WQ0030132_2022 Residual Annual Report_20230213 (2)

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * WQ0030132
Applicant/Permittee Town of Plymouth
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Washington
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Drew Matthews
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
2528839301
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0030132
Has Current Existing permit number
Applicant/Permittee Address*
124 East Water Street Plymouth, NC 27962
Facility Name*
Town of Plymouth Class B Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2022 Plymouth Annual Report.pdf 4.37MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
01f1 i �4e*A~
Submission Date 2/13/2023

TOWN OF PLYMOUTH
2022 ANNUAL LAND APPLICATION OF
RESIDUAL BIOSOLIDS REPORT
CLASS B PROGRAM
WQ0030132
Submitted by:
Soil Plus
P.O. Box 1396
Oxford, North Carolina 27565
February 8, 2023
SOIL PLUS

SOIL PLUS
February 8, 2023
NCDEQ-DWR
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Re: 2022 LAND APPLICATION ANNUAL REPORT
Town of Plymouth "Class B" Program
NC Permit No.: WQ0030132
Soil Plus Project No. 200701.A10
Information Processing Unit:
Soil Plus, LLC (Soil Plus) is submitting all monitoring and reporting requirements as
specified in the above referenced permit for the Town of Plymouth on behalf of Granville
Farms, Inc. Soil Plus compiled this report using data gathered during the compliance year.
This data includes (1) certification form, (2) residual sampling, (3) field loading calculations,
(4) pathogen and vector attraction reduction documentation, (5) standard soil fertility
nutrient analysis.
The Town of Plymouth conducted application events on permitted fields in Washington
County during 2022. A total of 40.42 Dry Tons or 322,000 Gallons of permitted residual
biosolids were land applied to permitted fields.
If there is any further information required or questions regarding this report, please do
not hesitate to contact me or the Town of Plymouth (252-793-9101) for further assistance.
Respectfully,
Drew Matthews, Soil Plus
cc: Mike Wright, Town of Plymouth
Bryan A. Smith, Granville Farms
P.O. Box 1396
Oxford, NC 27565
[phone]
dmatthewsgsoilplus. ne t
www.soilplusuc.com

Town of Plymouth
2022 Annual Land
Application of
Residual Bio s olid s
Report
WQ0030132
Plymouth, NC
ANNUAL LAND
APPLICATION
CERTIFICATION FORM
Field Loading & Source Summary
ANNUAL RESIDUAL
SAMPLING SUMMARY
FORM
Annual Analytical Data
FIELD LOADING
SUMMARY FORM
Mizelle Farm (Site 2)
ANNUAL PATHOGEN &
VECTOR ATTRACTION
REDUCTION FORM
Fecal Coliform Data
30-Day Bench Scale Test
SOIL SAMPLES
X izelle Farm (Site 2)

Town of Plymouth
2022 Class B Annual Report
WQ Permit# WQ0030132
Annual Certification Form
Source Summary
Field Loading Summary

ANNUAL LAND APPLICATION CERTIFICATION FORM
PermitNumber FacilityName Land Application Operator County Phone Number
WQ0030132 Town of Plymouth Granville Farms, Inc. Washington [phone]
Year: 2022
Land application of residuals as allowed by the permit occurred during the past calendar year? If No, skip Part A, and Part Yes No
B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the FV A
residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in the permit: 3
Total number of fields utilized for land application during the year: 3
Total amount of dry tons applied during the year for all application sites: 40.42
Total number of acres utilizes for land application during the year: 16.67
Part B - Annual Compliance Statement:
Facility was compliant during calendar year with all conditions of the land application permit? Yes No
Including but not limited to items 1-13 below) issued by the Division of Water Quality S6 A
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites
2. Soil pH was adjusted as specified in the permit and time was applied (if needed) to achieve a soil pH of at least 6
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory
results are attached
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified
laboratory results are attached
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T
7. All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated
facilities)
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities)
9. All operations and maintenance requirements in the permit were -complied with or, in the case of a deviation, prior authorization was
received from the Division of Water Quality
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to
include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibi ity of fines and
imprisonment for knowing violations."
Mike Wright, Public Works Director
Pe agm�e and/Title (type or print): ig ature of e i tee ate
rY�l 1 /25/23
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

Source Summary Report
WWTP VolumeApplied
Town of Plymouth WWTP 322,000
Total Dry Tons,
40.42
Total 322,000 40.42

Site# Site 2
YEAR TO DATE FIELD LOADING SUMMARY
CROPS USED AND VOLUME APPLIED PERMITTED CROPS AND LOADING RATES
Acres Volume Crop 1 PAN Crop 2 PAN Crop 1 PAN 1 Crop 2 PAN 2
Field Used Applied Total DT lbs/Ac. lbs/Ac. Crop 1 Name PAN Used Crop 2 Name PAN Used
1 3.88
63,000
7.91
35.66
Fescue Hay
138
25.8%
2 5.1
112,000
14.06
48.23
Fescue Hay
138
35.0%
3 7.69
147,000
18.45
41.99
Fescue Hay
138
30.4%
Total 322,000

Town of Plymouth
2022 Class B Annual Report
WQ Permit# WQ0030132
Residual Saml2ling Summary Form
Field Loading Calculations
2022 Analytical
2022 TCLP

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
WQ Permit No. WQ0030132 Facility Name Town of Plymouth Source Permit No. NCO020028 Source Name Town of Plymouth W WTP
Laboratory 1 Mentech, Inc.
Laboratory 2
Sample or CompositeDate 7/18/2022
Parameter (mg/Kg) Class A Class B
Aluminum
N/A
N/A
10,100
Ammonia Nitrogen
N/A
N/A
837
Arsenic
41
75
0.33
Cadmium
39
85
1.2
Calcium
N/A
N/A
3,700
Copper
1,500
4,300
229
Lead
300
840
20.1
Magnesium
N/A
N/A
4,920
Mercury
17
57
0.1
Molybdenum
N/A
75
2.6
Nickel
420
420
9.4
Nitrate -Nitrite Nitrogen
N/A
N/A
332
Percent Solids
N/A
N/A
3.01
PH (no units)
N/A
N/A
7.20
Phosphorus
N/A
N/A
16,000
Potassium
N/A
N/A
2,870
PAN (Inj./Inc.)
N/A
N/A
9,168
PAN (Surface)
N/A
N/A
8,749
Selenium
100
100
1.66
Sodium
N/A
N/A
10,500
SAR
N/A
N/A
2,80
TEN
N/A
N/A
27,500
Zinc
2,800
7,500
591
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

1 ,
yr,WID. .
Facility Town of Plymouth WWTP
Sampling Date
7/18/2022
%Solids
3.01
Mineralization Rate
0.30
Gallons per DT
7,967.05
pH
7.2
FIELD LOADING ESTIMATES
Sodium Absorpotion 2.80 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION NUTRIENT APPLICATION
TKN (mg/Kg) 27,500 lbs./1,000 gal 6.90
Ammonia Nitrogen (mg/Kg) 837.00 lbs./1,000 gal 0.21
Nitrate -Nitrite (mg/Kg) 332.00 lbs./1,000 gal 0.08
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 8,749 lbs./1,000 gal 2.20
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 9,168 lbs./1,000 gal 2.30
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
HEAVY METAL CONCENTRATION
Potassium lbs./1,000 gal 0.72
Phosphorus lbs./1,000 gal 4.02
Calcium lbs./1,000 gal 5.95
Magnesium lbs./1,000 gal 1.24
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL LOADING
Arsenic (mg/Kg)
0.33
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
1.20
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
229.00
Copper lbs./1,000 gal
0.06
Lead (mg/Kg)
20.10
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.10
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
9.40
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
1.66
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
591.00
Zinc lbs./1,000 gal
0.15
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
27,500
8,749 17.50
18,751
27,500
9,168 18.34
18,332
18,751
2,813 5.63
15,938
18,332
2,750 5.50
15,582
15,938
1,195 2.39
14,743
15,582
1,169 2.34
14,414
14,743
553 1.11
14,190
14,414
541 1.08
13,873
14,190
266 0.53
13,924
13,873
260 0.52
13,613
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 13,576 27.15
Total 13,887 27.77

Contact: Drew Matthews
Client: Soil Plus
P.O. Box 1396
Oxford, NC 27565
Meritech Work Order # 07182244
Parameters
% Total Solids
Ammonia, Nitrogen
TKN
Nitrate/Nitrite, Nitrogen
Aluminum, total
Arsenic, total
Cadmium, total
Calcium, total
Copper, total
Lead, total
Magnesium, total
Mercury, total
Molybdenum, total
Nickel, total
Phosphorus, total
Potassium, total
Selenium, total
Sodium, total
Zinc, total
PH
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Sample: PL 071822 Grab
Results
3.01 %
837 mg/kg
27,500 mg/kg
<332 mg/kg
10100 mg/kg
<0.330 mg/kg
1.20 mg/kg
23,700 mg/kg
229 mg/kg
20.1 mg/kg
4,920 mg/kg
0.100 mg/kg
2.60 mg/kg
9.40 mg/kg
16,000 mg/kg
2,870 mg/kg
<1.66 mg/kg
10,500 mg/kg
591 mg/kg
7.2 S.U.
Analysis Date
7/20/22
7/19/22
7/26/22
7/20/22
7/31/22
7/31/22
7/31/22
7/31/22
7/31/22
7/31/22
7/31/22
7/26/22
7/31/22
7/31/22
7/31/22
7/31/22
8/5/22
7/31/22
7/31/22
7/21/22
Report Date: 8/8/2022
Project: Plymouth
Date Sample Rcvd: 7/18/2022
Reporting Limit
0-100 %
10 mg/kg
20 mg/kg
332 mg/kg
2.50 mg/kg
0.330 mg/kg
0.100 mg/kg
10.0 mg/kg
1.00 mg/kg
0.500 mg/kg
10.0 mg/kg
0.02 mg/kg
0.250 mg/kg
0.500 mg/kg
1.00 mg/kg
20.0 mg/kg
1.66 mg/kg
20.0 mg/kg
0.500 mg/kg
1.0 -14.0 S.U.
7/18/22
Method
SM 2540B
EPA 350.1
EPA 351.1
EPA 353.2
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 245.1
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
SM 4500-HB
I hereby certify that I have reviewed and approve these data.
i
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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Inc.
iMeritech,
Environmental Laboratory
AN
Laboratory Certification No. 165
Page 1
Contact: Drew Matthews
Report Date:
8/11/2022
Client: Soil Plus
P.O. Box 1396
Project:
Plymouth
Oxford, NC 27565
Date Sample Rcvd:
7/18/2022
Meritech Work Order # 07182245 Sample: PL 071822 Grab
7/18/2022
1311- TCLP Metals
Parameter
Results Analysis_Date Det. Limit
Reg. Limit
Method
Arsenic
<0.100 mg/L 8/2/2022 0.100
5.0
EPA 200.7
Barium
0.069 mg/L 8/2/2022 0.050
100.0
EPA 200.7
Cadmium
<0.020 mg/L 8/2/2022 0.020
1.0
EPA 200.7
Chromium
<0.005 mg/L 8/2/2022 0.050
5.0
EPA 200.7
Lead
<0.100 mg/L 8/2/2022 0.100
5.0
EPA 200.7
Mercury
<0.02 mg/L 8/2/2022 0.02
0.2
EPA 245.1
Selenium
0.103 mg/L 8/2/2022 0.100
1.0
EPA 200.7
Silver
<0.050 mg/L 8/2/2022 0.050
5.0
EPA 200.7
TCLP Organics
Parameter
Results
Analysis Date
Reporting Limit
Method
Volatiles 8260
Attached
7/27/2022
-
8260
Semi Vol. 8270
Attached
8/4/2022
-
8270
Other Tests
Parameter
Results
Analysis Date
Reporting Limit
Method
Cyanide, total
<0.500 mg/kg
7/19/2022
0.500 mg/kg
EPA 335.4
Sulfide
<10.0 mg/kg
7/22/2022
10.0 mg/kg
SM4500S2D
Flash Point
>140 °F
7/19/2022
-
EPA 1020C
Corrositivity [pH]
7.5 S.U.
7/19/2022
LO -14.0 S.U.
SM 4500 HB
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Drew Matthews
CIient: Soil Plus
Page 2
Report Date: 8/11/2022
P.O. Box 1396 Project: Plymouth
Oxford, NC 27565 Date Sample Rcvd: 7/18/2022
Meritech Work Order # 07182245 Sample: PL 071822 Grab
7/18/2022
1311- TCLP Pesticides & Herbicides
Pesticide - SW-846 8081A
Parameter Results Analysis Date Det. Limit Reg. Limit Dilution Factor
Endrin
Attached - - -
Chlordane
Attached - - -
Toxaphene
Attached - - -
Methoxychlor
Attached - - -
Heptachlor
Attached - - -
Lindane
Attached - - -
Herbicides - SW-846 8151A
Parameter
2,4-D
2,4,5-TP (Silvex)
Results Analysis Date Det. Limit Reg. Limit Dilution Factor
Attached
Attached
I hereby certify that I have reviewed and approve these data. .� 1�Q. �Qf1CAC fit.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

MERITECH, INC.
,..: Environmental Laboratories
.-r• Laboratory Certificate #165
Client: Soil Plus
Project: Plymouth
Client Sample ID. PL071822
Sample Collection: 07/18/22
Meritech Sample ID: 07182245
1311 - TCLP Organics
Volatiles: SW-846 8260
Analysis: 07/27/22
Extraction:
07/25/22
Analyst: VWV
Report Date:
07/29/22
Parameter
Result
Units
Det. Limit
Rea. Limit
Dilution Factor
Benzene
< 0.0100
mg/L
0.0100
0.50
10
Carbon Tetrachloride
< 0.0100
mg/L
0.0100
0.50
10
Chlorobenzene
< 0.0100
mg/L
0.0100
100
10
Chloroform
< 0.0100
mg/L
0.0100
6.0
10
1,2-Dichtoroethane
< 0.0100
mg/L
0.0100
0.50
10
1,1-Dichloroethene
< 0.0100
mg/L
0.0100
0.70
10
Methyl Ethyl Ketone
< 0.100
mg/L
0.100
200
10
Tetrachloroethylene
< 0.0100
mg/L
0.0100
0.70
10
Trichloroethene
< 0.0100
mg/L
0.0100
0.50
10
Vinyl Chloride
< 0.0200
mg/L
0.020
0.20
10
Semi-Volatiles: SW-846 8270
Analysis: 08/04/22
Extraction:
07/25/22
Analyst: PM
Report Date:
08/10/22
Parameter
Result
Units
Det. Limit
Reg. Limit
Dilution Factor
I,4-Dichlorobenzene
<0.100
mg/L
0.100
7.5
10
Hexachlorobenzene
<0.100
mg/L,
0.100
0.13
10
Hexachloro-1,3-butadiene
<0.100
mg/L
0.100
0.5
10
Hexachloroethane
<0.100
mg/L
0.100
3.00
10
o-cresol
<0.100
mg/L
0.100
200
10
m&p-cresol
<0.200
mg/L
0.200
200
10
Total cresols
<0.300
mg/L
0.300
200
10
Nitrobenzene
<0.100
mg/L
0.100
2.00
10
Pentachlorophenol
<0.500
mg/L
0.500
100
10
Pyridine
<0.100
mg/L
0.100
5.0
10
2,4,5-Trichlorophenol
<0.100
mg/L
0.100
400
10
2,4,6-Trichlorophenol
<0.100
mg/L
0.100
2.00
10
2,4-Dinitrotoluene
<0.100
mg/L
0.100
0.13
10
I hereby certify that I have reviewed and approve
these data.
Laboratory Representative
642 Tamco Road * Reidsville, NC 27320
[phone] * [e-mail]

Summit Environmental Technologies, Inc.
SUMM,nt
W04: 22071238
3310 Win St.
€NVIF60M
dENTAL
] �GAPid]L(F �t�F --N'c
Cuyahoga Falls, Ohio 44.,23
Date Reported: 8/2/2022
Auz,4,
cal Labcrgrorda:•
TEL: [phone] FAX.- [phone]
Company: Meritech
Environmental
Laboratories
Website: htra:/heww.settekcam
Address: 642 Tamco
Rd.
Reidsville
NC 27320
Received: 7/21/2022
Project#:
TCLP Pesticides Analysis (SW1311/8081)
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix Method
DF
RegLvl
Run
Analyst
071822-35
001
7/18/2022 Chlordane, total
25.0 NO pg/L
EPA 8081B
10
30.0
7/29/2022
PGP
071822-35
001
7/18/2022 Toxaphene
50.0 NO pg1L
EPA 8081 B
10
500
7/29/2022
PGP
071922-35
001
7/18/2022 Enddn
25.0 NO pglL
EPA 8081B
50
20.0
7/30/2022
PGP
071822-35
001
7/18/2022 gamma-BHC
5.00 NO pglL
EPA 8081 B
10
400
7/29/2022
PGP
071822-35
001
7/18/2022 Heptachlor
5M NO pg1L
EPA 8081B
10
8.00
7/29/2022
PGP
071822-35
001
7/18/2022 Heptachlor epoxide
5,00 NO pg/L
EPA 8081 B
10
8,00
7/29/2022
PGP
071822-35
001
7/18/2022 Methoxychlor
5.00 NO pg1L
EPA 80818
10
10000
7/29/2022
PGP
TCLP Herbicides by EPA 8321B
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix Method
DF
RegLvl
Run
Analyst
071822-35
001
7/18/2022 2,4-D
0.500 NO mg1L
EPA 8321B
50
10.0
7/30/2022
PGP
071822-35
001
7/18/2022 2,4,5-TP
0.500 NO mg/L
EPA 8321E
50
1.00
7/30/2022
PGP
TCLP Pesticides Analysis (SW1311/8081)
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix Method
DF
RegLvl
Run
Analyst
071822-45
002
7/18/2022 Chlordane, total
25.0 NO pg/L
EPA 8081 B
10
MO
7/29/2022
PGP
071822-45
002
7/18/2022 Toxaphene
50.0 NO pglL
EPA 8081B
10
500
7/29/2022
PGP
071822-45
002
7/18/2022 Endrin
25.0 NO pg/L
EPA 8081B
50
20.0
7/30/2022
PGP
071822-45
002
7/18/2022 gamma-BHC
5.00 NO pg/L
EPA 8081E
10
400
7/29/2022
PGP
071822-45
002
7/18/2022 Heptachlor
5.00 NO pg/L
EPA BOB18
10
8.00
7/29/2022
PGP
071822-45
002
7/18/2022 Heptachlor epoxide 5.00 NO pg1L
EPA 8081B
10
8.00
7/29/2022
PGP
071822-45
002
7/18/2022 Methoxychlor
5.00 NO pg/L
EPA 8081B
10
10000
7/29/2022
PGP
TCLP Herbicides by EPA 8321E
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix Method
DF
RegLvl
Run
Analyst
071822-45
002
7/18/2022 2,4-D
0.500 NO mg/L
EPA 8321 B
50
10.0
7/30/2022
PGP
071822-45
002
7118/2022 2,4,5-TP
0.500 NO mg/L
EPA 8321 B
50
1.00
7/30/2022
PGP
Page 4 of 11

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ID

Town of Plymouth
2022 Class B Annual Report
WQ Permit# WQ0030132
Land A1212lication Field Summary Forms

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0030132 Site# Site 2 County Washington Crop 1 Fescue Hay
Facility Name Town of Plymouth Field Name 1 SoilSeries Bojac Crop 1 Pan 138
LandOwner Marjory P. Mizelle Acres Permited 3.88 Soil Abbrevation: BoA Crop 2
Operator Granville Farms, Inc. Crop 2 Pan
Volume
Acres Dry
Soil
Application
Total
Nitrate- Crop 1
Crop 2
Date Measurement Applied
% Solids Used DT/Ac. Tons Source
Condition Precip
Method
P Volatilization Mineralization
TKN Ammonia Nitrite PAN
PAN Crop
07/19/2022 Gallons 49,000
3.01 3.88 1.59 6.15 Town of Plymouth WWTP
Dry < 0.5"
Surface
50.72 0.50 0.3
27,500 837.00 332.00 27.74
Crop 1
07/20/2022 Gallons 14,000
3.01 3.88 0.45 1.76 Town of Plymouth WWTP
Dry < 0.5"
Surface
14.49 0.50 0.3
27,500 837.00 332.00 7.93
Crop 1
Total Volume Applied
63,000
Total Dry Tons 7.91
Sum Total P 65.22
Total 35.66
Total
Reported in Gallons
Arsenic Cadmium
Copper Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.001
0.005
0.933
0.082
0.000
0.011
0.038
0.007
2.409
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
0.282
0.120
21.397 1.252
2.143
0.043
0.281
1.172
0.252
51.776
Cumulative Total
0.284
0.125
22.331
2.225
0.043
0.292
1.210
0.259
54.185
N/A
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information
submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
1 /25/23 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

PermitNumber WQ0030132
Facility Name Town of Plymouth
LandOwner Marjory P. Mizelle
Operator Granville Farms, Inc.
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Site# Site 2 County Washington Crop 1 Fescue Hay
Field Name 2 SoilSeries Bojac Crop 1 Pan 138
Acres Permited 5.10 Soil Abbrevation: BoA Crop 2
Crop 2 Pan
Volume
Acres Dry
Soil
Application
Total
Nitrate- Crop 1
Crop 2
Date Measurement Applied
%Solids Used DT/Ac. Tons Source
Condition Precip
Method
P Volatilization Mineralization
TKN Ammonia Nitrite PAN
PAN Crop
07/20/2022 Gallons 84,000
3.01 5.10 2.07 10.54 Town of Plymouth WWTP
Dry < 0.5"
Surface
66.15 0.50 0.3
27,500 837.00 332.00 36.18
Crop 1
07/21/2022 Gallons 28,000
3.01 5.10 0.69 3.51 Town of Plymouth WWTP
Dry < 0.5"
Surface
22.05 0.50 0.3
27,500 837.00 332.00 12.06
Crop 1
Total Volume Applied
112,000
Total Dry Tons 14.06
Sum Total P 88.21
Total 48.23
Total
Reported in Gallons
Arsenic Cadmium
Copper Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.002
0.007
1.262
0.111
0.001
0.014
0.052
0.009
3.258
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
0.379
0.171
33.168 1.693
3.292
0.050
0.437
1.688
0.386
75.761
Cumulative Total
0.381
0.178
34.430
3.402
0.050
0.452
1.740
0.395
79.020
N/A
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information
submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
n *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
1 /25/23 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0030132 Site# Site 2 County Washington Crop 1 Fescue Hay
Facility Name Town of Plymouth Field Name 3 SoilSeries Bojac Crop 1 Pan 138
LandOwner Marjory P. Mizelle Acres Permited 7.69 Soil Abbrevation: BoA Crop 2
Operator Granville Farms, Inc. Crop 2 Pan
Volume
Acres
Dry
Soil
Application
Total
Nitrate- Crop 1
Crop 2
Date
Measurement Applied
%Solids
Used DT/Ac. Tons Source
Condition Precip
Method
P
Volatilization Mineralization
TKN
Ammonia Nitrite
PAN
PAN Crop
07/18/2022
Gallons 35,000
3.01
7.69 0.57
4.39 Town of Plymouth WWTP
Dry G 0.5"
Surface
18.28
0.50 0.3
27,500
837.00 332.00
10.00
Crop 1
07/19/2022
Gallons 56,000
3.01
7.69 0.91
7.03 Town of Plymouth WWTP
Dry G 0.5"
Surface
29.25
0.50 0.3
27,500
837.00 332.00
15.99
Crop 1
07/21/2022
Gallons 56,000
3.01
7.69 0.91
7.03 Town of Plymouth WWTP
Dry G 0.5"
Surface
29.25
0.50 0.3
27,500
837.00 332.00
15.99
Crop 1
Total Volume Applied
147,000
Reported in Gallons
Arsenic Cadmium
Current Year
0.002
0.006
Prior Year
0.324
0.153
Cumulative Total
0.326
0.159
Permitted CPLR
36
34
Total Dry Tons 18.45
Copper Chromium
Lead
1.099
0.096
29.534 1.353
2.901
30.633
2.997
1338
267
Mercury Molybdenum
0.000 0.012
0.040 0.387
0.040 0.399
15
Sum Total P 76.78
Nickel
Selenium
Zinc
0.045
0.008
2.836
1.490
0.338
65.919
1.536
0.346
68.755
374
89
2498
Total 41.99 Total
Crop 1 Crop 2
PAN PAN
(lbs./Ac.) (lbs./Ac.)
Lime (T/Ac.) Date
N/A
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information
submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
4-x,e� 1 /25/23 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

Town of Plymouth
2022 Class B Annual Report
WQ Permit# WQ0030132
Pathogen & Vector Attraction Reduction Form
Fecal Coliform Geometric Mean
30-Day Bench Scale Test

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Plymouth WQ Permit Number: WQ0030132
WWTP Name: Town of Plymouth WWTP NPDES Number: NCO020028
Monitoring Period: 01/01/2022 to 12/31/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 1
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Not Applicable
Fecal Colifotm CFU Minimum Geo. Mean
(Dry Weight)
9,756 11,767
Technique SM 9222 D
Maximum # of Exceedences Frequency
15,957 0 Annually
Vector Attraction Reduction Performed (15A NCAC 02T .1107): Alt. 3 (30-day bench)
Sample Type
Grab Samples
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Roland Coburn, WVVTP Operator
Preparer Name and Title (type or print)
Signature of Preparer*
Bryan \. Smith, president
Land Applier Name and Title (if applicable)(type or print)
4­,;e-,�
1 /25/23
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

Meritech, Inc.
i-k
Environmental Laboratory
Ak"
Laboratory Certification No.165
Page 1
Contact: Drew Matthews
Report Date:
7/28/2022
Client: Soil Plus
P.O. Box 1396
Project:
Plymouth
Oxford, NC 27565
Date Sample Rcvd:
7/18/2022
Meritech Work Order #
07182236 Sample: PL 071822 (001) Grab
7/18/22
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
2.81 % 7/21/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
10,498 CFU/g dry wt 7/18/22
130 CFU/g dry wt
SM 9222D
Meritech Work Order #
07182237 Sample: PL 071822 (002) Grab
7/18/22
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
2.81 % 7/21/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
14,235 CFU/g dry wt 7/18/22
130 CFU/g dry wt
SM 9222D
Meritech Work Order #
07182238 Sample: PL 071822 (003) Grab
7/18/22
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
2.83 % 7/21/22
0-100 %
SM 2540B
Fecal Coliform (SIudge)
9,894 CFU/g dry wt 7/18/22
130 CFU/g dry wt
SM 9222D
Meritech Work Order #
07182239 Sample: PL 071822 (004) Grab
7/18/22
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
2.80 % 7/21/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
11,429 CFU/g dry wt 7/18/22
130 CFU/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

r
Contact: Drew Matthews
Client: Soil Plus
P.O. Box 1396
Oxford, NC 27565
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Meritech Work Order # 07182240 Sample: PL 071822 (005) Grab
Parameters Results Analysis Date
% Total Solids 2.78 % 7/21/22
Fecal Coliform (Sludge) 11,871 CFU/g dry wt 7/18/22
Meritech Work Order # 07182241
Parameters
Sample: PL 071822 (006) Grab
Results Analysis Date
Page 2
Report Date: 7/28/2022
Project: Plymouth
Date Sample Rcvd: 7/18/2022
7/18/22
Reg Limit Method
0-100 % SM 2540B
130 CFU/gdry wt SM 9222D
7/18/22
Reporting Limit Method
% Total Solids
2.87 %
7/21/22
0-100 %
SM 2540E
Fecal Coliform (Sludge)
9,756 CFU/g dry wt
7/18/22
130 CFU/g dry wt
SM 9222D
Meritech Work Order #
07182242 Sample: PL 071822 (007) Grab
7/18/22
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
2.82 %
7/21/22
0-100 %
SM 2540B
Fecal Coliform (Sludge)
15,957 CFU/g dry wt
7/18/22
130 CFU/g dry wt
SM 9222D
I hereby certify that have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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Contact: Drew Matthews
Client: Soil Plus
P.O. Box 1396
Oxford, NC 27565
Meritech, nc.
Environmental La oratory
Laboratory Certificatio No.165
Report Date: 8/31/2022
Project: PIymouth
Date Sample Rcvd: 7/18/2022
Vector Attraction Reduction
Aerobically
Digested Sludge
30 Day Test
Meritech
Work Order # 07182243
Sample: PL
71822 Grab
7/18/22
Total Solids
Volatile Solids
% Volatile Solids
Week 1
0.930
0.540
0.584
Week 2
0.820
0.500
0.611
Week 3
0.830
0.480
0.578
Week 4
0.790
0.460
0.587
Week 5
0.660
0.380
0.580
Mass Balance Equation = 0.66% Volatile Solids Reduction as per
I hereby certify that I have reviewed and approve these data.
642 Tamco Road, Reidsville, Nor
tel.[phone] fax.(33
EPA Part 503 Biosolids Rule
Laboratory Representative
th Carolina 27320
5] 342-1522

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Town of Plymouth
2022 Class B Annual Report
WQ Permit# WQ0030132
Soil Samples

Page 1 of 1
Report No: 22-307-0521
Account No: 04596
Advisor: Soil Plus, LLC
Joyce Barrette
P.O. Box 1396
Oxford NC 27565
Waypo'10 t
ANALYTICAL
Client: Granville Farms Inc
2850 Daisy Lane, Wilson, NC 27896
Main 252-206-1721 ° Fax [phone]
www.waypointanalytical.com
Farm: Mizzelle
Date Received: 11/03/2022
Date of Report: 11 /04/2022
Lab No Field ID
Sample ID
Soil Class HM% W/V pH
Ac
P-1
K-1
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
CEC BS %
Ca %
Mg %
ESP
Na
00601
1
MIN 0.9
6.4
1.1
253
14
27
56
44
0
348
348
210
8.0 86
62
22
1.0
0.1
Crop Recommendations:
1- Fescue Hay
Rec Uom
lb/acre
Lime (Vacre)
0.0
N
150
P205
0
K2
114
S
0
Mn
0
Zn
0
Cu
0
B
0
Mg
0
Last Crop
00602
2
MIN 0.8
6.5
1.0
323
18
33
69
51
0
568
568
360
8.4 89
66
21
1.2
0.1
Crop Recommendations:
1- Fescue Hay
Rec Uom
lb/acre
Lime (Vacre)
0.0
N
150
P205
0
K2
104
S
0
Mn
0
Zn
0
Cu
0
B
0
Mg
0
Last Crop
00603
3
MIN 1.0
6.6
1.0
279
13
29
56
41
0
588
588
375
8.7 88
65
22
1.0
0.1
Crop Recommendations:
1- Fescue Hay
Rec Uom
lb/acre
Lime (Vacre)
0.0
N
150
P205
0
K20
116
S
0
Mn
0
Zn
0
Cu
0
B
0
Mg
0
Last Crop
Comment
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/V in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Carolina, Inc.