WQ0034513_2022 Residual Annual Report_20230213 (2)

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * WQ0034513
Applicant/Permittee Brunswick County
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Wilmington
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Rob Willcox
Email Address*
[e-mail]
Project Information
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
3363399128
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0034513
Has Current Existing permit number
Applicant/Permittee Address*
Post Office Box 249; Bolivia, N.C. 28422
Facility Name*
Brunswick County Class B Residuals Program
Please provide comments/notes on your current submittal below.
Brunswick County - Class B Land Application Annual Report - WQ0034513
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2022 CLASS B ANNUAL REPORT-WQ0034513-Brunswick
14.92MB
County.pdf
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/13/2023

2022 ANNUAL REPORT
BRUNSWICK COUNTY PUBLIC UTILITIES
RESIDUALS LAND APPLICATION PROGRAM
NON -DISCHARGE PERMIT #WQ0034513
Prepared For:
Brunswick County
Public Utilities
Post Office Box 249
Bolivia, North Carolina 28422
Compiled By:
Willcox & Mabe Soil Solutions, PLLC
7231 B Summerfield Road
Summerfield, North Carolina 27358
February 2023

willcox&mate
SO I L SOL U T I ON S
February 9, 2023
N.C. Department of Environmental Quality
Division of Water Resources — Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Attention: Information Processing Unit
Reference: 2022 LAND APPLICATION ANNUAL REPORT
Brunswick County Public Utilities
Non -Discharge Permit No. WQ0034513
WMSS Project No. 15-04 Phase: 18
Information Processing Unit:
Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting
requirements as specified in the above referenced permit on behalf of Brunswick County
Public Utilities (Brunswick County). WMSS compiled this report using data gathered
during the compliance year by Brunswick County and BioGreen Services, Inc. This data
includes: 1) land application certification forms, 2) annual residual sampling summary
forms, 3) annual pathogen and vector attraction reduction forms, 4) annual field summary
forms and metals field loading summary forms, 5) lab sheets, and 6) soil analysis reports.
Brunswick County land applied a total of 61.91 dry tons of biosolids under Permit No.
WQ0034513 during the 2022 calendar year (West Brunswick Regional WWTP-61.91 dry
tons).
If there is any further information required or questions regarding this annual report please
do not hesitate to contact Mr. Donald Dixon, Deputy Director of Wastewater Operations
with Brunswick County at [phone] or Rob Willcox with WMSS for further
assistance.
Sincerely,
Willcox & Mabe Soil Solutions, PLLC
Martin Mabe
Agronomist/Partner
Enclosures
Rob Willcox, L.S.S.
Soil Scientist/Partner
Shared\WMSS Projects\2015\15-04 Brunswick County\Phase 18 - 2022 Annual Report\Class B\2022 CLASS B ANNUAL REPORT - Brunswick
County.doc
Willcox & Mabe Soil Solutions, PLLC / 7231 B Summerfield Road / Summerfield, NC 27358 / Rob 336.339.9128 or
Martin 336.312.1396 / www.willcoxmabesoil.com

TABLE OF CONTENTS
SECTION NO. TITLE
Annual Land Application Certification Forms
(Form ACF)
II Annual Residual Sampling Summary Forms
(Form RSSF)
III Annual Pathogen and Vector Attraction Reduction Forms
(503 Rules)
(Form PVRF 503)
IV Annual Land Application Field Summary Forms and Annual
Metals Field Loading Summary Forms
(Form FSF and MFLSF)
V Lab Sheets
VI Soil Analysis Reports

Brunswick County Public Utilities
Post Office Box 249
Bolivia, North Carolina 28422
RESIDUALS LAND APPLICATION PROGRAM
CLASS B RESIDUALS
PERMIT NO. WQ0034513
WEST BRUNSWICK REGIONAL WWTP
NON -DISCHARGE PERMIT NO. WQ0023693
Mr. Donald Dixon, Deputy Director of Wastewater Operations
Brunswick County Public Utilities
Post Office Box 249
Bolivia, North Carolina 28422
[phone]
2022 West Brunswick Regional WWTP Dry Tons - 61.91
2022 West Brunswick Regional WWTP Dry Metric Tons - 56.15

SECTION I
ANNUAL LAND APPLICATION CERTIFICATION FORMS
(Form ACF)

AININ UAL LAINO ArrLlt.AIRJIN LEKI It11.,AIIUM tVKIVI
WQ Permit#: WQ0034513 County:
Facility Name (as shown on permit):
Land Application Operator:
Brunswick
Year: 2022
Brunswick County
Bio-Green Services, Inc. Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
0 Yes El No - If No, skip Part A, and Part Band proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary.
West Brunswick Reeional WWTP
Total number of application fields in the permit:
31 ✓
Total number of fields utilized for land application during the year:
3
Total amount of dry tons applied during the year for all application sites:
61.91
Total number of acres utilizes for land application during the year:
26.3
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2022 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. 0 Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T. 1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T. I I 1 l were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the possibility
of fines and imprisonment for knowing violations."
Donald B. Dixon - Deputy Director ��`�� r�z�s h 3
Permittee Name and Title (type or print) Signature of Permittee Da e
1 '25 23
Signature of Preparer* West Brunswick WWTP Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1 102 (26) DFNA FnRM nrF 117/7nnrl

SECTION II
ANNUAL RESIDUAL SAMPLING SUMMARY FORMS
(Form RSSF)

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SECTION III
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORMS
(503 RULES)
(Form PVRF 503)

AIrIV UAL rA l HVULIN AIrU V Lk- 1 UK A 1 1 KAU 1 IUIV KLOUI, 1 IVIV ruKIVI (,uJ Kules)
Facility blame: Brunswick County
WQ Permit Number: _
WWTP Name: West Brunswick Regional WWTP NPDES Number: WQ0023693
Monitoring Period: From 1/1/2022 To 12:31:2022
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternativP nPrfnrmp.t•
WQ0034513
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
Alternative 4 ❑
Alternative 5 ❑
Alternative 6 ❑
If applicable to alternative performed (Class A only) indicate"Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑
1
Beta Rav ❑ Gamma Ray ❑ Pasteurization ❑
Class B:
I Alternative I ❑
Alternative 2
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization O Air Drying❑ Composting ❑ jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
Pathogen Density
g
Number of
Frequency
Sample
Analytical
Minimu
Geo. Mean
Maximum!Units
in Sludge
g
Excee-
deuces
of Analysis
Type
Tech -pique
2 x 10 to the
MPN
6th power
per gram of
Fecal Coliform
total solids
CFl
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
3 MPN per 4 grams
(in lieu of fecal
total solid (dry
coliform)
weight)
[long... Ate. ..a:
n l_at__
..�. •..■ rfu.■ aa.uVu 1\CUUMIDL k 4V L.r n :)u.3.3J) - rtease indicate option performed•
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
JAIt. 4 (Spec. 0, uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization El
Alt 7 (Drying - Stable) ❑
JAIt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CER I IFICArIUN STATEMENT (please check the appropriate statement)
G "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this
statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Ray Gambill, President - BioGreen
Preparer Name and Title (type or print)
1/25/23
Signature of Preparer* Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T . l 10' (26)
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SECTION IV
ANNUAL LAND APPLICATON FIELD SUMMARY FORMS
ANNUAL METALS LOADING SUMMARY FORMS
(Form FSF and MFLSF)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
Facility Name:
Owner:
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Brunswick County Permit #: WQ0034513 Annual Dry Tons Applied:
Richard Clemmons
Site #: NC -BR -RC Field #
Operator:
4
Richard Clemmons
Acres Utilized: 11.60
26.31
Predominant Soil Series: Onslow-On
Acres Permitted: 11.60
o
�*
Specify
Totals
Per
Acre
%
Solids
Dry Tons
Per Acre
Residual Sources
(Summarize)
ite
Cond.
Dry,
Wet
Moist
Inches
Precip.
Past 24
H
Hrs.
Appli-
cation
Meth-
od*
Vola-
till-
zation
Rate**
Miner-
all-
zation
Rate
TKN
Ammo-
ma -
Ni-
trogen
Ni-trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 or Crop
2
Gal.
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
Jan-22
110,500
9,526
5.71
2.2682
WestBniSwickRe€ioml 1AWT1
D
< 0.5"
S
0.50
0.30
34,700
25,900
0.35
70.723
#######
Wheat
1
0
0.0000
0.000
0.000
2
0
0.0000
0.000
0.000
3
0
0.0000
0.000
0.000
4
0
0.0000
0.000
0.000
5
0
0.0000
0.000
0.000
6
0
0.0000
0.000
0.000
7
0
0.0000
0.000
0.000
8
0
0.0000
0.000
1 0.000
9
0
0.0000
0.000
0.000
10
0
0.0000
0.000
0.000
11
0
0.0000
0.000
0.000
12
TOTALS:
9,526
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.0438
0.0397
0.1619
1.6195
0.0522
0.0039
0.0397
0.0857
0.0397
8.1655
33.615
70.723
0.000
Date
lbs/ac
Current Cumulative lbs/ac
0.3310 0.3629 2.6668 3.9791 0.4043 0.0211 0.374 0.4759 0.6359 31.8289
0.2872 0.3232 2.5049 2.3596 0.3522 0.0172 0.334 0.3902 0.5962 23.6633
36 34 1,338 267 15 374 89 2,498
1 106
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.***
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Arr 1/25/23
*Application Method: S -Surface, IN -Injection, INC -Incorporation
Signature of Land Applier Date **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
* * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same
numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DEN FORM FSF (5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Brunswick County Total Dry Tons Applied (Annual):
WQ0034513 Predominant Soil Series:
Richard Clemmons Owner: Richard Clemmons
26.31
Onslow-On
11.60 Acres Permitted: 11.60 Site #: NC -BR -RC Field #:
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
,� •-
�
©
0
©
0
�
0
SEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
H
1
21
3
4
5
6
71
8
9
10
11
12
O
.�
CD
o
2.2682
Arsenic
0.0438
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0438
Cadmium
0.0397
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0397
Chrommir
0.1619
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.1619
Copper
1.6195
0.0000
0.0000
0.0000
1 0.0000
0.0000
0.0000
1 0.0000
0.0000
0.0000
0.0000
0.0000
1 1.6195
Lead
0.0522
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0522
Mercury
0.0039
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0039
Molyb-
0.0397
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0397
denum
Nickel
0.0857
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0857
Selenium
0.0397
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0397
Zinc
8.1655
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
8.1655
Total
Phos-
33.6147
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.000
33.615
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility f fines and imprisonment for knowing violations"
1/25/23
Signature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM FSF (5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
Facility Name:
Owner: Richard Clemmons
Site #: NC -BR -RC
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Brunswick County Permit #: WQ0034513 Annual Dry Tons Applied:
Field #
Operator:
6
Richard Clemmons
13.93
Predominant Soil Series: Goldsboro-GoA
Acres Utilized: 4.50 Acres Permitted: 4.50
o
� o
Q
Specify
Totals
Per
Acre
%
Solids
Dry Tons
Per Acre
Residual Sources
(Summarize)
ite
Cond.
Dry
Wet
Moist
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Vola-
till-
zation
Rate**
Miner-
all-
nation
Rate
TKN
Ammo-
ma -
Ni-
trogen
Ni-trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 or Crop
2
Gal.
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
Jan-22
58,500
13,000
5.71
3.0954
Wet snuswiekRegioml WWTP
D
< 0.5"
S
0.50
0.30
34,700
25,900
0.35
96.516
#######
Wheat
1
0
0.0000
0.000
0.000
2
0
0.0000
0.000
0.000
3
0
0.0000
0.000
0.000
4
0
0.0000
0.000
0.000
5
0
0.0000
0.000
0.000
6
0
0.0000
0.000
0.000
7
0
0.0000
10.000
0.000
8
0
0.0000
0.000
0.000
9
0
0.0000
1 0.000
0.000
10
0
0.0000
0.000
0.000
11
0
0.0000
0.000
0.000
12
TOTALS:
13,000
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
I Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.0597
0.0542
0.2210
2.2101
0.0712
0.0053
0.0542
0.1170
0.0542
11.1434
45.874
1 96.516
0.000
Date
lbs/ac
Current Cumulative lbs/ac
0.4686 0.4807 7.9157 5.7675 0.6843 0.0365 0.552 0.8509 0.5804 57.1562
0.4089 1 0.4265 1 7.6947 3.5574 0.6131 0.0312 0.498 1 0.7339 0.5262 46.0127
36 34 1,338 267 15 374 89 2,498
135
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.***
Permit PAN Limit lst/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Arr 1/25/23
*Application Method: S -Surface, IN -Injection, INC -Incorporation
Signature of Land Applier Date **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
* * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the
same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DEN FORM FSF (5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Brunswick County Total Dry Tons Applied (Annual):
WQ0034513 Predominant Soil Series:
Richard Clemmons Owner: Richard Clemmons
13.93
Goldsboro-GoA
4.50 Acres Permitted: 4.50 Site #: NC -BR -RC Field #:
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
H
1
21
3
4
5
6
71
8
9
10
11
12
CD
O
.�
o
3.0954
Arsenic
0.0597
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0597
Cadmium
0.0542
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0542
Chrommir
0.2210
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.2210
Copper
2.2101
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.00001
2.2101
Lead
0.0712
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0712
Mercury
0.0053
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0053
Molyb-
0.0542
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0542
denum
Nickel
0.1170
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.1170
Selenium
0.0542
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0542
Zinc
11.1434
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
11.143
Total
Phos-
45.8738
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.000
0.0000
0.0000
0.0000
0.0000
45.874
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility fines and imprisonment for knowing violations"
A1/25/23
Signature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DEN FORM FSF (5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
Facility Name:
Owner:
Joyce Brown
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Brunswick County Permit #: WQ0034513 Annual Dry Tons Applied:
Site #: NC-BR-HB Field #:
Operator:
Harvey Bell
Acres Utilized: 10.20
21.67
Predominant Soil Series: Goldsboro-GoA
Acres Permitted: 10.20
o
Specify
Totals
Per
%
Solid
s
Dry Tons
Per Acre
Residual Sources
(Summarize)
ite
Cond.
Dry
Wet
Moist
Inches
Precip.
Past 24
Hrs.
A li-
cation
Meth-
od*
Vola-
till-
zation
Rate**
Miner-
all-
zation
Rate
TKN
Ammo-
ma -
Ni-
trogen
Ni-trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 or Crop
2
e Gal
Cu.vd.
Report
Totals
Totals
in Gal.
Crop Ticrop
2
0
0.0000
0.000
0.000
1
0
0.0000
0.000
0.000
2
0
0.0000
0.000
0.000
3
Apr-22
91,000
8,922
5.71
2.1243
WV l Bnuu wkRegi-l'A"1'TP
D
< 0.5"
S
0.50
0.30
34,700
25,900
0.35
66.237
#######
Coastal
4
0
0.0000
0.000
0.000
5
0
0.0000
0.000
0.000
6
0
0.0000
0.000
0.000
7
0
0.0000
0.000
0.000
8
0
0.0000
0.000
0.000
9
0
0.0000
0.000
0.000
10
0
0.0000
0.000
0.000
11
0
0.0000
0.000
0.000
12
TOTALS:
8,922
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.0410
0.0372
0.1517
1.5168
0.0489
0.0036
0.0372
0.0803
0.0372
7.6475
31.482
66.237
0.000
Date
lbs/ac
Current Cumulative lbs/ac
0.5901 0.4705 12.6470 4.5549 0.7611 0.0455 0.616 0.7574 0.6139 51.1701
0.5491 0.4333 12.4953 3.0381 0.7122 0.0419 0.579 0.6771 0.5766 43.5226
36 34 1,338 267 15 374 89 2,498
1 299
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.***
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
1/25/23
*Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of Land Applier Date **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
* * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the
same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DEN FORM FSF (5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Brunswick County Total Dry Tons Applied (Annual): 21.67
Permit #: WQ0034513 Predominant Soil Series: Goldsboro-GoA
Operator: Harvey Bell Owner: Joyce Brown
Acres Used: 10.20 Acres Permitted: 10.20 Site #: NC-BR-HB Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
. •
0. -
©
0
0
0
M
ED
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
H
1
2
3
_41
51
61
71
8
9
191
11
12
CD
O
.�
o
2.1243
Arsenic
0.0000
0.0000
0.0000
0.0410
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0410
Cadmium
0.0000
0.0000
0.0000
0.0372
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0372
Chromiuni
0.0000
0.0000
0.0000
0.1517
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.1517
Copper
0.0000
0.0000
0.0000
1.5168
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
1.5168
Lead
0.0000
0.0000
0.0000
0.0489
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0489
Mercury
1 0.0000
0.0000
1 0.0000
0.0036
0.0000
1 0.0000
0.0000
1 0.0000
0.0000
0.0000
0.0000
0.0000
0.0036
Molyb-
0.0000
0.0000
0.0000
0.0372
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0372
denum
Nickel
0.0000
0.0000
0.0000
0.0803
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0803
Selenium
0.0000
0.0000
0.0000
0.0372
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0372
Zinc
0.0000
0.0000
0.0000
7.6475
0.0000
0.0000
0.0000
0.0000
0.0000
0.00001
0.0000
0.0000
7.6475
Total
Phos-
0.0000
0.0000
0.0000
31.4821
0.0000
0.0000
0.000
0.0000
0.0000
0.0000
0.0000
0.0000
31.482
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibili y of fines and imprisonment for knowing violations"
1/25/23
Signature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM FSF (5/2003)

SECTION V
LAB SHEETS

BRUNSWICK COUNTY
LAND APPLICATION PROGRAM
BIOSOLIDS ANALYSIS
Residual Type: Wastewater Treatment Plant (Class B)
Date Sampled: January 25, 2022
Date Reported: February 17, 2022
West Brunswick Regional WWTP Permit No. WQ0034513
Mineralization Rate 0.30 5.71 % Solids Class B
11.78 pH
Parameter
F %
Mg/Kg Dry Weight
(% x 10.000)
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
3.470
34,700.000
69.400
Phosphorus
0.741
7,410.000
14.820
Potassium
0.398
3,980.000
7.960
PAN (injected)*
2.854
28,540.350
57.081
PAN (surface)*
1.559
15,590.350
31.181
Ammonia Nitrogen
2.590
25,900.000
51.800
Calcium
17.400
174,000.000
348.000
Calcium Carbonate Eq.
---
___
---
Magnesium
---
4,570.000
9.140
Sodium
---
1,820.000
3.640
Sulfur
--_
___
Nitrate N / Nitrite N
---
0.350
0.001
Barium
---
---
SAR
Chloride
___
___
0.28
Iron
---
---
---
Ceiling Concen.
Aluminum
---
20,200.00
40.400
(Mg/Kg)
Arsenic
---
9.65
0.019
75
Cadmium
---
8.76
0.018
85
Chromium
---
35.70
0.071
---
Copper
---
357.00
0.714
4,300
Lead
---
11.50
0.023
840
Mercury
---
0.856
0.002
57
Molybdenum
---
8.76
0.018
75
Nickel
---
18.90
0.038
420
Selenium
---
8.76
0.018
100
Zinc
---
1,800.00
3.600
7,500
Envirochem: 2022-01396
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

r_ -7 Environmental Chemists, Inc.
envirochem6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
sM, 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Brunswick County Public Utilities
Date of Report: Feb 17, 2022
Post Office Box 249
Customer PO #:
Bolivia NC 28422
Customer ID: 08100011
Attention:
Report #: 2022-01396
Project ID: WEIR WWTP Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-03351 Site: WEIR - Sludge
1/25/2022 9:40 AM Solid/Sludge Blake Ellis
Test
Method
Results Date
Analyzed
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4,1994
20200 mg/kg
01/26/2022
Arsenic
EPA 2D0.7, Rev 4,4,1994
9.65 mg/kg
01/26/2022
Cadmium
EPA 200.7, Rev, 4.4, 1994
<8.76 mg/kg
01/26/2022
Calcium
EPA 200.7, Rev 4.4,1994
174000 mg/kg
01/26/2022
Chromium
EPA 200.7, Rev, 4.4, 1994
35.7 mg/kg
01/26/2022
Copper
EPA 200.7, Rev, 4.4, 1994
357 mg/kg
01/26/2022
Lead
EPA 200.7, Rev 4.4, 1994
11.5 mg/kg
01/26/2022
Magnesium
EPA 200.7, Rev 44, 1994
4570 mg/kg
01/26/2022
Molybdenum
EPA 200.7, Rev 4 4.1994
<8.76 mg/kg
01/26/2022
Nickel
EPA 200.7, Rev 4 4, 1994
18.9 mg/kg
01/26/2022
Potassium
EPA 200.7, Rev. 44, 1994
3980 mg/kg
01/31/2022
Selenium
EPA 200.7, Rev. 4 4, 1994
<8.76 mg/kg
01/26/2022
Sodium
EPA 200,7, Rev.4A, 1994
1820 mg/kg
01/31/2022
Zinc
EPA 200.7, Rev. 4 4. 1994
1800mg/kg
01/26/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2
<0.35 mg/kg
02/03/2022
Total Solids (%)
SM 2540 B
5,71 %
01/26/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
25900 mg/kg
01/27/2022
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
34700 mg/kg
01/27/2022
Total Phosphorous
SM 4500 P (F-H)-2011
7410 mg/kg
02/01/2022
pH
Result estimated. Analyzed out of 15 minutes
SW 846 Method 9045D
hold time.
11,78 units
02/16/2022
Mercury
SW-8467471 B
0.856 mg/kg
01/28/2022
Comment: Sludge residual results
reported on a dry weight basis,
i %`'
Reviewed by. -
Report #:: 2022-01396
Page 1 of 1

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client: QP LA Date: � Report NumberQa �� 37
bSM]U
t of sample: ECHEM Pickup Client Delivery ❑ UPS ❑ FedEx O Other O
N/A Were custody seals present on the cooler?
N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt "C
How temperature taken: ❑ Temperature Blank V Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
❑ YES ❑ NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
V( YES ❑ NO 4 Were ro or— t d
YES
❑
NO
p p s o y procedures (relinquished/received) followed?
5.
Were sample ID's listed on the COC?
YES
❑
NO
6. Were samples ID's listed on sample containers?
$( YES
❑
NO
7. Were collection date and time listed on the COC?
YES
❑
NO
8. Were tests to be performed listed on the COC?
YES
❑
NO
9. Did samples arrive in proper containers for each test?
YES
❑
NO
10. Did samples arrive in good condition for each test?
-0 YES
❑
NO
11. Was adequate sample volume available?'
YES
❑
NO
12. Were samples received within proper holding time for requested tests?
❑ YES
❑
NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑
NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑
NO
15. Were sulfide samples received at a pH >97
❑ YES
❑
NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES
❑
NO
17, Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
I0
NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): HZS04 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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re"nvirochem'
ANALYTICAL & CONSULTING CHEMISTS
Brunswick County Public Utilities
Post Office Box 249
Bolivia NC 28422
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Jan 26, 2022
Customer PO #:
Customer ID: 08100011
Report #: 2022-00351
Project ID: WBR WWTP Sludge
Lab ID Sample ID:
22-00892 Site: Sludge
Test
Collect Date/Time
1/6/2022 7:36 AM
Method
Matrix
Solid/Sludge
Results
Sampled by
Joshua Cavenaugh
Date Analyzed
Chlordane (TCLP)
SW-846 8081 B
<0.02 mg/L
01/12/2022
Endrin (TCLP)
SW-846 8081 B
<0.0005 mg/L
01/12/2022
Heptachlor (TCLP)
SW-8468081 B
<0.0005mg/L
01/12/2022
Heptachlor epoxide (TCLP)
SW-846 8081 B
<0.0005 mg/L
01/12/2022
Lindane (TCLP)
SW-8468081 B
<0.0005mg/L
01/12/2022
Methoxychlor (TCLP)
SW-846 5081 B
<0.0005 mg/L
01/12/2022
Toxaphene (TCLP)
SW-846 8081 B
<0.05 mg/L
01/12/2022
2,4,5-TP (TCLP)
SW-8468151 A
<0.003mg/L
01/11/2022
2,4-D (TCLP)
SW-846 8151 A
<0.003 mg/L
01/11/2022
1,4-Dichlorobenzene (TCLP)
SW-8468270E
<0.050mg/L
01/11/2022
2,4,5-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
01/11/2022
2,4,6-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
01/11/2022
2,4-Dinitrotoluene(TCLP)
SW-8468270E
<0.050mg/L
01/11/2022
Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
01/11/2022
Hexachlore-1,3-butadiene(TCLP)
SW-8468270E
<0.050mg/L
01/11/2022
Hexachlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
01/11/2022
Hexachloroethane (TCLP)
SW-8468270E
<0.050mg/L
01/11/2022
m + p-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
01/11/2022
Nitrobenzene (TCLP)
SW-8468270E
<0.050mg/L
01/11/2022
o-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
01/11/2022
Pentachlorophenol (TCLP)
SW-8468270E
<0.250mg/L
01/11/2022
Pyridine (TCLP)
SW-846 8270 E
<0.050 mg/L
01/11/2022
1,1-Dichloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/19/2022
1,2-Dichloroethane (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/19/2022
Benzene (TCLP)
SW-846 Method 82601D
<0.01 mg/L
01/19/2022
Carbon Tetrachloride (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/19/2022
Report #., 2022.00351
Page 1 of 4

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 & 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 0 910.347.5843 Lab/Fax
info(genvironmentalchemists.com
Brunswick County Public Utilities
Date of Report: Jan 26, 2022
Post Office Box 249
Customer PO #:
Bolivia NC
28422
Customer ID: 08100011
Attention:
Report #: 2022-00351
Project ID: WBR WWTP Sludge
Chlorobenzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/19/2022
Chloroform (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/19/2022
Methyl ethyl ketone (TCLP)
SW-846 Method 8260D
<0.05 mg/L
Tetrachloroethylene (TCLP)
SW-846 Method 82600
<0.01 mg/L
01/19/2022
01/19/2022
Trichloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/19/2022
Vinyl Chloride (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/19/2022
RCI
Cyanide
SM 4500 CN D
<1.0 mg/kg
01/11/2022
Sulfide
SM 4500 S D
0.21 mg/kg
01/21/2022
Ignitability
SW 846 method 1010
>158 `F
01/14/2022
pH SW 846 Method 9045D
Result estimated. Analyzed out of 15 minutes hold time.
8.25 units
01/24/2022
dge Residuals
Alumin
EPA 200 7, Rev. 4A. 1994
25 0 m kg
01/11/2
Arsenic
EPA 200 7, Rev. 4.4, 1994
<1
.9 m kg
/2022
Cadmium
EPA 2007, Rev. 4.4, 1994
<1
.9 m /kg
01/11/2022
Calcium
EPA 2007, Rev 4.4, 1994
28
Q0 rn /kg
01/11/2022
Chromium
EPA 200.7, Rev 4.4, 1994
3
.5 g
01/11/2022
Copper
00.7,Rev, 4.4.1994
6m /kg
01/11/2022
Lead
EPA 200.7, 4.4, 1994
<1
.9 m /kg
01/11/2022
Magnesium
EPA 200.7, Rev, 4A, 4
5
0 m /kg
01/11/2022
Molybdenum
EPA 200.7,Rev, 4.4,1994
<1
.9m /kg
01/11/2022
Nickel
EPA 200.7,Rev, , 994
2
.6m /kg
01/11/2022
Potassium
EPA , ev 4.4, 1994
7
0m /kg
01/11/2022
Selenium
PA 2003. Rev., 4.4, 1994
rn /kg
01/11/2022
Sodium
EPA 200.7. Rev 4.4, 1994
3
0
m
01/11/2022
Zinc
EPA 200 7, Rev 4.4, 1994
1
0 m /kg
01/11/2022
Nitrate+Nitrit rogen
EPA 353.2
8 n1 /kg
01/07/2022
Total ds (%)
SM 2540 8
3
8
7l2022
monia Nitrogen
SM 4500 NH3 C-2011
45
0 m /kg
01/10/
Report # 2022-00351
Page 2 of 4

Environmental Chemists, Inc.
1 1 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
sM; 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Brunswick County Public Utilities Date of Report: Jan 26, 2022
Post Office Box 249 Customer PO #:
Bolivia NC 28422 Customer ID: 08100011
Attention: Report #: 2022-00351
Project ID: WBR WWTP Sludge
Furc I KN)
SM 4500 Norg B-2011
85 00 g/k
Total Phosphorous
42 0 g/kg 01/11/2022
SW-846 7471 B
0. 11 g/kg
TCLP Metals
Arsenic
EPA 200.7, Rev, 4.4, 1994
<1 mg/L
01/14/2022
Barium
EPA 200.7,Rev, 4A.1994
<1 mg/L
01/14/2022
Cadmium
EPA 200.7, Rev. 4.4,1994
<1 mg/L
01/14/2022
Chromium
EPA 200.7,Rev 4.4.1994
<1 mg/L
01/14/2022
Lead
EPA 200.7, Rev. 4.4, 1994
<1 mg/L
01/14/2022
Selenium
EPA 200.7, Rev. 4 4, 1994
<1 mg/L
01/14/2022
Silver
EPA 200.7, Rev. 4.A. 1994
<1 mg/L
01/14/2022
Mercury
EPA 245.1
<0.0002 mg/L
01/14/2022
Lab ID Sample ID:
Collect Date/Time
Matrix
Sampled by
22-00893 Site: 1
1/6/2022 7:37 AM
Solid/Sludge
Joshua Cavenaugh
Test
Method
Results
Date Analyzed
Total Solids (%)
SM 2540 B
3.11 %
01/07/2022
Fecal Density
SM 9221C E-2014
15 MPN/g
01/06/2022
Lab ID Sample ID:
Collect Date/Time
Matrix
Sampled by
22-00894 Site: 2
1/6/2022 7:38 AM
Solid/Sludge
Joshua Cavenaugh
Test
Method
_Results
Date Analyzed
Total Solids (%)
SM 2540 B
3.36 %
01/07/2022
Fecal Density
SM 9221C E-2014
<6 MPN/g
01/06/2022
Lab ID Sample ID:
Collect Date/Time
Matrix
Sampled by
22-00895 Site: 3
1/6/2022 7:39 AM
Solid/Sludge
Joshua Cavenaugh
Test
Method
Results
Date Analyzed
Total Solids
SM 2540 B
3.44
01/07/2022
Fecal Density
SM 9221C E-2014
<6 MPN/
9
01/06/2022
Report # 2022-00351
Page 3 of 4

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
info(iz;environmentalchemists.com
Brunswick County Public Utilities Date of Report: Jan 26, 2022
Post Office Box 249 Customer PO #:
Bolivia NC 28422 Customer ID: 08100011
Attention: Report #: 2022-00351
Project ID: WBR WWTP Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-00896 Site: 4 1/6/2022 7:40 AM Solid/Sludge Joshua Cavenaugh
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
Lab ID Sample ID:
22-00897 Site:5
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
22-00898 Site:6
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
22-00899 Site:7
Test
SM 2540 B
SM 9221C E-2014
3.38 % 01/07/2022
<6 MPN/g 01/06/2022
Collect Date/Time Matrix Sampled by
1/6/2022 7:41 AM Solid/Sludge Joshua Cavenaugh
Method Results Date Analyzed
SM 2540 B
SM 9221C E-2014
Collect Date/Time
1/6/2022 7:42 AM
Method
SM 2540 B
SM 9221C E-2014
Method
Collect Date/Time
1/6/2022 7:43 AM
Total Solids (%) SM 2540 B
Fecal Density SM 9221 C E-2014
Comment: Sludge residuals on a dry weight basis.
Reviewed by:
3.44 % 01/07/2022
<6 MPN/g 01/06/2022
Matrix Sampled by
Solid/Sludge Joshua Cavenaugh
Results Date Analyzed
3.51 % 01/07/2022
<6 MPN/g 01/06/2022
Matrix Sampled by
Solid/Sludge Joshua Cavenaugh
Results Date Analyzed
3.43 % 01/07/2022
<6 MPN/g 01/06/2022
Report #_ 2022-00351
Page 4 of 4

Environmental Chemist, Inc., Wilmington, INC Lab #94
6602 Windmill Way
Wilmington, NC 28405
Sample Receipt Checklist 910.392.0223
J6
Client: e) Date: oC� Report Number.QA 3 SI
Receipt f sample:
❑ YES ❑ NO
ECHEM Pickup Client Delivery ❑ UPS ❑ FeclEx ❑ Other ❑
❑
N/A Were custody seals present on the cooler?
YES ❑ NO
12 N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt .p °CI Ck,, Corrected temperature upon receipt ° C
How temperature taken:
❑ Temperature Blank k? Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
❑ YES ❑ NO
YES ❑
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
NO
4. Were proper custody procedures (relinquished/received) followed?
YES ❑ NO
5. Were sample ID's listed on the COC?
YES ❑ NO
6. Were samples ID's listed on sample containers?
YES ❑ NO
7. Were collection date and time listed on the COC?
YES ❑ NO
8. Were tests to be performed listed on the COC?
YES ❑ NO
9. Did samples arrive in proper containers for each test?
YES ❑ NO
10. Did samples arrive in good condition for each test?
YES ❑ NO
11. Was adequate sample volume available?'
YES ❑ NO
12. Were samples received within proper holding time for requested tests?
❑ YES ❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ YES ❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES ❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES ❑ NO
❑
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
YES ❑ NO
❑
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
YES ❑ NO
118. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked
at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked
for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation:
(Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s)
by adding (circle one):
were received incorrectly preserved and were adjusted accordingly
H25O4
HNO3 HCI NaOH
Time of preservation:
If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s)
were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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