WQ0001953_2022 Residual Annual Report_20230215 (2)

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * W00001953
Applicant/Permittee Town of Spindale
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Asheville
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Guy O'Connor
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
8284479588
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0001953
Has Current Existing permit number
Applicant/Permittee Address*
327 Ecology Street Spindale NC 28160
Facility Name*
Town of Spindale Class B Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2022 land application report.pdf 14.06MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
�J 00atraot
Submission Date 2/15/2023

ANNUAL. LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0001953 County:
Facility Name (as shown on permit):
Land Application Operator:
Rutherford
Year: 2022
Town of Spindale
US Biosolids. Inc. Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year"
0 Yes L.1 No - If No, skip Part A, and Part R and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in the permit J 6
_ Total number of fields utilized for land application during the year: 4
Total amount of dry tons applied daring the year for all application sites: 102.38
Total number of acres utilizes for land application during the year: _ 58.3
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2022 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. rJ Yes 1 No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were app_Ifed to the permitted sites.
2) Soil pli was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pl1 of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TC'LP analysis (if required)1vas performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during; the year as required and three
(3) copies ofcertified laboratory results are attached.
6) The facility did not exceed any ofthe Pollutant Concentration Limits in 15A NCAC 02T .1 105(a) or the Pollutant
Loading Rates in 15A NCAC 021' .1 105(b) (applicable to 40,CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 (FR Part
503 regulated (acilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1 1 1 1 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) Ail operations and maintenance requirements in the permit were complied with or. in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
I ) ) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoffof residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification: -
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Perrrtittee Name and Title (type or print) Signature of Permittee Date
2lj /a
Signature of Preparer* Date.
(if'different from Permittee)
* Preparcr is defined in 40 CFR Part 503.9 (r) and 15A NCAC 021
SighSture of band Applier
'21,0- ?o 33
Date
(if'different from Permittee and Prcparer)
.1 102 (26) DENR FORM ACF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Spindale 'Total Dry Tons Applied (Annual):
Permit #: WQ0001953 Cation Exchange Capacity (non 503 only):
Operator: John McFadden Owner: John McFadden Predominant Soil Series:
Acres Used: 15.1 Acres Permitted: 15.1 Site #: M I Field #:
10.40
PaC2
MI
Residual Analysis Data (liesvv Metnic and Tntal Ptrnenhn...c ..moo ..,.,n,.. 01 ..-- 11_... n_____. -
Total
Phos-
Total
2;
__..
3i
4'
S
6'
7
8
9j
10
11'
12'
DT Ac.,,
App-�^,
Event
0.69
Arsenic
0.034
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.034
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
0.689
a.000
0.000
0.000
0.000
0.000
0.00o
0.000
0.000
0.000
0.000
0.000
0.689
Chromium
0.117
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,117
Lead
0.066
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.066
Mercury
0. 001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb"
denu
denum
0.017
o.a00
o.a0o
0.000
0.000
0.a00
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Nickel
0.033
0.000
O.Oa0
O.aaO
0.000
0.000
0.000
0.000
O.OaO
0.000
0.000
0.000
0.033
Selenium
0.034
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.034
/..inc
1.971
0.000
0,000
0.000
0.()00
0.0000.000
0.000
0.000
0.000
0.000
0.000
1.971
Tool
0.000
22.875
- f'hos-
22.875
0.000
0.000
0.0 00
0.000
0.000
0.000
0.000
0.000
0.000
0.000
horns
"I certify.
under
nenalty nr
law
,,..,.�....y U.IUVt1Vll vrsupervision in accoruance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL. METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Spindale Total Dry Tons Applied (Annual):
Permit #: WQ0001953 Cation Exchange Capacity (non 503 only):
Operator: John McFadden Owner: John McFadden Predominant Soil Series:
Acres Used: 15.5 Acres Permitted: 15.5 Site #: M3 Field 4:
18.62
PaC2
M3
Residual Analvsis Data fNeavv Metatc anti Tata) phnwc t,nr..a ..on .,,..1Ir,. oi.
Total
_
3..2.
4 '
�
6_
_�
`
110,
11
12
DT/Ac./
_8
_9
App.
0
a
Event
120
Arsenic
0.060
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.060
Cadmium
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
moo
0.000
0.000
0.000
0.012
Copper
1.201
0.000
0.000
O.000
0.000
0.000
0.000
0-000
0.000
0.000
0.000
0.000
1.201
Chromium
0.204
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.204
Lead
0.116
0.000
0.000
o.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.116
Mercury
0.002
0.000
0.000
0.00o
0.000
0.000
0.00U
0.000
0.000
0.000
0.000
0.000
0.002
Mot};' 1
del
0.030
0.000
0.000
O.000
o.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
o.U3o
Nickel
0.058
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.058
Selenium
0.060
0.000
0.000
0.000
0.00U
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.060
Zinc
3.435
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.435
Total
' F'hos
39.873
0.000
OAOo
0.000
0.000
0-000
0.000
0.000
0.000
0.000
0.000
0.000
39.873
horns
"I Certifv-
undpr
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oh.,..w:
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- - - - ----- --------••-•-•••�••. ••wu �,act,a,cu Y..UC! [fly "'rauuon or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Sigrtbturc of an Applier- - - Date
DENR FORM MFLSF (12/2006)

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ANNUAL, METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Spindale Total Dry Tons Applied (Annual): 50.92
Permit #: WQ0001953 Cation Exchange Capacity (non 503 only):
Operator: John McFadden Owner: John McFadden Predominant Soil Series: PaC2
Acres Used: 17.1 Acres Permitted: 17.1 Site #; M4 Field #: M4
Residual Analvsis Data (1leavv Metals and 'intnl Phncnhnriac step malira 0/ C..1-1r ..ram. D-... 441.
C0111-
posite
Date
Totaj
phorus 1
0
- �� � �.Zl�.f nll•1..f1.J.11w:�.YitY, ..:i\YI11 �.1IYY.lY l�H
Total
1_
__..
4 _
5'
6
7 _
8
9!
12;
DT/Ac.!
_..
A PP•
0
>v
Event
2.98
Arsenic
0.149
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.149
Cadmium
0.030
0.000
0.000
0.000
0.000
0.000
0.o00
0.000
0.000
0.000
0.000
0.000
0.030
Copper
2.978
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.978
Chromium
0.506
0.000
0.000
0,000
0.000
"00
0.000
0.000
0.000
0.000
0.000
0.000
0.506
Lead
0.286
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.286
Mercury
0.004
0.00U
0.000
0.000Molyb
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
denum
denum
0.074
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.074
Nickel
0.145
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.145
Selenium
0.149
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
a.000
0.149
Zinc
8.517
0.000
U00
0.000
0.000
0.000
0.000
0.000
0.000
0 .000
0.000
0.000
$.517
'roial
- Phos-
98.870
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
98.870
horus
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with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
---_ rp�ier
Its-Signature of [.and pate
DENR FORM MF!_SF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field loading Summary Form to be submitted in Annual Report
Facility Name: Town of Spindale Total Dry "Pons Applied (Annual): 22.45
Permit #: WQ0001953 Cation Exchange Capacity (non 503 only):
Operator: John McFadden (honer: John McFadden Predominant Soil Series: CaB2
Acres Used: 10.6 Acres Permitted: 10.6 Site #: M5 Field #: M5
Residual Analysis Data (Heavy Metals and Total Phosphorus use m2/ka. Solids use Raw Percent #):
Com-
posite
Date
Annual Heavv Metal Field Loadines (Calculated in Ibs/acre):
Total
Annual Heavv Metal Field Loadines (Calculated in Ibs/acre):
Total
1
21
3i
4I
5-
6`
7
8i
9"
10
11!
12!
DT/Ac./
o
App.
sti
Event
2.12
Arsenic
0.106
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.106
Cadmium
0.021
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.021
Copper
2.118
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.118
Chromium
0.360
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.360
I..ead
0.204
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.204
Mercury
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Molyb
0.053
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.053
denum
Nickel
0.103
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.103
Selenium
0.106
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.106
Zinc
6.057
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
6.057
Total
Phos-
70.31 g
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
70.318
liorus
t ceraty, unuer penalty of taw, inat ints document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
t am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
1-7
Signature
Signature of hand Applier
[date
DENR FORM MFLSF (12/2006)

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7
n
0
C
N
z
as
A
m
C>
rn
M-
0
m

ANNUAL, PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Spindale
W WTP Name: Town of Spindale W WTP
Monitoring Period: From 1/l/2022
WQ Permit Number: WQ0001953
NPDES Number: NCO020664
To t 2/31 /2022
Patho en Reduction t15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
g
Class A: Alt. A (tiniciteni p)
Alt II (Ark Treatment) ❑
At. C (Prior Testing)❑
AIt.D (No Prior Test) LJ
PI'occs,, to Further Reduce Patho¢engs ❑
If applicable to alternative pciformed (Class A only) indicate "Process to Further Reduce Pathogens".
Compost 01
Heat Drying ❑
Heat Treatment ❑
Thermoplulic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization
Class B: jAlt,
(1) Fecal Density !] I
All. (2) Process to Sittniticantly Reduce Pathogen ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Redu 'rPathogens":
.L1
Lime Stabilization ❑
AIL' Drying
Composting LJ
Aeio' bic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
nt er o
Allowable Level Pathogen Density u
E;xcee
Frequency Sample Analytical
Tech -
Parameter
in Sludge Minimut Geo. Mean Maximum Units
of'Analysis Type
2 x 10 to the
MPN
1010
3090
6468
MPN/g
0
7
grab
sm9221
6th power
per gram of
Fecal Coliform
total solids
C1'tl
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
3 MPN per 4 grams
(in lieu of fecal
total solid (dry
coliform)
Wei ht
Vector Attraction Reduction i15A NCAC 02T .11071 -Please indicate alternative performed:
All.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) 0
Alt. 4 (Spec. O, uptake) Li
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) 0
Alt. 9 (injection) ❑
Alt. 10 (incorporation) Lj
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
21 "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
LJ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector- atlrai•tion reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
G11r f�\C.�nn cT 1,. ,,Tf S,p c;,4 Dennis Key US Biosolids, Inc.
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(typc or print)
Signature of Preparer* Date Sigat re of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26)
DENR FORM PVRF 02T (12/2006)

Waypoint(D
ANALYTICAL
46381
7621 Whitepine Road, Richmond, VA 23237
Main 804-743.9401 0 Fax [phone]
www.waypointanalytical.com
US Biosolids Inc Project Spindale
Dennis Key Report Date : 05/03/2022
958 Hoots Road Information : Received : 04/21/2022
Roaring River , NC 28669
?Aw,:
Report Number; 22-111-0005 REPOR T OF A NA L Y515 Pauric Mc Groary Ph.D., CPA
Agronomist
is
Lab No : 57632 Matrix: Solids
Sample ID: Spindale Sampled: 4/20/2022 0:00
Test Results Units MQL OF Date / Time By Analytical
Analyzed Method
Moisture
98.0
%
0.010
1
04/22/2216:21
FMM
SM-254OG
Sulfur
11400
mg/Kg - dry
500
1
04/27/22 D1:50
JTR
6010D
Calcium
14400
mg/Kg - dry
2500
1
04/27/22 01:50
JTR
601 OD
Aluminum
20000
-mg/Kg - dry
250
1
04/27/22 01:50
JTR
6010D
Manganese
S4S
mg/Kg - dry
25.0
1
04/27/22 01:50
JTR
6010D
Organic N
62900
mg/Kg - dry
12500
1
05/01/22 12:30
CALCULATION
Nickel
24.3
mg/Kg - dry
12.5
1
04/27/22 01:50
JTR
6010D
Lead
48.1
mg/Kg - dry
15.0
1
04/27/22 01:50
JTR
6010D
Arsenic
<25.0
mg/Kg - dry
25.0
1
04/27/22 01:50
JTR
6010D
Selenium
<25.0
mg/Kg - dry
25.0
1
04/27/22 18:09
JTR
6010D
Test
Results
Units
MQL
OF
Date / Time
By
Analytical
Analyzed
Method
Total Solids
2.02
%
0,010
1
04/22/22 16:21
FMM
SM-254OG
Phosphorus
16600
mg/Kg - dry
250
1
04/27/22 01:50
JTR
6010D
Copper
S00
mg/Kg - dry
25.0
1
04/27/22 01:50
JTR
6010D
Total Kjeldahl Nitrogen
74000
mg/Kg - dry
12500
1
05/01/22 12:30
JPJ eM-4500-NH3C-TKP
Qualifiers/ OF
Dilution Factor
MQL Method Quantitation Limit
.
Definitions

(2)
Wa olnt.
YPNALYTICAI
46381
US Biosolids Inc Project. Spindale
Dennis Key
958 Hoots Road Information
Roaring River , NC 28669
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalyticaLcom
Report Date : 05/03/2022
Received : 04/21/2022
T",: rylt Gtva'r
Report Number :22-ill-0005 REPORTOFA/YALYSIS Pauric Mc Groary Ph.D., CPAAgronomist
Lab No ; 57632 Matrix: Solids
Sample ID: Spindale Sampled: 4/20/2022 0:00
Potassium
4650
mg/1(g - dry
500
1
04/27/22 01:50
JTR
6010D
Magnesium
3220
mg/Kg - dry
250
1
04/27/22 01:50
JTR
6010D
Sodium
8950
mg/Kg - dry
1250
1
04/27/22 01:50
JTR
6010D
Iron
19600
mg/Kg - dry
500
1
04/27/22 01:50
JTR
6010D
Zinc
k4l30
mg/Kg - dry
62S
1
04/27/22 01:50
JTR
6010D
Ammonia Nitrogen
11100
-mg/Kg - dry
5000
1
05/03/22. 08:00
)PI
SM-4500-NH3C
Nitrate+Nitrite-N
377
mg/Kg - dry
245
1
04/25/22 14:36
ZBD
4500NO3F-2011
Cadmium
<5.00
mg/Kg - dry
5.00
1
04/27/22 01:50
JTR
6010D
Chromium
85.0
mg/Kg - dry
12.5
1
04/27/22 01:50
JTR
6010D
Mercury
<0350
mg/Kg - dry
0.750
1
04/26/22 13:53
ZMT
SW-7471B
pH
6.3
s.u.
1
04/27/2215:50
DRS
9045D
Molybdenum
<12,5
mg/Kg - dry
12.5
1
04/27/22 01:50
JTR
6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

SAR
Sodium Absorption Ratio
Na Sodium (Mg/L) Equivalent weight: 23
Ca. Calcium (Mg/L) Equivalent weight: 20
Mg : Magnesium (Mg/L) Equivalent weight. 12
Milli Equivalent = MgIL / Equivalent weight
M
[— }
N180, 7 L� Ca {g
180.79 290.$8 r 365,04
Na jME) Ca �ME) M_q..( )
7,860435 14.544 30.42
SAR= Na Milli Equivalent/10.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power
SAR = 1.657788 (From Mg/L entered above)
SAR= 1.65777 (From ME entered below)
Na (ME) C1a (ME) Mg tME)
The amour
amount of i
Permitting

E
p
E
If
It
If
II
N
0
0
z
O
CD
to
0
:3
CAI
z
O
iw
04
z
z
q
< Lp
M
< (i
r
co
q
a.
(L
" -0
0
a
0
Al u
M
F-
a)
>, m
4)
>1 u
th
V-

Analytical Results
U.S. Biosolids Inc
958 Hoots Road
Roaring River, NC 28669
Receive Date: 05/05/2022
Reported: 05/0612022
For: SPINDALE
Comments:
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
220505-22-01
Fecal Coliforms
S1
3922
MPN/g
SkO7210E-2006
051G5/2022
MD
220505-22-01
Percent Solids
S1
2:04
%
W2WB-2011
05/05/2022
MID
220505-22-02
Fecal Coliforms
S2
6468
MPN/g
SM92710E-2006
05/0512022
MD
220505-22-02
Percent Solids
S2
2,01
%
SWW94011
05/0512022
MID
220505-22-03
Fecal Coliforms
S3
<1010
MPN/g
SMMICE-2006
05/0512022
MID
220605-22-03
Percent Solids
S3
1.98
%
SM2MOO.2011
05105/2022
MID
220505-22-04
Fecal Coliforms
S4
3941
MPN/g
W9221cF-2006
05105/2022
MID
220505-22-04
Percent Solids
S4
2.03
%
SM2WS-2011
0510512022
MID
220505-22-05
Fecal Coliforms
S5
3500
MPN/g
SW2210E-2006
0510512022
MID
220505-22-05
Percent Solids
S5
2.0
%
SM25405-2011
05105/2022
MID
220505-22-06
Fecal Coliforms
S6
4000
MPN/g
SM92210E-M6
05/0512022
MID
220505-22-06
Percent Solids
S6
ZO
%
so-wa-2011
05/05/2022
MD
220505-22-07
Fecal Coliforms
S7
2000
MPN/g
SM92210E-2M
05/0512022
MD
220505-22-07
Percent Solids
S7
ZO
%
SM25OB-2011
05105/2022
MD
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 a Statesville, NC 28687 - 704/872/4697
Page 1 of 4

Analytical Results n STATESVILLE
ANALYTICAL
U.S. Biosolids Inc
958 Hoots Road
Roaring River, NC 28669
Receive Date: 05/05/2022
Reported: 06110/2022
For: SPINDALE
Comments:
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
220505-24-01
30 Day Benchscale
SPINDALE
217
%
EPA625-R,92'O
0510512022
MD
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 5

Analytical Results
US Biosolids
958 Hoots Rd
Roaring River, NC 28669
Entered: 5/5/22
Reported: 6/10/22
Sample 10, 220505-24-01
PARAMETER: Vector Attraction Reduction/Aerobically Digested Sludge (30day)
Total Solids Volatile Solids % Volatile Solids
Week 1 1.02 0.71 0.6824
Week 2 0,97 0.67 0,6907
Week 3 1.01 0.68 0.6733
Week 4 0,96 0.64 0,6667
Week 5 0.96 Oks 0.6771
Week 6 033 0.63 0,6224
Volatile Solids Reduction: 0.6824 - 0,6774 X 100 = 2.27 'Yo
0.6824 - (0.6824 X 0,6774)
Respectfully submitted,
Melissa Myers I
Statesville Analytical, Inc.
NC WW Cert.10 440NC
PO Box 228 * Statesville, NC 28687 * 704/872/4697
Page 4 of 5

30 Day Bench Worksheet
Sample ID # 220503-24-01
WEEK 1 Date_ 516/22 10.45
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
1.02
0.71
_
2
1.02
0.71
3
1.01
0.71
Average:
1.02
1 0.71
1 0.68.24
WR IC 2 natem 5/12/22 15:Mi
Samples
Total Solids
Volatile Solids
%Volatile Fraction
1
0.97
0.69
2
0.93
0.62
3
1.00
0.69
Average:
0.97 _ ..._
........._............O.b7......._-._......
0.6907
WEEK 3 Date: 5/1R/22 16!00
Samples
Total Solids
Volatile Solids
% VolatileIraction
1
0.99
0,66
- 2
1.04
0.71
3
1.00
_
0.68
....._..... -._.._.._.....-......
Average:
1.01
0.68
0.6733
WEEK 4 Date: 5/24/22 16:00
Sam lea
Total Solids
Volatile Solids
°!o Volatile Fraction
1
0.98
0.65
2
0.93
0.61
3
Average:
0.98
0.66
0.%
0.64
0.6667
WEEK 5 Date: 5/31/22 16:00
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.97
0.65
2
0.95
0.64
3
0.97
0.65
Average.
0.96
0.65
0.6771
WEEK 6 Date: 6/6/22 15:00
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.93
0.63
2
0,93
0.62
3
0.93
0.63
Average:
0.93
0.63
_
0.6774
Van Met& Reduction: 0.6824 - 0.6774 X 100 = 2.27 %
0.6824 - (0:6$24 X 0,6774)
Final Result: 2.27%
PO Box 228 * Statesville, NC 28687 • 704/872/4697
Page 5 of 5

U
Analytical Results
U.S. Biosolids Inc
958 Hoots Road
Roaring River, NC 28669
Receive Date: 05105/2022
Reported: 06/15/2022
For: SPINDALE
Comments:
Sample Number Parameter Sample 10 Result Unit Method Analyzed Analyst
220505-25-01 TCLP SPINDALE See Attached 05106/2022 PACE
Respectfully submitted,
;1*41:11
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 - 704/872/4697
Page 1 of 36,

/�aceAnaVicaf'
ANALYTICAL RESULTS
Paco Analytical Services, LLC
9W Kincey Ave, Suite 100
Huntorsviiii, NC 28078
(704)87-1W92
Project; 220505-25-01
Pace Project No: 92603539
SampW 220SCS-25-01 SPINDALE Lab& 92603539001 Coltocted: 0510542 1015 Reorved: 05IM2 1313 Matrix. Solid
Results reported on a *dry weight' basis and are adjusted for percent moisture, sample size and any dilution,
Parameters Results Units Report Limit OF prepared Analyzed CAS No Oust
$061 TCLP Pesticides RYE
Analytical Method, EPA W81 8 Preparation Method: EPA 35 10C
Leachate Meltio&Data EPA 1311; 05i1Z(22 15:04
Initial pH; 518; Final pH: 5
Pace Analytical
Services - Charlotte
gamma-SHC (Undane)
NO
ugil.
0,50
1
0V16122 1314 0507122 1416 58-99-9
Chlordams (Technical)
NO
u91L
3.0
1
051161221314 06117/221416 57-74-9
Endrin
No
ug&
0,50
1
05t10f22 1314 05M7122 14AG 72-2"
Reptactitor
NO
UO&
0,50
1
0506122 1314 05117122 14:1e 76-44-6
Heptachlor epoxide
NO
k4t
0,50
1
051161221314 051171221416 1024-57-3
Melkloxychlof
NO
ug/L
low
I
05116122 1314 05il V22 14,16 72-43-5
Toxapherie
NO
uq;L
10
1
061161221314 05f1712214113 $W1-36-2
Surrogates
Deochlomblpheriyl (S)
97
%
10-200
1
051161221314 061171221416 2051-24-3
Telnichloro-m-xyferie (S)
84
%
1%0-182
1
O5fl6/22 1314 05f17122 14:16 877-0"
8082 TCLP PCBs RVE
Ans"calMalhod EPA8082A Preparation Method; EPA 3510C
Leachate MemodMatw EPA 1311, 05/I2i22 15,04 trittial pil, 5,78: Final pHs 5
Pao Anatytical Services - Charlotte
PCB-1016 (AroClor 1016)
No uq1L
1000
1 05116122 13:16 W18122 04:10 12674-11.2
PCB-1221 (Aruclor 1221)
NO ug,L
1000
1 0506122 13; 15 0&l&2204A0 11104-28-2
PCB-1232 (ArocW 1232)
NO ug/L
IDW
I 051I6t= 13:15 05f1&22 04A0 11141.16-5
PCB-1242 (Aroclor 1242)
NO uWL
Iwo
1 051161241315 05AW22 04:10 5"a469.21-9
PCB-1248 (Aroefor 1248)
NO ugil.
1000
1 0&16M 13:15 0511 W22 04:10 12672-2"
PC8-1264. (Aroclor 1254)
NO UA
1000
1 M16/22 13:15 0611&'2204:10 11097-WI
PCB- 1260 (Arocior I 2W)
NO uW`L
1000
I 05116122 1315 DWISM 0410 11096-N2-5
surmg8fais,
Decactilorobipherryl (S)
100
10-181
1 05MW2 1315 W1&122 0410 2061-24-3
6010 MET ICP, TCLP
Analytical Method: EPA 60100 Preparation Me", EPA 301 OA
Leachate Methr Dsle. EPA 1311: 05MV22 15-,04 initial pH: 5,78, Final pH: 2
Pace Anatyk-at Ser-fi.cas - AsheAle
Arsenic
NO mgfL
0.w
I 05114120014 M$122 IT26 7440-W2
Barium
0135 mgifL
025
1 C& I V22 ft 14 05r26122 1716 7"0-39-3
Cadmium
NO mg1l.
O.OV40
I 051141220014 0&26= IT26 7440-434
Chrorrijurn
NO mg1l.
0050
1 05114122 GD14 05126122 1716 7440-47-3
Lead
NO m9VL
0,025
1 MIV220014 05426W 17:26 7439.92-1
Selenium
NO M91L
0.10
1 05t141220014 0512612217:26 7782-49.2
Silver
NO rVL
0,025
1 05AV22 00' 14 08126122 17:26 7440-22-4
7470 Mercury, TCLP
Analytical Method, EPA 7470A Preparation Metho& EPA 7470A
Leachate Method)l)atir EPA 1311, 05112122 15:04
faitialpH: 6,76; Final pK 2
Pace Analytical Services - Asheville
Mercury
NO moil,
O.00020
1 050V22 1712 05117t22 1410 7434-97-6
Date. O&O3i2022 0511 PM
REPORT OF LABORATORY ANALYSIS
This report shah not tee nivfodu�Ad, excalit in full,
voithout the W~ Consent of Pare AnAlAral Sermes, LLC
Page 4 of 33
PC) Box 228 * Statesville, NC 28687 # 704/872/4697
Page 7 of 36

,11�alceAnaVical'
ANALYTICAL RESULTS
Project. 220505.25-01
Pate ProjeCt No, 92603539
Pace Analytical Services, LLC
9600 Kw.*y Ave, Sure 100
HuntemmyAle, NC 28078
(70407&W92
Sample 22005.2541 SPINDALE Lab ID: 92603539001 Collected 05,105122 1015 Received: G5t09122 1123 Matrix: Solid
Reauffs raportedon a *dry weight' basis and are adjusted for pwant moisture, sample size and any dilutions
Parameters Results Units Report Lima DF Prepared Analyzed CAS No, Qual
4270E TCLP RVE
Analytical Method, EPA8270E Preparation Method: EPA 3610C
Leachate Mathod/Oartw EPA 1311; 05/11122
15.04
Initial PH: 5,76; Final pH. 5
Pace Analytical Services - Charlotte
1,4-Otchlorobenzene
NO
u9il.
50,0
1
05116r22 19.10 W712216-,0-1 106464
2A.Dindrotoluene
NO
u9I
60,0
1
05116122 1140 0607122 i6MT 121-14-2
Hexachkyo-1,3-butadiefte
NO
ugll.
5010
1
0511612211:09 OVI 7422 15:07 87-W3
Haxachkyotionzene
NO
ugit,
50,0
1
05/16122 11.09 OSAT122 1547 118-74-1
Hexachloroatharte
NO
UDI
50,0
1
0511&22 11;09 W17122 l&07 67-72-1
2-Methyiphenot(o-Cresol}
NO
ugiL
50,0
1
O5d16C22 11:09 OWi 7t22 15:07 95-48.7
X4-Mvthylpherid(m&p Cresol)
NO
ug(L
SO'D
I
05116= 11i09 WIT= 15;07 15831-10-4
Nitrobenzene
NO
uqrL
50,0
1
Wl&22 11:09 OWITM 15W 9645-3
Pentachloropheriol
NO
uWL
100
1
W16122 W09 05117J22 15,07 $746-5
Pyridine
NO
uW1.
50.0
1
05118122 11;09 WI7P22 1507 11 Q-Wl v I
2,4,5-Trichroroptntriciii
NO
uglL
50,0
1
05116122 ll:09 03iIV22 15:07 95-954
2,4,64neNorophenol
NO
ugVL
50,0
1
051I6P22 WW 05117122 15W 88-06-2
Surrogates
Nitrobenzene-05 (S)
W
10-144
1
06(16(22 11.09 OW172216;07 416"0-0
2-Fluorobtpt,ertyl (S)
67
%
10-130
1
015116M, W09 05t1722 15.07 321.60-8
TarphenyL414 (S)
4I
%
34-163
1
05116W ItOq O51ITt2215W 1718-51-0
Phenol -de (S)
45
% , - ,
10-130
1
05110t22 ILI;09 W17r22 15.07 1312748-3
2-Fluorophenof (S)
61
%
10-130
1
05116122 W09 05117W 1647 367-12-4
2.4.6-TrlbromoDhanol (S)
84
%
10-1"
I
owl W2 11 :C* 06fl7*2 15,07 118-7"
$2600 MSV TCLP AnNytral Method: EPA 8260D EPA 1311: W12rZ2 1310
Pace Ailamical Services - Charlotte
Benzene
NO Uq&
100
20
M1422 OT33 71434
2-Butanone (MEK)
NO U9111-
200
20
05114122 0733 78-93-3
Carboni tetrachloride
NO ugA-
100
20
W14/22 07:33 W23-5
Chlorobenzene
NO UW`L
100
20
051022 0713 108.90-7
chloroform
NO UWL
IW
20
OV1*22 0733 674 3
1.4-01chWobanzene
NO uq;L
100
20
0511V2207:33 10646-7
1,2•Dichkiroelhane
NO ugIL
100
20
05114122 07:33 107406-2
1,1-Dich$oroethene
NO u9fL
100
20
05114122 07:33 75-35-4
Totrachloroathene
NO uglL
100
20
050412207:33 127-18-4
Inchloroethene
NO uq1L
100
Zo
OW14122 0713 7"1.6
Vinyl chloride
NO UgIL
100
20
05t14i22 07:33 75-01-4
surrogates
1,2-Dichloroeithane-d4(S)
97 %
70-130
20
0r.a#14122 0713 1 T060.07-0
Toluene-<18 (S)
105 %
67-135
20
05i14t22 07;33 2031,26-5
4-Bromfluarobanizer* (S)
101 %
70-130
20
05114122 0713 46OW4
Percent Moisture
Analytical Method, SW-846
Pace Analytical Services - Ctarlotle
Percent Moisture
981 %
0.10
1
0"012 16!59 N2
REPORT OF LABORATORY ANALYSIS
This repart shali not be 1hplod.,ed except in fuit,
Date: W0312022 05:51 PM Without the Virriften Conserl of Pare Alla0cal Services i.LC Page 5 of 33
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 8 of 36

Pace Ana"sol Sarvices. LLC
,
98001(inmy Ave, Suite 100
aceAnaliNcalHur'WSAIG, NC 25078
www pacsfabs (104)875-9M
ANALYTICAL RESULTS
Project, 220505-25-01
Pace Project No: 92603539
Sample: 220505-25w01 SPINDALE
dab la:. 92603539001 Collected: 05/05122 1015 Received, 0609M 13,23 Me" Solid
Results reported on a 'dry weight" basis and are adjusted for percent moisture, sample size and any diturtions
Parameters
Results Units Report Limit DF Prepared Analyzed CA$ No Quad
1010 FlashpolnLclosed Cup
Analytical Method EPA 1010E
Pace Analytical Services - Asheville
Flashpamt
),200 deg F 700 1 15s00
9045 ph Soil
Analytical Method: EPA 90450
Pace Analytical Services - Asheville
pH at 25 Degrees C
7.0 Std. Units 0,10 1 05113122 10:29 H3
W95 Paint Filter Liquid Test
Analytical Method, EPA 909W
Pace Analytical Services -Asheville
Free Liquids
FAIL 10 1 05120122 12�1
733C 3 Reactive Cyanide
Analytical Method: SW-846 7,342 Preparation Method: SW-W 7,3,32
Few Anatyt"% Services - New Oiiaans
Cyanide, Reactive
No mgAg 25,0 1 05i23122 08,00 05r"22 1Z,03
731C S Row:tivia Cyanide
Analytical Method EPA 9014 Preparation Method SW-W 7.3,3,2
Pace Analytical Services - Greensburg
Cyanide, Reactive
NO ... rrV*9 83'8 1 0606/22 1150 05116122 14AS
734E Reactive Sulfide
Analytical Mail-& SM 4500-SY-F-2011 Preparation Method SW-W 7,3A 2
Pace Analytical! Services - Greensburg
Sulfide, Reactive
NO mUrkll $38 1 W161221150 0W16r22 1169 HI.H2
Sample: 220505.2"1 SPINDALE
Lab JO,- 92603535002
Collected 05AW2 V, 15
Received. 051OW22 13:23 MaWx Water
Parameters
Results
units
Report Limit
OF
Prepared Analyzed CAS No. Qual
8082 GCS PCB RYE
AnatyDcaf Method: EPA 8082A Preparation Method EPA3510C
Pace Ans"cat Services -
Charlotte
PCB-1016 (Arocior 1016)
NO
uglit.
5,0
1
05M2 18:01 05*W2 14:08 121674-11.2
PC8-1221 (Arockir 1221)
NO
ug(L
6,0
1
0512=2 W01 05tM2 14,06 11104-28-2
PCB-1232 (Aroclor 1232)
NO
t4t
5,0
1
05t=22 W01 0613W 4.08 W41-I6-5
PCB- 1242 (Aroclor 1242)
NO
VGVL
5°0
I
0512=2 W01 05t23122 14,,08 5346941.9
PCS- 1248 (Arockx 1248)
NO
VWL
5,0
1
05f2=2 18;01 05f23122 14;08 12672-29-6
PCB-1254 (Arodor 1254)
NO
4L
5,0
1
0&20,22 1&01 0S(23)22%08 11097-69-1
PC& 1260 (ArWor 1260)
NO
uGVL
5,0
1
0SW/22 18:01 05123122 14c00 1109"2-5
Surrogates
D*CaChI0h)b4p41enyl (S)
27
%
10-181
1
05.20t22 1&01 05t23122 1*06 2051-24-3
REPORT OF LABORATORY ANALYSIS
'T114 reach. shail rat be reproduced, except 0 V,
Dais, 06M=22 05:51 PM mltlovt " wriften wns*mi of Pace Anaytit'Z SeNt", LLC, Page 6 of 33

Analytical Envlrommental Services, Inc
Date: 17-May-22
Client: Pace Analytical Services, Inc. Client Sample ID: 220505-25.01 SPINDALE
Project Name: 92603539 Collection Date: 5/5022 10:15:00 AM
Lab ID: 2205886.001 Matrix: Aqueous
Analym
Result
Reporting
Qoal Units BatchlD Dilution
DateAaafyzed Analyst
HERBICIDF,S, TCLP SW1311/8151A
(SW351.0C)
2,4,5-TP(Silvex)
BRL
0.20
mail 336236 1
05117t202211:37 KH
2,4-D
BRL
0.20
MWL 3362M 1
05117/20221::37 KH
Surn: DCAA
84
50.1-120
"sniic 336236 1
0511712022 11:37 KH
clumtWrc valwex.amM traxinwwn c.....w atinxl
BRL BeJom rsFmtiaf litrit
H Ho" tii— for pretxuadmm M Maly— qc. ycd
N AMyr raa NFLAC ee r d
R Ami}te cheered in dx enocinud mo%W plink
0rena mas R-ok
F Fsti—W(,W..lure quxmimiionnWi
5 SP,kc Ra—Y mmtaidc lima dce to matrix
Harr Sec cwc nurwiv<
F Amy2cd in dte teb whicA is a r4wlot=an from dte mcdwd
� Len than Roeuir xnua
! u ma ed darted W— Rq-fins Lim t Pogo 30 Ot 33
Page 3 of 6
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 33 of 36

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