WQ0018525_2022 Residual Annual Report_20230217 (2)

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * WQ0018525
Applicant/Permittee Barnes Environmental Waste and Hauling, Inc.
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Wilmington
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Martin Mabe
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
3363121396
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0018525
Has Current Existing permit number
Applicant/Permittee Address*
PO Box 654, Newport, NC 28570
Facility Name*
Barnes Environmental Class B Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Barnes Environmental 2022 Annual Report WQ0018525.pdf 26.81 MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/17/2023

2022 ANNUAL REPORT
LAND APPLICATION PROGRAM
BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
PERMIT #WQ0018525
WMSS Project No. 15-02 Ph: 01
Prepared for:
Barnes Environmental Waste and Hauling, Inc.
Post Office Box 654
Newport, North Carolina 28570
Compiled by:
Willcox & Mabe Soil Solutions, PLLC
7231B Summerfield Road
Su nmerfield, North Carolina 27358
February 2023

Willcox&mate
SOIL SOLUTIONS
February 17, 2023
NCDEQ-DWR Non -Discharge Compliance Unit
512 North Salisbury Street
9th Floor, Office# 942X
Raleigh, North Carolina 27604
Attention: Non -Discharge Compliance Unit
Reference: 2022 ANNUAL REPORT FOR WQ0018525
Barnes Environmental Waste and Hauling, Inc.
WMSS, Inc. Project No. 15-02 Ph: 01
Non -Discharge Compliance Unit:
Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting
requirements as specified in the above referenced permit on behalf of Barnes Environmental
Waste and Hauling, Inc. (Barnes Environmental Waste). WMSS compiled this report using
data gathered during the compliance year by Barnes Environmental Waste.
If there is any further infonnation required or questions regarding this land application
program please do not hesitate to contact Mr. Steve Barnes, with Barnes Environmental
Waste 252-241-5014 for further assistance.
Sincerely,
Willcox & Mabe Soil Solutions, PLLC
AZA�IYU_40
Martin Mabe
NC Land Application/Residuals Operator
#22753
Enclosure(s)
cc Barnes Environmental Waste
SharedlWMSS Projects12015\15-02 Barnes Environmental12022 Annual Report12022 ANNUAL REPORT,doc
Willcox & Mabe Soil Solutions, PLLC / 7231 B Summerfield Road / Summerfield, NC 27358 / Rob 336.339.9128 or
Martin 336.312.1396 / www.willcoxmabesoil.com

TABLE OF CONTENTS
SECTION NO. TITLE
Certification Form
II Residuals Analyses & Pathogen and Vector Attraction
III Application Summary and Field Loading Rate Reports
IV Soil Analysis

CERTIFICATION FORM

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0018525 County:
Facility Name (as shown on permit):
Land Application Operator:
Year: 2022
Barnes Environmental Waste and Hauling, Inc.
Steven M. Barnes Phone: [phone]
Carteret
Lancl application of residuals as allowed by the permit occurred during the past calendar year?
El Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Ippncarion Jummarv:
Total number of application fields in the r
Total number of fields utilized for land application during the
Total amount of dry tons applied during the year for all application sites: K74
Total number of acres utilized for land application during the year: 24.7
Part B - Annual Compliance Statement-
Facility was compliant during calendar year 2022 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality, El Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
I) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC. 02T . 1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1 111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Steven M. Barnes, President
Permittee Name and Title (type or print) Signature of Permittee Date
29—y2 NXned Feb 17, 2023
Steve M Barnes IFeb 17.2023 1433 EST}
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
DEN FORM ACF (12/2006)

RESIDUAL ANALYSES REPORTS AND
PATHOGEN AND VECTOR ATTRACTION REDUCTION

Permit Number WOOOIBS25
Facility Name Barnes Environmental
NPDES # See Below
WWTP Name See Below
RESIDUAL ANALYSIS DATA
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding laboratory analysls.
Please note that your permit may conlain additional parameters to be analyzed than those required to be summarized on this roan.
Laboratory 1 Environment 1, Inc.
2 Environmental Chemists Inc.
3
NPDES#
WOOOD4059 Wpo013676
VI.14-13
I W00003044
VW5.13
W00006063
VI-02-18
VI-27-17-1
I DEN - Local 1 VI.12-18
WWiP Norma
Atlanlic Station Beacons Reach
Colony by Sea
Dunescape
Eight VZ Marina
Genesis Condos
Hampton Suites
Harkers Point
Kingsbrid a II McGinnis Point
Compasited l Grab
41/13/22 02/15/22
04121/22
02103/22
03122122
02/15/22
02/01/22
03129/22
04/28/22 02 O8122
,., Percent5olids
J 0.53 2.03
1.63
1.04
0.63
1,54
1.17
0.97
1.30 1.49
Arsenic
2.50
2.50
2.50
2.50
3.50
1 2-50
1 2.50
2,50
2.50
2.90
Cadmium
0.54
0.77
1.10
0.92
1.40
0.96
0.50
1.20
2.00
0.56
Copper
427.00
945.00
212.00
695.00
1,060.00
454.00
1.377.00
529.00
263.00
1,448,00
Lead
7.80
13.00
10.00
12.00
20.00
9.70
5.50
22.00
28.00
22.00
Mercury,
0.15
0.22
0.21
0.15
OAS
0.18
0.10
0.04
0.36
0.45
Molybdenum
5.00
8.00
5.00
5.00
5.00
6.00
6.00
5.00
5.00
8.00
Nickel
7.00
16.00
11.00
13.00
11.00
10.00
11.00
11.00
13.00
11,QD
Selenium
5.00
5,00
5.00
5.00
5.00
5.00
5.00
5.00
5.70
5.90
Zinc
999,00
1,039.00
2,123.00
2.501.00
2,259.00
867.00
949.00
1.849.00
4.313.00
1,361.00
TKN
21,010,00
78,980.00
40.790.00
66.800.00
42,770,00
99.940.00
63,450.OD
66,070.00
60,220.00
63.490.00
Ammonia-Ni1rogen
10.99
1,746.00
863.80
69.47
46.98
2,851.OD
322.40
350.50
41%00
519,40
Nilrate-Nilrogen
112.90
3,559.00
12.94
10.92
233.90
11.95
662.60
46.93
24.94
28,97
Total Phosphorus 1
9.061.00
21.210.00
8,290.00
19,890.00
16,820,OD
21,290.00
16,520.00
15.370.00 1
13.660.00
24,620.00
NPDES# _ W00079331 I WQ0003067 �_ WODD18420 V1-00-16 W00002128
WTP Name NC Aquarium Ocean Bay Villas Ocean Cluh Ocean Condos Pebble Beach
td/Grab I 08118/22 1 04/28122 02117/22 02115122 031151
Solids 1.85 0.43 0.68 1,66 1,34
Resort
WQOOM24
VI-03.17
Arsenic
2.50
2.50
2.50
1 2.50
2.50
2.50
2.50
2.50
2.50
2.50
Cadmium
8.40
1.20
0.57
0.84
1.20
1,20
0.98
0.85
0.74
0.73
Copper
305.00
287.00
282.00
494.00
303.00
446,00
541.00
255.00
168.00
1,048.01)
Lead
26.00
27.00
7.30
15.00
16.00
16.00
50,00
7-80
32,00
20.00
Mercury
0.11
0.42
0.21
0.17
0.26
0.29
0.36
0.23
0.13
0.26
Molywerturn
13.00
5.00
6.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
Nickel
25,00
12.00
9.00
10.00
7.00
12.00
12.00
12,00
14,00
13.00
Selenium
5.00
6.00
5,00
5.00
5.00
5.00
6.20
5.00
5.00
5.00
Zinc
1.053.00
1,290.00
1.387.00
1,163.00
2,227.00
2,50100
2.389.00
1.293.00
987,00
1,499,00
TKN
52,470.00
55,450.00
60,330.00
72,980,00
66,650.00
44,140.00
61,580.00
73.240.00
58.270.00
46,360.00
Ammonia -Nitrogen
1,502.OD
50.93
1,573-00
1.162.00
1.955.00
100.60
346.90
1.800.00
419AG
109.40
Nitrale-Nitrogen
9.99
609.10
5.97
6.96
7.94
676.00
4.98
3.99
10,96
0.99
Total Phosphorus
25,290.00
10,690.00
24.200.00
15.180.00
8,551.00
17.340.00
14,050.0D
21.990.00
18,820. 00
21.730.00
Steve M Barnes Feb 17, 2023
(SIGNATURE OF PREPARER) DATE
I certify, under penalty of law, that this document was prepared under my direclion or supervision in accordance with a system designed
to assure thal qualified personnel property gathered and evaluated the information submitted, I am aware that there are significant
penalties for submitting false information, including the possibility offines and imprisonment for knowing violations.
Page 1

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding tebaratM analysis.
Praase note that your permit may contain additional parameters to be analysed than those required to be summarized on this Fenn,
Permit Number W00018525 Laboratory 1 Environment 1, Inc.
Facility Name Barnes Environmental 2 Environmental Chemists. �Inc.
NPDES ;1 See Below 13)
WWTP Name See Below
x SpSteve M Barnes Feb 17, 2023
(SIGNATURE OF PREPARER) DATE
I certify, under penalty of law, that this document was prepared under my direction or supervision In accordance with a system designed
to assure that qualified personnel property gathered and evaluated the Information submitted. I am aware that there are significant
penalties for submitting false Information, including the possibility of fines and imprisonment for knowing violations.
Page 2

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 13, 2022
Permit No. WQ0018525
Atlantic Station 0.53 % Solids
12.3 PH (taken from lime stabilization event)
Parameter
%
Mg/Kg Dry Weight
(% x 10,1
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
0.723
21,010.000
42.020
Phosphorus
0.263
9,051.000
18.102
Potassium
0.449
6,469.000
12.938
PAN (injected)*
0.265
2,650.800
5.302
PAN (surface)*
0.239
2,387.300
4.775
Ammonia Nitrogen
0.053
I0.990
0.022
Calcium
3.558
21,168.000
42.336
Calcium Carbonate E .
---
---
Magnesium
---
11,780.000
23.560
Sodium
---
87,351.000
174.702
Sulfur
---
___
Nitrate N / Nitrite N
---
112.900
0.226
Curium
---
---
---
SAR
8.66
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(M /K )
Aluminum
---
1,795.00
3.590
Arsenic
---
2.50
0.005
75
Cadmium
---
0.54
0.001
85
Chromium
---
8,Q00
___
---
Copper
---
427.00
0.854
4,300
Lead
---
7.80
0.016
840
Mercury
---
0.15
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
7.00
0,014
420
Selenium
---
5.00
0.010
100
Zinc
---
999.00
1.998
7,500
Environment [,Incorporated 108A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.

u
mo limil (IM % honn @TOW
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
ATLANTIC STATION (F'ORTIN)
MR. DAFT FORTIN
FORTIN CONTRACT SERVICES
P.O, BOX 4188
EMERALD ISLE, NC 28594
PARANIETERS
Aluminum, (dry Wt. basis), mg/Itg
Arsenic (dry wt. basis), mglkg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mglltg
Chromium, T.(dry Wt. basis),mg/ltg
Lead (dry weight basis), mg/kg
Nlagnesiu n (dry wt. basis), mg/lig
Rlercury (dry wt. basis), Ing/kg
Nickel (dry wt, basis), mg/kg
Potassium (dry wt. basis), mglltg
Selenium (dry wt. basis), mg/hg
Sodium (dry wt. basis), mglltg
Zinc (dry Wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/itg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/1%
Nitrate-f-Nitrite (dry wt.), mg/lig
Plant Available Nitrogen, mg/kg
141olybdemnn (dry wt. basis), mg/kg
Sludge Analysis method
Sample late Analyst Code
1795
02/01/22
LI`J
EPA200.7
C 2.5
02/01/22
MT141
3113B-04
21168
02/01/22
LFJ
EPA200.7
0.54
02/02/22
114TM
311313-04
427
02/01/22
LFJ
EPA200.7
8
02/01/22
LFJ
EPA200.7
7.8
02/03/22
MTNJ
3113B-04
11780
02/01/22
LFJ
EPA200.7
0.15
01/19/22
MTi41
EPA7471B
7
02/01/22
LFJ
EPA200.7
6469
02/01/22
LFJ
EPA200.7
G 5.0
02/04/22
NNIT11
311313-04
87351
02/01/22
LFJ
EPA200.7
999
02/01/22
LFJ
EPA200.7
0.53
01/13/22
DNS
2540G-15
c 21010
01/20/22
KES
351.2 R2-93
c 10.99
01/24/22
B11'1D
350.1 R2-93
c 9051
01/24/22
KES
365.4-74
e 112.9
01/24/22
TRJ
353.2 R2-93
6418
02/15/22
NIAO
C5.0
0210I/22
LFJ
EPA200.7
Drinking Water ID: 37715
Wastewater IDI 10
PHONE [phone]
FAX [phone]
ID#: 108 A
DATE COLLECTED: 01/13/22
DATE REPORTED : 02/16/22
REVIEWED BY:
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

A'
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El
Environment 1, Inc. CHAIN OF CUSTODY RECORD
P.U. Box 7085. 114 Oakmont 1)r, PaEe
(ircenville. NC -7858 `
envilYlllnlc:lil I Inc.00111
DISINFECTION
Phone [phone] • I'ax (252) 756-063 3
CHLORINE NEUTRALIZED AT COLLECTION
CHI_OIZINE
pH CHECK (LAB)
CLIENT: 108 A Wee x: s
u
p
p
p
p
p
p
CONTAINER TYPE, P/G
rLANTIC STATION (FORTIN)
❑ NONE
R. DAN FORTIN
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CHEMICALPRESERVATION
3RTIN CONTRACT SERVICES
O. SOX 4188
A
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A
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19ERAL D ISLE NC 28594
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SAMPLE LOCATION
DATE
TIME
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CLASSIrICATION�
WASTEWATER(NPDES)
DRINKING WATER
DWRDGW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SHIPMENT/DELIVERY
0 N
SAMPLES COLLEC D BY:
(N.: , Print)
Lr/G
SAMPLES RECEIVED IN LAB AT :C
RE! I i B' (SIG.) (S 1PLER)
I AT ME ;
` p 1
R IVED BY (SIG.}
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DATEMME
COMMENTS:
1`
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1 j 2a 21S I
R NOUISH D BY (SIG.)
DATETIME
RECEIVED BY (SIG.)
DATEMME
RELINQUISHED BY (SIG.)
DATEMME
RECEIVED BY (SIG.)
DATEMME
?LEASE REACT Instructions for- compieling this farm on the icverse side, Sampler must place a "C' far composite ;ample or a "G" far NQ 4�0260
Foam rs Grab sample in the blocks above for each parameter requested.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 15, 2022
Permit No. WQ0018525
Beacons Reach 2.03 % Solids
5.9 PH
Parameter
%
Mg/Kg Dry Weight
Pounds/Dry Too
(% x 10,000)
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
7.898
78,980.000
157.960
Phosphorus
2.121
21,210,000
42.420
Potassium
0.531
5,312.000
10.624
PAN (injected)*
2.848
28,475.200
56.950
PAN (surface)*
2.760
27,602.200
55.204
Ammonia Nitrogen
0.175
1,746.000
3.492
Calcium
2.443
24,432.000
48.864
Calcium Carbonate E .
---
---
---
Magnesium
---
3,435.000
6.870
Sodium
---
9,034.000
18.068
Sulfur
---
Nitrate N / Nitrite N
---
3,559.000
7.118
Barium
---
---
---
SAR
2.04
Chloride
---
---
---
Iron
---
---
---
Ceiling Coneen.
(M /K )
Aluminum
---
2.302.00
4.604
Arsenic
---
2.50
0.005
75
Cadmium
---
0.770
0.002
85
Chromium
---
11.000
Copper
---
945.00
I.890
4,300
Lead
---
13.00
0.026
840
Mercury
---
0.22
0.000
57
Molybdenum
---
8.00
0.016
75
Nickel
---
16.00
0.032
420
Selenium
---
5.00
0.010
100
Zinc
---
1,039.00
2.078
7,500
Environment I # 554A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

KRAnfimin % Wmpo umbd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
BEACON'S REACH I/POND (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE, NC 28594
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
PH (not to be used for reporting)
5.9
02/15/22
JMS
4500HB-11
Aluminum, (dry wt. basis), mg/kg
2302
02/22/22
LFJ
EPA200.7
Arsenic (dry wt. basis), mg/kg
2.5
02/23/22
MTM
3113B-04
Calcium (dry wt. basis), mg/ltg
24432
02/22/22
LFJ
EPA200.7
Cadmium (dry wt. basis), mg/kg
0,77
02/22/22
MTM
3113B-04
Copper (dry wt, basis), mgllcg
945
02/22/22
LFJ
EPA200.7
Chromium, T.(dry wt. basis),mg/kg
11
02/22/22
LF.T
EPA200.7
Lead (dry weight basis), mgllcg
13
02/24/22
MTM
3113B-04
Magnesium (dry wt. basis), mg/icg
3435
02/22/22
LFJ
EPA200.7
Mercury (dry wt. basis), mg/kg
0.22
02/23/22
MTM
EPA7471B
Nicket (dry wt. basis), mgllcg
16
02/28/22
LFJ
EPA200.7
Potassium (dry wt. basis), mg/kg
5312
02/22/22
LFJ
EPA200.7
Selenium (dry wt. basis), mgllcg
C5.0
02/24/22
MTM
3113E-04
Sodium (dry wt. basis), mg/kg
9034
0212Z/22
LFJ
EPA200.7
Zinc (dry wt. basis), mg/kg
1039
02/22/22
LFJ
EPA200.7
Total Solids, %
2.03
02/16/22
JMS
254OG-15
TKN (dry wt.), mgllcg
c 78980
03/01/22
TRJ
351.2 R2-93
Ammonia Nitrogen (dry wt.),mg1kg
c 1746
02/17/22
TRJ
350.1 R2-93
Phosphorus, T. (dry wt.), mgllcg
c 21210
03/01/22
BMD
365.4-74
Nitratc-l-Nitrite (dry wt.), mg/kg
c 3559
02/17/22
KES
353.2 R2-93
Molybdenum (dry wt. basis), mgllcg
8
02/22/22
LFJ
EPA200.7
Drinking Water IDi 37715
Wastewater IDi 30
PHONE [phone]
FAX [phone]
ID#: 554 A
DATE COLLECTED: 02/15/22
DATE REPORTED : 03/02/22
REVIEWED BY:
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

Environment I, Inc. CHAIN OF CUSTODY RECORD
P.G. Box 7085. 114 Oakmont Dr. Pace I of 1
Greenville, NC 27858
environment] ine.corn
DISINFECTION
Phone [phone] ° Fax [phone]
CHLORINE NEUTRALIZED AT COLLECTION
CHLORINE
pH CHECK (LAB)
CLIENT: 554 A Week: 8
UV
P
P
P
P
P
P
P
CONTAINER TYPE, P/G
EACON'S REACH IIPOND (HYDROTECH)
NONE
M: DON O'MARA
YDROTECH
O. BOX 4602
A
A
A
A
A
A
A
CHEMICALPRESERVAnON
HERALD ISLE NC 28594
Eo
A -NONE D-NAOH
52) 725-2319
z J
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=
oo
a
C B• HNO E• HCL
cr
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=
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COLLECTION
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s
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a
SA,'�PLELOCAMON
DATE
11ME
Sludge Sample
L�
^.L
53;
'�
'hY.
{
rE
'y
CLASSIFICATION:
WASTEWATER (NPDES)
v
DRINKING WATER
I DWRIGW
SOLID WAS TESECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING,SWMENT/DELIVERY
Y�l N
SAMPLES COLLECTED BY-
(PIWBE 1)
E�b'l �"tint
SPAIPLESRECEIVED INLAB AT �. °C
R IN SHED BY (SIG.) (SAMPLER)
DAT ErnME
EIVED BY (SIG.)
DATUnME
COMMENTS:
RELINQUISHED BY (SIG.)
DAT'EJ i1ME
RECEIVED BY (SIG.)
DATEMME
RELINQUISHED BY (SIG.)
DAT IDTIME
RECEIVED BY (SIG,)
DATE MME
Sampler must place a "C" for composite sample or a `G for 400'143
PLEASE READ instructions for completing this form on the reverse side. a
FORM 45 Grab sample in the blacks above for each parameter requested.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: April 21, 2022
Permit No. WQ0018525
Colony By The Sea 1.63 % Solids
12.2 pH (taken from lime stabilization event)
Parameter
%
Mg/Kg Dry Weight
(% x t0,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002) :1
Nitrogen (TKN)
4.079
40,790.000
81.580
Phosphorus
0.829
8,290.000
16.580
Potassium
0.298
2,984.000
5.968
PAN (injected)*
1.285
12,854,600
25.709
PAN (surface)*
1.242
12,422,700
24.845
Ammonia Nitrogen
0.086
863.800
1.728
Calcium
2.283
22,830.000
45.660
Calcium Carbonate E .
---
---
Magnesium
---
2,238.000
4.476
Sodium
---
7,614.000
15.228
Sulfur
---
___
-__
Nitrate N / Nitrite N
---
12.940
0.026
Barium
---
---
---
SAR
1.64
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
2,763.00
5.526
Arsenic
---
2.50
0.005
75
Cadmium
---
1.10
0.002
85
Chromium
---
16.000
---
---
Copper
---
212.00
0.424
4,300
Lead
---
10.00
0.020
840
Mercury
---
0.21
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
11.00
0.022
420
Selenium
---
5.00
0.010
100
Zinc
---
2,123.00
4.246
7,500
Environment I # 616A
*Determination of Plant Available Nitrogen (PANT).
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.

Eawd"m[ (IM % hCwV@WA%d
114 OAKMONT DRIVE_
GREENVILLE, N.C. 27858
COLONY BY THE SEA (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE, NC 28594
PARAMETERS
Aluminum, (dry wt. basis), mg/lig
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt, basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mglkg
Lead (dry weight basis), mg/lig
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mglkg
Phosphorus, T. (dry wt.), mgllig
Nitrate+Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mg/lig
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
2763
05/04/22
LFJ
EPA200.7
<2.5
05/04/22
MTM
3113E-04
22830
05/04/22
LFJ
EPA200.7
1.1
05/06/22
MTM
3I1313-04
212
05/04/22
LFJ
EPA200.7
16
05/04/22
LFJ
EPA200.7
10
05/04/22
MTM
3113E-04
2238
05/04/22
LFJ
EPA200.7
0.21
04/27/22
MTM
EPA747113
11
05/04/22
LFJ
EPA200.7
2984
05/04/22
LFJ
EPA200.7
<5.0
05/05/22
MTM
3113E-04
7614
05/04/22
LFJ
EPA200.7
2123
05/04/22
LFJ
EPA200.7
1.63
04/21/22
HCE
254OG-15
c 40790
04/27122
TRJ
351.2 112-93
c 863.8
04/26/22
TRJ
350.1 R2-93
c 8290
04/28/22
ICES
365.4-74
c 12.94
04/26/22
ICES
353.2 R2-93
12423
04/29/22
ICES
<5.0
05/04/22
LFJ
EPA200.7
Drinking Water ID: 37715
Wastewater IDS 16
PHONE [phone]
FAX [phone]
ID#: 616 A
DATE COLLECTED: 04/21/22
DATE REPORTED : 05/16/22
REVIEWED BY: �� 1
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

(2
Environnnent 1, Inc. CHAIN OF CUSTODY RECORD
P.O. Box 7085, 114 Oakmont Dr. Page I Of 1
Greenville, NC 27858
env i ron anen t 1 i nc.c oni
DISINFECTION
Phone [phone] • Fax [phone]
CHLORINE NEUTRALIZED AT COLLECTION
Ij CHLORINE
pH CHECK (LAB)
CLIENT: 616 A Week: S
uv
P
P
P
P
P
P
CONTAINER TYPE, PIG
DLONY BY THE SSA (HYDROTECII)
NONE
rTN: DON O'MARA
CHEMICALPRESERVATION
YDROTECH
O. SOX 4602
A
A
A
A
A
A
gERALD ISLE NC 28544
; z
cn
ELLi
A -NONE D-NAOH
52) 725-2319
z
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0 �� ir
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COLLECTION
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SAMPLELOCAT10N
DATE
TIME
Sludge Sample �'�,
_Z
�
4
%
O
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Y `i
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< �.
;
CLASSIFICATION'
L.J-IM-STEWATER (NPDES)
JDRINKING WATER
DWRIGW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING
SH�SHIPMENTIDELIVERY
Oy N
SAMPLES COLLECTED BY:
(Please P, t) ( f�
a
l ` e Q�r
SAMPLES RECEIVED IN LAB AT Ll "C
RELINQUISHED BY (SIG.) (SAMPLER)
DATE/TlME
EiVED BY (SIG.)
DATEMME
COMMENTS:
RELIN DISHED BY (SIG.)
DATEMME
RECEIVED BY (SIG.)
DATEMME
RELINQUISHED BY (SIG.)
DATEMME
RECEIVED BY (SIG.)
DATEiTIME
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G" for
FORM V5 Grab sample in the blocks above for each parameter requested. N- 400111

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 3, 2022
Permit No. WQ0018525
Dunescape 1.04 % Solids
7.0 pH
Parameter
%
Mg/Kg Dry Weight
Pounds/Dry Ton
(% x 10,000)
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
6.680
66,800.000
133.600
Phosphorus
1.989
19,890.000
39.780
Potassium
0.332
3,319.000
6.638
PAN (injected)*
2.010
20,099.549
40.199
PAN (surface)*
2.006
20,064,814
40.I30
Ammonia Nitrogen
0.007
69.470
0.139
Calcium
3.861
38,608.000
77.216
Calcium Carbonate E .
---
---
Magnesium
---
2,664.000
5.328
Sodium
---
13,521.000
27.042
Sulfur
---
---
---
Nitrate N / Nitrite N
---
10.920
0.022
Barium
---
---
---
SAR
1.83
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(M /I( )
Aluminum
---
2,847.00
5.694
Arsenic
---
2.50
0.005
75
Cadmium
---
0.92
0.002
85
Chromium
---
11.000
---
---
Copper
---
695.00
1.390
4,300
Lead
---
12.00
0.024
840
Mercury
---
0.15
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
t3.00
0.026
420
Selenium
---
5.00
0.010
100
Zinc
---
2,501.00
5.002
7,500
Environment 1 # 556 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

ROWDhIME&d % hmp mbd
114 OAKMONT ©RIVE
GREENVILLE. N.C. 27858
DUNESCAPE (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE, NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/Ifg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/lig
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), sng/lig
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mglkg
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
SamPIC Date Analyst Code
7.0
02/03/22
D1J
4500HB-11
2947
02/08/22
LFJ
EPA200.7
<2.5
02/10/22
MTM
3113B-04
38608
02/08/22
LFJ
EPA200.7
0.92
02/08/22
MTM
311313-04
695
02/08/22
LFJ
RPA200.7
11
02/08/22
LFJ
E' PA200.7
12
02/09/22
MTM
3113B-04
2664
02/08/22
LFJ
EPA200.7
0.15
02/10/22
MTM
EPA7471B
13
02/08/22
LFJ
EPA200.7
3319
02/09/22
LFJ
EPA200.7
<5.0
02/11/22
MTM
311313-04
13521
02/08/22
LFJ
EPA200.7
2501
02/08/22
LFJ
EPA200.7
1.04
02/03/22
BLV
254OG-15
c 66800
02/11/22
TRJ
351.2 R2-93
c 69.47
02/08/22
IMS
350.1 R2-93
c 19890
02/11/22
KES
365.4-74
c 10.92
02/09/22
TRJ
353.2 R2-93
<5.0
02/08/22
LFJ
EPA200.7
Drinking Water IDs 37715
Wastewater IDs 10
PHO19E [phone]
FAX [phone]
ID#: 556 A
DATE COLLECTED: 02/03/22
DATE REPORTED ; 02/25/22
REVIEWED BY:
c Uncertified data. DWR does not offer non-aque0u8 certification for this analytical procedure.

G
Environment I, Inc. CHAIN OF CUSTODY RECORD
P.O' Box 7085, 114 Oakmont Dr. Pa- e I o f 1
�YPPi1VIIIP N(' JiRSR
environment 1 inc.com
DISINTECTION
Plione [phone] • Fax [phone]
CHLORINE NEUTRALIZEDAT COLLECTION
Ij Ci-ILORCNE
pH CHECK (LAB)
CLIENT: 556 A Week: 8
UV
UNESCAPE (HYDROTECH)
NONE
P
P
P
P
P
P
P
CONTAINER TYPE, PIG
ITN: DON O'MARA
CHEMICAL PRESERVATION
YDROTECH
.O. BOX,1642
A
A
A
A
A
A
A
VIERALD ISLE NC 28594
E. a
Cl) A -NONE D-NAOH
52) 725-2319
z J
Ld =
W
:_
Cn
C B - HNO, E - HCL
Cc Oo
-
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= F
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GOLLECTIQN
¢
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z
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SAMPLE LOCATION
DATE
TIME
5ladge Sample
_ j - �Z
% (]
5
¢
t> <
.a
Dui
#";e
�
"M
CLASS9CATION:
WASTEWATER (NPDES)
DRINKINGWATER
DWR/GW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SHIPMENT/DELIVERY
N
SAMPLES COLLECTED BY
(Please Print)
TjSAMPLES
RECEIVED W LAB AT4— tC
RELINQUISHED BY ) (S INP ER)
_ DATEMME
RECEIV D BY (SI
DATEMME
COMMENTS:
RELINQUISHED BY (SIG.)
DATEMME
RE EIVED BY (SIG.)
DATEMME
RELINQUISHED BY (SIG.)
DATEMME
RECEIVED BY (SIG.)
DATEMME
PLEASE READ instructions for completing this far5ampter must place a m on the reverse side. "C" for
for composite sample or a "G" Ng 400� 42
FORM ;, Grab sample in the blacks above for each parameter requested.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: March 22, 2022
Permit No. WQ0018525
Eight 1/2 Marina 0.63 % Solids
12.4 pH (taken from lime stabilization)
Parameter
% --
I Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kgx 0.002)
Nitrogen (TKN)
2.438
42,770.000
85.540
Phosphorus
0.244
16,820.000
33.640
Potassium
0.349
4,152.000
8.304
PAN (injected)*
0.761
7,613.746
15.227
PAN (surface)*
0.757
7,565.856
15.132
Ammonia Nitrogen
0.010
46.980
0.094
Calcium
45,874.000
91.748
Calcium Carbonate E .
---
---
---
Magnesium
---
3,089.000
6.178
Sodium
---
21,422.000
42.844
Sulfur
---
---
---
Nitrate N / Nitrite N
---
233.900
0.468
Barium
---
---
---
SAR
2.07
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(M /K )
Aluminum
---
4,792.00
9.584
Arsenic
---
3.50
0.007
75
Cadmium
---
1.40
0.003
85
Chromium
---
26,000
---
---
Copper
---
1,060.00
2.120
4,300
Lead
---
28.00
0.056
840
Mercury
---
0.45
0.001
57
Molybdenum
---
5.00
0.010
75
Nickel
---
11.00
0.022
420
Selenium
---
5.00
0.010
100
Zinc
---
2,259.00
4.518
7,500
Environment 14 196A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

mmk(OREM % kwPufflUd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
EIGHT & ONE-HALF MARINA(FORTIN)
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE, NC 28594
PARAMETERS
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mglkg
Cadmium (dry wt. basis), mglkg
Copper (dry wt. basis), rng/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), tug/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/Icg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mglkg
Nitrate+Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mgllcg
Sludge
Analysis
Method
Sample
Date Analyst
Code
4792
03/30/22
LFJ
EPA200.7
3.5
03/30/22
MTM
3113B-04
45874
03/30/22
LFJ
EPA200.7
1.4
03/31/22
IVITM
311313-04
1060
03/30/2Z
LFJ
EPA200.7
26
03/30/22
LFJ
EPA200.7
28
03/29/22
i4TTM
3113B-04
3089
03/30/22
LFJ
EPA200.7
0.45
03/30/22
rvlTA1
EPA7471B
11
03/30/22
LFJ
EPA200.7
4152
03/30/22
LFJ
EPA200.7
<5.0
03/31/22
MTM
3113E-04
21422
03/30/22
LFJ
EPA200.7
2259
03/30/22
LFJ
EPA200.7
0.63
03/24/22
JMS
254OG-15
c 42770
03/29/22
BMD
351.2 112-93
c 46.98
03/28/22
ICES
350.1 112-93
c 16820
03/29/22
TRJ
365.4-74
c 233.9
03/29/22
KES
353.2 112-93
13074
04/01/22
KES
<5.0
03/30/22
LFJ
EPA200.7
Drinking Water ID: 37715
Wastewater ID: 10
PHONE [phone]
FAX [phone]
ID#: 196 A
DATE COLLECTED: 03/22/22
DATE REPORTED : 04/04/22
REVIEWED 8Y:
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

En.vi-unment 1.Inc. CHAIN OF CUSTODY RECORD
P.O. Box 7085, 114 Oakmont Dr. Paue I of I
Greenville. NC 27358
environment l inc-coin
DISINFECTION
Phone [phone] - Fax [phone]
CHLORINE NEUTRALIZED AT COLLECTION
j—'j CHLORINE
pH CHECK (LAB)
CLIENT: 196 A Week:10
`��
UV
P
P
P
P
P
P
CONTAINER TYPE, PIG
IGHT & ONE-HALF MARINA(FORTIN)
❑ NONE
IR. DAN FORTIN
CHEMICAL PRESERVATION
ORTIN CONTRACT SERVICES
.O. BOX 4188
A
A
A
A
A
A
MERALD ISLE NC 28594
c z
a a
E
A -NONE D-NAOH
:52) 393-8720
z
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w
B -HNO, E HCL
O o
_ �
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¢ E
z
c
i
r
C - H_SO, F - ZINC ACETATEJNAOH
¢
LU
COLLECTION
F
o
w-j
� 00
�-u
0
0
F
0
d
2
� G-NATHIOSULFATE
SAMPLE LOCATION
DATE
TIME
`
Sample
4Slud
CLASSIFICATION:
WASTEWATER (NPDES)
DRINKING WATER
� j DWRIGW
Ij SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SHIPMENT/DELIVERY
O N
SAMPLES COLLEC D BY:
(Pie t)
SAMPLES AECEIVED IN LAB AT i C
RE ED Y (SIG.) ( AMPLER)
. DATE/TIM
RECE BY (SIG.)
OATEMME
COMMENTS:
312E l 2z 3 .
ELINQUI H D BY (SIG.)
DATErrJME
RECEIVED BY (SIG.)
DATEMME
RELINQUISHED BY (SIG.)
DATEMME
RECEIVED BY (SIG.)
DATEMME
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C for composite sample or a "G" for NQ 399533
FORM a5 Grab sample in the blocks above for each parameter requested.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 15, 2022
Permit No. WQ0018525
Genesis Condos 1.54 % Solids
6.8 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
7.994
79,940.000
159.880
Phosphorus
2.129
21,290.000
42.580
Potassium
0.659
6,586.000
13.172
PAN (injected)*
2.599
25,989.650
51.979
PAN (surface)*
2.456
24,564.130
49.128
Ammonia Nitrogen
0.285
2,851.000
5.702
Calcium
2.900
28,995.000
57.990
Calcium Carbonate E .
---
___
---
Magnesium
---
4,166.000
8.332
Sodium
---
6,999.000
13.998
Sulfur
Nitrate N / Nitrite N
---
11.950
0,024
Barium
---
---
---
SAR
1.26
Chloride
---
___
___
Iron
---
---
---
Ceiling Coneen.
(M /K )
Aluminum
---
1,867.00
3.734
Arsenic
---
2.50
0.005
75
Cadmium
---
0.66
0.001
85
Chromium
---
9.000
---
---
Copper
---
454.00
0.908
4,300
Lead
---
9.70
0.019
840
Mercury
---
0.18
0.000
57
Molybdenum
---
6.00
0,012
75
Nickel
---
10.00
0.020
420
Selenium
---
5.00
0.010
100
Zinc
---
867.00
1.734
7,500
Environment 14 68 C
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

rmwo" mmM 1, hCopma" lod
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
GENESIS CONDO ASSO. (HYDROTECH)
DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE, NC 28594
PARAMETERS
PH (not to be used for reporthig)
Aluminum, (dry wt. basis), mgllig
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), ntglkg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight Basis), mg/lig
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/lig
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/lig
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/lig
Total Solids, %
TKN (dry wt.), mgllig
Ammonia Nitrogen (dry ivt.),mg/kg
Phosphorus, T. (dry wt.), mg/Irg
Nitrate+Nitrite (dry wt.), mglkg
Molybdenum (dry wt. basis), mgllig
Sludge Analysis Method
Sample Date Analyst Code
6.8
02/15/22
JMS
4500HB-ll
1867
02/22/22
LFJ
EPA200.7
C2.5
02/23/22
MTM
3113E-04
28995
02/22/22
LFJ
EPA200.7
0.66
02/22/22
MTM
3113E-04
454
02/22/22
LFJ
EPA200.7
9
02/22/22
LFJ
El PA200.7
9.7
02/24/22
MTM
3113B-04
4166
02/22/22
LFJ
EPA200.7
0.18
02/23/22
MTM
EVA7471B
10
02/28/22
LFJ
EPA200.7
6586
02/22/22
LFJ
EPA200.7
5.0
02/24/22
MTM
3113B-04
6999
02/22/22
LFJ
EPA200.7
867
02/22/22
LFJ
EPA200.7
1.54
02116/22
JMS
2540G-15
c 79940
03/01/22
TRJ
351.2 R2-93
c 2851
02/17/22
TRJ
350.1 R2-93
c 21290
03/01/22
BMD
365.4-74
c 1I.95
02/17/22
KES
353.2 R2-93
6
02/22/22
LFJ
EPA200.7
Drinking Water Im 37715
Waatewatar lul 10
PHONE [phone]
FAX [phone]
ID#: 68 C
DATE COLLECTED: 02/15/22
DATE REPORTED : 03/02/22
REVIEWED BY:
0 Uncertified data. DWR doee not offer non-agueoue certification for thie analytical procedure.

Environment 1, Inc. CHAIN OF CUSTODY RI EICORD
P.0:. Box 7085, 114 Oakmont Dr. pane 1 of 1
Greenville, NC 27858
environment 1 inc.com
DISINFECTION
Phone [phone] a Fax [phone];
CHLORINE
CHLORINE NEUTRALIZED AT COLLECTION
CLIENT: 68 C Weep: 10
UVpH
CHECK (LAB)
ENESIS CONDO ASSO. (HYDROTECH)
NONE
P
P
P
P
P
P
P
CONTAINER TYPE, PIG
ON O'MARA
YDROTECH
CHEMICALPRESERVATION
O. SOX 4602
A
A
A
A
A
A
A
VMRAI,D ISLE INC 28594
�- z
E o
A -NONE D-NAOH
52) 725-23I9
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SAMPLE LOCATION
DATE
TIMEcc
:J ..�
,vY',�rJ4
Gas.
a•} ��{
4j�� .
,P1 *
?, +t
Sludge Sample
S.`
CLASSIFICATION:
WASTEWATER (NPDES)
DRINKING WATER
DWRIGW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING '�PMENT/DELIVERY
N
SAMPLES COLLECTED BY.
(Please nnt)
c �� ,
SAMPLES RECEIVED IN LAB AT s LI` °C
RELIIKUISHED BY (SIG.) (SAMPLER)
DATEfTIME
R EIVED BY (SIG.)
DATEMME
COMMENTS:
.1: �
'i
RI=LINQUISHED BY (SIG.)
DATEMME
RECEIVE} BY (SIG.)
DATEJi1ME
RELINQUISHED BY (SIG,)
DATEPME
I
RECEIVED BY (SIG.)
DATETnME
I
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G" for �0 3�9$$.�
FORD is Grab sample in the blocks above for each parameter requested.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February I, 2022
Permit No. WQ0018525
Hampton Suites 1.17 % Solids
7.30 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(MZLKZ x 0.002)
Nitrogen (TKN)
6.345
63,450.000
126.900
Phosphorus
1.652
16,520.000
33.040
Potassium
0.273
2,729,000
5.458
PAN (injected)*
1.992
19,923.280
39.847
PAN (surface)*
1.976
19,762.080
39.524
Ammonia Nitrogen
0.032
322.400
0.645
Calcium
4.907
49,065.000
98.130
Calcium Carbonate E .
---
---
Magnesium
---
2,570.000
5A40
Sodium
---
22,395.000
44.790
Sulfur
---
---
---
Nitrate N / Nitrite N
---
662.600
1.325
Barium
---
---
---
SAR
2.88
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
2748.000
5.496
Arsenic
---
2.50
0.003
75
Cadmium
---
0.50
0.001
85
Chromium
---
9.000
---
---
Copper
---
1,377.00
2.754
4,300
Lead
---
5.50
0.011
840
Mercury
---
0.10
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
11.00
0.022
420
Selenium
---
5.00
0,010
100
Zinc
---
949.00
1.898
7,500
Environment 1, Incorporaled 551 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

EnAmn(M % hmpumbd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
HAMPTON INN (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE, NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/lcg
Calcium (dry wt. basis), mg/Icg
Cadmium (dry wt. basis), mg/Icg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mglkg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/Icg
Nickel (dry wt. basis), mgllcg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mgllcg
Zinc (dry wt. basis), mgllcg
Total Solids, %
TI{N (dry wt.), mgllcg
Ammonia Nitrogen (dry wt.),mg/lcg
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/Icg
Sludge Analysis Method
Sample Date Analyst Code
7.3
02/01/22
DIJ
4500HB-11
2748
02/08/22
LFJ
EPA200.7
<2.5
02/10/22
NTTM
3113E-04
49065
02/08/22
LFJ
EPA200.7
<0.5
02/08/22
MTM
3113B-04
1377
02/09/22
LFJ
EPA200.7
9
02/08/22
LFJ
EPA200.7
5.5
02/09/22
MTM
3113B-04
2570
02/08/22
LFJ
EPA200.7
0.10
02/10/22
MTM
EPA7471B
11
02/08/22
LFJ
EPA200.7
2729
02/09/22
LFJ
EPA200.7
< 5.0
02/11/22
MTM
3113E-04
22395
02/08/22
LFJ
EPA200.7
949
02/08/22
LFJ
EPA200.7
1.17
02/01/22
DNS
254OC-15
c 63450
02/08/22
TRJ
351.2 R2-93
c 322.4
02/04/22
BMD
350.1 R2-93
c 16520
02/08/22
BMD
365.4-74
c 662.6
02/04/22
TRJ
353.2 R2-93
5
02/08/22
LFJ
EPA200.7
Drinking Water IDs 37719
Wastewater ID= 10
PHONE [phone]
FAX [phone]
ID#: 551 A
DATE COLLECTED; 02/01/22
DATE REPORTED : 02/25/22
REVIEWED BY:
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

I
E
I
I
I
(
Environment 1, Inc. CHAIN Off' CUSTODY RECORD
P.O. Box 7085. 114 Oakmont Dr.
Greenville_ NC 27858
Page I of 1
environment Iinc.com
DISINFECTION
Phone [phone]OR • Fax [phone]
CHLORINE NEUTAALIZEDATCOLLECTION
CHLORINE
pH CHECK (LAB)
CLIENT: S51 A Week: 9
uv
tAM -rON INN (HYDROTECH)
, ONE
P
p
P
P
P
P
P
CONTAINER TYPE, PIG
,TTN: DON O'MARA
CHEMICAL PRESERVATION
TYDROTECH
.O. BOX 4602
A
A
A
A
A
A
A
IMEIZALD ISLE NC 28594
g
A -NONE D-NAOH
t52) 725 2319
z L
w
L
CO
C B- HNO E. HCL
0 0
rc
Uj
z
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0
O
`�
c
a
C- HxSO, F- ZINC ACETATEINAOH
COLLECTION
_, ¢
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LU J
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W e
C
n.
4
�-
`'
G- NATHIOSULFATE
SAMPLELOCAT10N
DATE
TIME
Sludge Sample
CLASSIFICAT10N,
WASTEWATER(NPDES)
L] DRINKINGWATER
❑ DWR/(3W
USOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SHIPMENT/DELIVERY
0 N
SAMPLES COLLECTED BY:
(Please Prim)
SAMPLES RECEIVED IN LAB AT
RELINQUISHED BY SIG.) (SAMPLER)
DATEITIME
RE IVED BY (SIG.)
ATFJTIME
COMMENTS:
1 3 1�
RELINQUI HED BY (SIG.)
DATEMME
RECEIVED BY (SIG,)
DATEMNIE
RELINQUISHED BY (SIG,)
DATFITIME
RECEIVED BY (SIG.)
DATIDTIME
PLEASE MEAD Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "Gn for No 5995��
FORM .; Grab sample in the blocs above for each parameter requested.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: March 29, 2022
Permit No. WQ0018525
Harker's Point 0,97 % Solids
12.20 pH (Taken from Lime Stabilization)
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
6.607
66,070.000
132A40
Phosphorus
1.537
15,370.000
30.740
Potassium
0.495
4,954.000
9.908
PAN (injected)*
2.011
20,113,280
40.227
PAN (surface)*
1.994
I9,938.030
39.876
Ammonia Nitrogen
0.035
350.500
0.701
Calcium
1,836
18,358.000
36.716
Calcium Carbonate E .
---
---
---
Magnesium
---
3,187.000
6.374
Sodium
---
21,764.000
43.528
Sulfur
---
___
Nitrate N / Nitrite N
---
46.930
0.094
Barium
---
Chloride
---
--_
_..
Iron
---
---
Aluminum
---
3259.000
6.518
Arsenic
---
2.50
0.005
Cadmium
---
1.20
0.002
Chromium
---
15.000
---
Co er
---
529.00
1.058
Lead
---
22.00
0.044
�4ercury
0.04
0.000
Ao[ bdenum
---
5.00
0.010
Vickel
---
11.00
0.022
Selenium
---
5.00
0.010
7-inc
---
1,849.00
3.698
Environment 1, Incorporaled 95S
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SA R
3.83
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

EflWoT@fiffW % hmpr ghd
114 OAKMONT DRIVE
GREET'WILLE. N.C. 27856
HARKER'S POINT SUBDIVISION(FORTIN)
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE, NC 28594
PARAMETERS
Aluminum, (dry wt. basis), mglkg
Arsenic (dry wt. basis), mglkg
Calcium (dry wt. basis), mg/lig
Cadmium (dry wt. basis), mglkg
Copper (dry wt. basis), mg/lig
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mgflig
Nickel (dry wt, basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
3259
04/18/22
LFJ
EPA200.7
<2.5
04/13/22
MTM
311313-04
18358
04/18/22
LFJ
EPA200.7
1.2
04/14/22
MTM
311313-04
529
04/18/22
LFJ
EPA200.7
15
04/18/22
LFJ
EPA200.7
22
04/12/22
MTM
3113E-04
3187
04/18/22
LFJ
EPA200.7
<0.04
04/18/22
MTM
EPA7471B
11
04/18/22
LFJ
EPA200.7
4954
04/18/22
LFJ
EPA200.7
<5.0
04/20/22
MTM
3113E-04
21764
04/18/22
LFJ
EPA200.7
1849
04/18/22
LFJ
EPA200.7
0.97
03/31/22
BLV
2540G15
c 66070
04/13/22
BMD
351.2 R2-93
c 350.5
04/01/22
TRJ
350.1 R2-93
c 15370
04/13/22
TRJ
365.4-74
c 46.93
04/01/22
BMD
353.2 R2-93
26510
04/22/22
KES
<5.0
04/18/22
LFJ
EPA200.7
Drinking Water ID: 37715
Wastewater sae 10
PHONE [phone]
FAX [phone]
ID#: 95 S
DATE COLLECTED: 03/29/22
DATE REPORTED : 04/27/22
REVIEWED BY:��,�
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

Er�rirnnmet�t 1. Irac. CHAIN OF CUSTODY RECORD
P.O. Box 7085, 114 Oakmont Dr. Page I of
Greenville. NC 27858
envil-onment I inc.com
DISINFECTION
Phone [phone] . Fax [phone]
CHLORINE NEU IRALEEDATCOLLECTION
CHLORINE
pH CHECK (LAB)
CLIENT: 95 S Week: 10
t_rV
F
CONTAINER TYPE, P1G
HARKER'S POINT SUBDIVISION(FORTIN)
NONE
MR. DAN FORTIN
L j
FORTIN CONTRACT SERVICES
P.O. BOX 4188
CHEMICALPRESERVAT ION
EMERALD ISLE NC 28594
�'
c z
A - NONE 0 - NAOH
[phone]
i
�
.�
cn
w
B HNO, E HCL
a_
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¢ o
¢
z
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Uj
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C - H fSO, F - ZINC ACETATEfNAOH
w
COLLECTION
or Ir o
w -J
a- o
�"- ¢
4
N
�'
< G - NATHIOSULFATE
SAMPLE LOCATION
DATE
TIME
Sludge Sample
):.. ` -�<
4
CLASSIFICATION:
Cis WASTEWATER (NPDES)
DRINKING WATER
l DWRIGW
SCUD WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAENED
DURING S IPMENTJDELIVERY
Y N
SAMPLES CO TED BY:
(Please Print)
SAMPLES RECEIVED IN LAB AT °C
RELINQUISHED BY (SIG.) (SAMPLER)
;. ?DATEITI�Ir
R EIVED BY (SIG.)
DATEffIME
COMMENTS:
22�
/
RELINQUISHED BY (SIG..)
DATErnME
RECEIVED BY (SIG.)
DATErrIME
RELINQUISHED BY (SIG.)
DATE ME
RECEIVE{ BY (SIG.)
DATEInME
PLEASE READ Instructions for completing this form Dn the reverse side. Sampler must place a T" for composite sample or a "G' for /�
FORM 45 Grab Sample in the biocks above for each parameter requester(. N 40652

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: April 28, 2022
Permit No. WQ0018525
Kin sbrid a II 1.30 % Solids
7.00 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,D00)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
6.022
60,220.000
120.440
Phosphorus
1.366
13,660.000
27.320
Potassium
0.262
2,619.000
5.238
PAN (injected)*
1.838
18,384.240
36.768
PAN (surface)*
1,817
18,174.740
36.349
Ammonia Nitrogen
0,042
419.000
0,838
Calcium
2.309
23,085.000
46.170
Calcium Carbonate E .
---
Magnesium
---
1,686.000
3.372
Sodium
---
8,046.000
16.092
Sulfur
___
...
---
Nitrate N / Nitrite N
---
24.940
0.050
Barium
---
---
---
SAR
1.57
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
7559.000
15.118
Arsenic
---
2.50
0.005
75
Cadmium
---
2.00
0.004
85
Chromium
---
23.000
---
---
Copper
- -
283.00
0.566
4,300
Lead
---
28.00
0.056
840
Mercury
---
0.36
0.001
57
Molybdenum
---
5.00
0.010
75
Nickel
---
13.00
0.026
420
Selenium
---
5.70
0.011.
100
Zinc
---
4,313.00
8.626
7,500
Environment 1, Incorporated 216
*Determination of Plant Available Nitrogen (PAIN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

Ewuhnifugml T, hmp fflUd
04 OAKMONT DRIVE
GREENVILLE. N.C. 27858
KINGSBRIDGE (FORTIN)
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE, NC 26594
PARAMETERS
PH, Units (Non -Aqueous)
Alumintim, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry cvt. basis), mg/icg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/Icg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt, basis), mg/ki;
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/lcg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mglkg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), rag/kg
Sludge Analysis Method
Sample Date Analyst Code
c 7.0
05/02/22
DNS
4500HB-11
7559
05/04/22
LFJ
EPA200.7
C2.5
05/04/22
MTM
31131E-04
23085
05/04/22
LFJ
EPA200.7
2.0
05/06/22
MTM
311313-04
283
05/04/22
LFJ
EPA200.7
23
05104/22
LFJ
EPA200.7
28
05/04/22
MTM
3113B-04
1686
05/04/22
LFJ
EPA200.7
0.36
05112122
MTM
EPA7471B
13
05/04/22
LFJ
EPA200.7
2619
05/04/22
LFJ
EPA200.7
5.7
05/05/22
MTM
3113E-04
8046
05/04/22
LFJ
EPA200.7
4313
05/04/22
LFJ
EPA200.7
1.30
04/28/22
HCE
2540G15
c 60220
05/03/22
BMD
351.2 112-93
c 419.0
05/02/22
BMD
350.1 112-93
c 13660
05/03/22
KES
365.4-74
c 24.94
05/03/22
TRJ
353.2 112-93
C 5.0
05/04/22
LFJ
EPA200.7
Drinking Water ID: 37715
Wastewater ID: 10
PHONE [phone]
FAX [phone]
ID#; 216
DATE COLLECTED: 04/28/22
DATE REPORTED : 05/16/22
REVIEWED BY:
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

Envirottntent 1, Inc.
CHAIN
OF
CUSTODY
RECORD
P.O. Box 7085. 114 Oakmont Dr.
1 1
Greenville, NC 27858
Page of
environmeutl inc-corn
DISINFECTION
Phone [phone] • Fax [phone]
NEUTRALIZED AT COLLECTION
CHLORINECHLORINE
L
CHECK (LAB)
CLIENT: 216 Week: 10
Ij UV
P
P
P
P
P
P
P
CONTAINER TYPE, PIG
HINGSBRIDGE (FORTIN)
Ij NONE
MR. DAN FORTIN
CHEMICAL PRESERVATION
FORTIN CONTRACT SERVICES
Ij
P.O. BOA 4188
A
A
A
A
A
A
A
EMERALD ISLE NC 28594
za z
E O
"' A -NONE D-NAOH
[phone]
uj 15
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DATE
TTIME
o_
%'�
}-`
Sludge Sample
$
.
a
CLASSIFICATION:
WASTEWATER(NPDES)
UDRINKING WATER
Ij DWRiGW
L] SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SHIPMENT/DELIVERY
U N
SAMPLES COLLECTED BY-
ea- _ Print)
LN I PY N
SAMPLES RECEIVED IN LA13 AT I C
R tJ OUISHEfl BY 1G.) (fi MPLER)
DATEriIME
R EIUED BY (SIG.)
DATP1TlME
COMMENTS:
R LINQUISHED BY IG.J
DATEMME
RECEIVED BY (SIG.)
DATEMME
BY (SIG.) I L}Ak EJ 1 IME I RECEIVED BY (SIG.)
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G" for �° 399824
FORM #s Grab sample in the blocks above for each parameter requested.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 8, 2022
Permit No. WQ0018525
McGinnis Point 1.49 % Solids
7.3 aH
Parameter
%
Mg/Kg Dry Weight
PoundslDry Ton
(% x 10,000)
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
6.349
63,490.000
126.980
Phosphorus
2.462
24,620,000
49.240
Potassium
0.208
2,079.000
4.158
PAN (injected)*
1.944
19,439.550
38.879
PAN (surface)*
1.918
19,179.850
38.360
Ammonia Nitrogen
0.052
519.400
1.039
Calcium
3.992
38,921.000
77.842
Calcium Carbonate E .
---
---
---
Magnesium
---
2,792.000
5.584
Sodium
---
16,406.000
32.812
Sulfur
--_
__-
Nitrate N / Nitrite N
---
28.970
0.058
Barium
---
--_
---
SAR
2.64
Chloride
---
___
---
Iron
---
---
CeilingConcen.
(Mg/Kg)
Aluminum
---
5,131.00
10.262
Arsenic
---
2.90
0.006
75
Cadmium
---
0.56
0.001
85
Chromium
---
27,000
---
-.-
Copper
---
1,448.00
2.896
4,300
Lead
---
22.00
0.044
840
Mercury
---
0.45
0.001
57
Molybdenum
---
8.00
0.016
75
Nickel
---
11.00
0,022
420
Selenium
---
5.90
0.012
1 100
Zinc
---
1,361.00
2.722
7,500
Environment 19 555 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + ,Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

EAUTmEW % hmpQmbdo
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
MCGINNIS POINT (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE, NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mgllcg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/Icg
Copper (dry wt. basis), niglkg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), u1g/kg
Mercury (dry wt, basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mgllcg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mglkg
Phosphorus, T. (dry wt.), nig/kg
Nitrate-+-N€trite (dry wt.), mglIcg
Molybdenum (dry wt. basis), mgllcg
Sludge Analysis Method
Sample Date Analyst Cade
7.3
02/08/22
CAW
45001-fB-11
5131
02/22/22
LFJ
EPA200.7
2.9
02/23/22
MTM
3113B-04
38921
02122122
LFJ
EPA200.7
0.56
02/22/22
MTM
3113B-04
1448
02/22/22
LFJ
EPA200.7
27
02/22/22
LFJ
EPA200.7
22
02/24/22
NITM
3113E-04
2792
02/22/22
LFJ
EPA200.7
0.45
02/23/22
MTM
EPA7471 B
II
02/28/22
LFJ
EPA200.7
2079
02/22/22
LFJ
EPA200.7
5,9
02/24/22
MTM
3113B-04
16406
02/22/22
LFJ
EPA200.7
1361
02/22/22
LFJ
EPA200.7
I.49
02/08/22
JMS
254OG-15
c 63490
02/11/22
TRJ
351.2 R2-93
c 519.4
02/15/22
BMD
350.1 R2-93
c 24620
02/11/22
KES
365.4-74
c 28.97
02/14122
BMD
353.2 R2-93
8
02/22/22
LFJ
EPA200.7
Drinking water IDi 37715
want awater ID: 10
PHONE [phone]
FAX [phone]
ID)#: 555 A
DATE COLLECTED: 02/08/22
DATE REPORTED : 03/02/22
REVIEWED BY: _ f+
c uncartified data. DwR does not offer non -aqueous certification for this analytical procedure.

M
A
H
P
E
(2
Environment 1.Ine.
P.O. Box 7085, 114 Oakmont Dr.
(,raanvillr1\Tf' 7i521R
CHAIN OF CUSTODY RECORD
Page 1 of I
environment 1 ine.com
DISINFECTION
CHLORINE NEUTRALIZED AT COLLECTION
Phone [phone] • Fax [phone]
'
CHLORINE
CLIENT: 555 A Week: 9
Ij UV
pH CHECK (LAB)
CGINTNIS POINT (HYDROTECH)
INTONE
P
P
P
P
P
P
P
CONTAINERTYPE. P!G
ITN: DON O'MARA
YDROTECH
CHEMICAL PRESERVATION
O. BOX 4602
A
A
A
A
A
A
A
VIERALD ISLE NC 28594
A NONE D NAOH
o
52) 725-2319
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CD
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SAMPLELOCATION
DATE
TIME
Sludge Sample
l
v
CLASSIFICATION:
WASTEWATER (NPDES)
DRINKING WATER
DWRIGW
SOl1D WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING S MENT/DELIVERY
Y N
SAMPLES COLLECTED BY:
(P ase Prtni)
4LAB
SAMPLES RECEIVED IN ATQ — � —G
RELIN UISH D BY (SIG.) (SAMPLER)
DATEI VIE
RECEIVE BY (SIG?
DATET1 N E
COMMENTS:
0 ,
Zlwyez j 3, z.s
REUNQU SHED BY (SIG.)
DATEMME
RECEIVED BY (SIG.)
DATEMME
RELINQUISHED BY (SIG.)
DATEMME
RECEIVED BY (SIG.)
DATEMME
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G" for �0 399589
FORM „; Grab sample in the blocks above for each parameter requested.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: August 18, 2022
Permit No. WQ0018525
NC Aquarium at Pine 1.85 % Solids
Knoll Shores 12.4 pH (taken from lime stabilization event)
Parameter
%
Mg/Kg Dry WeljiFT
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
5.247
52,470.000
104.940
Phosphorus
2.529
25,290.000
50.580
Potassium
0.552
5,516.000
11.032
PAN (injected)*
1.680
16,802.390
33.605
PAN (surface)*
1.605
16,051.390
31103
Ammonia Nitrogen
0.150
1,502.000
3.004
Calcium
5.403
54,030.000
108.060
Calcium Carbonate E .
---
---
Magnesium
---
8,934.000
17.869
Sodium
---
53,295.000
106.590
Sulfur
---
---
---
Nitrate N / Nitrite N
---
9.990
0.020
Barium
---
---
---
SAR
7.59
Chloride
--
---
---
Iron
---
---
---
Ceiling Concert.
(M /K )
Aluminum
---
1,859.00
3.718
Arsenic
---
2.50
0.005
75
Cadmium
---
8.40
0.017
85
Chromium
---
24.000
---
---
Copper
---
385.00
0,770
4,300
Lead
---
26.00
0.052
840
Mercury
---
0.11
0.000
57
Molybdenum
---
13.00
0.026
75
Nickel
---
25.00
0.050
420
Selenium
---
5.00
0.010
100
Zinc
---
1,053.00
2.106
7,500
Environment 1 # 444 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

RMAnfin( % hcwpoOTMUd
114 OAKIAONT DRIVE
GREEIIVILLE. N.C. 27B58
NC AQUARIUM AT PINE KNOLL SHORES
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE, NC 28594
PARAMETERS
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium. (dry wt. basis), mg/Iig
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/lig
Magnesium (dry wt. basis), mg/lig
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TIN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/leg
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
1859
09/20/22
MTM EPA200.7
C2.5
09/20/22
MTM 3113E-04
54030
09/06/22
MTM EPA200.7
8.4
09/20/22
MTM 3113E-04
385
09/06/22
MTM EPA200.7
24
09/06/22
MTM EPA200.7
26
09/20/22
MTM 311313-04
8934
09/06/22
MTM EPA200.7
0.11
09/07/22
MTM EPA7471B
25
09/06/22
MTM EPA200.7
5516
09/06/22
MTM EPA200.7
[5.0
09/21/22
MTM 3113E-04
53295
09/06/22
MTM EPA200.7
1053
09/06/22
MTM EPA200.7
1.85
08/23/22
JMS 2540G-15
c 52470
08/23/22
TRJ 351.2 R2-93
c 1502
08/24/22
KES 350.1 R2-93
c 25290
08/23/22
BMD 365.4-74
c 9.99
08/25/22
KMS 353.2 112-93
16051
08/29/22
KES
13
09/06/22
MTM EPA200.7
Drinking Water ID: 3771s
Wastewater IDz 10
PHONE [phone]
FAX [phone]
ID#: 444 A
DATE COLLECTED: 08/18/22
DATE REPORTED : 09/22/22
REVIEWED 8Y:
c uncertified data. DNA does not offer non -aqueous certification for this analytical procedure.

Environment 1, Inc. CHAIN OF CUSTODY RECORD
P.O. Box 7085, I14 Oakmont Dr.
Greenville. NC 27858 Page 1 of
er=v i ro ninent 1 ine.com
DISINFECTION
Phone [phone] e Fax [phone]
CHLORINE NEUTRALIZED AT COLLECTION
Ij CHLORINE
y
pH CHECK (LAB)
CLIENT: 444 A Week: 9
UV
C AQUARIUM AT PINE KNOLL SHORES
NONE
p
p
p
p
p
p
CONTAINER TYPE, PIG
[R. DAN FORTIN
CHEMICAL PRESERVATION
ORTIN CONTRACT SERVICES
.O. BOX 4188
A
A
A
A
A
A
MERALD ISLE NC 28594
z
o
ELj
A -NONE D-NAOH
52) 393-8720
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co
=
=
w
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C • H=SO, F - ZINC ACETATE/NAOH
COLLECTION
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G- NATHIOSULFATE
SAMPLE LOCATION
DA
TIME
Sludge Samplers
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4
.:
CLASSIFICATION:
WASTEWATER(NPDES)
DRINKINGWATER
DWFIIGW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SHIPMENT/DELIVERY
N
SAMPLES COLLECTED BY.
(PI Print)
SAMPLES RECEIVED IN LAB AT:3b___°C
RELIN ED '. SA PLE
��TEITt c -17
ECEIV BY (SIG
DATEMME
COMMENTS:
�
(
l! zz 3`5Z
RELIN UISH D BY (SIG.)
DATEtrIME
RECEIVED BY (SIG.)
DATEl11ME
RELINQUISHED BY (SIG.)
DATE/TIME
RECEIVED BY (SIG.)
DATEIi1ME
PLEASE READ [nstructions for completing this form on the reverse side. Sampler must place a "C° for composite sample or a "G" for N° 399625
FORM P-s Grab sample in the blocks above for each parameter requested,

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: April 28, 2022
Permit No. WQ0003067
Ocean Bav Villas 0.43 % Solids
12.45 pH (taken from lime stab.)
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg�Eg x 0.002)
Nitrogen (TKN)
5.545
55,450.000
110.900
Phos horus
1.069
10,690.000
21.380
Potassium
0.382
3,821.000
7.642
PAN (injected)*
1.728
17,279.751
34.560
PAN (surface)*
1.725
17,254.286
34.509
Ammonia Nitrogen
0.005
50.930
0,102
Calcium
3.600
35,998.000
71.996
Calcium Carbonate E .
---
---
---
Magnesium
---
2,852.000
5.704
Sodium
---
19,927.000
39.854
Sulfur
---
---
---
Nitrate N / Nitrite N
---
609.100
1.218
Barium
---
---
---
SAR
1.78
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
4,144.00
-[
8.288
Arsenic
---
2.50
0.005
75
Cadmium
---
1.20
0.002
85
Chromium
---
16.000
---
---
Copper
---
287.00
0.574
4,300
Lead
---
27.00
0.054
840
Mercury
---
0.42
0.001
57
Molybdenum
---
5.00
0,010
75
Nickel
---
12.00
0.024
420
Selenium
--- 1
5.00
0.010
100
Zinc
---
1,290.00
2.580
7,500
Environment 19 442 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitratc N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

Nin'Umflum Ala WaTpuMd
11/1, OAKIv1ONT DRIVE
GREENVILLE, N.C. 27858
C&P ENTERPRISES (FORTIN)
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. SOX 4188
EMERALD ISLE, NC 28594
PARAMETERS
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/ltg
Capper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mglkg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/lig
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Sodium Adsorption Ratio (calc)
Total Solids,
TKN (dry wt.), mg/lcg
Ammonia Nitrogen (dry wt.),mglkg
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry riot.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
4144
05/04/22
LFJ
EPA200.7
C 2.5
05/04/22
MTM
3113B-04
34998
05/04/22
LFJ
EPA200.7
1.2
05/06/22
MTM
3113E-04
287
05/04/22
LFJ
EPA200.7
16
05/04/22
LFJ
EPA200.7
27
05/04/22
MTM
3113E-04
2852
05/04/22
LFJ
EPA200,7
0.42
05/12/22
MTM
EPA7471B
12
05/04/22
LFJ
EPA200.7
3821
05/04/22
LFJ
EPA200.7
C 5.0
05/05/22
MTM
3113B-04
19927
05/04/22
LFJ
EPA200.7
1290
05/04/22
LFJ
EPA200.7
27.5
0.43
04/28/22
HCE
254OG-15
c 55450
05/03/22
BMD
351.2 R2-93
c 50.93
05/02/22
BMD
350.1 R2-93
c 10690
05/03/22
KES
365.4-74
c 609.1
05/03/22
TRJ
3512 R2-93
C 5.0
05/04/22
LFJ
EPA200.7
Drinking water ID: 37715
wastewater ID: 10
PHONE [phone]
FAX [phone]
ID#: 442 A
DATE COLLECTED: 04/28/22
DATE REPORTED : 05/19/22
REVIEWED BY:
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure,

Environment 1, Inc.
P.O- Box 7085, 114 Oakmont Dr.
Greenville, NC 27958
CHAIN OF CUSTODY RECORD
environment 1 inc.com
DISINFECTION
Phone [phone] • Fax [phone]; i
CHLORINE
CLIENT: 442 A Week- 10
UV
P
P
P
P
P
P
C&P ENTERPRISES (FORTIN)
NONE
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
A
A
A
A
A
A
A
EMERALD ISLE NC 28594
o
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[phone]
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COLLECTION
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SAMPLE LOCATION
DATE
TIME
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BY (SIG.) I DATEMME I RECEIVED
BY (SIG.) I DAI FJTIME I RECEIVED BY (SIG.)
FOFiM 45 PLEASE READ Instructions for completing this form on the reverse side.
Pate
CHLORINE NEUTRALIZEDAT COLLECTION
pH CHECK (LAB)
CONTAINER TYPE, PIG
CHEMICAL PRESERVATION
A -NONE D-NAOH
LU
B-HNO; E-HCL
LU
w C- H,SO, F - ZfNC ACETATE/NAOH
G - NA THIOSULFATE
ii
CLASSIFICATION:
WASTEWATER(NPDES)
DRINKING WATER
Ij DWRIGW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING PMENTIDELIVERY
Y N
SAMPLES C TED BY:
(Plea 6 ,
SAMPLES RECEIVED IN LAB AT IC
COMMENTS:
Sampler must place a "C"for composite sample or a "G" for �° 399773
Grab sample in the blocks above for each parameter requested,

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 17, 2022
Permit No. WQ0018525
Ocean Club 0.68 % Solids
12.1 1pH (taken from lime stabilization event)
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
6.033
60,330.000
120.660
Phosphorus
2.420
24,200.000
48.400
Potassium
0.868
8,680.000
17.360
PAN (injected)*
1.921
19,206.070
38.412
PAN (surface)*
1.842
18,40.570
36.839
Ammonia Nitrogen
0.157
1,573.000
3.146
Calcium
3.014
30,139.000
60.278
Calcium Carbonate E .
---
---
Magnesium
---
4,269.000
8.538
Sodium
---
25,920.000
51.840
Sulfur
---
-_.
Nitrate N / Nitrite N
---
5.970
0.012
Barium
---
---
---
SAP.
3.05
Chloride
---
___
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
1,736.00
3.472
Arsenic
---
2.50
0.005
75
Cadmium
---
0.57
0.001
85
Chromium
---
8.000
---
---
Copper
---
282.00
0.564
4,300
Lead
---
7.30
0.015
840
Mercury
---
0.21
0.000
57
Molybdenum
---
6.00
0.012
75
Nickel
---
9.00
0.018
420
Selenium
---
5.00
0.010
100
Zinc
---
1,387.00
2.774
7,500
Environment I # 404 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection Iimits are listed as detection limits
for calculation purposes.

ERWO OMEM 10 Mmprmud
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
OCEAN CLUB (FORTIN)
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE, KC 28594
PARAMIJTERS
Aluminum, (dry wt. basis), mg/lig
Arsenic (dry wt. basis), mg/lig
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt, basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/lig
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonin Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (day wt.), mg/kg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analy51 Code
1736
02/22/22
LFJ
EPA200.7
C2.5
02/23/22
lvlTrvl
3113E-04
30139
02/22/22
LFJ
EPA200.7
0.57
02/22/22
MTM
3113B-04
282
02/22/22
LFJ
EPA200.7
8
02/22/22
LFJ
EPA200.7
7.3
02/24/22
MTM
3113B-04
4269
02/22/22
LFJ
EPA200.7
0.21
03/14/22
MTM
EPA7471B
9
02/28/22
LFJ
EPA200.7
8680
02/22/22
LFJ
EPA200.7
C 5.0
02/24/22
MTIM
31138-04
25920
02/22/22
LFJ
EPA200.7
1387
02/22/22
LFJ
EPA200.7
0.68
02/17/22
JMS
254OG-15
c 60330
02/22/22
BNID
351.2 R2-93
c 1573
02121/22
KES
350.1 R2-93
c 24200
02/22/22
TRJ
365.4-74
c 5.97
02/22/22
KES
353.2 R2-93
18420
03/18/22
KES
6
02/22/22
LFJ
EPA200.7
Drinking Water ;D1 37115
Wastewater IDs 10
PHONE [phone]
FAX [phone]
ID#: 404 A
DATE COLLECTED: 02/17/22
DATE REPORTED : 03/21/22
REVIEWED BY:
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

EavironnIent I, InC. CHAIN OF CUSTODY RECORD
P.O. E ox 7085. 114 Oakmont Dr. Paee I of I
NiC 17R5R
en v iroimiie nt I i nc.com
DISINFECTION
CHLORINE NEUTRALIZED AT COLLECTION
Phone [phone] • Fax [phone]
CHLORINE
CLIENT: 404 A Week: 9
pH CHECK (LAB)
U1
P
P
P
P
P
P
CONTAiNERTYPE, PIG
CEAN CLUB (FORTIN)
LNONE
R. DAN F•ORTIN
DRTIN CONTRACT SERVICES
CHEL4ICALPRESERVAT10N
.0. SOX 4188
A
A
A
A
A
A
VIERALD ISLE NC 28594
A - NONE D - NAOH
—
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52) 393-8720
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=
C B HNO: E HCL
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COLLECTION
m
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0.
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a
SAMPLE LOCATION
DATE
TIME
°2
r
Sludge Sample
4BEG&
CLASSIFICATION:
WASTEWATER(NPDES)
DRINKING WATER
DWR/GW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURINGHIPMENT/DELIVERY
Y� N
SAMPLES COLLECTED BY:
(Please Prid)l f
SAMPLES RECEIVED IN LAB AT r f,
RELI ISHED BY (SI ) ( )
DrAJTEErnME
REC ED BY (SiG.)
COMMENTS:��
y�/�
L[ W
(�/}/� %DAATE(I'i//M}E
/ // U Li
DATEMME
RE QUISHED 6Y (51 .
DATEMME
A EIVED BY (SfG.)
9EL4\0UISHED BY (SIG.)
DATFJT N E
RECEIVED BY (SIC,)
DATET1ME
PLEASE REAR instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G" for NQ 399637
FORM 05 Grab sample in the block above for each parameter requested.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 15, 2022
Permit No. WQ0018525
Oceans Condominiums 1.66 % Solids
7.1 VH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(MgfKg x 0.402)
Nitrogen (TKN)
0.330
72,980.000
145.960
Phosphorus
0.266
15,180.000
30,360
Potassium
0.504
5,501,000
11.002
PAN (injected)*
0.118
1,184.360
2.369
PAN (surface)*
0.105
1,049.860
2.100
Am mo n is N itrogen
0.027
1,162.000
2.324
Calcium
5.876
16,182.000
32.364
Calcium Carbonate E .
---
---
Magnesium
0.4I8
2,949.000
5.898
Sodium
---
10,105.000
20.210
Sulfur
Nitrate N / Nitrite N
---
6.960
0.014
Barium
---
---
---
SA R
2.46
Chloride
---
---
--
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
I,552.00
3.104
Arsenic
Cadmium
Chromium
Copper
Lead
Mercury
---
---
---
---
---
---
2.50
0.84
6.000
494.00
15.00
0.17
0.005
0.002
---
0.988
0.030
0.000
75
85
---
4,300
840
57
Molybdenum
Nickel
Selenium
Zinc
---
---
---
---
5.00
10.00
5.00
1,163.00
0.010
0.020
0.010
2.326
75
420
100
7,500
Environment i # 566 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
(Vote: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

EmhungfiSR �' hcmpm mNd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
OCEANS CONDOMINIUMS (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE, NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/Icg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), nig/lcg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mgllcg
Chromium, T.(dry wt, basis),mg/kg
Lead (dry weight basis), mg/Icg
Magnesium (dry wt. basis), mgllcg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mgllcg
Total Solids, TD
TKN (dry wt.), mg/kg
Annnonin Nitrogen (dry wt.),mg/Icg
Phosphorus, T. (dry ►vt.), mg/kg
Nitrate+Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
7A
02/15/22
JMS
4500HB-11
1552
02/22/22
LFJ
EPA200.7
2.5
02/23/22
MTM
3113B-04
16182
02122122
LFJ
EPA200.7
0.84
02/22/22
MTM
3113B-04
494
02/22/22
LFJ
EPA200.7
6
02/22/22
LFJ
EPA200.7
15
02/24/22
MTM
31I3B-04
2949
02/22/22
LFJ
EPA200.7
0.17
02/23/22
MTM
L-PA7471B
10
02/28/22
LFJ
EPA200.7
5501
02/22/22
LFJ
EPA200.7
[5.0
02/24/22
MTM
311311-04
10105
02/22/22
LFJ
EPA200.7
1163
02/22/22
LFJ
EPA200.7
1.66
02/16/22
JMS
254OG-15
c 72980
02122/22
BMD
351.2 R2-93
c 1162
02/21/22
KES
350.1 R2-93
c I5180
02/22/22
TRJ
365.4-74
c 6,96
02/22/22
ICES
353.2 R2-93
5
02/22/22
LFJ
EPA200.7
Drinking Water ID: 377Is
Wastewater IDS 10
PHONE [phone]
FAX [phone]
ID#: 566 A
DATE COLLECTED: 02/15/22
DATE REPORTED : 03/02/22
REVIEWED BY:
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure,

C
A
I�
P
E
G
Environment 1, Inc.
P.O. Box 7095, I14 Oakmont Dr.
Greenville_ NC 77952
GRAIN OF CUSTODY RECORD
Pa-e I of I
environmentlinc.cotn
DISINFECTION
Phone [phone] - Fax [phone]
CHLORINE NEUTRALIZED AT COLLECTION
CHLORINE
CHECK (LAB)
CLIENT: 566 A Week. 8
UVpH
P
p
P
P
P
P
P
CONTAINERTYPE, PIG
CEANS CONDONJINILINIS (RYDROTECH)
ONE
ITN: DON O'MARA
YDROTECH
,O. SOX 4602
A
A
A
A
A
JA
A
CHEMICAL PRESERVATION
NAERALD ISLE NC 28594
c z
E
A NONE D NAOH
52) 725-2319
J
a
w
B -HNO, E-HCL
in �
�
O
c
ro
�
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t
w
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+
C- H2S0,, F - ZINC ACETATEINAOH
's'
COLLECTION
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¢
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=
4
R
F
E"
°
Q
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;r
z
G-NATHIOSULFATE
a
SAMPLE LOCATION
DATE
TIME
Sludge Sample
5`
' n
?'
l
�.�
CLASSIFICATION:
WASTEWATER(NPDES)
Lj DRINKINGWATER
DWRIGW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SHIPMENT/DELIVERY
Y N
SAMPLES COLLECTED BY:
(Please Print)
MAPLES RECEIVED IN LAB AT
RELINQUISHED BY (SIG.) (SAMPLER)
DATEiT1ME
RECEIVED BY (SIG.)
DATETIME
COMMENTS:
0-t —
0)
R NQUI5HED BY (SIG.)
DA"IFJTIME
RECEIVED Rf (SIG.)
DATEMME
RELINQUISHED BY (SIG.)
DATFJTIME
RECEIVED BY (SIG.)
DATFJTIME
PLEASI PI AD InStrLICt10f15 fOr COrRpleting ti115 form OfI the reVEr52 51[€e. Sampler must place a "C" for composile sample or a "G" for n
FORM +1s — — Grab sample in the blocks above for each parameter requested. N- 4 00139

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: March 15, 2022
Permit No. WQ0018525
Pebble Beach 1.34 % Solids
6.4 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000}
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
6.565
65,650.000
131.300
Phosphorus
0.855
8,551.000
17.102
Potassium
0.259
2,588.000
5.176
PAN (injected)*
2.107
2,464.097
4.928
PAN (surface)*
2.009
2,435.542
4.871
Ammonia Nitrogen
0.196
1,955.000
3,910
Calcium
1.406
14,060.000
28.120
Calcium Carbonate Eq.
---
---
---
Magnesium
---
2,266.000
4.532
Sodium
---
5,935.000
I L870
Sulfur
Nitrate N / Nitrite N
---
7.940
0.016
Barium
---
___
---
SA R
1.41
Chloride
Iron
---
---
---
---
---
---
Ceiling Concen.
(M /K )
Aluminum
---
3,709.000
7.418
Arsenic
Cadmium
Chromium
---
---
---
2.50
1.20
13.000
0,005
0.002
---
75
85
---
Copper
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
---
---
---
---
---
---
---
303.00
16.00
0.26
5.00
7.00
5.00
2,227.00
0.606
0.032
0.001
0.010
0.014
0.010
4.454
4,300
1 840
57
75
420
1 100
7,500
Environment I # 287A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0,5)(Ammonia N) +Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

% hmpoTmUd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
PEBBLE BEACH (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE, NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt- basis), mg/lcg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry ivt. basis), mglkg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry W. basis), mg/kg
Potassium (dry wt. basis), mg/lig
Selenium (dry Avt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mglkg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mglkg
Nitrate+Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Nlethod
Sample Date Analyst Code
6.4
03/15/22
DU
45001FIB-11
3709
03130/22
LFJ
EPA200.7
<2.5
03/30/22
MTM
3113E-04
14060
03/30/22
LFJ
EPA200.7
1.2
03/31/22
MTM
3113B-04
303
03/30/22
LFJ
EPA200.7
13
03/30/22
LFJ
EPA200.7
16
03/29/22
MTM
3113E-04
2266
03/30/22
LFJ
EPA200.7
0.26
03/30/22
MTM
EPA7471B
7
03/30/22
LFJ
EPA200.7
2588
03/30/22
LFJ
EPA200.7
<5.0
03/31/22
MTNI
3113B-04
5935
03/30/22
LFJ
EPA200.7
2227
03/30/22
LFJ
EPA200.7
1.34
03/15/22
JMS
2540G-15
c 65650
03/22122
BMD
351.2 112-93
c 1955
03/26/22
KES
350.1 R2-93
c 8551
03/22/22
TRJ
365.4-74
c 7.94
03/21/22
KES
353.2 R2-93
20094
04/01/22
KES
<5.0
03/30/22
LFJ
EPA200.7
Drinking Water ID: 37715
Wastewater ID: 10
PHONE [phone]
FAX [phone]
ID#: 287 A
DATE COLLECTED: 03/15/22
DATE REPORTED : 04/04/22
REVIEWED BY:
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

PI
A'
fi
P.
EI
%:ivironment I, Inc. CHAIN OF CUSTODY RECORD
P.D. Box 7085. 114 Oakmont Dr. PatTe 1 of I
Greenville. NC 27858 `
environment 1 inc.com
DISINFECTION
Phone [phone] • Fax [phone]
CHLORINENEUTRALIZEDATCOLLECTION
CHLORINE
pH CHECK (LAB)
CLIENT: 287 A Week: 8
UV
P
P
P
P
P
P
P
CONTAINER TYPE. PIG
3BBLE BEACH (HYDROTECH)
NONE
rTN. DON O'MARA
CHEMICALPRESERVATION
YDROTECH
O. BOX 4602
A
A
A
A
A
A
A
VIERALD ISLE NC 28594
E Q
El) A -NONE D-NAOH
52) 725-2319
z w
z
Q
12
LU
� B-HNO E-HCL
op
a
=1g
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1U
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C - H,SO, F - ZINC ACETATEINAOH
COLLECTION
¢
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H'
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C,
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7
0.
< G - NATHIOSULFATE
SAMPLELOCATION
DATE
TIME
5
��
Y
f Y;
$
?/
;
�
fFy
�
ff
Sludge Sample
�
>_
GLASSIFlCATION:
STEWATER (NPDES)
DRINKING WATER
DWRIGW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING �5H1�MENTJDELIVERY
Y 1 N
SAMPLES COLLECTED BY:
(Pease 'nt)
SAMPLES RECEIVED IN LAB AT 1'� =
RELI SHED BY (SIG.) (SAMPLER)
DATEITIME
RE VED BY (S1G.)
DATEMME
COMMENTS:
..
!
�*z2- l3
RELINQUISHED B (SIG.)
DATEMME
RECEIVED BY (SIG.)
DATEMME
RELINQUISHED BY (SIG.)
DATEMME
RECEIVED BY (SIG.)
DATEITIME
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G" for N� 4��21 S
FORM 05 Grab sample in the blacks above for each parameter requested,

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: March 22, 2022
Permit No. WQ0018525
Peppertree 0.41 % Solids
12.4 pH (taken from lime stabilization event)
Parameter
%
Mg/Kg Dry Weigbt
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
4.414
44,140.000
88.280
Phosphorus
I.734
17,340.000
34.680
Potassium
0.433
4,328.000
8.656
PAN (injected)*
1.399
13,990.420
27.981
PAN (surface)*
1.394
13,940.120
27.880
Ammonia Nitrogen
0.010
100.600
0.201
Calcium
3.772
37,716.000
75.432
Calcium Carbonate E .
---
___
Magnesium
---
2,552.000
5.104
Sodium
---
25,1 I0.000
50.220
Sulfur
---
--_
Nitrate N / Nitrite N
---
678.000
L356
Barium
---
---
---
SA R
2.16
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
g
(M /K )
Aluminum
---
3,539.000
7.078
Arsenic
---
2.50
0.005
75
Cadmium
---
1.20
0.002
85
Chromium
---
18.000
---
---
Copper
---
446.00
0.892
4,300
Lead
---
16.00
0.032
840
Mercury
---
0,29
0.001
57
Molybdenum
---
5.00
0.010
75
Nickel
---
12.00
0.024
420
Selenium
---
5.00
0.010
100
Zinc
---
2,503.00
5.006
7,500
Environment I # 129 C
*Determination of Plant Available Nitrogen (PAN):
Injected Application;
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

Enw, nEw Flo hmppTOW
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
PEPPERTREE RESORTS (FORTIN)
ATTN: MR. DAN FORTIN
P.O. Box 1068
ATLANTIC BEACH, NC 28512
PARAMETERS
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mgllig
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mglkg
Chromium, T.(dry wt. basis),mgliig
Lead (dry weight basis), mglkg
Magnesium (dry wt. basis), mglkg
Mercury (dry wt. basis), mglkg
Nickel (dry wt. basis), mglkg
Potassium (dry wt. basis), mglkg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mglkg
Total Solids, %
TKN (dry wt.), mglkg
Ammonia Nitrogen (dry wt.),mglkg
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt.), mgllig
Plant Available Nitrogen, mglkg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
3539
03/30/22
LFJ
EPA200.7
<2.5
03/30/22
MTM
311313-04
37716
03/30/22
LFJ
EPA200.7
1.2
03/31/22
MTM
3113E-04
446
03/30/22
LFJ
EPA200.7
18
03/30/22
LFJ
EPA200.7
16
03/29/22
MTM
311313-04
2552
03/30/22
LFJ
EPA200.7
0.29
03/30/22
MTM
EPA7471B
12
03/30/22
LFJ
EPA200.7
4328
03/30/22
LFJ
EPA200.7
<5.0
03/31/22
MTM
3113E-04
25110
03/30/22
LFJ
EPA200.7
2503
03/30/22
LFJ
EPA200.7
0,41
03/24/22
JMS
254OG-15
c 44140
03/29/22
BMD
351.2 R2-93
c I00.6
03/28/22
ICES
350.1 R2-93
c 17340
03/29/22
TRJ
365.4-74
c 678.0
03/29/22
ICES
353.2 R2-93
I3940
04/01/22
ICES
5
03/30/22
LFJ
EPA200.7
Drinking Water YD.s 37715
Waetewatet ID1 10
PHONE [phone]
FAX [phone]
ID#: 129 C
DATE COLLECTED: 03/22/22
DATE REPORTED : 04/04/22
REVIEWED BY:
c Uncertified data_ DWR does not offer non -aqueous certification for thia analytical procedure.

PI
A'
P.
A'
En-viron!nent 1, Inc. CHAIN OF CUSTODY RECORD
1 1
P.O. Box 7085. 114 Oakmont Dr. I,.of
Greenville. NC 278-58
environment I inc.coin
DISINFECTION
CHLORINENEUTRAUZEDATCOLLECTION
Phone (252) 75ti-62Q8 •Fax [phone]
Ij CI-ELOR[NL
pHCHECK (LAB)
CLIENT: 129 C Week: 10
Ij UV
P
P
P
P
P
P
CONTAINER TYPE, PIG
uPPERTREE RESORTS (FORTIN)
L) NONE;
I'TN: MR. DAN FORTIN
O. BOX 1068
CHEMICAL PRESERVATION
TLANTIC BEACH NC 28512
A
A
A
A
A
A
E o
A -NONE D-NAOH
52) 247-5841
� zo
z
c
Z
L
I- B- HNO, E. HCL
r
v
x
Cr
w C- H,SO, F- ZINC ACETATEINAOH
COLLECTION
a
a
20¢
w
a o0
¢
a
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o
=
:9
�°
G - NATHIOSULFATE
SAMPLELOCATION
DATE
TIME
G
g Lf
r•+
Y�
e Sample
J'
4»
:�'r
CLASSIFICATION:
WASTEWATER(NPDES)
Ij DRINKING WATER
DWRIGW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING HIPMENT/DELIVERY
N
SAMPLES COLLECTED BY:
(PI Print)
G
SAMPLES RECEIVED IN LAB AT -� `I_ 2C
RELIN =IL(SIG.)
Z DATE TINT •
Z-ZL oL
R EIVED BY (SIG.)
DATE(IIME
COMMENTS:
.
31 1�12a
RELINQUISHED 8Y (SIG.)
DATEMME
RECEIVED BY (SIG.)
DATEMME
RELINQUISHED BY (SIG.)
DAT8TIME
RECEIVED BY (SIG.)
DATE MME
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G" for N� 399847
FoRM 95 Grab sample in the blocks above {or each parameter requested.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: April 28, 2022
Permit No. WQ0018525
Point Emerald Villas 1.35 % Solids
7.9 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
5.254
61,580.000
123.160
Phosphorus
1.482
14,050.000
28.100
Potassium
0.273
3,099.000
6.198
PAN (injected)*
1.600
16,004.780
32.010
PAN (surface)*
1.583
15,834.280
31.669
Ammonia Nitrogen
0.034
346.900
0.694
Calcium
4.028
17,306.000
34.612
Calcium Carbonate E .
---
---
_--
Ma nesium
---
2,651.000
5.302
Sodium
---
22,489.000
44.978
Sulfur
-_-
---
Nitrate N / Nitrite N
---
4.980
0.010
Barium
---
---
---
SAR
4.87
Chloride
---
---
---
Iron
---
---
---
Ceiling Coneen.
(M !K )
Aluminum
---
5,420.00
10.840
Arsenic
---
2.50
0.005
75
Cadmium
---
0.98
0.002
85
Chromium
---
18.000
---
-._
Copper
---
541.00
1.082
4,300
Lead
---
60.00
0.I20
840
Mercury
---
0.36
0.001
57
Molybdenum
---
5.00
0.010
75
Nickel
---
12.00
0.024
420
Selenium
---
6.20
0.012
100
Zinc
---
2,389.00
4.778-1
7,500
Environment I # 348 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection Iimits are listed as detection limits
for calculation purposes.

ENWO pnEgM �' himppTC(Nd
114 OAKMONT DRIVE
GREE=NVILLE, N,C, 27858
POINT EMERALD VILLAS (FORTIN)
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE, NC 28594
PARAMETERS
PH, Units (Non -Aqueous)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry ivt. basis), mg/lcg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mglkg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mglkg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mglkg
Zinc (dry wt. basis), mg/kg
Total Solids, %
T1IN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
c 7.9
05/02/22
DNS
4500HB-11
5420
05/04/22
LFJ
EPA200.7
G2.5
05/04/22
MTM
3113E-04
17306
05/04/22
LFJ
EPA200.7
0.98
05106/22
MTM
311311-04
541
05/04/22
LFJ
EPA200.7
18
05/04/22
LFJ
EPA200.7
60
05/04/22
MTM
31138-04
2651
05/04/22
LFJ
EPA200.7
0.36
05/12/22
MTM
EPA7471B
12
05/04/22
LFJ
EPA200.7
3099
05/04/22
LFJ
EPA200.7
6.2
05/05/22
MTM
311313-04
22489
05/04/22
LFJ
EPA200.7
2389
05/04/22
LFJ
EPA200.7
1.35
04/28/22
HCE
254OG-15
c 61580
05/03/22
BMD
351.2 R2-93
c 346.9
05/02/22
BMD
350.1 R2-93
c 14050
05/03/22
KES
365.4-74
c 4.98
05/03/22
TRJ
353.2 R2-93
5.0
05/04/22
LFJ
EPA200.7
Drinking Water IDt 37715
Wastewater ID: 10
PHONE [phone]
FAX [phone]
ID#: 348 A
DATE COLLECTED: 04/28/22
DATE REPORTED : 05/16/22
REVIEWED BY: / ✓'J �\
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

P1
M
F,
P
E
(2
Environment 1, Inc. CHAIN OF CUSTODY RECORD
P.Oj Box 7085. 114 Oakmont Dr. Paoe I of 1
Xrr -17Q�Q
en v i ro nment I i nc.com
DISINFECTION
CHLORINE NEUTRALIZED AT COLLECTION
Phone [phone] • Fax [phone]
CIiI.OItINE
CLIENT: 348 A Week: 8
G
pH CHECK (LAB)
UV
P
P
P
P
P
P
P
CONTAINER TYPE, P/G
)INT EMERALD VILLAS (FORTIN)
NONE
R. DAN FORTIN
CHEh41CALPRESERVAT40N
)RTIN CONTRACT SERVICES
J
O. BOX 4188
A
A
A
A
A
A
A
VIERALD ISLE NC 28594
A -NONE D-HACH
mo
E
52) 393-8720
B - HNO_ E - HCL
0LLF
o
z
do
z
Ir
a
00
+
� C - H,SO, F - ZINC ACETATE/NAOH
LU
COLLECTION
m
o
LU �
o
�" a
o
LL
a
E,
7
E"
�
p
OkIS
z
G NATHIOSULFATE
a
SAMPLE LOCATION
DATE
TTIME
IS
Sludge Sample
o:
5
n
=
CLASSIFICATION:
LLJ WASTEWATER (NPDES)
DRINKING WATER
DWA/GW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SHIPMENT/DELIVERY
V N
SAMPLES COLLECTED BY:
(Please
iPrint)
1
SAMPLES RECEIVED IN LAB AT Z , cc
R LI QUiSHED BY IG.) ( AMPLER)
QATEMME
X� ll: po.
R EIVED BY (SIC.)
:.
DATEITIME
3 a
COMMENTS:
R LINQUISHED B (SIG.)
DATEMME
RECEIVED BY (SIG.)
DATEMME
REUNQUISHED BY (SIG.)
DATEMME
RECEIVED BY (SIGJ
DATEIFIME
PLEASE READ Instructions for completing this form on the reverse sida.1 Sampler must place a "C" for composite sample or a "G' for N° 400200
FORM #S Grab sample in the blocks above for each parameter requested.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 3, 2022
Permit No. WQ0018525
Sands Villas 1.64 % Solids
6.9 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(MvEg x 0.002)
Nitrogen (TKN)
7.324
73,240.000
146,480
Phosphorus
1 199
21,990.000
43.980
Potassium
0.295
2,948.000
5.896
PAN (injected)*
2.324
23,235.990
46A72
PAN (surface)'
2.234
22,335.990
44.672
Ammonia Nitrogen
0.180
1,800.000
3.600
Calcium
3.000
29,996.000
59.992
Calcium Carbonate E .
---
--_
---
Magnesium
---
3,113.000
6.226
Sodium
---
8,462.000
16.924
Sulfur
_-_
Nitrate N / Nitrite N
---
3.990
0.008
Barium
---
---
SA R
1.59
Chloride
-__
___
_._
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
2,997.00
5.994
Arsenic
---
2.50
0.005
75
Cadmium
---
0.85
0.002
85
Chromium
---
13.000
---
---
Copper
---
255.00
0.510
4,300
Lead
---
7.80
0.016
840
Mercury
---
0.23
0.000
57
Molybdenum
---
5.00
0,010
75
Nickel
---
12.00
0.024
420
Selenium
---
5.00
0.010
100
Zinc
---
1,293.00
2.586
7,500
Environment l # 559
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

Emkofin(W 1, hmpumbd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27358
SANDS VILLA (HYDROTECH)
DON OIMARA
HYDROTECH
P.O. BOIL 4602
EMERALD ISLE, NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/lcg
Arsenic (dry wt. basis), mgllcg
Calcium (dry wt. basis), mgllcg
Cadmium (dry wt. basis), mgllcg
Copper (dry wt. basis), mgllcg
Chromium, T.(dry wt. basis),mg/lcg
Lead (dry weight basis), mg/Itg
Magnesium (dry wt. basis), mg/lcg
Mercury (dry wt, basis), mgllcg
Nickel (dry wt. basis), mgllcg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), ingllcg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/Icg
Total Solids, %
TKN (dry wt.), mg/4
Ammonia Nitrogeu (dry wt.),mg/kg
Phosphorus, T. (dry wt.), ing/Icg
Nitrate+Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/Icg
Sludge Analysis Method
Sample Date Analyst Code
6.9
02/03/22
DIJ
4500HB-11
2997
02/08/22
Li+J
EPA200.7
<2,5
02/10/22
MTM
3113B-04
29996
02/08/22
LCJ
EPA200.7
0.85
02/08/22
MTM
3113E-04
255
02/08/22
LFU
El PA200.7
13
02/08/22
LFJ
EPA200.7
7.8
02/09/22
MTM
3113B-04
3113
02/08/22
LFJ
EPA200.7
0.23
02/10/22
MTM
EPA7471B
12
02/08/22
LFJ
EPA200.7
2948
02/09/22
LTJ
EPA200.7
<5.0
02/11/22
NITNI
3113B-04
8462
02/08/22
LFJ
EPA200.7
1293
02/08/22
LTJ
EPA200.7
1.64
02/03/22
BLV
254OG-15
c 73240
02/11/22
TRJ
351.2 R2-93
c 1800
02/08/22
KES
350.1 R2-93
c 21990
02/11/22
KES
365.4-74
c 3,99
02/09/22
TRJ
353.2 R2-93
5
02/08/22
LrU
EPA200.7
Drinking Water ID! 37715
Wastewater ID: 10
PHONE [phone]
FAX [phone]
ID#: 559
DATE COLLECTED: 02/03/22
DATE REPORTED ; 02/25/22
REVIEWED BY:
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure,

S
D
H
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Environment 1, Inc.
P.O. Box 7085- 114 Oakmont Dr-
Cireenville. NC 27R5R
CHAIN OF CUSTODY RECORD
Page 1 of 1
env ironment linc.com
DISINFECTION
Phone [phone] • Fax [phone]
CHLORINE NEUTRALIZED AT COLLECTION
Ij CHLORINE
pH CHECK (LAB)
CLIENT: 559 Week: S
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NONE
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WERALD ISLE NC 28594
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CLASSIFICATION:
WASTEWATER(NPDES)
UDRINKING WATER
L] DWRIGW
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CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SHITENTIDELIVERY
?�
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SAMPLES COLLECTED BY.
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SAMPLES RECEIVED IN LAB AT °C
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PLEASE READ instructions for completing this form on the reverse side. Sampler must place a "C for composite sampie or a'G" for �° 400� 4�
FORM =s Grab sample in the blocks above for each parameter requested.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 24, 2022
Permit No. WQ0018525
Sea Isle Plantation 0.71 % Solids
12.1 t)H (taken from lime stabilization event)
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
1.917
58,270.000
116.540
Phos horus
0.675
18,820.000
37.640
Potassium
0.452
6,864.000
13.728
PAN (injected)*
0.582
5,815.128
11.630
PAN (surface)*
0.578
5,776.308
11.553
Ammonia Nitrogen
0.008
419.400
0.839
Calcium
4.831
27,439.000
54,878
Calcium Carbonate E .
---
---
Magnesium
---
3,052.000
6.104
Sodium
---
22,215.000
44.430
Sulfur
_-_
_--
Nitrate N / Nitrite N
---
10.980
0.022
Barium
---
---
---
SAR
2.85
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(M /K )
Aluminum
---
2,010.00
4.020
Arsenic
---
2.50
0.005
75
Cadmium
---
0.74
0.001
85
Chromium
---
13.000
---
---
Copper
---
168.00
0.336
4,300
Lead
---
32.00
D.064
840
Mercury
---
0.13
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
14.00
0.028
420
Selenium
---
5.00
0.010
1 100
Zinc
---
987.00
1.974
7,500
-Ji
Environment 14 96A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

EflAummm (PH alp kc©Qpombd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27658
SEA ISLE PLANTATION (FORTIN)
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE, NC 28594
PARAMETERS
Aluminum, (dry wt. basis), mg/lig
Arsenic (dry wt. basis), mg/lig
Calcium (dry wt. basis), mgllig
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/lig
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/lig
Potassium (dry wt. basis), mgllig
Selenium (dry wt. basis), nig/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/Iig
Total Solids, %
TICN (dry wt.), mgllig
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/Iig
Nitrate+Nitrite (dry wt.), mg/Iig
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
2010
03/07/22
LFJ
EPA200.7
<2.5
03/08/22
A4TM
31138-04
27439
03/07/22
LFJ
EPA200.7
0.74
03/08/22
MTNI
311313-04
168
03/07/22
LF.1
EPA200.7
13
03/07/22
LFJ
EPA200.7
32
03/09/22
NUM
3113B-04
3052
03/07/22
LFJ
EPA200.7
0.13
03/14/22
AITM
EPA747IB
14
03/07/22
LFJ
EPA200.7
6864
03/07/22
LFJ
EPA200.7
<5.0
03/08/22
MTM
3113B-04
22215
03/07/22
LFJ
EPA200.7
987
03/07/22
LFJ
EPA200.7
0.71
02/24/22
JMS
254OG-15
c 58270
03/01/22
TRJ
351.2 112-93
c 4I9.4
03/01/22
KES
350.I 112-93
c 18820
03/01/22
BMD
365.4-74
c 10.98
03/01/22
KES
353.2 112-93
17576
03/18/22
ICES
< 5.0
03/07/22
LFJ
EPA200.7
Drinking Water IDs 37115
Wastewater IDo 10
PHONE [phone]
FAX [phone]
ID#: 96 A
DATE COLLECTED: 02/24/22
DATE REPORTED : 03/21/22
REVIEWED BY:
c Uncertified data. DWU does not offer non -aqueous certification for this analytical procedure.

Environment 1, Inc. CHAIN OF CUSTODY RECORD
- F.O.`Bor 7085. 114 Oakmont Dr. Pace 1 or I
Greenville. NC 27858 `
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environment I inc.com
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MR.
1VIERALD
DISINFECTION
Phone f2521 75G-(i2(}8 • Fax (2.i'_) 756-0633
CHLORINE NEUTRALIZED AT COLLECTION
Ij CHLORINE
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CLIENT: 96 A Week: 8
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ISLE PLANTATION (FORTIN}
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52) 393-8720
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GLASSIFlCAiION:
I� WASTEWATER(NPDES)
DRINKINGWATER
DWRIGW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING ENT/DELIVERY
Y N
SAMPLES .,' � CTED BY:
(Rease Print)
Wig T
SAMPLES RECEIVED IN LAB AT 'C
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Sampler must place a "C" for composite sample or a "G" for
PLEASE READ Instructions for completing this farm on the reverse side. NQ 400262
FORM as Grab sample in the blocks above for each parameter requested.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 17, 2022
Permit No. WQ0018525
Sea spray 1.68 % Solids
7.4 p II
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(MgLKg x 0.002)
Nitrogen (TKN)
2.885
46,360.000
92.720
Phosphorus
0.416
21,730.000
43.460
Potassium
0.100
2,083.000
4.166
PAN (injected)*
0.888
8,879.190
17.758
PAN (surface)*
0.872
8,720.190
17.440
Ammonia Nitrogen
0.032
109,400
0.219
Calcium
3.890
60,44T000
120.894
Calcium Carbonate E .
---
Magnesium
---
2,999.000
5.998
Sodium
---
7,873 A00
15.746
Sulfur
---
Nitrate N / Nitrite N
---
0.990
0.002
Barium
---
---
---
SAR
1.10
Chloride
---
__-
Iron
---
---
-E:
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
4,596.00
9.I92
Arsenic
---
2.50
0.005
75
Cadmium
---
0.73
0.001
85
Chromium
---
16.000
---
---
Copper
---
1,048.00
2.096
4,300
Lead
---
20.00
0.040
840
Mercuty
0.26
0.001
57
Molybdenum
---
5.00
0.010
75
Nickel
---
I3.00
0.026
420
Selenium
---
5.00
0.010
100
Zinc
---
1,499.00
2.998
7,500
Environment 19 560
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

E nm'mfima % hmpa n0da
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
A PLACE AT THE BEACH II(HYDROTECH)
DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE, NC 28594
PARAMETERS
PH (not to be used for reporthig)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt, basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/lcg
Lead (dry weight basis), mg/leg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/Irg
Selenium (dry wt. basis), mg/Icg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mgllig
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate + Nitrite (dry wt.), mgllcg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
7.4
02/17/22
JNIS
45001IB-11
4596
03/07/22
LFJ
EPA200.7
<2.5
03/08/22
MTM
3113B-04
60447
03/07/22
LFJ
EPA200.7
0.73
03/08/22
MT1"%•1
3113B-04
1048
03/07/22
LFJ
EPA200.7
16
03/07/22
LFJ
EPA200.7
20
03/09/22
MTNI
3113B-04
2999
03/07/22
LFJ
EPA200.7
0.26
03/14/22
NUM
EPA7471B
13
03/07/22
LFJ
EPA200.7
2083
03/07/22
LFJ
EPA200.7
<5.0
03/08/22
NUM
3113E-04
7873
03/07/22
LFJ
64PA200.7
1499
03/07/22
LFJ
EPA200.7
1.68
02/17/22
JNIS
254OG-15
e 46360
02/22/22
BAID
351.2 R2-93
c 109A
02/21/22
ICES
350.1 R2-93
c 21730
02/22/22
TRJ
365.4-74
c 0.99
02/22/22
KES
353.2 R2-93
5.0
03/07/22
LFJ
EPA200.7
Drinking Water TDf 377L5
Wastewater ID% 10
PHONE [phone]
FAX [phone]
xD#: 560
DATE COLLECTED: 02/17/22
DATE REPORTED : 03/15/22
REVIEWED BY:
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

Environment I. Inc. CHAIN OF CUSTODY RECORD
F:G. Box 7085. 114 Oakmont I)r.
Grcenvilic. NC 27858 Page 1 n1' I
cnvir om-nent I inc.com
DISINFECTION
Phone [phone] • Fax [phone]
CHLORINE NEElTRALIZEDATCCk3ECTI0N
CIif.ORINE
CLIENT: 560 Week: 9
UV
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pH CHECK (LAB)
P
P
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CONTAINERTYPE,PIG
PLACE AT THE BEACH II(HYDROTECH)
❑ NONE
ON O' eLNL&RA
CHEMICAL PRESERVATION
YDROTECH
.O. BOX 4602
A
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CLASSIFICATION:
WASTEWATER (NPDES)
LlDRINKING WATER
DWRIGW
SOLID WASTE SECTION
CHAIN Or CUSTODY (SEAL) MAINTAINED
DURIN(', c'MENT/DELIVERY
Y N
SAMPLES u ' 'TED BY:
(Please Prtnl)
SAMPLES RECEIVED IN LAB ATZ. 7 -C
RELINQUISHED (SIG.)45AMPLER)
DATEfiME I
REM, Y{SI ; l _
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MMENrS:
�AVED
RELINQUISHED BY (SIG.)
DATE ME
BY {SIG.)
DATEMME
RELINQUISHED BY (SIG.)
DATEI TIME
RECEIVED BY (SIG.)
DATErnME
PLEASE READ InStT00011S for completing this form on the reverse side. Sampler must place a "C" for composite sample or a °G" for N� 399584
FORM n5 Grab sample in the blocks above for each parameter requested.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 3, 2022
Sound Of The Sea
Parameter
Potassium
PAN (injected)* _
PAN (surface)*
Ammonia Nitrogen
Calcium
Calcium Carbonate
Magnesium
Sodium
Sulfur
Nitrate N / Nitrite N
Barium
inum
is
ium
nium
ickel
slenium
1.24
6.8
2.885
0.416
0.100
0.888
0.872
0.032
3.890
% Solids
pH
Mg/Kg Dry Weight
(% x 10,000)
75,420.000
24,270.000
4,790.000
8,882.180
8,723.180
1,745.000
25,839.000
3,438.000
3.980
3,131.00
2.50
1.30
14.000
t,335.00
23.00
0.15
5.00
12.00
5.00
2,574.00
Permit No. WQ0018525
Pounds/Dry Ton
(Mg/Kg x 0.002)
150.840
48.540
9.580
17,764
17.446
3.490
51.678
Environment 14 561
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection Iimits
for calculation purposes.
6.876
18.850
0.008
6.262
0.005
0.003
2.670
0.046
0.000
0.010
0.024
0,010
5.148
SAR
1.62
Ceiling Cone n.
(M/K)
75
85
4,300
840
57
75
420
100
7,500

Rdwohmumd % Rumpumbd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27058
SOUND OF THE SEA CONDO.
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE, NC 28594
PARAMETERS
PH (not to be used for reporting)
Alumimcm, (dry wt. basis), mg/kg
Arsenic ((Try wt. basis), nlg/lcg
Calcium (dry wt, basis), mgllcg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mgllcg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mgllcg
Nickel (dry wt, basis), mg/kg
Potassium (dry wt. basis), mgllcg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt, basis), mgllcg
Zinc (dry wt. basis), mgllcg
Total Solids, %
TICN ((Try wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mgllcg
Nitrate+Nitrite (dry wt,), mgllcg
Molybdenum (dry wt. basis), mg/Icg
Sludge
Sample
MASTERS
6.8
3131
<2.5
25839
1.3
1335
14
23
3438
0.15
12
4790
< 5.0
9425
2574
1.24
c 75420
c 1745
c 24270
c 3.98
< 5.0
Analysis Method
Date Analyst Code
02/03/22
DIJ
45001IB-11
02/08/22
LFJ
EPA200.7
02/10/22
MTM
3113B-04
02/08/22
LFJ
EPA200.7
02/08/22
NITM
311313-04
02/08/22
LFJ
EPA200.7
02/08/22
LFJ
EPA200.7
02/09/22
MTM
3113E-04
02/08/22
LFJ
EPA200.7
02/10/22
MTM
EPA7471B
02/08/22
LFJ
EPA200.7
02/09/22
LFJ
EPA200.7
02/11/22
NITM
3113B-04
02/08/22
LFJ
EPA200.7
02/08/22
LFJ
EPA200.7
02/03/22
BLV
2540G-15
02/11/22
TRJ
351.2 112-93
02/08/22
ICES
350.1 112-93
02/11/22
ICES
365.4-74
02/09/22
TRJ
353.2 R2-93
02/08/22
LFJ
EPA20D.7
Drinking water ID, 37715
Wastewatar ID: 10
PHONE [phone]
FAX [phone]
ID#: 561
DATE COLLECTED: 02/03/22
DATE REPORTED : 02/25/22
REVIEWED BY:
c Uncertified data. aWR does not offer non -aqueous certification for thin analytical procedure,

Environment 1, Inc.
P_O. Box 7085, 114 Oakmont'Dr.
Greenville, NC 27858
CHAIN OF CUSTODY RIC1CORD
environmentlinc.com
DISINFECTION
'
Phone [phone] a Fax [phone]
CHLORINE
Pr__6
CLIENT: 561 Week:I1
UV
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SOUND OF THE SEA CONDO. MASTERS
NONE
p
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ATTN- DON O'MAR4
HYDROTECH
JA
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P.O. BOX 4602
A
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EMERALD ISLE NC 28594
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RELI LSISHED G.)(SAMPLER) DATUTIME RECEIV BY 1 ATEMME
REUNQUISFI ' BY (SIG.} DATEIiIUE R CBVED BY (SIG.) DATE/TIM�
REUNQUISHED BY (SIG.) DATEITIME RECEIVED BY (SIG.) DATEIITME
COMMENTS:
Pa-e 1 of 1
CHLORINE NEUTRALIZED AT COLLECTION
pH CHECK (LAB)
CONTAINER TYPE, PJG
CHEMICAL PRESERVATION
A -NONE D-NAOH
LU
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B-HNO, E-HCL
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CLASSIFICATION:
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WASTEWATER(NPDES)
Ij
DRINKING WATER
DWR/GW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURIN
r PMENTIDELfVERY
Y N
SAMPLES OL.LECTED BY:
(Please Print)
SAMPLES RECXIVED IN LAB AT I r b IC
PLEASE READ Instructions for completing this form on the reverse side_ Sampler must place a "C' for composite sample or a "G" for �� 3i9997%
FORM ::5 Grab sample in the blocks above for each parameter requested.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 8, 2022
Permit No. WQ0018525
Southwinds Condominiums 1.28 % Solids
7.3 pH
Parameter
%
I Mg/Kg Dry Weight
x 10,000)
Pounds/Dry Ton
(M IK x 0.002)
Nitrogen (TKN)
3.804
38,040.000
76.080
Phosphorus
1.960
19,600.000
39.200
Potassium
0.181
1,811.000
3.622
PAN (injected)*
1.168
11,675.700
23.351
PAN (surface)*
1.149
11,493.050
22.986
Ammonia Nitrogen
0.037
365.300
0.731
Calcium
3.852
38,52 L000
77.042
Calcium Carbonate E .
---
---
---
Magnesium
---
2,231,000
4.462
Sodium
---
5,875.000
11.750
Sulfur
---
---
---
Nitrate N / Nitrite N
---
7.990
0.016
Barium
---
---
---
SAR
0.89
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
3927.000
7.854
Arsenic
---
2.50
0.005
75
Cadmium
---
0.50
0.001
85
Chromium
---
13.000
---
---
Copper
---
543.00
1.086
4,300
Lead
---
10.00
0.020
840
Mercury
---
0.40
0.001
57
Molybdenum
---
5.00
0.010
75
Nickel
---
7.00
0.014
420
Selenium
---
5.00
0.010
100
Zinc
---
1,084.00
2.168
7,500
Environment 1 # 562 B
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N +Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or a detection limits are listed as detection limits
for calculation purposes.

Em,mu(M I b1cupumbd
114 OAKMONT DRIVE
GREENVIL.LE, N.C. 27858
SOUTHWINDS (HYDROTECH)
DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE, NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/lig
Arsenic (dry wt. basis), mg/lig
Calcium (dry wt. basis), mglkg
Cadmium (dry wt. basis), mglkg
Copper (dry wt. basis), mgllig
Chromium, T.(dry wt, basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), nig/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), ing/lig
Zinc (dry wt. basis), mgJkg
Total Solids, %
TICN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, 1'. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt.), mg/lig
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis 14fethod
Sample Date Analyst Code
7.3
02/08/22
CAW
45001-IB-11
3927
02/22/22
LFJ
EPA200.7
<2.5
02/23/22
MTM
31138-04
38521
02/22/22
LFJ
EPA200.7
<0,5
02/22/22
MTM
3113B-04
543
02/22/22
LFJ
EPA200.7
13
02/22/22
LFJ
EPA200.7
10
02124/22
MTM
311313-04
2231
02/22/22
LTJ
EPA200.7
0.40
02/23/22
MTM
EPA7471D
7
02/28/22
LFJ
EPA200.7
1811
02/22/22
LFJ
EPA200.7
<5.0
02/24/22
MTNi
3113B-04
5875
02/22/22
LFJ
EPA200.7
1084
02/22/22
LFJ
EPA200.7
1.28
02/08/22
JMS
2540G-15
c 38040
02/11/22
TRJ
351.2 R2-93
c 365.3
02/17/22
TRJ
350.1 R2-93
c 19600
02/11/22
KES
365.4-74
c 7.99
02/14/22
BMD
353.2 R2-93
5
02122122
LFJ
EPA200.7
Drinking Water IDS 37715
Wastewater IDi 10
PHONE (252) /56-6208
FAX [phone]
ID#: 562 B
DATE COLLECTED; 02/00/22
DATE REPORTED ; 03/02/22
REVIEWED BY: J �`
e Uncertified data. DWR does not offer non-egUaqua certification for this analytical procedure.

Environment 1. Inc. CHAIN OF CUSTODY RECORD
P.O. Box 70$5. 114 Oakmont Dr. Pagge 1 of I
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CHLORINE NEUTRALIZED AT COLLECTION
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DWR/GW
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CHAIN OF CUSTODY (SEAL) MAINTAINED
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I
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G" for FORM -e Grab sample in the blocks above for each parameter requested. No— 399582

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 15, 2022
Permit No. WQ0018525
Summer Winds 1.01 % Solids
6.6 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
7.690
76,900.000
153.800
Phosphorus
1.696
16,960.000
33.920
Potassium
0.344
3,437.000
6.874
PAN (injected)*
2.376
23,763.660
47.527
PAN (surface)*
2.344
23,438.260
46.877
Ammonia Nitrogen
0.065
650,800
1.302
Calcium
3.295
32,946.000
65.892
Calcium Carbonate E .
---
---
Magnesium
---
2,798.000
5.596
Sodium
---
19,549.000
39.098
Sulfur
---
...-
Nitrate N I Nitrite N
---
238.100
0.476
Barium
---
---
---
SAR
2.79
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
4,003.00
8.006
Arsenic
---
2.50
0.005
75
Cadmium
---
0.60
0.001
85
Chromium
---
20.000
---
---
Copper
---
1,143.00
2.286
4,300
Lead
---
18.00
0.036
840
Mercury
---
0.50
0.00I
57
Molybdenum
---
5.00
0.010
75
Nickel
---
12.00
0.024
420
Selenium
---
5.00
0.010
100
Zinc
---
1,930.00 1
3.860
7,500
Environment 14 119A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

Enwok mmfll % hCupufflUd
11-1 OAKMONT DRIVE
GREENVILLE, N.C. 27858
SWNC MASTER OWNERS ASSOC, INC
ATTN: DON OtMARA
HYDROTECH; SUMMER WINDS
P.O, sox 4602
EMERALD ISLE, NC 28594
PARAMETERS
PH (not to be used For reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mgllcg
Calcium (dry wt. basis), mgllcg
Cadmium (dry wt. basis), mgllcg
Copper (dry wt. basis), mgllcg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mgllcg
Magnesium (dry wt. basis), mgllcg
Mercury (dry wt. basis), mgllcg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mgllcg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mgllcg
Nitrate+Nitrite (dry wt.), mgllcg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
6.6
02/15/22
JMS
4500HB-11
4003
02/22/22
LFJ
EPA200.7
<2.5
02/23/22
MTM
311313-04
32946
02/2Z/22
LFJ
EPA200.7
0.60
02/22/22
MTM
311313-04
1143
02/22/22
LFJ
11;PA200.7
20
02/22/22
LFJ
EPA200.7
18
02/24/22
MTM
311313-04
2798
02/22/22
LFJ
EPA200.7
0,50
02/23/22
MTM
EPA7471B
12
02/28/22
LFJ
EPA200.7
3437
02/22/22
LFJ
EPA200.7
< 5.0
02/24/22
MTM
3113B-04
19549
02/22/22
LFJ
EPA200.7
1930
02/22/22
LFJ
EPA200.7
1.01
02/16/22
JMS
254OG-15
c 76900
03/01/22
TRJ
351.2 112-93
c 650.8
02/17/22
TRJ
350.1 R2-93
c 16960
03/01/22
BMD
365.4-74
c 238.1
02/17/22
KES
353.2 112-93
<5.0
02122122
LFJ
E, PA200.7
Drinking Water Tns 37715
wastewater YD: 10
PHONE [phone]
FAX [phone]
ID#: 119 A
DATE COLLECTED: 02/15/22
DATE REPORTED : 03/02/22
REVIEWED BY:
c Uncartified data. DWR does not offer non-aqueoua certification for this analytical procedure.

Environment 1, Inc. CHAIN OF CUSTODY RECORD
P.O. Box 7085, 114 Oalunont Dr- Page 1 of I
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CLIENT: 119 A Week: 10
pH CHECK (LAB)
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DRINKING WATER
DWR4W
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SRLPMENT/DELIVERY
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SAMPLES COLLECTED BY.
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DATEMME
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(SIG.)
RECEIVED BY SIG.
DATE/TIME
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G" for N° 399552
FORM -5 Grab sample in the blocks above for each parameter requested.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 8, 2022
Permit No. WQ0024756
The Grove WWTP 1.33 % Solids
8.1 pH
Parameter
%
Mg1Kg Dry Weight
(% x 10,000}
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
5.433
54,330.000
108.660
Phosphorus
1.714
17,140.000
34.280
Potassium
0.312
3,115.000
6.230
PAN (injected)*
1.760
17,600.160
35.200
PAN (surface)*
1.668
16,682.160
33364
Ammonia Nitrogen
0.184
1,836.000
3.672
Calcium
2.433
24,333.000
48.666
Calcium Carbonate E ,
---
---
Magnesium
.._
2,237.000
4.474
Sodium
---
8,534,000
17.068
Sulfur
---
___
Nitrate N / Nitrite N
---
15.960
0.032
Barium
Chloride
Iron
---
---
---
Aluminum
---
1415.000
2.830
Arsenic
---
2.50
0.005
Cadmium
---
0.52
0.001
Chromium
---
9.000
---
Copper
---
121.00
0.242
Lead
---
3.40
0.007
Mercury
---
0.11
0.000
Molybdenum
---
9.00
0.0I8
Nickel
---
9.00
0.018
Selenium
---
5.00
0.010
Zinc
---
698.00
1.396
Environment 1 4 549 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or ¢ detection limits are listed as detection limits
for calculation purposes.
SAR
1.62
�-(MgX
ling Concen.
75
85
4,300
840
57
75
420
100
7,500

EnwUhRoo 1, hoQporood
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
THE GROVE WWTP (HYDROTHCH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE, NC 26594
Sludge
Analysis
Method
PARAMETERS
Sample
Date
Analyst
Code
PH (not to be used for reporting)
8.1
02/08/22
CAW
4500BB-11
Aluminum, (dry wt. basis), mg/kg
1415
02/22/22
LFJ
EPA200.7
Arsenic (dry wt. basis), mg/kg
<2.5
02/23/22
MTM
311313-04
Calcium (dry wt. basis), mg/kg
24333
02/22/22
LFJ
EPA200.7
Cadmium (dry wt. basis), mg/kg
0.52
02/22/22
MTM
311313-04
Copper (dry wt, basis), mg/lcg
121
02/22/22
LFJ
EPA200.7
Chromium, T.(dry wt. basis),mg/lcg
9
02/22/22
LFJ
EPA200.7
Lead (dry weight basis), mg/kg
3.4
02/24/22
MTM
3113E-04
Magnesium (dry wt. basis), mg/kg
2237
02/22/22
LFJ
EPA200.7
Mercury (dry wt. basis), mg/kg
0.11
02/23/22
MTM
EPA7471B
Nickel (dry wt. basis), mg/kg
9
02/28/22
LFJ
EPA200.7
Potassium (dry wt. basis), mg/kg
3115
02/22/22
LFJ
EPA200.7
Selenium (dry wt. basis), mg/kg
<5.0
02/24/22
MTM
311313-04
Sodium (dry wt. basis), mg/kg
8534
02/22/22
LFJ
EPA200.7
Zinc (dry wt. basis), mg/kg
698
02/22/22
LFJ
EPA200.7
Total Solids, %
1.33
02/08/22
JMS
254OG-15
TKN (dry wt.), mg/kg
c 54330
02/11/22
TRJ
351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/kg
c 1836
02/15/22
BMD
350.1 112-93
Phosphorus, T. (dry wt.), mg/kg
c 17140
02/11/22
ICES
365.4-74
Nitrate+Nitrite (dry wt.), mg/kg
c 15.96
02/14/22
BMD
353.2 R2-93
Molybdenum (dry wt. basis), mg/kg
9
02/22/22
LFJ
EPA200.7
Drinking water ID: 37715
wastewater ID: 10
PHONE [phone]
FAX [phone]
ID#: 549 A
DATE COLLECTED: 02/08/22
DATE REPORTED : 03/02/22
REVIE B .
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

CHAIN Or- CUSTODY RECORD
Environment 1, Inc.
P.O. Box 7085, 114 Oakmoni Dr.
Greenvi116,NC 27858
environmentlinc.coin
DISINFECTION
Phone [phone].• Fax (252) 75G-0633
CHLORLNE
CLIENT: 549. A Week: '10
THE GROVE WWTP WDRO'TECM .
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PLEASE READ:InStruct 0[1S forcornp)eting this form an the reverse side:
FOAM #5
= C.OMNIENTS:.
Page 1 nF 1
CHLORINE NEUTRAUZED ATCOLLECTION
pH CHECK (LAB)
CONTAINER TYPE, NG
CHEMICAL PRESERVATION
�2 A -NONE D-NAOH
w
B -HNO�. E-HCL
C-H,80x F-ZINC ACETATE/NAOH
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CLASSIFICATION:
WASTEWATER(NPOES)
DRINKINGWATER
DWFYGW
SOLIDWASTESECTION
CHAIN OF CUSTODY (SERL) MAINTAINED
DURING MEODELIVERY
Y 1 N
SAMPLES COLLECTED BY.
(Please Prijtt)
SMIPLES.FIECEIVED')NLABATU-.'0 °C
Sampler must place a "C" forcomposite sample or a V for N 399742
:Grab sample in the blacks above for each parameter requested.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: December 30, 2022
Permit No. WQ0018525
Whaler Inn 0.88 % Solids
7.3 PH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(MZ/Kg x 0.002)
Nitrogen (TKN)
1.601
35,710.000
71.420
Phosphorus
0.397
7,727,000
15.454
Potassium
0.399
3,221.000
6.442
PAN (infected)*
0.501
5,008.800
10.018
PAN (surface)'
0.486
4,863.800
9.728
Ammonia Nitrogen
0.029
619.300
1.239
Calcium
5.591
42,093.000
84.186
Calcium Carbonate E .
---
---
Magnesium
---
2,891.000
5.782
Sodium
---
11,862.000
23.724
Sulfur
---
---
---
Nitrate N / Nitrite N
---
1.600
0.003
Barium
---
---
---
SAR
1.41
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
8,921.00
17.842
Arsenic
---
2.50
0.005
75
Cadmium
---
0.90
0.002
85
Chromium
---
11.000
---
---
Copper
---
794.00
1.588
4,300
Lead
---
8.00
0.016
840
Mercury
---
0.21
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
12.00
0.024
420
Selenium
---
5.00
0.010
100
Zinc
---
1,239.00
2.478
7,500
Environment 1 # 70A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are Iisted as detection limits
for calculation purposes.

Environment 1, Incorp
��'{-�,.i i n i�•j,�� hill li'h CAI � i'.:'� I,1 i;.i:RP �P�,f �I
{
P.O. BOX 7085, 114;OAKMONT DRIVE
GREENVILLE,N.C.'27835 7085 . ''.' ..':
orated
THE WHALER INN (BUCK)
C/O MR. STANLEY BUCK
1745 BELGRADE-SWANSBORO RD.
MAYSVILLE, NC 28555
PARAMETERS
PH (not to be used. for reporting)
Aluminum, (dry wt. Basis), Ing/kg
Arsenic (dry wt. basis), mg/lcg
Calcium (dry wt, basis), mg/Icg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt, basis), mg/kg
Chromium, T.(dry wt. basis),mg/Icg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/]cg
Mercury (dry wt. basis), nig/kg
Nickel (dry wt. basis), ing/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), nig/I{g
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt.), mg/!cg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), Ing/kg
{�31 NII�,E'h�4kl'!'I',jll�i,,'�I,�fl�! �' �I;I�i41E1III, Illlll if�,Jl�,ifll' �� E, I •�
I' I PROM (252) 75&6208',.
EAX°(252):7,56.0633.'
r
Sludge Analysis Method
Sample Date Analyst Code
7.3
01/12/23
BLV 4500HB-11
8921
01/20/23
MTM EPA200.7
< 2.5
01/20/23
DRC 3113B-04
42093
01/20/23
MTM EPA200.7
0.9
01/24/23
DRC 3113B-04
794
01/27/23
MTM EPA200.7
11
01/20/23
MTM EPA200.7
8.0
01/23/23
DRC 3113B-04
2891
01/20/23
MTM EPA200.7
0.21
01/24/23
DRC EPA7471B
12
01/20/23
MTM EPA200.7
3221
01/20/23
MTM EPA200.7
< 5.0
OV23/23
DRC 311313-04
11862
01/20/23
MTM EPA200.7
1239
01/20/23
MTM EPA200.7
0.88
0I/12/23
JMS 2540G-15
c 35710
01/18/23
BMD 351.2 112-93
c 619.3
01/24/23
KES 350.1 112-93
c 7727
01/18/23
TRJ 365.4-74
c 1.60
01/25/23
BMD 353.2 R2-93
14348
02/02/23
TRJ
< 5.0
OV20123
MTM EPA200.7
ID#1 70 A
DATE COLLECTEDs 12/30/22
DATE REPORTED 1 02/03/23
1 �
RE AEWEs
' OA
c Vncartified data. DWR does not offer non -aqueous certification for this analytical ptaeadura.

PATHOGEN AND VECTOR ATTRACTION REDUCTION MONITORING

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Barnes Environmental Waste and Hauling, Inc. WQ Permit Number: WQ0018525
WWTP Name: SEE ATTACHED LIST NPDES Number: SEE ATTACHED
Monitoring Period: From 1/1/2022 To 12/31/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative
Class A: Alt, A (time/temp) ❑ I Alt B (Alk Treatment) ❑ Alt. C (Prior Testir
AIt-D (No Prior Test) ❑ Process to Further Reduce PatlM
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogen:
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermo phili
Beta Ray ❑ Gatuma Ray ❑ Pasteurization ❑
Class B: JAIL (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Path(
Lime Stabilization El Air Drying ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class
Parameter Allowable Level Pathogen DE
in Sludge Minima Geo. Mean K
2 x 10 to the MPN
6th power
per gram of
Fecal Coliform total solids CFU
1000 mpn per gram
oftotal solid (dry
nmoneua Dacterial 3 MFN per 4 grams
(in lieu of fecal I total solid (dry
Composting ❑ JAerobic I
complete the following monitor
um er o
ty Excee- Frequency
au Units ae. e� of Analysis
performed:
ig)❑
tas ❑
�gens":
gestion ❑
g data:
Sample na ytr(
-. I Tech -
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.] (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑ Alt, 6 (Alk. Stabilization 0 Alt 7 (Drying- Stable) ❑ Alt. 8 (Drying- Unstable) ❑
Alt. 9 (injection) ❑ Alt. 10 (incorporation) ❑ No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Steven M. Barnes, President
Preparer Name and Title (type or print)
Jteye #14keelf
Steve M Bames (Feb 17 2023 14:33 EST!
Signature of Preparer*
Lana appiier Name and l the (it applicable)(type or print)
Feb 17, 2023
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503,9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (1212006)

BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Atlantic Station
Batch Size (gallons): 80,500
P.O.#
Lbs. or Gallons Used: 1,600
Material Used For Stabilization: Lime
Initial
pH
>12 pH
2 Hour
pH
24 Hour
pH
Operato
Date
pH
Temp C
Corr.
Factor+
Corrected
pH
Time
pH
Temp C
Corr,
Factor +
Corrected
pH
Time
pH
Temp C
Corr.
Factor +
Corrected
pH
Time
pH
Temp C
Corr.
Factor +
Corrected
pH
Time
Initials
2/12/2022
7.45
21
-0.12
7.33
10:OOAM
12.41
21
-0.12
12.29
10:05
12.43
21.0
-0.12
12.31
12:05
12.41
22.0
-0.09
12.32
11:00
SMB
4112/20z2
6.78
25
0
6.78
9:30AM
12.23
25
0
12.23
9:40
12.26
24.0
-0.03
12.23
11:40
12.29
24.0
-0.03
12.26
10:00
SMB
5/24/2022
7.32
27
0.06
7.38
10:30AM
12.32
27
0.06
12.38
10:35
12.41
28.0
0.09
12.50
12:35
12.32
28.0
0.09
12.41
11:30
SMB
5/28/2022
6.98
27
0.06
7.04
9:15AM
12.28
27
0.06
12.34
9:20
12.35
27.0
0.06
12.41
11:20
12.39
27.0
0.06
12.45
10:00
SMB
513azozz
6.87
27
0.06
6.93
10:OOAM
12.26
27
0.06
12.32
10:10
12.33
27.0
0.06
12.39
12:10
12.31
28.0
0.09
12.40
11:00
SMB
6/9/2022
7.13
28
0.09
7.22
11:30AM
12.22
28
0.09
12.31
11:40
12.29
27.0
0.06
12.35
13:40
12.36
28.0
0.09
12.45
12:00
SMB
6/28/2022
7.34
30
0.15
7.49
11:OOAM
12.10
30
0.15
12.25
11:10
12.12
30.0
0.15
12.27
13:10
12.21
30.0
0.15
12.36
13:00
SMB
7/15/2022
6.99
32
0.21
720
13:OOPM
12.04
32
0.21
12.25
13:10
12.09
32.0
0.21
12.30
15:10
12.23
32.0
0.21
12.44
14:15
SMB
8/6/2022
7.06
35
0.3
7.36
11:15AM
12.05
35
0.3
12.35
11.20
12.23
36.0
0.33
12.56
12:20
12.15
36.0
0.33
12.48
12:45
SMB
8/11/2022
7.01
36
0.33
7.34
9:30AM
12.16
36
0.33
12.49
9:40
12.26
35.0
0.3
12.56
11:40
12.17
35.0
0.30
12.47
10:30
SMB
9/13/2022
6.66
35
0.3
6.96
8:30AM
12.07
35
0.3
12.37
8:35
12.15
35.0
0.3
12.45
10:35
12.14
36.0
0.33
12.47
9:30
SMB
9/15/2022
7
35
0.3
7.30
8:30AM
12.10
35
0.3
12.40
8:40
12.13
36.0
0.33
12.46
10:40
12.13
36.0
0.33
12.46
10:00
SMB
10/4/2022
6.82
30
0.15 1
6.97
9:45AM
12.09
30
0.15
12.24
9:50
12.18
31.0
0.18
12.36
11:50
12.2
31.0
0.18 112.38
10:00
SMB
10/19/2022
7.14
31
0.18
7.32
9:30AM
12.22
31
0.18
12.40
9:35
12.27
30.0
0.15
12.42
11:35
12.3
30.0
0.15
12.45
10:15
SMB
1112212022
7.42
27
0.06
7.48
1O:OOAM
12.01
27
0.06
12.07
10:05
12.09
28.0
0.09
12.18
12:05
12.12
29.0
0.12
12.24
11:15
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Beacons Reach
Batch Size (gallons): 63,000
Lbs. or Gallons Used:
P.O.#
1,300 Material Used For Stabilization: Lime
Initial
pH
>12 pH
2 Hour pH
24 Hour pH
Operator
Date
pH
Temp C
Corr.
Factor +
Corrected
pH
Time
pH
Temp C
Corr.
Factor +
Corrected
pH
Time
pH
Temp C
Corr.
Factor +
Corrected
pH
Time
pH
Temp C
I
Corr.
Factor +
Corrected
pH
Time
Initials
1/13/2022
6.88
21
-0.12
6.76
10:OOAM
12.08
21
-0.12
11.96
10:05
12.31
21.0
-0.12
12.19
12:05
12.33
22.0
-0.09
12.24
10:30
SMB
3/24/2022
7.03
24
-0.03
7.00
9:30AM 1
12.05
24
-0.03
12.02
9:35
12.13
24.0
-0.03
12.10
11:35
12.17
24.0
-0.03
12.14
11:00
SMB
5/6/2022
7.12
25
0
7.12
1O:OOAM
12.20
25
0
12.20
10:10
12.23
25.0
0
12.23
12:10
12.23
26.0
0.03
12.26
11:00
SMB
5/10/2022
7.08
26
0.03
7.11
10:45AM
12.15
26
0.03
12.18
10:50
12.19
27.0
0.06
12.25
12:50
12.24
27.0
0.06
12.30
12:00
SMB
6/7/2022
7.32
31
0.18
7.50
8:OOAM
12.01
31
0.18
12.19
8:05
12.04
31.0
0.18
12.22
10:05
12.1
1 32.0
0.21
12.31
10:00
SMB
6/1B12022
7.3
32
0.21
7.51
8:30AM
12.06
32
0.21
12.27
8:40
12.12
33.0
0.24
12.36
10:40
12.091
34.0
0.27
12.36
10:30
SMB
7/12/2022
7.41
34
0.27
7.68
9:00AM
12.10
34
0.27
12.37
9.05
12.14
34.0
0.27
12.41
11:05
12.16
35.0
0.30
12.46
10:00
SMB
8/5/2022
7.23
37
0.36
7.59
9:OOAM
12.03
37
0.36
12.39
9:05
12.05
37.0
0.36
12.41
11:05
12.1
38.0
0.39
12.49
10:30
SMB
9/21/2022
7.22
34
0.27
7.49
10:00AM
12.11
34
0.27
12.38
10:10
12.16
35.0
0.3
12.46
12:10
12.15
36.0
0.33
12.48
11:30
SMB
10/25/2022
7.13
30
0.15
7.28
11:00AM
12.29
30
0.15
12.44
11:05
12.33
30.0
0.15
12.48
13:05
12.35
29.0
0.12
12.47
12:00
SMB
12/8/2022
6.93
23
-0.06
6.87
11:30AM
12.25
23
-0.06
12.19
11:35
12.24
24.0
-0.03
12.21
13:35
12.2
23.0
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12.14
12:30
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Colony By the Sea
Batch Size (gallons): 3,500 Lbs. or Gallons Used:
P.O.#
100 Material Used For Stabilization: Lime
ITMI •
•
• • I
• •
•.
Eww=w=Ew=ffiMwM
RMEW
SEM
1 1®
ME
KM
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Dunescape
Batch Size (gallons): 2,100 Lbs, or Gallons Used:
P.O*
450 Material Used For Stabilization: Lime
MEW
Knum
CO L
_
0
+�
N U
U
to
o
N
7
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: 8 112 Marina
Batch Size (gallons): 3,500
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P.O.#
100
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Genesis
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER SIOSOLIDS
Facility Name: Hampton Inn P.0.#
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Harkers Island
Batch Size (gallons): 14,000
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Kings Bridge P.O.#
Batch Size (gallons): 10,500
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250 Material Used For Stabilization: Lime
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOL1DS
Facility Name: McGinnis PT
Batch Size (gallons): 10,500
Lbs. or Gallons Used:
P.O.#
200 Material Used For Stabilization: Lime
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: NC Aquarium P.O.#
Batch Size (gallons): 10,500
Lbs. or Gallons Used:
250
Material Used For Stabilization: Lime
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Ocean Bay Villas
Batch Size (gallons): 3,500 Lbs. or Gallons Used:
P.O.#
100 Material Used For Stabilization: Lime
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Ocean Club P.O,#
Batch Size (gallons): 31,500
Lbs. or Gallons Used:
650
Material Used For Stabilization: Lime
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Hour pH
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Date
pH
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Initials
2/12/2022
7.34
23
-0.06
7.28
13:OOAM
12.08
23
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12.02
13:10
12.1
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12.04
15:10
12.13
24.0
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12.10
14:001
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3/15/2022
7.13
24
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7.10
11:00AM
12.30
24
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12.27
11:05
12.33
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12.30
13:05
12.4
24.0
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12.37
12:001
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4/6/2022
6.98
25
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6.98
10:OOAM
12.19
25
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12.19
10:05
12.21
26.0
0.03
12.24
12:05
12.27
25.0
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12.27
11:00
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5/24/2022
6.76
27
0.06
6.82
9:30AM
12.22
27
0.06
12.28
9:35
12.24
27.0
0.06
12.30
11:351
12.23
27.0
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12.29
10:30
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6/16/2022
7.3
29
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7.42
9:15AM
12.01
29
0.12
12.13
9:20
12.02
39.0
0.42
12.44
11:20
12.04
30.0
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12.19
10:00
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7/19/2022
6.8
31
0.18
6.98
9:45AM
12.07
31
0.18
12.25
9:50
12.1
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0.21
12.31
14:25
12.15
32.0
0.21
12.36
11:00
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8/9/2022
6.88
33
0.24
7.12
10:30AM
12,34
33
0.24
12.58
10:40
12.44
33.0
0.24
12.68
12:40
12.13
32.0
0.21
12.34
11:30
SMB
9/21/2022
7.11
30
0.15
7.26
12:OOAM
12.27
30
0.15
12.42
12:05
12.361
30.0
0.15
12.51
14:05
12.12
31.0
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12.30
13:00
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name:
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Pebble Beach
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Peppertree
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P.O.#
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOL1DS
Facility Name: PT Emerald Villa
Batch Size (gallons):
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOL1DS
Facility Name: Sands Villa
Batch Size (gallons): 21,500
Lbs. or Gallons Used:
P.O.#
400
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Sea Isle Plantation
Batch Size (gallons): 28,000
Lbs. or Gallons Used:
P.O.#
600 Material Used For Stabilization: Lime
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pH
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Initials
2/8/2022
6.7
21
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12.20
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12.25
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12.13
10:05
12.27
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3/18/2022
7.23
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12.19
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9:40
12.21
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5/30/2022
7.5
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7.59
9:OOAM
12.06
28
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12.15
9:05
12.09
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12.18
11:05
12.11
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10:00
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6/28/2022
6.89
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12.29
33
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12.53
12:05
12.31
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12.55
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12.14
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12.41
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7/5/2022
6.93
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9/21/2022
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12.12
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10/28/2022
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12.20
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12.22
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11/29/2022
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Sea Spray P.O.#
Batch Size (gallons): 14,000
Lbs. or Gallons Used:
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Sound of Sea
Batch Size (gallons): 7,000
Lbs. or Gallons Used:
150
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Southwinds
Batch Size (gallons): 28,000
Lbs. or Gallons Used:
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600 Material Used For Stabilization: Lime
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Summerwinds
Batch Size (gallons): 133,000
P.O.#
Lbs. or Gallons Used: 2,700
Material Used For Stabilization: Lime
Initial
pH
>12 pH
2 Hour pH
24 Hour pH
Operator
Date
pH
Temp C
Corr.
Factor +
Corrected
pH
Time
pH
Temp C
Corr.
1Factor+1
Corrected
pH
Time
pH
Temp C
Corr.
Factor +
Corrected
pH
Time
pH
Temp C
Corr.
Factor +
Corrected
pH
Time
Initials
1/312022
7.35
19
-0.18
7.17
8:OOAM
12.23
19
-0.18
1 12.05
8:05
12.2
20.0
-0.15
12.05
10:05
12.26
20.0
-0.15
12.11
9:00
SMB
2/24/2022
6.92
21
-0.12
6.80
9:OOAM
12.13
21
-0.12
12.01
9:05
12.8
21.0
-0.12
12.68
11:05
12.12
21.0
-0.12
12.00
10:30
SMB
3/2/2022
7.21
23
-0.06
7.15
8:30AM
12.09
23
-0.06
12.03
8:35
12.12
25.0
0
12.12
10.35
12.31
26.0
0.03 1
12.34
9:00
SMB
3/19/2022
7.3
24
-0.03
7.27
10:OOAM
12.25
24
-0.03
12.22
10:05
12.23
25.0
0
12.23
12:05
12.25
25.0
0.00
12.25
11:00
SMB
5/12/2022
7.13
29
0.12
7.25
9:OOAM
12.23
29
0.12
12.35
9:05
12.2
29.0
0.12
12.32
11:05
12.3
28.0
0.09
112.39
9:30
SMB
5/26/2022
7.32
30
0.15
7.47
10:OOAM
12.38
30
0.15
12.53
10:05
12.42
30.0
0.15
12.57
12:05
12.28
31.0
0.18
12.46
11:30
SMB
6/21/2022
7.38
32
0.21
7.59
10:OOAM
12.10
32
0.21
12.31
10:10
12.13
33.0
0.24
12.37
12:10
12.24
32.0
0.21
12.45
10:30 1
SMB
8/2/2022
7.28
34
0.27
7.55
9:30AM
12.20
34
0.27
12.47
9:40
12.21
35.0
0.3
12.51
11:40
12.13
35.0
0.30
12.43
10:00
SMB
9/2/2022
7.31
33
0.24
7.55
11.30AM
12.151
33
0.24
12.39
11:35
12.18
33.0
0.24
12.42
13:35
12.19
34.0
0.27
12.46
12:00
SMB
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOL1DS
Facility Name: The Grove
Batch Size (gallons): 56,000
P.O.#
Lbs. or Gallons Used: 1,150
Material Used For Stabilization: Lime
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Whaler Inn
Batch Size (gallons):
3,500
Lbs. or Gallons Used:
P.O.#
100 Material Used For Stabilization: Lime
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2022 APPLICATION SUMMARY

BARNES ENVIRONMENTAL WASTE
Permit# WQ 0018625
RESIDUALS APPLICATION
2022 APPLICATION
SUMMARY
T.,
'A0:
Will Turner
Site WT
2022
1
6.20
136,500
7.49
32.50
10.08
2022
2
5.00
188,500
3.92
45.02
19.12
2022
3
8.00
133,000
6.26
29.24
0.00
2022
5
2.60
84,000
4.49
29.37
30.02
2022
6
2.90
84,000
1 3.58
129.42
1 8.40
Totals
4
Total Gallons 626,000
WWTP - Metric Tons 27.88

FIELD APPLICATION SUMMARIES

JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Corn
Rye
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Corn
Rye
BARNES ENVIRONMENTAL WASTE
2022 FIELD APPLICATION SUMMARY FORM
Permit WQ0018525
FIELD WT-01 6.2 ACRES TOTAL GALLONS 136,500
-----------------
-----
-
-
----------
-----------------
-----------------
-
----------------
-----------------
0
111
000©©©00000
I 11
000
0
11 1
00000000000
I l i
000
--
-
--------------
0
1 1
0
�0000
000000000
-----------------
-----------------
-----------------
-----------------
-----------------
------------
-----
li
0
0
0
0
1 11
0
0
11
0
I li
11
11
0
111
111
0
31,500
0
0 0
0
10,500 0
0 3,500
0
10,500
3,500
3,500
0
7,000
17,500
0
0
0
0 0
0
0 0
0 0
0
0
0
0
0
0
24,500
10

JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
13ARNES ENVIRONMENTAL WASTE
2022 FIELD APPLICATION SUMMARY FOR114
Permit WQ0018525
FIELD WT-02 5.0 ACRES TOTAL GALLONS 188,500
----------------LA
-
---------
--------
-----------------
111
111
----
11
----------
-----------------
-
----------------
11I
11
000©
I 11
0©0
11
II
0�0�
I11
38,500
21,000 0 0
0
0
7,000
0 0 0 1 3,500
0
0
0
0
0
7,000
3,500
0 0 0
0
0
3,500
0 0 0 0
3,500
0
0
0
3,500
0
The
Grove
Ocean Bay
Villas
pcean
Club
Ocean
Condos
Ocean
Terrace
Pebble
Beach
Peppertree
Resort
Prne
Knol]
Pomt
Emerald
Queens
Court
Sands
Villa
Sea island
Plantation
Sea
Spray
Sound of
The Sca
Southwtnds
Condos
Summer
Winds
Whaler [nn
3,500
14,000
7,000
3,500
3,500
21,000
7,000
3,500
2,500
3,500
17,500
3,500
3,500
4,000
0
0 1
10,500
0
0
0
0
0
2,500
0
11,000
14,000
14,000
0
7000
38,500
0
0
0
3,500
0
0
0
1 0
0
2,500
0
11,000
10,500
0
0
0
17,-50-0T
0
0
0
7,000
0
0
0
0
0
0
0
0
3,500
14,000
0
1 7,000
21,000
1 0

JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
BARNES ENVIRONMENTAL WASTE
2022 FIELD APPLICATION SUMMARY FORM
Permit WQ0018525
FIELD WT-03 8.0 ACRES TOTAL GALLONS 133,000
-----------------
-----------------
-----------------
-----------
--
----
---------
1
-----------------
III
---------------
11
III
©0000
lil
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1 1
11 1
00©00
1 I 1
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000000
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-----------------
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--
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--------------
00
I 11
00
1 11
i l l
0
11
00
111
00
111
11
0
0
10,500
0
0
10,500
7,000
0
3,500
0
0
7,000
0
0
7,000
14,000
3,500
0
0--..].--
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
BARNES ENVIRONMENTAL WASTE
2022 FIELD APPLICATION SUMMARY FORM
Permit WQ0018525
FIELD WT-05 2.6 ACRES TOTAL GALLONS 84,000
-----------------
-
----------------
-----------------
----------------
-
-----------------
-----------------
-----------------
1 11
I11
000000000000©
111
11
1 1 1
111
0000000000000
111
1 1
0
I11
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--
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--------
---------
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-------------
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--------
--------
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11
0
111
00
111
11
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111
000
00
111
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11
000000
11 I
000
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JAN
FEB
MAR
APR
MAY
J UN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
BARNES ENVIRONMENTAL WASTE
2022 FIELD APPLICATION SUMMARY FORM
Permit WQ0018525
FIELD WT-06 2.9 ACRES TOTAL GALLONS 84.000
Station
Reach
0.
-----------------
-------
----------
-----------------
-----------------
-----------------
-----------------
-----------------
----------
-------
i l i
00���000�
11
I 11
00��0
7,000
0
0
0 0 3,500 0
0
0
0
3,500
7,000
0
0
0
0
0
3,500
0
0
0 0 0 0
0
0
0
0
3,500
0
0
0
0
0
MEMO
-----------------
-----------------
------------
---
-
-----------------
---
--------------
-----------------
0
11
11
11
0
0
11
0
0
0
0©
111
0
111
11
0
0
3,500
3,500
3,500
0
0
3,500
0
0
0
0
0
0
0
0
24,500
0
0
0
0
0
0
0
0
0
0
0
0
3,500
7,000
0
7,000
0
0

FIELD LOADING RATE REPORTS

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name: nerves Fnvironmenial write& Houtlne Permit #: W00018525 Annuni Dry Tons Applied: 7.49
Owner: Will Turner Operator: Steve Barnes Cation Exchange Capacity ( non 503): 2.2
Site #. WT Field #: 1 Acres Utilized: 6.20 Acres Permitted: 6.20
Application Method*: S Volatilization Rnte**: 0.5 Mineralization Rate: 30 %
Predaminnnt Rnil Revircr r:nA
:=as
€
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�
i'
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... �..
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. t4i-t1.
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iN3
2022
14,000
2,259
2.03
0.19
deacons Reach
G/D
0.001
0.000
0.361
0.005
0.000
0.003
0.006
0.002
0.397
5.28
2.28
8.11
Corn
Rye
30.19
0.67
1.36
2022
10,500
1.694
1.30
0.09
Kingsbridge11
GAD
0.000
0.000
0.052
0.005
0.000
0-001
0.002
0.001
0.792
3.34
2.51
Cam
11.06
0.08
0.00
2022
31,500
5,081
1.33
0.28
Tile Grove WWrP
G/D
0.001
0.000
0.068
0.002
0.000
0.005
0.005
0.003
0.393
9.40
9.66
Cam
30,62
1.03
0.01
2022
2022
10,500
3,500
1,694
565
1.34
L35
0.09
0.03
Pebble Beach
I'omi Lincrald
Villa,
G/D
2/D
1 0.000
0.000
0,000
1 0.000
0.057
0.034
1 0,003
0.004
0.000
0.000
0.001
0.000
0,001
0.001
0.00E
0.000
1 0.421
0_152
0.46
1.01
1
1.62
0-89
Cam
Co.
1
12.43
3.91
0.37
0.02
0.00
0.00
2022
10,500
1.694
1.64
0.12
Sands villas
G/D
0.001
1 0.000
0.0591
0.002
0.000
0.001
0.003
0.001
0300
5.17
5.09
Cam
16.97
0.42
1 0.00
2022
3,500
565
0.71
0.02
Sea isle Plantation
G/D
0.000
0.000
0.006
0,001
0.0001
0.000
10.000
0.000
0.033
0.19
0.63
Cam
1.95
0.01
0.00
2022
2022
3,500
7,000
565
1,129
1.69
1.28
0.04
0.06
sea spray
Suuthwm s
do •, ,
G/D
GAD
0.000
0.000
0.000
0.000
0.083
0.065
1 0.002
0.001
0.0001
0.000
0.0001
0,001
0.001
0,001
0.000
0.001
0.119
0.131
0.69
1.39
1.72
2.36
Corn
Corn
3.67
4.58
0.01
0.04
0.00
0.00
2022
42,000
6,774
1.01
0.29
Summer winds
GAD
0.001
0.000
0.652
0.010
0.000
0.003
0,007
0.003
1.101
5.57
7.80
9.68
Cam
Rye
43.88
0.37
0.14
Total
136,500
Annuallbslncre 0.006 0,002 1.438 0.035 0.001 0.015 0.028 0.0I2 3.839 32.50 10.08 42.27
Lime
Arm.
Date
Lbs/Ac
Current Cumulative Ibslncre 0.10 0.06 22.98 0.41 0.01 0.15 0.25 0.14 32.40 147 50 Permit PAN Limt Ist/2nd Crop
Prior Years Crtmrtlative Ibs/acre 0.09 0.06 21.55 0.37 0.01 0.14 0.22 0.13 28.56
PcrmittC,P.L.R."*• 36 34 1338 267 IS N1A 374 89 2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
S1491/9 , x"ej Feb 17 2023
X Steve &I Barnes I.Feb 17, 2023 14:32 FST} , *Application Method: S - Surface, IN - Injection, INC - Incorporation
(Signature of Land Applier) Date **Volatilization Rate: Surface - 0,5, Injection/Incorporation - 1.0
***C.P,L.R.: Cumulative Pollutant Loading Rate
WMSS, PLLC DENR FORM FSF (7A2002) Mod.

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name: names FnvirnnmentaI wnsle & tinulinn Permit 9: W000I8525 Annnal Dry Tons Applied: 8.92
Owner: Will Turner Operator: Steve Barnes Cation Exchange Capacity ( non 503): 6.8
Site #: NVT Field P: 2 Acres Ulilized: 5.00 Acres Permitted: 5.00
Application Method*: S Volatilization Rate**: 0.5 Mineralization Rate: 30 % Predominant Soil Series: GoA
2022
2022
42,000
21.000
8,400
4,200
0.53
2.03
0.19
0.36
Atlantic Station
Beacons Reach
IGID
GID
0.001
0.002
10.000
0.001
0.159
0.672
1 0.003
0,009
0.0001
0.000
0.002
1 0.006
10.003
0.011
0.0021
0,004
0,371
0.739
0.81
19.63
0.08
3.36
15.08
Coastal
Coastal
Rye
7.80
56.16
0.00
1.24
0.04
2.53
2022
10,500
2,100
1.17
0.10
Hampton Suites
GID
0.001
0.000
0.282
0.001
0.000
0.001
0.002
0.001
0,194
2.70
1.35
3.39
Constnl
Rya
13.00
0.07
0.14
2022
3,500
700
1.54
0.04
Genesis Condos
G/D
0.000
0.000
0.041
0.001
0.000
0.001
0.001
0.000
0.072
2.21
1.91
Coastal
7.19
0.26
0,00
2022
3,500
700
0.97
0.03
Hatkers Point
GID
0.000
0.000
0.030
0,001
0.000
0,000
0.001
0.000
0.105
1.13
0.87
Rye
3.74
0.02
0,00
2022
3,500
700
1.49
0.04
McGinnis Point
GID
0.000
0.000
0.126
0.002
0.0001
0.001
1 0.001
0.001
0,118
1.67
2.14
Rye
5.52
0.05
0.00
2022
7,000
1,400
L85
0.11
NC Aquarium m
GID
0.001
0,002
0.083
0.006
0.000
10.003
0.005
0.001
1 0.227
3.47
5.46
Cosslal
11_33
0.32
0.00
2022
10,500
2.100
0.68
0.06 1
Ocean Club
G/D
0.000
0.000
0,034
0.001
0.000
0.001
0.001
0.001
0.165
0.73
1.46
2.88
Coasinl
Rye
7.19
0.19
0.00
2022
2.500
500
1.35
0.03
Point Lmctald
G/D
0.000
0.000
0.030
0.003
0.000
0.000
0.001
0.000
0.134
0.89
0,79
coastal
3.47
0.02
0.00
2022
11,000
2,200
1.64
0.15
Sands Villas
CID
0.001
0.000
0.077
0.002
0.000
0,002
0.004
0.002
0.389
6.72
6.62
Coastal
22.04
0.54
1 0.00
2022
14,000
2,800
0.71
0.08
Sea We Plantation
G/D
1 0.000
0,000
0.026
1 0.005
0,000
0.001
0.002
0,001
0.164
0.96
3.12
Coastal
9.66
0.07
0.00
2022
14.000
2,800
1.68
0.20
Sea spray
GID
0.001
0.000
0.41 l
0.008
D.000
0.002
0.005
D.002
0.588
3.42
8.52
Rye 1
18.19
0.04
0.00
2022
7,000
1.400
1.28
0.07 1
Sau[hwmds
G/D
0.000
0.000
0.081
0.001
0.OD0
0.001
0.001
0.001
0.162
1.72
2.93
Rpt 1
5.69
0.05 1
0.00
2022 1
38,500 i
7.700 1
1.01 1
0.32
Summcrwinds
GID
0.002 I
0.000
0.741
0.012
0.000
0.003
0.008
0.003
1.252
6.9!
8.29
11.00
Coastal
Rve 149.88
0.42
0.15
188,500
Annui! fhs/acre 0.009 0,004 2.795 0.056 0.001 1 0.022 1 0.046 0,018 1 4.687 45.02 19.12 68.08
Current Cumulative Ibslacre 1.89 0.11 81-26 25.16 0.46 0.34 1.07 0.68 99.44 299 1 50 jPertnit PAN Limt lst/2nd
Prior Vears Cumulative lbs/acre 1.88 0.11 78.47 25.10 0.46 0.32 1.02 0.66 94.75
Permiu CT' It.**• 36 34 1338 267 IS NIA 374 89 2498
9certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure triall qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations."
S49yl° IW XN-hEf Feb 17 2023
Y Steve M Barnes (Feb 17, 2023 14:33 EST) t *Application Method: S - Surface, IN - Injection, INC - ]ncorporation
(Signature of Land Applier) Date **Volatilization Rate: Surface - 0.5, Injection./Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
Lime
Date 1
WMSS, PLLC DENR FORM FSF (7/2002) Mod.

ANNUAL LANs} APPLICATION FIELD SUMMARY FORM
Facility Name- tlaraesEnvironmental Wnsle&Hauling Permit#:WOOOIS525 Annual Dry Tons Applied: 6.26
Owner: Will Turner Operator: Steve 1larnes Cation Exchange Capacity ( non 503): 8.2
Site #: WT field ff.- 3 Acres Utilized: 8.00 Acres Permitted: 8.00
Application Method: S Volatilization state": 0.5 Mineralization Rate: 30 %
Predominant19MISorirt- CnA
a::p:p:i:E::
•....1.1?....'•:
::::::::.:::::::>.atti.....
• (tlsF?
f .::f}1
.•
::.1'Csl !: c
�.::IGID
l ..
::fiar;
o-:.:.:.:::.:.:::::•:.:.:.:::.;.;.:.:
.. - - - .......
, .........iklrt37s..#Ili;il,le)
;.::::::..::::.:.:.:.:.:.;,.-.-......::.o-:.:.:•:•::.::-:.:':
.......:.:.:.:.:-:.:::::::::::.:.::•:::.
>::,:':':':::.:.;.;.;.:.;.;.:.: ........... .....:.•
, ....:.:.:-:::::::.:�::.. .......3Vutl`.It:ar3:• 1 .rt
:.:.: ;.;-:-:•:.:.:.;.:.,,...:.:.•.•,
:: . , ......
-
•...
G:
•, - .:i��-l3:2022
17,500
2,188
0,53
0.05
AtlanticStation
G/D
0.000
0.000
0.041
0.001
0.000
0.000
0.001
0.000
0.097
0.23
0,88
Coastal
2.03
0.00
0.012022
28,000
3,500
2.03
0.30
ocasonsResel.
0.001
0.000
0.560
0.008
0,000
0.005
0.009
0.003
0,616
16.36
12.57
Coastal
46.80
1,03
2.11
2022
21,000
2.625
1.04
0.11
ounescape
GID
0.001
0.000
0.158
0.003
D.000
0.001
0.003
0.001
0.569
4,57
4.53
Coastal
15.21
0.02
0.00
2022
3,500
438
0.63
0.01
Eight I!3 Marina
GID
0.000
0.000
0.024
0.001
0.000
0,000
0,000
0.000
0.052
0.17
0.39
Coastal
0.98
0.00
0.01
2022
10,500
1,313
0.68
0.04
Ocean Club
G1D
0.000
0.000
0.021
0.001
0.000
0.000
0.001
0.000
0.103
1,37
1.80
Coastal
4.49
0.12
0.00
2022
10,500
1,313
1.34
0.07
Pebble Beach
CID
0.000
0,000
0.044
0.002
0.000
0.001
0.001
0.061
0.327
0,36
1.25
Coastal
9.63
0.29
0.00
2022 •
2022
7,000 975
3.500 438
0.41 0.01 Pcppenrce G/D
Point Emerald
1.35 0.02 G/D
0.000
0,0001
0.000
0.000
0.013
0.027
0.000
1 0.003
0.000
0.000
0,000
0.000
0,000
0,001
0.000
0.000
0.075
0.118
0,42
0.78
0-52
0.69
Coastal
coastal
1.32
3.03
0.00
0.02
0-02
0.00
2022
2022
7,000 875
7,000 875
0.71 0.03 Sw Isle Plantation G/D
Southrvmds
1.28 0.05 G/D
0.0001
0.000
0.000
0.000
0.009
0.05E
0,002
0.22I
0.000
0,000
0.0001
0.000
0.001
0.00 [
0.000
0.000
0-051
0.101
0.30
1.07
0.98
1.83
Coastal
Coastal
3.02
3.55
1 0.02
0.03
0.00
0.00
2022
14 000 1,750
1.01 0.07 Sumner Windy CID
0.000
0.000
0.168
0.001
0.000
0.001
0.002
0.001
0.285
3,46
2.50
Coastal
11.34
0,10
0.04
2022
3,500 438
0-88 0.02 whaler tnn G/D
0.000
0.000
0.025
0.000
0A00
0.000
0.000
0.000
0.040 1
0,10
0.25
1 Coastal
1.15
0.02
0,00
Total
133,000
Annual lbslacre
0.004
0.001
1.143
0.024
0.00D
0,010
0.020
0.008
2.4.33
29.24 0.00
78.13
Lint
App.
Date
LbsIA
Current Cumulative Ibslacm
0.22
0.41
64.71
1.03
0.01
0.27
0.69
0.24
71.29
299 50
Permit PAN
Limit 1s112nd
Crop
Prlor Years Cumulative Ibs/acre 0.21 0.41 63.57 1.00 0.01 0.26 0.67 0.23 68.85
Permilt C.P.LR.A**
36
34
1338
267
15
NIA
374 1
89
2498
°1 certify, under penally of law, that this document %vas prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, Including the
possibility
of fines and
imprisonment for knowing
violations."
(JAM f "/ �_t��C�iJ
X Steve M Barnes (Feb 17, 2023 i4:33 EST) Feb 17, 2023 *Application Method: S - Surface, IN - Injection, INC - Incorporation
(Signature of Land Applier) Date **Volatilization Rate: Surface - 0,5, Injection/lncorporalion - 1.0
***C.P.L.R.: Cumufalive Pollutant Loading Rote
WMSS, PLLC DENR FORM FSF (7/2002) Mod.

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
f ncility Name: Barnes Enviranmtntat Waste & rlauline Permit #: W 0018525 Annual Dry Tons Applied: 4.49
Owner: Will Turner Operator: Steve Barnes Cation Exclinnge Capacity ( non 503): 5.9
Site #: %VT field #.- 5 Acres Utilized: 2.60 Acres Permitted: 2.60
Application Method*: S Volatilization Rate"*: 0.5 Minernlization Rate: 30 % Predominant Soil Series: GoA
2022
10,500
1 4,038
0.53
0,09
Atlantic Station
G/C
2022
14,000
5,385
2.03
OA6
Beacons Reach
G/D
2022
7,000
2,692
1.49
0.17
McGinnis Point
G/D
2022
3,500
1,346
1,85
0.10
NC Arineriann al
1 Pine Knoll Shores
GID
-Ue Grove
2022
24,500
9,423
1.33
0.52
>,vtv-rP
G/D
2022
7,000
2,692
0.68
0.08
Ocean Club
G/D
2022
7,000
2.692
1.34
0.15
Pebble Beach
G/D
2022
3.500
1,346
0.41
0.02
1'eRl"nr`°
G/D
2022 1
7.000
1 2,692
1.24
0.14
Sound 0l The Sca
C,/p
Total
Annual Ibs/acre
Current Cumulative Ibs/acre
Prior Years Cumulative Ibs/acre
Permitt C.P.L.R.***
1 certify, under penalty of law, that this document was p
designed to assure that qualified personnel properly Bathe
significant penalties for submitting false information, incl
repared
red
'sib, t ..••�
t k1411'f
S¢..:, f�.
.. Ibs
_
:i..:.
.p .a:
�t'a•:,::::
- ..
..
0.000
0.000
0.076
0.001
0.000
0,001
0,001
0.001
0,178
0.43
1.62
Coesral
3.75
0.00
0.02
0.002
0.001
0,861
0.012
0,000
0.007
0.015
0,005
0,947
12,58
12.58
19.34
Co,stol
Rye
72.00
1.59
3.24
0.001
0.000
0.484
0.007
0.000
0,003
0.004
0.002
0.455
6.42
8.24
Coastal
21.24
0.t7
0.01
0.001
0.002
0.080
0.005
0.000
0,003
0.005
0.001
0.219
3.33
5.25
Coastal
10.90
0.31
0.00
0.003
0.001
0.126
0.004
0.000
0.009
0.009
0.005
0.730
17.44
17.92
Rye
56.79
1.92
0.02
0.000
0.000
0.043
0.001
0.000
0.001
0.001
0.00E
0.212
2.91
3.70
Cna41a1
9.21
0.24
0.00
0.001
0.000
0.091
0.005
0.000
0.002
0.002
0.002
0.670
0-73
2.57
Coastal
19,75
0.59
0.00
0.000
0.000
0.02E
0.001
0.000
0.000
0.001
0.000
0.115
0.64
0.80
Coastal
2.03
0.00
0.03
0-001
0,000
0.372
0,006
0.000
0.001
0.003
0.001
0.717
2.43
6.76
Coastal
21.00
0.49
0,00
0.009
0.004
2.155
0.043
0.001
0.027
0.04E
0.018
4.243
29.37
30.02
66.18
Li mc
A
0.129
0.088
22.593
0,568
O.OI 1
0.205
0,371
0.184
36.492
299
50
Permit PAN Limt Ist/2ad Crop
Date
Lbs/Ac
0.120 0.084 20.428 0.526 0.010 0.178 0,329 0.167 32.249
36 34 1338 267 15 NIA 374 89 2498
under my direction or supervision in accordance with a system
and evaluated the information submitted. I am aware that there are
uding the possibility of fines and imprisonment for knowing violations."
c�t2Y2 /G/&wf
X Steve tv1 Barnes (Feb 17, 202314:33 EST) Feb 17, 2023 *Application Method: S - Surface, IN - Injection, INC - Incorporation
(Signature of Land Applier) Date **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
WMSS, PLLC DENR FORM FSF (712002) Mod.

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name: 13nrnesrwiranorce.0 Waste& Muting Permit H: W00018525 Annual Dry Tons Applied: 3.58
Owner: Will Turner Operator: Steve Ilnrnes Cation Exchange Capacity J; P ty (non 503): 6,7
Site #: PVT Field f: 6 Acres Utilized: 2.90 Acres Permitted: 2.90
Application Method*: S Volatilization Rate**: 0,5 Mineralization Rate: 30 % Predominant Soil Series: GoA
2022
10,500
1 3,621
0.53
10.08
AdantieStation
I GID
0,000
10.000
10.068
10.00110.000
0.001
10.0011
0.001
0.1601
0.25
0.12
Colony Uy I tic
2022
3,500
1,207
1.63
0.08
sea
GID
0.000
0.000
0.035
0.002
0.000
0.001
0.002
0.001
0.348
2.04
2022
3,500
1,207
1.54
0.08
Genesis Condos
G1D
0.000
0.000
0.070
0.002
0,000
0.001
0.002
0.001
0.134
3.81
2022
10,500
3,621
0.97
0,15
Parker's Point
GID
0,001
0,000
0.155
0.006
0.000
0.001
0.003
0.001
0.542
3.89
1,95
2022
3,500
1,207
1 0.43
0,02
1 ocean Bay Villas
GID
1 0.000
0.000
0.012
0.001
0.000
0.000
0.001
0,000
0.056
0.75
2022
3.500
1,207
0.68
0.03
OceaaClub
Oceans
GID
0.000
0.000
0,019
0.000
0.000
0.000
0.001
0,000
0.095
1.26
2022
3.500
1,207
1.66
0.08
Condominiums
GID
0.000
0.000
0,083
0.003
0.000
0.001
1 0.002
0.001
0.194
0.18
2022
3,500
1,207
0.41
0.02
Peppenree
GID
0.000
0.000
0.018
0,001
0.000
0.000
0000
0,000
0.103
0.58
2022
3.500
1,207
0,71
0.04
Sea Isle,Planiatlon
GID
0,000
0.000
0.012
0.002
0.000
0.000
1 0,001
0.000
0.071
0.41
2022
7,000
2,414
L68
0.17
Sn Spray
GID
J 0.001
0.000
0.354
1 0.007
0.000
0.002
0.004
0.002
0.5071
2.95
2022
7,000
2,414
1.28
0.13
Condominiums
GID
1 0.001
0.000
0,140
0,003
0.000
0.001
1 0,002
0.001
0.279
2.96
2022 1
24,500
8,448
1,01
0,36
Summcrlvinds
GID
0,002
O.D00
1 0.913
0.013
0.000
0.004
0,009
0.004
1.3731
115.68
Annual lbslacre 1 0,0061 0.0021 1.7811 0.0401 0.001_1 0.0131 0.0271 0.01213.863129.42 1 8.41
Current Cumulative lbslacre 10.10910.060 127,I461 0.6201 0.011 1 0.193I 0.409I 0.193143,8731 299 1 50
Prior Years Cumulative lbstacrel 0.103 10.058 25.365 0.580 0.010 0.171 0.382 0.181 140.015
Permilt C.P.L.R.*** 1 36 1 34 1 1338 L267 L.15 I N/A 1 374 1 89 2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
�. eve Rxamff b
1.45
Coastal
Rye
3.36
0.00
0.02
1.36
Coastal
6.69
0.14
0.00
3.30
Coastal
12.39
0.44
0.00
4.50
Coastal
Rye
19.35
0.10
0.01
0.46
Coastal
2,40
0.00
0.03
L66
Coastal
4.13
0,11
0.00
2.54
coastal
12.19
0.19
0.00
0.72
Coastal
1.82
0.00
0.03
1.34
Rye
4.16
0.03
0.00
7.35
Rye
15,68
0.04
0.00
5.05
Ryc
9.80
0.09
0.0
�0,170
2.07
Coasts[
54.72
0.46
Lime
PAN Limit Istl2nd Cron Date 1
X Steve M Barnes17, 2023 14:33 EST) Fe L r , 2023
(Feb( *Application Method; 5 -Surface, IN - Injection, INC -Incorporation
(Signature of Land Applier) Date "Volatilization Rate: Sutface -0.5, InjectiontIncorporation - 1.0
'•'C.P.L.R.: Cumulative Pollutant Loading Rate
WN1SS, ?LLC
DENR FORM FSF (712002) Mod.

Barnes Environmental -2022 Signature Pages
Final Audit Report 2023-02-17
Created:
2023-02-17
By:
Martin Mabe ([e-mail])
Status:
Signed
Transaction ID:
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SOIL ANALYSIS REPORTS

Page 1 of 2
Report Number: 22-024-1380
°
Account Number:08361
��
po
7621 Whitepine Road, Richmond, VA 23237
M
Main 804-743-9401 ° Fax [phone]
Send To:
Willcox & Mabe Soil Solutions, PLLC
ANALYTICAL
www,waypointanalytical.com
7231 B. Summe>field Rd
Every acre ...Fveryyear."„r
Grower: Steve Barytes
Summerfield NO 27358
WMSS Jab No. 15+-02
SOIL ANALYSIS REPORT
AnalyticalMethod(s): Mehlich3 SMPBufferpH LossOnlgniffon
waterpH
Date Received: 01/24/2022 Date Of Analysis, 01/25/2022
Date Of Report: 01/2512022
Sample ID
Lab OM WN LcNR
Phosphorus Potassium
Magnesium Calcium Sodium pH Acidity
C-E.0
Field ID
Number O/C Saif tbs/A
M3
K
Mg Ca Na Soil Buffer H
Rate Class
ppm Rate
ppm Rate ppm Rate ppm Rate
ppm Rate ppm Rate ppm Rate PH index meq/100g
meg1140g
WRT-01
22809 1.1 70
232 VH
42 L
31 H 164 L 11 L 5.4 6.88 0.5
1.7
L
NC=193
NC=21
I
WRT 02
22810 2.3 94
133 VH
13 VL
28 M 194 M 16 M 5.6 6.89 0.4
1.7
L
NC=Ill
NC=7
WRT-03
22811 8.2 150
623 VH
29 VL
144 L H 35 VL 6.5 1.2
15.9
VH
NC=519
NC=15
12650
WRT-05
22812 2.3 83
472 VH
39 VL
84 L 1514 H 26 VL 6.5 0.7
9.2
L
NC=393
NC=20
WRT 06
22813 1.7FT 79
114 VH
15 VL
44 M 476 M 20 L 6.0 6.88 0.5
3.4
L
NC=95
NC=B
Sample ID
Percent Base Saturation
Nitrate
Sulfur Zinc Manganese
Iron Copper Boron Soluble Sails
Field ID
K Mg Ca Na H
NO, N
S Zn Mn
Fe Cu B SS
% % % % %
ppm Rate
ppm Rate pprn Rate ppm Rate
ppm Rate ppm Rate ppm Rate mslcm Rate
WRT01
6.3 15.2 46.2 2.8 29.4
9 VL 2.1 L 2 VL
176 VH 1.7 H 0.2 VL
NC-19 NC=52.5 NO 13
NC=85.0
WRT02
2.0 13.7 57.1 4.1 23.5
13 L 2.9 M 1 VL
367 VH 5.5 VH 0.2 VL
NC=27 NC=72.5 NC
NC=275.0
WRT-03
0.5 7.5 83.3 1.0 7.5
17 M 77.8 VH 4 L
300 VH 45.8 VH 1.8 H
NC = 35 NC = 1945.0 NO = 25
NC = 2290.0
WRT-05
1.1 7.6 82.3 1 1.2 7.6
25 M 56.0 VH 4 L
178 VH 17.0 VH 0.6 M
NO = 52 NO = 1400.0 NC = 25
1 NC = 850.0
WRT-06
1.1 10.8 70.0 2.6 14.7
16 M 14.6 VH 1 VL
4.4 VH 0.4 L
179 VHTNC
NC=33 NC=365.0 NC=6
=220.0
Values on this report represent the plant available nuirients In the
Explanalion of symbols: % (percent), ppm (pails per million), Ibs1A
This report applies to sample(s) tested. Samples are retained a
soil. Rating after each
value: VL (Very Low), L (Low), M (Medium),
(pounds per acre),
ms/cm (milli -mhos per centimeter), meg1100g
maximum of thirty days after testing.
H (High), VH (Very High). ENR - Eslimated Nitrogen Release.
(milli -equivalent per 100 grams), Conversions: ppm x 2 - Ibs1A, Soluble
pp
by: 7ay.Y Mr
Analysis
frrvw
C.E.C. - Callan Exchange Capacity.
Sails mslcm x 640 n ppm.
prepared by: waypointAnalytical Virginia, Inc.
Pauric Mc Groary
Ph,D., CPAg

Page 2 of 2
Report Number: 22-024-1380 °
a
Account Number:08361 ��l�w 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
Send To: Willcox & Mabe Soil Solutions, PLLC ANALYTICAL www.waypointanalytical.com
7231 B. Summerfield Rd "Every acre ...Everyyear Grower: Steve Barnes
Summerfield NC 27358 WMSS Job No. 15+-02
Date Received: 01/24/2022
Date Of Report: 01/25/2022
SOIL FERTILITY RECOMMENDATIONS
Sample !D
Nitrogen Phosphate Potash Magnesium
Yield Goal Lime
Sulfur
Zinc
Manganese
ron
Copper
Boron
Field Ib
Intended Crap
bu TonslA N Pab 5 K0 M9 z
S
Zn
Mn
Fe
�b/A
Cu
13
lb/A lb/A Ib1A Ib/A
Ib/A
1b1A
Ib/A
Ib/A
Ib/A
WRT01
Soybeans
45 0.8 15 0 95 19
11
3.0
4
0
0
1.0
W RT-01
Corn
125 0.8 153 0 122 19
22
2.4
6
0
0
1.5
W R7 oz
Bermuda, Coastal
5 0.8 75 0 467 21
22
0
4
0
0
0.5
W RT-03
Bermuda, Coastal
5 0.0 75 0 500 0
17
0
3
0
0
0
W RT-05
Bermuda, Coastal
5 0.0 75:10 492 0
9
D
3
0
0
0
W RT-06
Bermuda, Coastal
5 0.5 75 0 483 14 F
19
0
4
0
0
0.5
Comments:
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning
crop performance is made."
Our reports
and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the
l tic
r
(rrowq/
work,the
results, or the company In any advertising, news release, or other public anouncements wllhout obtaining our prior written authorization. Copy right
1977.
o
Pauric Mc Groary Ph.D., CPAg