NC0080853_Application_20230302

/� _COM Imagine it.
/�+�� Delivered.
March 2, 2023
Mr. Douglas Dowden
Division of Water Quality / Permitting
North Carolina Department of Environmental Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Subject: NPDES Permit Renewal
Permit NCO080853
Salem Business Park Remediation Site
Nokia of America Corporation (Former Alcatel -Lucent Facility)
Winston-Salem, Forsyth County, North Carolina
Dear Mr. Dowden:
AECOM
5438 Wade Park Blvd, Suite 200
Raleigh, NC 27607
T 919.461.1100
F 919.461.1415
aecom.com
On behalf of Nokia of America Corporation (Nokia), please find the attached permit renewal package for
Permit NCO080853 for treatment of groundwater containing chlorinated volatile organic compounds
(cVOCs). There are no proposed changes to the current permitted operation of the groundwater treatment
system featuring a low -profile air stripper. Updates since the previous permit was issued on January 2,
2019, are summarized as follows:
• Granulated Activated Carbon (GAC) was recognized as back-up in the prior permit, available in the
event of an increase in influent contaminant concentrations. GAC carbon has not been used during
the current permit term.
On March 22, 2021, AECOM notified the Water Quality Permitting section of the North Carolina
Department of Environmental Quality (NCDEQ) of Nokia's intention to discontinue filtration in the
treatment process. AECOM noted that the filters were part of the permitted treatment system primarily
to prevent clogging within the GAC treatment units. Removal of the GAC units from normal operation
eliminated the need to maintain the filtration units. They remain in the treatment building but have
been bypassed, as was approved by the Water Quality Permitting section by email the same day that
the request was made.
• Chemical additives formerly added to control fouling were eliminated prior to the January 2019 permit.
As was confirmed by email correspondence with the Water Quality Permitting section on February 13,
2023, no additional analyses beyond what is required under the permit is necessary for this submittal.
Representative analytical reports from December 2022 for influent, effluent, and discharge (Sample ID FE-
151) are included in this attachment. Further analytical reports are available upon request.
If you have any questions or need additional information, please contact Conan Fitzgerald at (919) 461-
1260.
Yours sincerely,
Conan Fitz e "" d� John Moran El
g ,
AVP - Engineering Environmental Engineer
cc: John Galasso — Nokia of America Corporation

EPA Identification Number
NPDES Permit Number
Facility Name
Form Approved 03/05/19
NCDO03213907
NCO080853
Salem Bus. Park Remediation
OMB No. 2040-0004
Form
U.S. Environmental Protection Agency
1
\�/EPA
Application for NPDES Permit to Discharge Wastewater
NPDES
GENERAL INFORMATION
SECTION•
-•
1.1
Applicants Not Required to Submit Form 1
1.1.1
Is the facility a new or existing publicly owned
1.1.2
Is the facility a new or existing treatment works
treatment works?
treating domestic sewage?
If yes, STOP. Do NOT complete ❑✓ No
If yes, STOP. Do NOT ✓❑ No
Form 1. Complete Form 2A.
complete Form 1. Complete
Form 2S.
1.2
Applicants Required to Submit Form 1
1.2.1
Is the facility a concentrated animal feeding
1.2.2
Is the facility an existing manufacturing,
operation or a concentrated aquatic animal
commercial, mining, or silvicultural facility that is
a
production facility?
currently discharging process wastewater?
o❑
Yes 4 Complete Form 1 ❑✓ No
❑ Yes 4 Complete Form No
a
and Form 2B.
1 and Form 2C.
z
1.2.3
Is the facility a new manufacturing, commercial,
1.2.4
Is the facility a new or existing manufacturing,
mining, or silvicultural facility that has not yet
commercial, mining, or silvicultural facility that
commenced to discharge?
discharges only nonprocess wastewater?
Yes 4 Complete Form 1 ❑✓ No
❑ Yes 4 Complete Form No
and Form 2D.
1 and Form 2E.
Vl
1.2.5
Is the facility a new or existing facility whose
'—
discharge is composed entirely of stormwater
a
associated with industrial activity or whose
discharge is composed of both stormwater and
non-stormwater?
Yes -+ Complete Form 1 ❑✓ No
and Form 2F
unless exempted by
40 CFR
122.26(b)(14)(x) or
b (15).
SECTIONDD-
• • i
2.1
Facility Name
Salem Business Park Remediation Site
0
2.2
EPA Identification Number
;5
V
C
J
NCDO03213907
2.3
Facility Contact
fp
L
Name (first and last)
Title
Phone number
Q
John Galasso
Remediation Manager
[phone]
Email address
[e-mail]
2.4
Facility Mailing Address
ZStreet
or P.O. box
600 Mountain Avenue
City or town
State
ZIP code
Murray Hill
New Jersey
07974
EPA Form 3510-1 (revised 3-19) Page 1

EPA Identification Number
NPDES Permit Number
Facility Name
Form Approved 03/05/19
NCDO03213907
NCO080853
Salem Bus. Park Remediation
OMB No. 2040-0004
y
2.5
Facility Location
Street, route number, or other specific identifier
Q 0
3370 Lexington Road
rn
0
County name
County code (if known)
Forsythe
E
City or town
State ZIP code
z @
Winston-Salem
North Carolina 27107
SECTIONI
NAICS CODES1
3.1
SIC Code(s)
Description (optional)
5629
Remediation
w
a
0
U
N
U
z
3.2
NAICS Code(s)
Description (optional)
U
562910
Remediation Services
N
4.1
Name of Operator
AECOM Technical Services of North Carolina, Inc.
0
4.2
Is the name you listed in Item 4.1 also the owner?
r
R
0
❑ Yes ❑✓ No
0
4.3
Operator Status
S
R
❑ Public —federal ❑ Public —state ❑ Other public (specify)
o
❑✓ Private ❑ Other (specify)
4.4
Phone Number of Operator
[phone]
4.5
Operator Address
Street or P.O. Box
E m
3458 Wade Park Blvd
;0
City or town
State
ZIP code
o 0
m
Raleigh
INC
27607
Q
Email address of operator
O
[e-mail]
SECTION1
0
5.1
Is the facility located on Indian Land?
❑ Yes ❑✓ No
EPA Form 3510-1 (revised 3-19) Page 2

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCDO03213907 NCO080853 Salem Bus. Park Remediation OMB No. 2040-0004
'ECTION 6. EXISTING ENVIRONMENTAL1
6.1 Existing Environmental Permits (check all that apply and print or type the corresponding permit number for each)
❑ NPDES (discharges to surface
❑ RCRA (hazardous wastes)
❑ UIC (underground injection of
r_
water)
fluids)
•�—y
> E
NCO080853
NCDO032139907
w a
rn
ElPSD (air emissions)
❑ Nonattainment program (CAA)
ElNESHAPs (CAA)
c
x
❑ Ocean dumping (MPRSA)
❑ Dredge or fill (CWA Section 404)
❑ Other (specify)
LU
7.1 Have you attached a topographic map containing all required information to this application? (See instructions for
C specific requirements.)
2
✓❑ Yes ❑ No ❑ CAFO—Not Applicable (See requirements in Form 213.)
8.1 Describe the nature of your business.
Groundwater recovery and treatment system to address legacy groundwater contamination by chlorinated solvents
y System operation is required under the RCRA permit.
9.1 Does your facility use cooling water?
L ❑ Yes ❑✓ No -* SKIP to Item 10.1.
L
9.2 Identify the source of cooling water. (Note that facilities that use a cooling water intake structure as described at
a, 40 CFR 125, Subparts I and J may have additional application requirements at 40 CFR 122.21(r). Consult with your
oY NPDES permitting authority to determine what specific information needs to be submitted and when.)
U
10.1 Do you intend to request or renew one or more of the variances authorized at 40 CFR 122.21(m)? (Check all that
y apply. Consult with your NPDES permitting authority to determine what information needs to be submitted and
when.)
❑ Fundamentally different factors (CWA ❑ Water quality related effluent limitations (CWA Section
Section 301(n)) 302(b)(2))
❑ Non -conventional pollutants (CWA ❑ Thermal discharges (CWA Section 316(a))
Section 301(c) and (g))
❑✓ Not applicable
EPA Form 3510-1 (revised 3-19) Page 3

EPA Identification Number
NPDES Permit Number
Facility Name Form Approved 03/05/19
NCD003213907
NC0080853
Salem Bus. Park Remediation OMB No. 2040-0004
SECTION•
1
11.1
In Column 1 below, mark the sections of Form 1 that you have completed and are submitting with your application.
For each section, specify in Column 2 any attachments that you are enclosing to alertthe permitting authority. Note
that not all applicants are required to provide attachments.
Column 1
Column 2
Section 1: Activities Requiring an NPDES Permit
❑ wl attachments
❑ Sections 2: Name, Mailing Address, and Location
❑ wi attachments
Section 3: SIC Codes
❑ wl attachments
❑✓ Section ?: Operator Information
❑ wl attachments
Section 5: Indian Land
❑ wl attachments
❑ Section 6: Existing -Environmental Permits
❑ w1 attachments
XD
E
❑✓ Section 7: Map
wl topographic
❑✓ additional attachments
is
mapElw/
Section 8: Nature of Business
❑ wi attachments
'
❑ Section 9: Cooling Water intake Structures
❑ wi attachments
_d
a
0 Section 10: Variance Requests
❑ wl attachments
0 Section 11: Checklist and Certification Statement
❑ w/ attachments
11.2
Certification Statement
1 certify under penalty of law that this document and al/ attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the
information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and
belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fine and imprisonment for knowing violations.
Name (print or type first and last name)
Official title
Yt�
Signature
Date signed 11
EPA Form 3510-1 (revised 3-19) Page 4

Salem Business Park - NCO080853
USGS Quad Name: Winston-Salem East Lat.: 36003'18"
Receiving Stream: UT Salem Creek Long.: 80013'51"
Stream Class: C
Subbasin: Yadkin Pee Dee — 030704
Facility
Location Aw"
North Not to SCALE

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCDO03213907 NCO080853 Salem Bus. Park Remediation OMB No. 2040-0004
Form U.S. Environmental Protection Agency
2C EPf1 Application for NPDES Permit to Discharge Wastewater
NPDES EXISTING MANUFACTURING, COMMERCIAL, MINING, AND SILVICULTURE OPERATIONS
SECTIONOUTFALL LOCATION1
1.1 Provide information on each of the facility's outfalls in the table below.
Outfa
Nu ber Receiving Water Name Latitude Longitude
0 J 001 Salem Creek 30' 03' 18" IN80' 13' 51.1" W
12
7
O
o 0
SECTIOND' 1
a, 2.1 Have you attached a line drawing to this application that shows the water flow through your facility with a water
3 balance? (See instructions for drawing requirements. See Exhibit 2C-1 at end of instructions for example.)
J `
o ❑✓ Yes ❑ No
SECTION• 1
3.1 For each outfall identified under Item 1.1, provide average flow and treatment information. Add additional sheets if
necessary.
**Outfall Number** 001
Operations Contributing to Flow
Operation Average Flow
Groundwater Extraction 0.07 mgd
Y
E mgd
R
d
mgd
y mgd
3
0 Treatment Units
U_
a, Description Code from Final Disposal of Solid or
(include size, flow rate through each treatment unit, Table 2C-1 Liquid Wastes Other Than
> retention time, etc.) by Discharge
1000 Gallon Feed Water Equalization Tank Non -hazardous solid waste
2 Bag Filters in Series (0 GPM - Bypassed) 1-M None - Bypassed
120 GPM Low Profile Six Tray Air Stripper ST Non -hazardous solid waste
Granular Activated Carbon (currently Bypassed) 2-A None - Bypassed
EPA Form 3510-2C (Revised 3-19) Page 1

EPA Identification Number
NPDES Permit Number
Facility Name
Form Approved 03/05/19
NCDO03213907
NCO080853
Salem Bus. Park Remediation
OMB No. 2040-0004
3.1
**Outfall Number**
cont.
Operations
,
Operation
Average Flow
mgd
mgd
mgd
mgd
Treatment
Description
Units
Code from
Final Disposal of Solid or
(include size, flow rate through each treatment unit,
Table 2C-1
Liquid Wastes Other Than
retention time, etc.)
by Discharge
0
CU
w.
c
a>
E
w.
a
a>
L
**Outfall Number**
Operations
o
Operation
Average Flow
U-
mgd
L
d
<
mgd
mgd
mgd
Treatment
Description
Units
Code from
Final Disposal of Solid or
(include size, flow rate through each treatment unit,
Table 2C-1
Liquid Wastes Other Than
retention time, etc.)
by Discharge
3.2
Are you applying for an NPDES permit to operate a privately owned treatment works?
j2
❑✓ Yes ❑ No 4 SKIP to Section 4.
N3.3
Have you attached a list that identifies each user of the treatment works?
❑✓ Yes ❑ No
EPA Form 3510-2C (Revised 3-19) Page 2

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCDO03213907 NCO080853 Salem Bus. Park Remediation OMB No. 2040-0004
SECTION• I
4.1 Except for storm runoff, leaks, or spills, are any discharges described in Sections 1 and 3 intermittent or seasonal?
❑ Yes ❑✓ No 4 SKIP to Section 5.
4.2
Provide information
on intermittent or seasonal flows for each applicable outfall. Attach additional pages, if necessar .
Outfall
Operation
Frequency
Flow
Rate
Average
Average
Long -Term
Maximum
Number
(list)
Duration
Da sMeek
MonthsNear
Average
Dail
days/week
months/year
mgd
mgd
days
c
days/week
months/year
mgd
mgd
days
U_
days/week
months/year
mgd
mgd
days
w
E
days/week
months/year
mgd
mgd
days
w
c
days/week
months/year
mgd
mgd
days
days/week
months/year
mgd
mgd
days
days/week
months/year
mgd
mgd
days
days/week
months/year
mgd
mgd
days
days/week months/year mgd mgd days
SECTION•••1
• I
5.1
Do any effluent limitation guidelines (ELGs) promulgated by EPA under Section 304 of the CWA apply to your facility?
❑ Yes ❑✓ No 4 SKIP to Section 6.
5.2
Provide the following information on applicable ELGs.
i
ELG Category
ELG Subcategory
Regulatory Citation
w
n
ca
Q
CL
5.3
Are any of the applicable ELGs expressed in terms of production (or other measure of operation)?
❑ Yes ❑✓ No 4 SKIP to Section 6.
0
5.4
Provide an actual measure of daily production expressed in terms and units of applicable ELGs.
J
Outfall
Operation, Product, or Material
Quantity per Day
Unit of
Number
Measure
d
m
0
w
c.�
0
L
a
EPA Form 3510-2C (Revised 3-19) Page 3

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCDO03213907 NCO080853 Salem Bus. Park Remediation OMB No. 2040-0004
SECTION • 1
6.1 Are you presently required by any federal, state, or local authority to meet an implementation schedule for constructing,
upgrading, or operating wastewater treatment equipment or practices or any other environmental programs that could
affect the discharges described in this application?
❑ Yes ❑✓ No 4 SKIP to Item 6.3.
6.2
Briefly identify each applicable project in the table below.
Affected
Final Compliance Dates
E
Brief Identification and Description of
Outfalls
Source(s) of
oProject
(list outfall
Discharge
Required
Projected
CL
number
E
M
CL
CL
6.3
Have you attached sheets describing any additional water pollution control programs (or other environmental projects
that may affect your discharges) that you now have underway or planned? (optional item)
❑ Yes ❑ No ✓❑ Not applicable
SECTION
7. EFFLUENT AND INTAKE CHARACTERISTICS i
See the instructions to determine the pollutants and parameters you are required to monitor and, in turn, the tables you must
complete. Not all applicants need to complete each table.
Table A. Conventional and Non -Conventional Pollutants
7.1
Are you requesting a waiver from your NPDES permitting authority for one or more of the Table A pollutants for any of
your outfalls?
❑✓ Yes ❑ No -* SKIP to Item 7.3.
7.2
If yes, indicate the applicable outfalls below. Attach waiver request and other required information to the application.
Outfall Number 001 Outfall Number Outfall Number
7.3
Have you completed monitoring for all Table A pollutants at each of your outfalls for which a waiver has not been
requested and attached the results to this application package?
L
2
No; a waiver has been requested from my NPDES
✓❑ Yes ❑
R
permitting authority for all pollutants at all outfalls.
Table B.
Toxic Metals, Cyanide, Total Phenols, and Organic Toxic Pollutants
7.4
Do any of the facility's processes that contribute wastewater fall into one or more of the primary industry categories
=
listed in Exhibit 2C-3? (See end of instructions for exhibit.)
R
❑ Yes ✓❑ No -* SKIP to Item 7.8.
7.5
Have you checked "Testing Required" for all toxic metals, cyanide, and total phenols in Section 1 of Table B?
LU
❑ Yes ❑ No
7.6
List the applicable primary industry categories and check the boxes indicating the required GC/MS fraction(s) identified
in Exhibit 2C-3.
Primary Industry Category
Required GC/MS Fraction(s)
Check applicable boxes.
❑ Volatile ❑ Acid ❑ Base/Neutral ❑ Pesticide
❑ Volatile ❑ Acid ❑ Base/Neutral ❑ Pesticide
❑ Volatile ❑ Acid ❑ Base/Neutral ❑ Pesticide
EPA Form 3510-2C (Revised 3-19) Page 4

EPA Identification Number
NPDES Permit Number
Facility Name
Form Approved 03/05/19
NCDO03213907
NCOO8O853
Salem Bus. Park Remediation
OMB No. 2040-0004
7.7
Have you checked "Testing Required" for all required pollutants in Sections 2 through 5 of Table B for each of the
GC/MS fractions checked in Item 7.6?
❑ Yes ❑ No
7.8
Have you checked "Believed Present' or "Believed Absent' for all pollutants listed in Sections 1 through 5 of Table B
where testing is not required?
❑✓ Yes ❑ No
7.9
Have you provided (1) quantitative data for those Section 1, Table B, pollutants for which you have indicated testing is
required or (2) quantitative data or other required information for those Section 1, Table B, pollutants that you have
indicated are `Believed Present' in your discharge?
✓❑ Yes ❑ No
7.10
Does the applicant qualify for a small business exemption under the criteria specified in the instructions?
❑ Yes -* Note that you qualify at the top of Table B, ❑✓ No
then SKIP to Item 7.12.
7.11
Have you provided (1) quantitative data for those Sections 2 through 5, Table B, pollutants for which you have
c
determined testing is required or (2) quantitative data or an explanation for those Sections 2 through 5, Table B,
pollutants you have indicated are "Believed Present' in your discharge?
y
✓❑ Yes ❑ No
Table C. Certain Conventional and Non -Conventional Pollutants
7.12
Have you indicated whether pollutants are "Believed Present' or "Believed Absent' for all pollutants listed on Table C
for all outfalls?
U
❑ Yes ❑✓ No
Y
c
7.13
Have you completed Table C by providing (1) quantitative data for those pollutants that are limited either directly or
indirectly in an ELG and/or (2) quantitative data or an explanation for those pollutants for which you have indicated
"Believed Present'?
d
❑ Yes ❑✓ No
LU
Table D. Certain Hazardous Substances and Asbestos
7.14
Have you indicated whether pollutants are "Believed Present' or "Believed Absent' for all pollutants listed in Table D for
all outfalls?
❑ Yes ❑✓ No
7.15
Have you completed Table D by (1) describing the reasons the applicable pollutants are expected to be discharged
and (2) by providing quantitative data, if available?
❑ Yes ❑✓ No
Table E. 2,3,7,8-Tetrachlorodibenzo-p-Dioxin 2,3,7,8-TCDD
7.16
Does the facility use or manufacture one or more of the 2,3,7,8-TCDD congeners listed in the instructions, or do you
know or have reason to believe that TCDD is or may be present in the effluent?
❑ Yes 4 Complete Table E. ❑✓ No -* SKIP to Section 8.
7.17
Have you completed Table E by reporting qualitative data for TCDD?
❑ Yes ❑ No
SECTIONOR
MANUFACTURED TOXICSi
8.1
Is any pollutant listed in Table B a substance or a component of a substance used or manufactured at your facility as
an intermediate or final product or byproduct?
3
❑ Yes ❑✓ No HI► SKIP to Section 9.
3
8.2
List the pollutants below.
1. 4. 7.
0
2. 5. 8.
fp
3. 6. 9.
EPA Form 3510-2C (Revised 3-19) Page 5

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCDO03213907 NCO080853 Salem Bus. Park Remediation OMB No. 2040-0004
SECTION' BIOLOGICAL TOXICITY1
9.1 Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made
within the last three years on (1) any of your discharges or (2) on a receiving water in relation to your discharge?
U) ❑✓ Yes ❑ No 4 SKIP to Section 10.
U.
W
9.2
Identify the tests and their
purposes below.
Submitted to NPDES
.5
Test(s)
Purpose of Test(s)
Date Submitted
x
Permitting Authority?
0
H
INC Phs II Chronic Whole
Multiple Concentration
✓❑ Yes ❑ No
02/02/2023
.I
2
Effluent Toxicity
following recent Failure
0
m
INC Phs II Chronic Whole
Permit re uired quarterly
q q Y
✓❑ Yes ❑ No
01/27/2023
Effluent Toxicity
analyses
NC Phs II Chronic Whole Multiple Concentration ✓❑ Yes ❑ No 12/20/2022
Effluent Toxicity following recent Failure
SECTION1
CONTRACT
ANALYSES (40
10.1
Were any of the analyses reported in Section 7 performed by a contract laboratory or consulting firm?
❑✓ Yes ❑ No 4 SKIP to Section 11.
10.2
Provide information for each contract laboratory or consulting firm below.
Laboratory Number 1
Laboratory Number 2
Laboratory Number 3
Name of laboratory/firm
pace Analytical Services, LLC
ETT Environmental Inc.
d
Laboratory address
9800 Kincey Ave. Ste 100
4 Craftsman Court
Q
Huntersville INC 28078
Greer SC 29605
i�
0
L
i5
0
Phone number
[phone]
[phone]
Pollutant(s) analyzed
VOCs by EPA 8260D
North Carolina Phase II Chronic
HEM, Oil & Grease by 1664E
Whole Effluent Toxicity
TSS by SM2540D-2015
SECTIONDD
• •R• I
11.1
Has the NPDES permitting authority requested additional
information?
❑ Yes
❑✓ No 4 SKIP to Section 12.
0
L
11.2
List the information requested and attach it to this application.
?
1. 4.
0
2. 5.
3. 6.
EPA Form 3510-2C (Revised 3-19) Page 6

EPA Identification Number
NPDES Permit Number Facility Name Form Approved 03/05/19
NCDO03213907
NCO080853 Salem Bus. Park Remediation OMB No. 2040-0004
SECTION1
CERTIFICATION STATEMENT (40 and o
12.1
In Column 1 below, mark the sections of Form 2C that you have completed and are submitting with your application.
For each section, specify in Column 2 any attachments that you are enclosing to alert the permitting authority. Note
that not all applicants are required to com fete all sections or provide attachments.
Column 1
Column'2
✓❑ Section 1: Outfall Location
❑ wf attachments
❑✓ Section 2: Line Drawing
❑ w/ line drawing ❑✓ w/ additional attachments
Section 3: Average Flows and
❑✓
w/ list of each user of
❑ w/ attachments ❑ privately owned treatment
Treatment
works
❑✓ Section 4: Intermittent Flows
❑ w/ attachments
❑✓ Section 5: Production
❑ wl attachments
w/ optional additional
❑✓ Section 6: Improvements
❑ w/ attachments ❑ sheets describing any
additional pollution control
plans
❑ w/ request for a waiver and ❑ w/ explanation for identical
supporting information outfalls
d
w/ small business exemption w/ other attachments
❑ ❑
request
✓❑ Section 7: Effluent and Intake
❑✓ w/ Table A ❑✓ w/ Table B
Characteristics
❑ w/ Table C ❑ w/ Table D
v
w/ Table E w/ analytical results as an
❑ ❑
attachment
_
Section 8: Used or Manufactured
❑✓
❑ wl attachments
N
Toxics
Y
Section 9: Biological Toxicity
❑
❑ w/ attachments
Tests
c.�
❑✓ Section 10: Contract Analyses
❑ w/ attachments
0 Section 11: Additional Information
❑ w/ attachments
❑ Section 12: Checklist and
❑ wl attachments
Certification Statement
12.2
Certification Statement
l certify under penalty of law that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly
responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fine and imprisonment for knowing violations.
Name (print first and last name)
Official title
6— toorrttyypF
io 6ro, � 6t 0
0,4naq,!�,�
Sign a
Date signed
7 A 9 k11--'
-3 — ( rz3
L-v 'I -
EPA Form 3510-2C (Revised 3-19) Page 7

This page intentionally left blank.

EPA Identification Number NPDES Permit Number Facility Name Outfall Number
NCDO03213907 NCO080853 Salem Bus. Park Remediation
Form Approved 03/05/19
OMB No. 2040-0004
• •
• • • ' • I
Effluent
Intake
Waiver
o tional
Maximum
Maximum
Long -Term
IE01
Pollutant
Requested Units
(specify)
Daily
Monthly
Average Daily
Number of
Long -Term
Number of
(if applicable)
Discharge
Discharge
Discharge
Analyses
Average Value
Analyses
(required)
if available
if available
Check here if you have applied to your NPDES permitting authority for a waiver for all of the pollutants listed on this table for the noted outfall.
1
Biochemical oxygen demand
Concentration
Mass
(BOD5)
2
Chemical oxygen demand
❑✓
Concentration
Mass
(COD)
Concentration
3.
Total organic carbon (TOC)
✓❑
Mass
Concentration
mg/L
<2.5
12
4.
Total suspended solids (TSS)
❑
Mass
Concentration
5.
Ammonia (as N)
✓❑
Mass
6.
Flow
❑
Rate
MGD
0.077
361
Temperature (winter)
❑✓
°C
°C
7.
Temperature (summer)
✓❑
°C
°C
pH (minimum)
✓❑
Standard units
s.u.
8.
pH (maximum)
✓❑
Standard units
I s.u.
1 Sampling shall be conducted according to sufficiently sensitive test procedures (i.e., methods) approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR chapter I, subchapter N or 0. See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2C (Revised 3-19) Page 9

This page intentionally left blank.

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCDO03213907 NCO080853 Salem Bus. Park Remediation OMB No.2040-0004
Presence or Absence
Intake
check one
Effluent
(optional)
Pollutant/Parameter
Testing
Units
Maximum
Maximum
Long -Term
Long -
(and CAS Number, if available)
Required
Believed
Believed
(specify)
Daily
Mony
thl
Average
Number
Term
Number
Present
Absent
Discharge
Discharge
Daily
of
Average
of
(required)
(if available)
Discharge
Analyses
Value
Analyses
if available
❑ Check here if you qualify as a small business per the instructions to Form 2C and, therefore, do not need to submit quantitative data for any of the organic toxic pollutants in Sections
2 through 5 of this table. Note, however, that you must still indicate in the appropriate column of this table if you believe any of the pollutants listed are present in your discharge.
Section 1. Toxic Metals, Cyanide, and Total Phenols
1.1
Antimony, total
Concentration
Mass
(7440-36-0)
1.2
Arsenic, total
Concentration
Mass
(7440-38-2)
1.3
Beryllium, total
❑
❑
✓❑
Concentration
Mass
(7440-41-7)
1.4
Cadmium, total
El
El
✓
Concentration
Mass
(7440-43-9)
1.5
Chromium, total
❑
❑
✓❑
Concentration
Mass
(7440-47-3)
1.6
Copper, total
Concentration
Mass
(7440-50-8)
1.7
Lead total
✓
Concentration
Mass
(7439-92-1)
1.8
Mercury, total
Concentration
Mass
(7439-97-6)
1.9
Nickel, total
❑
❑
✓❑
Concentration
Mass
(7440-02-0)
1.10
Selenium, total
❑
El✓❑
Concentration
Mass
(7782-49-2)
1.11
Silver, total
Concentration
Mass
(7440-22-4)
EPA Form 3510-2C (Revised 3-19) Page 11

EPA Identification Number
NCDO03213907
Permit Number
NCO080853
Facility Name Outfall Number
Salem Bus. Park Remediation
Form Approved 03/05/19
OMB No. 2040-0004
Presence or Absence
Intake
check one
Effluent
(optional)
Pollutant/Parameter
Testing
Units
Maximum
Maximum
Long -Term
Long -
(and CAS Number, if available)
Required
Believed
Believed
(specify)
Daily
Monthly
Average
Number
Term
Number
Present
Absent
Discharge
Discharge
Daily
of
Average
of
(required)
(if available)
Discharge
g
Analyses
Value
Analyses
f available
1.12
Thallium, total
El
El
IZI
Concentration
Mass
(7440-28-0)
1.13
Zinc total
❑
❑
❑✓
Concentration
Mass
(7440-66-6)
1.14
Cyanide, total
El
❑
0Concentration
Mass
(57-12-5)
1.15
Phenols, total
❑
❑
❑✓
Concentration
Mass
Section 2.Organic Toxic Pollutants (GC/MS Fraction
—Volatile Compounds)
2.1
Acrolein
Concentration
Mass
(107-02-8)
2 2
Acrylonitrile
Concentration
Mass
(107-13-1)
2.3
Benzene
❑
❑
❑✓
Concentration
Mass
(71-43-2)
2.4
Bromoform
❑
❑
Concentration
Mass
(75-25-2)
2.5
Carbon tetrachloride
❑
❑
❑✓
Concentration
Mass
(56-23-5)
2 6
Chlorobenzene
Concentration
Mass
(108-90-7)
2.7
Chlorodibromomethane
1:1
El
✓
Concentration
Mass
(124-48-1)
2.8
Chloroethane
❑
❑
❑✓
Concentration
Mass
(75-00-3)
EPA Form 3510-2C (Revised 3-19) Page 12

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCDO03213907 NCO080853 Salem Bus. Park Remediation OMB No. 2040-0004
Presence or Absence
Intake
check one
Effluent
(optional)
Pollutant/Parameter
Testing
Units
Maximum
Maximum
Long -Term
Long -
(and CAS Number, if available)
Required
Believed
Believed
(specify)
Daily
Monthly
Average
Number
Term
Number
Present
Absent
Discharge
Discharge
Daily
of
Average
of
(required)
(if available)
Discharge
g
Analyses
Value
Analyses
f available
2.9
2-chloroethylvinyl ether
❑
❑
❑✓
Concentration
Mass
(110-75-8)
2.10
Chloroform (67-66-3)
❑
❑
❑✓
Concentration
Mass
2.11
Dichlorobromomethane
❑
❑
❑✓
Concentration
Mass
(75-27-4)
212
11-dichloroethane
❑
❑
❑
Concentration
Mass
(75-34-3)
2.13
1,2-dichloroethane
❑
El
❑✓
Concentration
Mass
(107-06-2)
2.14
1,1-dichloroethylene
❑
El
❑
Concentration
Mass
(75-35-4)
2.15
12-dichloropropane
❑
❑
❑✓
Concentration
Mass
(78-87-5)
2.16
13-dichloropropylene
❑
❑
❑✓
Concentration
Mass
(542-75-6)
2.17
Ethylbenzene
❑
❑
❑✓
Concentration
Mass
(100-41-4)
2.18
Methyl bromide
Concentration
Mass
(74-83-9)
2.19
Methyl chloride
Concentration
Mass
(74-87-3)
2.20
Methylene chloride
Concentration
Mass
(75-09-2)
2.21
1 1,2 2- tetrachloroethane
El
❑
❑✓
Concentration
Mass
(79-34-5)
EPA Form 3510-2C (Revised 3-19) Page 13

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCDO03213907 NC0080853 Salem Bus. Park Remediation OMB No. 2040-0004
Presence or Absence
Intake
check one
Effluent
(optional)
Pollutant/Parameter
Testing
Units
Maximum
Maximum
Long -Term
Long -
(and CAS Number, if available)
Required
Believed
Believed
(specify)
Daily
Monthly
Average
Number
Term
Number
Present
Absent
Discharge
Discharge
Daily
of
Average
of
(required)
(if available)
Discharge
Analyses
Value
Analyses
f available
2.22
Tetrachloroethylene
❑✓
❑
❑
Concentration
ug/L
2.7
Mass
gram
0.2
(127-18-4)
2.23
Toluene
❑
❑
❑
Concentration
Mass
(108-88-3)
2.24
1 2-trans-dichloroethylene
❑
❑
❑✓
Concentration
Mass
(156-60-5)
2.25
1 1,1-trichloroethane
❑
El❑
Concentration
Mass
(71-55-6)
2.26
1 1,2-trichloroethane
❑
El
❑✓
Concentration
Mass
(79-00-5)
2.27
Trichloroethylene
❑
❑
❑
Concentration
Mass
(79-01-6)
2.28
Vinyl chloride
❑
❑
❑✓
Concentration
Mass
(75-01-4)
Section 3.Organic Toxic Pollutants (GC/MS Fraction
—Acid Compounds)
3.1
2-chlorophenol
❑
❑
❑✓
Concentration
Mass
(95-57-8)
24-dichlorophenol
✓
Concentration
Mass
63.2 20-83-2)
.3
1:1
El
✓
Concentration
Mass
6324-dimethylphenol
05-67-9)
3.4
4 6-dinitro-o-cresol
Concentration
Mass
(534-52-1)
3.5
2 4-dinitrophenol
❑
❑
❑✓
Concentration
Mass
(51-28-5)
EPA Form 3510-2C (Revised 3-19) Page 14

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCDO03213907 NCO080853 Salem Bus. Park Remediation OMB No.2040-0004
Presence or Absence
Intake
check one
Effluent
(optional)
Pollutant/Parameter
Testing
Units
Maximum
Maximum
Long -Term
Long -
(and CAS Number, if available)
Required
Believed
Believed
(specify)
Daily
Monthly
Average
Number
Term
Number
Present
Absent
Discharge
Discharge
Daily
of
Average
of
(required)
(if available)
Discharge
g
Analyses
Value
Analyses
f available
3.6
2-nitrophenol
❑
❑
✓❑
Concentration
Mass
(88-75-5)
3.7
4-nitrophenol
❑
❑
✓❑
Concentration
Mass
(100-02-7)
3.8
p-chloro-m-cresol
❑
❑
✓❑
Concentration
Mass
(59-50-7)
3 9
Pentachlorophenol
Concentration
Mass
(87-86-5)
3.10
Phenol
Concentration
Mass
(108-95-2)
3.11
2 4,6-trichlorophenol
Concentration
Mass
(88-05-2)
Section 4.Organic Toxic Pollutants (GCIMS Fraction
—Base /Neutral
Compounds)
4.1
Acenaphthene
❑
❑
✓❑
Concentration
Mass
(83-32-9)
4.2
Acenaphthylene
❑
❑
✓❑
Concentration
Mass
(208-96-8)
4.3
Anthracene
❑
❑
Concentration
Mass
(120-12-7)
4.4
Benzidine
❑
❑
❑✓
Concentration
Mass
(92-87-5)
4.5
Benzo (a) anthracene
❑
❑
❑
Concentration
Mass
(56-55-3)
4.6
Benzo (a) pyrene
❑
❑
❑
Concentration
Mass
(50-32-8)
EPA Form 3510-2C (Revised 3-19) Page 15

EPA Identification Number NPDES Permit Number Facility Name Outfall Number
NCDO03213907 NCO080853 Salem Bus. Park Remediation
Form Approved 03/05/19
OMB No. 2040-0004
Presence or Absence
Intake
check one
Effluent
(optional)
Pollutant/Parameter
Testing
Units
Maximum
Maximum
Long -Term
Long -
(and CAS Number, if available)
Required
Believed
Believed
(specify)
Daily
Monthly
Average
Number
Term
Number
Present
Absent
Discharge
Discharge
Daily
of
Average
of
(required)
(if available)
Discharge
g
Analyses
Value
Analyses
f available
4.7
3 4-benzofluoranthene
❑
❑
❑✓
Concentration
Mass
(205-99-2)
4.8
Benzo (ghi) perylene
❑
❑
❑✓
Concentration
Mass
(191-24-2)
4.9
Benzo (k) fluoranthene
Concentration
Mass
(207-08-9)
4.10
Bis (2-chloroethoxy) methane
❑
❑
❑
Concentration
Mass
(111-91-1)
4.11
Bis (2-chloroethyl) ether
❑
❑
❑✓
Concentration
Mass
(111-44-4)
4.12
Bis (2-chloroisopropyl) ether
❑
❑
❑
Concentration
Mass
(102-80-1)
4.13
Bis (2-ethylhexyl) phthalate
❑
❑
❑
Concentration
Mass
(117-81-7)
4.14
4-bromophenyl phenyl ether
❑
❑
❑✓
Concentration
Mass
(101-55-3)
4.15
Butyl benzyl phthalate
❑
❑
❑✓
Concentration
Mass
(85-68-7)
4.16
2-chloronaphthalene
❑
❑
❑
Concentration
Mass
(91-58-7)
4.17
4-chlorophenyl phenyl ether
Concentration
Mass
(7005-72-3)
4.18
Chrysene
❑
❑
❑✓
Concentration
Mass
(218-01-9)
4.19
Dibenzo (a,h) anthracene
❑
El
❑✓
Concentration
Mass
(53-70-3)
EPA Form 3510-2C (Revised 3-19) Page 16

EPA Identification Number NPDES Permit Number Facility Name Outfall Number
NCDO03213907 NCO080853 Salem Bus. Park Remediation
Form Approved 03/05/19
OMB No. 2040-0004
Presence or Absence
Intake
check one
Effluent
(optional)
Pollutant/Parameter
Testing
Units
Maximum
Maximum
Long -Term
Long -
(and CAS Number, if available)
Required
Believed
Believed
(specify)
Daily
Monthly
Average
Number
Term
Number
Present
Absent
Discharge
Discharge
Daily
of
Average
of
(required)
(if available)
Discharge
g
Analyses
Value
Analyses
f available
4.20
12-dichlorobenzene
❑
❑
✓❑
Concentration
Mass
(95-50-1)
4.21
13-dichlorobenzene
❑
❑
✓❑
Concentration
Mass
(541-73-1)
4.22
1 4-dichlorobenzene
❑
❑
✓❑
Concentration
Mass
(106-46-7)
4.23
3 3-dichlorobenzidine
❑
❑
❑✓
Concentration
Mass
(91-94-1)
4.24
Diethyl phthalate
❑
❑
❑✓
Concentration
Mass
(84-66-2)
4.25
Dimethyl phthalate
❑
❑
❑✓
Concentration
Mass
(131-11-3)
4.26
Di-n-butyl phthalate
❑
❑
❑✓
Concentration
Mass
(84-74-2)
4.27
2 4-dinitrotoluene
❑
❑
❑✓
Concentration
Mass
(121-14-2)
4.28
2 6-dinitrotoluene
❑
❑
❑✓
Concentration
Mass
(606-20-2)
4.29
Di-n-octyl phthalate
❑
❑
❑✓
Concentration
Mass
(117-84-0)
4.30
1,2-Diphenylhydrazine
❑
El
❑✓
Concentration
Mass
(as azobenzene) (122-66-7)
4.31
Fluoranthene
❑
❑
❑✓
Concentration
Mass
(206-44-0)
4.32
Fluorene
❑
❑
❑✓
Concentration
Mass
(86-73-7)
EPA Form 3510-2C (Revised 3-19) Page 17

EPA Identification Number
NCDO03213907
NPDES
NCO080853
Facility Name Outfall Number
Salem Bus. Park Remediation
Form Approved 03/05/19
OMB No. 2040-0004
Presence or Absence
Intake
check one
Effluent
(optional)
Pollutant/Parameter
Testing
Units
Maximum
Maximum
Long -Term
Long -
(and CAS Number, if available)
Required
Believed
Believed
(specify)
Daily
Monthly
Average
Number
Term
Number
Present
Absent
Discharge
Discharge
Daily
of
Average
of
(required)
(if available)
Discharge
g
Analyses
Value
Analyses
f available
4.33
Hexachlorobenzene
❑
❑
✓❑
Concentration
Mass
(118-74-1)
4.34
Hexachlorobutadiene
❑
❑
❑✓
Concentration
Mass
(87-68-3)
4.35
Hexachlorocyclopentadiene
❑
❑
❑✓
Concentration
Mass
(77-47-4)
4.36
Hexachloroethane
❑
❑
❑
Concentration
Mass
(67-72-1)
4.37
Indeno (1,2,3-cd) pyrene
❑
El
❑✓
Concentration
Mass
(193-39-5)
4.38
Isophorone
❑
❑
❑✓
Concentration
Mass
(78-59-1)
4.39
Naphthalene
❑
❑
❑✓
Concentration
Mass
(91-20-3)
4.40
Nitrobenzene
❑
❑
❑✓
Concentration
Mass
(98-95-3)
4.41
N-nitrosodimethylamine
❑
❑
❑✓
Concentration
Mass
(62-75-9)
4.42
N-nitrosodi-n-propylamine
❑
❑
❑
Concentration
Mass
(621-64-7)
4.43
N-nitrosodiphenylamine
❑
❑
❑
Concentration
Mass
(86-30-6)
4.44
Phenanthrene
❑
❑
❑✓
Concentration
Mass
(85-01-8)
4.45
Pyrene
El
1:1
El
Concentration
Mass
(129-00-0)
EPA Form 3510-2C (Revised 3-19) Page 18

EPA Identification Number
NCDO03213907
)ES Permit Number Facility Name
NCO080853 Salem Bus. Park Remediation
Number
Form Approved 03/05/19
OMB No. 2040-0004
Presence or Absence
Intake
check one
Effluent
(optional)
Pollutant/Parameter
Testing
Units
Maximum
Maximum
Long -Term
Long -
(and CAS Number, if available)
Required
Believed
Believed
(specify)
Daily
Monthly
Average
Number
Term
Number
Present
Absent
Discharge
Discharge
Daily
of
Average
of
(required)
(if available)
Discharge
Analyses
Value
Analyses
f available
4.46 1 2 4-trichlorobenzene
❑
❑
✓❑
Concentration
Mass
(120-82-1)
1
1
Section 5.Organic Toxic Pollutants (GC/MS Fraction
—Pesticides)
5.1
Aldrin
El
El
Concentration
Mass
(309-00-2)
5.2
a-BHC
El
El
IZI
Concentration
Mass
(319-84-6)
5.3
R-BHC
0
Concentration
Mass
(319-85-7)
5.4
V-BHC
El
El
0
Concentration
Mass
(58-89-9)
5.5
b-BHC
El
El
El
Concentration
Mass
(319-86-8)
5.6
Chlordane
El
El
✓
Concentration
Mass
(57-74-9)
5.7
4 4'-DDT
El
El
0
Concentration
Mass
(50-29-3)
5.8
4 4'-DDE
El
1:1
0
Concentration
Mass
(72-55-9)
5.9
4,4'-DDD
✓
Concentration
Mass
(72-54-8)
5.10
Dieldrin
✓
Concentration
Mass
(60-57-1)
5.11
a-endosulfan
Concentration
Mass
(115-29-7)
EPA Form 3510-2C (Revised 3-19) Page 19

EPA Identification Number NPDES Permit Number Facility Name Outfall Number
NCDO03213907 NCO080853 Salem Bus. Park Remediation
Form Approved 03/05/19
OMB No. 2040-0004
Pollutant/Parameter
(and CAS Number, if available)
Testing
Required
Presence or Absence
check one
Units
(specify)
Effluent
Intake
(optional)
Believed
Present
Believed
Absent
Maximum
Daily
Discharge
(required)
Maximum
Monthly
Discharge
(if available)
Long -Term
Average
Daily
Discharge
g
f available
Number
of
Analyses
Long -
Term
Average
Value
Number
of
Analyses
5.12
R-endosulfan
(115-29-7)
El
El
IZI
Concentration
Mass
5.13
Endosulfan sulfate
(1031-07-8)
Concentration
Mass
5.14
Endrin
(72-20-8)
Concentration
Mass
5.15
Endrin aldehyde
(7421-93-4)
Concentration
Mass
5.16
Heptachlor
(76-44-8)
Concentration
Mass
5.17
Heptachlor epoxide
(1024-57-3)
Concentration
Mass
5.18
PCB-1242
(53469-21-9)
Concentration
Mass
5.19
PCB-1254
(11097-69-1)
IZI
Concentration
Mass
5.20
PCB-1221
(11104-28-2)
El
Concentration
Mass
5.21
PCB-1232
(11141-16-5)
Concentration
Mass
5.22
PCB-1248
(12672-29-6)
Concentration
Mass
5.23
PCB-1260
(11096-82-5)
0
Concentration
Mass
5.24
PCB-1016
(12674-11-2)
Concentration
Mass
EPA Form 3510-2C (Revised 3-19) Page 20

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCDO03213907 NCOO8O853 Salem Bus. Park Remediation OMB No.2040-0004
Presence or Absence
Intake
check one
Effluent
(optional)
Pollutant/Parameter
Testing
Units
Maximum
Maximum
Long -Term
Long -
(and CAS Number, if available)
Required
Believed
Believed
(specify)
Daily
Mony
thl
Average
Number
Term
Number
Present
Absent
Discharge
Discharge
Daily
of
Average
of
(required)
(if available)
Discharge
g
Analyses
Value
Analyses
if available
Toxaphene
Concentration
5.25 (8001-35-2)
❑
❑
❑✓
Mass
1 Sampling shall be conducted according to sufficiently sensitive test procedures (i.e., methods) approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR chapter I, subchapter N or 0. See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2C (Revised 3-19) Page 21

This page intentionally left blank.

EPA Identification Number
NCDO03213907
)ES Permit Number Facility Name
NCOO8O853 Salem Bus. Park Remediation
Number
Form Approved 03/05/19
OMB No. 2040-0004
TABLE C. CERTAIN CONVENTIONAL
AND NON•
• ••
i
■
Presence or Absence
Intake
check one
Effluent
(Optional)
ant
V
Believed
Believed
Units
(specify)
Maximum Daily
Maximum
Monthly
Long -Term
Average Daily
Number of
Long -Term
Number of
Present
Absent
Discharge
Discharge
Discharge
Analyses
Average
Analyses
(required)
if available
if available
Value
❑ Check here if you believe all pollutants on Table C to be present in your discharge from the noted outfall. You need not complete the "Presence or Absence" column of Table C for
each pollutant.
❑✓ Check here if you believe all pollutants on Table C to be absent in your discharge from the noted outfall. You need not complete the "Presence or Absence" column of Table C for
each pollutant.
1
Bromide
❑
❑
Concentration
Mass
(24959-67-9)
2'
Chlorine, total
El
❑
Concentration
Mass
residual
3.
Color
El
❑
Concentration
Mass
4.
Fecal coliform
❑
El
Concentration
Mass
5
Fluoride
❑
❑
Concentration
Mass
(16984-48-8)
6
Nitrate -nitrite
❑
❑
Concentration
Mass
7'
Nitrogen, total
El
El
Concentration
Concentration
organic (as N)
8.
Oil and grease
El
❑
Concentration
Mass
9
Phosphorus (as
❑
❑
Concentration
Mass
P), total (7723-14-0)
10.
Sulfate (as SO4)
❑
❑
Concentration
Mass
(14808-79-8)
11.
Sulfide (as S)
El
ElConcentration
Mass
EPA Form 3510-2C (Revised 3-19) Page 23

EPA Identification Number
NCDO032139O7
)ES Permit Number Facility Name
NCOO8O853 Salem Bus. Park Remediation
Number
Form Approved 03/05/19
OMB No. 2040-0004
TABLE
C. CERTAIN CONVENTIONAL
AND NON•
• •• i
■
ant
V
Presence or Absence
check one
Units
(specify)
Effluent
Intake
(Optional)
Believed
Present
Believed
Absent
Maximum Daily
Discharge
(required)
Maximum
Monthly
Discharge
if available
Long -Term
Average Daily
Discharge
if available
Number of
Analyses
Long -Term
Average
Value
Number of
Analyses
12
Sulfite (as S03)
(14265-45-3)
ElConcentration
El
Mass
13.
Surfactants
❑
Concentration
Mass
14.
Aluminum, total
(7429-90-5)
❑
❑
Concentration
Mass
15.
Barium, total
(7440-39-3)
❑
❑
Concentration
Mass
16.
Boron total
(7440-42-8)
El
Concentration
Mass
17.
Cobalt, total
(7440-48-4)
❑
❑
Concentration
Mass
18
Iron total
(7439-89-6)
❑
❑
Concentration
Mass
19
Magnesium, total
(7439-95-4)
❑
Concentration
Mass
20.
Molybdenum,
total
7439-98-7
❑
❑
Concentration
Mass
21
Manganese, total
(7439-96-5)
Concentration
Mass
22
Tin, total
(7440-315)
Concentration
Mass
23
Titanium, total
(7440-32-6)
❑
❑
Concentration
Mass
EPA Form 3510-2C (Revised 3-19) Page 24

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCDO03213907 NCOO8O853 Salem Bus. Park Remediation OMB No.2040-0004
Intake
Presence or Absence
check one
Effluent
(Optional)
Pollutant
Believed
Believed
Units
(specify)
Maximum Daily
Maximum
Monthly
Long -Term
Average Daily
Number of
Long -Term
Number of
Present
Absent
Discharge
Discharge
Discharge
Analyses
Average
Analyses
(required)
if available
if available
Value
24.
Radioactivity
Alpha, total
❑
❑
Concentration
Mass
Beta, total
❑
❑
Concentration
Mass
Radium, total
El
El
Concentration
Mass
Radium 226, total
El
ElConcentrationMass
Sampling shall be conducted according to sufficiently sensitive test procedures (i.e., methods) approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR chapter I, subchapter N or 0. See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2C (Revised 3-19) Page 25

This page intentionally left blank.

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCDO03213907 NCO080853 Salem Bus. Park Remediation OMB No. 2040-0004
I I Will P11111 0 If 11111]
Presence or Absence
Pollutant check one) 7ReasonPollutant Believed Present in Discharge Available Quantitative Data
Believed Believed (specify units)
Present Absent
1.
Asbestos
❑
�
2.
Acetaldehyde
El
�
3.
Allyl alcohol
❑
0
4.
Allyl chloride
❑
0
5.
Amyl acetate
❑
0
6.
Aniline
❑
0
7.
Benzonitrile
❑
0
8.
Benzyl chloride
❑
0
9.
Butyl acetate
❑
❑✓
10.
Butylamine
❑
❑✓
11.
Captan
❑
❑✓
12.
Carbaryl
❑
❑✓
13.
Carbofuran
❑
❑✓
14.
Carbon disulfide
❑
❑✓
15.
Chlorpyrifos
❑
❑✓
16.
Coumaphos
❑
❑✓
17.
Cresol
❑
❑✓
18.
Crotonaldehyde
❑
❑✓
19.
Cyclohexane
❑
❑✓
EPA Form 3510-2C (Revised 3-19) Page 27

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCDO03213907 NCO080853 Salem Bus. Park Remediation OMB No. 2040-0004
I I Will P11111 0 If 11111]
Presence or Absence
Pollutant check one) 7ReasonPollutant Believed Present in Discharge Available Quantitative Data
Believed Believed (specify units)
Present Absent
20.
2,4-D (2,4-dichlorophenoxyacetic acid)
❑
❑✓
21.
Diazinon
El
❑✓
22.
Dicamba
❑
❑✓
23.
Dichlobenil
❑
❑✓
24.
Dichlone
❑
❑✓
25.
2,2-dichloropropionic acid
❑
❑✓
26.
Dichlorvos
❑
❑✓
27.
Diethyl amine
❑
❑✓
28.
Dimethyl amine
❑
❑✓
29.
Dintrobenzene
❑
❑✓
30.
Diquat
❑
❑✓
31.
Disulfoton
❑
❑✓
32.
Diuron
❑
❑✓
33.
Epichlorohydrin
❑
❑✓
34.
Ethion
❑
❑✓
35.
Ethylene diamine
❑
❑✓
36.
Ethylene dibromide
❑
❑✓
37.
Formaldehyde
❑
❑✓
38.
Furfural
❑
❑✓
EPA Form 3510-2C (Revised 3-19) Page 28

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCDO03213907 NCO080853 Salem Bus. Park Remediation OMB No. 2040-0004
•�P111 0 If 11111]
Presence or Absence
Pollutant check one) 7ReasonPollutant Believed Present in Discharge Available Quantitative Data
Believed Believed (specify units)
Present Absent
39.
Guthion
❑
0
40.
Isoprene
El
�
41.
Isopropanolamine
❑
0
42.
Kelthane
❑
0
43.
Kepone
❑
0
44.
Marathion
❑
0
45.
Mercaptodimethur
❑
0
46.
Methoxychlor
❑
0
47.
Methyl mercaptan
❑
0
48.
Methyl methacrylate
❑
0
49.
Methyl parathion
❑
0
50.
Mevinphos
❑
0
51.
Mexacarbate
❑
0
52.
Monoethyl amine
❑
0
53.
Monomethyl amine
❑
0
54.
Naled
❑
0
55.
Naphthenic acid
❑
0
56.
Nitrotoluene
❑
0
57.
Parathion
❑
0
EPA Form 3510-2C (Revised 3-19) Page 29

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCDO032139O7 NCOO8O853 Salem Bus. Park Remediation OMB No. 2040-0004
I I Will P11111 0 If 11111]
Presence or Absence
Pollutant check one) 7ReasonPollutant Believed Present in Discharge Available Quantitative Data
Believed Believed (specify units)
Present Absent
58.
Phenolsulfonate
El
�
59.
Phosgene
El
0
00.
Propargite
❑
F1
61.
Propylene oxide
❑
0
62.
Pyrethrins
❑
0
63.
Quinoline
❑
0
64.
Resorcinol
❑
0
65.
Strontium
❑
0
66.
Strychnine
❑
0
67.
Styrene
❑
0
68
2,4 5-T (2,4,5-trichlorophenoxyacetic
acid
❑
0
69.
TDE (tetrachlorodiphenyl ethane)
❑
0
70.
2,4,5-TP [2-(2,4,5-trichlorophenoxy)
anoic acid
Elro
71.
Trichlorofon
❑
0
72.
Triethanolamine
❑
0
73.
Triethylamine
❑
0
74.
Trimethylamine
❑
0
75.
Uranium
❑
0
76.
Vanadium
❑
0
EPA Form 3510-2C (Revised 3-19) Page 30

EPA Identification Number
NPDES Permit Number Facility Name Outfall Number
Form Approved 03/05/19
NCDO03213907
NCOO8O853 Salem Bus. Park Remediation
OMB No.2040-0004
1 'I•
1 � I
Presence or Absence
Pollutant
check one
Reason Pollutant Believed Present in Discharge
Available Quantitative Data
Believed Believed
(specify units)
Present Absent
77.
Vinyl acetate
❑
✓❑
78.
Xylene
❑
✓❑
79.
Xylenol
❑
✓❑
80.
Zirconium
❑
✓❑
1 Sampling shall be conducted according to sufficiently sensitive test procedures (i.e., methods) approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR chapter I, subchapter N or 0. See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2C (Revised 3-19) Page 31

This page intentionally left blank.

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCDO03213907 NCO080853 Salem Bus. Park Remediation OMB No. 2040-0004
•'• I• I• 1 1 1 I
TCDD Presence or
Congeners Absence
Pollutant Used or check one Results of Screening Procedure
Manufactured Believed Believed
Present Absent
2,3,7,8-TCDD ❑ ❑ ❑✓
EPA Form 3510-2C (Revised 3-19) Page 33

i
z
a
0
a
L
WELL GROUPINGS:
NETWORK A NETWORK B NETWORK TPH
EW-4 EW-17 DT-1
EW-5 EW-19 EW-18
------ ----- EW-6 EW-22
EW-12
EW-14
I I I I EW-16
I I I
FEEDANKTER I FEEANKTER I EW-21
FT-100 I FT-107
1 4-F -2 I -F -36
FIR WOFIE °
EXHAUST
BUILDING 46 BUILDING 46 BUILDING 46
SUMP-156 AREA SUMP-151 AREA SUMP-152 AREA —
IRANSITION TO 60 GPM INSTANTANEOUS r — 1 TRUCK
DOUBLE WALL 50 GPM AVERAGE COURT
PIPE COMBINED INFLUENT I TRANSITION TO I WALL
SINGLE WALL PIPE
4-FW-36
(NETWORK B)
TRANSITION TO
SINGLE WALL PIPE 4-FW-26
(NETWORK A) I — — — — — — —
3FW-522 $. P. L C
(NETWORK TPH) I NPDES No BAG FILTERS
BF-01A & BF-01B IN I PERMIT
N
FROM I I I NC
O CARBON COMPLIANCE
a-EWszz IDS pWS TRANSFER IN IN TRANSFER VESSEL
WELL FIELD I I PUMP oUT OUT PUMP _
EQUALIZATION TANK TP-1 C C GAC-01 I SAMPLE
BUILDING 46 I I T-01 NH NO
AIR STRIPPER TP2 jVHVW' our I LOCATION
— SUMP-153 AREA — I I C DPI Nc. AS-01 C
r — — — — — —
NO
EQUALIZATION TANK SKID BAG FILTER SKID AIR STRIPPER SKID GAC SKID 01
I II
SYMBOLS LEGEND
ACTIVE PIPING
INACTIVE PIPING AND EQUIPMENT
>< PARSHALL FLUME
D&� BALL VALVE
N CHECK VALVE
PUMP
BLOWER
NOTES AND ABBREVIATIONS
1. THE PURPOSE OF THIS DIAGRAM IS TO DESCRIBE THE OVERALL
PROCESS. SOME DETAILS HAVE BEEN OMITTED FOR CLARITY.
2. GATHERING NETWORKS WERE PREVIOUSLY USED TO SUPPLY
SEPARATE TREATMENT SYSTEMS CIRCA 1999-2012. AS
INDICATED ON THIS FIGURE, NETWORK A, NETWORK B, AND
NETWORK TPH DISCHARGE TO THE INFLUENT EQUALIZATION
TANK. WELL GROUPINGS ARE PERIODICALLY RECONFIGURED
AT THE DISCRETION OF THE OPERATOR.
3. GRAY LINEWORK INDICATES EQUIPMENT AND PIPING THAT IS
NORMALLY BYPASSED.
FOIT = FLOW TOTALIZING INDICATING TRAMSMITTER
FE = FLOW ELEMENT
NO = NORMALLY OPEN, NC = NORMALLY CLOSED
SP = SAMPLE PORT
BLOWER FAIT 4-F W 304
B-01 01
TREATED
S.P. I ATER TANP TO NPDES
NPDES PERMIT I I TWT-136 4FW-3ICHE04
CHEMICAL AIR STRIPPER SKID FE-151 ouTFALL
DRU2 M.I FEED PUMP TRANSITION ToiFROM
0I P 3 FLOW METER I I DOUBLE WALL
— — — — — — — — — — — — — — — — BUILDING 46 TRUCK COURT SECONDARY CONTAINMENT AREA BUILDING 46 SUMP-153 AREA
T-01
B-01
AS-01
TP-1 & TP-2
EQUALIZATION
AIR STRIPPER BLOWER
AIR STRIPPER
TRANSFER PUMPS
TANK
CINCINNATI FAN
MID -ATLANTIC ENVIROMENTAL
GRUNDFOS TPE3
NORWESCO N-40892
MODEL HP-4C21
EQMT.
40-150
1,000 GAL. WATER
600 ACFM @ 30 IN.
MODEL 2-6-6
70 GPM @ 25 FT. TDH
CAPACITY
7.5 HP MOTOR
120 GPM (MAX.), 600 SCFM
0.75 VARIABLE SPEED
MOTOR
BF-01A & BF-01 B GAC-01
BAG FILTERS CARBON ADSORPTION
PENTEK 4BB26 VESSEL
200 GPM MAX. 3,000 LB FILL
100 PSIG, 300 F MAX
P-3
CHEMICAL FEED PUMP
CHEM-TECH/PULSAFEEDER
XPV XP055LV4X
2 GPH (MAX), 80 PSI
(MAX)
%3 HP MOTOR
O
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as
3
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Z LL

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
December 19, 2022
Conan Fitzgerald
AECOM
5438 Wade Park Boulevard
Suite 200
Raleigh, NC 27607
RE: Project: Nokia
Pace Project No.: 92641172
Dear Conan Fitzgerald:
Enclosed are the analytical results for sample(s) received by the laboratory on December 09, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
�¢
Bonnie Vang
[e-mail]
[phone]
Project Manager
Enclosures
cc: Shelley Acheson, AECOM
John Moran, AECOM
Jon Wakeman, AECOM Environment
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 12

lacmnalyfica('
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: Nokia
Pace Project No.: 92641172
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 12

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Nokia
Pace Project No.: 92641172
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92641172001 FE-151
EPA1664B
REL
1
PASI-C
EPA 8260D
CL
4
PASI-C
SM 2540D-2015
CS1
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 12

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Nokia
Pace Project No.: 92641172
Sample: FE-151
Lab ID: 92641172001 Collected:
12/06/22
10:30
Received: 12/09/22 16:25 Matrix: Water
Parameters
Results Units Report
Limit
DF
Prepared Analyzed
CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Oil and Grease
ND mg/L
4.9
1
12/16/22 22:15
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Tetrachloroethene
2.7 ug/L
1.0
1
12/13/22 10:01
127-18-4
Surrogates
4-Bromofluorobenzene (S)
94 %
70-130
1
12/13/22 10:01
460-00-4
1,2-Dichloroethane-d4 (S)
99 %
70-130
1
12/13/22 10:01
17060-07-0
Toluene-d8 (S)
101 %
70-130
1
12/13/22 10:01
2037-26-5
2540D Total Suspended Solids
Analytical Method: SM 2540D-2015
Pace Analytical Services -Asheville
Total Suspended Solids
ND mg/L
2.5
1
12/12/22 19:06
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/19/2022 12:16 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 12

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Nokia
Pace Project No.: 92641172
QC Batch: 743997 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92641172001
METHOD BLANK: 3870952
Associated Lab Samples: 92641172001
Parameter
Units
Oil and Grease
mg/L
LABORATORY CONTROL SAMPLE:
3870953
Parameter
Units
Oil and Grease
mg/L
MATRIX SPIKE SAMPLE:
3870954
Parameter
Units
Oil and Grease
mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 12/16/22 22:15
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
40 33.9 85 78-114
92640922001 Spike MS MS % Rec
Result Conc. Result % Rec Limits Qualifiers
ND 38.5 32.1 82 78-114
SAMPLE DUPLICATE: 3870955
92640912002 Dup
Parameter Units Result Result
Oil and Grease mg/L ND ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/19/2022 12:16 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 12

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Nokia
Pace Project No.: 92641172
QC Batch: 742802
Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D
Analysis Description: 8260D MSV Low Level
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92641172001
METHOD BLANK: 3864507
Matrix: Water
Associated Lab Samples: 92641172001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Tetrachloroethene
ug/L
ND 1.0
12/13/22 00:55
1,2-Dichloroethane-d4 (S)
%
98 70-130
12/13/22 00:55
4-Bromofluorobenzene (S)
%
97 70-130
12/13/22 00:55
Toluene-d8 (S)
%
101 70-130
12/13/22 00:55
LABORATORY CONTROL SAMPLE:
3864508
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Tetrachloroethene
ug/L
50 51.0
102 70-130
1,2-Dichloroethane-d4 (S)
%
99 70-130
4-Bromofluorobenzene (S)
%
100 70-130
Toluene-d8 (S)
%
99 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3864509 3864510
MS MSD
92641101002
Spike Spike MS
MSD MS MSD
% Rec
Parameter
Units
Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Tetrachloroethene
ug/L
ND
20 20 24.8
21.1 124 105
70-145 16
1,2-Dichloroethane-d4 (S)
%
97 99
70-130
4-Bromofluorobenzene (S)
%
100 100
70-130
Toluene-d8(S)
%
100 100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/19/2022 12:16 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 12

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QUALITY CONTROL DATA
Project: Nokia
Pace Project No.: 92641172
QC Batch: 742782 Analysis Method: SM 2540D-2015
QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92641172001
METHOD BLANK: 3864420
Associated Lab Samples: 92641172001
Parameter
Units
Total Suspended Solids
mg/L
LABORATORY CONTROL SAMPLE:
3864421
Parameter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 3864620
Parameter
Units
Total Suspended Solids
mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 12/12/2219:05
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 234 93 90-110
92640030003 Dup
Result Result RPD Qualifiers
66.7 76.0 13
SAMPLE DUPLICATE: 3864621
92640675002 Dup
Parameter Units Result Result
Total Suspended Solids mg/L 2270 2410
RPD Qualifiers
6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALIFIERS
Project: Nokia
Pace Project No.: 92641172
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Nokia
Pace Project No.: 92641172
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
92641172001
FE-151
EPA1664B
743997
92641172001
FE-151
EPA 8260D
742802
92641172001
FE-151
SM 2540D-2015
742782
Date: 12/19/2022 12:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
Page 9 of 12

DC# Title: ENV-FRM-HUN1•0083 02 Sample Condition Upon Receipt
urntfic�r�Cs!
Effective POO.11/.4,4/Z022 8t18'30 'AM
Laboratory recelving samples:
Ashevtlle Eden❑ Greenwood ❑ 'H.untersvllle ❑ Raleigh[] Merhnnir«il€Ion Atlant;t l Wornersvillcirl
Sample Lorldition citene Name: WO # : 92.'641172
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COMMENTS/SAMPLE 131SCREPANCY
z
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CjLlENTNMFICATIpN/RE QLUTIpN
Person contacted:
Project Manager SCURF Review:
Project Manager SKIT Review:
pate/Tune:
Date:
Dater
Field Data Required? UYes U No
nsicaitrw In. A.oni4 Pann of
Page 10 of 12

DC#Title: i+NV-FRM-AUN1.0083 02,,$athple, Condition UpLori Receipt.
LiF.f1:f)11irfL75
Effecti aPate:11/14/2022 8:18:30 AM
*Chad mark top half of box If pH and/or. dechlorination N verified and
wi"thlp the :acceptance range for preservation samples.
.Or4pllotis: VOA, Collforrn,'TM, 031 and Grease, DRO/8415 (water)'DOC, LLHA
"hottom half of Isox is to list numhar.of itottlos
'*!`Check jLJ1 'unp_r-served Nftfates for chlorite
Project# WN : 92641172 ---
AM: 8v Due Date: 12/20/22
CLIENT: 92-RECOM-RAL
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Page 11 of 12

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Section A
Required Client Information:
1600 Perimeter Park Drive
+ADrris'ville. NC 275
'Ir�frorernneeeerrrs
{904 690-9272 JFax_
Due Date:
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain-of-Cuslody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
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I

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
December 13, 2022
Conan Fitzgerald
AECOM
5438 Wade Park Boulevard
Suite 200
Raleigh, NC 27607
RE: Project: Nokia
Pace Project No.: 92641169
Dear Conan Fitzgerald:
Enclosed are the analytical results for sample(s) received by the laboratory on December 09, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely, Ck,c.
U
Bonnie Vang
[e-mail]
[phone]
Project Manager
Enclosures
cc: Shelley Acheson, AECOM
John Moran, AECOM
Jon Wakeman, AECOM Environment
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 20

lacmnalyfica('
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Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: Nokia
Pace Project No.: 92641169
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 2 of 20

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[phone]
SAMPLE SUMMARY
Project: Nokia
Pace Project No.: 92641169
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92641169001
92641169002
AS Influent
AS Effluent
Water
Water
12/06/22 10:40
12/06/22 10:35
12/09/22 16:25
12/09/22 16:25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 20

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[phone]
SAMPLE ANALYTE COUNT
Project: Nokia
Pace Project No.: 92641169
Analytes
Lab ID Sample ID
Method Analysts Reported Laboratory
92641169001 AS Influent
EPA 8260D SAS 62 PASI-C
92641169002 AS Effluent
EPA 8260D SAS 62 PASI-C
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 4 of 20

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[phone]
PROJECT NARRATIVE
Project: Nokia
Pace Project No.: 92641169
Method: EPA 8260D
Description: 8260 MSV Low Level SC
Client: AECOM, Raleigh
Date: December 13, 2022
General Information:
2 samples were analyzed for EPA 8260D by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: Nokia
Pace Project No.: 92641169
Sample: AS Influent Lab ID: 92641169001 Collected: 12/06/22 10:40 Received: 12/09/22 16:25 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level SC
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
125
25.6
5
12/13/22 02:50
67-64-1
Benzene
ND
ug/L
5.0
1.7
5
12/13/22 02:50
71-43-2
Bromobenzene
ND
ug/L
5.0
1.4
5
12/13/22 02:50
108-86-1
Bromochloromethane
ND
ug/L
5.0
2.3
5
12/13/22 02:50
74-97-5
Bromodichloromethane
ND
ug/L
5.0
1.5
5
12/13/22 02:50
75-27-4
Bromoform
ND
ug/L
5.0
1.7
5
12/13/22 02:50
75-25-2
Bromomethane
ND
ug/L
10.0
8.3
5
12/13/22 02:50
74-83-9
2-Butanone (MEK)
ND
ug/L
25.0
19.8
5
12/13/22 02:50
78-93-3
Carbon tetrachloride
2.4.1
ug/L
5.0
1.7
5
12/13/22 02:50
56-23-5
Chlorobenzene
ND
ug/L
5.0
1.4
5
12/13/22 02:50
108-90-7
Chloroethane
ND
ug/L
5.0
3.2
5
12/13/22 02:50
75-00-3
Chloroform
ND
ug/L
5.0
2.2
5
12/13/22 02:50
67-66-3
Chloromethane
ND
ug/L
5.0
2.7
5
12/13/22 02:50
74-87-3
2-Chlorotoluene
ND
ug/L
5.0
1.6
5
12/13/22 02:50
95-49-8
4-Chlorotoluene
ND
ug/L
5.0
1.6
5
12/13/22 02:50
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
10.0
1.7
5
12/13/22 02:50
96-12-8
Dibromochloromethane
ND
ug/L
5.0
1.8
5
12/13/22 02:50
124-48-1
Dibromomethane
ND
ug/L
5.0
2.0
5
12/13/22 02:50
74-95-3
1,2-Dichlorobenzene
ND
ug/L
5.0
1.7
5
12/13/22 02:50
95-50-1
1,3-Dichlorobenzene
ND
ug/L
5.0
1.7
5
12/13/22 02:50
541-73-1
1,4-Dichlorobenzene
ND
ug/L
5.0
1.7
5
12/13/22 02:50
106-46-7
Dichlorodifluoromethane
ND
ug/L
5.0
1.7
5
12/13/22 02:50
75-71-8
1,1-Dichloroethane
ND
ug/L
5.0
1.8
5
12/13/22 02:50
75-34-3
1,2-Dichloroethane
ND
ug/L
5.0
1.6
5
12/13/22 02:50
107-06-2
1,1-Dichloroethene
ND
ug/L
5.0
1.7
5
12/13/22 02:50
75-35-4
cis-1,2-Dichloroethene
147
ug/L
5.0
1.9
5
12/13/22 02:50
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
5.0
2.0
5
12/13/22 02:50
156-60-5
1,2-Dichloropropane
ND
ug/L
5.0
1.8
5
12/13/22 02:50
78-87-5
1,3-Dichloropropane
ND
ug/L
5.0
1.4
5
12/13/22 02:50
142-28-9
2,2-Dichloropropane
ND
ug/L
5.0
1.9
5
12/13/22 02:50
594-20-7
1,1-Dichloropropene
ND
ug/L
5.0
2.1
5
12/13/22 02:50
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
5.0
1.8
5
12/13/22 02:50
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
5.0
1.8
5
12/13/22 02:50
10061-02-6
Diisopropyl ether
ND
ug/L
5.0
1.5
5
12/13/22 02:50
108-20-3
Ethylbenzene
ND
ug/L
5.0
1.5
5
12/13/22 02:50
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
10.0
7.6
5
12/13/22 02:50
87-68-3
2-Hexanone
ND
ug/L
25.0
2.4
5
12/13/22 02:50
591-78-6
p-Isopropyltoluene
ND
ug/L
5.0
2.1
5
12/13/22 02:50
99-87-6
Methylene Chloride
ND
ug/L
25.0
9.8
5
12/13/22 02:50
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
25.0
13.6
5
12/13/22 02:50
108-10-1
Methyl-tert-butyl ether
ND
ug/L
5.0
2.1
5
12/13/22 02:50
1634-04-4
Naphthalene
ND
ug/L
5.0
3.2
5
12/13/22 02:50
91-20-3
Styrene
ND
ug/L
5.0
1.5
5
12/13/22 02:50
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
1.6
5
12/13/22 02:50
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
5.0
1.1
5
12/13/22 02:50
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/13/2022 04:16 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 20

leAnalyiical
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Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Nokia
Pace Project No.: 92641169
Sample: AS Influent
Lab ID:
92641169001
Collected:
12/06/22 10:40
Received: 12/09/22 16:25 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level SC
Analytical
Method: EPA 8260D
Pace Analytical
Services
- Charlotte
Tetrachloroethene
706
ug/L
5.0
1.5
5
12/13/22 02:50
127-18-4
Toluene
ND
ug/L
5.0
2.4
5
12/13/22 02:50
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
5.0
4.0
5
12/13/22 02:50
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
5.0
3.2
5
12/13/22 02:50
120-82-1
1,1,1-Trichloroethane
ND
ug/L
5.0
1.7
5
12/13/22 02:50
71-55-6
1,1,2-Trichloroethane
ND
ug/L
5.0
1.6
5
12/13/22 02:50
79-00-5
Trichloroethene
80.7
ug/L
5.0
1.9
5
12/13/22 02:50
79-01-6
Trichlorofluoromethane
1.91
ug/L
5.0
1.5
5
12/13/22 02:50
75-69-4
1,2,3-Trichloropropane
ND
ug/L
5.0
1.3
5
12/13/22 02:50
96-18-4
Vinyl acetate
ND
ug/L
10.0
6.6
5
12/13/22 02:50
108-05-4
Vinyl chloride
ND
ug/L
5.0
1.9
5
12/13/22 02:50
75-01-4
Xylene (Total)
ND
ug/L
5.0
1.7
5
12/13/22 02:50
1330-20-7
m&p-Xylene
ND
ug/L
10.0
3.5
5
12/13/22 02:50
179601-23-1
o-Xylene
ND
ug/L
5.0
1.7
5
12/13/22 02:50
95-47-6
Surrogates
4-Bromofluorobenzene (S)
105
%
70-130
5
12/13/22 02:50
460-00-4
1,2-Dichloroethane-d4 (S)
117
%
70-130
5
12/13/22 02:50
17060-07-0
Toluene-d8 (S)
107
%
70-130
5
12/13/22 02:50
2037-26-5
Date: 12/13/2022 04:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 20

leAnalyiical
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9800 Kincey Ave. Suite 100
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[phone]
ANALYTICAL RESULTS
Project: Nokia
Pace Project No.: 92641169
Sample: AS Effluent Lab ID: 92641169002 Collected: 12/06/22 10:35 Received: 12/09/22 16:25 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level SC
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
12/13/22 02:15
67-64-1
Benzene
ND
ug/L
1.0
0.34
1
12/13/22 02:15
71-43-2
Bromobenzene
ND
ug/L
1.0
0.29
1
12/13/22 02:15
108-86-1
Bromochloromethane
ND
ug/L
1.0
0.47
1
12/13/22 02:15
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
12/13/22 02:15
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
12/13/22 02:15
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
12/13/22 02:15
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
12/13/22 02:15
78-93-3
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
12/13/22 02:15
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
12/13/22 02:15
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
12/13/22 02:15
75-00-3
Chloroform
ND
ug/L
1.0
0.43
1
12/13/22 02:15
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
12/13/22 02:15
74-87-3
2-Chlorotoluene
ND
ug/L
1.0
0.32
1
12/13/22 02:15
95-49-8
4-Chlorotoluene
ND
ug/L
1.0
0.32
1
12/13/22 02:15
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
12/13/22 02:15
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
12/13/22 02:15
124-48-1
Dibromomethane
ND
ug/L
1.0
0.39
1
12/13/22 02:15
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
12/13/22 02:15
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.0
0.34
1
12/13/22 02:15
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
12/13/22 02:15
106-46-7
Dichlorodifluoromethane
ND
ug/L
1.0
0.35
1
12/13/22 02:15
75-71-8
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
12/13/22 02:15
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
12/13/22 02:15
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
12/13/22 02:15
75-35-4
cis-1,2-Dichloroethene
2.5
ug/L
1.0
0.38
1
12/13/22 02:15
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
0.40
1
12/13/22 02:15
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.36
1
12/13/22 02:15
78-87-5
1,3-Dichloropropane
ND
ug/L
1.0
0.28
1
12/13/22 02:15
142-28-9
2,2-Dichloropropane
ND
ug/L
1.0
0.39
1
12/13/22 02:15
594-20-7
1,1-Dichloropropene
ND
ug/L
1.0
0.43
1
12/13/22 02:15
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
12/13/22 02:15
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
12/13/22 02:15
10061-02-6
Diisopropyl ether
ND
ug/L
1.0
0.31
1
12/13/22 02:15
108-20-3
Ethylbenzene
ND
ug/L
1.0
0.30
1
12/13/22 02:15
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1.5
1
12/13/22 02:15
87-68-3
2-Hexanone
ND
ug/L
5.0
0.48
1
12/13/22 02:15
591-78-6
p-Isopropyltoluene
ND
ug/L
1.0
0.41
1
12/13/22 02:15
99-87-6
Methylene Chloride
ND
ug/L
5.0
2.0
1
12/13/22 02:15
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
2.7
1
12/13/22 02:15
108-10-1
Methyl-tert-butyl ether
0.47J
ug/L
1.0
0.42
1
12/13/22 02:15
1634-04-4
Naphthalene
ND
ug/L
1.0
0.64
1
12/13/22 02:15
91-20-3
Styrene
ND
ug/L
1.0
0.29
1
12/13/22 02:15
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.31
1
12/13/22 02:15
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
12/13/22 02:15
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/13/2022 04:16 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 20

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Nokia
Pace Project No.: 92641169
Sample: AS Effluent
Lab ID:
92641169002
Collected:
12/06/22 10:35
Received: 12/09/22 16:25 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level SC
Analytical
Method: EPA 8260D
Pace Analytical
Services
- Charlotte
Tetrachloroethene
2.3
ug/L
1.0
0.29
1
12/13/22 02:15
127-18-4
Toluene
ND
ug/L
1.0
0.48
1
12/13/22 02:15
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
1.0
0.81
1
12/13/22 02:15
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
1.0
0.64
1
12/13/22 02:15
120-82-1
1,1,1-Trichloroethane
ND
ug/L
1.0
0.33
1
12/13/22 02:15
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.32
1
12/13/22 02:15
79-00-5
Trichloroethene
ND
ug/L
1.0
0.38
1
12/13/22 02:15
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.30
1
12/13/22 02:15
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.26
1
12/13/22 02:15
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.3
1
12/13/22 02:15
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.39
1
12/13/22 02:15
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.34
1
12/13/22 02:15
1330-20-7
m&p-Xylene
ND
ug/L
2.0
0.71
1
12/13/22 02:15
179601-23-1
o-Xylene
ND
ug/L
1.0
0.34
1
12/13/22 02:15
95-47-6
Surrogates
4-Bromofluorobenzene (S)
106
%
70-130
1
12/13/22 02:15
460-00-4
1,2-Dichloroethane-d4 (S)
115
%
70-130
1
12/13/22 02:15
17060-07-0
Toluene-d8 (S)
109
%
70-130
1
12/13/22 02:15
2037-26-5
Date: 12/13/2022 04:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 20

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Nokia
Pace Project No.: 92641169
QC Batch: 742759 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260 MSV Low Level SC
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92641169001, 92641169002
METHOD BLANK: 3864246
Associated Lab Samples: 92641169001, 92641169002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.31
12/13/22 00:48
1,1,1-Trichloroethane
ug/L
ND
1.0
0.33
12/13/22 00:48
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
12/13/22 00:48
1,1,2-Trichloroethane
ug/L
ND
1.0
0.32
12/13/22 00:48
1,1-Dichloroethane
ug/L
ND
1.0
0.37
12/13/22 00:48
1,1-Dichloroethene
ug/L
ND
1.0
0.35
12/13/22 00:48
1,1-Dichloropropene
ug/L
ND
1.0
0.43
12/13/22 00:48
1,2,3-Trichlorobenzene
ug/L
ND
1.0
0.81
12/13/22 00:48
1,2,3-Trichloropropane
ug/L
ND
1.0
0.26
12/13/22 00:48
1,2,4-Trichlorobenzene
ug/L
ND
1.0
0.64
12/13/22 00:48
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
0.34
12/13/22 00:48
1,2-Dichlorobenzene
ug/L
ND
1.0
0.34
12/13/22 00:48
1,2-Dichloroethane
ug/L
ND
1.0
0.32
12/13/22 00:48
1,2-Dichloropropane
ug/L
ND
1.0
0.36
12/13/22 00:48
1,3-Dichlorobenzene
ug/L
ND
1.0
0.34
12/13/22 00:48
1,3-Dichloropropane
ug/L
ND
1.0
0.28
12/13/22 00:48
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
12/13/22 00:48
2,2-Dichloropropane
ug/L
ND
1.0
0.39
12/13/22 00:48
2-Butanone (MEK)
ug/L
ND
5.0
4.0
12/13/22 00:48
2-Chlorotoluene
ug/L
ND
1.0
0.32
12/13/22 00:48
2-Hexanone
ug/L
ND
5.0
0.48
12/13/22 00:48
4-Chlorotoluene
ug/L
ND
1.0
0.32
12/13/22 00:48
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
2.7
12/13/22 00:48
Acetone
ug/L
ND
25.0
5.1
12/13/22 00:48
Benzene
ug/L
ND
1.0
0.34
12/13/22 00:48
Bromobenzene
ug/L
ND
1.0
0.29
12/13/22 00:48
Bromochloromethane
ug/L
ND
1.0
0.47
12/13/22 00:48
Bromodichloromethane
ug/L
ND
1.0
0.31
12/13/22 00:48
Bromoform
ug/L
ND
1.0
0.34
12/13/22 00:48
Bromomethane
ug/L
ND
2.0
1.7
12/13/22 00:48
Carbon tetrachloride
ug/L
ND
1.0
0.33
12/13/22 00:48
Chlorobenzene
ug/L
ND
1.0
0.28
12/13/22 00:48
Chloroethane
ug/L
ND
1.0
0.65
12/13/22 00:48
Chloroform
ug/L
ND
1.0
0.43
12/13/22 00:48
Chloromethane
ug/L
ND
1.0
0.54
12/13/22 00:48
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.38
12/13/22 00:48
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.36
12/13/22 00:48
Dibromochloromethane
ug/L
ND
1.0
0.36
12/13/22 00:48
Dibromomethane
ug/L
ND
1.0
0.39
12/13/22 00:48
Dichlorodifluoromethane
ug/L
ND
1.0
0.35
12/13/22 00:48
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/13/2022 04:16 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 20

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Nokia
Pace Project No.: 92641169
METHOD BLANK: 3864246
Associated Lab Samples: 92641169001, 92641169002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
Diisopropyl ether
ug/L
ND
1.0
0.31
12/13/22 00:48
Ethylbenzene
ug/L
ND
1.0
0.30
12/13/22 00:48
Hexachloro-1,3-butadiene
ug/L
ND
2.0
1.5
12/13/22 00:48
m&p-Xylene
ug/L
ND
2.0
0.71
12/13/22 00:48
Methyl-tert-butyl ether
ug/L
ND
1.0
0.42
12/13/22 00:48
Methylene Chloride
ug/L
ND
5.0
2.0
12/13/22 00:48
Naphthalene
ug/L
ND
1.0
0.64
12/13/22 00:48
o-Xylene
ug/L
ND
1.0
0.34
12/13/22 00:48
p-Isopropyltoluene
ug/L
ND
1.0
0.41
12/13/22 00:48
Styrene
ug/L
ND
1.0
0.29
12/13/22 00:48
Tetrachloroethene
ug/L
ND
1.0
0.29
12/13/22 00:48
Toluene
ug/L
ND
1.0
0.48
12/13/22 00:48
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.40
12/13/22 00:48
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.36
12/13/22 00:48
Trichloroethene
ug/L
ND
1.0
0.38
12/13/22 00:48
Trichlorofluoromethane
ug/L
ND
1.0
0.30
12/13/22 00:48
Vinyl acetate
ug/L
ND
2.0
1.3
12/13/22 00:48
Vinyl chloride
ug/L
ND
1.0
0.39
12/13/22 00:48
Xylene (Total)
ug/L
ND
1.0
0.34
12/13/22 00:48
1,2-Dichloroethane-d4 (S)
%
113
70-130
12/13/22 00:48
4-Bromofluorobenzene (S)
%
104
70-130
12/13/22 00:48
Toluene-d8 (S)
%
109
70-130
12/13/22 00:48
LABORATORY CONTROL SAMPLE:
Parameter
3864247
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
51.6
103
70-130
1,1,1-Trichloroethane
ug/L
50
58.8
118
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
52.0
104
70-130
1,1,2-Trichloroethane
ug/L
50
55.5
111
70-130
1,1-Dichloroethane
ug/L
50
54.9
110
70-130
1,1-Dichloroethene
ug/L
50
56.2
112
70-130
1,1-Dichloropropene
ug/L
50
62.1
124
70-130
1,2,3-Trichlorobenzene
ug/L
50
50.8
102
70-130
1,2,3-Trichloropropane
ug/L
50
53.0
106
70-130
1,2,4-Trichlorobenzene
ug/L
50
52.0
104
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
51.3
103
70-130
1,2-Dichlorobenzene
ug/L
50
49.2
98
70-130
1,2-Dichloroethane
ug/L
50
60.5
121
70-130
1,2-Dichloropropane
ug/L
50
54.9
110
70-130
1,3-Dichlorobenzene
ug/L
50
48.6
97
70-130
1,3-Dichloropropane
ug/L
50
53.4
107
70-130
1,4-Dichlorobenzene
ug/L
50
48.2
96
70-130
2,2-Dichloropropane
ug/L
50
55.0
110
70-130
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/13/2022 04:16 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 20

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Nokia
Pace Project No.: 92641169
LABORATORY CONTROL SAMPLE:
Parameter
3864247
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2-Butanone (MEK)
ug/L
100
121
121
70-130
2-Chlorotoluene
ug/L
50
50.9
102
70-130
2-Hexanone
ug/L
100
117
117
70-130
4-Chlorotoluene
ug/L
50
51.3
103
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
116
116
70-130
Acetone
ug/L
100
123
123
70-130
Benzene
ug/L
50
52.8
106
70-130
Bromobenzene
ug/L
50
49.8
100
70-130
Bromochloromethane
ug/L
50
50.2
100
70-130
Bromodichloromethane
ug/L
50
57.3
115
70-130
Bromoform
ug/L
50
53.4
107
70-130
Bromomethane
ug/L
50
49.9
100
70-130
Carbon tetrachloride
ug/L
50
57.4
115
70-130
Chlorobenzene
ug/L
50
48.7
97
70-130
Chloroethane
ug/L
50
51.3
103
70-130
Chloroform
ug/L
50
59.9
120
70-130
Chloromethane
ug/L
50
60.1
120
70-130
cis-1,2-Dichloroethene
ug/L
50
55.7
111
70-130
cis-1,3-Dichloropropene
ug/L
50
57.4
115
70-130
Dibromochloromethane
ug/L
50
51.6
103
70-130
Dibromomethane
ug/L
50
52.0
104
70-130
Dichlorodifluoromethane
ug/L
50
59.4
119
70-130
Diisopropyl ether
ug/L
50
54.0
108
70-130
Ethylbenzene
ug/L
50
49.5
99
70-130
Hexachloro-1,3-butadiene
ug/L
50
49.8
100
70-130
m&p-Xylene
ug/L
100
102
102
70-130
Methyl-tert-butyl ether
ug/L
50
56.8
114
70-130
Methylene Chloride
ug/L
50
52.4
105
70-130
Naphthalene
ug/L
50
53.8
108
70-130
o-Xylene
ug/L
50
49.2
98
70-130
p-Isopropyltoluene
ug/L
50
53.4
107
70-130
Styrene
ug/L
50
49.9
100
70-130
Tetrachloroethene
ug/L
50
44.5
89
70-130
Toluene
ug/L
50
50.8
102
70-130
trans-1,2-Dichloroethene
ug/L
50
56.0
112
70-130
trans- 1,3-Dichloropropene
ug/L
50
59.6
119
70-130
Trichloroethene
ug/L
50
52.0
104
70-130
Trichlorofluoromethane
ug/L
50
49.5
99
70-130
Vinyl acetate
ug/L
100
118
118
70-130
Vinyl chloride
ug/L
50
59.6
119
70-130
Xylene (Total)
ug/L
150
151
101
70-130
1,2-Dichloroethane-d4 (S)
%
111
70-130
4-Bromofluorobenzene (S)
%
104
70-130
Toluene-d8 (S)
%
103
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/13/2022 04:16 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 20

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QUALITY CONTROL DATA
Project: Nokia
Pace Project No.: 92641169
MATRIX SPIKE SAMPLE:
3864249
92641169002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
21.4
107
73-134
1,1,1-Trichloroethane
ug/L
ND
20
26.7
133
82-143
1,1,2,2-Tetrachloroethane
ug/L
ND
20
22.1
111
70-136
1,1,2-Trichloroethane
ug/L
ND
20
22.3
112
70-135
1,1-Dichloroethane
ug/L
ND
20
23.5
118
70-139
1,1-Dichloroethene
ug/L
ND
20
25.4
127
70-154
1,1-Dichloropropene
ug/L
ND
20
26.6
133
70-149
1,2,3-Trichlorobenzene
ug/L
ND
20
21.9
110
70-135
1,2,3-Trichloropropane
ug/L
ND
20
22.6
113
71-137
1,2,4-Trichlorobenzene
ug/L
ND
20
21.8
109
73-140
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20.9
105
65-134
1,2-Dichlorobenzene
ug/L
ND
20
21.7
109
70-133
1,2-Dichloroethane
ug/L
ND
20
26.5
133
70-137
1,2-Dichloropropane
ug/L
ND
20
23.8
119
70-140
1,3-Dichlorobenzene
ug/L
ND
20
21.6
108
70-135
1,3-Dichloropropane
ug/L
ND
20
22.3
112
70-143
1,4-Dichlorobenzene
ug/L
ND
20
21.1
105
70-133
2,2-Dichloropropane
ug/L
ND
20
27.3
136
61-148
2-Butanone (MEK)
ug/L
ND
40
47.8
119
60-139
2-Chlorotoluene
ug/L
ND
20
22.9
115
70-144
2-Hexanone
ug/L
ND
40
46.7
117
65-138
4-Chlorotoluene
ug/L
ND
20
23.1
116
70-137
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
47.7
119
65-135
Acetone
ug/L
ND
40
49.5
124
60-148
Benzene
ug/L
ND
20
23.6
118
70-151
Bromobenzene
ug/L
ND
20
21.6
108
70-136
Bromochloromethane
ug/L
ND
20
21.7
109
70-141
Bromodichloromethane
ug/L
ND
20
24.8
124
70-138
Bromoform
ug/L
ND
20
21.5
108
63-130
Bromomethane
ug/L
ND
20
23.1
115
15-152
Carbon tetrachloride
ug/L
ND
20
26.2
131
70-143
Chlorobenzene
ug/L
ND
20
21.3
106
70-138
Chloroethane
ug/L
ND
20
24.8
124
52-163
Chloroform
ug/L
ND
20
24.3
121
70-139
Chloromethane
ug/L
ND
20
22.3
112
41-139
cis-1,2-Dichloroethene
ug/L
2.5
20
24.6
110
70-141
cis-1,3-Dichloropropene
ug/L
ND
20
24.0
120
70-137
Dibromochloromethane
ug/L
ND
20
21.3
106
70-134
Dibromomethane
ug/L
ND
20
22.4
112
70-138
Dichlorodifluoromethane
ug/L
ND
20
17.8
89
47-155
Diisopropyl ether
ug/L
ND
20
23.8
119
63-144
Ethylbenzene
ug/L
ND
20
22.6
113
66-153
Hexachloro-1,3-butadiene
ug/L
ND
20
24.6
123
65-149
m&p-Xylene
ug/L
ND
40
45.6
114
69-152
Methyl-tert-butyl ether
ug/L
0.47J
20
23.4
115
54-156
Methylene Chloride
ug/L
ND
20
23.4
117
42-159
Naphthalene
ug/L
ND
20
21.9
109
61-148
Results presented on
this page are in the units indicated
by the "Units" column except where
an alternate unit is
presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/13/2022 04:16 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 20

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Nokia
Pace Project No.: 92641169
MATRIX SPIKE SAMPLE:
3864249
92641169002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
o-Xylene
ug/L
ND
20
21.5
108
70-148
p-Isopropyltoluene
ug/L
ND
20
24.3
122
70-146
Styrene
ug/L
ND
20
21.6
108
70-135
Tetrachloroethene
ug/L
2.3
20
19.8
87
59-143
Toluene
ug/L
ND
20
23.2
116
59-148
trans-1,2-Dichloroethene
ug/L
ND
20
26.3
131
70-146
trans- 1,3-Dichloropropene
ug/L
ND
20
25.6
128
70-135
Trichloroethene
ug/L
ND
20
24.6
123
70-147
Trichlorofluoromethane
ug/L
ND
20
24.0
120
70-148
Vinyl acetate
ug/L
ND
40
46.2
115
49-151
Vinyl chloride
ug/L
ND
20
24.1
120
70-156
Xylene (Total)
ug/L
ND
60
67.1
112
63-158
1,2-Dichloroethane-d4 (S)
%
111
70-130
4-Bromofluorobenzene (S)
%
104
70-130
Toluene-d8 (S)
%
102
70-130
SAMPLE DUPLICATE: 3864248
92641048012
Dup
Max
Parameter
Units
Result
Result
RPD
RPD
Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,1-Trichloroethane
ug/L
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,2-Trichloroethane
ug/L
ND
ND
30
1,1-Dichloroethane
ug/L
ND
ND
30
1,1-Dichloroethene
ug/L
ND
ND
30
1,1-Dichloropropene
ug/L
ND
ND
30
1,2,3-Trichlorobenzene
ug/L
ND
0.98J
30
1,2,3-Trichloropropane
ug/L
ND
ND
30
1,2,4-Trichlorobenzene
ug/L
ND
0.71J
30
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
30
1,2-Dichlorobenzene
ug/L
ND
ND
30
1,2-Dichloroethane
ug/L
ND
ND
30
1,2-Dichloropropane
ug/L
ND
ND
30
1,3-Dichlorobenzene
ug/L
ND
ND
30
1,3-Dichloropropane
ug/L
ND
ND
30
1,4-Dichlorobenzene
ug/L
ND
ND
30
2,2-Dichloropropane
ug/L
ND
ND
30
2-Butanone (MEK)
ug/L
ND
ND
30
2-Chlorotoluene
ug/L
ND
ND
30
2-Hexanone
ug/L
ND
ND
30
4-Chlorotoluene
ug/L
ND
ND
30
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
30
Acetone
ug/L
ND
ND
30
Benzene
ug/L
ND
ND
30
Bromobenzene
ug/L
ND
ND
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/13/2022 04:16 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 20

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Nokia
Pace Project No.: 92641169
SAMPLE DUPLICATE: 3864248
Parameter
Units
92641048012
Result
Dup
Result
Bromochloromethane
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Bromomethane
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
ND
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
ND
ND
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dibromomethane
ug/L
ND
ND
Dichlorodifluoromethane
ug/L
ND
ND
Diisopropyl ether
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
Hexachloro-1,3-butadiene
ug/L
ND
ND
m&p-Xylene
ug/L
ND
ND
Methyl-tert-butyl ether
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
Naphthalene
ug/L
ND
0.82J
o-Xylene
ug/L
ND
ND
p-Isopropyltoluene
ug/L
ND
ND
Styrene
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
ND
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans- 1,3-Dichloropropene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl acetate
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
Xylene (Total)
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
110
121
4-Bromofluorobenzene (S)
%
104
105
Toluene-d8 (S)
%
111
108
Max
RPD RPD Qualifiers
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/13/2022 04:16 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 20

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Nokia
Pace Project No.: 92641169
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/13/2022 04:16 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 20

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Nokia
Pace Project No.: 92641169
Lab ID Sample ID QC Batch Method QC Batch
92641169001 AS Influent EPA 8260D 742759
92641169002 AS Effluent EPA 8260D 742759
Date: 12/13/2022 04:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical Method
Analytical
Batch
Page 17 of 20

DC# Tftle: ENV.-FRWHUN1-083 v02_Sample Condition Upon Receipt
(-�UMroil.Uvcu
Effective n.a#e: 3.1/14/2022 8:18;30 AM
Ubo.ratoryr receiving samples
A hevllid l d.e"D Greenwood [3 H'Untersuille ❑ Raleigh[l Mechanicsville[:] Atlanta[] Kernersviife[]
-Chant Name, Project ' W01P 926411169
pAF-Lf7 Ommerclal qpn
a c: L UPS. ❑Oth r, Client
Custody Sail Present? ❑Yes
*0 Seals Intact!
❑Yes 00
Racking Material: ❑ Bubble Wisp �02uhlile Bags 0 None [. Other
Thermometeri. _
7 IR Gulf ID �� Type of Ice: let © Blue
j Correcitian: Factor;
CaOler Temp: `--'— Add/5ubtraot ('C) Q
Cooler renAP Corrected °Cj: .. 0
USDA Regulated5o,N/A, water sample)
.Did samples originate n a qunrantlne, zone within the United States: CA, NY, orS
(check maps)?''QYes ❑No
92641169
L
Dateflnitlals person Examining ContentsAIYY g
Biological Tissue Frozen?
❑ Yes 1 No D N/A
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TOMP'shoWd be above froadng.to 5°C
05amplesout of.temp.criterla. Samples on' Ice, OWN process
hasbegun
frld samp%toriginale#rom a foreign. source (internationally,
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tommentslDlaCrepan Cy:
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1.
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C7wok.
2,
5hcgt,Hald tme Analysls (472 hr:)T
❑Yet
No
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Rush Turn'Around Time: Re vested?
[I Yes
1�96
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4'.
SufficientVoluine?
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©N'o .
❑N/A
51
correct ContalnemUsed?.
-Pate Containers Used?
ds
tai
ON'�o
❑ No
f2N/A
❑ N/A,
6.
Containerslntact?.
"Yes
No
❑NIA
7,
DissalYedanaiysis:;Samplesfield Filtered?
OYes
EaAo
ONIA
a.
sample Labels Match COC7
-Includes➢ate/time/iD/Analysis Matrix:__
Vyes
El No
ON/A
9.
Headspace in VOA V1216 (>5-6mm)?
Oyes
to
O WA.
10.
Trip Blank Present?
Trip Blarik:Custody Seals Present?
❑Yes
❑Yes
No.
No
❑.NIA
❑NIA
11.
COMMENTS/SAMPLE 015CREPANCY
Lot ID of split containers:
CLIENT NO -RI ICATION/RE5t?LUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Tune:
Date:
D ate:
Field Data Required? UYus LJ No
rlr im1 ray IM, RAR1d Clain 1 of 7
Page 18 of 20

GCB'.
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DC#_Tltle: ENV-FRM-HUHi-0033 02-5ampie Condition Upon Receipt.
.sate+ 1,1/1412022 9,18:30
Check rnark top:haif of box if pH and/or dachlarination. is verified and prq� # ^4 92641169
Within the acceptance range far preservation samples. PM: BY Due Date: 12/20/22
Exceptions; VOA, Call(orm, TpC; Oil ar d Grease, 0907pQX5 (wster) QOC,, .ILHg. CLIEN'r : 92-AECOM-RAL
*"torn half of box>is=to Hsi number.of•bottles
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pH Adjustment
Lag for preserved Samples
Sample ID
'type of Preservative
pH upon recelpt
pate preservation -adjusted
Time preservation
adjusted
Amount of Preservative
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CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chainraf-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
s sample via th;s chain of custody consdtutes acknewiedgment and acceplanen of the Pace Terms and Condlh'ons found at https:;linfO.pat:elebs.camlhubfypas-standard-terms.odf.
Section 13 Section C
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