WQ0034806_2022 Residual Annual Report_20230215 (2)

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * WQ0034806
Applicant/Permittee Coastal Farms and Residuals, LLC
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Wilmington
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Martin Mabe
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
3363121396
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0034806
Has Current Existing permit number
Applicant/Permittee Address*
8155 Malpass Corner Road, Currie, NC 28435
Facility Name*
Coastal Farms and Residuals Class B Residuals
Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Coastal Farms 2022 Annual Report WQ0034806
24.36MB
(NCDEQ).pdf
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/15/2023

2022 ANNUAL REPORT
LAND APPLICATION PROGRAM
COASTAL FARMS AND RESIDUALS, LLC
PERMIT #WQ0034806
Prepared For:
Coastal Farms and Residuals, LLC
8155 Malpass Corner Road
Currie, North Carolina 28435
Compiled By:
Willcox & Mabe Soil Solutions, PLLC
7231B Summerfield Road
Summerfield, North Carolina 27358
February 2023

Willcox&mabe
SOIL SOLUTIONS
February 14, 2023
NCDEQ-DWR Non -Discharge Compliance Unit
512 North Salisbury Street
91h Floor Office# 942X
Raleigh, North Carolina 27604
Attention: Non -Discharge Compliance Unit
Reference: 2022 LAND APPLICATION ANNUAL REPORT
Coastal Fanns and Residuals, LLC
Permit No. WQ0034806
WMSS Project No. 15-19 Ph:01
Non -Discharge Compliance Unit:
Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting
requirements as specified in the above referenced permit on behalf of Coastal Farms and
Residuals, LLC. WMSS compiled this report using data gathered during the compliance year
by Coastal Farms and Residuals, LLC. This data includes: 1) certification form, 2) residuals
analyses and pathogen 1 vector data, 3) application summaries and field loading rate reports, 4)
soil analyses.
If there is any further information required or questions regarding this annual report please do
not hesitate to contact Coastal Farms and Residuals, LLC or WMSS for further assistance.
Sincerely,
Willcox & Mabe Soil Solutions, PLLC
A"�
Martin Mabe
NC Land Application/Residuals Operator
#22753
Enclosures
Shared=MSS PrcjecW2015115-19 Coastal Residuals12022 Annual Report12022 ANNUAL REPORT - COASTAL FARMS.doc
Willcox & Mabe Soil Solutions, PLLC / 7231 B Summerfield Road / Summerfield, NC 273581 Rob 336.339,9128 or
Martin 336.312.1396 / www.willcoxmabesoil.com

TABLE OF CONTENTS
SECTION NO. TITLE
Certification Form
II Residuals Analyses & Pathogen / Vector Attraction Data
III 2022 Application Summary and Field Loading Rate Reports
IV Soil Analysis

CERTIFICATION FORM

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0034806 County:
Facility Name (as shown on permit):
Pender
Year: 2022
Coastal Farms and Residuals, LLC
Land Application Operator: Mr. Wesley Wooten Phone:
910-283-5444
Land application of residuals as allowed by the permit occurred during the past calendar year?
0 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Summary:
Total number of
Total number of fields utilized for land
Total amount of dry tons applied durin¢ the
Total number of acres utilized for land
Part B.- Annual Comniance Statement:
;ion fields in the permit:
12
lication during the year:
2
for all application sites:
584.26
lication durinh the year:
_
175.3
Facility was compliant during calendar year 2022 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. 0 Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and Iimc was applied (if needed) to achieve a soil pH of at least
6.0 or the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3)
copies of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are
5) All other monitoring was performed in accordance with the permit and reported during the year as required and
three (3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40
CFR Part 503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .111 I were complied with (applicable to 40 CFR
Part 503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation,
prior authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations
are attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Mr. Wesley W000ten, President 2/14/2023
Permittee Name and Title (type or print) Signature f Pennittee Date
Signature of Preparer* Date Signature of Land Applier Date
(if different from Pennittee) (if different from Perm ittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

RESIDUAL ANALYSES
TCLP ANALYSES IF REQUIRED
AND PATHOGEN AND VECTOR ATTRACTION REDUCTION

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding laboratory analysis.
Please note (hat your permit may contain addilional parameters to be analyzed than those required to be summarized on this form.
Permit Number WQ0034806
Facility Name Coastal Residuals
NPDES # See Below
WWTP Name See Below 2022 DATA
RESIDUAL ANALYSIS DATA
Laboratory 1) Environmental Chemist, Inc.
2
3
NPDES #
W00030775
NCO023256
NCO026611
WQ0034367
WQ0005790
I W00037287
WQ0013200
WQ0029955
I W00000795
I W00023261
WWCP Name
Avendale
Carolina Beach
Morehead City
NW Regional WRF
Oak Island WWTP
Pluris Hampstead
SE Brunswick
Summerhouse
Surf Cily WWTP
Swansboro
CompositedlGrab
02/03/22
06/07/22
03/29/22
11/15/22
01/12/22
1 04/06/22
04/27/22
11/02/22
11/07/22
09/07/22
Percent Solids
1.44
3.82
24.3
1.36
2.33
1 1.38
2.21
0.72
1.74
1.94
PARAMETERS (molt dry weicht)
Arsenic
44.30
33.80
7.08
35.60
27.50
33.00
21.60
26.80
19.80
16.50
Cadmium
44.30
25.00
3.88
35.60
20.40
33.00
21.60
26.80
19.60
16.50
Copper
133.00
654.00
638.00
342.00
200.00
126.00
176.00
143.00
420.00
281.00
Lead
44.30
25.00
12.60
35.60
20.40
33.00
21.60
26.80
19.60
16.50
Mercury
1.17
0.49
0.94
8.680
0.72
1.26
0.81
2.51
1.100
0.99
Molybdenum
44.30
25.00
5.18
35.60
20,40 1
33.00
21.60
26.80
19.60
16.50
Nickel
44.30
25.00
10.60
35.60
20.40
33.00
21.60
26,80
19.60
16,50
Selenium
44.30
25,00
3.88
35.60
20.40
33,00
21.60
26.80
19.60
16,50
Zinc
764.00
1,180.00
938.00
1,370.00
1,020.00
449,00
643.00
2,940.00
4,200.00
3,670.00
TKN
78,300.00
69,700.00
66,200.00
36,800.00
46.000.00
64,900.00
59,500.00
67,100A0
67,400.00
36,200.00
Ammonia -Nitrogen
6,130.00
2.62
25,300.000
1,690.00
4,260.00
1,420.00
1,250,00
3,310.00
1,250.00
792.00
Nitrate -Nitrogen
15.80
16.25
10.50 1
3,460.00
2.48
1.45
10.60
1,980.00
194.00
9,050.00
Total Phosphorus
14,300.00
1 12,500.00
60100 1
38,100.00
12,400,00 1
241,700.01)
1 33,500.00 1
39,300.00 1
22,600.00
15,900.00
RESIDUAL ANALYSIS DATA
I
Total Phosiific�
X NIA due to number of sources
(SIGNATURE OF PREPARER) DATE
I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.

COASTAL RESIDUALS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 3, 2022
Avendale WWTP
1.44 % Solids
7.31 PH
Permit No. WQ0030775
Parameter
%
Mg/Kg Dry Weight
x 10,000)
Pounds/Dry Ton
(Mg/Kg (Mg/Kgx 0.002
Nitrogen (TKN)
7.830
78,300.000
156.600
Phosphorus
1.430
14,300.000
28.600
Potassium
0.488
4„880.000
9.760
PAN injected)*
2.780
27,796.800
55.594
PAN surface)*
2.473
24,731.800
49.464
Ammonia Nitrogen
0.613
6,130.000
12.260
Calcium
1.170
11,700.000
23.400
Calcium Carbonate E .
---
---
Magnesium
---
3,730.000
7.460
Sodium
---
6,260.000
12.520
Sulfur
---
---
---
Nitrate N / Nitrite N
---
15.800
0.032
Barium
Chloride
---
---
---
---
---
---
SAR
1.54
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
2,280.00
4.560
Arsenic
---
44.30
0.089
75
Cadmium
---
44.30
0.089
85
Chromium
---
44.300
0.089
---
Copper
---
I33.00
0.266
4,300
Lead
---
44.30
0.089
840
Mercury
---
L 170
0.002
57
Molybdenum
---
44.30
0.089
75
Nickel
---
44.30
0.089
420
Selenium
---
44.30
0.089
100
Zinc
---
764.00
1.528
7,500
Environmental Chemists 9 2022-02087
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

COASTAL FARMS AND RESIDUALS, LLC
WQ0034806
Avendale WWTP
02/03/22
61,745
4.7906
02/03/22
80,000
4.9031
02/03/22
48,422
4.6850
02/03/22
55,422
4.7437
02/03/22
38,572
4.5863
02/03/22
114,286
5.0580
02/03/22
33,541
4.5256
Total 1 33,2923
Average 1 4.7560
Geometric Mean I�Qa;'jjij Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction
requirement.

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 + 910.347.5843 Lab/Fax
[e-mail]
Lewis Farms & Liquid Waste, INC.
Date of Report: Feb 17, 2022
8155 Malpass Corner Road
Customer PO #:
Currie NC 28435
Customer ID: 14020008
Attention: Martin Mabe
Report #: 2022-02087
Project ID: Aqua - Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-04938 Site: Avendale Sludge
2/3/2022
10:20 AM Solid/Sludge Kirkland Fields
Test
Method
Results
Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4, 1994
2280 mg/kg
02/09/2022
Arsenic
EPA 200.7, Rev. 4.4, 1994
<44,3 mg/kg
02/0912022
Cadmium
EPA 200.7, Rev. 4.4, 1994
<44.3mglkg
02/09/2022
Calcium
EPA 200.7, Rev. 4.4. 1994
11700 mg/kg
02/0912022
Chromium
EPA 200.7, Rev. 4.4, 1994
<44.3 mg/kg
02/09/2022
Copper
EPA 200.7. Rev, 4.4, 1994
133 mg/kg
02/09/2022
Lead
EPA 200.7, Rev. 4.4, 1994
<44.3 mglkg
02/09/2022
Magnesium
EPA 200.7, Rev. 4.4, 1924
3730 mg/kg
02/09/2022
Molybdenum
EPA 200.7, Rev, 4.4, 1994
<44.3 mglkg
02/09/2022
Nickel
EPA 200.7, Rev. 4.4, 1994
<44.3 mg/kg
02/09/2022
Potassium
EPA 200.7. Rev. 4.4, 1994
4880 mg/kg
02/09/2022
Selenium
EPA 200.7, Rev. 4.4, 1994
<44.3 mg/kg
02/09/2022
Sodium
EPA 200.7. Rev. 4,4, 1994
6260 mg/kg
02/11/2022
Zinc
EPA 200.7, Rev, 4A, 1994
764 mg/kg
02/09/2022
Nitrate+Nitrite-Nitrogen
EPA353.2
15.8mglkg
02/07/2022
Total Solids (%)
SM 2540 B
1 A4 %
02/03/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
6130 mg/kg
02/08/2022
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
78300 mg/kg
02/04/2022
Total Phosphorous
SM 4500 P (F-H)-2011
14300 mg/kg
02/16/2022
pH
Result estimated. Analyzed out of 15 minutes
SW 846 Method 90451]
hold time.
7.31 units
0211612022
Mercury
SW-846 7471 B
<1.17 mg/kg
02/07/2022
Report #:: 2022-02087 Page 1 of 3

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
71013owsertown Road, Manteo, NC 27954 o 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 a 910,347.5843 Lab/Fax
[e-mail]
Lewis Farms & Liquid Waste, INC. Date of Report: Feb 17, 2022
8155 Malpass Corner Road Customer PO #:
Currie NC 28435 Customer ID: 14020008
Attention: Martin Mabe Report #: 2022-02087
Project ID: Aqua - Sludge
Lab 1D Sample ID: Collect DatelTime Matrix Sampled by
22-04939 Site: Avendale Sludge 1 2/3/2022 10:20 AM Solid/Sludge Kirkland Fields
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
Lab ID Sample ID:
22-04940 Site: Avendale Sludge 2
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
22-04941 Site: Avendale Sludge 3
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
22-04942 Site: Avendale Sludge 4
SM 2540 B
SM 9221 C E-2o14
1.49 % 02/03/2022
61745 MPNIg 02/03/2022
Collect DatelTime Matrix Sampled by
2/3/2022 10:20 AM Solid/Sludge Kirkland Fields
Method Results Date Analyzed
SM 2540 B 1.15 % 02/03/2022
SM 9221C E-2014 80000 MPN/g 02/03/2022
Collect Date/Time Matrix Sampled by
2/3/2022 10:20 AM Solid/Sludge Kirkfand Fields
Method Results Date Analyzed
SM 254o a 1.90 % 02/03/2022
SM 9221C E-2014 48422 MPN/g 02/03/2022
Collect Date/Time Matrix Sampled by
2/3/2022 10:20 AM Solid/Sludge Kirkland Fields
Test Method Results Date Analyzed
Total Solids (°/a) SM 2540 B 1.$6% 02/03/2022
Fecal Density SM 9221C E-2014 55422 MPN/g 02/03/2022
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
22-04943 Site: Avendale Sludge 5 2/3/2022 10:20 AM Solid/Sludge Kirkland Fields
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 1.40 % 02/03/2022
Fecal Density SM 9221C E-2014 38572 MPNIg 02/03/2022
Report #:: 2022.02087 Page 2 of 3

r
eri�.r`a►chem
fir •I 3 ' at,= =zr�
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
[e-mail]
Lewis Farms & Liquid Waste, INC. Date of Report: Feb 17, 2022
8155 Malpass Corner Road Customer PO #:
Currie NC 28435 Customer ID: 14020008
Attention: Martin Mabe Report #: 2022-02087
Project ID: Aqua - Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-04944 Site: Avendale Sludge B 2/3/2022 10:20 AM Solid/Sludge Kirkland Fields
Test Method Results Date Analyzed
Total Solids SM 2544 B 1.40 % 02/03/2022
Fecal Density SM 9221 C E-2014 114286 MPN/g 02/03/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-04945 Site: Avendale Sludge 7 2/3/2022 10:20 AM Solid/Sludge Kirkland Fields
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 1.61 % 02/03/2022
Fecal Density SM 9221 C E-2014 33541 MPNIg 02/03/2022
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
Report #. 2022.02087 Page 3 of 3

Environmental Chemist, Inc,, Wilmington, NC Lab 994
6502 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client:
IS ��Date:�Report
Number: 2022- �Q$
Receipt of sample:
ECHEM Pickup ❑ Client Delivery
11P5 ❑ Fed Ex ❑ Other ❑
❑
YES
❑ NO
❑ N/A 1. Were custody seals present on the cooler?
❑ YES
❑ NO
❑ N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt cc
Original Corrected temperature upon receipt C
°
How temperature taken:
❑ Temperature Blank Against Bottles
IR Gun ID: Thomas Traceable S/N: 210835468 IR Gun Correction Factor °C: 0.0
❑ YES
❑ NO
3. If temperature of cooler exceeded 6'C, was Project Mgr./QA notified?
YES
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
YES
❑ NO
5. Were sample ID's listed on the COC?
YES
❑ NO
6. Were samples ID's listed on sample containers?
YES
❑ NO
7. Were collection date and time listed on the COC?
YES
❑ NO
8. Were tests to be performed listed on the COC?
YES
❑ NO
9. Did samples arrive in proper containers for each test?
YES
❑ NO
10. Did samples arrive in good condition for each test?
YES
YES
❑ NO
❑
11. Was adequate sample volume availableT
NO
12. Were samples received within proper holding time for requested tests?
❑ YES
❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES
11 NO
16. Were NH3/T'KN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
0 YES
10 NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* 70C/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
sample Preservation: (Must be completed for any sampie(sJ incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Vote: Notify customer service Immediately for Incorrectly preserved samples. Obtain anew sample or
ratify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Jolatiles Sample(s) were received with headspace
COMMENTS:
DOC, QA.002 Rev 1

ENVIRONMENTAL CHEMISTS, INC odml WayFFI E'n910I392-223fImingtonFAX 910-392-44245
Analytical & Consulting Chemists NCDENR: DWR CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalc hem ists.com
COLLECTION AND CHAIN C]F rI1STnnv
Client: Lewis Farms & Liquid Waste
PROJECT NAME: Aqua-Avendale
REPORT NO: zl -Q 2S.8
ADDRESS: ?/53- rl s5 Pld
CONTACT NAME: Wesley Wooten
PO NO:
.-P
REPORT TO: Martin Mabe/Mahe-Wilcox
PHONE/FAX:
COPY TO: ILLk A
email:
Sampled By:
ly SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection Y PRESERVATION
am a a cC7 =� n w
e a a; : L m e
R E ca o _o m g z ., o o zo a w ANALYSIS REQUESTED
N O IL U E G Y n Z Q =
Date Time Temp z z = z x ~ o
Sludge
a- 3- P.t Q Zp L` G Y �g X Nutrients/Metals
C
P
�`3
X
Fecal Density/%TS
G
G
2
C
P
%��
X
Fecal Density/%TS
-H
G
G
3
C
P
�f
f q `7 1
X
8
Fecal Density/ /oTS
G
G
C
P
ILO
G
G
4
z z
X
Fecal Densi /%TS
5
C
P
�
49 `{I3
X I
Fecal Density/%TS
G
G
C
P
G
G
6
X
Fecal Density/%TS
7
5L
C
P
(�
7
X
Fecal Densi /%TS
9 - 3- ,)
!Q c7 �,
G
G
Transfer Relinquished By: Date/Time Received By: I Date/Time
1.
2. I 1
~
Temperature when Received: • Accepted:
Delivered By: 9 Received By:
Comments:
Time:
TUR AROUND:

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Coastal Fanns and Residuals, LLC
WWTPName: AvendaleWWTP
Monitoring Period:
From
1/l/2022
To
WQ Permit Number: WQ0034806
NPDES Number: WQ0030775
12/31/2022
Alt.1 (VS reduction)
❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) UT
AIL 4 (Spec. O, uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization ❑
it 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable)
[IAlt.
9 (Injection)
ElAlt.
10 (Incorporation) ElNo
vector attraction reduction alternatives were performed
❑
k r,K.tiriuA i iun STATEMENT ATt;•tVE.t!rNT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance With the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonmerit."
Kirklyn Fields, ORC Wesley Wooten, President
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
z 2/23122
2/18122
Signature of reparer* Date Signature of Land pplier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (1212006)

COASTAL RESIDUALS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: June 7, 2022
Carolina Beach WWTP Permit No. NC0023256
3.82 % Solids
7.53 p H
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
Mg/KgMg/Kg x 0.002)
Nitrogen (TKN)
6.970
69,700.000
I39.400
Phosphorus
1.250
12,500.000
25.000
Potassium
0.250
2,500.000
5.000
PAN (injected)*
2.092
20,918.084
41.836
PAN (surface)*
2.092
20,916.774
41.834
Ammonia Nitrogen
0.000
2.620
0.005
Calcium
4.050
40,500.000
81.000
Calcium Carbonate E .
---
---
---
Magnesium
---
5,420.000
10.840
Sodium
---
7,700.000
15.400
Sulfur
---
---
---
Nitrate N / Nitrite N
---
6.250
0.013
Barium
---
---
---
SAR
1.86
Chloride
---
---
---
Iron
---
---
---
Ce�(Mg/Kg)
Aluminum
---
3,850.00
7.700
Arsenic
---
33.80
0.068
75
Cadmium
---
25.00
0.050
85
Chromium
---
25.000
0.050
---
Copper
---
654.00
1.308
4,300
Lead
---
25,00
0.050
840
Mercury
---
0,492
0.001
57
Molybdenum
---
25.00
0.050
75
Nickel
---
25,00
0.050
420
Selenium
---
25.00
0.050
100
Zinc
---
1,180.00
2.360
7,500
Environmental Chemists 4 2022-10463
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

COASTAL FARMS AND RESIDUALS, LLC
WQ0034806
Carolina Beach WWTP
06/07/22
4,734
3.6752
06/07/22
17,767
4.2496
06/07/22
3,413
3.5331
06/07/22
12,267
4.0887
06/07/22
4,896
3.6898
06/07/22
13,102
4.1173
06/07/22
5,914
3.7719
Total 1 27.1258
Average 3.8751
Geometric Mean
Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen Reduction
requirement.

rlT e-
"r i�'Vs':y'.•:.�1{t�::,�� .y,.:�,. GSM
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 26405 Q 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 e 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Town of Carolina Beach
Date of Report: Jul 15, 2022
1121 North Lake Park Blvd
Customer PO ##:
Carolina Beach NC 28428
Customer ID: 08100295
Attention:
Report #: 2022-10463
Project ID: Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-25297 Site: Sludge
6/7/2022
10:00 AM Solid/Sludge Bill Raymond
Test
Method
Results Date Analyzed
Total Organic Carbon (TOC)
9060
32300Dmg/kg
06/21/2022
Chlordane (TCLP)
SW-846 8001 B
<0.02 mg/L
06/23/2022
Endrin (TCLP)
SW-846 B081 B
<0.0005 mg/L
06/23/2022
Heptachlor (TCLP)
SW-846 8081 B
<0.0005 mg1L
06/23/2022
Heptachlor epoxide (TCLP)
SW-8468081 B
<0,D005mg1L
06/23/2022
Lindane (TCLP)
SW-846 8081 B
<0.0005 mg/L
06/23/2022
Methoxychlor (TCLP)
SW-846 B081 B
<0.0005 mg/L
06/23/2022
Toxaphene (TCLP)
SW-846 8081 B
<0.05 mg/L
06/23/2022
2,4,5-TP (TCLP)
SW-846 8151 A
<0.003 mg1L
06/29/2022
2,4-D (TCLP)
SW-846 8151 A
<0.003 mg/L
06/29/2022
1,4-Dichlorobenzene (TCLP)
SW-846 B270 E
<0.050 mg/L
06/21/2022
2,4,5-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
06/21/2022
2,4,6-Trichlorophenol (TCLP)
SW-845 8270 E
<0.050 mg/L
06/21/2022
2,4-Dinitrotoluene(TCLP)
SW-846 8270E
<0.050mg/L
06/21/2022
Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
06/21/2022
Hexachloro-1,3-butadiene(TCLP)
SW-8468270E
<0.050mg/L
06/21/2022
Hexachlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg1L
06/21/2022
Hexachloroethane (TCLP)
SW-846 8270 E
<0.050 mg1L
06/21/2022
m + p-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
06/21/2022
Nitrobenzene (TCLP)
SW-B46 8270 c
<0.050 mg/L
06/21/2022
o-Cresol (TCLP)
SW-846 8270 E
<0.050 mg1L
06/21/2022
Pentachlorophenol (TCLP)
SW-8458270E
<0.250mg/L
06/21/2022
Pyridine (TCLP)
SW-846 0270 E
<0.050 mg/L
06/21/2022
1,1-Dichloroethylene (TCLP)
SW-B46 Method B260D
<0,01 mg/L
06/22/2022
1,2-Dichloroethane (TCLP)
SW-846 Method 8260D
<0.01 mg1L
06/22/2022
Benzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
06/22/2022
Report #,- 2022.10463
Pagel of4

.+��y�ff';, w--,' ;�'��'. ��'•- t'�L' USIA,
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info(gcnvironmcritalcilemists cone
Town of Carolina Beach
1121 North Lake Park Blvd
Carolina Beach NC
Attention:
28428
Date of Report: Jul 15, 2022
Customer PO #:
Customer ID: 08100295
Report #: 2022-10463
Project ID: Sludge
Carbon Tetrachloride (TCLP)
SW-846 Method8260D
<0.01 mg/L
06/22/2022
Chlorobenzene (TCLP)
SW-646 Method 62600
<0.01 mg1L
06/22/2022
Chloroform (TCLP)
9W-546 Method 0260D
<0.01 mg/L
06/22/2022
Methyl ethyl ketone (TCLP)
SW-646 Method 0260D
<0,05 mg/L
06/22/2022
Tetrachloroethylene (TCLP)
SW-846 Method 82600
<0.01 mg/L
06/22/2022
Trichloroethylene (TCLP)
SW-846 Method 0260D
<0.01 mg/L
06/22/2022
Vinyl Chloride (TCLP)
SW-846 Method 82600
<0.01 mg/L
06/22/2022
RCI
Cyanide
SM 4500 CN D-2016
1,75 mg/kg
06/15/2022
Sulfide
SM 4500 S D
5.38 mglkg
0612412022
Ignitability
SW 846 method 1010
>157 °F
06/16/2022
Sludge Residuals
Aluminum
EPA 2007, Rev 44. 1994
3850 mg/kg
06/20/2022
Arsenic
EPA 200.7, Rev 4 4.1994
33,8 mglkg
06/20/2022
Cadmium
EPA 200.7. Rev, 4 4, 1994
<25.0 mglkg
06/20/2022
Calcium
EPA 200.7. Rev 4 4, 1994
40500 mg/kg
06/20/2022
Chromium
EPA 200.7, Rev 4 4, 1994
<25.0 mglkg
06/20/2022
Copper
EPA 200.7. Rev. 4 4, 1994
654 mglkg
06/20/2022
Lead
EPA 200.7, Rev, 4.4, 1994
<25,0 mg/kg
06120/2022
Magnesium
EPA 2a0.7, Rev 4A. 1994
5420 mglkg
06/20/2022
Molybdenum
EPA 200.7, Rev 4 4.1994
<25.0 mglkg
06/20/2022
Nickel
EPA 200.7, Rev. 4,4, 1994
<25.0 mglkg
06/20/2022
Potassium
EPA 200 7, Rev- 4 4, 1994
2500 mglkg
06/28/2022
Selenium
EPA 200 7, Rev. 4 4, 1994
<25.0 mglkg
06/20/2022
Sodium
EPA 200.7. Rev 4 4, 1994
7700 mg/kg
06/20/2022
Zinc
EPA 200 7, Rev 4 4, 1994
1180 mg/kg
06/20/2022
Nitrate+Nitrite-Nitrogen
EPA 3532
6,25mg/kg
06/09/2022
Total Solids (%)
SM 254D B
3,82 %
06/08/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
<2.62 mg/kg
06/08/2022
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
69700 mg/kg
06/08/2022
Report 9- 2022.10463
Page 2 of 4

Environmental Chemists Inc.
s 6 B 6602 Windmill Way, Wilmington, NC 28405 910.392.0223 Lab 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473,5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info@environ men talchemists.com
Town of Carolina Beach Date of Report: Jul 15, 2022
1121 North Lake Park Blvd Customer PO #:
Carolina Beach NC 28428 Customer ID: 08100295
Attention: Report #: 2022-10463
Project ID: Sludge
Total Phosphorus SM 4500 P (F-H)-2011 125DO mg/kg 06/11/2022
pH SW 846 Method 9045D 7.53 units 06/2812022
Result estimated. Analyzed out of 15 minutes hold time.
Mercury SW-0467471 B <0.492 mg/kg 06/09/2022
TCLP Metals
Arsenic
EPA 200.7. Rev, 4.4. 1994
<1.0 mg/L
06/28/2022
Barium
EPA 200.7, Rev. 4.4. 1994
<1.0 mg/L
06/28/2022
Cadmium
EPA 200.7, Rev. 4.4, 1994
<1.Omg1L
06/28/2022
Chromium
EPA 2003, Rev. 4.4. 1994
<1.0 mg/L
06/28/2022
Lead
EPA 200.7, Rev, 4.4, 1994
<1.0 mg/L
06/28/2022
Selenium
EPA 200.7, Rev. 4A. 1994
<1 ,0 mg/L
06/28/2022
Silver
EPA 200.7, Rev. 4.4. 1994
<1.0 mg1L
06128/2022
Mercury
EPA245.1
<0.0002 mg/L
06/28/2022
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
22-25298 Site: 1
6/7/2022 10:00 AM
Solid/Sludge Bill Raymond
Test
Method
Results Date
Analyzed
Total Solids (%)
SM 2540 B
4.12 % 06/08/2022
Fecal Density
SM 9221C E-2014
4734 MPN/g 06/07/2022
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
22-25301 Site: 2
6/7/2022 10:00 AM
Solid/Sludge Bill Raymond
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
3.94 % 06/08/2022
Fecal Density
SM 9221C E-2014
17767 MPN/g 06/07/2022
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
22-25302 Site: 3
6/7/2022 10:00 AM
Solid/Sludge Bill Raymond
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
3.81 % 06/08/2022
Fecal Density
SM 9221C E-2014
3413 MPNIg 06/07/2022
Report #_- 2022-10463 Page 3 of 4

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910-392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington 1-lighway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info(a-,envi ronmen talchemists.com
Town of Carolina Beach
Date of Report: Jul 15, 2022
1121 !North Lake Park Blvd
Customer PO #:
Carolina Beach NC
28426 Customer ID: OB100295
Attention:
Report #: 2022-10463
Project ID: Sludge
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
22-25303 Site: 4
6/7/2022 10:00 AM Solid/Sludge Bill Raymond
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 3,75 % 06/08/2022
Fecal Density
SM 9221C E-2014 12267 MPN/g 06/07/2022
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
22-25304 Site: 5
6/7/2022 10:00 AM Solid/Sludge Bill Raymond
Test
Method Results Date Analyzed
Total Solids (%)
s SM 2540 s 4.29 % 06/08/2022
Fecal Density
SM 9221C E-2014 4896 MPN/g 06/07/2022
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
22-25305 Site: 6
6/7/2022 10:00 AM Solid/Sludge Bill Raymond
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 3.74 % 06/08/2022
Fecal Density
SM 9221C E-2014 13102 MPN/g 06/07/2022
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
22-25306 Site: 7
6/7/2022 10:00 AM Solid/Sludge Bill Raymond
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 3,72 % 06108/2022
Fecal Density
SM 9221C E-2014 5914 MPN/g 06/07/2022
Comment: Results, except
pH, reported on a dry weight basis, pH reported on an as received basis.
Reviewed by: k
alilaOi
Report #.: 2022-10463
Page 4 of 4

Analytical Environmental Services, Inc Date: 22-Jun-22
Client: Environmental Chemists, Inc. Client Sample 1D: 22.25297
Project Name: 2077-10463 Collection Date: 6/7/2022 10:00:00AM
Lab ID: 2206C50-001 Matrix: Sludge
__
Analyses Reporting Dilution
} Result QuaE Units 13atcIilD Date Analyxrd Analyst Limit
Factor
Total Organic Carbon in Soil SW9060 (SW9060 Modified)
Total Organic Carbon (TOC) 323000 998 rnglKg-dry 338356 1 06/21/2022 16 32 GK
Quelifien: ' Value exceeds maximum cantammanr level E Estimated (value ahove guantitation range)
RRL Bclow reporting limit S SpI4 Rccoveryy outside hm its due to mmnxi
H Holding limes far prepamlion or mmlysts exceeded Narr See case nvnl,vc
N Anaiyle nor NELAC eernrscd F Analyzed in the lab Much is a dmabon from the method
B Analyle detected in the associated mcEhod blank K Less than Result value
Greater than Result value J Estimated value directed below Reporting Limit
Page 3 of 6

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
Sample Receipt Checklist 910.392.0223
Client: Vol i r1Ci �eC�cl )Date: `I ZZ
P,eport Number: _ 2022-
Receipt of sample: ECHEM Pickup Client Delivery, ❑ UP5 ❑ FedEx ❑ Other ❑
❑ YES ❑ NO ❑ N/A I
❑ YES ❑ NO
. Were custody seals present on the cooler?
N/A
Original temperature
2. If custody seals were present, were they intact/unbroken?
upon receipt °C
Corrected temperature upon receipt How temperature taken: ❑ Temperature Blankottles QC
IR Gun ID: Thomas Traceable S/N 192511657 gf-actoB
YES ❑ NO
IR Gun Correction C: 0.0
3. If temperature of cooler exceeded 6°C,
YES ❑ NO
was Project Mgr./Qq notified?
4. Were proper custody procedures (relinquished/received)
YES ❑ NO
followed?
5. Were sample 1D's listed on the COC?
YES ❑ NO
6. Were samples ID's listed on sample containers?
YES ❑ NO
7. Were collection date and time listed on the COC?
YES ❑ NO
8. Were tests to be performed listed on the COC?
�" YES I❑ NQ
r -. D!� 5?^',r!=a"?','_.� '_w_"'-_`�-..,'��.i `J� co4�i icSC' _-- -- ---- k
_ - --
20. Did samples arrive in good condition for each test?
YES ❑ NO
11. W35 adep!lata s=mniQ , nl�+ o �, , o�
, - m- a /affabfe '
YES ❑ NO
12, Were samples received within proper holding time for requested tests?
❑ YES ❑ NO
❑ YES I❑ NO
13. Were acid preserved samples received at a pH of <2?
❑
14. Were cyanide samples received at a pH >12?
YES ❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES ❑ NO
❑ YES ❑
16. Were NH3/TKN/Phenol received at a chlorine residual of <0,5 m/L?
NO
❑
17. Were Sulfide/Cyanide received at a chlorine residual of<0.5 m/L?
YES ❑ NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatile; are pH checked
at time of analysis and recorded on the bench5heet.
** Bacteria samples are checked
for Chlorine at time of analysis and recorded on the benchsheat.
Sample Preservation:
(Must be completed For any sample(s) incorrectly preserved or headspace)
Sample(s)
with
by adding (circle one):
were received incorrectly preserved and were adjusted accordingly
H2SO4 HNO3 HCl NaOH
Time of preservation:
If more than one preservative is needed,
notate in comments below
Nota: NotiFy custorn_r 5ePJice imm-ad;aiely For in correctiy Pre;e;Ned sampi=_s obtain a new
sam. P;e o.
10tiN the state lab if directed re analyzed by tl : cL'stom'_r. V,ho was notified, date and time:
Vola tiles Sample(s)
were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
Client: Carolina Beach 11UVVTP
PROJECT NAME: Sludge analysis
REPORT NO: C3� D�- I C -
ADDRESS: D .5. DO � j�cQ -
&6LC QC 2-q Z
CONTACT NAME: Bill Raymond, ORC
REPORT TO:
PO NO.
PHONEIFAX,
COPY TO: Lewis Farms/Martin Mabe
email: �; I I.0^a nond lFCaro I',I
Sampled By: 1 a ,,o., SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil SL = Sludge Other:
Sample Identification
Collection
qu
E�
N~
a o°
di
E Q
°a
o m
t�i 1=
m M
g�
z
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp"
i
°
z
.,
Y
o
N
o
Z
a
o
=
W
iz
o
Sludge 3)
CB SLUDGE
1 } F67CA t-
-� zz
DvD
a
2`f c
Z� .60C.
S L
5 L
C
_
��.�j
_
� �
X
X
Nut/Metals/Full TCLP/RCIffee�-6 ,Zz
fecal density/ %TS
(0-7—ZZ
1000
C
G
G
G
Cl S Lv]7GC
2 FCCAL
6-7-ZZ
1000
o
Zq.�
L
C
_
J
x
fecal density/ %TS
G
CA SL'mc E
3) FEG.4L
6 -'-ZZ
)00 0
��.o� L
C
J 1,G
C
_
x
fecal density/ %TS
Cif SLcI'D(; 95
`1') ECAL
Doa
Z� � (—
S L-
C
P
� �y
x
Ifecal
density/ %T$
G
C 8 S i.1 p G E
b) c A L
_"T-y2
1 Dt7 0
Z4,G cC
L
C
P
x
fecal density/ %TS
G
C8 SLo-pGE
6) CAL
- —ZZ
1000
2y
5�
C
P
5
x
fecal density/ %TS
G
Cg 'SLJOG it
7) FEcA+�
-7'ZZ
1000
Z4. 6
S L
C
P
o�
x
a
fecal density) %TS
G
��t�r
-7�22
1Daa
C
P
_.
Transfer
Relinquished By:
Date/Time
Recei y:
Datei'rime
1.
n.,.
_ 8 5
t
CA1 -1 2n
2.
r
2Z
Temperature when Received: Accepted:
Delivered By: Received By:
Comments:

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Coastal Farms and Residuals, LLC
WWTP Name. Carolina Beach WWTP
Monitoring Period: From 1/112022
WQ Permit Number: WQ0034806
NPDES Number: NCO023256
TO 12/31/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed•
Class A:
Alt. A (time/temp) ❑ Alt B (Alk Treatment) [l Alt. C (Prior Testing)❑
Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogeti�s Ld
if applicable to altertative
performed (Class A oitl') Indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑ Heat Treatment Ll Themio liilic ❑
Beta Ray El
Gamma Ray ❑ Pasteurization ❑
Class 8: Alt. (1) Fecal Density p Alt. (2} Process to Si iificaiitly Reduce Pathogens ❑
If applicable to alternative performer) (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Plying ❑ I Coni ostinE ❑ Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Allowable Level Pathogen Density
Pararrteter
urn er ot Frequency Sample Analytical
in Sludge Minimu Geo. Mean Maximo Units
Exeee a
s of Analysis Type To 1t
z x 10 to
Gil powerMPN 3,413 7,501
17,767
MPN/g
0
Annual
Grab
SM9221C:E
per gram of
l
Fecal Colifoun total solids CF,
1000 mpn per gram
oftotalsolid (diy
Wei fit)
Salmonella bacteria 3 MPN per 4 grains
(in lieu of fecal rota) solid (dry
coliforni) Weight)
1'ector Attraction Reduction (15A NCAC 62T .1107) -
Please indicate alternative performed:
Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑ JAII. 4 (Spec. 01 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) p Alt. 10 (Incorporation) El
!'VT3TTVF1-A Tl rl\T Clm A ^V`T+,. ., ,-.ir.., ,_
No vector attraction reduction alternatives were performed ❑
.. c.ial a -- K� r'% A A'JLI J 1 AL 1 2' 1Y1,C.1\ i klAease C11CCU the appropriate statement)
❑ "I certify, Lander penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T.1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T _1107 have not been met," (Please note if
You check this statement attach an explanation why you have not niet one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. 1 am aware that there are
significant penalties for false certification including tine and imprisonment."
William Raymond, ORC Wesley Wooten, President
Prepaarreer Name and Title (type or print) Land Applier Naine and
%Title (if applicable)(type or print)
1 1/2122
SiCrtawre rep r* Date Signature of Lan Applier (if applicable) Data
"Preparer is defined in 40 UK Part 503.9(r) and I iA NCAC 2T _ 1102 (26)
DENR FORM Pi1RF 02T (1212006)

COASTAL FARMS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: March 29, 2022
Morehead City
24.30 % Solids
8.52 pH
Permit No. NC002661 I
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
M/Kg x 0.002)
Nitrogen (TKN)
6.620
66,200.000
132.400
Phosphorus
0.060
603.000
1.206
Potassium
0.364
3,640.000
7.280
PAN (injected)*
3.758
3,869.500
7.739
PAN (surface)*
2.493
3,77T000
7.554
Ammonia Nitrogen
2.530
25,300.000
50.600
Calcium
3.310
33,100.000
66.200
Calcium Carbonate E .
---
.._
Magnesium
0,004
35.400
0.071
Sodium
0.415
4,150,000
8.300
Sulfur
-_-
---
Nitrate N / Nitrite N
---
10.500
0.021
Barium
Chloride
---
---
_--
---
---
---
SAR
3.09
Iron
---
__
---
Ceiling Concen.
(Mg/Kg)
Aluminum
--
13,600.00
27.200
Arsenic
---
7.08
0.014
75
Cadmium
---
3.88
0.008
85
Chromium
---
13.700
- -
-
Copper
---
638.00
1.276
4,300
Lead
---
12.60
0.025
840
Mercury
---
0.941
0.002
57
Molybdenum
---
5.18
0.010
75
Nickel
---
10.60
0.021
420
Selenium
---
3.88
0.008
100
Zinc
---
938.00
1.876
7,500
Environmental Chemists, Inc. 2022-05661
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 920.392.0223 Lab o 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info(4 environmentalchemists.cam
Town Of Morehead City
Date of Report: Apr 27, 2022
1100 Bridges Street
Customer PO #•
Morehead City NC 28557
Customer ID: 09020011
Attention: Nate Johnson
Report #: 2022-05661
Project ID: Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-13693 Site: Sludge
3/29/2022
10:30 AM Solid/Sludge Nate Johnson
Test
Method
Results
Date Analyzed
CCE
AOAC 1.005
1.9 %
04/21 /2022
Paint Filter Test
SW 846 Method 9095 A
pass
04/21/2022
Chlordane (TCLP)
SW-8468081 B
<0.02mg/L
04/05/2022
Endrin (TCLP)
SW-1346 8081 B
<0.0005 mglL
04/05/2022
Heptachlor (TCLP)
SW-846 8081 B
<0.0005 mg/L
04/05/2022
Heptachlor epoxide (TCLP)
sW-8468081 B
<0.0005mg/L
04/05/2022
Lindane (TCLP)
SW-846 B081 8
<0.0005 mg/L
04/05/2022
Methoxychlor (TCLP)
SW-846 8081 B
<0.0005 mg/L
04/05/2022
Toxaphene (TCLP)
sW-8468081 a
<0.05mg/L
04/05/2022
2,4,5-TP (TCLP)
SWa46 8151 A
<0.003 mg/L
04/04/2022
2,4-D (TCLP)
SW-846 8151 A
<0.003 mg/L
04/04/2022
1,4-Dichlorobenzene(TCLP)
SW-8468270E
<0.050mg/L
04/01/2022
2,4,5-Trichlorophenof (TCLP)
SW-8468270E
<0.050 mg/L
04/01/2022
2,4,6-Trichlorophenol (TCLP)
SW-846 827o E
<0.050 mg/L
04/01/2022
2,4-Dinitrotofuene (TCLP)
SW-8468270E
<0.050mg/L
04/01/2022
Cresol (TCLP)
SW-846 8270 E
3.47 mg/L
04/0112022
Hexachloro-1,3-butadiene (TCLP)
SW-846 B270 E
<A,050 mg/L
04/01/2022
Hexachlorobenzene(TCLP)
SW-8468270E
<0.050 mg/L
04/01/2022
Hexachloroethane (TCLP)
SW-5468270E
<0.050 mg/L
04/01/2022
m + p-Cresol (TCLP)
SW-846 8270 E
3.47 mg/L
04/01/2022
Nitrobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
04/01/2022
o-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
04/01/2022
Pentachlorophenol (TCLP)
SW-846 8270 E
<0.250 mg/L
04/0112022
Pyridine (TCLP)
SW-846 8270 E
<0.050 mg/L
04/01/2022
1. 1 -Dichloroethylene (TCLP)
SW-846 Method 0260D
<0.01 mg/L
04/07/2022
1,2-Dichloroethane (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04107/2022
Report #:: 2022-05661
Page 1 of 5

Environmental Chemists, Inca
i 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 8owsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
s� 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL. & CONSULTING CHEMISTS infoCa,environmentalcliemists.com
Town Of Morehead City
Date of Report: Apr 27, 2022
1100 Bridges Street
Customer PO #:
Morehead City NC
28557
Customer ID: 09020011
Attention; Nate Johnson
Report #: 2022-05661
Project ID: Sludge
Benzene (TCLP)
5W-646 Method 82601)
<0.01 mg/L
04/07/2022
Carbon Tetrachloride (TCLP)
SW846 Method 8260D
<0.01 mg/L
04/07/2022
Chlorobenzene (TCLP)
SW-646 Method 8260D
<0.01 mg/L
04/07/2022
Chloroform (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/07/2022
Methyi ethyl ketone (TCLP)
SW 646 Method 626oD
0.06 mg1L
04/07/2022
Tetrachloroethylene (TCLP)
SW-646 Method B2600
<0.01 mg/L
04/07/2022
Trichloroethylene (TCLP)
SW-846Method 8260D
<0.01 mg/L
04/07/2022
Vinyl Chloride (TCLP)
SW-846 Method 0260D
<0.01 mg/L
04/07/2022
RCi
Ignitability
EPA 103o
<0.8 mm/sec
04/01/2022
Cyanide
SM 4500 CN D-2016
1.18 mg/kg
04/05/2022
Sulfide
SM 4500 s D
<0.39 mg/kg
04/11 /2022
Sludge Residuals
Aluminum
EPA 200.7, Rev, 4A. 1994
13600 mg/kg
04/14/2022
Arsenic
EPA 200.7, Rev, 4A, 1994
7.08 mg/kg
04/14/2022
Cadmium
EPA 2o0.7, Rev. 4.4. 1994
<3.88 mg/kg
04/14/2022
Calcium
EPA 200.7, Rev. 4.4. 1994
33100 mg/kg
04/14/2022
Chromium
EPA 200.7, Rev. 4.4. 1994
13.7mg/kg
04/14/2022
Copper
EPA 200.7, Rev. 4.4. 1994
638 mg/kg
04/14/2022
Lead
EPA20o.7, Rev. 4.4. 1994
12.6 mg/kg
04/14/2022
Magnesium
EPA 200.7. Rev. 4.4, 1994
35.4 mg/kg
04/14/2022
Molybdenum
EPA 200.7, Rev, 4.4. 1994
5.18 mg/kg
04/14/2022
Nickel
EPA 200,7, Rev. 4.4, 1994
10.6mg/kg
04/14/2022
Potassium
EPA 200.7, Rev. 4.4, 1994
3640 mg/kg
04/14/2022
Selenium
EPA 200.7, Rev. 4,4, 1994
<3.88 mg/kg
04/14/2022
Sodium
EPA 200.7, Rev. 4A, 1994
4150 mg/kg
04/14/2022
Zinc
EPA 200.7, Rev. 4.4,1994
938 mg/kg
04/14/2022
Nitrate+Nitrite-Nitrogen
EPA363.2
10.5mglkg
03/30/2022
Total Solids (%)
SM 2540 8
24.3 %
03/30/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
25300 mg/kg
03/30/2022
Report #:: 2022.05681
Page 2 of 5

40 Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 9I0.392.0223 Lab • 910.392.4424 Fax
fs. t 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infoi2 jenvironmentaichemists.com
Town Of Morehead City
Date of Report: Apr 27, 2022
1100 Bridges Street
Customer PO #:
Morehead City NC
28557
Customer ID: 09020011
Attention: Nate Johnson
Report #: 2022-05661
Project ID: Sludge
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg a-2011
66200 mg/kg
03/30/2022
Total Phosphorus
SM 4500 P (F-H)-2011
603 mg/kg
04/04/2022
pH SW 846 Method 9045D
Result estimated. Analyzed out of 15 minutes hold time.
8.52 units
04/12/2022
Mercury
SW-846 7471 8
0.941 mglkg
04/04/2022
TCLP Metals
Arsenic
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
04/05/2022
Barium
EPA 200,7, Rev. 4.4,1994
<1.0 mg/L
04/05/2022
Cadmium
EPA 200.7. Rev. 4.4, 1994
<1.0 mg/L
04105/2022
Chromium
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
04/05/2022
Lead
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
04/05/2022
Selenium
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
04/05/2022
Silver
EPA200-7. Rev, 4A4 1994
<1.0 mg/L
04/05/2022
Mercury
EPA 245.1
<0.0002 mg1L
04/07/2022
Lab ID Sample ID:
Collect DatelTime
Matrix Sampled by
22-13695 Site: #1
3/29/2022 2:39 PM
Solid/Sludge Nate Johnson
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 8
24.8 %
03/30/2022
Fecal Density
SM 9221C E-2014
622 MPN/g
03/29/2022
Lab ID Sample ID:
Collect DatelTime
Matrix Sampled by
22-13697 Site: #2
3/29/2022
Solid/Sludge Nate Johnson
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 E
21.7 %
03/30/2022
Fecal Density
SM 9221C E-2014
2908 MPN/g
03/29/2022
Reporl #:: 2022-050,61
Page 3 of 5

Environmental Chemists, Inc.
1 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL_ & CONSULTING CHEMISTS into(a)cnvironmenialcliemists.com
Town Of Morehead City Date of Report: Apr 27, 2022
1100 Bridges Street Customer PO #:
Morehead City NC 28557 Customer ID: 09020011
Attention: Nate Johnson Report #: 2022-05661
Project ID: Sludge
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
22-13698 Site: #3 3/29/2022 Solid/Sludge Nate Johnson
Test
Total Solids (%)
Fecal Density
Lab 1D Sample ID:
22-13699 Site: #4
Test
Method
SM 2540 9
SM 9221C E-2014
Method
Collect DatefTime
3/29/2022
Results Date Analyzed
23.2 % 03/30/2022
<8 MPNIg 03/29/2022
Matrix Sampled by
Solid/Sludge Nate Johnson
Results Date Analyzed
Total Solids (%) SM 2540 B 22.5 % 03/30/2022
Fecal Density SM 9221C E-2014 9 MPNIg 03/29/2022
Lab ID Sample ID: Collect DatefTime Matrix Sampled by
22-13700 Site: #5 3/29/2022 Solid/Sludge Nate Johnson
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
Lab ID Sample ID:
22-13701 Site: #6
Test
SM 2540 B
SM 9221 C E-2014
Method
Collect Date/Time
3/29/2022
28.5 % 03/30/2022
386 MPNIg 03/29/2022
Matrix Sampled by
Solid/Sludge Nate Johnson
Results Date Analyzed
Total Solids (%) SM 2540 B 24.6 % 03/30/2022
Fecal Density SM 9221C E-2014 >64909 MPNIg 03/29/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-13702 Site: #7 3/29/2022 Solid/Sludge Nate Johnson
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 23.0 % 03/30/2022
Fecal Density SM 9221C E-2014 <8 MPN/g 03/29/2022
Report #:: 2022-05661 Page 4 of 5

��enviroch.em
ANALYTICAL & CONSULTING CHEMISTS
Town Of Morehead City
1100 Bridges Street
Morehead City NC 28557
Attention: Nate Johnson
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab + 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info (dienviro amen to tcli e[n is is. com
Date of Report: Apr 27, 2022
Customer PO #:
Customer ID: 09020011
Report #: 2022-05661
Project ID: Sludge
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
Report 2027.05681
Page 5 of 5

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
Sample Receipt Checklist 910.392.0223
Client: r
� Date: Zq
Report Number: _ 2022- ()J.,o
Receipt of sample:
❑ YES [EllNO
ECHEM Pickup Client Delive ❑ UPS ❑
rY FedEx ❑ Other ❑
N/A
❑ YES ❑ NO
1. Were custody seals present on the cooler?
N/A
Original temperature upon
2. If custody seals were present, were they intact/unbroken?
receipt °C
Corrected temperature upon receipt C
How temperature taken: ❑ Temperature Blank
Against ottles
Ili Gun ID: Thomas Traceable SIN 192511657 IR Gun Correction I ctoB C: 050
YES ❑ NO
YES ❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES ❑ NO
4. Were proper custody procedures (relinquished/received) followed?
5. Were sample ID's listed on the COC?
YES ❑ NO
6. Were samples ID's listed on sample containers?
YES ❑ NO
YES ❑
7. Were collection date and time listed on the COC?
NO
YES ❑
8. Were tests to be performed listed on the COC?
NO
YES ❑
9. Did samples arrive in proper containers for each test?
NO
YES ❑
10. Did samples arrive in good condition for each test?
Pi0
YES ❑ NO
11. IAI—adequate sample volume available?'
❑ YES ❑ NO
12. Were samples received within proper holding time for requested tests?
© YES ❑
13. Were acid preserved samples received at a pH of <2?
NO
❑ YES ❑
14. Were cyanide samples received at a pH >12?
NO
❑ YES ❑
15. Were sulfide samples received at a pH >9?
No
❑ YES ❑ NO
16. Were Nun /TKN/Phenol received at a chlorine residual of <0.5 m/L? *�
❑ YES ❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
18. Were orthophosphate samples filtered in the field within 15 minutes?
TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet
ample Preservation: (Must be completed for any sample(s) Incorrectly preserved or with headspace)
3mple(s) were received incorrectly preserved and were adjusted accordingly
r adding (circle one): H2504 HNO3 HCl NaOH
me of preservation; If more than one preservative is needed, notate in comments below
)te: Notify customer service immediately for incorrectly preserved samples. Obtain a new sampie or
tify the state lab if directed to analyzed by the customer. Who was notified, date and time:
)latiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

OF.,%) VVII idplif ftmj VI/11,11 �g
otf
ap, I F1 till m a
"19
keo. . ......
C. i, lit
..... ............
... .......
TO"
-.vy, w. Zo 5�
-IV . ..........
I t
1.1 1. I,f
I'M
......... .
. .......... ........ . ..•......
R C,
All
.. ......... ... . ...
... ........ 031'
. . ......... ................... . . . ...
. . . ....... ... . ...
.... ... . ... .... . ..... ............
......... . .
10 . ...........
"I . ....... .......
if �1�.. "r; .- �,t„ r,�l ..}�•

COASTAL FARMS AND RESIDUALS, LLC
WQ0034806
Morehead City WWTP
05/24/22
59
1.7709
05/24/22
3
0.4771
05/24/22
35
1.5441
05/24/22
39
1.5911
05/24/22
41
1.6128
05/24/22
183
2.2625
05/24/22—F
16
1.2041
Total 1 10.4625
Average 1 1.4946
Geometric Mean Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction
requirement.

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 e 910.392.0223 Lab . 910.392.4424 Fax
710 BOWSertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
in roCci;environmentalchemists.com
Town Of Morehead City
Date of Report: May 27, 2022
1100 Bridges Street
Customer PO #:
Morehead City NC
28557
Customer ID: 09020011
Attention: Nate Johnson
Report #: 2022-09519
Project ID: Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-22864 Site: Sludge 1
5/24/2022 11:00 AM Solid/Sludge Nate Johnson
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 6
56.4 % 05/2512022
Fecal Density
SM 9221C E-2014 59 MPN/g 05/24/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-22865 Site: Sludge 2
5/24/2022 11:01 AM Solid/Sludge Nate Johnson
Test
Method
Results Date Analyzed
Total Solids
SM 254o B
70.8 % 05/25/2022
Fecal Density
SM 9221C E-2014 <3 MPNIg 05/24/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-22866 Site: Sludge 3
5/24/2022 11:02 AM Solid/Sludge Nate Johnson
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
66.9 % 05/25/2022
Fecal Density
SM 9221C E-2014
35 MPN/g 05/24/2022
Lab lD Sample ID:
Collect Date/Time Matrix Sampled by
22-22867 Site: Sludge 4
5/24/2022 11:03 AM Solid/Sludge Nate Johnson
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
59.3 % 05/25/2022
Fecal Density
5M 9221C E-2014 39 MPNIg 05/24/2022
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
22-22868 Site: Sludge 5
5/24/2022 11:04 AM Solid/Sludge Nate Johnson
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
64,8 % 05/2512022
Fecal Density
SM 9221C E-2014 41 MPNIg 05/24/2022
Report #.: 2022.09519 Page 1 of 2

F
Environmental Chemists, Inc.
6 1 ` 1
6602 Windmill Way, Mming ton NC 28405 • 910.392.0223 Lab 9I0.392.4424 Fax
isFe
710 Sowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
^
255-A Wilmington Highway, Jacksonville, NC 28540 • 910,347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
[e-mail]
Town Of Morehead City
Date of Report: May 27, 2022
1100 Bridges Street
Customer PO M
Morehead City NC 28557
Customer ID: 09020011
Attention: Nate Johnson
Report M 2022-09519
Project ID: Sludge
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
22-22869 Site: Sludge 6
5/24/2022 11:05 AM Solid/Sludge Nate Johnson
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 6 60.3 % 05/25/2022
Fecal Density
SM 9221C E-2014 183 MPNIg 05/24/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-22870 Site: Sludge 7
5/24/2022 11:06 AM Solid/Sludge Nate Johnson
Test
Method Results Date Analyzed
Total Solids (%) SM 2540 s 69.5 % 05/25/2022
Fecal Density SM 9221C E-2014 16 MPNIg 05/24/2022
Comment: Results reported on a dry weight basis.
Reviewed by -
Report # : 2022-09519 Page 2 of 2

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
`` .. !-r t) - Sample Receipt Checklist
Client:M.DLE(l�) Date: Y as Report Number: 690
0 r u —
Receipt of sample:
ECHEM Pickup Af Ciient Delivery ❑
1 UPS ❑ FedEx ❑ Other ❑
❑
YES
10
NO
' N/A
1. Were custody seals present on the cooler?
❑
YES
10
NO
N/A
2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt
How temperature taken:
❑ Temperature Blank K Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
❑
YES
❑
NO
3. If temperature of cooler exceeded 6'C, was Project Mgr./QA notified?
ID
YES
❑
NO
4. Were proper custody procedures (relinquished/received) followed?
f�l
YES
❑
NO
5. Were sample ID's listed on the COC?
YES
❑
NO
6. Were samples ID's listed on sample containers?
YES
❑
NO
7. Were collection date and time fisted on the COC?
YES
❑
NO
8. Were tests to be performed listed on the COC?
YES
❑
NO
9. Did samples arrive in proper containers for each test?
YES
❑
NOE13.were
Didamples arrive in good condition for each test)
YES
Cl
NOadequate
sample volume available?'
YES
❑
NO
samples received within proper holding time for requested tests?
❑
YES
❑
NO
acid preserved samples received at a pH of <2?
❑
YES
❑
NO
cyanide samples received at a pH >12?
❑
YE5
❑
NO
sulfide samples received at a pH >9?
❑
YES
❑
NO
NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑
YES
IT
NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑
YES
❑
NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Voiatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H250q HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state tab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

II# dial`
Mlimf�fuaqr lit ail 11\4
N Kjrl, ' !,)"
C,l.b
........ . .........
............ ..........
..........
... .......
4001
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.... .. .......
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Ell
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Cyr 4 af r4� 4

ANNUAL PATEIOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Coastal Fanns and Residuals, LLC WQ Permit Number: WQ0034806
WWTP Name: Town of Morehead City NPDES Number: NCO026611
Monitoring Period: From I/l/2022 To 12/31/2022
Pathogen Reduction (40 CFR 503.321 - Please indicate level achieved and adfPr-nafivP norinrm.ri-
Class A: Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
Alternative 4 ❑
Alternative 5 ❑
Alternative 6 ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thennophilic ❑
Leta Ray 01
Gantma Ray ❑
Pasteurizatmn ❑
Class B: Alternative I El Altemative 2 ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Cl Air Drying❑ Compostin ❑ Aerobic Digestion ❑
Anaerobic Di estion ❑
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Allowable Level Pathogen Density
Parameter g y
Number o na ytica
Frequency Sample
in Slud0e Minimu Geo. Mean Maximu Units
Fscee- Tech -
� af1lnalysis Type
2 x 10 to the
6th power
WN
3
31
183
MPN/g
0
Annual
Grab
SM9221CL
Fecal Coliform
per gram of
total solids
CFU
1000 mpn per gram
oftotalsolid (dry
weight)
Salmonella bacteria
3 MPN per 4 grams
(in lieu of fecal
total solid (dry
colifomi)
Wei fit)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option nerformed_
Alt.l (VS reduction)
❑
Alt. 2 (40-day bench)
❑
Alt. 3 (30-day bench) ❑ JAIt. 4 (Spec. Q, uptake)
❑
Alt. 5 (14-Day Aerobic)
Alt. 9 (Injection)
❑
❑
Alt, 6 (AIk. Stabilization
Alt. 10 (Incorporation)
❑
a
Alt 7 (Drying - Stable) ❑ lAh. 8 (Drying - Unstable)
No vector attraction reduction alternatives were performed
❑
❑
C.ER I it iC:A t JON STATEMENT (please check the appropriate statement)
El `°I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "1 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in Oil CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties far false certification including fine and imprisonment."
Chad Sutton, WWTP Superintendent Wesley Wooten, President
Preparer Na e and T Ie ype or print) Land Applier Name and Title (if applicable)(type or print)
Vv
7' . 11 /2/22
Signature of Preparer* Date Signature of4Lan�Applier (if applicable) Date
"Preparer is defined in 40 CFR Part 503.9(r) and I SA NCAC 2T .l 102 (26)
of=Kiprr)PRA Pi/mr gnzmotonnn%

COASTAL RESIDUALS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: November 15, 2022
Northwest ReZional WRF Permit No. WQ0034367
1.36 % Solids
7.3 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
3.680
36,800.000
73.600
Phosphorus
3.810
38,100.000
76.200
Potassium
0.539
5,390.000
10.780
PAN (injected)*
1.568
15,683.000
31.366
PAN (surface)*
1.484
14,838.000
29.676
Ammonia N itrogen
0.169
1,690.000
3,380
Calcium
2.460
24,600.000
49.200
Calcium Carbonate E .
---
---
....
Magnesium
---
3,040.000
6.080
Sodium
---
11,300.000
22.600
Sulfur
---
---
---
Nitrate N I Nitrite N
---
3,460.000
6.920
Barium
Chloride
---
---
---
---
---
---
SAR
2.10
Iron
---
-._
---
Ceiling Concen.
(M /K )
Aluminum
---
36,500.00
73.000
Arsenic
---
35.60
0.071
75
Cadmium
---
35.60
0.071
85
Chromium
---
35.600
---
--
Copper
---
342.00
0,684
4,300
Lead
---
35.60
0.071
840
Mercury
---
8.680
0,017
57
Molybdenum
---
35.60
0.071
75
Nickel
---
35.60
0.071
420
Selenium
---
35.60
0.071
100
Zinc
---
1,370.00
2,740
7,500
Environmental Chemists # 2022-22759
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

Environmental Chemists, Inc.
nto,
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Faxo 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347,5843 Lab/Fax
ANALYTICAL $ CONSULTING CHEMISTS info @environmentalchemists.com
Onslow Water & Sewer Authority
Date of Report: Dec 16, 2022
228 Georgetown Road
Customer PO #:
Jacksonville NC 28540
Customer ID: 08100092
Attention: Todd Roberts
Report #: 2022-22759
Project ID: Northwest Reg. WRF
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-55920 Site: Digester
11/15/2022
7:30 AM Solid/Sludge Randal Riggs
Test
Method
Results Date Analyzed
Chlordane (TCLP)
SW-846 8081 B
<0.02 mg/L
11/22/2022
Endrin (TCLP)
SW-8468081 a
<0,0005 mg/L
11/22/2022
Heptachlor (TCLP)
SW-846 80818
<0.0005 mg1L
11/22/2022
Heptachlor epoxide (TCLP)
SW-846 8081 B
<0.0005 mg/L
11/22/2022
Lindane (TCLP)
SW-84680B1 B
<0.0005mg/L
11/22/2022
Methoxychlor (TCLP)
$W-846 80818
<0.0005 mg/L
11/22/2022
Toxaphene (TCLP)
SW-546 8081 B
<0.05 mg1L
11 /2212022
2,4,5-TP(TCLP)
SW-8468151A
<0.003mg/L
11/25/2022
2,4-D (TCLP)
SW-8468151 A
<0.003 mg/L
11/25/2022
1,4-Dichlorobenzene (TCLP)
SW846 8270 E
<0.050 mg/L
11/22/2022
2,4,5-Trichlorophenol (TCLP)
SW-B46 8270 E
<0.050 mg/L
11/22/2022
2,4,6-Trichlorophenol (TCLP)
SW-8468270E
<0.050mg/L
11/22/2022
2,4-Dinitrotoluene (TCLP)
SW-846 8270 E
<0.050 mg/L
11/22/2022
Cresol (TCLP)
SW-646 8270 E
<0.050 mg/L
11/22/2022
Hexachloro-1,3-butadiene (TCLP)
SW-846 B270 E
<0.050 mg/L
1112212022
Hexach loro benzene (TCLP)
SW-646 02711 E
<0.050 mg/L
11/22/2022
Hexachloroethane (TCLP)
SW.846 827o E
<0.050 mg/L
11/22/2022
m t p-Cresol (TCLP)
SW-845 B270 E
<0-050 mg/L
11/22/2022
Nitrobenzene (TCLP)
SW-646 8270 E
<0.050 mg/L
11/22/2022
o-Cresol (TCLP)
SW-8468270 E
<0.050 mg/L
11/22/2022
Pentachlorophenol (TCLP)
SW-846 8270 E
<0.250 mg/L
11122/2022
Pyridine (TCLP)
SW-546 B270 E
<0.050 mg/L
1112212022
1, 1 -Dichforoethylene (TCLP)
SW-846 Method826oD
<0,01 mg/L
11129/2022
1,2-Dichloroethane (TCLP)
SW-846 Melhod 826aD
<0.01 mg/L
11/29/2022
Benzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
11/29/2022
Carbon Tetrachloride (TCLP)
SW-846 Method 8260D
<0.01 mg/L
11/29/2022
Reporl #:; 2022-22759
Page 1 of 3

Environmental. Chemists, Inc,
!! 9 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392,4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Onslow Water & Sewer Authority
Date of Report: Dec 16, 2022
228 Georgetown Road
Customer PO #:
Jacksonville NC 28540
Customer ID: 08100092
Attention, Todd Roberts
Report #: 2022-22759
Project ID: Northwest Reg, WRF
Chlorobenzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
11/29/2022
Chloroform (TCLP)
SW-846 Method 8260D
<0.01 mg/L
11/29/2022
Methyl ethyl ketone (TCLP)
SW-846 Method 0260D
<0.05 mg/L
11/29/2022
Tetrachloroethylene (TCLP)
SW-846 Method 8250D
<0.01 mg/L
11/29/2022
Trichloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
11/29/2022
Vinyl Chloride (TCLP)
SW-846 Method B260D
<0.01 mg/L
11/29/2022
RCI
Cyanide
SM 4500 CN 0-2016
<1 mg/kg
11/21/2022
Sulfide
SM 4500 S D
0.11 mg/kg
11/28/2022
Ignitabllity
SW 846 method 1010
> 158 °F
12/12/2022
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4. 1994
36500 mglkg
12/07/2022
Arsenic
EPA 200.7. Rev. 4.4,1994
<35.6 mg/kg
12/07/2022
Cadmium
EPA 200.7. Rev. 4.4, 1994
<35.6 mglkg
12/07/2022
Calcium
EPA 200.7, Rev. 4.4, 1994
24600 mg/kg
12/07/2022
Chromium
EPA 200.7, Rev, 4.4, 1994
<35.6 mg/kg
12/07/2022
Copper
EPA 200,7, Rev, 4.4, 1994
342 mg/kg
12/07/2022
Lead
EPA 200.7, Rev. 4A, 1994
<35.6 mglkg
12107/2022
Magnesium
EPA 200.7, Rev. 4.4, 1994
3040 mg/kg
12/07/2022
Molybdenum
EPA 200.7. Rev. 4.4. 1994
<35.6 mg/kg
12/07/2022
Nickel
EPA 200.7, Rev. 4.4, 1994
<35.6 mg/kg
12/07/2022
Potassium
EPA 200.7. Rev. 4A. 1994
5390 mg/kg
12107/2022
Selenium
EPA 200,7, Rev. 4.4, 1994
<35.6 mg/kg
12/07/2022
Sodium
EPA 200.7. Rev. 4.4, 1994
11300 mg/kg
12/07/2022
Zinc
EPA 200.7, Rev. 4.4, 1994
1370 mg/kg
12/07/2022
Nitrate+Nitrite-Nitrogen
EPA353.2
3460mg/kg
11/16/2022
Total Solids N
SM2540s
1,36%
11/16/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
1690 mg/kg
11/16/2022
Total K)eldahl Nitrogen (TKN)
SM 4500 Norg 8-2011
36800 mg/kg
11/16/2022
Total Phosphorus
SM4500 P iF-rq-2011
38100 mg/kg
11/29/2022
Report C 2022-22759
Page 2 0f 3

Environmental. Chemists, Inc.
4
r+ f 6 6602 Windmill Way, Wilmington, NC 28405 ■ 910,392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 e 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Onslow Water & Sewer Authority
228 Georgetown Road
Jacksonville NC 28540
Attention: Todd Roberts
Date of Report: Dec 16, 2022
Customer PO #:
Customer ID: 08100092
Report #: 2022-22759
Project ID: Northwest Reg. WRF
pH
SW 646 Method 9045D
7.30 units
11/30/2022
Result estimated. Analyzed out of 15 minutes
hold time.
Mercury
sW-0467471 s
8.68mg/kg
12/09/2022
TCLP Metals
Arsenic (TCLP)
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
11/29/2022
Barium
EPA 200.7, Rev, 4.4. 1994
<1.0
11/29/2022
Cadmium
EPA 200.7, Rev, 4A. 1994
<1,0
11/29/2022
Chromium
EPA 200.7, Rev. 4.4, 1994
<1.0
11/29/2022
Lead (TCLP)
EPA 200.7. Rev. 4.4, 1994
<1.0 mg/L
11/29/2022
Selenium
EPA 200.7, Rev, 4.4, 1994
<1,0
11 /29/2022
Silver
EPA 200.7. Rev.4A, 1994
<1,0
12/07/2022
Mercury
EPA 245.1
<0.0002
11/30/2022
Comment: Sludge residuals, except pH, reported on a dry weight basis, pH reported on an as received basis
Reviewed by: A Q>-JA
Report #:: 2022-22759 Page 3 or 3

Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Client: vl�Date: �Report Number: _ 2022-��, �- p
Receipt of sample:
❑ YES ❑
E HEM Pickup Client Delivery ❑ UPS ❑ FedEx ❑ Other ❑
NO
N/A 1. Were custody seals present on the cooler?
❑ YES
I0
NO
N/A 2. if custody seals were present, were they intact/unbroken?
Original temperature upon receipt_ °C Corrected temperature upon receipt
How temperature taken:
❑ Temperature Blank Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor T. 0.0
YES
❑
NO
3. If temperature of cooler exceeded 6'C, was Project Mgr./QA notified?
YES
❑
NO
4. Were proper custody procedures (relinquished/received) followed?
YES
❑
NO
S. Were sample ID's listed on the COC?
YES
❑
NO
6. Were samples ID's listed on sample containers?
YES
❑
NO
7. Were collection date and time listed on the COC?
YES
❑
NO
8. Were tests to be performed listed on the COC?
YES
❑
NO
9. Did samples arrive in proper containers for each test?
YES
❑
NO
10. Did samples arrive in good condition for each test?
YES
❑
NO
11. Was adequate sample volume available?'
YES
❑
NO
12. Were samples received within proper holding time for requested tests?
❑ YES
❑
NO
13, Were acid preserved samples received at a pH of <2?
❑ YES
❑
NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑
NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑
NO
16, Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? *'
❑ YE5
❑
NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YE 5
❑
NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SOI HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1
°C

o e
6602
ENVIRONMENTAL CHEMISTS, INC OFF! EWindmll Way:9 0I392-0223,IFAX910392-44245
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: Onslow Water & Sewer Authority (ONWASA) PROJECT NAME: Northwest Regional WRF REPORT NO: 2Z ZZ7
ADDRESS. 228 Georgetown Rd CONTACT NAME: Mark Young PO NO:
Jacksonville, NC 28540 REPORT TO: [e-mail] PHONE/FAX: 910-54M877
17 COPY TO: [e-mail] email: [e-mail]
Sampled By: 4 , SAMPLE TYPE, I =Influent E - Effi t W - -
Sample Identification
VtgrYj
,Digester
Collection
Date
11/15/22
Time
`"
Temp
/ 7,/-
Transfer
1.
2.
Temperature when
Delivered By: ,
Rel
we", - Well, ST - Stream, SO = 5n,1, SL = Sludge; Other:
CL
_ PRESERVATION
m° a a a � m
ELo° c r E m z $ c a ANALYSIS REQUESTED
U t] U Z i = = s y p
C
SL
Received By:
5�"I x
Annual Sludge Analysis/ TCLP / P,QZ
Nutrient & Metals
pie Requested:
D: -Z 2- Time:
TURNAROUND:
C
SL
Received By:
5�"I x
Annual Sludge Analysis/ TCLP / P,QZ
Nutrient & Metals
pie Requested:
D: -Z 2- Time:
TURNAROUND:

COASTAL FARMS AND RESIDUALS, LLC
WQ0034806
Northwest Regional WRF
06/06/22
78
1.8921
06/06/22
76
1.8808
06/06/22
75
1.8751
06/06/22
216
2.3345
06/06/22
71
1.8513
06/06/22
74
1.8692
06/06/22
448
2.6513
Total 1 14.3542
Average 1 2.0506
Geometric Mean Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction
requirement.

env��r`ac�em'
Onslow Water & Sewer Authority
228 Georgetown Road
Jacksonville NC 28540
Attention: Mark Young
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ° 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 26540 • 910.347.5843 Lab/Pax
infora�environmentalcllejnists.com
Date of Report: Jun 14, 2022
Customer PO #:
Customer ID: 08100092
Report #: 2022-10300
Project ID: Northwest RWRF Digester
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
22-24910 Site: Digester #1 6/6/2022 10:55 AM Solid/Sludge Young/Baker
Test Method Results Date Analyzed
Total Solids (%
Fecal Density
Lab ID Sample ID:
22-24911 Site: Digester #2
Test
SM 2540 B
SM 9221C E-2014
2.33 % 06/07/2022
<78 MPN/g 06/06/2022
Collect Date/Time Matrix Sampled by
6/6/2022 11:00 AM Solid/Sludge Young/Baker
Method Results Date Analyzed
Total Solids (%)
SM 2540 B
2.37 %
06/07/2022
Fecal Density
SM 9221C E-2014
<76 MPN/g
06106/2022
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
22-24912 Site: Digester#3
6/6/2022 11:01 AM
Solid/Sludge Young/Baker
Test
Method
Results Date Analyzed
Total Solids {%)
SM 2540 B
2.67 %
06/07/2022
Fecal Density
SM 9221C E-2014
75 MPN/g
06/06/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-24913 Site: Digester 94 6/6/2022 11:03 AM Solid/Sludge Young/Baker
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.09 % 06/07/2022
Fecal Density SM 9221C E-2014 216 MPN/g 06/06/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-24914 Site: Digester#5 6/6/2022 11:04 AM Solid/Sludge Young/Baker
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E-2014
2.57 % 06/07/2022
71 MPN/g 06/06/2022
Report #:: 2022.10300 Page 1 of 2

ANALYTICAL & CONSULTING CHEMISTS
Onslow Water & Sewer Authority
228 Georgetown Road
Jacksonville NC 28540
Attention: Mark Young
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Load, Manteo, NC 27954 e 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info{i�environmen talchemists.com
Date of Report: Jun 14, 2022
Customer PO #:
Customer ID: 08100092
Report #: 2022-10300
Project ID: Northwest RWRF Digester
Lab ID Sample ID: Collect DatetTime Matrix Sampled by
22-24915 Site: Digester #6 6/6/2022 11:05 AM Solid/Sludge Young/Baker
Test Method Results Date Analyzed
Total Solids {%) SM 2540 B 2.46 % 06/07/2022
Fecal Density SM 9221C E-2014 74 MPN/g 06/06/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-24916 Site: Digester#7 6/6/2022 11:07 AM Solid/Sludge Young/Baker
Test Method Results Date Analyzed
Total Solids (°/a) SM 2540 B 2.46 % 06/07/2022
Fecal Density SM 9221C E-2014 448 MPN/g 06/06/2022
Comment: 1
Reviewed by:
Report #:: 2022-10300 Page 2 of 2

Analytical & Consulting Chemists
Client: Onslow Water & Sewer Authority
ADDRESS: 228 Georgetown Rd
Jacksonville, NC 28540
Sam led B
ENVIRONMENTAL CHEMISTS, INC OFFI E.,9 0-3 2-0223Windmill Way'IFAX 910-392-44245
@
NCDENR: DWQ CERTIFICATION # 94 NCDHH5: DLS CERTIFICATION # 37729 infoenvironmentalchemists.com
COLLECTION AND CHAIN OF CUSTODY
ONWASA PROJECT NAME: Northwest Regional WRF REPORT NO:
CONTACT NAME: Mark YoungPO NO:
REPORT TO: [e-mail] PHONE/FAX: [phone]
COPY TO: Martin WILLCOXMABESOiL.COM email: m oun onwasa.com
p y
a Aia IMM
Qm9k
SAMPLE TYPE: I = lnfiuent, E = Effluent, W = Weffeefft; $p= Soil' SL=Mudge; DtYter.
It
Collection
o
PRESERVATION
Sample Identification
p
E a
e F
a. V
E 0
9"
=
—�� E
m m
i
H
o
a
a
w
ANALYSIS REQUESTED
Date
Time
Tempy
U
"
z'
z
_"
r
-?
o
----- _.
6/6/22
°
O
Digester- Fecal 1
SL
Q
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X
Fecal Densit
5 (M o
6/6122
J 00
3o
Z
c
®
Digester- Fecal 2
SL
Q
G
X
Fecal Densit
6/6/22
0
-7 t?
C
I fp
Digester- Fecal 3
SL
QG)
I G
X
Fecal DensityDigester-
Fecal 4
SL
G
Yg f
X
Fecal Density'
6/6122
p
C
P
Digester- Fecal 5
qq
r�
SL
OD
G
p
-X
Fecal Density
Digester-
616122
C
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Fecal 6
5L
©
G
X
Fecal Density
Digester- Fecal 7
616122
°
C
P
SL
G
G
X
Fecal Density
Transfer
Relinquished By:
Date/Time
a ei d y:
1 Oaterrime
t.
— - _ -
-
a J
0q-P-
2..
Temperature when Received:
Delivered
Accepted:
ejected:
Resampip -qeqested:
By:
C.
Received
By:
Date:
(4 Time:
Comments:
TUR
AROUND:

Environmental Chemist, Inc., Wilmington, NC Lab 094 6602 Windmill Way
Wilmington, NC 28405
910,392.0223
Sample Receipt Checklist
Client: Sco Date: Report Number:
Receipt of sample:
ECHEM Pickup Client Delivery ❑
LIPS ❑ FeclEx ❑ Other ❑
❑
YES
JE1
NO
N/A
1. Were custody seals present on the cooler?
❑
YES
113
NO
N/A
2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt
oC Corrected temperature upon receipt
How temperature taken:
❑ Temperature Blank Against Bottles
IR Gun ID: Thomas Traceable
S/N 192511657 IR Gun Correction Factor "C: 0.0
❑
YES
10
NO
3. If temperature of cooler exceeded VC, was Project Mgr./QA notified?
YES
❑
NO
4. Were proper custody procedures (relinquished/received) followed?
�]
YES
❑
NO
5. Were sample ID's listed on the COC?
YES
❑
NO
6. Were samples ID's listed an sample containers?
YES
❑
NO
7. Were collection date and time listed on the COU
YES
❑
NO
8. Were tests to be performed listed on the COC?
YES
❑
NO
9. Did samples arrive in proper containers for each test?
YES
❑
NO
10. Did samples arrive in good condition for each test?
7�
YES
❑
NO
11. Was adequate sample volume available?'
21
YES
❑
NO
12. Were samples received within proper holding time for requested tests?
❑
YES
❑
NO
13. Were acid preserved samples received at a pH of <2?
❑
YES
❑
NO
14. Were cyanide samples received at a pH >12?
❑
YES
❑
NO
115. Were sulfide samples received at a pH >9?
❑
YES
❑
NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑
YES
❑
NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑
YES
❑
NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
" TOC/Volatifes are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Vote: Notify customer service immediately for Incorrectly preserved samples. Obtain a newsample or
iotify the state lab if directed to analyzed by the customer, Who was notified, date and time:
Jolatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1
"C

RWRF
189 Mills Field Rd
city
Richlands
State/Zip
NC, 28574
Phone/Fax
[phone]
Sample Name or Field 10
NW Fecal # 1
NW Fecal # 2
NW Fecal # 3
NW Fecal # 4
NW Fecal # 5
NW Fecal # 6
NW Fecal # 7
ONWASA Laboratory
228 Georgetown Road
Jacksonville, North Carolina 28540
NW Solids
Project Number
[none]
Project Description
Sludge Fecal C
PO Number
ihipped By
rrackina Number
Sampled Date
Sampled Tlme
Code
6/6/2022
(4
G
6/6/2022
Di7
G
6/6/2022
G
6/6/2022
1 lips
G
6/6/2022
G
6/6/2022
G
6/6/2022
i )
G
CHAIN OF CUSTODY IIIIlIlll�lll�� I�Illlllil� I II�
Pagi 1 of 1 N222411
Phone: [phone] _ -. . COC Number
Fax: [phone] Lab Work Order Numl N222411
W rL
U O
a
N
N
01
ul
N
—
u]
4
ae
N
W
G
a
�—
O
m
in
hi
V
a
ut
o
Preservation
MaLrix Lantainer
Code Count
P::C
P::A
WW 1
ID
WW 1
1
0
WW 1
1
0
WW 1
1
0
WW 1
1
0
ww 1
1
0
Ww 1
1 1
0
--_ tto Rushrequestssubjec
"(D additional charge.
' — --Rush requests sub]eLftolo
(DL approval.
n
� 5taodard (days) _-
- a 10
o Expedited (days)
..— ... I—.. VVW=5L Preserv.Codes: A=CoolSdegC,C--0.000B%Na2S203
' Indicates Field Test Analysis Cont. Codes P="' DEFAULT CONTAINER—,P--120 Sterile N22SZ03

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Coastal Farms and Residuals, LLC WQ Permit Number: WQ0034806
WWTP Name: NorthwestRegianal WRF NPDES Number: WQ0034367
Monitoring Period: From 1/l/2022 To 12/31/2022
Pathogen Reduction (15A NCAC 02T 1106) - Please indicate level achieved and alternative performed:
Class A: Alt. A (time/temp) ❑ 1 Alt B (Alk Treatment) ❑ I Alt. C (Prior Testing) ❑
AILD (No Prior Test) ❑ I Process to Further Reduce PatIiogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thennophilic ❑
Beta Ray ❑ Gamma Ray ❑ - Pasteurization ❑ :..._ ,,............. .
Class B: I Alt. (1) Fecal Density
If applicable to alternative performed (Ch
Lime Stabilization ❑ Air
Anaerobic
Digestion
If applicable to alternative performed l
Parameter Allowable Level
in Sludge 6—inilt
2 x 10 to the MPN 71
6th power
per gram of
Fecal Coliform total solids CFU
1000 mpn per gram
of total solid (dry
ilmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid (dry
coliform) weight)
Alt. (2) Process to Significantly Reduce Pathogens ❑
B only) indicate "Process to Significantly- Reduce Pathogens":
Yin ❑ Composting ❑ Aerobic Digestion ❑
ass A or Class B) complete the following monitoring data:
Pathogen Density um er ot Frequency Sample nay c
Excee- of Anal s Tech-
Geo. Mean Maximu Units deuces y ks Type „;nnv
112 1 216 1 MPN/g 1 0 1 Annual j Grab
vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ I Alt. 4 (Spec. O, uptake) ❑
Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying -Stable) ❑ I Alt. 8 (Drying - Unstable) ❑
Alt. 4 (Injeckion} I] Alt. 10 {Incorporation) I] No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been stet."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T 1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mark Young, ORC Wesley Wooten, President
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
_ _ 6 _ 1/5/2023 ,�, 1/5/23
Signature of Prepar e Date Signature of Lan Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRE 02T (1212006)

COASTAL RESIDUALS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 12, 2022
Oak Island WWTP
2.33 % Solids
6.75 pH
Permit No. WQ0005790
Parameter
%
1Mg/KgDryWeight1
(% x 10,000)
Pounds/Dry Ton
(M x 0.002)
Nitrogen (TKN)
4.600
46,000.000
92.000
Phosphorus
1.240
12,400,000
24.900
Potassium
0.321
3,210,000
6.420
PAN (injected)*
1.678
16,784.480
33.569
PAN (surface)*
1.465
14,654.480
29.309
Ammonia Nitrogen
0.426
4,260.000
8.520
Calcium
3.960
38,600.000
77.200
Calcium Carbonate E .
---
---
---
Magnesium
---
2,770.000
5.540
Sodium
---
6,270.000
12.540
Sulfur
---
---
Nitrate N / Nitrite N
---
2.480
0.005
Barium
---
---
---
SAR
L 1.27
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
3,510.00
7.020
Arsenic
---
27.50
0.055
75
Cadmium
---
20.40
0.041 185
Chromium
---
20.400
0.041
--
Copper
---
200.00
0.400
4,300
Lead
---
20.40
0.041
840
Mercury
---
0.72
0,001
57
Molybdenum
---
20.40
0.041
75
Nickel
--
20.40
0.041
420
Selenium
---
20.40
0.041
100
Zinc
---
1,020.00
2.040
7,500
Environmental Chemists# 2022-00764
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

C f rY,
s��env�:rache��
ANALYTICAL & CONSULTING CHEMISTS
Town of Oak Island
4601 East Oak Island Drive
Oak Island NC 28465
Attention:
Lab ID Sample ID:
22-01885 Site: Sludge
Test
Sludge Residuals
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Nitrate+!Nitrite-Nitrogen
Total Solids (%)
Ammonia Nitrogen
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Feb 03, 2022
Customer PO #:
Customer ID: 1110D035
Report #: 2022-00784
Project ID: Sludge
Collect DatelTime Matrix Sampled by
1/12/2022 11:40 AM Solid/Sludge Kenneth Von Voigt
Method
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4. 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev, 4.4, 1994
EPA 200.7, Rev, 4.4. 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4. 1994
EPA 20o.7, Rev. 4.4, 1994
EPA 200,7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4. 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 353.2
SM 2540 B
SM 4500 NH3 C-2011
Total Kjeldahl Nitrogen (TKN) SM 4500 Norg B-2011
Total Phosphorous SM 4500 P (F-H)-2011
pH SW 846 Method 9045D
Result estimated. Analyzed out of 15 minutes hold time.
Mercury sW-B46 7471 B
Comment: .gyp
Reviewed by: L
Results
3510 mglkg
27.5 mglkg
<20.4 mg/kg
38600 mg/kg
<20.4 mg/kg
200 mglkg
<20.4 mg/kg
2770 mglkg
<20.4 mglkg
<20.4 mglkg
3210 mglkg
<20.4 mg/kg
6270 mglkg
1020 mglkg
2.48 mg/kg
2.33 %
4260 mglkg
46000 mglkg
12400 mglkg
6.75 units
<0.717 mg/kg
Date Analyzed
01/26/2022
01126/2022
01 /26/2022
01 /26/2022
01/26/2022
01 /26/2022
01126/2022
01/26/2022
01 /26/2022
01 /26/2022
01131 /2022
01 /31/2022
01 /31 /2022
01/26/2022
01114/2022
01114/2022
01/17/2022
01/17/2022
01 /16/2022
01 /24/2022
01 /14/2022
Report #.: 2022-00764 Page 1 of 1

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910-392.0223
Sample Receipt Checklist
Client- 0M
I'sLa N» `1Z WIQ Date: (Z c�a Report Number.QA 0^]�0
Receipt of sample:
ECHEM Pickup Client Delivery ❑ UPS ❑ FedEx ❑ Other ❑
❑ YES
❑
NO
Z N/A I. Were custody seals present on the cooler?
❑ YES
10
NO
1� N/A 12. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt ,I— -C Corrected temperature upon receipt
How temperature taken:
❑ Temperature Blank Vr Against Bottles
IR Gun (D: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
❑ YES
10
NO
1 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA
V YES
10
NO
notified?
1 4. Were proper custody procedures (relinquished/received) followed?
YES
10
NO
S. Were sample ID's listed on the COC?
IM YES
10
NO
6. Were samples ID's listed on sample containers?
[ YES
❑
NO
7. Were collection date and time listed on the COC?
YES
10
NO
8. Were tests to be performed listed on the COC?
YES
❑
NO
9. Did samples arrive in proper containers for each test?
YES
❑
NO
10. Did samples arrive in good condition for each test?
1�1 YES
10
NO
Ill. Was adequate sample volume available?'
YES
❑
NO
112. Were samples received within proper holding time for requested tests?
❑ YES
❑
NO
113. Were acid preserved samples received at a pH of <2? #
❑ YES
ID
NO
114. Were cyanide samples received at a pH >12?
❑ YES
10
NO
115. Were sulfide samples received at a pH >9?
❑ YES
10
NO
116. Were NH3/TKN/Phenol received at a chlorine residual of <0,5 m/L? **
❑ YES
❑
NO
1.17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 rn/I_?
❑ YES
10
NO
118. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatifes are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation; {Must be completed for any samples) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): HZSO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
dolatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1
"C

ltl,t.1bn
`may
Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF Cl1ST()nv
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
CLIENT: Town of Oak Island
PROJECT NAME: Fish Factory WWTP
REPORT NO: ' ' J- - 7 (,4
ADDRESS: 4601 East Oak Island Drive
Oak Island, NC 28465
CONTACT NAME: David Kelly, II (Director)
REPORT TO: Tray Bivins ([e-mail]
PO NO:
PHONEIFAX: 201.80411278.7438
Permit # WQOD05790
[e-mail]
Sampled By: cw1 a Ira ��
SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream,
SO = Soil, SL = Sludge, Other:
Collection
L
.a
cl7
Ky 0 W
PRESERVATION
Sample Identification
a
o
c o
o m
E a
o o Q u,
z a
ANALYSIS REQUESTED
Date
tq
Time Temp
o
U
4.
r
U J
_o
O i n z Q = N
_ = z ~ a
C
P
Effluent
G
G
X X
BOD, NO3 KN
C
P
Effluent
G
G
X
Fecal Coliform
C
P
21month Apr -October
G
G
C
P
1/month Nov -March
G
G
C
P
G
G
C
P
Feb/June/October
G
G
X X
TDS, TOC, Chloride
� L� ��G-
�
S L L/
A r4f
C
P
ml"Fl �s
G
G
C
P
G
G
C
P
G
G
LIMITS (daily): BOD 15 mglL, NH3 6 mglL, TSS 10 mg1L, Fecal 25 colonlesf100 ml
Transfer
Re-Rej4i
Date/Time
Received By:
Date/Time
2.
Temperature when Received: 4/
Accepted:
Rejected:
Resample Requested:
Delivered By: / - Received By:
Comments:
: i
4t a- Time:
TURNAROUND:

COASTAL FARMS AND RESIDUALS, LLC
WQ0034806
Oak Island WWTP
aeeCa�kivig
02/09/22
535,118
5.7284
02/09/22
454,546
5.6576
02/09/22
526,316
5.7212
02/09/22
599,441
5.7777
02/09/22
590,406
5.7712
02/09/22
466,473
5.6688
02/09/22
43 7,15 9
5.6406
Total 1 39.9656
Average 1 5.7094
Fecal Coliform MPN / gram
Geometric Mean Q
Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen Reduction
requirement.

r Environmental Chemists Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Mantea, NC 27954 252.473.5702 Lab/Fax
s` 255-A Wilmington Highway, Jacksonville, NC 28540 ° 910.347..5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info!ic`environmenielcllemists.com
Town of Oak Island
Date of Report: Mar 15, 2022
4601 East Oak Island Drive
Customer PO #:
Oak Island NC
28465 Customer ID: 11100035
Attention:
Report #: 2022-02447
Project ID: Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-05794 Site: Sludge
2/9/2022 9:15 AM Solid/Sludge Kenneth Von Voigt
Test
Method Results Date Analyzed
Total Solids (%}
SM 2540 s 2.99 % 02110/2022
Fecal Density
SM 9221C E-2014 535118 MPN/g 02/09/2022
Lab 1D Sample ID:
Collect Date/Time Matrix Sampled by
22-05795 Site: Sludge
2/9/2022 9:16 AM Solid/Sludge Kenneth Von Voigt
Test
Method Results Date Analyzed
Total Solids
SM 2540 8 3.52 % 02/10/2022
Fecal Density
SM 9221C E-2014 454546 MPNIg 02/09/2022
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
22-05796 Site: Sludge
2/9/2022 9:20 AM Solid/Sludge Kenneth Von Voigt
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 3.04 % 02/10/2022
Fecal Density
SM 9221C E-2014 526316 MPNIg 02/09/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22--05797 Site: Sludge
2/9/2022 9:21 AM Solid/Sludge Kenneth Von Voigt
Test
Method Results Date Analyzed
Total Solids (%)
SM 254o a 2.86 % 02/10/2022
Fecal Density
SM9221C E-2014 599441 MPNIg 02/09/2022
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
22-05798 Site: Sludge
2/9/2022 9:22 AM SolidlSludge Kenneth Von Voigt
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 2.71 % 02/10/2022
Fecal Density
SM 9221 c E-2014 590406 MPNIg 02/09/2022
Report #;; 2022-02447 Pagel of 5

Environmental Chemists, Inc.
env
1 6602 Windmill Way, Wilmington, NC 28405 9I0.392.0223 Lab 9I0.342.4424 Fax
710 Botvsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
9M.
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSUI.TING CHEMISTS info(4,',environmentalchetnists.com
Town of Oak Island Date of Report: Mar 15, 2022
4601 East Oak Island Drive Customer PO #:
Oak Island NC 28465 Customer ID: 11100035
Attention: Report #: 2022-02447
Project ID: Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-05799 Site: Sludge 2/9/2022 9:23 AM Solid/Sludge Kenneth Von Voigt
Test Method Results Date Analyzed
Total Solids (%} SM 2540 B 3.43 % 02/10/2022
Fecal Density SM 9221C E-2014 466473 MPN/g 02/09/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-05800 Site: Sludge 2/9/2022 9:24 AM Solid/Sludge Kenneth Von Voigt
Test Method Results Date Analyzed
Total Solids (%) SM 2540 s 3,66 % 02/10/2022
Fecal Density SM 9221C E-2014 437159 MPN/g 02/09/2022
Report #:: 2022-02447 Page 2 of 5

�.: Environmental Chemists, Ines
' 0 "6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab 9 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax
5�'` 255-A Wilmington Highway, Jacksonville, NC 28540 • 910,347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infora;environnlentalclternists.coni
Town of Oak Island
4601 Bast Oak Island Drive
Oak Island NC 28465
Attention:
Date of Report: Mar 15, 2022
Customer PO #:
Customer ID: 11100035
Report #: 2022-02447
Project ID: Sludge
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
22-05BOl Site: Sludge
2/9/2022
9:00 AM Solid/Sludge Kenneth Von Voigt
Test
Method
Results
Date Analyzed
Chlordane (TCLP)
SW-846 8001 B
<0.02 mg/L
02/21/2022
Bndrin (TCLP)
SW-646 8081 B
<0.0005 mg/L
02/21/2022
Heptachlor (TCLP)
SW-846 8081 B
<0.0005 mg/L
02/21/2022
Heptachlor epoxide (TCLP)
SW-846 8081 B
<0.0005 mg/L
02/21/2022
Lindane (TCLP)
SW-846 8081 B
<0.0005 mg/L
02/21/2022
Methoxychlor (TCLP)
SW-846 8081 B
<0,0005 mg/L
02/21/2022
Toxaphene (TCLP)
SW-8468081 B
<0.05mg/L
02/21/2022
2,4,5-TP (TCLP)
SW-846 8151 A
<0.003 mg/L
02/21/2022
2,4-0 (TCLP)
SW-846 B151 A
<0.003 mg/L
02121/2022
1,4-Dichlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
02/24/2022
2,4,5-Trichlorophenol (TCLP)
sW-8468270 E
<0.050 mg/L
02/24/2022
2,4,6-Trichlorophenol (TCLP)
SW-646 8270 E
<0.050 mg/L
02124/2022
2,4-Dinitrotoluene (TCLP)
SW-846 8270 E
<0.050 mg/L
02/24/2022
Cresol (TCLP)
SW-846 8270 E
0.079 mg/L
02/24/2022
Hexachloro-1,3-butadiene (TCLP)
SW-8468270E
<0,050mg/L
02/24/2022
Hexachlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
02/24/2022
Hexachloroethane (TCLP)
SW-846 5270 E
<0.050 mg/L
02/24/2022
m + p-Cresol (TCLP)
SW-846 8270 E
0.079 mg/L
02/24/2022
Nitrobenzene (TCLP)
SW-8468270E
<0.050mg/L
02/24/2022
o-Cresol (TCLP)
SW846 8270 E
<0.050 mg/L
02/24/2022
Pentachlorophenol (TCLP)
SW-646 8270 E
<0.250 mg/L
02/24/2022
Pyridine (TCLP)
SW-6468270E
<0,050mg/L
02/24/2022
1,1-Dichloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
02/22/2022
1,2-Dichloroethane (TCLP)
SW-846 Method 8260D
<0.01 mg/L
02/22/2022
Benzene (TCLP)
SW-846 Method 8260D
<0,01 mg/L
02/22/2022
Carbon Tetrachloride (TCLP)
SW-84B Method 8260D
<0.01 mg/L
02/22/2022
ReportV 2022.02447
Page 3 of 5

Environmental Chemists Inc.
6602 Windmill Way, Wilmington, NC 28405 9103910223 Lab 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 252.473.5702 Lab/Fax
4 xx, 255-A Wilmington Highway, Jacksonville, NC 28340 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info!g-cnvironmentit lchemists,com
Town of Oak Island Date of Report: Mar 15, 2022
4601 East Oak Island Drive Customer PO #:
Oak Island NC 28465 Customer ID: 11100035
Attention: Report #: 2022-02447
Project ID: Sludge
Chlorobenzene (TCLP) $W-646 Method 02600 <0.01 mg/L 02/22/2022
Chforoform (TCLP) SW-046Method 82600 <0.01 mg/L 02/22/2022
Methyl ethyl ketone (TCLP) SW-846 Method B250D <0.05 mg/L 02/22/2022
Tetrachloroethylene (TCLP) SW-646 Method8260D <0,01 mg/L 02/22/2022
Trichloroethylene (TCLP) SW-646 Method 8260D <0.01 mg1L 02/22/2022
Vinyl Chloride (TCLP) SW-646 Method8260D <0.01 mg/L 02/22/2022
RCI
Cyanide
SM 4500 CN D-2016
2.00 mg/kg
02/14/2022
Sulfide
SM 4500 S D
77.2 mg/kg
02/15/2022
lgnitability
SW 646 method 1010
>158 °F
0211812022
pH SW 646 Method 9045D
Result estimated. Analyzed out of 15 minutes hold time.
7.06 units
03/14/2022
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4, 1994
2340mg/kg
02/15/2022
Arsenic
EPA 200.7, Rev. 4.4, 1994
<37,5 mg/kg
02/15/2022
Cadmium
EPA 200.7, Rev- 4.4, 1994
<37.5 mglkg
02/15/2022
Calcium
EPA 200.7, Rev, 4.4, 1994
23500 mg/kg
02/15/2022
Chromium
EPA 200.7, Rev. 4.4,11394
<37,5 mg/kg
02/15/2022
Copper
EPA 200.7, Rev. 4A, 1994
196 mg/kg
02/15/2022
Lead
EPA 200.7, Rev. 4.4, 1994
<37.5 mg/kg
02/15/2022
Magnesium
EPA 200.7, Rev. 4.4, 1994
2060 mg/kg
02/15/2022
Molybdenum
EPA 200.7, Rev. 4.4, 1994
<37.5 mg/kg
02/15/2022
Nickel
EPA 200.7, Rev. 4,4, 1994
<37.5 mg/kg
02/16/2022
Potassium
EPA 200.7, Rev. 4.4, 1994
3990 mg/kg
02/15/2022
Selenium
EPA 200.7, Rev. 4.4, 1994
<37.5 mg/kg
02/15/2022
Sodium
EPA 200.7, Rev. 4.4, 1994
2610 mg/kg
02/15/2022
Zinc
EPA 200.7, Rev. 4.4, 1994
861 mg/kg
02/15/2022
Nitrate+Nitrite-Nitrogen
EPA353.2
9.43mg/kg
02/10/2022
Total Solids (%)
SM 2540 B
2.88%
02/10/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
1980 mg/kg
02/10/2022
Report #:: 2022-02447
Page 4 of 5

Environmental Chemists, Inc®
6602 Whidmill Way, Wilma igton, NC 28405 910.392 0223 Lab 910.392.4424 Fax
M MA
f _ 710 Bowsertown Road, Manteo, NC 27954 252.473.5702 Lab/Fax
fykSU. 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info(i?environmentalcliemists.com
Town of Oak Island Date of Report: Mar 15, 2022
4601 East Oak island Drive Customer PO #:
Oak Island NC 28465 Customer ID: 11100035
Attention: Report #: 2022-02447
Project ID: Sludge
Total Kjeldahl Nitrogen (TKN) SM 4500 Norg B-2011 61400 mg/kg 02/10/2022
Total Phosphorus SM 4500 P (F-H)-2011 16800 mg/kg 02/17/2022
Mercury SW-8467471 B 1.25 mg/kg 02/10/2022
TCLP Metals
Arsenic
EPA 200.7, Rev. 4 4, 1994
<1.0 mg/L
02/21/2022
Barium
EPA 200.7, Rev 4 4, 1994
<1.0 mg/L
02/21/2022
Cadmium
EPA 200.7, Rev 4 4, 1994
<1.0 mg/L
02/21/2022
Chromium
EPA 200.7, Rev 4 4, 1994
<1.0 mg/L
02/21/2022
Lead
EPA 200.7, Rev. 4 4.1994
<1.0 mg/L
02/21/2022
Selenium
EPA 200.7, Rev. 4 4.1994
<1.0 mg/L
02/21/2022
Silver
EPA 200.7. Rev, 4.4. 1994
<1,0 mg/L
02/22/2022
Mercury
EPA 245A
<0.0002 mg/L
02/24/2022
Comment:
Sludge residual reported on a dry weight basis.
by:
CReviewed -�
Report 4:; 2022-02447 Page 5 or 5

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
91O
Sam 1 .392.0223
p e Receipt CheCKUSt
Client: � �� � "� � � Date: 2/A�
Report Number: _ 2022- 6 ZY V7
Receipt of sample: ECHEM Pickup Client Delivery ❑ FedEx ❑ Other LJP5 ❑
❑ YES El NO El
N/A 1. Were custody seals present on the cooler?
❑ YES ❑ NO N/A 2, if custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C
How temperature taken: ❑ Temperature Blank Corrected temperature upon receipt
Against Bottles
IR Gun iD: Thomas Traceable 5/N: 210835468 1R Gun Correction Factor °C: 0.0
❑ YES El NO 3, if temperature of cooler exceeded 6°C, was Project Mgr.
QA
YES ❑ NO 4. Were proper custody procedures (relinquished/received) folllowed?d?
YES ❑ NO 5. Were sample iD's listed on the COC?
YES ❑ NO 6. Were samples iD's listed on sample containers?
YES ❑ NO 7. Were collection date and time listed on the COC?
YES ❑ NO B. Were tests to be performed listed on the COC?
YES ❑ NO 9. Did samples arrive in proper containers for each test?
YES ❑ NO 10. Did samples arrive in 000ri condition for ra-r?
J� YE5 oa,h
•-•
(❑ NO 111. Was adequate sample volume available?'
YES 11 NO 12. Were samples received within proper holding time for requested tests?
❑ YES ❑ NO 13. Were acid preserved samples received at a pH of <2?
❑ YES ❑ NO 14. Were cyanide samples received at a pH >12?
❑ YES ❑ NO I5. Were sulfide samples received at a pH >9?
❑ YES ❑ NO 1F,. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded an the benchsheet.
sample lreservation: {Must be completed for any sample ]
s) incorrectly preserved or with headspace
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
+late: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
iotify the state lab if directed to analyzed by the customer. Who was notified, date and time:
(alatiles Sarriple(s) were received with headspace
COMMENTS;
DOC. QA.002 Rev 1

-.,IiWII.�1.r:" e' ENVIRONMENTAL CHEMISTS, INC
Analytical & Consulting Chemists NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
CLIENT: Town of Oak Island
PROJECT NAME: Fish Factory WWTP
REPORT NO: 2- Z - Q Z 4
ADDRESS: 4601 East Oak Island Drive
CONTACT NAME: David Kelly, II (Director)
PO NO:
Oak Island, NC 28465
REPORT TO: Tray Bivins [e-mail]
PHONE/FAX: [phone]
Permit # W00005790
email:dkelly ci.oak-island.ne.us
Sampled By: Y- ,.� V'6M SAMPLE TYPE. I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil SL = Sludge Other:
le Identification
Collection
a
Q
U)
Qc b
o Q
c =
'
L)
p
MSam
z
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
o
z
o0
z
z'
y
Uj
r
o
Effluent
C
P
X
X
BOD S,N 3, NH3, TKN
G
G
Effluent
C
P
X
Fec form
G
G
2/month Apr -October
C
P
G
G
1/month Nov -March
C
P
G
G
C
P
G
G
Feb/June/October
C
P
X
X
TDS, TOC, Chloride
G
G
P
GJifc�
LU D G-(f-
GJ
G
G
C
P
G
G
C
P
G
G
LIMITS {daily}: BOD 15 mg1L., NH3 6 mglL, TSS 10 mg/L. Fecal 25 colonies1100 ml
Transfer j
1.
jRelin u'
Date/Time
acd
Received By:
P6b
Date/Time
2.
I erniperature wnen rceceivea: ti Accepted: 11 Rtahe to : Resample Requested:
Delivered By. _ Received By: _ Date: `9 - Crl Time:
Comments: TURNAROUND:

ENVIRONMENTAL CHEMISTS, INC
ngton
OFFICE: 910'392-D
23FIAX910-3 2-44 45
Analytical & Consulting Chemists
NCDENR: DWQ CERTIFICATION # 94 NCDIIHS: DLS CERTIFICATION #
37729
[e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: Town of Oak island
PROJECT NAME: Fish Factory
REPORT NO: ZZ - 0 Z �-
ADDRESS: 4601 East Oak Island Drive
CONTACT NAME:
PO NO:
Oak Island, NC 28465
REPORT TO:
PHONE/FAX:
COPY TO:
email:
Sampled Ely:p O
SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, $O = Soil, SL = Sludge, Other.
Collection PRESERVATION
Sample Identification
a o M m
m CL CL `o w o
E
F
o o
ANALYSIS REQUESTED
Date Time
y o p n s g 5 rn
Temp U" z
y
`a
� C P
1
�J S[f G G 51Qq
X
Fecal Density/% TS
2}
rJ�• G G Jr" -7 C1
X
Fecal Density!% TS
3)
C
G G 157q
Fecal Density/% TS
4)
C P
G G 5Ci
X
Fecal Density!% TS
i
5)
� C P
S
G G
X
Fecal Density!% TS
6)
��
X
Fecal Density/% TS
G
G
7}
X
Fecal Density/%TS
G
G
G
G
Transfer
1.
2.
Temperature when Received: Accepted:
Delivered By: Received By:
Comments:
Dateriime Received By:
: N ---rdol Time:
TURNAROUND:
Date/Time

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORtNI (02T Mules)
FacilityName: Coastal Farms and Residuals, LLC WQ Permit Number: WQ0034806
WNN'TP Name: Oak Island 1VIVTP NrDL, S Number: WQ0005790
Nlonituring Period: From 1/1/2022 To 12/31/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (lime/tern) ❑ Alt Q (Alk 1'rcattucnt) ❑ Alt. C (Prior Testing)❑
Alt.D (No Prior'Cest) ❑ Process to Further Reduce Patho en s ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑ Thcrnto hilic ❑
Beta Ray 01
Gamma Ray ❑
Pasteurization ❑
Class B:
Alt. (])Fecal Densi p Alt. (2) Process to Significantly Reduce Aatlio ens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pntltogens":
Lime Stabilization ❑ AirDrying ❑ Composling jAerobic Digestion ❑
Anaerobic Digestion ❑ • - - - •
g
If applicable to alternative performed (Class A or Class B) complete the fo11Divin monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen [tensity
Excee- um er al
rncv�
Frequency
afAnalysis
Sample
Type
ytica
Analytical
Tcch-
nigue
Minimurr
Gt o. Mean
Maximo
Untls
Fecal Coliform
2 s l0 to the
6th power
per gram of
total solids
WN
CFU
I OOO mpn per gram
oftotal solid (dry
wet ht}
437,159
512,126
599,441
WN/g
0
Annual
Grab
S%IMICE
Salmonella bacteria
(in lieu of feral
coliform)
3 MPN per 4 grams
total solid (dry
weight)
FT
I
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction)
[Ell
It. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 0, uptake)
ElAlt.
5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization El
Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
El
Alt. 10 (Incorporation) El
No vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in ISA NCAC 02T.1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements Itave been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kenny Von Voigt, ORC Wesley Wooten, President
PreparerNarne 7inditte w4rin. Land Applier ;`lame and Title (if applicable)(type or print)
I, b/2,
Signature of Preparers` Date Signature of La Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 5039(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

COASTAL RESIDUALS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: April 6, 2022
Pluris Hampstead WWTF Permit No. WQ0037287
1.38 % Solids
6.82 pH
Parameter
%
JMg/KgDryWeightJ
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.0021
Nitrogen (TKN)
6.490
64,900.000
129.800
Phosphorus
2.470
24,700.000
49.400
Potassium
1,310
13,100.000
26.200
PAN (injected)*
2,047
20,465.450
40.931
PAN (surface)*
1.976
19,755.450
39.511
Ammonia Nitrogen
0.142
1,420.000
2.840
Calcium
1.220
12,200.000
24.400
Calcium Carbonate E .
---
---
---
Magnesium
...
5,410.000
10.820
Sodium
---
6,980.000
13.960
Sulfur
---
---
.._
Nitrate N / Nitrite N
---
1.450
0.003
Barium
---
---
---
SAR
1.55
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/KS)
Aluminum
---
4,320.00
8.640
Arsenic
---
33.00
0.066
75
Cadmium
---
33.00
0.066
85
Chromium
---
33.000
0.066
---
Copper
---
126.00
0.252
4,300
Lead
---
33.00
0.066
840
Mercury
---
1.26
0.003
57
Molybdenum
---
33.00
0.066
75
Nickel
---
33.00
0.066
420
Selenium
---
33.00
0.066
1 100
Zinc
---
449.00
0.898
1 7,500
Environmental Chemists # 2022-06277
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

COASTAL FARMS AND RESIDUALS, LLC
WQ0034806
Pluris Hampstead WWTF
04/06/22
630,137
5.7994
04/06/22
360,000
5.5563
04/06/22
1,066,667
6.0280
04/06/22
975,610
5.9893
04/06/22
987,655
5.9946
04/06/22
1,012,659
6.0055
04/06/22
593,549
5.7735
Total 1 41.1466
Average 1 5.8781
Geometric Mean I I Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction
requirement.

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 0 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
inFoCq;environmen ta[chemists.com
Pluris LLC,
P. O. Box 856
Sneads Ferry NC
Attention: Randy Hoffer
28460
Date of Report: Apr 27, 2022
Customer PO #:
Customer ID: 09110001
Report #: 2022-06277
Project ID: Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-15287 Site: Sledge
4/6/2022
11:40 AM Solid/Sludge Kris King
Test
Method
Results
Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4. 1994
4320 mg/kg
0411412022
Arsenic
EPA 200.7, Rev, 4.4, 1994
<33.0 mg/kg
04/14/2022
Cadmium
EPA 200.7. Rev. 4A. 1994
<33.0 mg/kg
04/14/2022
Calcium
EPA 200.7, Rev, 4.4. 1994
12200 mg/kg
04/14/2022
Chromium
EPA 200.7, Rev. 4.4, 1994
<33.0 mg/kg
04/14/2022
Copper
EPA 200.7, Rev. 4.4. 1994
126 mg/kg
04/14/2022
Lead
EPA 200.7, Rev. 4.4, 1994
<33.0 mg/kg
04/14/2022
Magnesium
EPA 200.7, Rev. 4.4, 1994
5410 mg/kg
04/14/2022
Molybdenum
EPA 200.7, Rev, 4.4, 1994
<33.0 mg/kg
04/14/2022
Nickel
EPA 200.7, Rev. 4.4, 1994
<33.0 mg/kg
04/14/2022
Potassium
EPA 200.7, Rev. 4.4, 1994
13100 mg/kg
04/14/2022
Selenium
EPA 200.7, Rev. 4.4, 1994
<33.0mg/kg
0411412022
Sodium
EPA 200.7. Rev. 4.4, 1994
6980 mg/kg
04/14/2022
Zinc
EPA 200.7, Rev. 4 4, 1994
449 mg/kg
04/14/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2
<1.45 mg/kg
04/13/2022
Total Solids (%)
SM 2540 B
1.38 %
04/07/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
1420 mg/kg
04/07/2022
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
84900 mglkg
04/07/2022
Total Phosphorus
SM 4500 P (F-H)-2011
24700 mg/kg
04/20/2022
pH
SW 845 Method 9045D
6,82 units
04/12/2022
Result estimated. Analyzed out of 15 minutes hold time.
Mercury
SW-846 7471 a
<1.26 mg/kg
04/25/2022
Report #:: 2022-06277 Pagel of 3

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 4 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
�M} 255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347,5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS in%�rlenvironmentalchemists.com
Pluris LLC.
Date of Report: Apr 27, 2022
P. O. Box 856
Customer PO #:
Sneads Ferry NC
28460 Customer ID: 09110001
Attention: Randy Hoffer
Report #: 2022-06277
Project ID: Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-15288 Site: 001
4/6/2022 11:40 AM Solid/Sludge Kris King
Test
Method Results Date Analyzed
Total Solids
SM 2540 B 1.46 % 04/07/2022
Fecal Density
SM 9221C E MPN 24 hr 503 630137 MPN/g 04/06/2022
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
22-15289 Site: 002
4/6/2022 11:40 AM Solid/Sludge Kris King
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 a 1.50 % 04/07/2022
Fecal Density
SM 9221C E MPN 24 hr 503 360000 MPN/g 04/0612022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-15290 Site: 003
4/6/2022 11:40 AM Solid/Sludge Kris King
Test
Method Results Date Analyzed
Total Solids (%)
SM 254o u 1.50 % 04/07/2022
Fecal Density
$M 9221C E MP 24 hr 503 1066667 MPN/g 04/06/2022
Lab ID Sample 1D:
Collect Date/Time Matrix Sampled by
22-15291 Site: 004
4/6/2022 11:40 AM Solid/Sludge Kris King
Test
Method Results Date Analyzed
Total Solids
SM 2540 B 1.64 % 04/07/2022
Fecal Density
SM 9221C E MPN 24 hr 503 975610 MPN/g 04/06/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-15292 Site: 005
4/6/2022 11:40 AM Solid/Sludge Kris King
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 1.62 % 04/07/2022
Fecal Density
SM 9221C E MPN 24 hr 503 987655 MPN/g 04/06/2022
Report #:: 2022.06277
Page 2 of 3

Pluris LLC.
P. O. Box 856
Sneads Ferry NC
Attention: Randy Hoffer
Lab ID Sample ID:
22-15293 Site:006
Environmental Chemists, Inc.
6602 Windmill Way Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info/rilenvi ro nmen t a lchem ists. com
Date of Report: Apr 27, 2022
Customer PO ##:
28460 Customer ID: 09110001
Report #: 2022-06277
Project ID: Sludge
Collect Date/Time Matrix Sampled by
4/6/2022 11:40 AM Solid/Sludge Kris King
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
Lab ID Sample ID:
22-15294 Site:007
Test
Total Solids (%)
Fecal Density
SM 2540 a 1.58 % 04/07/2022
SM 9221C E MPN 24 hr503 1012659 MPN/g 04106/2022
Collect Date/Time Matrix Sampled by
4/6/2022 11:40 AM Solid/Sludge Kris King
Method
SM 2540 B
SM 9221 C E MPN 24 iv 503
Comment: i
Reviewed by:,A
f
Results Date Analyzed
1.55 % 04/07/2022
593549MPN/g 04106/2D22
Report A. 2022-06277 Page 3 of 3

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392,0223
Sample Receipt Checklist
Client_--? tom[ S Date: Report Number: _ o (� Z
Receipt of sample:
ECHEM Pickup Client Delivery ❑
JUPS ❑ FeclEx ❑ Other ❑
ElYES
❑
NO
N/A 11. Were custody seals present on the cooler?
❑
YES
113
NO
Q N/A 12. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt
How temperature taken:
❑ Temperature Blank ❑ Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
❑
YES
❑
NO
3. If temperature of cooler exceeded 6"C, was Project Mgr./QA
j l
YES
❑
NO
notified?
4. Were proper custody procedures (relinquished/received) followed?
YES
10
NO
5. Were sample ID's listed on the COC?
YES
❑
NO
6. Were samples ID's listed on sample containers?
YES
❑
NO
7. Were collection date and time listed on the COC?
YES
❑
N0
8. Were tests to be performed listed on the COC?
YES
❑
NO
9. Did samples arrive in proper containers for each test?
YES
❑
NO
10, Did samples arrive in good condition for each test?
YES
❑
NO
11. Was adequate sample volume available?'
YES
❑
NO
12. Were samples received within proper holding time For requested tests?
❑
YES
❑
NO
13. Were acid preserved samples received at a pH of <2?
❑
YES
❑
NO
14. Were cyanide samples received at a pH >12?
❑
YES
❑
NO
15. Were sulfide samples received at a pH >9?
❑
YES
❑
NO
16, Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑
YES
❑
NO
117. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑
YES
❑
NO
I18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: if more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sampfe or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1
'C

INC6602WindmillWayWilmington,NC28405
ENVIRONMENT}4L �HEII�IMISTS
Analytical $ Consulting Chemists
NCDENR: DWO CERTIFICATION it 94 NCDHHS: DL.S CERTIFICATION # 37729 iin@a n i
nforenme talchem stscom dd24
COLLECTION AND CHAIN OF CUSTODY
Client: �%Uj-f �� G�� PROJECT f�AME:
T REPORT NO:
ADDRESS:CONTACT DAME; +
l PO NO:
REPORT TO: UA PHONE/FAX:
COPY TO: JL( , email:
Sam led B : , , SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream SO = Soil SL = Slud Oth c 11
Sample Identification
O eCtlOn
a,
o
�'
o
Date
Time
Temp
C
E
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R 17
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"
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C m A to
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11,t ll d
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-%9
2 .3 tr
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)TICE - DECHi 010-1 T
ZB
PRESERVATION
ge. er.
o:
w
ANALYSIS REQUESTED
O
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0
0
=
O
w
cc
2
z
z
r
s
z
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LL
0
ION. Samples for Ammonla. TKN, Cyanide, Phenol and Bacteria must be decntonnated (p.s ppm or less) in the field at the time of collection. See reverse for instructions
Transfer Relinquished By: DatelTime
1. ;$ p ei d By: D eliime
2.
Temperature w c i d C: Accepted:
Delivered By� p Rene ed: Resarpipl Re uest;ed-.
Comments:Received By; Date. '# 6 . Time:
TURNAR NO:

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
FacilityName: Coastal Farms and Residuals, LLC
WWTP Name: Pluris Hampstead WWTF
Monitoring Period: From 1/1/2022 To
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A: Alt. A (timeltennp) ❑ I Alt B (Aik Treatment) ❑ I Alt. C (Prior Testing) ❑
AIt.D (No Prior Test) ❑ I Process to Further Reduce Patliogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ _ Thennophilic ❑
Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑
WQ Permit Number: WQ0034806
NPDES Number: WQ0037287
12/3I/2022
Class B: lAlt. (1) FecaI Density El I Alt. (2) Process to Significantly Reduce Pathogens n
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Di inQ ❑ Coillposting ❑ Aerobic Digestion ❑
An _ aerobic Di estion
If applicable
pp able to alternative performed (C1ass.A .or Class .B)..complete the following..monitoring'data:
Parameter Allowable bevel Pathogen Density NUM er o Frequency Sample na ica
in Sludge ccMinimu Geo. Mean Maximu Units dense, of Analysis Type Tech-
2 x 10 to the 61h power MPN 360,000 755,233 1,066,667 MPN/g 0 Annual Grab SM92210E
per grant of CFU
Fecal Colifoim total solids
1000 mpn per gram
of total solid (dry
Imonella bacterial 3 MPN per 4 grams
(in lieu of fecal I total solid (dry
Vector Attraction Reduction (15A NCAC 02T 1107) - Please indicate alternative performed:
Alt. I (VS reduction) ❑ Alt. 2 (40-day bench) [IAlt. 3 (30-day bench) [IAlt. 4 (Spec. 0, uptake) ❑
Alt. 5 (14-Day Aerobic) [[:]I Kit. 6 (Alk. Stabilization ❑ WE 7 (Drying - Stable) ❑ I Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) p 10. 10 (Incorporation) p No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T A 107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements,)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
//W1 7-C Wesley Wooten, President
Preparer Name and Title (type or print) Land Applier Name and
Title (if applicable)(type or print)
4/27/22
S�ia ure of Prepafe'Or Date Signature of Lan Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (1212006)

COASTAL RESIDUALS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: April 27, 2022
Southeast Brunswick Sanitary District WWTP Permit No. WQ0013200
2.21 % Solids
5.81 pH
Parameter
%
JMg/KgDryWeight�(Mg/KgxO.002)
(% x I0,000)
Pounds/Dry Ton
Nitrogen (TKN)
5.950
59,500.000
119,000
Phosphorus
3.350
33,500.000
67.000
Potassium
0.516
5,160.000
10.320
PAN (injected)*
1.874
18,735.600
37.471
PAN (surface)*
1.811
18,110.600
36.221
Ammonia Nitrogen
0.125
1,250.000
2.500
Calcium
1.960
19,600.000
39.200
Calcium Carbonate E .
---
---
---
Magnesium
---
3,600.000
7.200
Sodium
---
2,680.000
5.360
Sulfur
---
--_
Nitrate N / Nitrite N
---
10.600
0.021
Barium
---
---
---
SAR
0.68
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/kg)
Aluminum
---
18,500.00
37.000
Arsenic
---
21.60
0.043
75
Cadmium
---
21.60
0.043
85
Chromium
---
26.500
---
--_
Co er
---
176.00
0,352
4,300
Lead
---
21.60
0,043
840
Mercury
---
0.805
0.002
57
Molybdenum
---
21.60
0.043
75
Nickel
---
21.60
0.043
420
Selenium
---
2I.60
0.043
t00
Zinc
---
643.00
1,286
17,500
Environmental Chemists # 2022-07642
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

COASTAL FARMS AND RESIDUALS, LLC
WQ0034806
Southeast Brunswick Sanitary District WWTF
' cL
V Q..i
04/27/22
69,125
4.8396
04/27/22
21,778
4.3380
04/27/22
33,475
4.5247
04/27/22
53,399
4.7275
04/27/22
120,604
5.0814
04/27/22
62,802
4.7980
04/27/22
84,159
4.9251
Total 33.2343
Average 4.7478
Geometric Mean s- ��;' 9-4 Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction
requirement.

ANALYTICAL & CONSULTING CHEMISTS
Envirolink, Inc.
PO Box 670
Bailey NC 27807
Attention: Stephanie Moore
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ° 9I0-392.0223 Lab O 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info(i i-environmentalchemists.com
Date of Report: May 18, 2022
Customer PO #:
Customer ID: 16040014
Report #: 2022-07642
Project ID: SBSD-Sludge
Lab ID Sample ID:
22-18497 Site: Sludge
Test
Collect DatelTime
4/27/2022 9:00 AM
Method
Matrix Sampled by
Solid/Sludge Stephanie Moore
Results Date Analyzed
Total Organic Carbon (TOC)
8060
395000 mg/kg
05/12/2022
Chlordane (TCLP)
SW-846 8081 B
<0.02 mg/L
04/27/2022
Endrin (TCLP)
SW-846 8081 B
<0.0005 mg/L
04/27/2022
Heptachlor (TCLP)
SW-846 8081 B
<0.0005 mglL
04/27/2022
Heptachlor epoxide (TCLP)
SW-B46 8081 8
<0.0005 mg/L
04127/2022
Lindane (TCLP)
SW-846 8081 B
<0.0005 mg/L
04/27/2022
Methoxychlor (TCLP)
SW-846 8081 B
<0.0005 mg/L
04/27/2022
Toxaphene (TCLP)
SW-846 8081 6
<0.05 mg/L
04/27/2022
2,4,5-TP (TCLP)
SW-B46 8151 A
<0.003 mg/L
05/03/2022
2,4-D (TCLP)
$W-848 8151 A
<0.003 mg1L
05/03/2022
1,4-Dichlorobenzene (TCLP)
SW-8468270 E
<0.050 mg/L
04/29/2022
2,4,5-Trichlorophen ol (TCLP)
SW-846 8270 E
<0.050 mg/L
04/29/2022
2,4,6-Trichlorophenol (TCLP)
SW-646 8270 E
<0.050 mg/L
04/29/2022
2,4-Dinitrotoluene (TCLP)
SW-845 8270 E
<0.050 mg/L
04/29/2022
Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
04/29/2022
Hexachloro-1,3-butadiene (TCLP)
SW-846 8270 E
<0.050 mg/L
04/29/2022
Hexachlorobenzene (TCLP)
9w-846 8270 E
<0.050 mg/L
04/29/2022
Hexachloroethane (TCLP)
SW-846 8270 E
<0-050 mg/L
04/29/2022
m + p-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
04/29/2022
Nitrobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
04/29/2022
o-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
04/29/2022
Pentachlorophenol (TCLP)
SW-846 8270 E
<0.250 mg/L
04/29/2022
Pyridine (TCLP)
SW-846 8270 E
<0.050 mg/L
04/29/2022
1,1-Dichloroethylene (TCLP)
SW-846 Method8260❑
<0.01 mg/L
05/03/2022
1,2-Dichloroethane (TCLP)
SW-1346 Meihod 8260D
<0.01 mg/L
05/03/2022
Benzene (TCLP)
SW-846 Method8260D
<0,01 mg/L
05/03/2022
Report k:: 2022-07642
Page i of 5

. . •:� - al,� ,��; fir:°r
ANALYTICAL & CONSULTING CHEMISTS
Envirolink, Inc.
PO Box 670
Bailey NC 27807
Attention: Stephanie Moore
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 > 252-473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
infota)environmen tale hemists.corn
Date of Report: May 18, 2022
Customer PO #:
Customer ID: 16040014
Report #: 2022-07642
Project ID: SBSD-Sludge
Carbon Tetrachloride (TCLP)
SW-846 Method 826DD
<0.01 mg/L
05/03/2022
Chlorobenzene (TCLP)
SW-846 Method6260❑
<0.01 mg/L
05/03/2022
Chloroform (TCLP)
SW-846 Method 8260D
<0.01 mg/L
05/03/2022
Methyl ethyl ketone (TCLP)
SW-848 Method 8260D
<0.05 mg/L
05/03/2022
Tetrachloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
05/03/2022
Trichloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
05/03/2022
Vinyl Chloride (TCLP)
SW-846 Method 8260D
<0.01 mg/L
05/03/2022
RCI
Cyanide
SM 4500 CN D-2016
2.55 mglkg
05/09/2022
Sulfide
Analyzed outside of hold time.
SM 4500 s D
0.93 mg/kg
06/16/2022
Ignitability
SW 846 method 1010
>158 °F
05/06/2022
Sludge Residuals
Aluminum
EPA 200.7. Rev. 4.4, 1994
18500 mg/kg
05/02/2022
Arsenic
EPA 20o.7, Rev. 4.4, 1994
<21.6 mg/kg
05/02/2022
Cadmium
EPA 2oo.7, Rev.4.4,1994
<21.6 mglkg
05/02/2022
Calcium
EPA 200.7, Rev. 4.4. 1994
19600 mg/kg
05/02/2022
Chromium
EPA 200.7. Rev, 4.4, 1994
26.5 mg/kg
05/02/2022
Copper
EPA 200.7, Rev. 4.4. 1994
176 mg/kg
05/02/2022
Lead
EPA 200,7, Rev. 4.4, 1994
<21.6 mglkg
05/02/2022
Magnesium
EPA 200.7. Rev. 4.4, 1994
3600 mg/kg
05/02/2022
Molybdenum
EPA 2001. Rev. 4.4,1994
<21.6 mg/kg
05/02/2022
Nickel
EPA 200.7, Rev. 4.4, 1994
<21.6 mg/kg
05/02/2022
Potassium
EPA 200.7, Rev, 4.4, 1994
5160 mg/kg
05/02/2022
Selenium
EPA 200.7, Rev. 4.4, 1994
<21.6 mg/kg
05/02/2022
Sodium
EPA 200.7, Rev. 4.4, 1994
2680 mg/kg
05/02/2022
Zinc
EPA 200.7, Rev. 4.4, 1994
643 mg/kg
05/02/2022
Nitrate+Nitrite-Nitrogen
EPA353,2
10.6mg/kg
04/28/2022
Total Solids (%)
SM 2540 8
2.21 %
04/28/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
1250 mg/kg
04/28/2022
Report #:: 2D22-07642
Page 2 of 5

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc,
6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
inro(ei,environmentulcliemists.com
E=nvirolink, Inc. Date of Report: May 18, 2022
PO Box 670 Customer PO #:
Bailey NC 27807 Customer ID: 16040014
Attention: Stephanie Moore Report #: 2022-07642
Project ID: SBSD-Sludge
Total Kjeidahl Nitrogen (TKN) SM 4500 Norg B-2011 59500 mglkg 04/28/2022
Total Phosphorus SM 4500 P (F-H)-2011 33500 mg/kg 05/03/2022
pH SW 946 Method 9045D 5.81 units 05/03/2022
Result estimated. Analyzed out of 15 minutes hold time.
Mercury
TCLP Metals
SW-646 7471 B
0.805 mglkg 05104/2022
Arsenic
EPA 200.7, Rev, 4.4, 1994
<1.0 mg/L 05/02/2022
Barium
EPA 200.7, Rev 4.4, 1994
<1,0 mg/L 05/02/2022
Cadmium
EPA 200.7, Rev. 4.4, 1994
<1.0 mg1L 05/02/2022
Chromium
EPA 200.7, Rev 4.A, 1994
<1.0 mg/L 05/02/2022
Lead
EPA 2007, Rev. 4.4. 1994
<1.0 mg1L 05/02/2022
Selenium
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L 05/02/2022
Silver
EPA 200.7, Rev 4.4, 1994
<1.0 mg/L 05/02/2022
Mercury
EPA 245.1
<0.0002 mg/L 05/0412022
Lab ID
Sample ID:
Collect Date/Time
Matrix Sampled by
22-16498
Site: # 1
4/2712022 9:00 AM
Solid/Sludge Stephanie Moore
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
2.17 % 04/28/2022
Fecal Density
SM 9221C E-2014
69125 MPN/g 04/27/2022
Lab ID
Sample ID:
Collect DatelTime
Matrix Sampled by
22-18500
Site: # 2
4/27/2022 9.00 AM
Solid/Sludge Stephanie Moore
Test
Method
Results Date Analyzed
Total Solids (%) SM 2540 B 2.25 % 04/28/2022
Fecal Density SM 9221c E-2014 21778 MPN/g 04/27/2022
Report #:: 2022-07642 Page 3 of 5

L Environmental Chemists Inc.
® 6602 Windmill Way, Wilmington, NC 213405 ° 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A, Wilmington Highway, Jacksonville, NC 28540 0 910,347.5843 Lab/Fax
ANALYTICAL 8, CONSULTING CHEMISTS info a,environmentalchemists.com
Envirolink, Inc. Date of Report: May 18, 2022
PO Box 670 Customer PO #;
Bailey NC 27807 Customer ID: 16040014
Attention: Stephanie Moore Report #: 2022-07642
Project ID: SBSD-Sludge
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
22-18501 Site: # 3 4/27/2022 9:00 AM Solid/Sludge Stephanie Moore
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.36 % 04/28/2022
Fecal Density SM 9221C E-2014 33475 MPN/g 04/27/2022
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
22-18502 Site: # 4 4/27/2022 9.00 AM Solid/Sludge Stephanie Moore
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
Lab ID Sample ID:
22-18503 Site: # 5
Test
SM 2540 B 2.06 % 04/28/2022
SM 9221C E-2014 53399 MPN/g 04/27/2022
Collect DatelTime Matrix Sampled by
4/27/2022 9:00 AM Solid/Sludge Stephanie Moore
Method
Results Date Analyzed
Total Solids (%) SM 2540 a 1.99 % 04/28/2022
Fecal Density SM 9221C E-2014 120604 MPNIg 04/27/2022
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
22-18504 Site: # 6 4/27/2022 9:00 AM Solid/Sludge Stephanie Moore
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.07 % 04/28/2022
Fecal Density SM 9221C E-2014 62802 MPNIg 04/27/2022
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
22-18505 Site: # 7 4/27/2022 9:00 AM Solid/Sludge Stephanie Moore
Test Method Results Date Analyzed
Total Solids (%} SM 2540 B 2.02 % 04/28/2022
Fecal Density SM 9221C E-2014 84159 MPNIg 04/27/2022
Report A% 2022-07642 Page 4 of 5

Lenvirochem
ANALYTICAL. & CONSULTING CHEMISTS
Envirolink, Inc.
PO Box 670
Bailey NC 27807
Attention: Stephanie Moore
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 0 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 e 910,347.5843 Lab/Fax
infoCa.envi ronmen talchemists.com
Date of Report: May 18, 2022
Customer PO #:
Customer ID: 16040014
Report #: 2022-07642
Project ID: SBSD-Sludge
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
Reporl #:: 2022-07642 Page 5 of 5

Analytical Environmental Services, Inc Date: 13-May-22
Client: Environmental Chemists, Inc, Client Sample ID: 22-18497
Project Name: 2022-07642 Collection Date: 4/27/2022 9:00:00 AM
Lab ID: 2205020-001 Matrix: Solid
Analyses Reporting Dilution
y Result Limit Qual Units BaYchID Factor DatcAnalyzctl Analyst
Total Organic Carbon in Soil SW9060 (SW9060 Modified)
Total Organic Carbon (TOC) 395000 999 rnence•dry 336037 1 05/12/2022 13:46 GK
Quali l'": Value exceeds moximunt contaminant level C Fstlmnicd (value above quanntanan mnse)
BRL Below reporting limit S Spike Recovery outside limits due to mavrx
H Hold ins limes far preparation or analysis acceded Nasf See erase narmlivc
N Anelym not NELAC cernfied F Analyzed in the lab which is a deviation from the method
B Analyle detected in the assamtcd method blank a Lass than Ruult value
L Cheater Than Result -lue ] Estimated value detacted below Reporting Limit
Page 4 of 7

Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Client: �� -D __ Elnvi -(ok--L Date: L3 2--: 2Z Report Number. 2022-1 (-,a4 �
Receipt of sample:
❑
ECHEM Pickup Client Delivery ❑ Ups ❑ FedEx ❑ Other
YES ❑ NO
N/A PLWere custody seals present on the cooler?
❑ YES ❑ NO
N/A .f custody seals were present, were they intact/unbroken?
Driginal temperature upon receipt a.a_°C Corrected temperature upon receipt
How temperature taken:
❑ Temperature Blank I Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor°C; 0.0
YES ❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES ❑ NO
4. Were proper custody procedures (relinquished/received) followed?
YES ❑ NO
5. Were sample ID's listed on the COC?
YES ❑ NO
6. Were samples ID's listed on sample containers?
YES ❑ NO
7. Were collection date and time listed on the C0C?
YES ❑ NO
8. Were tests to be performed listed on the COC?
YES ❑ NO
9. Did samples arrive in proper containers for each test?
YES ❑ NO
10. Did samples arrive in good condition for each test?
YES ❑ NO
11. Was adequate sample volume available r
YES ❑ NO
12. Were samples received within proper holding time for requested tests?
❑ YES ❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ YES ❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES ❑ NO
15, Were sulfide samples received at a pH >9?
❑ YES ❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? *'
❑ YES ❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES ❑ NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation;
(Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s)
were received incorrectly preserved and were adjusted accordingly
by adding (circle one):
H2SO4 HNO3 HCl NaOH
Time of preservation;
If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s)
were received with head-
spa
"C
DOC. QA.002 Rev 1

Analytical & Consulting Chemists
Client:
ADDRESS:
Sampled B :
Sample Identification
Date
(I
- DECHLORINATION: Samples for
Transfer
'2.
Temperature when Received °C:
Delivered By:
Comments:
ENVIRONMENTAL CHEMISTS, INC OPFICE'n910-392-02 3ilPAX910-392-44245
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
JREPORTTO:
ECT NAME: REPORT NO: ��L4
ACT NAME: PO NO:
PHONE/FAX:
TO: email:
SAMPLE TYPE: I = Influent. E = Effltuenf W = wan RT = c+.., — cr%
d
PRESERVATION
o
W
g
ANALYSIS REQUESTED
o
u
z
o
O
=
Q
z
z==
z
z
+acWi
.�
U,
�-
Q
I LAP
�I �t roc des �clu� is
i. TKN, Cyanide, Phenol and Bacteria must be dechlorinated IQ.5 ppm or less) in the Feld at the time of collection. See reverse for Instructions
relinquished By: DatelTime Received By.- Date/
lz-;� J_�L
61, Rejected: Resample/Regjaested:
give@ By: G�-�-- Date: 11(�-? - Time: ;-- -"0^--
TURNAROUND:

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
FacilityName: Coastal Farms and Residuals, LLC WQ Permit Number: WQ0034806
WWTP Name: Southeast Brunswick Sanitary District WWTP NPDFS Number: WQ0013200
Monitoring Period: From 1/1/2022 To 12/31/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative perfor
Class A: Alt. A (time/temp) ❑ I Alt B (Alk Treatment) ❑ Alt. C (,Prior Testing) ❑
AIt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class' only) indicate "Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ ThennovNlic ❑
Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ :..,..,.,...............
Class B: jAk. (1) FecalDensi
if applicable to alternative performed (Cl.
Lime Stabilization ❑ Air
Anaerobic Di estion
_
If applicable
pp ble to alternative performed
Parameter Allowable Level
in Sludge
2 x 10 to the MPN
6th power
per gram of Fecal Coliform total solids CFIJ
1000 mpn per gram
of total solid (dry
umonctla bacteria 3 MPN.per 4 grams
(in lieu of fecal total solid (dry
Alt. (2) Process to Si t if can
B only) indicate "Process to Sign
ying El Couipostil
ass A or Class B) complete the
Pathogen Density
Geo. MeanlMaximurd Units
s ❑
antly Reduce Pathogens":
❑ 1 Aerobic Digestion
[lowing monitoring data:
um ero Frequency Sample
Excee- of Analysis Type
ed:
u
Tech-
21,778 1 55,945 ! 120,604 1 MPN/g 1 0 1 Annual I Grab lsM922i
Vector Attraction Reduction (HA NCAC.02T .1107) - Please indicate alternative performed:
Alt.] (VS reduction) ❑ Alt. 2 (40-day bench) E1EDJ1 Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 03 uptake) ElAlt. 5 (14-Day Aerobic) ElAlt. 6 (Alk. StabilizatioAlt 7 (Drying - Stable) ❑Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) El Alt. 10 (Incorpotation) I] No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T ,1107 have been met,"
❑ "I certify, tinder penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification Including fine and imprisonment."
Stephanie Moore, ORC Wesley Wooten, President
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) 5/20I22
Signature o reparer* Date Signature of Land A plier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (1212006)

COASTAL FARMS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: November 2, 2022
Summerhouse
0.72 % Solids
7_R3 nN
Permit No. WQ0029945
Parameter
%
Mg/Kg Dry Weight
x 10,000)
Pounds/Dry Ton
(Mg/Kg x 0.0021
Nitrogen (TKN)
6.710
67,100.000
134.200
Phosphorus
3.930
39,300.000
78.600
Potassium
0.736
7,360.000
14.720
PAN (injected)*
2.443
24,427.000
48.854
PAN (surface)*
2.277
22,772.000
45.544
Ammonia Nitrogen
0.331
3,310.000
6.620
Calcium
4.850
48,500.000
97.000
Calcium Carbonate E .
---
---
Magnesium
---
4,040.000
8.080
Sodium
---
18,100,000
36.200
Sulfur
___
---
Nitrate N / Nitrite N
---
1,980,000
3960
Barium
---
_--
-
Chloride
-__
.....
__-
Iron
---
...
---
Aluminum
---
1,880.00
3.760
Arsenic
---
26.80
0.054
Cadmium
---
26.80
0.054
Chromium
---
26.800
---
Copper
---
143.00
0.286
Lead
---
26.80
0.054
Mercury
---
2.51
0.005
Molybdenum
---
26.80
0.054
Nickel
---
26.80
0.054
Selenium
---
26.80
0.054
Zinc
---
2,940.00
5,880
Environmental Chemists # 2022-21867
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N � % PAN
SAR
2.42
Ceiling Concen.
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
75
85
840
57
75
420
100
7.501

COASTAL FARMS & RESIDUALS, LLC
WQ0034806
Summerhouse
11/02/22
13,000
4.1139
11/02/22
6,320
3.8007
11/02/22
12,154
4.0847
11/02/22
12,381
4.0928
11/02/22
10,237
4.0102
11/02/22
4,852
3.6859
11/02/22
6,221
3.7939
Total 1 27.5821
Average 3.9403
Geometric Mean Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 pathogen for Reduction
requirement.

Onslow Water & Sewer Authority
228 Georgetown Road
Jacksonville NC 28540
Attention: Todd Roberts
Environmental Chemists, Inc,
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5943 Lab/Fax
info@env iron mentalchemists.corn
Date of Report: Dec 12, 2022
Customer PO M
Customer ID: 08100092
Report #: 2022-21867
Project ID: Summerhouse
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-53610 Site: Fecal # 1 11/2/2022 8:10 AM Solid/Sludge Kary Herndon
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 1.00 % 11/03/2022
Fecal Density SM 9221C E-2014 13000 MPNIg 11/02/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-53611 Site: Fecal # 2 11/2/2022 8:12 AM Solid/Sludge Kary Herndon
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 1.25 % 11/03/2022
Fecal Density SM 9221 C E-2014 6320 MPNIg 11/02/2022
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
22-53612 Site: Fecal # 3 11/2/2022 8:14 AM Solid/Sludge Kary Herndon
Test Method Results Date Analyzed
Total Solids (%) SM 254o a 0.65 % 11 /03/2022
Fecal Density SM 9221C E-2o14 12154 MPNIg 11/02/2022
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
22-53613 Site: Fecal # 4 11/2/2022 8:16 AM Solid/Sludge Kary Herndon
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
SM 254o a
SM9221C E-2014
1.05 %
12381 MPN/g
11 /03/2022
11/02/2022
Lab ID Sample ID:
Collect DatelTime
Matrix Sampled by
22-53614 Site: Fecal # 5
11/2/2022 8:18 AM
Solid/Sludge Kary Herndon
Test
Method
Results Date
Analyzed
Total Solids (°/a)
SM 2540 B
1.27 %
11 /03/2022
Fecal Density
SM 9221C E-2014
10237 MPN/g
11/02/2022
Reportk: 2022-21867 Page 1 or 3

F77Environmental Chemists, Inc.
1 111 6602 Windmill Way, Wilmington, NC 28405 Y 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
U 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.51343 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infoCenvironmentalchemists.com
Onslow Water & Sewer Authority
Date of Report:
Dec 12, 2022
228 Georgetown Road
Customer PO M
Jacksonville NO 28540
Customer ID:
08100092
Attention: Todd Roberts
Report #:
2022-21867
Project ID: Summerhouse
Lab ID Sample ID:
Collect Date/Time Matrix
Sampled by
22-53615 Site: Fecal # 6
11/212022 8:20 AM Solid/Sludge
Kary Herndon
Test Method Results Date Analyzed
Total Solids (%) SM 2540 a 1.01 % 11103/2022
Fecal Density SM 9221C E-2014 4852 MPNIg 11/02/2022
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
22-53616 Site: Fecal # 7 11/2/2022 8:22 AM Solid/Sludge Kary Herndon
Test Method Results Date Analyzed
Total Solids {%) SM 2540 a 1.27 % 11/03/2022
Fecal Density SM 9221C E•2014 6221 MPNIg 11/0212022
Report #:: 2022-21867 Page 2 of 3

rm+ew _>>
ANALYTICAL & CONSULTING CHEMISTS
Onslow Water & Sewer Authority
228 Georgetown Road
Jacksonville NC 28540
Attention: Todd Roberts
Lab ID Sample ID:
22-53617 Site: Sludge
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 Y 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Dec 12, 2022
Customer PID #:
Customer ID: 08100092
Report #: 2022-21867
Project ID: Summerhouse
Collect Date/Time Matrix Sampled by
11/2/2022 8:27 AM Solid/Sludge Kary Herndon
Test
Method
Results
Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4, 1994
1880 mg/kg
11/16/2022
Arsenic
EPA 200.7, Rev. 4.4, 1994
<26.8 mg/kg
11/16/2022
Cadmium
EPA 200.7, Rev. 4.4.1994
<26.8 mg/kg
11/16/2022
Calcium
EPA 200.7, Rev. 4.4,1994
48500 mg/kg
11/16/2022
Chromium
EPA 200.7. Rev. 4.4, 1994
<26.8 mg/kg
11/16/2022
Copper
EPA 200.7, Rev, 4.4, 1994
143 mg/kg
11/16/2022
Lead
EPA 200.7, Rev. 4.4, 1994
<26.8 mg/kg
11/16/2022
Magnesium
EPA 200.7. Rev. 4.4, 1994
4040 mg/kg
11/16/2022
Molybdenum
EPA 200.7, Rev. 4.4. 1994
<26.8 mg/kg
11/16/2022
Nickel
EPA 200.7, Rev. 4.4, 1994
<26.Bmg/kg
1111612022
Potassium
EPA 200.7, Rev. 4.4, 1994
7360 mg/kg
11116/2022
Selenium
EPA 200.7, Rev. 4,4, 1994
<26.8 mg/kg
11/16/2022
Sodium
EPA 200.7, Rev. 4.4, 1994
18100 mg/kg
12/06/2022
Zinc
EPA 200.7, Rev_ 4.4, 1994
2940 mg/kg
11/16/2022
N itrate+N itrite- Nitrogen
EPA353.2
1980mg/kg
11/04/2022
Total Solids (%)
SM 2540 8
0.72 %
11/03/2022
Ammonia Nitrogen
SM 4500 NH3 C-2ot1
3310 mg/kg
11/03/2022
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg a-2011
67100 mglkg
11/03/2022
Total Phosphorus
SM 4500 P (F-H)-2011
39300 mg/kg
11/11/2022
pH
SW 846 Method 9045D
7.83 units
11/14/2022
Result estimated. Analyzed out of
15 minutes hold time.
Mercury SW-846 7471 a <2.51 mg/kg 11/14/2022
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
11
Report #F: 2022-21867 — Page 3 of 3

Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Client: Date: f 2 122- Report Number; _ 2022- 7
Receipt of sample:
E HEM Pickup , Client Delivery ❑
I UPS ❑ FedEx ❑ Other ❑
© YES
❑
NO
N/A 1. Were custody seals present on the cooler?
❑ YES
❑
NO
N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt
How temperature taken:
❑ Temperature Blank Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
YES
❑
NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
❑
NO
4. Were proper custody procedures (relinquished/received) followed?
YES
❑
NO
5. Were sample ID's listed on the COC?
YES
❑
NO
6. Were samples ID's listed on sample containers?
YES
❑
NO
7. Were collection date and time listed on the COC?
YES
❑
NO
8. Were tests to be performed listed on the COC?
YES
❑
NO
9. Did samples arrive in proper containers for each test?
YES
❑
NO
10. Did samples arrive in good condition for each test?
YES
❑
NO
11. Was adequate sample volume available?'
YES
❑
NO
12. Were samples received within proper holding time for requested tests?
❑ YES
❑
NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑
NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑
NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑
NO
16_ Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES
❑
NO
17. Were Sulfide/Cyanide received at a chlorine residual of <05
❑ YES
❑
NO 118.
m/L?
Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pX checked at time of analysis and recorded on the benchsheet.
�* Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2504 HNO., HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS;
DOC. QA.002 Rev 1
°C

Analytical 8 Consulting Chemists
CLIENT: ONWASA-Summer House WRF
ADDRESS 228 Georgetown Road
Jacksonville, NC 28540
ampled By:.M-*s.r
Sample Identification
Q224505-02 Fecal # 9
Q224505-03 Fecal # 2
0224505-04 Fecal # 3
Q224505-05 Fecal # 4
Q224505-06 Fecal # 5
0224505-07 Fecal # 6
Q224505-08 Fecal # 7
Q224505-01SH Digestor
Transfer
1.
2.
Temperature It
Delivered By:,
Comments:
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
PROJECT NAME: ONWASA Summer House Solids
CONTACT NAME: Kary Herndon ([e-mail]
REPORT TO: Kary Herndon
COPY TO: ONWASA Laboratory
nernaon
Collection
Date I Time
11/2/2022 8:10
11/2/2022
8:12
11/2/2022
8:14
11/2/2022
8=16
11/2/2022
8:18
11/2/2022
8:20
11 /212022
8:22
11/2/2022
8:27
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
i nfo@e nviron mentalc hem is Is. corn
REPORT NO:
PO NO:
PHONE/FAX:
2-2 - Z1S'1'�+
SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO Soil, SL = Sludge, Other:
m m
a'
„ F
u a
`o
c l7
:° `p
C
`o rn
Q W
m m
g
PRESERVATION
ANALYSIS REQUESTED
W
z
1
0
0
x
o
w
Temp
A
�a
"E
gz
x
_
z
a
18
SL
C
3bl
x
Fecal Density
�
18
SL
C
?)
x
Fecal Density
G
18
C
P
�?,V,12-
X
Density
G
GFecal
18
SL
�3bI
x
Fecal Density
G
G
18
SL
C
x
Fecal Density
G
Gbi�
18
SL
C
`
x
Fecal Density
G
G
18
SL
C 1
P
G
�
x
Fecal Density
18
SL
�JIQ
x
Residuals
10
G
C
P
G
G
C
P
G
G
quished
t;
Accepted:
n
By:
Datefrime
Daterrime
'ample Requested:
Date: 1 1 -2�L Time: Q
TURNAROUND:

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Coastal Farms and Residuals, LLC WQ Permit Number: WQ0034806
WWTP Name: Summerhouse WWTP NPDES Number: WQ0029945
Monitoring Period: From 1/1/2022 To 12/31/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A: Alt. A (tire/temp) ❑ 1 Alt B (Alk Treatment) ❑ I Alt. C (Prior Testing) ❑
AIt.D (No Prior Test) ❑ Process to Furtlier Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑
Beta Ray ❑ Gamin Ray ❑ Pasteurization ❑
Class B: Alt. (1) Fecal Density El I Alt. (2) Process to Significantly Reduce Patliogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion Cl
Ana
erobic Di esti 017 ❑
If applicable to alternative performed (Class A or Class B) complete the following 'monitoring data:
Allowable Level Pathogen Density Number ot Frequency Sample na ytica
Parameter in Sludge Excee- of Anal y —docesType Tech-
2 x 10 to the
6th power MPN 4,852 8,716 13,000 MPN/g 0 Annual Grab SM922LCE
per gram of
Fecal Coliform total solids CFU
1000 mpn per gram
of total solid (dry
wei ht)
Salmonel[a bacteria 3 MPN per 4 grams
(in lieu of fecal total solid (dry
coliform) I weight)
Vector Attraction Reduction (15A NCAC 02T .1107) -Please indicate alternative performed:
Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑_I Alt. 4 (Spec. O, uptake) ❑
Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying -Stable) ❑ 1 Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) p Alt. 10 (Incorporation) p No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kary Herndon, ORC Wesley Wooten, President
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
�112/20/22 12/16/22
Signature of Pt`e rer* Date Signature of Lan Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26)
DEN FORM PVRF 02T (12/2006)

COASTAL RESIDUALS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: November 7, 2022
Surf City WWTP
1.74 % Solids
7.43 pH
Permit No. WQ0000795
Parameter
%
Mg/Kg Dry Weight
{% x 10,000}
Pounds/Dry Ton
M /K x 0.002}
Nitrogen (TKN)
6.740
67,400.000
134.800
Phosphorus
2.260
22,600.000
45.200
Potassium
0.440
4,400.000
8.800
PAN (injected)*
2.129
21,289.000
42.578
PAN (surface)*
2.066
20,664.000
41.328
Ammonia Nitrogen
0.125
1,250.000
2.500
Calcium
4.440
44,400.000
88.800
Calcium Carbonate E .
---
---
Magnesium
---
4,470.000
8.940
Sodium
---
16,300.000
32.600
Sulfur
---
---
---
Nitrate N / Nitrite N
---
194.000
0.388
Barium
--
---
.__
SAR
2.60
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
IK )
Aluminum
---
4,190.00
8.380(M
Arsenic
---
19.80
0.040
75
Cadmium
---
19.60
0.039
85
Chromium
---
19.600
0.039
—
Copper
---
420.00
0.840
4,300
Lead
---
19.60
0.039
840
Mercury
---
1.100
0.002
57
Molybdenum
---
19.60
0.039
75
Nickel
---
19.60
0.039
420
Selenium
---
19.60
0.039
100
Zinc
---
4,200.00
8.400
7,500
Environmental Cheinists # 2022-22123
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

LEWIS FARMS
WQ0000455
Surf City WWTP
..... g..........:...::.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.
11/07/22
12,207
4.0866
11/07/22
21,974
4.3419
11/07/22
12,265
4.0887
11/07/22
15,208
4.1821
11/07/22
15,137
4.1800
11/07/22
3,727
3.5714
11/07/22
11,941
4.0770
Total 1 28.5277
Average 4.0754
Geometric Mean I X f 1 Fecal Coliform MPN 1 gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction
requirement.

M-Fe
Environmental. Chemists,
Inc.
V !
6602 Windmill Way,
Wilmington, NC 28405 6 910.392.0223 Lab ° 910.392.4424
Fax
I.. ±t t -
tt
710 Bowsertown
Road, Manteo, NC 27954 ` 252.473.5702 Lab/Fax
`
255-A Wilmington Highway, Jacksonville, NC 28540 910.347.5843 Lab/Fax
ANALYTICAL& CONSULTING CHEMISTS
int'orenvironmentalchemists.com
Town of Surf City
Date of Report: Dec 13, 2022
Post Office Box 2475
Customer PO #•
Surf City NC 28445
Customer ID. 08110024
Attention:
Report #: 2022-22123
Project ID: Sludge
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
22-54265 Site: Sludge
11/7/2022
11:50 AM Solid/Sludge Mike Hash
Test
Method
Results Date Analyzed
Chlordane (TCLP)
SW-8468081 B
<0.02mg1L
11/09/2022
Endrin (TCLP)
SW-846 60B1 8
<0.0005 mg/L
11/09/2022
Heptachlor (TCLP)
SW-8468081 B
<0.0005 mg/L
11/09/2022
Heptachlor epoxide (TCLP)
SW-846 e081 B
<0.0005 mg/L
11/09/2022
Llndane (TCLP)
SW-84680a1 B
<0-0005mg/L
11/09/2022
Methoxychlor (TCLP)
SW-8468081 B
<0.0005mg/L
11/09/2022
Toxaphene (TCLP)
SW-846 8081 B
<0-05 mg/L
11/09/2022
2,4,5-TP (TCLP)
SW-846 8151 A
<0.003 mg/L
11/09/2022
2,4-D (TCLP)
SW-846 0151 A
<0.003 mg/L
11/09/2022
1,4-Dichlorobenzene (TCLP)
SW-845 8270 E_
<0.050 mg/L
11/22/2022
2,4,5-Trichlorophenol(TCLP)
SW-6468270E
<0.050mg/L
11/22/2022
2,4,6-Trichlorophenol (TCLP)
SW-8468270 E
<0.050 mg/L
11/22/2022
2,4-Dinitroto[uene (TCLP)
SW-846 8270 E
<0.050 mg/L
11/22/2022
Cresol (TCLP)
SW-B46 8270 E
<0.050 mg/L
11/22/2022
Hexachloro-1,3-butadiene (TCLP)
SW-8468270E
<0.050mg/L
11/22/2022
Hexachiorobenzene (TCLP)
SW-846 6270 E
<0.050 mg/L
11/22/2022
Hexachloroethane (TCLP)
SW-846 8270 E
<0.050 mg/L
11/22/2022
m + p-Cresol (TCLP)
SW-646 8270 E
<0,050 mg/L
11/22/2022
Nitrobenzene (TCLP)
SW-8468270E
<0.050mg/L
11/22/2022
o-Cresal (TCLP)
SW-846 0270 E
<0.050 mg/L
11/22/2022
Pentachloropheno[ (TCLP)
SW-646 8270 E
<0.250 mglL
11/22/2022
Pyridine (TCLP)
SW-B46 0270 E
<0.050 mg/L
11/22/2022
1, 1 -Dichloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
11/18/2022
1,2-Dichloroethane (TCLP)
SW-846 Method 8260D
<0.01 mg/L
11/18/2022
Benzene (TCLP)
SW-846 Method 0260D
<0.01 mg/L
11/18/2022
Carbon Tetrachloride (TCLP)
SW-e46 Method 8260D
<0.01 mg/L
11/18/2022
Report #:: 2022-22123
Page 1 of 4

pqm
In �'
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ° 910.392.4424 Fax
710 Bowsertown Road, Man teo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
[e-mail]
Town of Surf City
Date of Report: Dec 13, 2022
Post Office Box 2475
Customer PO #:
Surf City NC 28445
Customer ID: 08110024
Attention:
Report #: 2022-22123
Project ID: Sludge
Chlorobenzene (TCLP)
SW-846 Method8260D <0.01 mg/L
11/18/2022
Chloroform (TCLP)
SW-846 Method 8260D <0.01 mg/L
11/18/2022
Methyl ethyl ketone (TCLP)
SW-846 Method 8260D <0.05 mg/L
11/18/2022
Tetrachloroethylene (TCLP)
SW-846 Method 8260D <0.01 mg/L
11/18/2022
Trichioroethylene (TCLP)
SW-845 Method 8260D <0.01 mg/L
11/18/2022
Vinyl Chloride (TCLP)
SW-846 Method 8260D <0.01 mg/L
11/18/2022
RCI
Cyanide
SM 4500 CM D-2016
<1.0 mg/kg
11 /1812022
Sulfide
SM 4500 s D
0.18 mg/kg
11/2B/2022
Ignitability
sw 846 method loin
>157'F
12/13/2022
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4, 1994
4190mg/kg
11/16/2022
Arsenic
EPA 200.7, Rev, 4.4, 1994
19.8 mg/kg
11/16/2022
Cadmium
EPA 200.7,Rev. 44,1994
<19.6mg/kg
11/16/2022
Calcium
EPA 200.7, Rev. 4.4, 1994
44400 mg/kg
11/16/2022
Chromium
EPA 200.7. Rev. 4.4, 1994
<19.6 mg/kg
11/16/2022
Copper
EPA 200.7, Rev. 4.4, 1994
420 mg/kg
11/16/2022
Lead
EPA 200.7, Rev. 4.4, 1994
<19.6 mg/kg
11/16/2022
Magnesium
EPA 200.7, Rev. 4.4. 1994
4470 mg/kg
11/16/2022
Molybdenum
EPA 200.7, Rev. 4.4. 1994
<19.6 mg/kg
11116/2022
Nickel
EPA 200.7, Rev. 4.4, 1994
<19.6 mg/kg
11/1612022
Potassium
EPA 200.7. Rev. 4.4. 1994
4400 mg/kg
11/16/2022
Selenium
EPA 200.7, Rev. 4.4, 1994
<19.6 mg/kg
11/16/2022
Sodium
EPA 200.7, Rev. 4.4, 1994
16300 mg/kg
12/08/2022
Zinc
EPA 200.7, Rev. 4.4, 1994
4200 mg/kg
11/16/2022
Nitrate+Nitrite-Nitrogen
EPA353.2
194mg/kg
11/08/2022
Total Solids (%)
SM 2540 8
1.74 %
11/08/2022
Ammonia Nitrogen
SM 4500 NH3 C-20i1
1250 mg/kg
11 /08/2022
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg 6.2011
67400 mg/kg
11/08/2022
Total Phosphorus
SM4500P(F-H)-2011
22600mg/kg
11/21/2022
Report #:: 2022-22123
Page 2 of 4

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ° 252.473,5702 Lab/Fax
t 5� 255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info( environmentalchemists.corn
Town of Surf City Date of Report: Dec 13, 2022
Post Office Box 2475 Customer PO #:
Surf City NC 28445 Customer ID: 08110024
Attention: Report #: 2022-22123
Project ID: Sludge
pH SW 646 Method 9045D 7.43 units 11/14/2022
Result estimated. Analyzed out of 15 minutes hold time.
Mercury
SW-8467471 B
<1.10 mg/kg
11114/2022
TCLP Metals
Arsenic (TCLP)
EPA 200.7, Rev, 4.4. 1994
<1.0 mg/L
11/14/2022
Barium
EPA 200.7, Rev, 4.4, 1994
<1.0
11/14/2022
Cadmium
EPA 200.7, Rev. 4.4, 1994
<1.0
11/14/2022
Chromium
EPA 200.7, Rev, 4A, 1994
<1.0
11/14/2022
Lead (TCLP)
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
11 /14/2022
Selenium
EPA 200.7, Rev. 4.4. 1994
<1.0
11/14/2022
Silver
EPA 200.7, Rev. 4.4, 1994
<1.0
11/14/2022
Mercury
EPA 245A
<0.0002
11/14/2022
Lab ID Sample ID:
Collect DatelTime
Matrix Sampled by
22-54266 Site: Sludge 1
11/7/2022 11:50 AM
Solid/Sludge Mike Hash
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
2-13 %
11/08/2022
Fecal Density
SM 9221C E-2014
12207 MPN/g
11/07/2022
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
22-54267 Site: Sludge 2
11/7/2022 11:50 AM
Solid/Sludge Mike Hash
Test
Method
Results
Date Analyzed
Total Solids (%)
SM 2540 B
2.23 %
11/08/2022
Fecal Density
SM 9221C E-2014
21974 MPN/g
11/07/2022
Lab ID Sample ID:
Collect Date[Time
Matrix Sampled by
22-54268 Site: Sludge 3
11/7/2022 11:50 AM
Solid/Sludge Mike Hash
Test
Method
Results
Date Analyzed
Total Solids (%)
SM 2540 B
2,12 %
1110812022
Fecal Density
SM 9221C E-2014
12265 MPNIg
11/07/2022
Report #:: 2022.22123
Page 3 of 4

Lenvrochem :}
ANALYTICAL & CONSULTING CHEMISTS
Town of Surf City
Post Office Box 2475
Surf City NC
Attention:
Lab ID Sample ID;
22-54269 Site: Sludge 4
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
22-54270 Site: Sludge 5
Test
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ' 910,392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lair/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Dec 13, 2022
Customer PO #:
28445 Customer ID: 08110024
Report #: 2022-22123
Project ID: Sludge
Collect DatelTime Matrix Sampled by
11/7/2022 11:50 AM Solid/Sludge Mike Hash
Method Results Date Analyzed
SM 2540 B
SM 9221C E•2014
2.17 % 11/08/2022
15208 MPN/g 11/07/2022
Collect DatelTime Matrix Sampled by
11/7/2022 11:50 AM Solid/Sludge Mike Hash
Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.18 % 11/08/2022
Fecal Density SM 9221C E-2014 15137 MPNIg 11/07/2022
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
22-54271 Site: Sludge 6 11/7/2022 11:60 AM Solid/Sludge Mike Hash
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
Lab ID Sample ID:
22-54272 Site: Sludge 7
Test
SM 2540 B
SM 9221 C E-2014
2.12 % 11/08/2022
3727 MPN/g 11 /07/2022
Collect DatelTime Matrix Sampled by
11/7/2022 11:50 AM Solid/Sludge Mike Hash
Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.01 % 11/08/2022
Fecal Density SM92210E-2014 11941 MPNIg 11/07/2022
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: u'L
Report #:: 2022-22123 Page 4 of 4

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client SL.(11— �lA Date: Report Number: _ 2022- ol—a
Receipt of sample:
ECHEM Pickup Client Delivery ❑
UPS ❑ FedEx ❑ Other ❑
❑
YES
❑
NO
Ig N/A
I. Were custody seals present on the cooler?
❑
YES
❑
NO
N/A
2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt "C Corrected temperature upon receipt
How temperature taken:
❑ Temperature Blank Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 iR Gun Correction Factor °C: 0.0
YES
❑
NO
3. If temperature of cooler exceeded 6"C, was Project Mgr./CIA notified?
YES
❑
NO
4. Were proper custody procedures (relinquished/received) followed?
L9
YES
❑
NO
5. Were sample ID's listed on the COC?
YES
❑
NO
6. Were samples ID's listed on sample containers?
[4
YES
I ❑
NO
7. Were collection date and time listed on the COC?
iSl
YES
❑
NO
8. Were tests to be performed listed on the COC?
[
YES
❑
NO
9. Did samples arrive in proper containers for each test?
YES
ElNO
10. Did samples arrive in good condition for each test?
[�
YES
❑
NO
Ill. Was adequate sample volume availableT
EY
YES
❑
NO
12. Were samples received within proper holding time for requested tests?
❑
YES
❑
NO
13. Were acid preserved samples received at a pH of <2?
❑
YES
❑
NO
14. Were cyanide samples received at a pH >12?
❑
YES
❑
NO
15. Were sulfide samples received at a pH >9?
❑
YES
❑
NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? i
❑
YES
❑
NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑
YES
❑
NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the bench -sheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2504 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediatelyfor incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. 4A.002 Rev 1
°C

6602 Windmill Way , NC
ENVIRONMENTAL CHEMISTS, INC OFFICE: 910-392-0231IFAX 910392-4245
Analytical & Consulting Chemists NCDENR: DWa CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: Town of Surf City WWTP PROJECT NAME: Sludge analysis REPORT NO:
ADDRESS: CONTACT NAME: PO NO:
REPORT TO: PHONE/FAX:
COPY TO: Lewis Farms/Martin Mahe email:
Sampled By:— SAMPLE TYPE• I = I fl t E = ="I
Sample. •
•
'•ii11l�s'1�il�J-
�rl
rMR
��
MW
Transfer
1.
2.
Temperature when
Delivered By;.- �
Comments: �-
a
as
E >,
~
o
n a E
C3
a _
cC?
:° o
O Q
CS
n
c J
`o rn
s:
uen ,
O W
m
z
uent,
PRESERVATION
Yv
= Well,
a =
Stream,
SO = Soil, SL = Sludge, Other:
ANALYSIS REQUESTED
w
O
z
U
=
o'
w
=
z
s
r
¢
z
o
s
r
x
O
C
X
Nutrients / Metals / Full TCLP / RCI
G
II
�7
(Z
��7.��
IN Z'D
yZ7
I
x
x
x
x
x
x
x
fecal density/%TS
fecal density/%TS
fecal density/%TS
fecal density/%TS
01
C
Gcb
P
c
G
c
P
C
G
o
fecal density/ /oTS
fecal density/%TS
fecal density/%TS
c
G
G
C-13C
C
G
P
G
G
pted:
_Received By:
Date/Time
Resamp a equested: ti
Date:' I Time:
TURNAROUND:

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Coastal Farms and Residuals, LLC WQ Permit Number: WQ0034806
WWTP Name: Surf City WWTP NPDES Number• WQ0000795
Monitoring Period: From 1/1/2022 To 12/31/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative perfor
Class A: Alt. A (time/temp) I Alt B (AIk Treatment) ❑ Alt_ C (Prior Testing) ❑
AIt.D (No Prior Test) ❑I Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01 Heat Drying ❑ Heat Treatment ❑ TliennopluIic ❑
Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑
Class B: Alt. (1) Fecal Density
If applicable to alternative performed (Clas
Lime Stabilization ❑ Air I
Anaerobic Digestion ❑ _
If applicable to alternative performed (C
Parameter Allowable Level
in Sludge Minimu
2 x 10 to the MPN 3,727
6th power
per gram of
Fecal Coliform total solids CFU
1000 mpn per gram
oftotal solid (dry
ilmonella bacteria 3 MPN per 4 grams
(in lieu offecal total solid (dry
Alt. (2) Process to Siguifican
B only) indicate "Process to Sign
yija ❑ Com ostil
ass A or Class B) c . omblete the
Geo. MeanlMaximun� Units
Reduce Pathogens [:] I—
antly Reduce Pathogens":
❑ Aerobic Digestion ❑
monitori
denceeV+l Frequency I Sample I "1 ,,h-
Irxcee- I Teeh-
of Analysis Type
nirt��a
11,896 1 21,974 1 MPN/g 1 0 1 Annual I Grab 15M9221
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt. I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ JAIL 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) El Alt. l0 (Incorporation) p No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Zachary Butler, ORC Wesley Wooten, President
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
(tl/. 12/15/22 ,�. 12115/22
Sign re of Pre rer* Date Signature of Lan Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (1212006)

COASTAL FARMS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: September 7, 2022
Swansboro
1.94 % Solids
6.77 pH
Permit No. WQ0034806
Parameter
%
�Mg/KgDryWeighj
(% x 10,000)
Pounds/DryTon
(MgtKg x 0.002)
Nitrogen (TKN)
3.620
36,200.000
72.400
Phosphorus
1.590
15,900.000
31.800
Potassium
0.305
3,050.000
6.100
PAN (injected)*
2.046
20,464,400
40.929
PAN (surface)*
2.007
20,068.400
40.137
Ammonia Nitrogen
0.079
792.000
1.584
Calcium
3.080
30,800.000
61.600
Calcium Carbonate E .
---
---
---
Magnesium
---
1,830.000
3.660
Sodium
---
5,820.000
11.640
Sulfur
---
---
Nitrate N / Nitrite N
---
9,050.000
18.100
Barium
Chloride
---
---
---
---
---
---
SAR
2.96
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
2,590.00
5.180
Arsenic
---
16.50
0.033
75
Cadmium
---
16.50
0.033
85
Chromium
---
16.500
---
---
Copper
---
281.00
0.562
4,300
Lead
---
16.50
0.033
840
Mercury
---
0.985
0.002
57
Molybdenum
---
16.50
0.033
75
Nickel
---
16.50
0.033
420
Selenium
---
16.50
0.033
100
Zinc
---
3,670.00
7.340
7,500
Environmental Chemists # 2022-17562
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

COASTAL FARMS AND RESIDUALS, LLC
WQ0034806
Swansboro WRF
09/07/22
544,379
5.7359
09/07/22
554,217
5.7437
09/07/22
560,976
5.7489
09/07/22
296,704
5.4723
09/07/22
193,371
5.2864
09/07/22
218,750
1 5.3399
09/07/22
3 23,3 54 1
5.5097
Total 1 38.8369
Average 5.5481
Geometric Mean 'N3 3 4 Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction
requirement.

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 e 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info@cnvi ronmen to Icllem is ts, coni
Onslow Water & Sewer Authority Date of Report: Sep 22, 2022
228 Georgetown Road Customer PO #:
Jacksonville NC 28540 Customer ID: 08100092
Attention: Mark Young Report #: 2022-17562
Project 1D: Swansboro WRF
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
22-43084 Site: Sludge 9/7/2022 8.01 AM Solid/Sludge Samantha Howard
Test
Method
Results
Date Analyzed
Sludge Residuals
Aluminum
EPA 2003, Rev. 4.4, 1994
2590 mg/kg
09/17/2022
Cadmium
EPA 200.7, Rev. 4.4, 1994
<16.5 mg/kg
09/17/2022
Calcium
EPA 200.7, Rev. 4.4, 1994
30800 mg/kg
09/17/2022
Chromium
EPA200,7, Rev. 4.4, 1994
<16.5 mg/kg
09/17/2022
Copper
EPA 200.7, Rev. 4.4, 1994
281 mg/kg
09/17/2022
Lead
EPA 200.7, Rev. 4.4. 1904
<16.5 mg/kg
09/17/2022
Magnesium
EPA 200.7, Rev. 4.4, 1994
1830 mg/kg
09/17/2022
Molybdenum
EPA 200.7, Rev. 4.4, 1994
<16.5 mg/kg
09/17/2022
Nickel
EPA 200.7, Rev. 4.4, 1994
<16.5 mg/kg
09/17/2022
Potassium
EPA 200.7, Rev. 4.4, 1994
3050 mg/kg
09/17/2022
Selenium
EPA 200.7. Rev. 4.4, 1994
<16.5mg/kg
09/17/2022
Sodium
EPA 200.7, Rev. 4.4, 1994
5820 mglkg
09/17/2022
Zinc
EPA 200.7, Rev. 4.4, 1994
3670 mg/kg
09/17/2022
Arsenic
EPA 2oo.9, Rev. 5.4, 1994
<16.5 mg/kg
09/20/2022
Nitrate+Nitrite-Nitrogen
EPA 353,2
9050 mg/kg
09/12/2022
Total Solids N
SM 2540 s
1.94 %
09/08/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
792 mg/kg
09/08/2022
Total Kjeldahl Nitrogen (TKN)
SM 450o Norg 8-2011
36200 mg/kg
09/09/2022
Total Phosphorus
SM 4500 P (F-H)-2011
15900 mg/kg
09/14/2022
PH
SW 646 Method 9045D
6.77 units
09/12/2022
Mercury
SW646 7471 6
<0.985 mg/kg
09/17/2022
Report #:: 2022-17562 Page 1 of 3

Environmental Chemists, Inc.
A 6602 Windmill Way, Wilmington, NC 28405 " 910.392.0223 Lab a 910.392.4424 Fax
710 $owsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
sa+ 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5643 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Onslow Water & Sewer Authority
Date of Report: Sep 22, 2022
228 Georgetown Road
Customer PO #:
Jacksonville NC 28540
Customer ID: 08100092
Attention: Mark Young
Report #: 2022-17562
Project ID: Swansboro WRF
Lab ID Sample ID:
Collect DatefTime Matrix Sampled by
22-43085 SIte: Sludge 1
9/7/2022 7:47 AM Solid/Sludge Samantha Howard
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 8 1,69 % 09/08/2022
Fecal Density
SM 13221C E-2014 544379 MPN/g 09/07/2022
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
22-43094 Site: Sludge 2
9/7/2022 7:49 AM Solid/Sludge Samantha Howard
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 a 1.66 % 09/08/2022
Fecal Density
SM 9221C E-2014 554217 MPN/g 09/07/2022
Lab ID Sample ID:
Collect DatetTime Matrix Sampled by
22-43095 Site: Sludge 3
9/7/2022 7:51 AM Solid/Sludge Samantha Howard
Test
Method Results Date Analyzed
Total Solids (%) SM 2540 B 1.64 % 09/08/2022
Fecal Density SM 9221C E-2014 560976 MPNIg 09/07/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-43096 Site: Sludge 4 9/7/2022 7:53 AM Solid/Sludge Samantha Howard
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
Lab ID Sample ID:
22-43097 Site: Sludge 5
Test
SM 2540 B
SM 9221C E-2014
Method
Collect Daterrime
9/7/2022 7:55 AM
1.82 % 09/08/2022
296704 MPNIg 09/07/2022
Matrix Sampled by
Solid/Sludge Samantha Howard
Results Date Analyzed
Total Solids (%) SM 2$40 B 1.81 % 09/08/2022
Fecal Density SM 9221C E-2014 193371 MPNIg 09/07/2022
Report #;; 2022.17562 Page 2 of 3

Environmental Chemists, Inc.
1 R i 1 6602 Windmill Way, Wilmington, NC 28405 • 910,392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fix
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Onslow Water & Sewer Authority
Date of Report: Sep 22, 2022
228 Georgetown Road
Customer PO #:
Jacksonville NC 28540
Customer ID: 08100092
Attention: Mark Young
Report M 2022-17562
Project 1D: Swansboro WRF
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-43098 Site: Sludge 6
9/7/2022 7:57 AM Solid/Sludge Samantha Howard
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 a 1.60 % 09/08/2022
Fecal Density
SM 9221C E-2414 218750 MPN/g 09/07/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-43099 Site: Sludge 7
9/712022 7:59 AM Solid/Sludge Samantha Howard
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 1.67 % 09/08/2022
Fecal Density
SM 4221C E-2014 323354 MPNIg 09/07/2022
Comment: Sludge residuals, except pH, reported on a dry weight basis, pH reported on an as received basis.
r
Reviewed by:
l'
Report # : 2022.17562 Page 3 of 3

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmilf Way
Wilmington, NC 28405
910.392.0223
��}} ! Y Sample Receipt Checklist
Uf�[ Client: �>'`IA6A Date: 9 a Report Number._2022- 75
Receipt of sample:
❑
ECHEM Pickup Client Delivery ❑ 11P5 ❑ FedE>; ❑ Other ❑
YES
❑
NO
IX N/A 1. Were custody seals present on the cooler?
❑
YES
❑
NO
N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt
-----------------
How temperature taken:
❑ Temperature Blank f Against Bottles
1R Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C. 0.0
f
YES
❑
NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
❑
NO
4. Were proper custody procedures (relinquished/received) followed?
CO
YES
❑
NO
S. Were sample Us listed on the COV
!�
YES
❑
NO
6. Were samples ID's listed on sample containers?
YES
❑
NO
7. Were collection date and time fisted on the COC?
I�
YES
❑
NO
8. Were tests to be performed listed on the COC?
f
YES
LLU
NO
1 9_ Did samples arrive in proper containers for each test?
�l
YES
❑
NO
10. Did samples arrive in good condition for each test?
f�
YES
❑
NO
11. Was adequate sample volume availableT
f
YES
❑
NO
12. Were samples received within proper holding time for requested tests?
❑
YES
❑
NO
13. Were acid preserved samples received at a pH of <2?
❑
YES
❑
NO
14. Were cyanide samples received at a pH >12?
❑
YES
❑
NO
15. Were sulfide samples received at a pH >9?
❑
YES
❑
NO
16. Were NH3/TI<N/Phenol received at a chlorine residual of <0.5 m/L?' -
❑
YES
❑
NO
17. Were Sulfide/Cyanide received at a chlorine residual
❑
YES
❑
NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. who was notified, date and time:
Volatiles Samples) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1
°C

6602 Way
ton
ENVIRONMENTAL CHEMISTS, INC OFFICE: 01392-02 311FAX[phone]
Analytical & Consulting Chemists NCDENR: DWq CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 Info@envlronmentalchemists_com
C:C)1 I FrTION am In r I-IAIAI nC f'I Ierrwiv
Client: Onslow Water & Sewer Authority ONWASA
PROJECT NAME: Swansboro WRF
REPORT NO:
ADDRESS: 228 Georgetown Rd
CONTACT NAME: Mark Young
PO NO:
Jacksonville, NC 28540
REPORT TO: [e-mail]
COPY TO: Martin WILLCOXMABESOIL.COM
PHONEIFAX: 910-545.6877
email: m oun onwasa.com
Sampled Oy:,��.
Sample Identification
n
7w
r- Fecal 1
r- Fecal 2
r- Fecal 3
r- Fecal 4
r- Fecal 5
r- Fecal 6
r- Fecal 7
Transfer
1.
2.
Temperature
Delivered By:
Comments:
SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Collection m PRESERVATION
a m c a c Vim' c J a w
w o° ° �' m i a o o AliALY5ES REQUESTED
s E g o u �n x e z s
Date
9/7/2022
Time
;Q3•
Tem
D
SL
U"
Cp
2
X
2
=
x
~
o
Annual Sludge Analysis 1 Nutrient &
Q
G
9/7/2022
v
" G
D
a�
0
SL
SL
SL
C
,
` Id
X
X
X
Fecal Densi
Fecal Density
Fecal Density
9/7/2022
C
G
9/7/2022
'
©
C
G
ODD
9/7/2022
07:
0
C
G
OP
9/7/2022
Q 5
3a'
�
31. 1 C
o�
3 a' 5
SL
5L
5L
SL
C
G
V30
` 309
(� C
73 1e
(�
V3 � -!
`
4
X
X
X
X
I
Fecal De
Fecal De
Fecal De
Fecal De
917/2 222
p*57k.�o
G0
C
G
9/7/2022
Q
0
C
G
P
©
G
Daterrime I 0.AbCeiivAdBy:-- D terrime
cf 'T a --J- 0 `::�
a
d: jected: Resample17 qu sted:
Received By: Date: Time:
TURN OUND:

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Coastal Farms and Residuals, LLC WQ Permit Number: WQ0034806
WWTP Name: Swansboro W WTP NPDES Number: WQ0023261
Monitoring Period: From 1/1/2022 To 12/31/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
A (tine/temp) El Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑
+Alt.
lt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens" -
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thennophilic ❑
Beta Rayntna
❑
GatRay ElPasteurization
El
Class B!
AIt. (1) Fecal Don sity El
I Alt. (2) Process to Sign ifi cmi t!Reduce Patlio ens ❑
If applicable to alternative performed (Class I3 only) indicate "Process to Significant$• Reduce Pathogens":
Lime Stabilization ❑ Air Di ing ❑ Com ostin ❑ Aerobic Digestion ❑
Anaerobic Digestion ❑ >::�:=:°•':
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g y
n
Excee-
dencesof
Frequency
Analysis
Sample
Type
na yuca
Tech -
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
Gth power
per gram of
total solids
MPN
193,371
353,284
560,976
MPN/g
0
Annual
Grab
SM92210E
CFU
1000 mpu per gram
oftotal solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 M PN per 4 grams
total solid (dry
I weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.l (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec, 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization
lAlt 7 (Drying - Stable) ❑
1 Alt. 8 (Drying- Unstable) ❑
Alt. 9 (Injection) El
Alt. 10 (Incorporation)
INo vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please cheep the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .110b and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met" (Please note if
you cheep this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met, 1 am aware that there are
significant penalties for false certification including fine and imprisonment."
Mark Young, ORC Wesley Wooten, President
Preparer ame and Ti p {type or print) Land Applier Name and Title (if applicable)(type or print)
t 9126/22
Sri1-ure of Prepa r Date Signature of Land Applier (if applicable) Date
*Preparer is define n 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (2b)
DENR FORM PVRF 02T (1212006)

2022 APPLICATION SUMMARY

COASTAL FARMS AND RESIDUALS, LLC
Permit # WQ 0034806
2022
RESIDUALS APPLICATIONS
APPLICATION SUMMARY
Corbett Farming Company
CFC-1
81.9
2,874,500
217.48
78.74
31.53
Wilber Corbett
WC-1
93.4
3,292,455
528
366.78
81.62
30.06
Totals
Metric Tons 529.92

FIELD LOADING RATE REPORTS

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name: Coastal Farms and Residuals 1VQ Permit 11 1VQ0034806 Meld 8 1
Land Owner: Corbett Farming Annual DT`s Applied: 217.48 Site tl: CFC
Acres Utilized: 31.9
Acres Permifled: 81.9
Operator: Allen Wooten Predominant Sail Series: Norfolk- NoA Cation Exchange Capacity (non 503):
Crop 1 Name: Coastal Bermudr Crop 1 Max. PAN: 299 Crop 2 Name: Rye Crop 2 Max. PAN: 50
Application Method: S- Surface I I - Injected Volatilization Rote: Surface- 0.51 Injected or Inrorparated - 1.0
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2022
92,000
IJ23
1.44
1 0.07
Awadale W%M
Dry
0.006
0.0061
0.0181
0.006
0.000
0.006
0.006
0.006
0.103
3.10
0.65
1.93
Cougar
Ryx
10.56
0.83
0.00
2022
513,500
6,270
2.21
1 0.58
8op0ieur
D
0.025
0.0251
0.2031
0.029
0,001
0.025
0.025
0.025
0.743
14,57
6.36
38.71
Coaxal
Rye
68.76
1.44
0.01
2022
2,269,000
27,705
1.74
1 2.01
Surf0iyNV%VrP
Dry
0.080
0.0791
1,689
0.079
0.004
0.079
0.079
0.079
16.896
61.07
24.52
90.86
Coulat
RYE
270.97
5.03
0.79
Total
2,874,So0
Annual lbrlacre
Curren) Cumulafiv lhslncre
Prior Vears Cumulative Ibrincre
Pormitt C.P.L.R �••
0.111
0.110
1.910
0.110
0.006
0.110
0.110
0.110
17.732
78.74
31.53
131.50
Lim pp,
0.22
0.21
3.16
0.2I
0.01
0.21
0.21
0.21
29.58
299
-0
Permit PAN Limt IsItInd Crop
Dnte
LbslAc
0.11
0.10
1.25
0.10
0,00
0.10
0.10
0.10
11.85
36
34
1,336--1
267
15
n/n
374
89
2,498
'1 certify, under penalty oflaw, that this document was prepared under my direction or supervision in accordance witlh a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false inromhalion, Including Elie possibility of fines and imprisonment for knowing violations."
2114I23 *Application Method; S - Surface, IN - injection, INC - Incorporation
(Sign ure of L d Applier) Date "Volatilization Rare: Surface - 0.5, Injectiotd(ncorperalion -1.0
1•1C.P1,P.: Cumulative Pollutant Loading bate
Bold denotes application that was Injected or Incorporated
WMSS, PLLG f]ENR FORM FSF(12/2006) Mod_

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name Coastal Farms and Residuals WQ Permit 0
NVQ0034806 Field 0 1
Acres Utilized-
93.4
Land Owner; Wilber Corbett Annual DT's Applied: 366.78
Site 0: WC
Acres Permitted:
93.4
Operator. wesle 3Vy ooten Predominant Sail Series: AutrYville - Aull
Cation Exchnnge Capacity (non 503):
4.2
Crop I Name: f7ermuda Crap I Mox. PAN: I96
Crap 2 Name Rycgrass
Crop 2 Max. PAN:
50
Application Method: S - Surface I I -injected -
V012tilization Rate: Surface • 0.51lnjerled
or incornornled • 1.0
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2022
260,000
2.784
3.82
0.44
Carotins Utani
Dry
0.030
O.D22
0.590
0.022
0.000
0.022
0.022
0,022
1.046
18.55
11.09
Derma++
61.81
0.00
0.01
2022
528.0
R65
24.30
1.37
Maretread Gly
G/D
0.019
0.011
1.753
0.035
0,003
0.014
0.029
0.011
2,577
7.49
3.14
1.66
nomad.
nyezrass
381.88
69.51
0.03
2022
240,455
2,574
1.36
0,15
Non :west
C/D
Dry
0.010
0.026
0.010
0.0191
0.100
0.189
0.010
0,019
0.003
0,0011
0.010
0.019
0.010
0.019
0,010
0,019
0.400
0.966
4.58
10.44
5.45
11.13
11.74 1
Derm.&
0ernwds
R rrrs
10.73
43.55
0.49
4.03
1.01
0.00
2022
455.000
4,872
2.33
0.47
6ak island
2022
1,227,400
13,084
1.38
0.75
Pluru trmnps'ead
IMM
DU
0.050
0.050
0.190
0.050
0.002
0.050
0.0501
0.051)1
0.676
19.25
11.56
37.19
01mudal
pY[erass
97.73
2.I4
0.9D
2022
403,000
4,315
0.72
0.13
Sam ri`odre
CID
0.007
0.007
0.037
0.007
0.001
0.007
0.007
D.007
0.762
6.33
10.18
Bermuda
17.39
0.86
0.51
2022
702.000
7,516
1.94
0,6E
Swens6ara
CID
0.029
0.020
0,342
0.020
0.001
0.020
0.020
0.020
4.463
14.98
9.91
19.34
nem,ada
R e%rass
44.02
0,96
11.01
Total
3,232.993
AnmralIbs/atre
0.163
0.139
3.I91
0.163
0.010
0,143
0.158
0.139
10.890
8I.62
30,06
102.32
Lime Ann.
1.51
1.32
37.36
1.96
0.07
1.33
1.71
1.40
176.61
196
50
Permit PAN Liml Istl2nd Crop
Datc
LbslAc
Current Cnmulntive lbslacre
1.34
1.18
34.17
1.80
0.06
1,19
1.55
1,26
115.72
Prior Years Cumulativg11joAcre
36
34
1,338
267
15
n/a 1
374
89
2,498
Permiil CP,L.B,•'*
"I certify, under penalty of law, that ibis document seas prepared under my direction or supervision in accordancewish a system
designed to assure That qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false infonnalion, Including the possibility of fines and imprisonment for knowing violations."
X 2114123 'Application Method: S - Surface, IN - Injection, INC - Incorporation
(Signatur Lao pplier) Date -Volatilization (tale: Surface -0.5, Injectionllncorporation- 1.0
"•C.P.L.R.: Cumulative Pollutant Loading Rate
Bold denotes application that was Injected or incorporated
WMSS, PLLC
DENR FORM FSF(12/2008) Mad.

SOIL ANALYSIS REPORTS

Page 1 of 1
Report No: 22-046-1055
Account No: 08361
Advisor: Willcox & Mabe Soil Solutions, PLLC
7231 B. Summerfield Rd
Summerfield NC 27358
D
Waypotein
ANALYTICAL
Client: Coastal Farms
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm:
Date Received: 02/16/2022
Date of Report: 02/17/2022
Lab Ho Field 1D Sample ID Soil Class HM% W/V pH Ac P-1 K-I S-1 Mn-1 Mn-All Mn-Al2 Zn4 Zn-Al Cu-1 CEC BS% Ca% Mg% ESP Na
15713 CFC1 MIN 6.3 0.7 98 65 31 31 0 0 143 143 145 6.8 89 76 8 0.6 0
15714 WC1 MIN 5.5 0.7 155 28 27 25 0 0 73 73 245 2.9 75 55 13 1.8 0.1
Commant:
Test result units = CEC and Na in megl100cm3; NO3 N in mgldm3; WIV in glcm3
North Carolina Division of Water Quality Certification 4257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.