HomeMy WebLinkAboutWQ0011448_Residual Annual Report_20230317Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Permit Number (IR) *
W00011448
Applicant/Permittee
Town of Snow Hill
Email Notifications
Does this need review by the hydrogeologist? *
Yes No
Regional Office
Washington
CO Reviewer
Admin Reviewer
Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Drew Matthews
Email Address*
dmatthews@soilplus.net
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
252-883-9301
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0011448
Has Current Existing permit number
Applicant/Permittee Address*
PO Box 247 Snow Hill, NC 28580
Facility Name*
Town of Snow Hill Class B Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at nathaniel.thornburg@ncdenr.gov.
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2022 Snow Hill Annual Report.pdf 4.18MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
,►��Ati �atbFex�Z
Submission Date 2/17/2023
TOWN OF SNOW HILL
2022 ANNUAL LAND APPLICATION OF
RESIDUAL BIOSOLIDS REPORT
CLASS B PROGRAM
WQ0011448
Submitted by:
Soil Plus
P.O. Box 1396
Oxford, North Carolina 27565
February 16, 2023
SOIL PLUS
SOIL PLUS
February 16, 2023
NCDEQ-DWR
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Re: 2022 LAND APPLICATION ANNUAL REPORT
Town of Snow Hill "Class B" Program
NC Permit No.: WQ0011448
Soil Plus Project No. 200804.A10
Information Processing Unit:
Soil Plus, LLC (Soil Plus) is submitting all monitoring and reporting requirements as
specified in the above referenced permit for the Town of Snow Hill on behalf of Granville
Farms, Inc. Soil Plus compiled this report using data gathered during the compliance year.
This data includes (1) certification form, (2) residual sampling, (3) field loading calculations,
(4) pathogen and vector attraction reduction documentation, (5) standard soil fertility
nutrient analysis.
The Town of Snow Hill conducted application events on one permitted field in Greene
County during 2022. A total of 22.37 Dry Tons or 339,450 Gallons of permitted residual
biosolids were land applied to the permitted field.
If there is any further information required or questions regarding this report, please do
not hesitate to contact me or the Town of Snow Hill (252-747-3414) for further assistance.
Respectfully,
Drew Matthews, Soil Plus
cc: Todd Whaley, Town of Snow Hill
Jason Smith, Granville Farms
P.O. Box 1396
Oxford, NC 27565
(252)883-9301
dmatthewsgsoilplus. ne t
www.soilplusuc.com
Town of Snow Hill
2022 Annual Land
Application of
Residual Biosolids
Report
WQ0011448
Snow Hill, NC
ANNUAL LAND
APPLICATION
CERTIFICATION FORM
Source Summary
Field Loading Summary
ANNUAL RESIDUAL
SAMPLING SUMMARY
FORM
Analytical Data
TCLP
FIELD LOADING
SUMMARY FORM
Town of Snow Hill Farm
ANNUAL PATHOGEN &
VECTOR ATTRACTION
REDUCTION FORM
Fecal Coliform Data
30-Day Bench Scale Test
SOIL SAMPLES
Town of Snow Hill Farm
Town of Snow Hill
2022 Class B Annual Report
WQ Permit# WQ0011448
Annual Certification Form
Source Summary
Field Loading Summary
ANNUAL LAND APPLICATION CERTIFICATION FORM
PermitNumber FacilityName Land Application Operator County Phone Number
WQ0011448 Town of Snow Hill Granville Farms, Inc. Greene (252) 747-3414
Year: 2022
Land application of residuals as allowed by the permit occurred during the past calendar year? If No, skip Part A, and Part Yes No
B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the ❑� ❑■
residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in the permit: 1
Total number of fields utilized for land application during the year: 1
Total amount of dry tons applied during the year for all application sites: 22.37
Total number of acres utilizes for land application during the year: 11.4
Part B - Annual Compliance Statement:
Facility was compliant during calendar year with all conditions of the land application permit? Yes No
Including but not limited to items 1-13 below) issued by the Division of Water Quality ❑d ❑-
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory
results are attached
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of
certified laboratory results are attached
6.The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T
7. All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities)
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was
received from the Division of Water Quality
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to
include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, ' ing the possibility of fines and
imprisonment for knowing violations." /t . :4 ) //
Todd Whaley, Town Manager /�\LJ�-,
Af-
Permit a Name and Title (type or print): Signature of Permittee D
1/25/23
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
Source Summary Report
WWTP L VolumeApplied Total Dry TM
Town of Snow Hill WWTP 339,450 22.37
Total 339,450 2237
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Town of Snow Hill
2022 Class B Annual Report
WQ Permit# WQ0011448
Residual Sampling Summary Form
Field Loading Calculations
2022 Analytical
2022 TCLP
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&,,AGMAN FIELD LOADING ESTIMATES
Facility Town of Snow Hill VP P
Sampling Date 7/7/2022
Solids 1.58
Mineralization Rate 0.3
Gallons per DT 15,177.73
pH 6.5
Sodium Absorpotion 1.99 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 52,300 lbs./1,000 gal 6.89
Ammonia Nitrogen (mg/Kg) 829.00 lbs./1,000 gal 0.11
Nitrate -Nitrite (mg/Kg) 36.00 lbs./1,000 gal 0.00
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 15,892 lbs./1,000 gal 2.09
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 16,306 lbs./1,000 gal 2.15
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 1.20
Phosphorus lbs./1,000 gal 3.53
Calcium lbs./1,000 gal 1.69
Magnesium lbs./1,000 gal 0.60
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
3.16
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
1.54
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
392.00
Copper lbs./1,000 gal
0.05
Lead (mg/Kg)
23.20
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
1.33
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
91.80
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
3.16
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
645.00
Zinc lbs./1,000 gal
0.08
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
52,300
15,892 31.78
36,408
52,300
16,306 32.61
35,994
36,408
5,461 10.92
30,947
35,994
5,399 10.80
30,595
30,947
2,321 4.64
28,626
30,595
2,295 4.59
28,300
28,626
1,073 2.15
27,552
28,300
1,061 2.12
27,239
27,552
517 1.03
27,036
27,239
511 1.02
26,728
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 25,264 50.53
Total 25,572 51.14
Contact: Drew Matthews
Client: Soil Plus
P.O. Box 1396
Oxford, NC 27565
Meritech Work Order # 070722123
Parameters
% Total Solids
Ammonia, Nitrogen
TKN
Nitrate/Nitrite, Nitrogen
Aluminum, total
Arsenic, total
Cadmium, total
Calcium, total
Copper, total
Lead, total
Magnesium, total
Mercury, total
Molybdenum, total
Nickel, total
Phosphorus, total
Potassium, total
Selenium, total
Sodium, total
Zinc, total
pH
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Results
Sample: SH 070722 Grab
1.58 %
829 mg/kg
52,300 mg/kg
36 mg/kg
5,500 mg/kg
<3.16 mg/kg
1.54 mg/kg
12,800 mg/kg
392 mg/kg
23.2 mg/kg
4,580 mg/kg
1.33 mg/kg
5.33 mg/kg
91.8 mg/kg
26,800 mg/kg
9,100 mg/kg
<3.16 mg/kg
8,230 mg/kg
645 mg/kg
6.5 S.U.
Analysis Date
7/8/22
7/19/22
7/12/22
7/14/22
7/26/22
7/26/22
7/26/22
7/26/22
7/26/22
7/26/22
7/26/22
7/12/22
7/26/22
7/26/22
7/26/22
7/26/22
7/26/22
7/26/22
7/26/22
7/8/22
Report Date: 7/27/2022
Project: Snow Hill
Date Sample Rcvd: 7/7/2022
Reporting Limit
0-100 %
10 mg/kg
20 mg/kg
10.0 mg/kg
2.50 mg/kg
3.16 mg/kg
0.100 mg/kg
10.0 mg/kg
1.00 mg/kg
0.500 mg/kg
10.0 mg/kg
0.02 mg/kg
0.250 mg/kg
0.500 mg/kg
1.00 mg/kg
20.0 mg/kg
3.16 mg/kg
20.0 mg/kg
0.500 mg/kg
1.0 - 14.0 S.U.
7/7/22
Method
SM 2540B
EPA 350.1
EPA 351.1
EPA 353.2
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 245.1
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
SM 4500-HB
I hereby certify that I have reviewed and approve these data. J
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.(336)342-4748 fax.(336)342-1522
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Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
■
Page 1
Contact: Drew Matthews
Report Date:
7/28/2022
CIient: Soil Plus
P.O. Box 1396
Project:
Snow Hill
Oxford, NC 27565
Date
Sample Rcvd:
7/7/2022
Meritech Work Order # 070722122 Sample: SH 070722 Crab
7/7/2022
1311- TCLP Metals
Parameter
Results Analysis Date Det. Limit
Reg. Limit
Method
Arsenic
<0.100 mg/L 7/27/2022 0.100
5.0
EPA 200.7
Barium
<0.050 mg/L 7/27/2022 0.050
100.0
EPA 200.7
Cadmium
<0.020 mg/L 7/27/2022 0.020
1.0
EPA 200.7
Chromium
<0.050 mg/L 7/27/2022 0.050
5.0
EPA 200.7
Lead
<0.100 mg/L 7/27/2022 0.100
5.0
EPA 200.7
Mercury
<0.02 mg/L 7/12/2022 0.02
0.2
EPA 245.1
Selenium
<0.100 mg/L 7/27/2022 0.100
1.0
EPA 200.7
Silver
<0.050 mg/L 7/27/2022 0.050
5.0
EPA 200.7
TCLP Organics
Parameter
Results Analysis Date Reporting Limit
Method
Volatiles 8260
Semi Vol. 8270
Attached
Attached
7/15/2022
7/18/2022
-
-
8260
8270
Other Tests
Parameter
Results
Analysis Date
Reporting Limit
Method
Cyanide, total
<0.500 mg/kg
7/8/2022
0.500 mg/kg
EPA 335.4
Sulfide
<10.0 mg/kg
7/14/2022
10.0 mg/kg
SM4500S2D
Flash Point
>140 °F
7/8/2022
-
EPA 1020C
Corrositivity (pH)
6.5 S.U.
7/8/2022
1.0 -14.0 S.U.
SM 4500 HB
642 Tamco Road, Reidsville, North Carolina 27320
tel.(336)342-4748 fax.(336)342-1522
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
PA
.
Page 2
Contact: Drew Matthews Report Date: 7/28/2022
Client: Soil PIus
P.O. Box 1396 Project: Snow Hill
Oxford, NC 27565 Date Sample Rcvd: 7/7/2022
Meritech Work Order # 070722122 Sample: SH 070722 Grab 7/7/2022
1311 - TCLP Pesticides & Herbicides
Pesticide - SW-846 8O81A
Parameter Results Analvsis Date Det. Limit Reg._Urnit Dilution Factor
Endrin
Attached - - -
Chlordane
Attached - - -
Toxaphene
Attached - - -
Methoxychlor
Attached - - -
Heptachlor
Attached - - -
Lindane
Attached - - -
Herbicides - SW-846 8151A
Parameter
2,4-D
2,4,5-TP (Silvex)
Results Analysis Date Det. Limit Reg. Limit Dilution Factor
Attached
Attached
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.(336)342-4748 fax.(336)342-1522
:�. MERITECH, INC.
Environmental Laboratories
- Laboratory Certificate #165
Client: Soil Plus
Project: Snow Hill
Client Sample ID: SH070722
Sample Collection: 07/07/22
Meritech Sample ID: 070722122
1311 - TCLP Oraanics
Volatiles: SW-846 8260
Analysis: 07/ 15/22
Extraction:
07/ 11122
Analyst: VWV
Report Date:
07/18/22
Parameter
Result
Units
Det. Limit
Reg. Limit
Dilution Factor
Benzene
< 0.0100
mg/L
0.0100
0.50
10
Carbon Tetrachloride
< 0.0100
mg/L
0.0100
0.50
10
Chlorobenzene
< 0.0100
mg/L
0.0100
100
10
Chloroform
< 0.0100
mg/L
0.0100
6.0
10
1,2-Dichloroethane
< 0.0100
mg/L
0.0100
0.50
10
1,I-Dichloroethene
<0.0100
mg/L
0.0100
0.70
10
Methyl Ethyl Ketone
< 0.100
mg/L
0.100
200
10
Tetrachloroethylene
< 0.0100
mg/L
0.0100
0.70
10
Trichloroethene
< 0.0100
mg/L
0.0100
0.50
10
Vinyl Chloride
< 0.0200
mg/L
0.020
0.20
10
Semi-Volatiles: SW-846 8270
Analysis: 07/18/22
Extraction:
07/11/22
Analyst: PM
Report Date:
07/23/22
Parameter
Result
Units
Det. Limit
Reg, Limit
Dilution Factor
1,4-Dichlorobenzene
<0.100
mg/L
0.100
7.5
10
Hexachlorobenzene
<0.100
mg/L
0.100
0.13
10
Hexachloro-1,3-butadiene
<0.I00
mg/L
0.100
0.5
10
Hexachloroethane
<0.100
mg/L
0.100
3.00
10
o-cresol
<0.100
mg/L
0.100
200
I0
m&p-cresol
<0.200
mg/L
0.200
200
10
Total cresols
<0.300
mg/L
0.300
200
10
Nitrobenzene
<0.100
mg/L
0.100
2.00
10
Pentachlorophenol
<0.500
mg/L
0.500
100
10
Pyridine
<0.100
mg/L
0.100
5.0
10
2,4,5-Trichlorophenol
<0.100
mg/L
0.100
400
10
2,4,6-Trichlorophenol
<0.100
mg/L
0.100
2.00
10
2.4-Dinitrotoluene
<0.100
mg/L
0.100
0.13
10
I hereby certify that I have reviewed and approve these data. V. &I L/L,
Laboratory Representative
642 Tamco Road * Reidsville, NC 27320
(336) 342-4748 * info@meritechlabs.com
Summit Environmental Technologies. Inc.
W04; 22070645
*Y"
3310 Win St.
= :, • ^ Cuyahoga Falls, Ohio 44223
Date Reported: 7/22/2022
/L1h9iyG
L L*Y?!arr
TEL: (330) 2534211 FAX.- (330) 253-4484
Company: Meritech Environmental Laboratories
Websile: http:llWWW.settek.com
Address: 642 Tamco Rd.
Reidsville NC
27320
Received: 7/ 13/2022
Project#:
TCLP Pesticides Analysis (SW1311/8081)
Client ID#
Lab M# Collected Analyse Rep Lmt Result Units
Matrix Method DF
Re-Lvl
25
Run
Analyst
070722-122
001
7/7/2022 Chlordane, total 25.0 ND pg1L
Sludge EPA 8081 B 10
30.0
7/2112022
PGP
070722-122
001
717/2022 Toxaphene 50.0 ND pg1L
Sludge EPA 8081B 10
500
7/21/2022
PGP
070722-122
001
7/7/2022 Enddn 5.00 ND pg/L
Sludge EPA 8081 B 10
20.0
7121 t2022
PGP
070722-122
001
7/7/2022 gamma-BHC 5.00 ND pg/L
Sludge EPA8081B 10
400
7121t2022
PGP
070722-122
001
7/7/2022 Heptachlor 5.00 ND pg/L
Sludge EPA 8081B 10
8.00
7/21/2022
PGP
070722-122
001
7/7/2022 Heptachlor epoxide 5.00 ND pg/L
Sludge EPA 8081E 10
8.00
7/21/2022
PGP
070722-122
001
7/7/2022 Methoxychlor 5.00 ND pg/L
Sludge EPA 8081E 10
10000
7/21/2022
PGP
TCLP Herbicides by EPA 8321B
Client ID#
Lab ID#
Collected Analyte Rep Lmt Result Units
Matrix Method DF
RegLvl
Run
Analyst
070722-122
001
7/7/2022 2,4-D 0.500 ND mg/L
Sludge EPA8321B 50
10.0
7/20/2022
PGP
070722-122
001
7/7/2022 2,4,5-TP 0.500 ND mglL
Sludge EPA8321B 50
1.00
7/20/2022
PGP
Page 4 of 11
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Town of Snow Hill
2022 Class B Annual Report
WQ Permit# WQ0011448
Land Application Field Summary Form
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Town of Snow Hill
2022 Class B Annual Report
WQ Permit# WQ0011448
Pathogen & Vector Attraction Reduction Form
Fecal Coliform Geometric Mean
30-Day Bench Scale Test
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Snow Hill WQ Permit Number: WQ0011448
WWTP Name: Town of Snow Hill WWTP NPEDS Number: NCO020842
Monitoring Period: 01/01/2022 to 12/31/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not .-applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 1
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Not .-applicable
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 3,190 4,019 5,411 0 Annually Grab Samples
Weight)
Analytical Technique S1I 9222 D
Vector Attraction Reduction Performed (15A NCAC 02T .1107): Alt. 3 (30-day bench)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
❑ requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Drake Robart, OW'
Preparer Name and Title (type or print)
Signature of Preparer* Date
Jason Smith, V1'
Land Applier Name and Title (if applicable)(type or print)
' 1 /25/23
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Owl -
Page 1
Contact: Drew Matthews Report Date: 7/14/2022
Client: Soil Plus
P.O. Box 1396 Protect: Snow Hill
Oxford, NC 27565 Date Sample Rcvd: 7/7/2022
Meritech Work Order # 070722114 Sample: SH 070722 (001) Grab 7/7/22
Parameters Results Analysis Date Reporting_Limit Method
% Total Solids 1.69 % 7/8/22 0-100 % SM 2S40B
Fecal Coliform (Sludge) 3,766 CFU/g dry wt 7/7/22 130 CFU/g dry wt SM 9222D
Meritech Work Order #
Parameters
% Total Solids
Fecal Coliform (Sludge)
070722115 Sample: SH 070722 (002) Grab
Results Analysis Date
1.70 % 7/8/22
4,813 CFU/g dry wt 7/7/22
Reporting Limit
0-100 %
130 CFU/g dry wt
7/7/22
Method
SM 2540B
SM 9222D
Meritech Work Order #
070722116 Sample: SH 070722 (003) Grab
7/7/22
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
1.71 % 7/8/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
3,190 CFU/g dry wt 7/7/22
130 CFU/g dry wt
SM 9222D
Meritech Work Order #
070722117 Sample: SH 070722 (004) Grab
7/7/22
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
1.71 % 7/8/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
5,316 CFU/g dry wt 7/7/22
130 CFU/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.(336)342-4748 fax.(336)342-1522
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
4
Page 2
Contact: Drew Matthews Report Date: 7/14/2022
Client: Soil Plus
P.O. Box 1396 Project: Snow Hill
Oxford, NC 27565 Date Sample Rcvd: 7/6/2022
Meritech Work Order # 070722118 Sample: SH 070722 (005) Grab 7/7/22
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
1.71 %
7/8/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
3,190 CFU/g dry wt
7/7/22
130 CFU/g dry wt
SM 9222D
Meritech Work Order #
070722119 Sample: SH 070722 (006) Grab
7/7/22
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
1.68 %
7/8/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
5,411 CFU/g dry wt
7/7/22
130 CFU/g dry wt
SM 9222D
Meritech Work Order # 070722120 Sample: SH 070722 (007) Grab 7/7/22
Parameters Results Analysis Date Reporting Limit Method
% TotaI Solids 1.71 % 7/8/22 0-100 % SM 2540B
Fecal Coliform (Sludge) 3,190 CFU/gdry wt 7/7/22 130 CFU/g drywt SM 9222D
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.(336)342-4748 fax.(336)342-1522
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Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Ar-
r
Contact: Drew Matthews Report Date: 8/22/2022
Client: Soil Plus
P.O. Box 1396 Project: Snow Hill
Oxford, NC 27565 Date Sample Rcvd: 7/7/2022
Vector Attraction Reduction
Aerobically Digested Sludge
30 Day Test
Meritech Work Order # 070722121
Sample: SH 070722 Grab
7/7/22
Total Solids
Volatile Solids
% Volatile Solids
Week 1
1.63
1.18
0.724
Week 2
1.57
1.17
0.749
Week 3
1.58
1.17
0.744
Week 4
1.12
0.780
0.691
Week 5
1.00
0.740
0.739
Mass Balance Equation = -2.05% Volatile Solids Reduction as per EPA Part 503 Biosolids Rule
I hereby certify that have reviewed and approve these data. a
Laboratory Representative
642 Tamco Road, ReidsvilIe, North Carolina 2 73 20
tel.(336)342-4748 fax.(336)342-1522
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WQ Permit# WQ0011448
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