WQ0006245_2022 Residual Annual Report_20230206 (2)

Initial Review
Reviewer
Thornburg, Nathaniel D
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * WQ0006245
Applicant/Permittee City of Statesville
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Mooresville
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Ken Galloway
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
7048783438
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0006245
Has Current Existing permit number
Applicant/Permittee Address*
PO Box 1111 Statesville, NC 28687
Facility Name*
City of Statesville Class A Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Sta-Lime 2022.pdf 31.54MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
04;;C6r
Submission Date 2/6/2023

Waypoint.0
ANALYTICAL
1/19/2023
City of Statesville, NC
Ken Galloway
693 Bell Farm Road
Statesville, NC, 28625
Ref: Analytical Testing
Lab Report Number: 23-004-0012
Client Project Description: Quarterly Stalime
Dear Ken Galloway:
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Waypoint Analytical, LLC (Charlotte) received sample(s) on 1/4/2023 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Terri W Cole
Laboratory Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 17

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State
Program
Lab ID
Expiration Date
North Carolina
State Program
37735
07/31/2023
North Carolina
State Program
402
12/31/2023
South Carolina
State Program
99012
07/31/2023
South Carolina
State Program
99012
12,'31/2022
Page 1 of 1 00016,23-004-0012
Page 2 of 17

(2)
Waypoint 449 Springbrook Rd, Charlotte, NC 28217
Main 704,529.6364
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-004-0012
Client Project Description: Quarterly Stalime
Lab No
Client Sample ID
Matrix
Date Collected
Date Received Method Lab ID
96772
STA-Lime
Solids
01/04/202312:13
01/04/2023 13:36
96712
STA-Lime
Solids
01/04/202312:13
01/04/2023 13:36 6010D AES
96773
STA-Lime 1
Solids
01/04/2023 12:15
01/04/2023 13:36
96773
STA-Lime 1
Solids
01/04/2023 12:15
01/04/2023 13:36 350.1 AES
AES: Analytical Environmental Services, Inc., Atlanta, GA
Page 3 of 17

Waypointo
ANALYTICAL
Client: City of Statesville, NC
Project: Quarterly Stalime
Lab Report Number: 23-004-0012
Date: 1 /19/2023
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
CASE NARRATIVE
Nickel and ammonia subcontracted to Analytical Environmental Services lab ID #562.
Page 4 of 17

Waypoint,(2)
ANALYTICAL
01050
City of Statesville, NC Project
Ken Galloway
693 Bell Farm Road Information
Statesville , NC 28625
Report Number : 23-004-0012
Lab No : 96772
Sample ID : STA-Lime
449 Springbrook Rd, Charlotte, NC 28217
Maln 704.529.6364
www,waypointanalytical.com
Quarterly Stalime
REPORT OPANAL PSIS
Report Date : 01/19/2023
Received : 01/04/2023
60WLQ'&
Terri W Cole
Laboratory Project Manager
Matrix: Solids
Sampled: 1/4/ 2023 12:13
Test Results Units MOL DI= Date / Time By Analytical
Analyzed Method
Moisture 12.3 %
Nickel See attached mg/L
Qualifiers/ DF Dilution Factor
Definitions
1 01/04/2317:44 AMB SW-DRYWT
0.005 1 BKN 6010D
MQL Method Quantitation Limit
Page 5 of 17

Mai
NC 217
Waypoien 0 AA9 Springbrook Rd, Charlotte,Main7aa.5.529.b3643sa
ANALYTICAL www.waypointanalytical.com
01050
City of Statesville, NC Project Quarterly Stalime
Ken Galloway Report Date : 01/19/2023
693 Bell Farm Road information : Received : 01/04/2023
Statesville , NC 28625 /jAqU) /,.,o
Terri W Cole
Report Number :23-004-0012 REPORT OFANALrSIS Laboratory Project Manager
Lab No : 96773 Matrix: solids
Sample ID: STA-Lime 1 Sampled: 1/4/2023 12:15
Test Results Units MQL DF Date !Time By Analytical
Analyzed Method
Moisture 23.6
Ammonia Nitrogen See attached
Qualifiers/ DF Dilution Factor
Definitions
1 01/04/2317:44 AMB SW-DRYWT
1 350.1
MQL Method Quantitation Limit
Page 6 of 17

0 Ac ass
t � - o ANALWICAL, INC,
ANALYTICAL REPORT
CLIENT
Waypoint Analytical, LLC (Charlotte)
449 Springbrook Road
Charlotte NC 28217
ATTENTION
Terri W Cole
PROJECT ID
23-004-0012
LABORATORY REPORT NUAIBER
2301679
DATE
January 17, 2023
Primate Data Review By Secondary Data Review By
/ a
Ashley Amick
Chris Pafford
Project Manager, Access Analytical
Project Manager, AES [e-mail]
PLEASE NOTE.
Unless othem ise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc),
3080 Presidential Drive, Atlanta, GA 30340.
AES is SCDHEC certified laboratory # 98016, NCDEN I certified lab # 562, GA certified lab # EL-E87582,
NELAP certified laboratory # E87582
AIHA-LAP,LLC Laboratory ID:100671 for Industrial Hy-bicne samples (Organics, Metals, PCNI Asbestos,
Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fingal)
Direct Examination.
Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a
representative ofAES serving client in the SC/NC/GA areas. All questions regarding this report should be directed
to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243
Page 7 of 17 Page 1 of 9

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Analytical Environmental Services, Inc
Date: 17-Jan-23
Client: Waypoint Analytical, LLC (Charlotte)
Project: 23-004-0012
Case Narrative
Lab ID, 2301679
Total nickel leas analyzed per Angela Martin via email Ot-10-23 for requested "fCP Metals Analysis."
Page 9 of 17 Page 3 of 9

Analytical Environmental Services, Inc
Date: 17-Jan-23
Client:
%typoint Analytical, LLC (Charlotte)
Client Sample ID:
96772
Lab Order
2301679
"fag Number:
STA-Lime
Project Name:
23-004-0012
Collection Date:
1/4.12023 12:13:00 PM
Lab ID:
2301679-OOIA
Matrix:
Solid
Analyses Result Qual 11IDL Reporting Units RatchlD DF Date Analyzed Analyst
Limit
METALS, TOTAL SW601OD (SAV3050B)
Nickel 3.11 J 0.272 4.42 mgrlcg-dry 349297 1 01?12;202319:15 EO
PERCENT MOISTURE D2216
Percent Moisture 12.8 0 0 NN1% R505847 1 01/11/202300:00 AV
Qaaliriers: " Value exceeds maximum comaminant level
11Rt, Not Detected at Nil)],
n tloldin� time_ for pr.paraiion or—I,l ie exceeded
N Anal}le not NtLAC cenif-i
li Anat. to detected in the associated method blank
E fstimated wine shave quantitiien ranee
5 Spik,Racoven' emeide hmitsdue to maids
> G,r,,E r than Resole valor
1 Estiutated value detected belo, ttepening Limit
Less than Result came
Page 10 of 17
Page 4 of 9

Analytical Environmental Services, Inc
Date: 17-Jan-23
Client:
Waypoint Analytical, LLC (Charlotte)
Client Sample ID:
96773
Lab Order
2301679
Tag Number:
STA-Lime I
Project Name:
23-004-0012
Collection Date:
114,J2023 12:15:00 PM
Lab ID:
2301679-002A
Matrix:
Solid
Analyses Result Reporting
} Qual 11IllL Units I3atchlll DI' DateAnalyzed Analyst
Limit
Nitrogen, Ammonia (as N) Extractable E350.1 MOD (E350.1)
Nitrogen, Ammonia(As N)Extractable 206 6.37 12.9 mg:Kodry 349327 l 01/17/202311:07 7L
PERCENT MOISTURE D2216
Percent Moisture 23.4 0 0 tics% R505347 1 01/11/202300.00 JW
QnaliGrrs: ' 1'alue exceeds nmximum contaminant le,el L Fstfmated ,aloe above quant itation rune
6R1. Sot Detected at kIDL S Spike Recovery ontsidc limits due to matrix
fl holding tunes for preparnGon or anal. sis exceeded Crater 111111 Result slue
S Anal}u not SLL AC certified J Lstimated value detected bclmv Reporting limit
11 Atnlyle detected in the associated method blank < Less than Result value
Page 11 of 17
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End of Report
Page 15 of 17 Page 9 of 9

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 01050
Customer Name: City of Statesville, NC
Report Number: 23-004-0012
Shipping Method
Fed Ex 0 US Postal Lab
C UPS 0 Client Courier
`J Other:
Thermometer ID:
IIRT153.6C
Shipping container/cooler uncompromised?
C Yes
0 No
Number of coolers/boxes received
F 1
Custody seals intact on shipping container/cooler?
U Yes
U No
C Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
# Not Present
Chain of Custody (COC) present?
CYes
0 No
COC agrees with sample Iabel(s)?
0 Yes
Cj No
COC properly completed
C Yes
0 No
Samples in proper containers?
C Yes
0 No
Sample containers intact?
C Yes
0 No
Sufficient sample volume for indicated test(s)?
C Yes
0 No
All samples received within holding time?
C Yes
0 No
Cooler temperature in compliance?
C' Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
C Yes
0 No
Water - Sample containers properly preserved
Yes
�_ No
✓N/A
Water - VOA vials free of headspace
Yes
0 No
C NIA
Trip Blanks received with VOAs
0 Yes
0 No
C NIA
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
C NIA
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
[_ Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments:
0 Yes
CO No
1
Signature: Angelo Norvell _ Date & Time: 01/04/2023 14:31:31
Page 16 of 17

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Page 17 of 17

Waypoint.(D
ANALYTICAL
3/15/2022
City of Statesville, NC
Ken Galloway
693 Bell Farm Road
Statesville, NC, 28625
Ref: Analytical Testing
Lab Report Number: 22-059-0027
Client Project Description: Quarterly Sta-Lime
Dear Ken Galloway:
449 Springbrook Rd, Charlotte, NC 28217
Main 704.S29.6364
www.waypointanalytical.corn
Waypoint Analytical, LLC (Charlotte) received sample(s) on 2/28/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USFPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Terri W Cale
Laboratory Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 22

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytica l.corn
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State
Program
Lab ID
Expiration Date
North Carolina
State Program
37735
07/31/2022
North Carolina
State Program
402
12/31/2022
South Carolina
State Program
99012
07/31/2022
South Carolina
State Program
99012
12/31/2022
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2023
Arkansas
State Program
88-0650
02/07/2023
California
State Program
2904
06/30/2022
Florida
State Program
- NELAP
E871157
06/30/2022
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2022
Illinois
State Program
- NELAP
200078
10/10/2022
Kentucky
State Program
80215
06/30/2022
Kentucky
State Program
KY90047
12/31/2022
Louisiana
State Program - NELAP
LA037
12/31/2022
Louisiana
State Program
- NELAP
04015
06/30/2022
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
415
12/31/2022
Pennsylvania
State Program
- NELAP
68-03195
05/31/2022
South Carolina
State Program
84002
06/30/2022
South Carolina
State Program
84002
06/30/2022
Tennessee
State Program
02027
02/11/2023
Texas
State Program -
NELAP
T104704180
09/30/2022
Virginia
State Program
00106
06/30/2022
Virginia
State Program -
NELAP
460181
09/14/2022
Page 1 of 1 00016/22-059-0027
Page 2 of 22

Waypoin(Dt�
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytfcal.com
Sample Summary Table
Report Number: 22-059-0027
Client Project Description: Quarterly Sta-Lime
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
94994
Stalime 1
Solids
02/28/2022 12:00
02/28/2022 13:09
94995
Stalime 2
Solids
02/28/2022 12:00
02/28/2022 13:09
94996
Stalime 3
Solids
02/28/2022 12:00
02/28/2022 13:09
94997
Stalime 4
Solids
02/28/2022 12:00
02/28/2022 13:09
94998
Stalime 5
Solids
02/28/2022 12:00
02/28/2022 13:09
94999
Stalime 6
Solids
02/28/2022 12:00
02/28/2022 13:09
95000
Stalime 7
Solids
02/28/2022 12:00
02/28/2022 13:09
95001
Stalime
Solids
02/28/2022 12:00
02/28/2022 13:09
9S001
Stalime
Solids
02/28/2022 12:00
02/28/2022 13:09
350.1
AES
95001
Stalime
Solids
02/28/2022 12:00
02/28/2022 13:09
6010D
WP MTN
95001
Stalime
Solids
02/28/2022 12:00
02/28/2022 13:09
4500NO3F-2011
WP MTN
95001
Stalime
Solids
02/28/2022 12:00
02/28/2022 13:09
4500NORGD-2011
WP MTN
95280
Stalime
Solids
02/28/2022 12:00
02/28/2022 13:09
AES: Analytical Environmental Services, Inc., Atlanta, GA
WP MTN - Memphis, TN: Waypoint Analytical -TN, Memphis, TN
Page 3 of 22

Waypoint-(D
ANALYTICAL
Client: City of Statesville, NC
Project: Quarterly Sta-Lime
Lab Report Number: 22-059-0027
Date: 3/15/2022
449 Springbrook Rd, Charlotte, NC 28217
Main 704,529.6364
www.waypointanalytical.com
CASE NARRATIVE
Ammonia was subcontracted to Analytical Environmental Services.
Metals Analysis Method 6010D
Sample 56918 (BD-R2-C)
Analyte: Aluminum
QC Batch No: 1-60376411-603250
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 56918 (BD-R2-C)
Analyte: Selenium
QC Batch No: L603764/1-603250
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 95001 (StaLime)
QC Batch No: V15682/V15646
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Sample 95239 (2/28-312 Gypsum Composite)
Analyte: Potassium
QC Batch No: V156821V15646
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 95239 (2128-3/2 Gypsum Composite)
Analyte: Lead
QC Batch No: V15682/V15646
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected,
Solids Total Mercury Analysis - CVAA Method 7471 B
Analyte: Mercury
QC Batch No: V15596/V15551
ICV failed high. Sample concentration BRL. Results not affected.
SAR = [ 2.25 ] / SQRT { ( [52.4] + [<0.083]) 12 }
SAR =[2.251/SORT {(52.4])12}
SAR =[2.251/SORT {26.2}
SAR =[2.25]15.12
SAR = 0.439
Page 4 of 22

Waypoint.(2)
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates taking the
square root of the operand in parentheses.
PAN Equation = 0.3 * (TKN-Ammonia) + 0.5 * (Ammonia) + Nitrate -Nitrite
PAN = 0.3 x (5230-97.5) + .05 * (97.5) + 15.4
PAN = 1560.025 mg/kg
Page 5 of 22

•
Waypoint
449 5pringbrook Rd, Ch
Charlotte, NC 28217
Main 704.529.6164
ANALYTICAL
www.waypointanalytical.com
01050
City of Statesville, NC
Project
Quarterly Sta-Lime
Ken Galloway
Report Date : 03/15/2022
693 Bell Farm Road
Information
: Received: 02/28/2022
Statesville, NC 28625
6OW
�Terri
W Cole
Report Number :22-059-0027
REPORTOFANALY5I5
Laboratory Project Manager
Lab No : 94994
Matrix: Solids
Sample ID : Stalime 1
Sampled: 2/28/2022 12:00
Test
Results
Units MQL DF Dale / Time By Analytical
Analyzed Method
Fecal Coliform MPN/g
Q.0
MPN/g 2.0 1 02/28/22 14:20 SMW 9221E-2011
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 6 of 22

r
Waypoint
Charlotte, NC 28217
449 Springbrook Rd, Ch
Main 704.529.6364
ANALYTICAL
www.waypointanalytical.com
01050
City of Statesville, NC
Project
Quarterly Sta-Lime
Ken Galloway
Report Date : 03/15/2022
693 Bell Farm Road
Information :
Received : 02/28/2022
Statesville , NC 28625
jigW�
Terri W Cole
Report Number :22-059-0027
REPOR T OFANAL YSIS
Laboratory Project Manager
Lab No : 94995
Matrix: Solids
Sample ID : Stalime 2
Sampled: 2/28/2022 12.00
Test
Results
Units Mal-
DF Date / Time By Analytical
Analyzed Method
Fecal Coliform MPN/g
<2.4
MPN/g - dry 2.4
1 02/28/22 14:20 SMW 9221E-2011
Moisture
18.5
%
1 03/03/2210:30 SJL SW-DRYWT
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 7 of 22

Waypointo
ANALYTICAL
01050
City of Statesville, NC Project
Ken Galloway
693 Bell Farm Road Information
Statesville , NC 28625
Report Number : 22-059-0027
Lab No : 94996
Sample ID : Stalime 3
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypolntanalytical,com
Quarterly Sta-Lime
REPORT OFANAL Y5I5
Report Date : 03/15/2022
Received : 02/28/2022
UJUJ
Terri W Cole
Laboratory Project Manager
Matrix: Solids
Sampled: 2/ 28/ 2022 12:00
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Fecal Coliform MPN/g <2.2 MPN/g - dry
Moisture 12.3 %
Qualifiers/ DF Dilution Factor
Definitions
2.2 1 02/28/2214:20 SMW 9221E-2011
1 03/03/2210:30 S]L SW-DRYWT
MQL Method Quantitation Limit
Page 8 of 22

wavDoint,(D
ANALYTICAL
01050
City of Statesville, NC
Ken Galloway
693 Bell Farm Road
Statesville , NC 28625
Report Number:22-059-0027
Lab No : 94997
Sample ID : Stalime 4
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Project Quarterly Sta-Lime
Information :
REPORT OF ANALYSIS
Report Date : 03/15/2022
Received ; 02/28/2022
JOW
Terri W Cole
Laboratory Project Manager
Matrix: Solids
Sampled: 2/28/2022 12:00
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Fecal Coliform MPN/g <2.2 MPN/g - dry
Moisture 12.3 %
Qualifiers/ DF Dilution Factor
Definitions
2.2 1 02/28/22 14:20 SMW 9221E-2011
1 03/03/2210:30 SJL SW-DRYWT
MQL Method Quantitation Limit
Page 9 of 22

•
Waypoint, 449 5pringbrooic Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.corn
01050
City of Statesville, NC Project Quarterly Sta-Lime
Ken Galloway Report Date : 03/15/2022
693 Bell Farm Road Information : Received: 02/28/2022
Statesville, NC 28625 jigU14
Terri W Cole
Report Number :22-059-0027 REPORT OFANAL YSIS
Laboratory Project Manager
Lab No : 94998 Matrix: Solids
Sample ID : Stalime 5 Sampled: 2/28/2022 12:00
Test Results Units MQL DF Date 1 Time By Analytical
Analyzed Method
Fecal Coliform MPN/g <2.2 MPN/g - dry 2.2 1 02/28/22 14:20 SMW 9221E-2011
Moisture 12.8 % 1 03/03/2210:30 SJL SW-DRYWT
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 10 of 22

a
Waypoint
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL
www.waypointanalytical.com
01050
City of Statesville, NC
Project
Quarterly Sta-Lime
Ken Galloway
Report Date : 03/15/2022
693 Bell Farm Road
Information :
Received : 02/28/2022
Statesville , NC 28625
6OW
�Terri
W Cole
Report Number :22-059-0027
REPOR T OFANAL rSIS
Laboratory Project Manager
Lab No : 94999
Matrix: Solids
Sample ID : Stalime 6
Sampled: 2/28/2022 12:00
Test
Results
Units MQL
DF Date/Time By Analytical
Analyzed Method
Fecal Coliform MPN/g
<2.2
MPN/g - dry 2.2
1 02/28/22 14:20 SMW 9221E-2011
Moisture
11.8
%
1 03/03/2210:30 S31- SW-DRYWF
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 11 of 22

Waypoint, (2) 449 Springbroak Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL WWW.Waypointanalytical.com
01050
City of Statesville, NC Project Quarterly Sta-Lime
Ken Galloway Report Date : 03/15/2022
693 Bell Farm Road Information : Received : 02/28/2022
Statesville , NC 28625 VIA
Report Number :22-059 0027 REPpRTRPANALYSIS Terri W ColeLaboratory Project Manager
Lab No : 95000 Matrix: Solids
Sample ID : Stalime 7 Sampled: 2/28/2022 12:00
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Fecal Coliform h]PN/g
<2.0 MPN/g 2.0 1 02/28/2214:20 SMW 9221E-2011
Qualifiers/ OF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 12 of 22

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Maln 704.529.6364
www.wa ypo i nta n a lyt i c a l. c o m
01050
City of Statesville, NC Project Quarterly Sta-Lime
Ken Galloway Report Date : 03/15/2022
693 Bell Farm Road Information : Received : 02/28/2022
Statesville , NC 28625 619W�
Terri W Cole
Report Number :22-059-0027 REPORTOFANALYSIS
Laboratory Project Manager
Lab No : 95001 Matrix: Solids
Sample ID : StaLime Sampled: 2/28/2022 12:00
Test
Results
Units
MQL
DF
Date ITime
Analyzed
By
Analytical
Method
Moisture
33.1
°7Q
1
03/01/22 09:53
SJL
SW-DRYWT
Ammonia Nitrogen
97.5
mg/Kg AR
1
03/12/22 14:54
350.1
Nitrate+Nitrite-N
15.4
mg/Kg - dry
7.38
1
03/08/22 14:33
ZBD
4500NO3F-2011
Total Solids
67.2
%
0.010
1
03/01/22 09:53
SJL
254OG-2011
Total Kjeldahl Nitrogen
5230
mg/Kg - dry
166
1
03/09/22 15:53
CLP
4500NORGD-2011
Phosphorus
3170
mg/Kg - dry
7.47
1
03/09/22 02:18
TIS
6010D
Aluminum
12900
mg/Kg - dry
74.7
10
03/04/22 12:03
EDV
6010D
Arsenic
11.7
mg/Kg - dry
7.47
10
03/04/22 12:03
EDV
6010D
Cadmium
<1.49
mg/Kg - dry
1.49
10
03/04/22 12:03
EDV
6010D
Copper
79.8
m9/K9 - dry
3.74
10
03/04/22 12:03
EDV
6010D
Lead
9.69
rnglKg - dry
4.48
10
03/04/22 12:03
FDV
6010D
Mercury (Total)
<0.0448
mg/Kg - dry
0.0448
1
03/02/22 17:16
EDV
7471E
Molybdenum
<7.47
mg/Kg - dry
7.47
10
03/04/22 12:03
EDV
6010D
Potassium
5310
mg/Kg - dry
374
10
03/04/22 12:03
EDV
6010D
Selenium
<7.47
mg/Kg - dry
7.47
10
03/04/22 12:03
EDV
6010D
Sodium
1210
mg/Kg - dry
747
10
03/04/22 12:03
EDV
6010D
Zinc
82.8
mg/Kg - dry
7,47
10
03/04/22 12:03
FDV
6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 13 of 22

(2)
Waypoint,
449 SprEngbrook
Rd, Charl2821
Main ln 707t)4.5.529.6364
ANALYTICAL
www.waypointanalytical.com
01050
City of Statesville, NC
Project
Quarterly
Sta-Lime
Ken Galloway
Report Date : 03/15/2022
693 Bell Farm Road
Information :
Received : 02/28/2022
Statesville , NC 28625
jig
Report Number : 22-059-0027
REPORT
Terri W ColeOFANALYSIS
Laboratory Project Manager
Lab No: 95280
Matrix: Solids
Sample ID: StaLlme
Sampled: 2/28/2022 12:00
Test
Results
Units
MQL
DF Date 1 Time By Analytical
Analyzed Method
Calcium (saturated paste)
52.4
meq/L
0.050
1 03/09/22 12:57 EDV Saturate Paste
Magnesium (saturated paste)
0.010
meq/L
0.083
1 03/09/22 12:57 EDV Saturate Paste
Sodium (saturated paste)
2.25
meq/L
0.043
1 03/09/22 12:57 EDV Saturate Paste
Sodium Absorption Ratio
0.439
1 03/09/22 12:57 EDV Saturate Paste
Moisture
52.7
%
1 03/03/2215:40 ]MC SW-DRYWT
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 14 of 22

Am ss
ANALYTICAL, INC.
ANALYTICAL REPORT
CLIENT
Waypoint Analytical
PO Box 240543
Charlotte NC 292240543
ATTENTION
Terri W Cole
PROJECT ID
22-059-0027
LABORATORY REPORT NUMBER
2203226
DATE
March 14, 2022
Primary Data Review By Secondary Data Review By
Chris Pafford
Project Manager, AES
PLEASE NOTE:
Ashley Amick
Project Manager, Access Analytical
[e-mail]
Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc),
3080 Presidential Drive, Atlanta, GA30340.
AES is SCDHEC certified laboratory # 98016, NCDEN'R certified lab # 562, GA certified lab # FL-E87582,
NELAP certified laboratory # E87582
- AIHA-LAP,LLC Laboratory ID:100671 for Industrial Hygiene samples (Organics, Metals, PCM Asbestos,
Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal)
Direct Examination.
Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a
representative ofAES serving client in the SC/NC/GA areas. All questions regarding this report should be directed
to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315,4243
Page 15 of 22 Page 1 of 6

Jr
G6
al d
a
X
V
E
0
�a
UI 9
U) 19 K
a
CD
m
a

Analytical Environmental Services, Inc
Date: 14-hfar-22
Client:
Waypoint Analytical
Client Sample ID:
95001
Lab Order
2203226
Tag Number:
StaLinle
Project Name:
22-059-0027
Collection Date:
2/28/2022 12:00:00 PM
Lab Ill:
2203226-00]A
Matrix:
Solid
Analyses Result Qual I%IDL Reporting Units BatchlD DF Date Analyzed Analyst
Limit
Nitrogen, Ammonia (as N) Extractable E350.1 NIOD (E350.1)
Nitrogen, Ammonia (As N) Extractable 97.5 6.30 12.8 mg/Kg-dry 332162 1 03112/2022 14:54 KV
PERCENT MOISTURE D2216
Percent Moisture 21.8 0 0 AN1% R479042 1 03/03/2022 00:00 Jw
Qualifiers: . Value exceeds maximum contaminant level L Estimated value above quantihation range
13RL Sot ❑eteoted al hIDL S Spike Recovery outside limits due to matrix
11 holding times for preparation or anahsis exceeded > Greater than Reside vah,e
S Analyte not KELAC certified J Estimated value detected below Reporting Limit
n Analyle detected in the associated method blank < Less than Result value
Page 17 of 22
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End of Report
Page 20 of 22 Page 6 of 6

0
Waypoint
ANALYTICAL
449 Springbrook Rd, Charlotte, NC. 28217
Main 704.529.6364
www.wayp oin to n a lyti ca I.co m
Shipment Receipt Form
Customer Number: 01050
Customer Name: City of Statesville, NC
Report Number: 22-059-0027
Shipping Method
0 Fed Ex 0 US Postal C Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
F_
IRT-15 1.7 C
Shipping container/cooler uncompromised?
C Yes
' } No
Number of coolers/boxes received
I '
Custody seals intact on shipping container/cooler?
0 Yes
0 No
C Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
C Not Present
Chain of Custody (COC) present?
(* Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
O Yes
0 No
Samples in proper containers?
C Yes
0 No
Sample containers intact?
CO- Yes
0 No
Sufficient sample volume for indicated test(s)?
C Yes
0 No
All samples received within holding time?
C Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
C Yes
0 No
Water - Sample containers properly preserved
Yes
0 No
C NIA
Water - VOA vials free of headspace
0 Yes
0 No
CO) NIA
Trip Blanks received with VOAs
0 Yes
0 No
C NIA
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
C NIA
F_ High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
[_ Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
C No
Comments
Signature: Zoe S. Vigilant Date & Time: 102/28/2022 13afi:14
Page 21 of 22

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Page 22 of 22

Waypointo
ANALYTICAL
3/22/2022
City of Statesville, NC
Ken Galloway
693 Bell Farm Road
Statesville, NC, 28625
Ref: Analytical Testing
Lab Report Number: 22-074-0008
Client Project Description: Stalime Fecal Resample
Dear Ken Galloway:
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Waypoint Analytical, LLC (Charlotte) received sample(s) on 3/15/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
61W) LO
Terri W Cale
Laboratory Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 12

Waypoint,(2)
ANALYTICAL
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State
Program
Lab 1D _
Expiration Date
North Carolina
State Program
37735
07/31/2022
North Carolina
State Program
402
12/31/2022
South Carolina
State Program
99012
07/31/2022
South Carolina
State Program
99012
1213112022
Page 1 of 1 00016122-074-0008
Page 2 of 12

Waypoin(Dt�
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana"cal.com
Sample Summary Table
Report Number: 22-074-0008
Client Project Description: Stalime Fecal Resample
Lab No Client Sample ID Matrix Date Collected Date Received
96076
StaLime 1
Solids
03/i5/2022 09:51
03/15/2022 11:14
96077
Sta Lime 2
Solids
03/15/2022 09:52
03/15/2022 11:14
96078
StaLime 3
Solids
03/15/2022 09:53
03/15/2022 11:14
96079
StaLime 4
Solids
03/15/2022 09:54
03/15/2022 11:14
96080
StaLime 5
Solids
03/15/2022 09:55
03/15/2022 11:14
96081
StaLime 6
Solids
03/15/2022 09:56
03/1S/2022 11:14
96082
StaLime 7
Solids
03/15/2022 09:57
03/15/2022 11:14
Page 3 of 12

Waypointo
ANALYTICAL
01050
City of Statesville, NC Project
Ken Galloway
693 Bell Farm Road Information
Statesville , NC 28625
Report Number : 22-074-0008
Lab No : 96076
Sample ID : StaLime 1
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www,waypointana lytica l.com
Stalime Fecal Resample
REPORT OFANAL YSIS
Report Date : 03/22/2022
Received : 03/15/2022
JMW P'p
Terri W We
Laboratory Project Manager
Matrix: Solids
Sampled: 3/15/2022 9:51
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Fecal Coliform MPN/g <2.2 MPN/g - dry
Moisture 11.1 0/0
Qualifiers/ DL Dilution Factor
Definitions
2.2 1 03/15/2212:52 SMW 9221E-2011
1 03/18/2210:19 SJL SW-DRYWT
MQL Method Quantitation Limit
Page 4 of 12

0
Waypoint. 449 5prfngbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01050
City of Statesville, NC Project Stalime Fecal Resample
Ken Galloway Report Date : 03/22/2022
693 Bell Farm Road Information : Received : 03/15/2022
Statesville , NC 28625 619W�
Terri W Cole
Report Number :22-074-0008 REPORTOFANAL YSIS
Laboratory Project Manager
Lab No : 96077 Matrix: Solids
Sample ID : Sta Lime 2 Sampled: 3/15/2022 9:52
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Fecal Coliform MPN/g
Moisture
<2.1 MPN/g - dry 2.1
7.40 0/0
1 03/15/2212:52 SMW 9221E-2011
1 03/18/2210:19 SA SW-DRYWT
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 5 of 12

(2)
Waypoint
449 5pringbrook
Rd, Charlotte, 28217
Main 704.529.6364364
ANALYTICAL
www.waypointanalytical.com
01050
City of Statesville, NC
Project
Stalime Fecal Resample
Ken Galloway
Report Date : 03/22/2022
693 Bell Farm Road
Information
:
Received : 03/15/2022
Statesville , NC 28625
V
Report Number : 22-074 0008
REPORTOFAN4LYSIS
Terri W ColeLaboratory
Project Manager
Lab No : 96078
Matrix: Solids
Sample ID : StaLime 3
Sampled: 3/15/2022 9:53
Test
Results
Units MQL
DF Date ITime By Analytical
Analyzed Method
Fecal Coliform MPN/g
<2,1
MPN/g - dry 2.1
1 03/15/22 12:52 SMW 9221E-2011
Moisture
8.45
%
1 03/18/2210:19 SJL SW-DRYWT
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 6 of 12

Waypont.0i
ANALYTICAL
01050
City of Statesville, NC Project
Ken Galloway
693 Bell Farm Road Information
Statesville , NC 28625
Report Number:22-074-0008
Lab No : 96079
Sample ID : StaLime 4
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Stalime Fecal Resample
REPORT OF ANAL YSIS
Report Date : 03/22/2022
Received : 03/15/2022
60WCQk'-
Terri W Cole
Laboratory Project Manager
Matrix: Solids
Sampled: 3/15/2022 9:54
Test Results Units MOL DF Date / Time By Analytical
Analyzed Method
Fecal Coliform MPN/g ¢2.1 MPN/g - dry
Moisture 9.03 0/0
2.1 1 03/15/2212:52 SMW 9221E-2011
1 03/18/2210:19 SJL SW-DRYWT
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 7 of 12

•
Waypoint
4�i9 Springbrook
Rd, Charlotte, NC 28237
Main 704.529.6364
ANALYTICAL
www.waypointanalytical.com
01050
City of Statesville, NC
Project
Stalime Fecal Resample
Ken Galloway
Report Date : 03/22/2022
693 Bell Farm Road
Information
:
Received : 03/15/2022
Statesville , NC 28625
�19W
4b
Terri W Cole
Report Number! 22-074-0008
REPORTOPANALYSIS
Laboratory Project Manager
Lab No: 96080
Matrix: Solids
Sample ID : StaLime 5
Sampled: 3/15/2022 9:55
Test
Results
Units MOL
OF Date/Time By Analytical
Analyzed Method
Fecal Coliform MPN/g
<2.1
MFN/g - dry 2.1
1 03/15/22 12:52 SMW 9221E-2011
Moisture
9.04
%
1 03/18/2210:19 SIL SW-DRYWT
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 8 of 12

Waypointo
ANALYTICAL
01050
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
City of Statesville, NC Project Stalime Fecal Resample
Ken Gallaway Report Date : 03/22/2022
693 Bell Farm Road Information : Received : 03/15/2022
Statesville , NC 28625 JOW
Terri W Cole
Report Number :22-074-0008 REPORT OPANALY5IS
Laboratory Project Manager
Lab No: 96081 Matrix: Solids
Sample ID : StaLime 6 -Sampled: 3/15/2022 9:56
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Fecal Coliform MPN/g <2.3 MPN/g - dry
Moisture 13.4 %
Qualifiers/ DF Dilution Factor
Definitions
2.3 1 03/15/2212:52 SMW 9221E-2011
1 03/18/22 10:19 SJL SW-DRYWT
MQL Method Quantitation Limit
Page 9 of 12

Waypointe
ANALYTICAL
01050
City of Statesville, NC Project
Ken Galloway
693 Bell Farm Road Information
Statesville , NC 28625
Report Number : 22-074-0008
Lab No : 96082
Sample ID : StaLime 7
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Stalime Fecal Resample
REPORT OFANAL YSI'S
Report Date : 03/22/2022
Received : 03/15/2022
6OWUJUV
Terri W Cale
Laboratory Project Manager
Matrix: Solids
Sampled: 3/15/2022 9:57
Test Results Units MOL DF Date I Time By Analytical
Analyzed Method
Fecal Coliform MPN/g <2.2 MPN/g - dry
Moisture 9.70 11/0
Qualifiers/ DF Dilution Factor
Definitions
2.2 1 03/15/2212:52 SMW 922IL-2011
1 03/18/2210:19 SJL SW-DRYWT
MQL Method Quantitation Limit
Page 10 of 12

0
Waypoint
ANALYTICAL
449 Springbrook Rd, Charlotte, MC 28217
Main 704.529.6364
www.waypolntanalytical.com
Shipment Receipt Form
Customer Number: 01050
Customer Name: City of Statesville, NC
Report Number: 22-074-0008
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
') Other:
Thermometer ID:
IRT-15 6.0 C
Shipping container/cooler uncompromised?
C Yes
No
Number of coolers/boxes received
I '
Custody seals intact on shipping container/cooler?
U Yes
Lj No
C Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
CO Not Present
Chain of Custody (COC) present?
C Yes
0 No
COC agrees with sample label(s)?
C Yes
0 No
COC properly completed
C Yes
0 No
Samples in proper containers?
C Yes
0 No
Sample containers intact?
C Yes
0 No
Sufficient sample volume for indicated test(s)?
C Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
C Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
C' Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
C NIA
Water - VOA vials free of headspace
0 Yes
0 No
CO NIA
Trip Blanks received with VOAs
0 Yes
0 No
C NIA
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
O NIA
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
C No
Comments:
Signature: Zoe S. Vigilant I Date & Time: 03/15/2022 11;29:55
Page 11 of 12

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Page 12 of 12

Waypointo
ANALYTICAL
5/10/2022
City of Statesville, NC
Ken Galloway
693 Bell Farm Road
Statesville, NC, 28625
Ref: Analytical Testing
Lab Report Number: 22-116-0022
Client Project Description: Quarterly Stalime
Dear Ken Galloway:
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Waypoint Analytical, LLC (Charlotte) received sample(s) on 4/26/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Am) )
6
Terri W Cole
Laboratory Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 22

•
Waypoint
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Certification Summary
Laboratory 1D: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State
Program
Lab ID
Expiration Date
North Carolina
State Program
37735
07/31/2022
North Carolina
State Program
402
12/31/2022
South Carolina
State Program
99012
07/31/2022
South Carolina
State Program
99012
12/31/2022
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2023
Arkansas
State Program
88-0650
02/07/2023
California
State Program
2904
06/30/2022
Florida
State Program
- NELAP
E871157
06/30/2022
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2022
Illinois
State Program
- NELAP
200078
10/10/2022
Kentucky
State Program
80215
06/30/2022
Kentucky
State Program
KY90047
12/31/2022
Louisiana
State Program
- NELAP
LA037
12/31/2022
Louisiana
State Program
- NELAP
04015
06/30/2022
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
415
12/31/2022
Pennsylvania
State Program -
NELAP
68-03195
05/31/2022
South Carolina
State Program
84002
06/30/2022
South Carolina
State Program
84002
06/30/2022
Tennessee
State Program
02027
02/11/2023
Texas
State Program -
NELAP
T104704180
09/30/2022
Virginia
State Program
00106
06/30/2022
Virginia
State Program -
NELAP
460181
09/14/2022
Page 1 of 1 00016/22-116-0022
Page 2 of 22

Waypoint,(2)
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www,waypointa na lytical.com
Sample Summary Table
Report Number; 22-116-0022
Client Project Description: Quarterly Stalime
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
89362
Stalime SAR
Solids
04/26/2022 11:07
04/26/2022 13:00
99575
Stalime 1
Solids
04/26/2022 11:07
04/26/2022 13:00
99576
Stalime 2
Solids
04/26/2022 11:07
04/26/2022 13:00
99577
Stalime 3
Solids
04/26/2022 11:07
04/26/2022 13:00
99578
Stalime 4
Solids
04/26/2022 11.07
04/26/2022 13:00
99579
Stalime 5
Solids
04/26/2022 11:07
04/26/2022 13:00
99580
Stalime 6
Solids
04/26/2022 11:07
04/26/2022 13:00
99581
Stalime 7
Solids
04/26/2022 11:07
04/26/2022 13:00
99582
Stalime
Solids
04/26/2022 11:07
04/26/2022 13:00
99582
Stalime
Solids
04/26/202711:07
04/26/2022 13:00 350.1
99582
Stalime
Solids
04/26/2022 11:07
04/26/2022 13:00 6010D
99582
Stalime
Solids
04/26/2022 11:07
04/26/2022 13:00 4500NORGD-2011
99583
Stalime+Stalime 1st Quarter
Solids
04/26/2022 11:07
04/26/2022 13:00
AES: Analytical Environmental Services, Inc., Atlanta, GA
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
AES
WP MTN
WP MTN
Page 3 of 22

Waypointo
ANALYTICAL
Client: City of Statesville, NC
Project: Quarterly Stalime
Lab Report Number: 22-116-0022
Date: 5/10/2022
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
CASE NARRATIVE
Ammonia was subcontracted to Analytical Environmental Services.
SAR = [ 2.28 ] 1 SQRT { ( [55] + [<0.042] )12 } = 0.435
SAR =[2.281/SQRT {( [55])12)=0.435
SAR = [ 2.28 ] 1 SQRT ( [27.5 } = 0.435
SAR= [2.28]/5.24=0.435
SAR = 0.435
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
PAN Equation = 0.3 * (TKN --- Ammonia) + 0.5 * (Ammonia) + Nitrate -Nitrite
Pan = 0.3 *(2670-88.4) + 0.5 — (88.4) + 24.9
Pan = 831.13
Metals Analysis Method 6010D
Sample 99582 (Stalime)
QC Batch No: V181871V18107
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Sample 99583 (Stalime+Stalime 1st Quarter)
QC Batch No: V181871V18107
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Analyte: Molybdenum
QC Batch No: V181871V18107
LLC failed high. Sample concentration BRL. Result not affected.
Sample 99679
Analyte: Lead
QC Batch No: V181871V18107
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Selenium
QC Batch No: V18187/V18107
LLC failed high. Sample concentration BRL Result not affected.
Page 4 of 22

r
f
Waypoint
Charlotte, NC 28Z17
449 5pringbrook Rd, Ch
Main 704.529.6364
ANALYTICAL
www.waypointanaiytical.com
01050
City of Statesville, NC
Project
Quarterly Stalime
Ken Galloway
Report Date: 05/10/2022
693 Bell Farm Road
Information
:
Received : 04/26/2022
Statesville , NC 28625
W
jigCQ)J
Terri W Cole
Report Number :22-116-0022
REPORTOFANALYSIS
Laboratory Project Manager
Lab No : 89362
Matrix: Solids
Sample ID : Stalime SAR
Sampled: 4/26/2022 11:07
Test
Results
Units MQL
DF Date / Time By Analytical
Analyzed Method
Calcium (saturated paste)
55.0
meq/L 0.250
1 05/06/22 10:40 EDV Saturate Paste
Magnesium (saturated paste)
<0.042
meq/L 0.042
1 05/06/22 10:40 EDV Saturate Paste
Sodium (saturated paste)
2.28
meq/L 0.217
1 05/06/22 10:40 EDV Saturate Paste
Sodium Absorption Ratio
0.435
1 05/06/22 10:40 EDV Saturate Paste
Moisture
59.4
%
1 05/06/22 08:38 EDV SW-DRYWT
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 5 of 22

Waypoint.(2)
ANALYTICAL
01050
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana"cal.com
City of Statesville, NC Project Quarterly Stalime
Ken Galloway Report Date : 05/10/2022
693 Bell Farm Road Information ; Received : 04/26/2022
Statesville , NC 28625
Terri W Cale
Report Number: 22-116-0022 REPORT OFANALYSIS Laboratory Project Manager
Lab No: 99575 Matrix: Solids
Sample ID; Stalime 1 Sampled: 4/26/2022 11:07
Test Results Units MQL DF Date 1 Time By Analytical
Analyzed Method
Fecal CoHomi MPN/g <2.1 MPN/g - dry
Moisture 6.29 %
Qualifiers/ DF Dilution Factor
Definitions
2.1 1 04/26/2214:33 SMW 9221E-2011
1 05/02/2210:17 ADC SW-DRYWT
MQL Method Quantitation Limit
Page 6 of 22

a
Charlotte, NC 2&217
Waypoint 449 5pringbrook Rd, Ch
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01050
City of Statesville, NC Project Quarterly Stalime
Ken Galloway Report Date : 05/10/2022
693 Bell Farm Road Information : Received : 04/26/2022
Statesville, NC 28625
Terri W Cole
Report Number :22-116-0022 REPOR T OF A NA L YSIS
Laboratory Project Manager
Lab No : 99576 Matrix: Solids
Sample ID : Stalime 2 Sampled: 4/26/2022 11:07
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Fecal Coliform MPN/g <2.2 MPN/g - dry
Moisture 10.9 %
Qualifiers/ DF Dilution Factor
Definitions
2.2 1 04/26/2214:33 SMW 9221E-2011
1 05/02/2210:17 ADC SW-DRYWT
MQL Method Quantitation Limit
Page 7 of 22

Waypoint(l)
ANALYTICAL
01050
City of Statesville, NC Project
Ken Galloway
693 Bell Farm Road Information
Statesville , NC 28625
Report Number: 22-116-0022
Lab No : 99577
Sample ID : Stalime 3
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quarterly Stalime
REPORT OF ANAL YSIS
Report Date : 05/10/2022
Received : 04/26/2022
60
Terri W Cole
Laboratory Project Manager
Matrix: Solids
Sampled: 4/26/2022 11:07
Test Results Units MOL OF Date 1 Time By Analytical
Analyzed Method
Fecal Coliform MPN/g <2.3 MPN/g - dry
Moisture 13.9 070
Qualifiers/ DF Dilution Factor
Definitions
2.3 1 04/26/2214:33 SMW 9221E-2011
1 05/02/2210:17 ADC SW-DR`!Wf
MQL Method Quanbtation Limit
Page 8 of 22

•
Charlotte, NC 28217
Waypoint 449 5pringbrook Rd, Ch
Main 704.529.6.964
ANALYTICAL www.waypointanatytical.com
01050
City of Statesville, NC Project Quarterly 5talime
Ken Galloway Report bate : 05/10/2022
693 Bell Farm Road information ; Received : 04/26/2022
Statesville , NC 28525 jig �
Terri W Cole
Report Number : 22-116-0022 REPORTOFANALYSIS
Laboratory Project Manager
Lab No : 99578 Matrix: Solids
Sample ID : Sta}ime 4 Sampled: 4/26/2022 11:07
Test Results Units MOL DF Date / Time By Analytical
Analyzed Method
Fecal Coliform MPN/g <2.2 MPN/g - dry
Moisture 11.5
Qualifiers/ DF Dilution Factor
Definitions
2.2 1 04/26/22 14:33 SMW 9221E-2011
1 05/02/2210:17 ADC SW-DRYWT
MQL Method Quantitation Limit
Page 9 of 22

Waypoint,(2)
ANALYTICAL
01050
City of Statesville, NC Project
Ken Galloway
693 Bell Farm Road Information
Statesville , NC 28625
Report Number : 22-116-0022
Lab No : 99579
Sample ID : Stalime 5
449 Springbrook Rd, Charlotte, NC 28217
Nlaln 704.529.6364
www.waypointanalytical.com
Quarterly Stalime
REPORT OPANAL r515
Report Date : O5/10/2022
Received : 04/26/2022
60 W /" 'P
Terri W Cole
Laboratory Project Manager
Matrix: Solids
Sampled: 4/26/2022 11:07
Test Results Units MOL DF Date 1 Time By Analytical
Analyzed Method
Fecal Coliform MPN/g <2,1 MPN/g -dry
Moisture 8.15 %
Qualifiers/ DF Dilution Factor
Definitions
2.1 1 04/26/2214:33 SMW 9221E-2011
1 05/02/2210:17 ADC SW-DRYWT
MQL Method Quantitation Limit
Page 10 of 22

Waypointo
ANALYTICAL
01050
City of Statesville, NC Project
Ken Galloway
693 Bell Farm Road Information
Statesville , NC 28625
Report Number :22-116-0022
Lab No : 99580
Sample ID : 5talime 6
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana"cal.com
Quarterly Stalime
REPORT OF ANAL Y51S
Report Date : 05/10/2022
Received : 04/26/2022
VOW
Terri W Cole
Laboratory Project Manager
Matrix: Solids
Sampled: 4/26/ 2022 11:07
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Fecal Conform MPN/g <2.2 MPN/g - dry
Moisture 10.9 0/0
2.2 1 04/26/22 14:33 SMW 9221E-2011
1 05/02/2210:17 ADC SW-DRYWT
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 11 of 22

Waypointo
ANALYTICAL
01050
City of Statesville, NC Project
Ken Galloway
693 Bell Farm Road Information
Statesville , NC 28625
Report Number : 22-116-0022
Lab No : 99581
Sample ID; Stallme 7
449 Springbrook Rd, Charlotte, NC 28217
Main 704,529.6364
www.waypotntanalytical.com
Quarterly 5talime
REPORT OF ANAL YSIS
Report Date : 05/10/2022
Received : 04/26/2022
1.l)w
Terri W Cole
Laboratory Project Manager
Matrix: Solids
Sampled: 4/26/ 2022 12:07
Test Results Units MOL DF Date I Time By Analytical
Analyzed Method
Fecal Coliform MPN/9 <2.0 MPN/g - dry
Moisture 4.63 %
Qualifiers/ DF Dilution Factcr
Definitions
2.0 1 04/26/2214:33 SMW 9221E-2011
1 05/02/2210:17 ADC SW-DRYWT
MQL Method Quantitation Limit
Page 12 of 22

•
Waypoint,
4A9 Springbroak Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01050
City of Statesville, NC Project Quarterly Stalime
Ken Galloway
Report Date : 05/10/2022
693 Bell Farm Road
Information:
Received : 04/26/2022
Statesville , NC 28625
JOW
�Terri
W Cole
Report Number : 22-116-0022
REPOR T OF A IVA L YSIS
Laboratory Project Manager
Lab No: 99582
Matrix:
Solids
Sample ID : Stalime
Sampled: 4/26/2022 11:07
Test
ReSU11S
Units
MQL
DP
Date 1 Time
By Analytical
Analyzed
Method
Moisture
4.34
%
1
04/29/2211:32
ADC SW-DRYWT
Ammonia Nitrogen
88.4
mg/Kg AR
1
05/03/22 11:48
350.1
Nitrate (NO3-N)
24.9
mg/Kg - dry
20.9
10
05/04/22 14:47
CEG 9056A
Nitrite (NO2-N)
<10.5
mg/Kg - dry
10.5
10
05/04/22 14:47
CEG 9056A
Nitrate+Nitrite-N
24.9
mg/Kg - dry
10.5
10
05/04/22 14:47
CEG 9056A
Total Solids
90.1
%
0.010
1
05/03/22 10:03
ADC 254OG-2011
Total Kjeldahl Nitrogen
2670
mg/Kg - dry
249
1
05/04/22 16:17
CLP 4500NORGD-2011
Phosphorus
2390
mg/Kg - dry
5.23
1
05/03/22 20:49
EAL 6010D
Aluminum
7010
mglKg - dry
26.1
5
04/29/22 14:29
EDV 6010D
Arsenic
3.92
mg/Kg - dry
2.61
5
04/29/22 14:29
EDV 6010D
Cadmium
<0.523
mg/Kg - dry
0.523
5
04/29/22 14:29
EDV 6010D
Chromium
8.39
mg/Kg - dry
2,61
5
04/29/22 14:29
EDV 60101)
Copper
34.6
mg/Kg - dry
1.31
5
04/29/22 14:29
EDV 6010D
Lead
4.36
mg/Kg - dry
1.57
5
04/29/22 14:29
EDV 6010D
Mercury (Total)
0.0369
mg/Kg - dry
0.0314
1
05/03/22 12:32
EDV 7471B
Molybdenum
<2.61
mg/Kg - dry
2.61
5
04/29/22 14:29
EDV 6010D
Potassium
2350
mg/Kg - dry
131
5
04/29/22 14:29
EDV 6010D
Selenium
<2.61
mg/Kg - dry
2.61
5
04/29/22 14:29
EDV 60100
Sodium
549
mg/Kg - dry
261
5
05/06/22 13:48
EDV 6010D
Zinc
54.2
mg/Kg - dry
2.61
5
04/29/22 14:29
EDV 6010D
Qualifiers/ DF Dilution Factor
MQL Method Quantitation Limit
Definitions
Page 13 of 22

Waypointo
ANALYTICAL
01050
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
City of Statesville, NC Project Quarterly Stalime
Ken Galloway Report Date : 05/10/2022
693 Bell Farm Road Information : Received : 04/26/2022
Statesville , NC 28625 60W
Cqk
Report Number ; 22-1160022 REPORTOPANALYSIS Terri W ColeLaboratory Project Manager
Lab No: 99583 Matrix: Solids
Sample ID : Stalime+Stalime 1st Quarter Sampled: 4/26/2022 11:07
Test Results Units MQL DF Date I Time By Analytical
Analyzed Method
Moisture 17.0
Nickel 9.99 mg/Kg - dry
1 05/02/2210:17 ADC SW-DRYWT
1.51 5 04/29/2214:33 EDV 6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 14 of 22

ACCEss
ANALYTICAL, INC.
ANALYTICAL REPORT
CLIENT
Waypoint Analytical
PO Box 240543
Charlotte NC 282240543
ATTENTION
Terri W Cole
PROJECT ID
22-116-0022
LABORATORY REPORT NUMBER
2204X01
DATE
May 03, 2022
Primary Data Review By Secondary Data Review By
Ashley Amick
Chris Pafford Project Manager, Access Analytical
Project Manager, AES [e-mail]
PLEASE NOTE:
Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc),
3080 Presidential Drive, Atlanta, GA30340.
AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # FL-E87582,
NELAP certified laboratory # E87582
AIHA-LAP,LLC Laboratory ID.100671 for Industrial Hygiene samples (Organics, ]Metals, PCM Asbestos,
Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal)
Direct Examination.
Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a
representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be directed
to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243
Page 15 of 22 Page 1 of 6

0
> _
f t
o
rb ®
7
c
§
J

Analytical Environmental Services, Inc
Date: 3-Flay-22
Client:
Waypoint Analytical
Client Sample ID:
99582
Lab Order
2204XU1
Tag Number:
Stalime
Project Name:
22-116-0022
Collection Date:
4/26/2022 11:07:OOAM
Lab ID:
2204XOI-OOIA
Matrix:
Soil
Analyses Result Qual 1•IDL ReportinPDattLl4itelyzBritchlD DE Analyst
Limit
Nitrogen, Ammonia (as N) Extractable E350.1 MOD
Nitrogen, Ammonia (As N) Extractable 88.4
PERCENT MOISTURE D2216
Percent Moisture 10.3
Qualifiers: • Value exceeds maKimmn contaminant level
BRI. Not Detected at XtDL
I I Holding times for preparation or analysis exceeded
Aaal}'te not NELAC certified
II Analyte detected in the associated method blank
(E350.1)
5.28 10.7 mgYg-dry 335537 1 05/03I202211:49 TL
0 0 tvl% R484656 1 05/01/2022 00:00 AV
E Estimated value above cl-ntitation range
S Spike Recovery outside limits due to matrn
> Greaterthar Result value
J Estimated value detected below Reporting Limit
< Less than Result value
Page 17 of 22
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End of Report
Page 20 of 22 Page 6 of 6

1 0
Waypoint
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28227
Main 704.529.6364
www.waypointanatytical.com
Shipment Receipt Form
Customer Number: 01050
Customer Name: City of Statesville, NC
Report Number: 22-116-0022
Shipping Method
0 Fed Ex 0 US Postal CO) Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
IRT-15 1.6 C
Shipping container/cooler uncompromised?
C Yes
O No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
U Yes
0 No
(De Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
(0) Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
C Yes
0 No
COC properly completed
CO) Yes
0 No
Samples in proper containers?
C Yes
0 No
Sample containers intact?
C Yes
0 No
Sufficient sample volume for indicated test(s)?
C Yes
0 No
All samples received within holding time?
C Yes
0 No
Cooler temperature in compliance?
C Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
C Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
C N/A
Water - VOA vials free of headspace
0 Yes
O No
C N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 NIA
Soil VOA method 5035 — compliance criteria met
Yes
0 No
C N/A
F_ High concentration container (48 hr)
r High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
C No
Comments:
Signature: i7oe S. Vigilant Date & Time: 104/26/2022 13:18:34 j
Page 21 of 22

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Waypointo
ANALYTICAL
8/12/2022
City of Statesville, NC
Ken Galloway
693 Bell Farm Road
Statesville, NC, 28625
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Ref: Analytical Testing
Lab Report Number: 22-207-0052
Client Project Description: 3rd CreekAth CreeklStalime
Dear Ken Galloway:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 7/26/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
L_OZA�) Loccc�
Terri W Cole
Laboratory Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 23

Waypoin(Dt�.
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Maln 704.529.6364
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State
Program
Lab ID
Expiration Date
North Carolina
State Program
37735
07/31/2023
North Carolina
State Program
402
12/31/2022
South Carolina
State Program
99012
07/31/2022
South Carolina
State Program
99012
12/31/2022
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
_ Program
Lab ID
Expiration Date
'
Alabama
State Program
40750
02/28/2023
Arkansas
State Program
88-0650
02/07/2023
California
State Program
2904
06/30/2023
Florida
State Program
- NELAP
E871157
06/30/2023
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2023
Illinois
State Program
- NELAP
200078
10/10/2022
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2022
Louisiana
State Program
- NELAP
LA037
12/31/2022
Louisiana
State Program
- NELAP
04015
06/30/2023
Mississippi
State Program
MS
02/11 /2023
North Carolina
State Program
415
12/31/2022
Pennsylvania
State Program -
NELAP
68-03195
05/31/2023
South Carolina
State Program
84002
06/30/2022
Tennessee
State Program
02027
02/11/2023
Texas
State Program -
NELAP
T104704180
09/30/2022
Virginia
State Program
00106
06130/2023
Virginia
State Program -
NELAP
460181
09/14/2022
Page 1 of 1 00016.22-207-0052
Page 2 of 23

Waypoint(l)
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypo inta na lytica l.co m
Sample Summary Table
Report Number: 22-207-0052
Client Project Description: 3rd Creek/4th Creek/Stalime
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
95326
3rd Creek
TCLP
07/26/2022
07/26/202211:46
95326
3rd Creek
TCLP
07/26/2022
01/26/2022 11:46
SW-1311
WP MTN
95326
3rd Creek
TCLP
07/26/2022
07/26/2022 11:46
8151A
WP MTN
95327
3rd Creek
Solids
07/26/2022
07/26/2022 11:46
95327
3rd Creek
Solids
07/26/2022
W/26/2022 11:46
SW-7.3.4
WP MTN
95327
3rd Creek
Solids
07/26/2022
07/26/2022 11:46
SW-7.3.3
WP MTN
95328
4th Creek
TCLP
07/26/2022
07/26/2022 11:46
95328
4th Creek
TCLP
07/26/2022
07/26/2022 11:46
8151A
WP MTN
95328
4th Creek
TCLP
07/26/2022
07/26/2022 11:46
SW-1311
WP MTN
95329
4th Creek
Solids
07/26/2022
07/26/2022 11:46
95329
4th Creek
Solids
07/26/2022
07/26/2022 11:46
SW-73.4
WP MTN
95329
4th Creek
Solids
07/26/2022
07/26/2022 11:46
SW-7.3.3
WP MTN
95330
Stalime
TCLP
07/26/2022
07/26/2022 11:46
95330
Stalime
TCLP
07/26/2022
07/26/2022 11:46
8151A
WP MTN
95330
Stalime
TCLP
07/26/2022
07/26/2022 11:46
SW-1311
WP MTN
95331
Stalime
Solids
07/26/2022
07/26/2022 11:46
95331
Stalime
Solids
07/26/2022
07/26/2022 11:45
SW-73.4
WP MTN
95331
Stalime
Solids
07/26/2022
07/26/2022 11:46
SW-7.3.3
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 23

Waypoint(l)
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28227
Main 704.529.6364
www.waypointanalytical.com
Client: City of Statesville, NC CASE NARRATIVE
Project: 3rd Creek/4th Creek/Stalime
Lab Report Number: 22-207-0052
Date: 8/12/2022
Metals Analysis (TCLP) Method 6010D
Sample 95337
Analyte: Selenium
QC Batch No: V221061V22072
ICSA/CCB failed above MDL. Sample concentration BRL. Result not affected.
Sample 95773 (7/28-7131 Gypsum Composite)
Analyte: Chromium
QC Batch No: V22236/V22192
CCB failed high. Result 1 Ox concentration. Result not affected.
Total Aqueous Mercury Analysis - CVAA (TCLP) Method 7470A
Sample 95513 (7/25-7127 Gypsum Composite)
Analyte: Mercury
QC Batch No: V22107N22089
ICV failed high. Sample concentration BRL. Result not affected.
Analyte: Mercury
QC Batch No: V22128/V22214
ICV failed high. Sample concentration BRL. Result not affected.
Organochlorine Pesticides by GC (TCLP) Method 8081B
Sample 95328 (4th Creek)
Analyte: Decachlorobiphenyl
QC Batch No: V222831V22260
Extraction analyst noted possible 2x surrogate which calculates to be 109% and is within limits
Sample 95330 (Stalime)
Analyte: Decachlorobiphenyl
QC Batch No: V22283N22260
Extraction analyst noted possible 2x surrogate which caluclates to 92.5% and is within limits
Analyte: Endrin
QC Batch No: V222831V22260
CCV for this analyte above range. Analyte not detected. No further action taken.
Analyte: Methoxychlor
QC Batch No: V222831V22260
Ending CCV above range for this analyte. for all samples except sample 95335, analyte not detected. No further
action taken.
Sample 95326 (3rd Creek)
Analyte: Tetra c h loro-m-xylene
QC Batch No: V22283N22260
Page 4 of 23

Waypointo
ANALYTICAL
449 5pringbrook Rd, Charlotte, NC 28217
Main 704,529.6364
www.waypointanalytical.com
Surrogate(s) were flagged for recoveries in the associated project sample. During the extraction step, the
extraction technician noted that a significant emulsion formed. Batch QC samples (Method Blank and Laboratory
Control Samples) all showed surrogate recoveries within QC limits, indicating that the biased recoveries were due
to the sample matrix.
Surrogate(s) were flagged for recoveries in the associated project sample. During the extraction step, the
extraction technician noted that an emulsion formed. Batch QC samples (Method Blank and Laboratory Control
Samples) all showed surrogate recoveries within QC limits, indicating that the biased recoveries were due to the
sample matrix.
Sample 95328 (4th Creek)
Analyte: Tetrachloro-m-xylene
QC Batch No: V222831V22260
Extraction analyst noted possible 2x surrogate which calculates to 53% and is within limits
Sample 95330 (Stalime)
Analyte: Tetrachloro-m-xylene
QC Batch No: V22283/V22260
Extraction analyst noted possible 2x surrogate which calculates to 40.5% and is within limits
Analyte: Toxaphene
QC Batch No: V222831V22260
ECV above range for this compound. Analyte ont detected in samples. No further action taken.
Volatile Organic Compounds - GCIMS (TCLP) Method 8260D
Analyte: 1,1-Dichloroethene
QC Batch No: V22574N22573
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Sample 95328 (4th Creek)
Analyte: 4-Bromofl uorobenzene
QC Batch No: V22574N22573
Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high
recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all
showed surrogates within QC limits.
Analyte: Carbon Tetrachloride
QC Batch No: V22574N22573
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Semivolatile Organic Compounds - GCIMS (TCLP) Method 8270E
QC Batch No: V22552N22270
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits for several
analytes..
Sample 95326 (3rd Creek)
QC Batch No: V22552/V22270
Surrogate(s) were flagged for recoveries in the associated project sample. During the extraction step, the
extraction technician noted that a significant emulsion formed. Batch QC samples (Method Blank and Laboratory
Control Samples) all showed surrogate recoveries within QC limits, indicating that the biased recoveries were due
to the sample matrix,
Analyte: Nitrobenzene
Page 5 of 23

waypoint.(D
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704,529.6364
www.waypointanalytical.co►n
QC Batch No: V22552/V22270
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this
analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias.
This target analyte was flagged for recoveries outside QC limits in the associated LCS. Data for this analyte is
flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low
bias.
Analyte: Nitrobenzene-d5
QC Batch No: V22223/V22270
LCS surrogate recovery found to be within QC limits and equal to the lower acceptance range.
Analyte: Nitrobenzene-d5
QC Batch No: V22552/V22270
Surrogate recovery is below range.
Page 6 of 23

Waypointo
ANALYTICAL
01050
City of Statesville, NC Project
Ken Galloway
693 Bell Farm Road Information
Statesville , NC 28625
449 Springbrook Rd, Charlotte, NC 28217
Maln 704.529.6364
www.waypointana"cal.com
3rd Creek/4th Creek/Stalime
Report Number :22-207-0052 REPORT OF ANALYSIS
Lab No : 95326
Sample ID : 3rd Creek
Report Date : 08/12/2022
Received : 07/26/2022
JOW�f
Terri W Cole
Laboratory Project Manager
Matrix: TCLP
Sampled: 7/26/2022 0:00
Test Results Units MQL DF Date ITime By Analytical
Analyzed Method
TCLP Herbicide Extraction
Leachate
1
08/08/22 12:00
ALM
SW-1311
TCLP Metals Extraction
Leachate
1
08/02/22 17:00
LMZ
SW-1311
TCLP Pesticide Extraction
Leachate
2
08/02/22 17:00
LMZ
SW-1311
TCLP SVOC Extraction
Leachate
1
08/02/22 17:00
LMZ
SW-1311
TCLP VOC ZHE Extraction
Leachate
1
08/09/22 14:00
TBL
SW-1311 (ZHE)
Analytical Method: 6010D
Prep Batch(es):
V22192
08/03/22 12:40
Prep Method: SW-3010A
Test
Results
Units
MQL
DF
Date 1 Time
By
Analytical
Analyzed
Batch
TCLP Arsenic
<0.050
mg/L
0.050
1
08/03/22 17:48
EDV
V22236
TCLP Barium
<0.050
mg/L
0.050
1
08/03/22 17:48
EDV
V22236
TCLP Cadmium
<0.0150
mg/L
0.0150
1
08/03/22 17:48
EDV
V22236
TCLP Chromium
<0.025
mg/L
0.025
1
08/03/22 17:48
EDV
V22236
TCLP Lead
<0.030
mg/L
0.030
1
08/03/22 17:48
LDV
V22236
TCLP Selenium
<0.100
mg1L
0.100
1
08/03/22 17:48
EDV
V22236
TCLP Silver
<0.025
mg/L
0.025
1
08/03/22 17:48
EDV
V22236
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions M Minimum value MQL Method Quantitation Limit
Page 7 of 23

0
449 SprEngbrook Rd, Charlotte, 28
Waypoint,
Main 7p4,529.fi364364
01050 ANALYTICAL www.waypointanalytical.com
City of Statesville, NC Project 3rd Creek/4th Creek/Stalime
Ken Galloway Report Date : 08/12/2022
693 Bell Farm Road Information : Received : 07/26/2022
Statesville, NC 28625
Report Number : 22-207-0052 REPORT OFANALYSIS Terri W ColeLaboratory Project Manager
Lab No : 95326 Matrix: TCLP
Sample ID: 3rd Creek Sampled: 7/26/2022 0:00
Analytical Method: 7470A Prep Batch(es): V22214 08/03/22 13:05
Prep Method: 7470A
Test Results Units MQL DF Date! Time By Analytical
Analyzed Batch
TCLP Mercury
<0,0002
mg/L
0.0002
1 08/04/22 14:10 EDV
V22290
Analytical Method: 80818
Prep Batch(es):
V22260 08/03/22
14:22
Prep Method: 3510C
Test
Results
Units
MQL
DF Date ITime By
Analytical
Analyzed
Batch
TCLP Fndrin
<0.2500
pg/L
0.2500
1 08/04/22 16:15 JC1
V22283
TCLP gamma-SHC
<0.2500
pg/L
0.2500
1 08/04/22 16:15 )CI
V22283
TCLP Methoxychlor
<0.5000
pg/L
0.5000
1 08/04/22 16:15 JCl
V22283
TCLP Toxaphene
<5.000
pg/L
5.000
1 08/04/22 16:15 JC1
V22283
TCLP Chlordane
<2.500
pg/L
2.500
1 08/04/22 16:15 JC1
V22283
TCLP Heptachlor Epoxide
<0.5000
pg/L
0.5000
1 08/04/22 16:15 JC1
V22283
TCLP Heptachlor
<0.2500
pg/L
0.2500
1 08/04/22 16:15 JC1
V22283
Surrogate: Decachlorobiphenyl
41.00
Limits: 13-186%
1 08/04/22 16:15 JC1
V22283
Surrogate: Tetrachloro-m-xylene
21.00 *
Limits: 40-134%
1 08/04/22 16:15 JCl
V22283
Analytical Method: 8151A
Prep Batch(es):
L631189 08/09/22
16:00
Prep Method: 8151A
Test
Results
Units
MQL
OF Date / Time By
Analytical
Analyzed
Batch
TCLP 2,4-D
<0.0200
mg/L
0.0200
1 08/12/22 04:33 VIC
L631909
TCLP 2,4,5-TP (Silvex)
<0.0020
mg/L
0.0020
1 08/12/22 04:33 VIC
L631909
Surrogate: DCAA
61.20
Limits: 20-120%
1 08/12/22 04:33
L631909
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions M Minimum value
MQL
Method Quantitation Limit
Page 8 of 23

•
•
W��po�nt
449 Springbrook Rd, Charlotte, NC 28217
Main 704,529.6364
ANALYTICAL
www,waypointanalytical.com
01050
City of Statesville, NC
Project
3rd Creek/4th Creek/Stalime
Ken Galloway
Report Date : 08/12/2022
693 Bell Farm Road
Information :
Received : 07/26/2022
Statesville , NC 28625
60W '- 'P
Qu
Terri W Cole
Report Number :22-207-0052
REPOR T OF A NAL Y515
Laboratory Project Manager
Lab No : 95326
Matrix: TCLP
Sample ID : 3rd Creek
Sampled: 7/26/2022 0:00
Analytical Method: 8260D
Prep Batch(es):
V22573 08/10/22 09:00
Prep Method: 5030B
Test
Results
Units
MQL
DF Date/Time By Analytical
Analyzed Batch
TCLP Benzene
<5.00
pg/L
5.00
10 08/10/22 21:16 JLB V22574
TCLP Carbon Tetrachloride
<20.0
pg/L
20.0
10 08/10/22 21:16 JLB V22574
TCLP Chlorobenzene
<5.00
pg/L
5.00
10 08/10/22 21:16 JLB V22574
TCLP Chloroform
<5.00
pg/L
5.00
10 08/10/22 21:16 JLB V22574
TCLP 1,4-Dichlorobenzene
<5.00
pg/L
5.00
10 08/10/22 21:16 JLB V22574
TCLP 1,2-Dichloroethane
<5.00
pg/L
5.00
10 08/10/22 21:16 JLB V22574
TCLP 1,1-Dichloroethene
<5.00
pg/L
5.00
10 08/10/22 21:16 JLB V22574
TCLP Methyl Ethyl Ketone (MEK)
<5.00
p9/L
5.00
10 08/10/22 21:16 JLB V22574
TCLP Tetrachloroethene
<5.00
pg/L
5.00
10 08/10/22 21:16 JLB V22574
TCLP Trichloroethene
<5.00
pg/L
5.00
10 08/10/22 21:16 JLB V22574
TCLP Vinyl Chloride
<5.00
pg/L
5.00
10 08/10/22 21:16 JLB V22574
Surrogate: 4-Bromofluorobenzene
100
Limits: 80-124%
10 08/10/22 21:16 JLB V22574
Surrogate: Dibromofluoromethane
96.4
Limits: 75-129%
10 08/10/22 21:16 JLB V22574
Surrogate: Toluene-d8
89.4
Limits: 77-123%
10 08/10/22 21:16 JLB V22574
Analytical Method: 8270E
Prep Batch(es):
V22270 08/04/22 09:15
Prep Method: 3510C
Test
Results
Units
MQL
DF Date / Time By Analytical
Analyzed Batch
TCLP 2-Methylphenol
<0.050
mg/L
0.050
1 08/04/22 18:14 JMV V22552
TCLP 3&4 Methylphenol
<0.050
mg/L
0.050
1 08/04/22 18:14 JMV V22552
TCLP 2,4-Dinitrotoluene
<0.050
mg/L
0.050
1 08/04/22 18:14 JMV V22552
TCLPliexachlorobenzene
<0.100
mg/L
0.100
1 08/04/22 18:14 JMV V22552
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions M Minimum value
MQL
Method Quantitation Limit
Page 9 of 23

Waypointo.
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28W
Maln 704.529.6364
www,waypotntanalytica l.com
01050
City of Statesville, NC Project 3rd Creek/4th Creek/Stalime
Ken Galloway Report Date : 08/12/2022
693 Bell Farm Road Information ; Received : 07/26/2022
Statesville , NC 28625 �Mw
Report Number :22-207-0052 REPORTOFANALYSIS Terri W Cole
Laboratory Project Manager
Lab No : 95326 Matrix: TCLP
Sample ID : 3rd Creek Sampled: 7/26/2022 0:00
Analytical Method: 8270E
Prep Method: 3510C
Test
Results
Prep Batch(es):
Units
V22270 08/04/22 09:15
MQL DF Date/Time By
Analyzed
Analytical
Batch
TCLP Hexachlorobutadiene
<0.100
mg/L
0.100
1
08/04/22 18:14 JMV
V22552
TCLP Hexachloroethane
<0,050
mg/L
0.050
1
08/04/22 18:14 JMV
V22552
TCLP Nitrobenzene
<0.050 M
mg/L
0.050
1
03/04/22 18:14 JMV
V22552
TCLP Pentachlorophenol
<0.250
mg/L
0.250
1
08/04/22 18:14 JMV
V22552
TCLP Pyridine
<0.050
mg/L
0.050
1
08/04/22 18:14 JMV
V22552
TCLP 2,4,5-Trichlorophenol
<0.100
mg/L
0.100
1
08/04/22 18:14 JMV
V22552
TCLP 2,4,6-Trichlorophenol
<0.100
mg/L
0.100
1
08/04/22 18:14 JMV
V22552
Surrogate: TCLP Phenol-dS
13.6
Limits: 11-100%
1 08/04/22 18:14 3MV
8270E
Surrogate: TCLP 2,4,6-Tribromophenol
30.0 *
Limits: 43-140%
1 08/04/22 18:14 JMV
V22552
Surrogate: TCLP 2-Fluorobiphenyl
28.4 *
Limits: 44-119%
1 08/04/22 18:14 JMV
V22552
Surrogate: TCLP 2-Fluorophenol
20.2
Limits: 20-1190/c
1 08/04/22 18:14 JMV
V22552
Surrogate: TCLP 4-Terphenyl-d14
37.2 *
Limits 44-1200%
1 08/04/22 18:14 JMV
V22552
Surrogate: TCLP Nitrobenzene-d5
24.4 *
Limits: 44-120%
1 08/04/22 18:14 JMV
V22552
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions M Minimum value MQL Method Quantitation Limit
Page 10 of 23

(2)
•
Waypo' nt,
449 Springbrddk Rd, Charlotte, 2821 7
2829.6367
Main 704.54
ANALYTICAL
www.waypointana"cal.com
01050
City of Statesville, NC
Project
3rd Creek/4th Creek/5talime
Ken Galloway
Report Date : 08/12/2022
693 Bell Farm Road
Information :
Received : 07/26/2022
Statesville , NC 28625
Terri W Cole
Report Number :22-207-0052
REFOR T OF ANAL YSIS
Laboratory Project Manager
Lab No : 95327
Matrix: Solids
Sample ID : 3rd Creek
Sampled: 7/26/2022 0:00
Test
Results
Units
MQL DF Date 1 Time By Analytical
Analyzed Method
Sulfide (Reactivity)
<25.0
mg/Kg
25.0 1 08/D4/22 14:18 FMM SW-7.3.4
Moisture
46.5
%
1 08/04/2210:38 ADC SW-DRYWT
Cyanide, Reactive <0.125
mg/Kg
0.125 1 08/04/22 14:18 FMM SW-7.3.3
Ignitability
0.000
mm/sec
1 07/27/2217:27 CEG SW-1030
pH
7.41
S.U.
1 07/29/2212:35 CLB 9045D
Qualifiers/ * Outside QC Limit
Definitions M Minimum value
DF Dilution Factor
MQL Method Quantitation Limit
Page 11 of 23

•
Waypoint 1 (D 449 Springbrook Rd, Charl28217
Mainie 70704.5.529.63fi4
01050 ANALYTICAL www.waypointanalytiical.com
City of Statesville, NC Project 3rd Creek/4th Creek/Stalime
IC G 11
en a oway
Report Date : 08/12/2022
693 Bell Farm Road
Information :
Received : 07/26/2022
Statesville , NC 28625
60w P
Report Number : 22-207-0052
REFORTOFANALYSIS
Terri W Cole
Laboratory Project Manager
Lab No : 95328
Matrix:
TCLP
Sample ID : 4th Creek
Sampled:
7/26/2022 0:00
Test
Results
Units
MQL
DF
Date 1 Time
By Analytical
Analyzed
Method
TCLP Herbicide Extraction
Leachate
1
08/08/22 12:00
ALM SW-1311
TCLP Metals Extraction
Leachate
1
07/28/22 18:11
EDV SW-1311
TCLP Pesticide Extraction
Leachate
1
07/28/22 18:11
EDV SW-1311
TCLP SVOC Extraction
Leachate
1
07/28/22 18:11
FDV SW-1311
TCLP VOC ZHE Extraction
Leachate
1
08/09/22 14:00
TBL SW-1311 (ZHE)
Analytical Method: 6010D
Prep Batch(es):
V22072
08/01/22 10:07
Prep Method: SW-3010A
Test
Results
Units
MQL
DF
Date/Time
By Analytical
Analyzed
Batch
TCLP Arsenic
<0.050
mg/L
0.050
1
08/01/22 15:02
EDV V22106
TCLP Barium
<0.050
m9/L
0.050
1
08/01/22 15:02
EDV V22106
TCLP Cadmium
<0.0150
mg/L
0.0150
1
08/01/22 15:02
EDV V22106
TCLP Chromium
<0.025
mg/L
0.025
1
08/02/22 14:31
EDV V22106
TCLP Lead
<0.030
mg/L
0.030
1
08/01/22 15:02
EDV V22106
TCLP Selenium
<0,100
mg/L
0.100
1
08/01/22 15:02
EDV V22106
TCLP Silver
<0.025
mg/L
0.025
1
08/01/22 15:02
EDV V22106
Qualifiers/ * Outside QC Limit
Definitions M Minimum value
DF Dilution Factor
MQL Method Quantitation Limit
Page 12 of 23

•
Charlotte, NC 28217
Waypoint, 449 Springbraok Rd, Ch
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01050
City of Statesville, NC Project 3rd Creek/4th Creek/Stalime
Ken Galloway Report Date : 08/12/2022
693 Bell Farm Road Information : Received : 07/26/2022
Statesville , NC 28625
Terri W Cole
Report Number :22-207-0052 REPORT OTANALYSIS Laboratory Project Manager
Lab No : 95328 Matrix: TCLP
Sample ID : 4th Creek Sampled: 7/26/2022 0:00
Analytical Method: 7470A Prep Batch(es): V22089 08/01/22 10:02
Prep Method: 7470A
Test Results Units MOL DF Date 1 Time By Analytical
Analyzed Batch
TCLP Mercury
Analytical Method: 8081B
Prep Method: 3510C
Test
TCLP Endrin
TCLP gamma-BHC
TCLP Methoxychlor
TCLP Toxaphene
TCLP Chlordane
TCLP Heptachlor Epoxide
TCLP Heptachlor
Surrogate: Decachlorobiphenyl
Surrogate: Tetrachloro-m-xylene
Analytical Method: 8151A
Prep Method: 8151A
Test
<0.0002 mg/L 0.0002 1 08/01/2215:24 EDV V22107
Prep Batch(es): V22260 08/03/22 14:22
Results Units MQL DF Date 1 Time By Analytical
Analyzed Batch
<0.2500
pg/L
0.2500
1
08/01/22
15:35
JC1
V22283
<0.2500
pg/L
0.2500
1
08/04/22
15:35
JC1
V22283
<0,5000
pg/L
0.5000
1
08/04/22
15:35
JC1
V22283
<5.000
hg/L
5.000
1
08/04/22
15:35
JC1
V22283
<2.500
pg/L
2.500
1
08/04/22
15:35
JC1
V22283
<0.5000
pg/L
0.5000
1
08/04/22
15:35
3C1
V22283
<0.2500
pg/L
0.2500
1
08/04/22
15:35
JC1
V22283
218.0 *
Limits: 13-186%
1 08/04/22 15:35
3C1
V22283
106.0
Limits:40-134%
1 08/04/2215:35
)Cl
V22283
Prep Batch(es):
L631189 08/09/22 16:00
Results Units MQL DF Date 1 Time By Analytical
Analyzed Batch
TCLP 2,4-1) <0.0200 mg/L 0.0200 1 08/12/22 04:58 VIC L631909
TCLP 2,4,5-TP (Silvex) <0.0020 mg/L 0,0020 1 08/12/22 04:58 VIC L631909
Surrogate: DCAA 46.20 Limits: 20-12011a 1 08/12/22 04:58 L631909
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions M Minimum value MQL Method Quanttation Limit
Page 13 of 23

r
•
Waypoint 449 Springbrook Rd, Charlotte, .5 28217
Main 704.529.6364
alaso ANALYTICAL www,waypointana lytica l.co m
City of Statesville, NC Project 3rd Creek/4th Creek/Stalime
K
en Galloway
Report Date : 08/12/2022
693 Bell Farm Road
Information :
Received : 07/26/2022
Statesville , NC 28625
60 CQ)'J
Report Number :22-z07 0052
REPORT OF ANALYSIS
Terri W ColeLaboratory
Project Manager
Lab No : 95328
Matrix:
TCLP
Sample ID : 4th Creek
Sampled:
7/26/2022 0:00
Analytical Method: 8260D
Prep Batch(es):
V22573 08/10/22 09:00
Prep Method: 5030B
Test
Results
Units
MQL
DF Date 1 Time
By Analytical
Analyzed
Batch
TCLP Benzene
<5.00
pg/L
5.00
10 08/10/22 20:28
JLB V22574
TCLP Carbon Tetrachloride
<20.0
ug/L
20.0
10 08/10/22 20:28
JLB V22574
TCLP Chlorobenzene
<5,00
pg/L
5.00
10 08/10/22 20:28
JLB V22574
TCLP Chloroform
<5.00
p9/L
5.00
10 08/10/22 20:28
JLB V22574
TCLP 1,4-Dichlorobenzene
<5.00
pg/L
5.00
10 08/10/22 20:28
JLB V22574
TCLP 1,2-Dichloroethane
<5,00
pg/L
5.00
10 08/10/22 20:28
JLB V22574
TCLP 1,1-Dichloroethene
<5.00
ug/L
5100
10 OS/10/22 20:28
JLB V22574
TCLP Methyl Ethyl Ketone (MEK)
<5.00
pg/L
5.00
10 08/10/22 20:28
JLB V22574
TCLP Tetrachloroethene
<5.00
pg/L
5.00
10 08/10/22 20:28
JLB V22574
TCLP Trichloroethene
<5.00
pg/L
5.00
10 08/10/22 20:28
JLB V22574
TCLP Vinyl Chloride
<5.00
pg/L
5.00
10 08/10/22 20:28
JLB V22574
Surrogate: 4-Bromofluorobenzene
140 *
Limits: 80-124%
10 08/10/22 20:28
JLB V22574
Surrogate: Dibromofluoromethane
75.8
Limits: 75-129%
10 08/10/22 20:28
JLB V22574
Surrogate: Toluene-d8
90.4
Limits: 77-123%
10 08/10/22 20:28
JLB V22574
Analytical Method: 82/OE
Prep Batch(es):
V22148 08/02/22
09:07
Prep Method: 3510C
Test
Results
Units
MQL
DF Date / Time
By Analytical
Analyzed
Batch
TCLP 2-Methylphenol
<0.050
mg/L
O.050
1 08/02/22 17:57
JMV V22223
TCLP 3&4 Methylphenol
<0.050
mg/L
0,050
1 08/02/22 17:57
JMV V22223
TCLP 2,4-Dinitrotoluene
<0.050
mg/L
0.050
1 08/02/22 17:57
JMV V22223
TCLP Hexachloro benzene
<0.100
mg/L
0.100
1 08/02/22 17:57
JMV V22223
Qualifiers/ Outside QC Limit
DF
Dilution Factor
Definitions M Minimum value
MQL
Method Quantitation
Limit
Page 14 of 23

Waypointo
ANALYTICAL
01050
City of Statesville, NC Project
Ken Galloway
693 Bell Farm Road Information ;
Statesville , NC 28625
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical,com
3rd Creek/4th Creek/Stalime
Report Number :22-207-0052 REPORT OFANALYSIS
Lab No : 95328
Sample ID : 4th Creek
Report Date : 08/12/2022
Received : 07/26/2022
6M U)
QU
Terri W Cole
Laboratory Project Manager
Matrix: TCLP
Sampled: 7/26/2022 0:00
Analytical Method: 8270E
Prep Method: 3510C
Test
Results
Prep Batch(es):
Units
V22148 08/02/22 09:07
MQL DF Date I Time By
Analyzed
Analytical
Batch
TCLP Hexachlorobutadiene
<0.100
mg/L
0.100
1
08/02/22 17:57 JMV
V22223
TCLP Hexachloroethane
<0.050
mg/L
0.050
1
08/02/22 17:57 JMV
V22223
TCLP Nitrobenzene
<0.050
mg/L
0.050
1
08/02/22 17:57 JMV
V22223
TCLP Pentachlorophenol
<0.250
mg/L
0.250
1
08/02/22 17:57 JMV
V22223
TCLP Pyridine
<0.050
mg/L
0.050
1
08/02/22 17:57 JMV
V22223
TCLP 2,4,5-Trichlorophenol
<0.100
mg/L
0.100
1
08/02/22 17:57 JMV
V22223
TCLP 2,4,6-Trichlorophenol
<0.100
mg/L
0.100
1
08/02/22 17:57 JMV
V22223
Surrogate: TCLP Phenol-d5
23.2
Limits: 11-100%
1 08/02/22 17:57 JMV
8270E
Surrogate: TCLP 2,4,6-Tribromophenol
63A
Limits: 43-140%
1 08/02/22 17:57 JMV
V22223
Surrogate: TCLP 2-Fluorobiphenyl
59.2
Limits: 44-119%
1 08/02/22 17:57 JMV
V22223
Surrogate: TCLP 2-Fluorophenol
36.6
Limits: 20-119%
1 08/02/22 17:57 JMV
V22223
Surrogate: TCLP 4-Terphenyl-d14
66.8
Limits: 44-120%
1 08/02/22 17:57 JMV
V22223
Surrogate: TCLP Nitrobenzene-d5
51.2
Limits: 44-120%
1 08/02/22 17:57 JMV
V22223
Qualifiers/ * Outside QC Limit
Definitions M Minimum value
DF Dilution Factor
MQL Method Quantitation Limit
Page 15 of 23

Waypoint,(D
ANALYTICAL
01050
City of Statesville, NC
Ken Galloway
693 Bell Farm Road
Statesville , NC 28625
Report Number : 22-207-0052
Lab No ; 95329
Sample ID : 4th Creek
Test
Project
Information
449 5pringbrook Rd, Charlotte, NC 28217
Main 704,529.6364
www,waypointa na lytica l.eo m
3rd Creek/4th Creek/Stalime
REPORT OF ANAL YSIS
Results Units MQL
Report Date ; 08/12/2022
Received : 07/26/2022
VMCQ�J
Terri W Cole
Laboratory Project Manager
Matrix: Solids
Sampled: 7/ 26/2022 0:00
DF Date / Time By Analytical
Analyzed Method
Sulfide (Reactivity)
<25.0
mg/Kg 25.0
1
08/04/22 14:18
FMM
SW-7,3.4
Moisture
81.0
0/0
1
08/04/2210:38
ADC
SW-DRYUUi"
Cyanide, Reactive
<0.125
mg/Kg 0.125
1
08/04/22 14;18
FMM
SW-7.3.3
Ignitability
0.000
mm/sec
1
07/27/2217:27
CEG
SW-1030
pH
12.3
S.u.
1
07/29/2212:35
CLB
9045D
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions M Minimum value MQL Method Quantitation Limit
Page 16 of 23

•
Waypoi�� , 0 449 5pringbraak Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalyLical.com
01050
City of Statesville, NC Project 3rd Creek/4th Creek/Stalime
Ken Galloway Report Date : 08/12/2022
693 Hell Farm Road Information : Received : 07/26/2022
Statesville , NC 28625 J0W�
Terri W Cole
Report Number :22-207-0052 REPOR T OF A NA L YSIS Laboratory Project Manager
Lab No ; 95330 Matrix: TCLP
Sample ID : Stalime Sampled: 7/26/2022 0:00
Test Results Units MQL DF Date ITime By Analytical
Analyzed Method
TCLP Herbicide Extraction
Leachate
1
08/08/22 12:00
ALM
SW-1311
TCLP Metals Extraction
Leachate
1
07/28/22 18:11
EDV
SW-1311
TCLP Pesticide Extraction
Leachate
1
07/28/22 18:11
EDV
SW-1311
TCLP SVOC Extraction
Leachate
1
07/28/22 18:11
EDV
SW-1311
TCLP VOC ZHE Extraction
Leachate
1
08/09/22 14:00
TBL
SW-1311 (ZHE)
Analytical Method: 6010D
Prep Batch(es):
V22072
08/01/22 10:07
Prep Method: SW-3010A
Test
Results
Units
MQL
DF
Date/Time
By
Analytical
Analyzed
Batch
TCLP Arsenic
<0.050
mg/L
0.050
1
08/01/22 15:06
EDV
V22106
TCLP Barium
1.66
mg/L
0.050
1
09/01/22 15:06
EDV
V22106
TCLP Cadmium
<0,0150
mg/L
0,0150
1
08/01/22 15:06
EDV
V22106
TCLP Chromium
<0.025
mg/L
0.025
1
08/02/22 14:35
EDV
V22106
TCLP Lead
<0.030
mg/L
0.030
1
08/01/22 15:06
EDV
V22106
TCLP Selenium
<0.100
mg/L
0.100
1
08/01/22 15:06
EDV
V22106
TCLP Silver
<0,025
mg/L
0.025
1
08/01/22 15:06
EDV
V22106
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions M Minimum value MQL Method Quantitation Limit
Page 17 of 23

•
Waypoint
449 Springbrook Rd, Ch
Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL
www.waypointanalytical.com
01050
City of Statesville, NC Project 3rd Creek/4th Creek/Stalime
Ken Galloway
Report Date : 08/12/2022
693 Bell Farm Road Information :
Received : 07/26/2022
Statesville , NC 28625
60W
Report Number : 22-207-0052
REPORT OFANALYSIS
Terri W ColeLaboratory
Project Manager
Lab No: 95330
Matrix:
TCLP
Sample ID: Stalime
Sampled:
7/26/2022 0:00
Analytical Method: 7470A
Prep Batch(es):
V22089
08/01/22 10:02
Prep Method: 7470A
Test Results
Units
MOL
DF Date lTime
By Analytical
Analyzed
Batch
TCLP Mercury <0.0002
mg/L
0.0002
1 08/01/22 15:26
EDV V22107
Analytical Method: 8081B
Prep Batch(es):
V22260
08/03/22 14:22
Prep Method: 3510C
Test Results
Units
MQL
DF Date / Time
By Analytical
Analyzed
Batch
TCLP Endrin <0.2500
ug/L
0.2500
1 08/04/22 15:48
JC1 V22283
TCLP gamma-BHC <0.2500
Pg/L
0.2500
1 08/04/22 15:48
ICI V22283
TCLP Methoxychlor <0.5000
ug/L
0.5000
1 08/04/22 15:48
JC1 V22283
TCLP Toxaphene <5.000
hg/L
5.000
1 08/04/22 15:48
JC1 V22283
TCLP Chlordane <2.500
pg/L
2.500
1 08/04/22 15:48
JC1 V22283
TCLP Heptachlor Epoxide <0.5000
hg/L
0.5000
1 08/04/22 15:48
JC1 V22283
TCLP Heptachlor <0.2500
Py/L
0.2500
1 08/04/22 15:48
JC1 V22283
Surrogate: Decachlorobiphenyl
195.0
Limits:
13-186% 1 08/04/22 15:48 JC1 V22283
Surrogate: Tetrachloro-m-xylene
81.00
Limits: 40-134% 1 08/04/22 15:48 JC1 V22283
Analytical Method: 8151A
Prep Batch(es):
L631189
08/09/22 16:00
Prep Method: 8151A
Test Results
Units
MQL
DF Date 1 Time
By Analytical
Analyzed
Batch
TCLP 2,4-D <0.0200
mg/L
0.0200
1 08/12/22 05:23
VIC L631909
TCLP 2,4,5-TP (Silvex) <0.0020
mg/L
0.0020
1 08/12/22 05:23
VIC L631909
Surrogate: DCAA
46.40
Limits: 20-12001c, 1 08/12/22 05:23
L631909
Qualifiers/ * Outside QC Limit
DF Dilution Factor
Definitions M Minimum value
M L Method Q Quantitation Limit
Page 18 of 23

Waypointo
ANALYTICAL
01050
City of Statesville, NC Project
Ken Galloway
693 Bell Farm Road Information
Statesville , NC 28625
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytical,cam
3rd Creek/4th Creek/Stalime
Report Number : 22-207-0052 REPORTOFANALYSIS
Lab No : 95330
Sample ID : Stalime
Report Date : 08/12/2022
Received : 07/26/2022
6)AW r %P
Terri W Cole
Laboratory Project Manager
Matrix: TCLP
Sampled: 7/26/2022 0:00
Analytical Method: 8260D
Prep Batch(es):
V22573 08/10/22 09:00
Prep Method: 5030B
Test
Results
Units
MQL
DF
Date/Time
By
Analytical
Analyzed
Batch
TCLP Benzene
<5.00
pg/L
5.00
10
08/10/22 20:52
JLB
V22574
TCLP Carbon Tetrachloride
<20.0
pg/L
20.0
10
08/10/22 20:52
JLB
V22574
TCLP Chlorobenzene
<5,00
pg/L
5.00
10
08/10/22 20:52
JLB
V22574
TCLP Chloroform
<5.00
pg/L
5.00
10
08/10/22 20:52
JLB
V22574
TCLP 1,4-Dichlorobenzene
<5.00
pg/L
5.00
10
08/10/22 20:52
JLB
V22574
TCLP 1,2-Dichloroethane
<5.00
pg/L
5.00
10
08/10/22 20:52
JLB
V22574
TCLP 1,1-Dichloroethene
<5.00
pg/L
5.00
10
08/10/22 20:52
JLB
V22574
TCLP Methyl Ethyl Ketone (MEK)
19.5
pg/L
5.00
10
08/10/22 20:52
JLB
V22574
TCLP Tetrachloroethene
<5.00
pg/L
5.00
10
08/10/22 20:52
JLB
V22574
TCLP Trichloroethene
<5.00
pg/L
5.00
10
08/10/22 20:52
JLB
V22574
TCLP Vinyl Chloride
<5.00
pg/L
5.00
10
08/10/22 20:52
JLB
V22574
Surrogate: 4-Bromofluorobenzene
97.4
Limits: 80-124%
10 08/10/22 20:52 JLB
V22574
Surrogate: Dibromofluoromethane
81.8
Limits: 75-129%
10 08/10/22 20:52 JLB
V22574
Surrogate: Toluene-&
86.8
Limits: 77-123%
10 08/10/22 20:52 JLB
V22574
Analytical Method: 8270E
Prep Batch(es):
V22148 08/02/2209:07
Prep Method: 3510C
Test
Results
Units
MQL
DF
Date ITime
By
Analytical
Analyzed
Batch
TCLP 2-Methylphenol
<0.050
mg1L
0.050
1
08/02/22 18:19
JMV
V22223
TCLP 3&4 Methylphenol
<0.050
mg1L
0.050
1
08/02/22 18:19
JMV
V22223
TCLP 2,4-Dinitrotoluene
<0.050
mg/L
0.050
1
08/02/22 18:19
JMV
V22223
TCLP Hexachlorobenzene
<0.100
mg/L
0.100
1
08/02/22 18:19
JMV
V22223
Qualifiers/ * Outside QC Limit
DF
Dilution
Factor
Definitions M Minimum value
MQL
Method
Quantitation Limit
Page 19 of 23

(2)
Waypoint,
444 5pringbrook Rd, Charlotte, 28217
Main T04.529.636464
ANALYTICAL
www,waypointana lytica l.com
01050
City of Statesville, NC Project
3rd Creek/4th Creek/Stalime
Ken Galloway
Report Date : 08/12/2022
693 Bell Farm Road Information :
Received : 07/26/2022
Statesville , NC 28625
60W 411
Report Number :22-207-DD52 REPORT
Terri W ColeOFANALYSIS
Laboratory Project Manager
Lab No : 95330
Matrix: TCLP
Sample ID : Stalime
Sampled: 7/26/2022 0:00
Analytical Method: 8270E Prep Batch(es):
V22148 08/02/22 09:07
Prep Method: 3510C
Test Results
Units
MQL
DF Date 1 Time By Analytical
Analyzed Batch
TCLP Hexachlorobutadiene <0.100
mg/L
0.100
1 08/02/22 18:19 JMV V22223
TCLP Hexachloroethane <0.050
mg/L
0.050
1 08/02/22 18:19 JMV V22223
TCLP Nitrobenzene <0,050
mg/L
0.050
1 08/02/22 18:19 JMV V22223
TCLP Pentachlorophenol <0,250
mg/L
0.250
1 08/02/22 18:19 JMV V22223
TCLP Pyridine <0.050
mg/L
0.050
1 08/02/22 18:19 JMV V22223
TCLP 2,4,5-Trichlorophenol <0.100
mg/L
0.100
1 08/02/22 18:19 JMV V22223
TCLP 2,4,6-Trichlorophenol <0.100
mg/L
0.100
1 08/02/22 18:19 JMV V22223
Surrogate: TCLP Phenol-d5 26.0
Limits: 11-100%
1 08/02/22 18:19 JMV 8270E
Surrogate: TCLP 2,4,6-Tribromophenol 78.2
Limits: 43-1400,lo
1 08/02/22 18:19 JMV V22223
Surrogate: TCLP 2-Fluorobiphenyl 71.6
Limits: 44-119%
1 08/02/22 18:19 JMV V22223
Surrogate: TCLP 2-Fluorophenol 39.0
Limits: 20-119%
1 08/02/22 18:19 JMV V22223
Surrogate: TCLP 4-Terphenyl-d14 81.6
Limits: 44-120%
1 08/02/22 18:19 JMV V22223
Surrogate: TCLP Nitrobenzene-d5 63.6
Limits: 44-120%
1 08/02/22 18:19 JMV V22223
Qualifiers/ Outside QC Limit DF Dilution Factor
Definitions M Minimum value MQL Method Quantitation Limit
Page 20 of 23

•
Waypoint,
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL
www.waypointana"cal.com
01050
City of Statesville, NC
Project
3rd Creek/4th Creek/Stalime
Ken Galloway
Report Date : 08/12/2022
693 Bell Farm Road
Information :
Received : 07/26/2022
Statesville , NC 28625
6AWLQ,&
Terri W Cole
Report Number : 22-207-0052
REPORT OPANACYSIS Laboratory Project Manager
Lab No : 95331
Matrix: Solids
Sample ID : Stalime
Sampled: 7/26/2022 0:00
Test
Results
Units
MOL DF Date! Time By Analytical
Analyzed Method
Sulfide (Reactivity)
<25.0
nag/Kg
25.0 1 08/04/22 14:18 FMM SW-7.3.4
Moisture
23.2
C/o
1 08/04/2210:38 ADC SW-DRYWT
Cyanide, Reactive <0.125
mg/Kg
0.125 1 09/04/22 14:18 FMM SW-7.3.3
Ignitability
0.000
mm/sec
1 07/27/2217:27 CEG SW-1030
pH
6.59
s.u.
1 07/29/2212:35 CLB 9045D
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions
Page 21 of 23

(D
Waypoint'
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 01050
Customer Name: City of Statesville, NC
Report Number: 22-207-0052
Shipping Method
0 Fed Ex 0 US Postal C Lab
o UPS 0 Client 0 Courier
Other:
Thermometer ID:
IRT-15 1.0 C
Shipping container/cooler uncompromised?
C Yes
ONO
Number of coolers/boxes received
r i
Custody seals intact on shipping container/cooler?
0 Yes
ONO
C; Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
CO Not Present
Chain of Custody (COC) present?
C Yes
ONO
COC agrees with sample label(s)?
* Yes
0 No
COC properly completed
C Yes
ONO
Samples in proper containers?
C Yes
ONO
Sample containers intact?
C Yes
ONO
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
C Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
00 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
C NIA
Water - VOA vials free of headspace
OJ Yes
0 No
CO) NIA
Trip Blanks received with VOAs
0 Yes
0 No
C N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
C N/A
F_ Nigh concentration container (48 hr)
r High concentration pre -weighed (methanol -14 d)
F Low concentration EnCore samplers (48 hr)
[_ Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? (D Yes C No
Comments: F_
Signature: ngela D Overcash Date & Time: 07/26/2022 12:53:56
Page 22 of 23

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Page 23 of 23
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Waypointo
ANALYTICAL
8/15/2022
City of Statesville, NC
Ken Galloway
693 Bell Farm Road
Statesville, NC, 28625
Ref: Analytical Testing
Lab Report Number: 22-207-0051
Client Project Description: Sta-Lime Quarterly Tests
Dear Ken Galloway:
449 Springbrook Rd, Charlotte, NC 28217
Main 704.S29.6364
www.waypointanalytical.com
Waypoint Analytical, LLC (Charlotte) received sample(s) on 7/26/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Terri W Cole
Laboratory Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 cf 19

(D
Waypoint
ANALYTICAL
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypo intana"cal.corn
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State
Program
Lab ID
Expiration Date
North Carolina
State Program
37735
07/31/2023
North Carolina
State Program
402
12/31/2022
South Carolina
State Program
99012
07/31/2022
South Carolina
State Program
99012
12/31I2022
Laboratory ID: WP MTN: Waypoint Analytical, LLC,, Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2023
Arkansas
State Program
88-0650
02/07/2023
California
State Program
2904
06/30/2023
Florida
State Program
- NELAP
E871157
06/30/2023
Georgia
Slate Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2023
Illinois
State Program
- NELAP
200078
10/10/2022
Kentucky
Stale Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2022
Louisiana
State Program -
NELAP
LA037
12/31/2022
Louisiana
State Program -
NELAP
04015
06/30/2023
Mississippi
Slate Program
MS
02/11/2023
North Carolina
State Program
415
12/31/2022
Pennsylvania
State Program -
NELAP
68-03195
05/31/2023
South Carolina
State Program
84002
06/30/2022
Tennessee
State Program
02027
02/11/2023
Texas
State Program -
NELAP
T104704180
09/30/2022
Virginia
State Program
00106
06,r3012023
Virginia
State Program -
NELAP
460181
09/14/2022
Page 1 of 1 00016/22-207-0051
Page 2 of 19

Waypoin(2)t�.
ANALYTICAL
449 SprIngbrook Rd, Charlotte, NC 28217
Main 7O4.529.6364
www.waypointa na"ca I.cam
Sample Summary Table
Report Number: 22-207-0051
Client Project Description: Sta-Lime Quarterly Tests
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
95318
#1
Solids
07/26/2022 10:13
07/26/2022 11:46
95319
#2
Solids
071261202210:13
07/26/2022 11:46
95320
#3
Solids
07/26/2022 10:13
07/26/2022 11:46
95321
#4
Solids
07/26/2022 10:13
07126/202211:46
95322
#5
Solids
011261202210:13
07/26/202211:46
95323
46
Solids
07/26/2022 10:13
07/26/2022 11:46
95324
#7
Solids
07/26/2022 10:13
07/26/2022 11:46
95324
#7
Solids
07/26/2022 10:13
07/26/2022 11:46 350.1 AES
95324
#7
Solids
07/26/2022 10:13
07/26/2022 11:46 6010D WP MTN
95324
47
Solids
07/26/2022 10:13
07/26/2022 11:46 4500NORGD-2011 WP MTN
95325
#7 SAR
Solids
07/26/2022 10:13
07/26/2022 11:46
AES: Analytical Environmental Services, Inc., Atlanta, GA
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 19

Waypointo
ANALYTICAL
01050
City of Statesville, NC Project
Ken Galloway
693 Bell Farm Road Information
Statesville , NC 28625
Report Number; 22-207-0051
Lab No : 95318
Sample ID : *1
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www,waypointanalytical.com
Sta-Lime Quarterly Tests
REPORT OF ANALYSIS
Report Date : 08/1512022
Received : 07/26/2022
60W
Terri W Cole
Laboratory Project Manager
Matrix: Solids
Sampled: 7/26/2022 10:13
Test Results Units MQL DF Date/Time By Analylical
Analyzed Method
Fecal Coiiform MPN/g <2.1 MPN/g - dry
Moisture 6.44 %
Qualifiers/ DF Dilution Factor
Definitions
2.1 1 07/26/2213:22 SMW 9221E-2011
1 08/04/2210:38 ADC SW-DRYWT
MQL Method Quantitation Limit
Page 4 of 19

Waypointo
ANALYTICAL
01050
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
City of Statesville, NC Project 5ta-Lime Quarterly Tests
Ken Galloway Report Date : 08/15/2022
693 Bell Farm Road Information : Received : 07/26/2022
Statesville , NC 28625 Jmw,-,P
Terri W Cole
Report Number : 22-207-0051 REPORrOF'ANALY5I5
Laboratory Project Manager
Lab No : 95319 Matrix: Solids
Sample ID : #2 Sampled: 7/26/2022 10:13
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Fecal Coliform MPN/g <2.2 MPN/g -dry
Moisture 10.6 %
Qualifiers/ DF Dilution Factor
Definitions
2.2 1 07/26/22 13:22 SNI W 9221E-2011
1 08/04/2210:38 ADC SW-DRYWT
MQL Method Quantitation Limit
Page 5 of 19

Main 7
•
Waypoint�. (D 449 Springbrook Rd, Charlotte, 28217
{}4.S.524.fi3fi4
01050 ANALYTICAL www.waypointanawcal.com
City of Statesville, NC Project Sta-Lime Quarterly Tests
Ken Galloway Report Date : 08/15/2022
693 Bell Farm Road Information : Received : 07/26/2022
Statesville , NC 28625 6OW
Report Number : 22-207-0051 REPORTOFANALYSIS Terri W ColeLaboratory Project Manager
Lab No : 95320 Matrix: Solids
Sample ID : #3 Sampled: 7/26/2022 10:13
Test Results Units MOL DF Date / Time By Analytical
Analyzed Method
Fecal Coliform MPN/g <2.3 MPN/g - dry
Moisture 15.6 %
2.3 1 07/26/2213:22 SMW 4221E-2011
1 08/04/2210:38 ADC SW-DRYWT
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 6 of 19

(2)
Wavpofnt�
ANALYTICAL
01050
City of Statesville, NC
Ken Galloway
693 Bell Farm Road
Statesville , NC 28625
Report Number :22-207-0051
Lab No : 95321
Sample ID : #4
449 Springbrook Rd, Charlotte, NC 28217
Main 704,529.6364
www.waypointanalytical.com
Project Sta-Lime Quarterly Tests
Information :
REPORT OFANALYSIS
Report Date : 08/15/2022
Received : 07/26/2022
6OWCQk
Terri W Cole
Laboratory Project Manager
Matrix: Solids
Sampled: 7/ 26/2022 10:13
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Fecal Coliform MPN/g <2,7 MPN/g —dry
Moisture 27.5
2.7 1 07/26/2213:22 SMW 9221E-2011
1 08/04/2210:38 ADC SW-DRYWT
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 7 of 19

Waypoint,(2)
ANALYTICAL
01050
City of Statesville, NC Project
Ken Galloway
693 Bell Farm Road Information
Statesville , NC 28625
Report Number : 22-207-0051
Lab No : 95322
Sample ID : #5
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Sta-Lime Quarterly Tests
REPORT OFANAL YSIS
Report Date : 08/15/2022
Received : 07/26/2022
6OW4
Terri W Cole
Laboratory Project Manager
Matrix: Solids
Sampled: 7/26/ 2022 10:13
Test Results Units MQL DF Date 1 Time By Analytical
Analyzed Method
Fecal CoVorm MPN/g ¢2.7 MPN/g - dry
Mofsture 27.7
Qualifiers/ DF Dilution Factor
Definitions
2.7 1 07/26/2213:22 SMW 9221E-2011
1 08/04/2210:38 ADC SW-DRYWT
MQL Method Quantitation Limit
Page 8 of 19

Waypoint,(D
ANALYTICAL
01050
City of Statesville, NC Project
Ken Galloway
693 Bell Farm Road Information
Statesville , NC 28625
Report Number : 22-207-0051
Lab No : 95323
Sample ID : #6
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6964
www.waypointana lytical.corn
Sta-Lime Quarterly Tests
REPORT OF ANAL Y515
Report Date ; 08/15/2022
Received : 07/26/2022
60
CQ'&
Terri W Cole
Laboratory Project Manager
Matrix: Solids
Sampled: 7/26/ 2022 10:13
Test Results Units MQL DF Date 1 Time By Analytical
Analyzed Method
Fecal Coliform MPN/g <2.2 MPN/g - dry
Moisture 10.4 11/0
Qualifiers/ DF Dilution Factor
Definitions
2.2 1 07/26/22 13:22 SMW 9221E-2011
1 08/04/2210:38 ADC SW-DRYWT
MQL Method Quantitation Limit
Page 9 of 19

Waypointo
ANALYTICAL
01050
City of Statesville, NC
Ken Galloway
693 Bell Farm Road
Statesville , NC 28625
Report Number : 22-207-0051
Lab No : 95324
Sample ID : #7
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Project Sta-Lime Quarterly Tests
Information :
REPORT OF ANAL YSIS
Report Date : 08/15/2022
Received : 07/26/2022
VO
Terri W Cole
Laboratory Project Manager
Matrix: Solids
Sampled: 7/ 26/ 2022 10:13
Test
Results
Units
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Fecal Coiiform MPN/g
¢2.3
MPN/g -dry
2.3
1
07/26/22 13:22
SMW
9221E-2011
Moisture
13.1
%
1
08/04/2210:38
ADC
SW-DRYWT
Nitrate (NO3-N)
48.8
mg/Kg - dry
23.0
10
08/02/22 14:08
CEG
9056A
Nitrite (NO2-N)
<11.5
mg/Kg - dry
11.5
10
09/02/22 14:08
CEG
9056A
Nitrate+ Nitrite-N
48.8
mg/Kg - dry
11.5
10
08/02/22 14:08
9056A
Total Solids
85.7
%
0.010
1
08/02/22 10:10
ADC
254OG-2011
Total Kjeldahl Nitrogen
1830
mg/Kg - dry
57.5
1
08/08/22 11:05
CLP 4500NORGD-2011
Phosphorus
2800
mg/Kg - dry
5.75
1
08/05/22 12:33
6010D
Aluminum
9640
mg/Kg - dry
28.8
5
08/03/22 12:48
EDV
6010D
Arsenic
6.31
mg/Kg - dry
2.88
5
08/03/22 12:0
EDV
6010D
Cadmium
<0.575
mg/Kg - dry
0.575
5
08/03/22 12:48
EDV
6010D
Copper
41.4
mg/Kg - dry
1,44
5
08/03/22 12:48
EDV
6010D
Lead
6.65
mg/Kg - dry
1.73
5
08/03/22 12:48
EDV
6010D
Mercury (Total)
<0.0345
mg/Kg - dry
0.0345
1
08/OS/22 12:05
EDV
7471B
Molybdenum
4.50
mg/Kg - dry
2.88
5
08/03/22 12:48
EDV
6010D
Nickel
9.22
mg/Kg - dry
1.44
5
08/03/22 12:48
EDV
6010D
Potassium
2800
mg/Kg - dry
144
5
09/03/22 12:48
EDV
6010D
Selenium
<2.88
mg/Kg - dry
2.88
5
08/03/22 12:48
EDV
6010D
Sodium
809
mg/Kg - dry
288
5
08/03/22 12:48
EDV
6010D
Zinc
68.8
mg/Kg - dry
2.88
5
08/03/22 12:48
EDV
6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 10 of 19

r
Waypoint
Charlotte, NC 2$217
4A9 SRringbrapk Rd, Ch
Main 704.529.6364
ANALYTICAL
www.waypointanalytical.com
01050
City of Statesville, NC
Project
Sta-Lime
Quarterly Tests
Ken Galloway
Report Date : 08/15/2022
693 Bell Farm Road
information :
Received : 07/26/2022
Statesville , NC 28625
6MU)�
Terri W Cale
Report Number :22-207-0051
REPOR TOF ANAL YSIS
Laboratory Project Manager
Lab No : 95325
Matrix: Solids
Sample ID : #7 SAR
Sampled: 7/26/2022 10:13
Test
Results
Units
MOL
DF Date/Time By Analytical
Analyzed Method
Calcium (saturated paste)
51.2
meq/L
0.250
1 08/03/22 15:00 LMZ Saturate Paste
Magnesium (saturated paste)
0.000
meq/L
0.417
1 08/03/22 15:00 LMZ Saturate Paste
Sodium (saturated paste)
2.85
meq/L
0.217
1 08/03/22 15:00 LMZ Saturate Paste
Sodium Absorption Ratio
0.562
1 08/03/22 15:00 LMZ Saturate Paste
Moisture
13.1
%
1 08/04/2210:38 ADC SW-DRYWT
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 11 of 19

AccEss
ANALYTICAL, INC.
ANALYTICAL REPORT
CLIENT
Waypoint Analytical, LLC (Charlotte)
449 Springbrook Road
Charlotte NC 28217
ATTENTION
Terri W Cale
PROJECT ID
22-207-0051
LABORATORY REPORT NUMBER
2207V44
DATE
August 03, 2022
Primate Data Review By Secondary Data Review By
Ashley Amick
Chris Pafford Project Manager, Access Analytical
Project Manager, AES [e-mail]
PLEASE NOTE:
Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc),
3080 Presidential Drive, Atlanta, CA 30340.
AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, CA certified lab # FL-E87582,
NELAP certified laboratory # E87582
- AIHA-LAP,LLC Laboratory ID:100671 for Industrial Hygiene samples (Organics, Metals, PCAI Asbestos,
Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental microbiology (Fungal)
Direct Examination.
Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a
representative of AES serving client in the SC/NUGA areas. All questions regarding this report should be directed
to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243
Page 12 of 19 Page 1 of 6

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Analytical Environmental Services, Inc
Date: 3-Aug-22
Client:
Waypoint Analytical, LLC (Charlotte)
Client Sample ID:
95324
Lab Order
2207V44
Tag Number:
#7
Project Name:
22-207-0051
Collection Date:
7/26/2022 10:13:00 AM
Lab ID:
2207V44-00IA
Matrix:
Solid
Analyses Result Reporting
y Qual AIDL Units BatchID DF DatcAnalyzed Analyst
Limit
Nitrogen, Ammonia (as N) Extractable E350.1 A[OD (E350.1)
Nitrogen, Ammonia (As N) Extractable 73.9 6.27 12.7 mg/Kg-dry 340523 1 07i29i2022 16:56 KV
PERCENT 1%[OISTURE D2216
Percent Moisture 21A 0 0 % t% R492633 1 OTO1/2022 00:00 AV
Qualifiers: _ Vatue exceeds maximum contaminant level
nRL Not Detected at A[[7L
11 Floldia& vines ror preparation or nnalrsis exceeded
N Anal�ie net NFLAC certified
n Analyte detected in the assuciated method blank
F Estimated value above quint nation range
S Spike Recovery outside limits due to matrix
> Greater than Result value
7 Estimated .Incvdetected below Reporting Limit
< Less than RMIlt value
Page 14 of 19
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End of Report
Page 17 of 19 Page 6 of 6

0
Waypoint
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 01050
Customer Name: City of Statesville, NC
Report Number: 22-207-0051
- Shipping Method
0 Fed Ex 0 US Postal C Lab
0 UPS 0 Client 0 Courier
C) Other:
Thermometer ID:
If3T 15 1.0 C
Shipping container/cooler uncompromised?
C Yes
0 No
Number of coolers/boxes received
�—
Custody seals intact on shipping container/cooler?
U Yes
O No
CO) Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
C Not Present
Chain of Custody (COC) present?
C Yes
0 No
COC agrees with sample label(s)?
C Yes
0 No
COC properly completed
C Yes
0 No
Samples in proper containers?
Yes
0 No
Sample containers intact?
�, Yes
0 No
Sufficient sample volume for indicated test(s)?
C Yes
0 No
All samples received within holding time?
C Yes
0 No
Cooler temperature in compliance?
C Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
CYes
0 No
Water - Sample containers properly preserved
0 Yes
C No
C NIA
Water - VOA vials free of headspace
0 Yes
0 No
C NIA
Trip Blanks received with VOAs
0 Yes
0 No
0 NIA
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
CO) NIA
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
C No
Comments:
Signature: Angela D Overcash _ bate & Time: 07126/2022 12:20:58
Page 18 of 19

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Page 19 of 19

January 31, 2022
Attention: NCDWR
Water Quality Non -Discharge Permitting Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1636
RE: Annual Report for 2022
Alkaline Stabilization (WQ0006245)
To Whom It May Concern:
Enclosed, you will find a copy of the required forms and lab data for the Alkaline Stabilization
program. Permit # WQ0006245.
Should you require more information, or if further action is required, please contact me at 704- 878-3438.
Sincerely
Ken Galloway
WWTP Supervisor, Fourth Creek WWTP

GENERAL INFORMATION
ALKALINE STABLIZATION REPORT
CALENDER YEAR 2022
PERMIT NO. WQ0006245
FACILITY NAME: Fourth Creak WWTP NPDES NCO031836
LOCATION: 693 Bell Farm Road
MAILING ADDRESS: P.O. Box 1111
Statesville, NC 28687-1111
[phone]
RESPONSIBLE OFFICIAL: Andy Smith, Operations Manager
Water Resources
P.O. Box 1111
Statesville, NC 28687-1111
[phone]
FACILITY OPERATOR: Ken Galloway
Plant Supervisor
P.O. Box 1111
Statesville, NC 28687-1111
[phone]
RESIDUALS ORC: Ken Galloway
Plant Supervisor
P.O. Box 1111
Statesville, NC 28687-1111
APPLICATION: Class A Exceptional Quality Product
Test Data and Summary Operations
Attached

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Fourth Creek WWTP AIkaline Stabilization
WWTP Name: Fourth Creek WWTP
WQ Permit Number: WQ0006245
NPDES Number: NCO031836
Monitoring Period: From 1/1/2022
To 12/31/2022
thogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (timattem) [3
Alt B (Alk Treatment) p
Alt. C (Prior Testing)❑...........
A1t.D (No Prior Test) p
Process to Further Reduce Pathogengs ❑
If applicable to alternative Eerformed Class A only Indicate "Process to Further Reduce Pathogens":
Compost 0 Heat Drying ❑ Hoat Treatment Cl
Thennophilic ❑
BetaRay ❑ Gamma Ra ❑ P€tsta ' Y unzation
Y
Class B:
JAIt. (1) Fecal Daasity ❑ Alt. (2) Process to Signifleantly Rerduce Pathogens ❑ ...........
If applicable to alternative performed Class B on indicate "Proms to SILAlficantly Reduce Pathogens":
Lime Stabilization Aix D!ying ❑
composdu Ct
JAcroble Di estion L
Anaerobic Di estiorz
g
:
:..:.•.• ::.....:...................... ...:., ...............
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in
in Sludge
Pathogen Density
Number of
Eacee-
deaces
Frequency
of Analysis
y
Sample
Type
Analytical
Tech -
ie
inim
Gco. Mean
aximt
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
WN
<2 0
<2 7
mpn/g
Quarterly
grab
sm9221
cFu
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform) I
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction)
Alt. 2 (40-day bench)
Alt. 3 (30-day bench) Alt. 4 (Spec. 02 uptake)
AIt. 5 (14-Day Aerobic)
Alt. 6 (Alk. Stabilization M
JAR 7 (Drying - Stable) Alt. 8 (Drying - Unstable)
Alt. 9 (Injection)1
Alt. 10 (Incorporation) Q
INo vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1.107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 an(] the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you cliecic this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designer] to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonnient."
Ken Galloway WWTP Supervisor
Preparer Name and Title e or print)
mature o reparer*
Land Applier Name and Title (if applicable)(type or print)
/ ^-3/ ,?3
Date Signature of Land Applier (if applicable) Date
"Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RVRF 02T (12/2006)

BIN # 7e ff Setup Date: J-gg-, 12
Removal From Bin ®ate: 1.31. ,
Date Time pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial pH: U 11 %
I -AC 12
i • �t'1! �
Corrected pH: /A V-1
'��3 103101
U85
Final pH: 511
Corrected pH: I J. 77
Has 12 Hour Terrin riteria Been
Mot.
BIN #qjve; Setup Date: 1e1V-dj�
I
Removal From Bin Date: f-,z_.'ka
Date
TPr ne pH >12.0 For 72 Firs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
JP�"J�
Initial pH:) , TY
�• a
Corrected pH: f Vi r/
lapp � yy
EJ� �i•I
1.111A kk
t!V
'?(( 4W
�• �a `�
Final pH: 1A. t
Corrected pH: 11,73
aS12 Hour elfiip riteria Been
et.
a5 72 Hour pH Criteria Been @t. '
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
phi >12.0 Foi- 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
I Operator
Initial pH:
Corrected pH:
Final pH:
Corrected pH:
I Has 12 Hour l emp Criteria i3een iviete Y N j
Has 7Z Hour pH Criteria Been ivlet� Y N

City Of Statesville A a ine Stabilization ecor For
Process To Further Reduce Pathogens (PFRP)
BIN # Setup Date:
Removal From Bin Date:
Date Time pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial pH: IZ-. y�
i ��rlrc Corrected pH.' 1 ,Q
� r
Final pH:CorrectedpH:
pr
� "��; )
Has 12 Hour Temp Criteria Been
Met:? Y N
BIN #
Has 72 Hour pR Criteria Been
Setup Date:
et
Removal From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
_{ L
j
Initial p.H.
Corrected pH: 12 _ 2 S
Final pH:
Corrected pH:
as 12 our emp rlteria Been
e .
Has our PH Criteria Been et ,_
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg, C For 12 Hrs.
Operator
s
Initial pH:
Corrected pH:12-99-59
l P
Final pH: `. s
�' -fig.
,
DF,
Corrected pH: r"
Has 1Z Hour I emp L ICeria LseOn Ivlcir"
as our p r er a een e
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
pH >12,0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Firs.
Operator
Initial pH:
Corrected pH:
Final pH:
Corrected pH:
H;i. 1.2 Hnur Tpmn Criteria Been
et.
Has 72 Hour PH Criteria Been et.
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial pH:
Corrected pH:
Final pH:
Corrected pH:
Hai 12 Hnur TPmn Criteria Been
Met. Y N
Has 72 Hour pH rlteria Been Met. Y N

y UT bTaTesville AlKaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN # j
Setup Date:
Removal From Bin Date:
Date Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
/
Initial pH: 2 • �
���� r�`;�
Corrected pH:
to4
Final pH: L
Corrected pH:
Has f2 R—our Ternp Criteria
een et.
Has Hour p rlteria een et.
BIN # ;7,00
Setup Date:
Removal From Bin Date:
Date I Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 lirs.
Operator
Initial pH:
OW
Corrected PH. I
t
Final pH:
Corrected pH:3�a
I ryas iz Hour I emp Lrlterja Keen ivietr W Iv I
F Has 7Z Hour pH Lriteria Keen Ivied () IN I
BIN # r{3
Setup Date:
Removal From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs,
Operator
Initial pH: %21 f'
Corrected pH: 12 -'
Final PH: 12,67
�
Corrected pH:
;;s 12 Anur Terno Criteria Been
et.
1 - f p. e 7 T
BIN ## '+
Setup Date:
Removal From Bin bate:
Date
I Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Firs.
Operator
I,
� �`
1
Initial H: � ,
p
t �' -
7 6
k
Corrected pH:
1,_ a,
Final pH: f
`'�F'#
�If
f
Iias Lz riour ittm#a UriWrici D1=11 IVI=L9 r F it
Has 7Z Hour pH Criteria Been et.
BIN # f
ISetup Date:
Removal From Bin Date:
Date
I Time
pH >1.2•.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
,.
Initial pH: j�t�
9.1 �� "'-
Corrected pH: [—
,2 2L}
l i
Final pH:
Corrected pH: r
i
v
T
Wnc Wm it Tprnn Uritpria Been
et. 69N
Has 72 Hour pH Criteria Been Met. Y N

City Ot Statesville Alkaline to I ization Record For
Process To Further Reduce Pathogens (PFRP)
BIN # Isetup Date: Removal From Bin Date:
Date Time I pH >12.0 For 72 Hrs. TEMP. >52 Deg. CFor12 Hrs. operator
Initial pH:
Corrected pH:
Final pH:
Corrected pH:
Has 17 Hour Ternp Criteria Been et. Y N
Has 72 Hour pH Criteria een Met Y N
BIN #
Setup Date:
Removal From Bin Date:
Date Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial pH:
Corrected pH:
Final pH:
Corrected pH:
Has 12 Hour Terrib riteria
een et.
Has 72. Hour p rlteria een et
BIN #
Setup Date:
Removal From Bin Date:
Date I Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial pH:
Corrected pH:
Final pH:
Corrected pH:
---Has 12 Hour Temn Criteria Been
eth
Has 72 Hour PH Criteria Been et.
OIN #
ISetup Date:
lRernoval From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial pH:
Corrected pal:
Final pH:
Corrected pH:
Has 12 Hour Torno Criteria Been
et. Y
Has our pH Criteria een et.
13IN #
Isetup Date:
Removal From Bin Date:
Date
Time
I pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial pH:
Corrected pH:
Final pH:
Corrected pH:
I I U ^ i iv "i'nsv,r, ri� +jn%-ji. ft.inY►
ll/in
Has 72 Hour pH Criteria Been Met. Y N
n, A