:50 |09/08/22 10:30 |09/15/22 09:20 Date/Time Out [08/17/22 15:55 |08/19/22 09:30 |08/26/22 09:10 |09/02/22 10:15 }09/09/22 11:00 }09/16/22 09:30 Dried Sample Wt +Tare Wt (g)16.8008 25.2627 17.4842 23.0560 17.3957 23.5100 Dried Sludge Wt (g)0.5051 0.1966 0.3765 0.3635 0.2227 0.3245 Fixed Solids Wt (g j 0.0408 0.0876 0.0930 0.0597 0.0900 Furnace Temp °C Date/Time In Date/Time Out ee 8/19/22 08:50 |08/26/22 15:40 |09/02/22 15:10 {09/09/22 15:05 |09/16/22 16:10 8,:: 15: /19/22 10:00 |08/26/22 16:45 {09/02/22 16:15 {09/09/22 16:20 {09/16/22 17:15 25.1069 17.1953 22.7855 17.2327 23.2755 1.8 1.8 |0.1558 0.2889 0.2705 0.1630 0.2345 1.88%1.83%1.87% 79.25%76.73%74.42%73.19%72.27% Y+Mass Fraction of Volatile Solids in Liquid (Feed)Yb Mass Fraction of Volatile Solids in Liquid (Bottom) Sludge atStart ofTest 0.0149011 Sludge atEnd ofTest!0.0135152 X¢Mass Fraction of Fixed Solids in Liquid (Feed)Sludge Xb Mass Fraction of Fixed Solids in Liquid (Bottom) atStart ofTest 0.0039022 Sludge atEnd ofTest}0.0051871 TS 0.1966 0.1558 Volatile Fraction In:0.42154 0.38647 P.O.Box 411483 @Charlotte,NC 28241-1483 Phone:(704)588-8333 @Fax:(704)588-8335 NC CERT #20;SC CERT #99003 Burned Sample Wt +Tare Wt (g) Volatile Solids Wt (g) TS% VS% |CHAIN OF CUSTODY )Phone (704)588-8333 Fax (704)588-8335PROMPTACCURATE>-RELIABLE LABORATORIES,INC Shipping &Mailing: 2217 Graham Park Drive Charlotte,NC28273 It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories,Inc.and the North Carolina Department of Environmental and Natural Resources. GB:nlids Line, Address |958 Moors Rol City,State &zip code boactn River c 2LLL4 Point of ConfAct &Telephone Number Zach [Ke S36-YS1-W550 Sample ‐ Taken By:SIGNATURE PRINTED NAME Caek Ke. ARE SAMPLES FOR STATE or EPA REPORTING?YES ~~NO *Sample Type:Dw ww GwMw HW Soil Other Sample Temp at time of sampling:°C Sample Temp upon receipt:°C **Field Preserved:Yes ___No __Teflon Liner/Zero Headspace:Yes ___No __nla Residual Chlorine checked at time of sampling (Y/N):Dechlorination Necessary (Y/N): Relinquished by:Date/Time Received |Date/Time iG f-6 2214:10 AM tiftee 0810-220 Relinquished by:Date/Time Received by:Date/Time *C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste LOWELL NC0025861 Waypoint ANALYTICAL 46381 US Biosol& Inc Project Lowell Dennis Key 95B Roots Road Information Roaring River. NC 28669 Report Number . 22-118-0003 Lab No: 57691 Sample ID Lowell Test 7621 Whitepme Road, Richmond, VA 23237 Main 804-743-9401 " Fax 804-271-6446 www.waypointanalytical.com RfPORTOF ANAL YSIS Results Units MOL Report Date. 05/06/2022 gg Received : 04/28/2022 la./.r or &e'wV Paunc Mc Groary Ph.D., CPA Agronomist MatrixSolids Sampled 4/261202211:15 DF Date/Time By Anmlytical Analyzed Method Moslure 98.4 % 0 010 1 05/02/22 16 15 FMM SM-254OG Ailfur 10400 mg/Kg - dry 625 1 05/03/22 20' 11 EAL 6010D Calcium 14200 mg/Kg - dry 3130 1 05/03/22 20.17 EAL 6010D Aluminum 8000 mq/K9 - dry 313 1 05/04/22 11:14 EAL 6010D Manganese 1000 mg/Kg - dry 31.3 1 05/03/22 20' 17 EAL 6010D Organic N 105400 mg/Kg - dry IS630 / 05/05/22 13:00 CALCULATION Nickel <15.6 mg/Kg - dry 15 6 1 05/03/22 20.17 EAL 6010D Lead 19.3 mg/Kg -dry 18,8 1 05/03/22 20:17 EAL 6010D Arsenic <31.1 mg/Kg - dry 31 3 1 05/03/22 20.17 EAL 6010D Selenium <31.3 mg/Kg - dry 31.3 1 05/03/22 20' 17 EAL 6010D Test Results Units MOL DF Date ITime By Analytical Analyzed Method Total Solids 1.57 % 0.010 1 05/02/22 16.15 FMM SM-25406 Phosphorus 29800 mg/Kg - dry 313 1 05/03/22 20.17 EAL 6010D Copper 306 mg/Kg - dry 31.3 1 05/03/22 20:17 EAL 60I0D Total Kjeldahl Nitrogen Qualifiers/ OF Definitions Dilution Factor 114000 mg/Kg - dry 15600 1 05/05/22 13:00 IP3 {tit-4500-NN3C-TKf MQL Method Quantitation Umrl Page 3 of 7 Waypoint ANALYTICAL 46381 US &osdids Inc Protect Lowell Dennis Key 958 Hoots Road tnformahon Roaring River, NC 28669 Report Number 22-118-0003 Lab No 57691 Sample ID . Lowell 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 " Fax 804.271.6446 www.waypoititanaiyrical.com REPOR T OF ANAL Y575 Report Date 05/06/2022 Received : 04/28/2022 TAW. t &".j✓ Paunc Mc Groary Ph.D., CPA Agronomist Matrix: Solids Sampled: 4 / 26 / 202 2 11:15 Potassium 7500 mg/Kg - dry 625 1 05/05/22 22 20 EAL 6010D Magnesium 4060 mg/Kg - dry 313 I 05/03/22 2D 17 EAL 6010D Sodium 5010 mg/Kg - dry 1560 1 05/03/22 20:17 EAL 6010D Iron 42400 mg/Kg - dry 625 t 05/03/22 20:17 EAL 6010D Zinc 1460 mq/Kg - dry 78 1 1 05/03/22 20:17 EAL 6010D Ammonia Nitrogen 8310 mq/Kg - dry 6250 1 05/05/22 13 00 JPJ SM-4500-NH3C Nitrate+Nitrite-N <287 mg/Kg - dry 287 1 05/02/22 14.42 ZBD 4SOONO3F-2011 Cadmium <6.25 mg/Kg - dry 6.25 1 05/03/22 20. 17 EAL 6010D Chromium 18.9 mg/Kg - dry 15 6 1 05/03/22 20:17 EAL 6010D Mercury <8.94 mg/Kg - dry 8.94 1 05/03/22 11:39 JTR SW-74716 PH 6.7 S.u. 1 OS/05/2214:58 DRS 9045D Molybdenum <I S.6 nri - dry 15.6 l OS/03/22 20.17 EAL 6010D Qualifiers/ DF Dilution Factor Definitions MQL Method Quanhtation Limit Page 4 of 7 SAR Sodium Absorption Ratio Na Sodium (Mg/L) Equivalent weight 23 78 657 222 94 63 742 Ca. Calcium (Mg/L) Equivalent weight 20 Mg Magnesium (Mg/L) Equivalent weight 12 Na (ME) Ca_(ME) Mg -(ME] 3 41987 11 147 5 311833 Milli Equivalent = Mg/L / Equivalent weight The amour amount of SAR= Na Milli Equwalent/10 5 X (Ca Milli Equivalent + Mg Milli eguivalenq]0 5 power Permitting I SAR = 1 192134'(From Mg/L entered above) SAR= 1 192137'(From ME entered below) Na(ME l Ca((ME) ` Mg (MEN 342 1115 I 531 Pace Analpmal Services, LLC r 9800 KP,,ey Ave Satle 1 m aceAnalytical N.mlom,We NC 28576 rw.aaWa►ttas )7040675-9062 ANALYTICAL RESULTS Pro act V12395 DRY BEDS Pace P,olect No. 92546522 Sample V12395 DRY BEDS Lab ID: 92546522001 Collected 06 24,21 10 36 Received 06 25i21 10 10 Matrix Solid Results reported on a 'dry weight' basis and are adjusted for percent moisture, sample site and any dilutions. Pa'ameers Results Units Report L mr, OF P,epa'ed Analyzed CAS No Qual Chlorinated Herb. (GC) 8151A Analytical Method EPA 8151 A Preparaucr Methoo 8151A Leachate Meth060ale 1311 06 30121 1' 07 Initial pH 5 36 Final pH 5 01 Pace National - Mi. Juliet 2 4.5-TP (Silvex) NO mg.L 0.00200 1 07106l21 19 33 07i07'21 15 15 93-72-1 2,4-0 ND mg'L 000200 1 07106,121 19 33 07i0T21 15 15 94-757 Surrogates 2.4-DCAA (S) 682 - 14 0.158 1 07r06!21 19 33 07:07:21 ' S 15 19719-28-9 8081 TCLP Pesticides RVE Analytical Method EPA 8081E Preparation Method EPA 3510C Leachate Method,Date EPA 1311 06:30.21 14 26 Initial pH 4 13 Fn1ai pHS Pace Analytical Services - Charlotte gamma-BHC iLrldane) NO ug l- 0 50 1 07.02.21 1637 07:06:21 1354 58-89-9 Chlordane ;Technical) NO ug:[- 30 i 0710221 16 37 O7,06121 1354 57-74-9 Erdnn NO ug: L 0 50 1 07 02:21 1637 07,06t21 1354 72-20-8 hepladnldr NO ug L 0 50 1 07;02'21 ' 6 37 0706l21 1354 76-44-8 Heptachlor epoxide ND uy�L 0 50 1 07102'21 16 37 07,06/21 1354 1024.57-3 Methoxychlor NO ug.L 1000 1 07102.'211637 0T06i211354 7243.5 Toxapnene NO uy:L 3 0 1 07:02!2' 1637 0710&2I 1354 8001.35-2 Surrogates Decachlorobipherevi tS i 105 1C-154 1 07102'2' 1637 0706121'354 2051.24-3 Tetrachloro--n-xylene (S) 100 -, 1 ;184 1 07,02'21 '6 37 07:05121 1354 877-09-8 8082 GCS PCB Analytical Method EPA 8082A Preparation. Method EPA 3546 Pace Analytical Services - Charlotte. PCB-1016(Aroclor 1016) NO ug-Kg 129 1 0630121 1242 07r01:21 13 12 12674.11.2 PCB-1221 ;Aroclor 1221) ND ug'kg 129 1 06/30/21 12.42 0710lf2l 13 12 11104-28-2 PCB-12321Aroclor 1232) NO ugrxg 129 1 06130!211242 07:01211312 11141-16.5 PCB-'2421Areclor 1242) NO uyrtig 129 1 06.30!211242 07:01211312 53469-21-9 PCB-1248:Aroclor 1248) NO ug kg 129 1 Ob30'21 '2 42 07,0121 '3 12 12672-29-6 PCB-1254 tAro for 1254) NO ug xg 129 1 063021 12 42 07 01,21 13 12 11097.69-1 PCB-1260 (Aroclor 1260) ND ug ky 129 1 06'30.21 12 42 01,01/21 13 12 11096-82-5 Surrogates Decachio'obtphenyl (S) 64 : 10-160 1 06 302, 1242 07:01;21 13 12 2051.24-3 6010 MET ICP, TCLP Analytical Method EPA 6010D Preparation Method EPA 3C10A Leachate MetMod;Date: EPA 1311. 06'2921 15 46 Initial pH 6 25 Final off 2 Pace Analytical Services - ASrevtlle. Arsenir, NO mg t :150 i 0701:2' C947 07;02'211217 7440-38-2 6am-rn NO m9L 025 0701:210947 07,02,211217 7440-39-3 Cadmit.m NO my L 00950 07 01 2' L9 47 0?,02'21 12 17 744043-9 Chromium NO rig L G C50 07,01:2' 0947 07i02.21 12 17 7440-47.3 Lead NO mg L 0 J25 i 07,0112' C947 0 iD2121 12 17 7439-92-1 Selenron' NO mg 010 1 07011210947 0702211217 778249-2 Silver NO my L (' 025 1 OT012' C9 47 07i02121 12 17 7440-22-4 REPORT OF LABORATORY ANALYSIS ' N. snar nni re rear u: n-eC e.Ceol r r,: Data 07;12:2021 04.48 PM 11, Serv.Ces , r i, Page 5 n' i5 Pace Analytical Services, LLC 4 9800 Klncey Ave Smte 1u0 ceAnaoical Humes<v,lle NC 2111 ew.�acatabarna tJ0418JS-£✓J92 ANALYTICAL RESULTS Project V12395 DRY BEDS Pace Project No. 92546522 Sample: V12395 DRY BEDS Lab ID: 92546522001 Collected 0624i211036 Received 0&25,21101D Mainx Solid Results reported on a 'dry weight' basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results units Report L inn OF Prepared Analyzed CAS No Qual 7470 Mercury, TCLP Mercury 8270E TCLP RVE 1 4-Dichlomoenzene 2.4-Dlntrutoluene Hexachloro-1 3-buladlene Mexachlorobenzene Hexachloroelhane 2-Methylpneno4 o-Cresol) 3&4-Methylphenol(m&p Cresol; Nitrobenzene Penachlorophenol Pyridine 2 4,5-Tnchioropnenol 2 4.6-Trlchlorophenol Surrogates N Itrobenzere-d5 IS t 2-Fluorcopneny,(S) Terphenyl-o 14 1S) Phenol-d6 IS I 2-FlUorophenol(S) 2.4.6-Tnoromophenoi (S) 826DD MSV TCLP Benzene 2-Butanone (MEK Cartel tetrachloride Cniorobenzene Cnjoro`orm 1,»-Dlchlorebencene 1 2-Ddhioroethane 1 1-D611loroethane Tetrachloroetnene Tnchloroelhene Vinyl chloride Surrogates ' 2-Deriloroethane-d4 (S) Toluene-d8 (S) 4-Bromotluorobenzene ;S) Analytical Methoe EPA 747JA Preparation Method EPA 7470A Leachate Rletnod,Dzte EPA 1311, 06.29, 21 15 46 Initial pH 6 25 Final off 2 Pace Ar iyacel Services-Ashe<dle NO mg L 000020 1 0710121 11 00 07/,01121 14 42 7439-97-6 Analyucalbtethod EPA8270E Preparation Method EPA3610C Leachate MethodiDate EPA 1311, 06i30i21 14 26 Initial pH 4 13 Final off 5 Pace Analytical Services - Charlotte NO ug'L 500 1 07'01;211347 01,01,211943 106-46-7 ND w'L 50.0 1 07.01211347 0701.2l'943 121-14-2 NO ug L 500 1 07'0',21 1347 Vi01.21 1943 87-68-3 NO uq'L 500 1 07'01.211347 07101;211943 118-74.1 NO ug;L 500 1 07,0'-211347 0701,21'943 67-72-1 NO unL 50o 107-01:21 1347 07!01:21'943 9548.7 NO ug.L 500 i 071012' 1347 07101i2l'943 15831.10-4 NO ugL 500 07'011;2' 1347 07,01,21'943 98-95.3 ND ug L 100 07,01:21 1347 07i0121 1943 87-86.5 NO r.3:t 50o 07:01:211347 07t01,2l 1943 110-86.1 NO ug L 50 0 07'01!21 13 47 07i01,21 19 43 95-954 ND ug'L 50.0 07i0 1r2' 1347 07101,211943 88-06-2 61 10-144 07'011:211347 07,01.211943 4165-60-0 48 10-1-J0 0701,21 13 47 0 7,01121 1943 321.60-8 ill -0 34.163 1 07'01,211347 07;01,211943 1718-51-0 34 .n 10.130 Uioli2l 1347 01;01, 211943 13127.B8-3 41 10-130 07011211347 07/01,211943 367-124 61 10-144 i 07101,211347 0701,211943 118-79-6 Analytical Method EPA 82600 Leachate hletnod.Date EPA 1311, 07 07,21 15 33 Pace Analytical Services - Charlotte NO ug'L la) 20 07i013,211515 71-43-2 NO ug L 200 20 0-081121 15 15 78-93-3 NO ug L 10h1 20 07108i21 15 15 56-23-5 NO ug L 100 20 07i08,221 15 15 108-90-7 NO ug'L 1C0 20 07:08121 15 15 67-66-3 NO ug L 100 20 07108/21 15 15 106-46.7 NO ug'L IGO 20 0'!08i2115'15 107-06.2 NO ug L 100 20 01r08,21 ' 5 15 75-354 NO up 1. 1C0 20 07;0821'515 127-184 NO ug L 100 20 0'i0&21 '5 15 79-01-6 NO ug L 1&0 20 07i08,121 15 15 75.01-4 99 70-13D 20 108 0 67-135 20 97 ,• 70-130 20 REPORT OF LABORATORY ANALYSIS 371081 15 ' 5 17060-07-0 07,08,211515 2037-2b-5 0';0&211515 460-00.4 t111'HVun SN111 "Or bH'HCf:rvi.l•'H•) a%Cent tr' fLi Date 07,1212021 04 48 PM Page 6 of 35 PaceAnalytical x ww.IKMaN.saa ANALYTICAL RESULTS Pace Analytical Services. LLC 9800 Kmce, Ave Sude'OU L.gter5e�lle NC 2&175 1704i875.9.;5_ Prceca V12395 DRY BEDS Pace Project No 92546522 Sample V12395 DRY BEDS Lab ID: 92546522001 Collected 062421 10 36 Received 06.25r21 10 10 Matrix Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Pa,ameters Results Units Report L milt DF Prepared Analyzed CAS No. Qual 2540G Total Percent Solids Analytical Method Silt 254OG-2011 Pace Analytical Services - Charlotte Total Solids 25.7 r. '0 i 06:25;21 '8 07 Percent Moisture Analytical Method SVV-846 Pace Analytical Services - Charlotte Percent Moisture 74.3 1, 0 10 i 06;2521 18 01 N2 1010 Flashpoin4Ciosed Cup Analytical Method EPA 1010E Pace Analytical Services -Asheville Flashpomt >200 deg F 1 07.09/21 11 55 9045 PH Sal Analytical Method FPA 9045D Pace Analytical Sery ces - Ashevdle cH at 25 Degrees C 5.6 Sto Unds 0 1C 1 01,12.21 -4 57 H3 9095 Paint Filter Ligatl Test Analytical Method EPA 9095E Pare Analytical Sery ces -Asheville Free L.guus Pass 10 07:06,21 14 47 ASTM D4239-05 Sulfur Analytical Method ASTM D4239-05 Pace Analytical Sery ces - Ashea Ile Sulf" 0.150 1 iWw 0020 1 071U2.21^984 N2 733C S Reactive Cyanide Analytical Method EPA 9014 Preparation Method SW-846 7 3 3 2 Pace Analytical Services - Greensburg Cyanide Rear:.ve ND eig kg 39 1 07101'2' 17 46 07102�21 'b 31 734S Reactive Sulfide Analytical Metrad SM 4500-32-F-2W 1 Preparation Method SW-846 7 3 4 2 Pace Aialytical Services - Greensburg Sulfide Reactive ND mg .g 391 07Vi211746 07,01:211-48 REPORT OF LABORATORY ANALYSIS 'nis reaon snail not x rsoror; n:er. x.�ept m fu, Dale 07122021 04.46 PM -i wul 11 e -nitro wisele N Pace Analp cal Services L.0 Page 7 of 35 II I 1 1111 1, 11.;I V12395 DRY BEDS SAMPLE RESULTS 01 o l:eceeC caee 2 06 ,c 21 16 3n 1'3M52 N.•,.df Ou•6he' P•a sx,I Analyze — .. ' .. `.1 Ni .. a p—,tl; O"'ll fc P[]t "I' Pd,Aron An,Iv,l Aa4t Analvir .. . .. III Page 31 of 3.5 ACCOUNT PROJtti SDG- UA't'iiME PAGE U.S. Biosolids Inc 958 Hoots Road Roaring River, NC 28669 Receive Date Reported: For: Comments: Analytical Results 09/22/2022 10/31 /2022 Lowell Sample Number Parameter Sample ID 220922-27-01 30 Day Benchscale Lowell Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 4 STATESVILLE 1 4 ANALYTICAL Result Unit Method Analyzed Analyst 2.41 % EPA626R-9210 09/22/2022 MD PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 5 30 Day Bench Worksheet Sample ID # 220922-27-01 WEEK 1 Samples Total Solids Volatile Solids % Volatile Fraction I 1 0.75 0.39 2 0.74 0.38 3 0.77 0.40 Average: 0.75 0.39 0.5200 1 WEEK 2 Samples Total Solids Volatile Solids % Volatile Fraction 1 0.75 0.39 2 0.79 0.41 3 0.78 0.41 1 Average: 0.77 0.40 0.5195 WEEK 3 Samples Total Solids Volatile Solids % Volatile Fraction 1 0.76 0.40 1 2 0.76 0.40 1 3 0.76 0.40 Average: 0.76 0.40 0.5263 WEEK 4 Samples Total Solids Volatile Solids % Volatile Fraction 1 1 0.76 0.41 2 0.75 0.40 1 3 0.74 0.39 1 Average: 0.75 0.40 _ 0.5333 WEEK 5 Samples Total Solids Volatile Solids % Volatile Fraction 1 1 0.74 I 2 0.74 139 0.38 3 0.74 0.37 Average: 0.74 0.38 0.5135 WEEK 6 Samples Total Solids Volatile Solids % Volatile Fraction 1 0.72 0.37 2 0.72 0.37 3 0.72 0.37 1 Average: 0.72 0.37 0.5139 1 Van Kleeck Reduction: 0.5200-0.5139 X 100- 2.41 % 0.5200 - ( 0.5200 X 0.5139) Final Result: 2.41 % PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 5 Analytical Results STATESVILLE ANALYTICAL v U.S. Biosolids Inc 958 Hoots Road Roaring River, NC 28669 Receive Date: 03/03/2022 Reported: 03/07/2022 For: LOWELL Comments: Geometric Mean: 17,725 MPN/g (most probable number) Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 220303-37-01 Fecal Colifonns L1 17241 MPN/g SM92210E2006 03/03/2022 MD 220303-37-01 Percent Solids L1 1.74 % SM2640e-2011 03/03/2022 MD 220303-37-02 Fecal Colifonns L2 17143 MPN/g SM92210E-2W6 03/03/2022 MD 220303-37-02 Percent Solids L2 1.75 % SM WS-2011 03/03/2022 MD 220303-37-03 Fecal Colifonns L3 16949 MPN/g SM92210E-2W6 03/03/2022 MD 220303-37-03 Percent Solids L3 1.77 % SM2540a-2011 03/03/2022 MD 220303-37-04 Fecal Colifonms L4 27933 MPN/g SM92210E-2W6 03/03/2022 MD 220303-37-04 Percent Solids L4 1.79 % SM25409-2011 03/03/2022 MD 220303-37-05 Fecal Colifonms L5 13143 MPN/g SM92210E-2006 03/03/2022 MD 220303-37-05 Percent Solids L5 1.75 % SM25 00-2011 03/03/2022 MD 220303-37-06 Fecal Colifonns L6 7386 MPN/g SM92210E-2006 03/03/2022 MD 220303-37-06 Percent Solids L6 1.76 % SM26WS-2011 03f03/2022 MD 220303-37-07 Fecal Colifonms L7 40462 MPN/g SMWME-2006 03/03/2022 MD 220303-37-07 Percent Solids L7 1.73 % SM25405-2011 03103/2022 MD Respectfully submitted, Melissa Myers NC Cart #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 4 BELMONT NC0021181 0waypoint 7621 Road, Richmond, 27 -6446 Main 804-743-9401°Fax 804-271-6446 ain 904-7 ANALYTICAL www.waypointanalytical.com 46381 US Biosolids Inc Project Belmont Dennis Key Report Date : 03/24/2022 958 Hoots Road Information . Received : 03/15/2022 Roaring River , NC 28669 Vl/ Grow/ Pauric Mc Groary Ph.D., CPA Report Number : 22-074-0005 REPORT OFANAL YSIS Agronomist Lab No : 57148 Matrix: Solids Sample ID : Belmont Sampled: 3/14/2022 11:30 Test Results Units MOL DF Date / Time By Analytical Analyzed Method Moisture 96.6 % 0.010 1 03/16/2216:04 FMM SM-254OG Sulfur 9470 mg/Kg - dry 294 1 03/22/22 23:49 JTR 60100 Calcium 16000 mg/Kg - dry 1470 1 03/22/22 23:49 JTR 6010D Aluminum 51200 mg/Kg - dry 147 1 03/22/22 23:49 ITR 6010D Manganese 1160 mg/Kg - dry 14.7 1 03/22/22 23:49 JTR 6010D Organic N 32060 mg/Kg - dry 7353 1 03/21/22 11:30 CALCULATION Nickel 21.7 mg/Kg - dry 7.35 1 03/22/22 23:49 JTR 60100 Lead 22.3 mg/Kg - dry 8.82 1 03/22/22 23:49 JTR 6010D Arsenic <14.7 mg/Kg - dry 14.7 1 03/22/22 23:49 JTR 6010D Selenium <14.7 mg/Kg - dry 14.7 1 03/22/22 23:49 JTR 6010D Test Results Units MOL DF Date / Time By Analytical Analyzed Method Total Solids 3.39 % 0.010 1 03/16/22 16:04 FMM SM-254OG Phosphorus 27400 mg/Kg - dry 147 1 03/22/22 23:49 JTR 6010D Copper 335 mg/Kg - dry 14.7 1 03/22/22 23:49 JTR 6010D Total Kjeldahl Nitrogen 32100 mg/Kg - dry 7350 1 03/2J/22 11:30 JPJ ,M-4500-NH3C-TKt Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Waypoint. ANALYTICAL 46381 US Biosolids Inc Project Belmont Dennis Key 958 Hoots Road Information Roaring River , NC 28669 Report Number:22-074-0005 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-94010Fax 804-271-6446 www.waypointanalytical.com REPORT OF ANAL YSIS Report Date: 03/24/2022 Received : 03/15/2022 T�,C PC &rear Paunc Mc Groary Ph.D., CPA Agronomist Lab No : 57148 Matrix: Solids Sample ID : Belmont Sampled: 3/14/2022 11:30 Potassium 3240 mg/Kg - dry 294 1 03/22/22 23:49 JTR 6010D Magnesium 3470 mg/Kg - dry 147 1 03/22/22 23:49 JTR 6010D Sodium 7820 mg/Kg - dry 735 1 03/23/22 23:24 JTR 6010D Iron 28300 mg/Kg - dry 294 1 03/22/22 23:49 JTR 6010D Zinc 1960 mg/Kg - dry 36.8 t 03/22/22 23:49 JTR 6010D Ammonia Nitrogen <2940 mg/Kg - dry 2940 1 03/22/22 09:30 JPJ SM-4500-NH3C Nitrate+Nitrate-N 721 mg/Kg - dry 147 1 03/22/22 14:30 ZBD 4500NO3F-2011 Cadmium <2.94 mg/Kg - dry 2.94 1 03/22/22 23:49 JTR 6010D Chromium 65.3 mg/Kg - dry 7.35 1 03/22/22 23:49 JTR 601OD Mercury 1.08 mg/Kg - dry 0.465 1 03/21/22 14:48 ZMT SW-7471B pH 5.9 S.U. 1 03/22/2215:55 DRS 9045D Molybdenum <7.35 mg/Kg - dry 735 1 03/22/22 23:49 JTR 6010D Qualifiers/ DF Dilution Factor MQL Method Quantrtation Limit Definitions mo Co O O N 0 O m a O c O c O 00 N m Z m Z N X y Y E — 0 C ry ry X N O O M O _ O X X X � M Y O 0)O Q Q E Z E O Z m + O y = Z Z m c n i F .2 + Z 0 m M = M S m_o� Z Z y O Y u e O F- Y F- '00 (0) K t6 N ZO — Z ` _ Z ` Q Q M— C O_ m �y d ` O O ZI^ Z"" Q Z"" Q U U 0 U «� v °a o °a =°mat m Usc w _a a N N ZIN � O # ?t � U 000 U d RQa, = Y C cm" am n. E o. E 10 m C V) m 0 O M p M O Z O Z a O v N Q N Q a N d 1 r c d 9 D m o o o Z r F m m T U SAR Sodium Absorption Ratio Na Sodium (Mg/L) Equivalent weight 23 Ca Calcium (Mg/L) Equivalent weight: 20 Mg : Magnesium (Mg/L) Equivalent weight: 12 Milli Equivalent = Mg/L / Equivalent weight Na(Mg/L) Ca(Mq/L) Mq(Mq/L) 26509 1 5424 1 11763 Na-JME) I Ca -(ME) I M-q i 11.525651 2712 1 9.8025 SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0 5 power I SAR = 2 682471 '(From Mg/L entered above) I SAR= 2.677316 (From ME entered below) Na ME Ca (ME) Mg (ME) 115 1 271 1 98 The amour amount of i Permitting! Analytical Results U.S. Biosolids Inc 958 Hoots Road Roaring River, NC 28669 Receive Date: 03/10/2022 Reported: 04/19/2022 For: Comments: Sample Number Parameter Sample ID Result 220310-21-01 30 Day Benchscale Belmont 4.6 220310-21-01 TCLP Belmont See Attached Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 Unit Method EPA625-R-92I0 as Noted Analyzed Analyst 03/10/2022 MD 03/11/2022 PACE PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 37 ai'--iAL Y s 1;,.::1,P. Analytical Results US Biosolids 958 Hoots Rd Roaring River, NC 28669 Entered: 3/10/22 Reported: 4/19/22 Sample ID: 220310-21-01 PARAMETER: Vector Attraction Reduction/Aerobically Dieested Sludee (30davi Total Solids Volatile Solids % Volatile Solids Week 1 1.67 0.91 0.5449 Week 2 1.61 0.87 0.5404 Week 3 1.60 0.86 0.5375 Week 4 1.58 0.86 0.5443 Week 5 1.53 0.81 0.5294 Week 6 1.52 0.81 0.5329 Volatile Solids Reduction: 0.5449 - 0.5329 X 100 = 4.6 % 0.5499 - (0.5449 X 0.5329) Respectfully submitted, Melissa Myers Statesville Analytical, Inc. NC W W Cert.4 440NC 30 Day Bench Worksheet Sample ID # 220310-21-01 WEEK I Samples 1 2 3 Average: WEEK 2 Samples 1 2 3 Average: WEEK 3 Samples 1 2 3 Average: WEEK 4 Samples I 2 3 Average: WEEK 5 Samples I 2 3 Average: WEEK 6 Samples I 2 I_Averagv: Total Solids 1.66 1.66 1.67 1.67 Total Solids 1.61 1.61 1.61 1.61 Total Solids 1.59 1.61 1.61 1.60 Total Solids 1.59 1.58 1.56 1.58 Volatile Solids 0.91 0.90 0.92 0.91 Volatile Solids 0.87 0.87 0.87 0.87 Volatile Solids 0.86 0.85 0.88 0.86 Volatile Solids 0.86 0.85 0.86 0.86 % Volatile Fraction 0.5449 % Volatile Fraction I 0.5404 % Volatile Fraction 0.5375 % Volatile Fraction 0.5443 Total Solids Volatile Solids I % Volatile Fraction 1.54 0.81 1.52 0.81 1.53 0.81 1.53 0.81 0.5294 Total Solids Volatile Solids % Volatile Fraction 1.52 0.81 1.53 0.81 1.51 0.81 1.52 0.81 0.5329 _ Van Kleeck Reduction: 0.5449 - 0.5329 X 100 - 4.6 0% 0.5449 - ( 0.5449 X 0.5329) Final Result: 4.6% PaceAnalXical wwr.Oasel dt.l. ANALYTICAL RESULTS Project BELMONT FULL TCLP Pace Project No 92593154 Sample: 220310-21-01 Lab IO: 92593154001 Collected 03/10/22 10 30 Received 03111/22 10 27 Results reported on a 'dry weight" basis and are adjusted for percent moisture, sample size and any dilutions Parameters Results Units Report Limit OF Prepared Analyzed Pace Analytical Services, LLC 9800 Kral Ave Suite 100 Huntersmlie, NC 28078 (704)875-9092 Matrix Solid CAS No Oust 8081 TCLP Pesticides RVE Analytical Method EPA 8081B Preparation Method EPA 3510C Leachate Method/Date EPA 1311 03/15122 15 08 initial pH 5 28. Final pH 5 Pace Analytical Services - Charlotte gamma-BHC (Lindane) ND ug/L 050 1 03/1622 17 21 03/17/22 12 04 58-89-9 Chlordane(Technical) NO ug/L 30 1 031l6/22 1721 03/17/22 1204 57-74-9 Endrin NO uglL 050 1 03/16/22 17 21 (17122 1204 72-20-8 Heptachor NO u9IL 050 1 03)16/221721 03117/221204 76-44-8 Heptachlor epoxide NO u91L 050 1 03116122 17 21 031171221204 1024-57-3 Methoxychlor ND ugi 1000 1 03/161221721 03/17122 12 04 72-43-5 Toxaphene NO ug/L 30 1 031161221721 03/171221204 8001-35-2 Surrogates Decachlorobiphenyl (S) 85 % 10-154 1 03116122 1721 03117122 12 04 2051.24-3 Tetrachloro-m-xylene (S) 104 % 10-184 1 03/16122 1721 03/17/22 12 04 877-09-8 8082 TCLP PCBs RVE Analytical Method EPA 8082A Preparation Method EPA 3510C Leachate Method/Date EPA 1311, 03/15/22 15 08 Initial pH 5 28, Final pH 5 Pace Analytical services - Charlotte PCB-1016 (Aroclor 1016) NO ug/L 1000 1 03/1622 1721 03/17/22 19 52 12674-11.2 PCB-1221 (Aroclor 1221) ND uglL 1000 1 03/16122 1721 03117/22 19 52 11104-28-2 PCB-1232 (Aroclor 1232) NO ug/L 1000 1 03/16/22 1721 03/17/22 19 52 11141-16-5 PCB-1242 (Aroclor 1242) NO ug/L 1000 1 03/16/22 1721 03/17/22 19 52 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 1000 1 03/16/22 1721 03J17122 1952 12672-29-6 PCa 1254 (Aroclor 1254) NO ug/L 1000 1 03/16122 1721 03117/22 1952 11097-69.1 PCB-1260 (Aroclor 1260) NO ug.iL 1000 1 03/16122 1721 03117/22 1952 11096-82-5 Surrogates Decachlorobiphenyl (S) 80 % 10-181 1 03116/22 1721 03117/22 1952 2051-24-3 6010D ATL ICP, TCLP Analytical Method EPA 6010D Preparation Method EPA 3010A Leachate Methotl/Date EPA 1311, 03/21/22 14 20 Initial pH 7 53 Final pH 7 54 Pace Analytical Services - Peachtni. (Afters, GA Arsenic NO mglL 0 30 1 03122/22 14 34 03/23122 1233 7440-38.2 Barium NO mg1L 0 50 1 03/22/22 14 34 03/23/22 1233 7440-39-3 Cadmium NO mg1L 0 10 1 03/22122 1434 03/23/22 1233 7440.43-9 Chromium NO of 0 10 1 0322122 14 34 0312322 1233 7440-47-3 Lead ND mglL 025 1 03/22122 14 34 03/23/22 1233 7439-92-1 Selenium NO ni 040 1 03/22122 14 34 03/23/221233 7782-49-2 Silver NO mg/L 0 10 1 03/22122 1434 0323122 1233 7440-22-4 7470 Mercury, TCLP Analytical Method EPA 7470A Preparation Method EPA 7470A Leachate Method/Date EPA 1311; 03121/22 14 20 Initial pH 7 53, Final pH 7 54 Pace Analytical Services - Peachtree Comers, GA Mercury ND mg/L 00050 1 03/22/22 15 00 03123Y22 11 00 7439-97-6 Date 03131/2022 0528 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced except m full. without the written consent of Pace Analytical Services LLC Page 5 of 33 PO Box 228 a Statesville, NC 28687 a 704/872/4697 Page 9 of 37 1 ;2ceAnalytical n aneelecMaWsam ANALYTICAL RESULTS Project BELMONT FULL TCLP Pace Project No 92593154 Sample220310-21-01 Lab ID: 92593154001 Collected 03/10122 10 30 Received 03111/22 1027 Results reported on s -dry weight- basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit OF Prepared Analyzed Pace Analytical Services, LLC 9800 Kinwy Ave Soite 1 W HuntersAle, NC 28078 (704)875-9092 Matrix Solid CAS No Coal 8270E TCLP RVE Analytical Method EPA8270E Preparation Method EPA3510C Leachate Method/Daw EPA 1311 031151221508 Imbal pH 5 28. Final pH 5 Pace Analytical Services - Charlotte 14-Dichlorobenzene NO ugll- 500 1 03/161221728 031171221303 106-46-7 2,4-Dimbotolueoe ND ug/L Soo 1 031161221728 031171221303 121-14-2 Hexachlom-1,3-buladiene NO ug1L 500 1 03116/22 17 28 03/17122 13 03 87-68-3 Hexachlorobenzene NO ugiL 500 1 03116122 17 28 031171221303 118-74-1 Hexachloroethane NO ug1L 500 1 03/16221728 03117122 13 03 67-72-1 2-Methylphenago-Cresol) NO ug/L 500 1 031161221728 031171221303 95-48-7 384-Methy1phenol(mBp Cresol) NO ugiL 500 1 031161221728 03/17122 13 03 15831-10.4 Nitrobenzene NO ugiL 500 1 031161221728 03/171221303 98-95-3 Pentachlorophenol NO ugiL 100 1 03/16122 17 28 03117122 1303 87-86-5 Pyridine NO ugiL 500 1 03/16122 17 28 03117/22 13 03 110-86-1 24,5-Trichlurophenol NO ug/L 500 1 03116221728 031171221303 95-95-4 2,46-Tri@ltoroplunol NO ugiL 500 1 031161221728 03/171221303 88-06-2 Surrogates Nitrobenzene-d5 (S) 38 36 10-144 1 03/16/22 17 28 03117122 1303 4165-60-0 2-Fluorobiphenyl(S) 39 % 10-130 1 03f16/22 1728 03117122 13 03 321-60-8 Terpher id(S) 96 34-163 1 031161221728 03117122 13 03 1718.51-0 Phenol-d6(S) 27 '16 10-130 1 031161221728 031171221303 13127-88-3 2-Fluorophenol(S) 33 °k 10-130 1 03/16/22 17 28 03/17221303 367-12.4 2 4 6-Tnbromophenol (S) 84 10-144 1 03/16122 17 28 03)17122 1303 118-79-6 8260D MSV TCLP Analytical Method EPA 8260D Leachate Method/Date. EPA 1311, 0306/22 13 08 Pace Analytical Services - Charlotte Benzene ND ug/L 100 20 031171221250 71-43-2 2-Butanooe (MEK) ND ug/L 200 20 03117/22 1250 78-93-3 Carbon tetrachloride NO ugiL 100 20 03117122 12 50 56.23-5 Chlorobenzene NO ugiL 100 20 03/17/22 12 50 108-90-7 Chloroform NO ug/L 100 20 03117122 12 50 67-66-3 1,4-Dichlorobenzene ND ug/L 100 20 03/17/22 12 50 106�6.7 1.2-Dichloroethane NO ug/L 100 20 03/17122 1250 107-06-2 1,1-Dichloroethene NO ugiL 100 20 0311722 1250 75-35-4 Tetrachloroethene NO ugiL 100 20 03117122 1250 127-184 Tnchloroethane NO ugiL 100 20 03/17/22 1250 79.01-6 Vinyl chloride ND ug/L 100 20 03/17122 12,50 75-014 Surrogates 1,2.Dichloroethane.d4 (3) 89 % 70-130 20 03117122 1250 17060-07-0 Toluene-d8 (S) 110 % 67.135 20 03117/22 1250 2037-26-5 4-Bromofluorobenzene tS) 96 % 70-130 20 03/17122 1250 460-00-4 Percent Moisture Analytical Method SW-846 Pace Analytical Services - Charlotte Percent Moisture 97.3 % 0 10 1 03/14/22 16 25 Date 03131/2022 05'28 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. w4hom the uper consent of Pace Analytical Seances, LLC N2 Page 6 of 33 PO Box 228 at Statesville, NC 28687 e 704/872/4697 Page 10 of 37 ' Pace Analytical Services, LLC 9800KineyAve Swte1002ceAnail Huntersvile, NC 28078 ew."oftle cen (7041875-9092 ANALYTICAL RESULTS Protect BELMONT FULL TCLP Pace Project No 92593154 Sample: 22031(1-01 Lab ID: 92593154001 Collected 03/10122 10 30 Received 03111122 10 27 Matrix Solid Results reported on a 'dry welght' basis and are adjusted for percent moisture, sample size and any dilutions, Parameters Results Units Report Limit DF Prepared Analyzed CAS No Goal 1010 Flashpoint,Closed Cup Analytical Method EPA 1010B Pace Analytical Services - Asheville Flashpoint >200 deg F 700 1 03/23/22 14 00 9045 pH Soil Analytical Method EPA 9045D Pace Analytical Services - Asheville pH at 25 Degrees C 6.7 Sid Units 0 10 1 03118122 13,07 H3 9095 Paint Filter Liquid Test Analytical Method EPA 90958 Pace Analytical Services - Asheville Free Liquids FAIL 1 0 1 03118/22 15 56 Percent Moisture Analytical Method Moisture Pace Analytical Services - New Orleans Percent Moisture 99.8 % 050 1 03/24/22 12 05 733C S Reactive Cyanide Analytical Method SW-846 7 3 3 2 Preparation Method SW-846 7 3 3 2 Pace Analytical Services - New Orleans Cyanide Reactive ND mg/kg 250 1 03/25/22 07 45 03125/22 13 14 734S Reactive Sulfide Analytical Method SM 4500-S2-P-2011 Preparation Method SW-846 7 3 4 2 Pace Analytical Services - Greensburg Sulfide, Reactive ND di 367 1 03116122 20 45 03/16122 20 48 Sample: 220310.21-01 Parameters 8082 GCS PCB FIVE PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Surrogates Decachlorobiphenyl(S) Date 0313112022 05 28 PM Lab ID: 92593154002 Collected 03/10/22 10 30 Received 03/11/22 10 27 Matrix Water Results Units Report Limit DF Prepared Analyzed CAS No Qual Analytical Method EPA8082A Preparation Method EPA 3510C Pace Analytical Services - Charlotte ND ug/L 50 1 031241221706 03125122 07 43 12674-11-2 NO ug/L 5.0 1 03/24/22 1706 03125/22 07 43 11104-28-2 ND ug/L 50 1 03124/221706 03/25/22 07 43 11141-16-5 NO ug/L 50 1 03124/221706 03125122 07 43 53469-21-9 ND ug/L 50 1 03/24/22 1706 03/25/22 07 43 12672-29-6 ND ug/L 50 1 03/24122 1706 03/25/22 07 43 11097-69-1 ND ug/L 50 1 03/24/22 1706 03/25122 07 43 11096-82-5 50 % 10-181 1 03124/221706 03125/2207.43 2051-24-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in lull, w4hout the written consent of Pace Analytical Services, LLC Page 7 of 33 PO Box 228 a Statesville, NC 28687 e 704/872/4697 Page 11 of 37 Analytical Environmental Services, Inc Dale: 22-Nl.ir-22 Client: Pace Ana l)ncaI Client Sample ID: 22031021-III Prgecl New: 92 i9l ] 14 Collection Dme: 3r 10,2022 10 30 nO AM Lafi ID: 2203173-001 Matrix: 0."Ihd Reporting Dihttlnn Anal)acs Result (jual Coils Ralchl0 Date:\nahzca Mal)sl Limit Factor HERBICIDES, TCLI' SW 1311/8151A (SN'3510C) 2.4.S7 P Is 11{'ex) RRI, 021) orgl li_'N?N 1 0, IN 2412217'_h Kit _'•l-D BRI, U._U rnS'1 1:282b 1 111Ih'_IC2112h Kit Surr DCAA 501-120 RII a'N'N1 IIS IN]II]2 172.\ K1i pn.ea.r. 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R.1,.xnk l,n,�r Page 30 of 33 Page 3 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 34 of 37 Analytical Results STATESVILLE ANALYTICAL U.S. Biosolids Inc 958 Hoots Road Roaring River, NC 28669 Receive Date: 03/1012022 Reported: 03/11/2022 For: Belmont Comments: GEOMETRIC MEAN: 8,270 MPN/g Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 220310-41-01 Fecal Coliforms B-1 16026 MPN/g SM92210E-2006 03/10/2022 MD 220310-41-01 Percent Solids B-1 3.12 % SWWB-2011 03/10/2022 MD 220310-41-02 Fecal Coliforms B-2 9376 MPN/g SM92210E-2006 03/10/2022 MD 220310-41-02 Percent Solids B-2 3.20 % SM254OB-2011 03/10/2022 MD 220310-41-03 Fecal Coliforms B-3 7279 MPN/g SM92210E-2006 03/10/2022 MD 220310-41-03 Percent Solids B-3 3.16 % SM254OB-2011 03/10/2022 MD 220310-41-04 Fecal Coliforms B-4 3406 MPN/g SM92210E-2006 03/10/2022 MD 220310-41-04 Percent Solids B-4 3.23 % SM254OB-2011 03/10/2022 MD 220310-41-05 Fecal Coliforms B-5 25478 MPN/g SM92210E-2006 03/10/2022 MD 220310-41-05 Percent Solids B-5 3.14 % SM2540B.2011 03/10/2022 MD 220310-41-06 Fecal Coliforms B-6 3963 MPN/g SM92210E-2006 03/10/2022 MD 220310-41-06 Percent Solids B-6 3.28 % SM254OB-2011 03/10/2022 MD 220310-41-07 Fecal Coliforms B-7 7034 MPN/g SM92210E-2006 03/10/2022 MD 220310-41-07 Percent Solids B-7 3.27 % SM25406-2011 03/10/2022 MD Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cart #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page t of 4 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL012310 Mehlich-3 Extraction Completed: Received:Sampled: Soil Report Farm: Client: Links to Helpful Information Advisor: 11/17/202210/31/202210/26/2022 Predictive Zach Key Southern Soil Builders 958 Hoots Rd Roaring River, NC 28669 Charlie Killian 114 Kimmswick Rd Charlotte, NC 28214 Sampled County : Gaston 272310 231531Client ID: Advisor ID: Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M 1.3 0.0 MH24 120-200 000 192895.42.6678.10.990.81 162586828471 0 100 Note: 12 187 868 (tons/acre) 333 0 54 12 Nutrients (lb/acre) 0.1 0 0 Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M 1.0 0.0 MH25 120-200 000 351865.62.57610.50.920.60 1556100533290 0 70 Note: 12 216 1005 (tons/acre) 333 0 59 15 Nutrients (lb/acre) 0.1 0 0 Thank you for using agronomic services to manage nutrients and safeguard environmental quality. through a grant from the North Carolina Tobacco Trust Fund Commission. Reprogramming of the laboratory-information-management system that makes this report possible is being funded - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL012310 Page 2 of 3Charlie Killian Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M 0.0 0.0 MH21 120-200 000 211336.41.38710.01.070.36 128533952244 0 100 Note: 12 324 339 (tons/acre) 333 0 64 22 Nutrients (lb/acre) 0.1 0 0 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL012310 Page 3 of 3Charlie Killian Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or lb/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no-till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at one time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-I levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to . In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot find the exact fertilizer grade recommended on the report, visit to find information that may help you choose a comparable alternate. For more information, read . Test Results The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-AI1, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS-I, Na, ESP, SS-I, NO 3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit Report Abbreviations Ac exchangeable acidity B boron BS% % CEC occupied by basic cations Ca%% CEC occupied by calcium CEC cation exchange capacity Cu-I copper index ESP exchangeable sodium percent HM%percent humic matter K-I potassium index K2O potash Mg%% CEC occupied by magnesium MIN mineral soil class Mn manganese Mn-Al1 Mn-availability index for crop 1 Mn-AI2 Mn-availability index for crop 2 Mn-I manganese index M-O mineral-organic soil class N nitrogen Na sodium NO3-N nitrate nitrogen ORG organic soil class pH current soil pH P-I phosphorus index P2O5 phosphate S-I sulfur index SS-I soluble salt index W/V weight per volume Zn-AI zinc availability index Zn-I zinc index Understanding the Soil Report: explanation of measurements, abbreviations and units $Note: Secondary Nutrients and Micronutrients www.ncagr.gov/agronomi/obpart4.htm#fs A Homeowner's Guide to Fertilizer. www.ncagr.gov/agronomi/uyrst.htm ncagr.gov/agronomi/pubs.htm. NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL012321 Mehlich-3 Extraction Completed: Received:Sampled: Soil Report Farm: Client: Links to Helpful Information Advisor: 11/17/202210/31/202210/26/2022 Predictive Zach Key Southern Soil Builders 958 Hoots Rd Roaring River, NC 28669 Warren/Lee Walker 4493 Clingman Rd Ronda, NC 28670 Sampled County : Wilkes 444516 231531Client ID: Advisor ID: Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M 0.0 0.0 LW1 120-200 pH$00 185406.80.79615.30.990.36 139970517637 0 100 Note: 12 Note: $ 111 705 (tons/acre) 333 0 89 6 Nutrients (lb/acre) 0.1 0 0 Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M 0.0 0.0 LW2 120-200 pH$00 145867.00.59717.11.010.32 142793419139 0 110 Note: 12 Note: $ 116 934 (tons/acre) 333 0 92 5 Nutrients (lb/acre) 0.1 0 0 Thank you for using agronomic services to manage nutrients and safeguard environmental quality. through a grant from the North Carolina Tobacco Trust Fund Commission. Reprogramming of the laboratory-information-management system that makes this report possible is being funded - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL012321 Page 2 of 3Warren/Lee Walker Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M 0.0 0.0 LW3 120-200 pH$00 265316.90.69615.01.030.32 131476316035 0 90 Note: 12 Note: $ 100 763 (tons/acre) 333 0 89 5 Nutrients (lb/acre) 0.1 0 0 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL012321 Page 3 of 3Warren/Lee Walker Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or lb/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no-till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at one time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-I levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to . In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot find the exact fertilizer grade recommended on the report, visit to find information that may help you choose a comparable alternate. For more information, read . Test Results The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-AI1, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS-I, Na, ESP, SS-I, NO 3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit Report Abbreviations Ac exchangeable acidity B boron BS% % CEC occupied by basic cations Ca%% CEC occupied by calcium CEC cation exchange capacity Cu-I copper index ESP exchangeable sodium percent HM%percent humic matter K-I potassium index K2O potash Mg%% CEC occupied by magnesium MIN mineral soil class Mn manganese Mn-Al1 Mn-availability index for crop 1 Mn-AI2 Mn-availability index for crop 2 Mn-I manganese index M-O mineral-organic soil class N nitrogen Na sodium NO3-N nitrate nitrogen ORG organic soil class pH current soil pH P-I phosphorus index P2O5 phosphate S-I sulfur index SS-I soluble salt index W/V weight per volume Zn-AI zinc availability index Zn-I zinc index Understanding the Soil Report: explanation of measurements, abbreviations and units $Note: Secondary Nutrients and Micronutrients www.ncagr.gov/agronomi/obpart4.htm#fs A Homeowner's Guide to Fertilizer. www.ncagr.gov/agronomi/uyrst.htm ncagr.gov/agronomi/pubs.htm. NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL012916 Mehlich-3 Extraction Completed: Received:Sampled: Soil Report Farm: Client: Links to Helpful Information Advisor: 11/21/202211/02/202210/28/2022 Predictive Zach Key Southern Soil Builders 958 Hoots Rd Roaring River, NC 28669 Bill Hinson 537 Rocky Ford Rd Roaring River, NC 28669 Sampled County : Wilkes 478377 231531Client ID: Advisor ID: Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M 1.2 0.0 BH01 120-200 000 242895.12.0665.81.000.86 37524729468 0 90 Note: 12 73 472 (tons/acre) 333 0 52 11 Nutrients (lb/acre) 0.2 0 0 Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M 0.9 0.0 BH02 120-200 000 581665.41.7715.90.981.25 349021011257 0 30 Note: 12 84 210 (tons/acre) 333 0 54 12 Nutrients (lb/acre) 0.2 0 0 Thank you for using agronomic services to manage nutrients and safeguard environmental quality. through a grant from the North Carolina Tobacco Trust Fund Commission. Reprogramming of the laboratory-information-management system that makes this report possible is being funded - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL012916 Page 2 of 4Bill Hinson Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M 0.8 0.0 BH03 120-200 000 531645.41.6746.11.010.76 269037310549 0 40 Note: 12 80 373 (tons/acre) 333 0 52 17 Nutrients (lb/acre) 0.1 0 0 Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M 0.8 0.0 BH04 120-200 000 301655.31.4684.51.060.66 472731310243 0 80 Note: 12 78 313 (tons/acre) 333 0 50 15 Nutrients (lb/acre) 0.2 0 0 Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M 1.8 0.0 BH05 120-200 000 393184.82.7535.80.961.19 374441012688 0 60 Note: 12 93 410 (tons/acre) 333 0 40 10 Nutrients (lb/acre) 0.2 0 0 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL012916 Page 3 of 4Bill Hinson Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M 1.0 0.0 CM1 120-200 000 42755.31.8736.80.990.81 340830711347 0 50 Note: 12 85 307 (tons/acre) 333 0 56 14 Nutrients (lb/acre) 0.2 0 0 Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M 1.0 0.0 CM2 120-200 000 751485.31.9726.81.080.66 135730213545 0 10 Note: 12 98 302 (tons/acre) 333 0 50 16 Nutrients (lb/acre) 0.1 0 0 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL012916 Page 4 of 4Bill Hinson Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or lb/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no-till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at one time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-I levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to . In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot find the exact fertilizer grade recommended on the report, visit to find information that may help you choose a comparable alternate. For more information, read . Test Results The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-AI1, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS-I, Na, ESP, SS-I, NO 3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit Report Abbreviations Ac exchangeable acidity B boron BS% % CEC occupied by basic cations Ca%% CEC occupied by calcium CEC cation exchange capacity Cu-I copper index ESP exchangeable sodium percent HM%percent humic matter K-I potassium index K2O potash Mg%% CEC occupied by magnesium MIN mineral soil class Mn manganese Mn-Al1 Mn-availability index for crop 1 Mn-AI2 Mn-availability index for crop 2 Mn-I manganese index M-O mineral-organic soil class N nitrogen Na sodium NO3-N nitrate nitrogen ORG organic soil class pH current soil pH P-I phosphorus index P2O5 phosphate S-I sulfur index SS-I soluble salt index W/V weight per volume Zn-AI zinc availability index Zn-I zinc index Understanding the Soil Report: explanation of measurements, abbreviations and units $Note: Secondary Nutrients and Micronutrients www.ncagr.gov/agronomi/obpart4.htm#fs A Homeowner's Guide to Fertilizer. www.ncagr.gov/agronomi/uyrst.htm ncagr.gov/agronomi/pubs.htm. NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL015859 Mehlich-3 Extraction Completed: Received:Sampled: Soil Report Farm: Client: Links to Helpful Information Advisor: 12/16/202211/15/202211/08/2022 Predictive Zach Key Southern Soil Builders 958 Hoots Rd Roaring River, NC 28669 Frank / Sherry Lawson 235 Ellenboro Henrietta Rd / PO Box 1061 Ellenboro, NC 28040 Sampled County : Rutherford 59779 231531Client ID: Advisor ID: Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M Fescue/OGrass/Tim, M 1.4 0.0 FLA1 120-200 120-200 0 0 0 0 0 0 214305.22.4606.01.010.81 311226869390 0 0 100 100 Note: 12 Note: 12 73 73 686 (tons/acre) 333 0 0 48 10 Nutrients (lb/acre) 0.2 0 0 0 0 Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M Fescue/OGrass/Tim, M 0.6 0.0 FLA2 120-200 120-200 0 0 0 0 0 0 291145.71.8798.70.990.66 246740512750 0 0 80 80 Note: 12 Note: 12 93 93 405 (tons/acre) 333 0 0 63 14 Nutrients (lb/acre) 0.2 0 0 0 0 Thank you for using agronomic services to manage nutrients and safeguard environmental quality. through a grant from the North Carolina Tobacco Trust Fund Commission. Reprogramming of the laboratory-information-management system that makes this report possible is being funded - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL015859 Page 2 of 4Frank / Sherry Lawson Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M Fescue/OGrass/Tim, M 1.6 0.0 FLB1 120-200 120-200 0 0 0 0 0 0 352025.12.6586.30.991.02 353436413272 0 0 70 70 Note: 12 Note: 12 96 96 364 (tons/acre) 333 0 0 44 12 Nutrients (lb/acre) 0.2 0 0 0 0 Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M Fescue/OGrass/Tim, M 1.4 0.0 FLB2 120-200 120-200 0 0 0 0 0 0 302455.22.4595.91.050.76 265039910558 0 0 80 80 Note: 12 Note: 12 80 80 399 (tons/acre) 333 0 0 44 13 Nutrients (lb/acre) 0.1 0 0 0 0 Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M Fescue/OGrass/Tim, M 1.0 0.0 FLB3 120-200 120-200 0 0 0 0 0 0 671125.42.0686.40.981.25 344022912053 0 0 20 20 Note: 12 Note: 12 89 89 229 (tons/acre) 333 0 0 49 14 Nutrients (lb/acre) 0.2 0 0 0 0 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL015859 Page 3 of 4Frank / Sherry Lawson Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M Fescue/OGrass/Tim, M 0.0 0.0 FLB4 120-200 120-200 0 0 0 0 0 0 701326.21.4859.21.020.60 256832816257 0 0 10 10 Note: 12 Note: 12 112 112 328 (tons/acre) 333 0 0 57 24 Nutrients (lb/acre) 0.2 0 0 0 0 Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M Fescue/OGrass/Tim, M 0.0 0.0 FLC1 120-200 120-200 pH$ pH$ 0 0 0 0 17857.00.5958.81.120.51 143323814741 0 0 110 110 Note: 12 Note: 12 Note: $ Note: $ 90 90 238 (tons/acre) 333 0 0 81 13 Nutrients (lb/acre) 0.1 0 0 0 0 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL015859 Page 4 of 4Frank / Sherry Lawson Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or lb/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no-till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at one time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-I levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to . In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot find the exact fertilizer grade recommended on the report, visit to find information that may help you choose a comparable alternate. For more information, read . Test Results The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-AI1, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS-I, Na, ESP, SS-I, NO 3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit Report Abbreviations Ac exchangeable acidity B boron BS% % CEC occupied by basic cations Ca%% CEC occupied by calcium CEC cation exchange capacity Cu-I copper index ESP exchangeable sodium percent HM%percent humic matter K-I potassium index K2O potash Mg%% CEC occupied by magnesium MIN mineral soil class Mn manganese Mn-Al1 Mn-availability index for crop 1 Mn-AI2 Mn-availability index for crop 2 Mn-I manganese index M-O mineral-organic soil class N nitrogen Na sodium NO3-N nitrate nitrogen ORG organic soil class pH current soil pH P-I phosphorus index P2O5 phosphate S-I sulfur index SS-I soluble salt index W/V weight per volume Zn-AI zinc availability index Zn-I zinc index Understanding the Soil Report: explanation of measurements, abbreviations and units $Note: Secondary Nutrients and Micronutrients www.ncagr.gov/agronomi/obpart4.htm#fs A Homeowner's Guide to Fertilizer. www.ncagr.gov/agronomi/uyrst.htm ncagr.gov/agronomi/pubs.htm. NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL015860 Mehlich-3 Extraction Completed: Received:Sampled: Soil Report Farm: Client: Links to Helpful Information Advisor: 12/16/202211/15/202211/08/2022 Predictive Zach Key Southern Soil Builders 958 Hoots Rd Roaring River, NC 28669 Javan Calton 660 Calton Rd. Bostic, NC 28018 Sampled County : Rutherford 133475 231531Client ID: Advisor ID: Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M Fescue/OGrass/Tim, M 0.0 0.0 FC2 120-200 120-200 0 0 0 0 0 0 663116.11.78511.80.890.81 281769014566 0 0 20 20 Note: 12 Note: 12 102 102 690 (tons/acre) 333 0 0 73 9 Nutrients (lb/acre) 0.2 0 0 0 0 Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M Fescue/OGrass/Tim, M 0.0 0.0 FC3 120-200 120-200 pH$ pH$ 0 0 0 0 474336.61.19213.20.910.66 2132178415084 0 0 50 50 Note: 12 Note: 12 Note: $ Note: $ 97 97 784 (tons/acre) 333 0 0 83 7 Nutrients (lb/acre) 0.3 0 0 0 0 Thank you for using agronomic services to manage nutrients and safeguard environmental quality. through a grant from the North Carolina Tobacco Trust Fund Commission. Reprogramming of the laboratory-information-management system that makes this report possible is being funded - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL015860 Page 2 of 2Javan Calton Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or lb/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no-till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at one time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-I levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to . In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot find the exact fertilizer grade recommended on the report, visit to find information that may help you choose a comparable alternate. For more information, read . Test Results The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-AI1, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS-I, Na, ESP, SS-I, NO 3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit Report Abbreviations Ac exchangeable acidity B boron BS% % CEC occupied by basic cations Ca%% CEC occupied by calcium CEC cation exchange capacity Cu-I copper index ESP exchangeable sodium percent HM%percent humic matter K-I potassium index K2O potash Mg%% CEC occupied by magnesium MIN mineral soil class Mn manganese Mn-Al1 Mn-availability index for crop 1 Mn-AI2 Mn-availability index for crop 2 Mn-I manganese index M-O mineral-organic soil class N nitrogen Na sodium NO3-N nitrate nitrogen ORG organic soil class pH current soil pH P-I phosphorus index P2O5 phosphate S-I sulfur index SS-I soluble salt index W/V weight per volume Zn-AI zinc availability index Zn-I zinc index Understanding the Soil Report: explanation of measurements, abbreviations and units $Note: Secondary Nutrients and Micronutrients www.ncagr.gov/agronomi/obpart4.htm#fs A Homeowner's Guide to Fertilizer. www.ncagr.gov/agronomi/uyrst.htm ncagr.gov/agronomi/pubs.htm. NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL015861 Mehlich-3 Extraction Completed: Received:Sampled: Soil Report Farm: Client: Links to Helpful Information Advisor: 12/16/202211/15/202211/08/2022 Predictive Zach Key Southern Soil Builders 958 Hoots Rd Roaring River, NC 28669 Norman McDaniel 167 McKinney Mill Rd. Ellenboro, NC 28040 Sampled County : Rutherford 139529 231531Client ID: Advisor ID: Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M Fescue/OGrass/Tim, M 0.5 0.0 NM01 120-200 120-200 0 0 0 0 0 0 212335.81.8819.50.980.92 352266925877 0 0 100 100 Note: 12 Note: 12 172 172 669 (tons/acre) 333 0 0 67 13 Nutrients (lb/acre) 0.3 0 0 0 0 Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M Fescue/OGrass/Tim, M 0.0 0.0 NM02 120-200 120-200 pH$ pH$ 0 0 0 0 33737.00.4959.01.080.46 213720418948 0 0 70 70 Note: 12 Note: 12 Note: $ Note: $ 115 115 204 (tons/acre) 333 0 0 82 11 Nutrients (lb/acre) 0.2 0 0 0 0 Thank you for using agronomic services to manage nutrients and safeguard environmental quality. through a grant from the North Carolina Tobacco Trust Fund Commission. Reprogramming of the laboratory-information-management system that makes this report possible is being funded - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL015861 Page 2 of 4Norman McDaniel Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Corn, silage 0.0 0.0 NM03 180-220 000 261536.21.3869.41.050.71 234063825974 0 150 Note: 3 169 638 (tons/acre) 333 0 74 11 Nutrients (lb/acre) 0.2 0 0 Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Soybean 1.3 0.0 NMA 0 000 241395.42.5739.20.920.76 251958066279 0 90 Note: 3 407 580 (tons/acre) 333 0 58 13 Nutrients (lb/acre) 0.2 0 0 Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Soybean 0.8 0.0 NMB 0 000 181385.62.0727.11.010.60 3566774106762 0 100 Note: 3 650 774 (tons/acre) 333 0 56 14 Nutrients (lb/acre) 0.2 0 0 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL015861 Page 3 of 4Norman McDaniel Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Soybean 0.0 0.0 NMC 0 pH$00 314737.40.010024.90.990.36 173797911769 0 80 Note: 3 Note: $ 58 979 (tons/acre) 333 0 96 4 Nutrients (lb/acre) 0.2 0 0 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL015861 Page 4 of 4Norman McDaniel Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or lb/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no-till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at one time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-I levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to . In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot find the exact fertilizer grade recommended on the report, visit to find information that may help you choose a comparable alternate. For more information, read . Test Results The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-AI1, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS-I, Na, ESP, SS-I, NO 3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit Report Abbreviations Ac exchangeable acidity B boron BS% % CEC occupied by basic cations Ca%% CEC occupied by calcium CEC cation exchange capacity Cu-I copper index ESP exchangeable sodium percent HM%percent humic matter K-I potassium index K2O potash Mg%% CEC occupied by magnesium MIN mineral soil class Mn manganese Mn-Al1 Mn-availability index for crop 1 Mn-AI2 Mn-availability index for crop 2 Mn-I manganese index M-O mineral-organic soil class N nitrogen Na sodium NO3-N nitrate nitrogen ORG organic soil class pH current soil pH P-I phosphorus index P2O5 phosphate S-I sulfur index SS-I soluble salt index W/V weight per volume Zn-AI zinc availability index Zn-I zinc index Understanding the Soil Report: explanation of measurements, abbreviations and units $Note: Secondary Nutrients and Micronutrients www.ncagr.gov/agronomi/obpart4.htm#fs A Homeowner's Guide to Fertilizer. www.ncagr.gov/agronomi/uyrst.htm ncagr.gov/agronomi/pubs.htm. NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL015862 Mehlich-3 Extraction Completed: Received:Sampled: Soil Report Farm: Client: Links to Helpful Information Advisor: 12/16/202211/15/202211/08/2022 Predictive Zach Key Southern Soil Builders 958 Hoots Rd Roaring River, NC 28669 Larry Bailey 2174 Salem Church Rd Bostic, NC 28018 Sampled County : Rutherford 492927 231531Client ID: Advisor ID: Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M Fescue/OGrass/Tim, M 0.0 0.0 LB1 120-200 120-200 pH$ pH$ 0 0 0 0 1001776.51.18910.51.000.66 161443213350 0 0 0 0 Note: 12 Note: 12 Note: $ Note: $ 89 89 432 (tons/acre) 333 0 0 57 28 Nutrients (lb/acre) 0.1 0 0 0 0 Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M Fescue/OGrass/Tim, M 0.0 0.0 LB2 120-200 120-200 0 0 0 0 0 0 481906.11.78310.21.010.66 271255312371 0 0 40 40 Note: 12 Note: 12 90 90 553 (tons/acre) 333 0 0 56 25 Nutrients (lb/acre) 0.2 0 0 0 0 Thank you for using agronomic services to manage nutrients and safeguard environmental quality. through a grant from the North Carolina Tobacco Trust Fund Commission. Reprogramming of the laboratory-information-management system that makes this report possible is being funded - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL015862 Page 2 of 4Larry Bailey Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M Fescue/OGrass/Tim, M 0.0 0.0 LB3 120-200 120-200 0 0 0 0 0 0 233336.31.28911.11.080.41 228955638259 0 0 90 90 Note: 12 Note: 12 242 242 556 (tons/acre) 333 0 0 78 10 Nutrients (lb/acre) 0.2 0 0 0 0 Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M Fescue/OGrass/Tim, M 0.0 0.0 LB4 120-200 120-200 pH$ pH$ 0 0 0 0 293617.00.69613.01.030.41 223651514348 0 0 80 80 Note: 12 Note: 12 Note: $ Note: $ 88 88 515 (tons/acre) 333 0 0 88 6 Nutrients (lb/acre) 0.2 0 0 0 0 Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M Fescue/OGrass/Tim, M 0.5 0.0 LB5 120-200 120-200 0 0 0 0 0 0 1472325.82.08110.60.990.66 253355616284 0 0 0 0 Note: 12 Note: 12 114 114 556 (tons/acre) 333 0 0 52 22 Nutrients (lb/acre) 0.2 0 0 0 0 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL015862 Page 3 of 4Larry Bailey Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M Fescue/OGrass/Tim, M 0.3 0.0 LB6 120-200 120-200 0 0 0 0 0 0 1162925.91.98311.10.970.76 275753421574 0 0 0 0 Note: 12 Note: 12 146 146 534 (tons/acre) 333 0 0 58 20 Nutrients (lb/acre) 0.2 0 0 0 0 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL015862 Page 4 of 4Larry Bailey Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or lb/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no-till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at one time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-I levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to . In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot find the exact fertilizer grade recommended on the report, visit to find information that may help you choose a comparable alternate. For more information, read . Test Results The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-AI1, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS-I, Na, ESP, SS-I, NO 3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit Report Abbreviations Ac exchangeable acidity B boron BS% % CEC occupied by basic cations Ca%% CEC occupied by calcium CEC cation exchange capacity Cu-I copper index ESP exchangeable sodium percent HM%percent humic matter K-I potassium index K2O potash Mg%% CEC occupied by magnesium MIN mineral soil class Mn manganese Mn-Al1 Mn-availability index for crop 1 Mn-AI2 Mn-availability index for crop 2 Mn-I manganese index M-O mineral-organic soil class N nitrogen Na sodium NO3-N nitrate nitrogen ORG organic soil class pH current soil pH P-I phosphorus index P2O5 phosphate S-I sulfur index SS-I soluble salt index W/V weight per volume Zn-AI zinc availability index Zn-I zinc index Understanding the Soil Report: explanation of measurements, abbreviations and units $Note: Secondary Nutrients and Micronutrients www.ncagr.gov/agronomi/obpart4.htm#fs A Homeowner's Guide to Fertilizer. www.ncagr.gov/agronomi/uyrst.htm ncagr.gov/agronomi/pubs.htm. NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL015863 Mehlich-3 Extraction Completed: Received:Sampled: Soil Report Farm: Client: Links to Helpful Information Advisor: 12/16/202211/15/202211/08/2022 Predictive Zach Key Southern Soil Builders 958 Hoots Rd Roaring River, NC 28669 Evelyn Davis 318 McKinney Mill Rd Ellenboro, NC 28040 Sampled County : Rutherford 514904 231531Client ID: Advisor ID: Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M Fescue/OGrass/Tim, M 0.5 0.0 RD1A 120-200 120-200 0 0 0 0 0 0 221075.81.8777.91.020.66 354540517554 0 0 100 100 Note: 12 Note: 12 122 122 405 (tons/acre) 333 0 0 62 14 Nutrients (lb/acre) 0.2 0 0 0 0 Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M Fescue/OGrass/Tim, M 0.0 0.0 RD1B 120-200 120-200 0 0 0 0 0 0 481076.11.5849.50.990.76 222031213750 0 0 40 40 Note: 12 Note: 12 97 97 312 (tons/acre) 333 0 0 59 22 Nutrients (lb/acre) 0.2 0 0 0 0 Thank you for using agronomic services to manage nutrients and safeguard environmental quality. through a grant from the North Carolina Tobacco Trust Fund Commission. Reprogramming of the laboratory-information-management system that makes this report possible is being funded - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL015863 Page 2 of 3Evelyn Davis Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Fescue/OGrass/Tim, M Fescue/OGrass/Tim, M 0.0 0.0 RD2 120-200 120-200 0 0 0 0 0 0 21746.01.4828.01.050.71 42002739063 0 0 100 100 Note: 12 Note: 12 70 70 273 (tons/acre) 333 0 0 57 24 Nutrients (lb/acre) 0.3 0 0 0 0 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL015863 Page 3 of 3Evelyn Davis Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or lb/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no-till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at one time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-I levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to . In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot find the exact fertilizer grade recommended on the report, visit to find information that may help you choose a comparable alternate. For more information, read . Test Results The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-AI1, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS-I, Na, ESP, SS-I, NO 3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit Report Abbreviations Ac exchangeable acidity B boron BS% % CEC occupied by basic cations Ca%% CEC occupied by calcium CEC cation exchange capacity Cu-I copper index ESP exchangeable sodium percent HM%percent humic matter K-I potassium index K2O potash Mg%% CEC occupied by magnesium MIN mineral soil class Mn manganese Mn-Al1 Mn-availability index for crop 1 Mn-AI2 Mn-availability index for crop 2 Mn-I manganese index M-O mineral-organic soil class N nitrogen Na sodium NO3-N nitrate nitrogen ORG organic soil class pH current soil pH P-I phosphorus index P2O5 phosphate S-I sulfur index SS-I soluble salt index W/V weight per volume Zn-AI zinc availability index Zn-I zinc index Understanding the Soil Report: explanation of measurements, abbreviations and units $Note: Secondary Nutrients and Micronutrients www.ncagr.gov/agronomi/obpart4.htm#fs A Homeowner's Guide to Fertilizer. www.ncagr.gov/agronomi/uyrst.htm ncagr.gov/agronomi/pubs.htm. NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL017501 Mehlich-3 Extraction Completed: Received:Sampled: Soil Report Farm: Client: Links to Helpful Information Advisor: 01/12/202311/21/202211/18/2022 Predictive Zach Key Southern Soil Builders 958 Hoots Rd Roaring River, NC 28669 William (Bill Jr)/Kathleen Porter 3573 Greenhorn Rd. Roaring River, NC 28669 Sampled County : Wilkes 151551 231531Client ID: Advisor ID: ATTENTION: This report was flagged with a "C" and/or "Z" to alert you that copper and/or zinc have accumulated in the soil and are approaching a level that could be detrimental to crop production. The C and Z symbols are printed on your report for soil test Zn and Cu index levels of 2000 or more for agronomic crops; for peanuts with zinc, the level is 250. This note is designed to be a "trigger" that allows enough time to either reduce the rate of application or find another field for application of biosolids and/or waste water. The CTL (critical toxic level) for Cu and Zn is set at a 3000 index; for peanuts with zinc, the level is 500. Maintaining a pH of 6.0 or higher may reduce potential for toxicity, especially for Zn. These levels are used by DENR as a benchmark to determine when application of waste products should be stopped. The CTL for copper and zinc was set to prevent levels from accumulating to the point where they become toxic to crops grown on a field. Agronomist's Comments: Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Corn, silage 0.5 0.0 BP1 180-220 000 1323435.81.88210.41.020.86 167041912152 0 0 Note: 3 90 419 (tons/acre) 333 0 63 13 Nutrients (lb/acre) 0.1 0 0 Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Corn, silage 0.7 0.0 BP3 180-220 000 264435.72.28212.11.000.66 1132288311667 0 150 Note: 3 87 883 (tons/acre) 333 0 70 11 Nutrients (lb/acre) 0.1 0 0 Thank you for using agronomic services to manage nutrients and safeguard environmental quality. through a grant from the North Carolina Tobacco Trust Fund Commission. Reprogramming of the laboratory-information-management system that makes this report possible is being funded - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL017501 Page 2 of 3William (Bill Jr)/Kathleen Porter Lime History: Sample ID: More Information Test Results [units - W/V in g/cm ; CEC and Na in meq/100 cm ; NO3-N in mg/dm ]: Soil Class: Ca%NO3-NSS-IESPNaCu-IZn-AIZn-IMn-AI2Mn-AI1Mn-IS-IMg%K-IP-IpHAcBS%CECW/VHM% 2 - 1 - Crop Recommendations:Lime BCuZnMnSMgK2OP2O5N Mineral Corn, silage 0.3 0.0 BP4 180-220 000 923615.91.98210.91.030.71 1200570810153 0 30 Note: 3 Note: $ 78 708 (tons/acre) 333 0 66 12 Nutrients (lb/acre) 0.1 0 C NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No.FY23-SL017501 Page 3 of 3William (Bill Jr)/Kathleen Porter Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or lb/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no-till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at one time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-I levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to . In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot find the exact fertilizer grade recommended on the report, visit to find information that may help you choose a comparable alternate. For more information, read . Test Results The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-AI1, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS-I, Na, ESP, SS-I, NO 3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit Report Abbreviations Ac exchangeable acidity B boron BS% % CEC occupied by basic cations Ca%% CEC occupied by calcium CEC cation exchange capacity Cu-I copper index ESP exchangeable sodium percent HM%percent humic matter K-I potassium index K2O potash Mg%% CEC occupied by magnesium MIN mineral soil class Mn manganese Mn-Al1 Mn-availability index for crop 1 Mn-AI2 Mn-availability index for crop 2 Mn-I manganese index M-O mineral-organic soil class N nitrogen Na sodium NO3-N nitrate nitrogen ORG organic soil class pH current soil pH P-I phosphorus index P2O5 phosphate S-I sulfur index SS-I soluble salt index W/V weight per volume Zn-AI zinc availability index Zn-I zinc index Understanding the Soil Report: explanation of measurements, abbreviations and units $Note: Secondary Nutrients and Micronutrients www.ncagr.gov/agronomi/obpart4.htm#fs A Homeowner's Guide to Fertilizer. www.ncagr.gov/agronomi/uyrst.htm ncagr.gov/agronomi/pubs.htm.