WQ0008778_2022 Residual Annual Report_20230227 (2)

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * W00008778
Applicant/Permittee Town of Farmville
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Washington
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Lysa Finnerty
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
4105376150
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0008778
Has Current Existing permit number
Applicant/Permittee Address*
435 Williams Court, Ste 100, Baltimore, MD 21220
Facility Name*
Town of Farmville Class B Residuals Program
Please provide comments/notes on your current submittal below.
2022 Annual Report for Town of Farmville, NC
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Farmville NC 2022 Annual Report FINAL.pdf 7.23MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/27/2023

435 Williams Court, Suite 100
Baltimore, MD 21220
www.synagro.com
FEBRUARY 27, 2023
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2022 Annual Report for Permit No. WQ0008778
Dear NCDEQ:
SYNAGRO
Synagro is submitting one electronic copy of the above referenced report on behalf of the Town
of Farmville, NC.
If you have any questions or need additional information, please do not hesitate to contact
David Hodgkins at [phone] or Matthew Carter at [phone].
Sincerely,
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: David Hodgkins
Matthew Carter, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

TOWN OF FARMVILLE, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0008778
2022 ANNUAL REPORT

Town of Farmville, NC
Residuals Land Application Program
2022 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and Residuals
Analyses
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit P: WQ0008778 County Pitt Year 2022
Facility Name (as shown on permit) Farmville WWTP NPDES No, NC0029572
Land Application Operator_ Synaero Phone# [phone]
Land application of residuals as allowed by the above permit occurred during tl►e past calendar year?
X YES NO. IfNO, skip Par# A, and Part Band proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 7
Total number of fields utilized for land application during the year: 3
Total amount of dry tons applied during the year for all application sites: 307.77
Total number of acres utilized for land application during tine year: 58.70
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2022 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Qualify X YES NO.
If no, please provide a written description why tine facility was not compliant, the dates, and explain corrective action taken,
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in tine permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
S. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or tine Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .111 I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received frorn the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and rennediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the pernnit.
12, No runoff of residuals $'otn the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to Lire best of my knowledge and belief, true, accurate, and complete. 1
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
David P, Hodgkins, Town Mana er
Permittee Name and Title (type or Tint) �2
ig€nature of Preparer* Date .
(if different from Permittee)
,d A'A ( z ,6 z3
Signature fPer t ljate
2/01/2023
Sign re of Land Mplier Date
(if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (1212006)

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 1/1/2022 - 12/31/2022
FARMVILLE, NC
FARMVILLE, NC WWTP AERATION BASIN LIQUID
MONTH/YEAR
July 2022
August 2022
IEel /_1I
FARMVILLE, NC AEROBICALLY DIGESTED LIQUID
MONTH/YEAR
March 2022
July 2022
TOTAL
Units Key: D - Dry Tons; G — Gallons; W — Wet Tons; Y — Cubic Yards
Report Date: 2/2/2023 1:04:25 PM
AMOUNT
UNIT
DRY TONS
UNIT
DRY METRIC TONS
124,000.00
G
22.44
D
20.35
248,000.00
G
44.88
D
40.71
372,000.00
G
67.32
D
61.06
AMOUNT
UNIT
DRY TONS
UNIT
DRY METRIC TONS
279,000.00
G
110.41
D
100.14
328,600.00
G
130.04
D
117.94
607,600.00
G
240.45
D
218.09

SECTION 2

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PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Chris Wynne
Project Name: Farmville VWVFP
Lot Number:XE19004
Date Completed:06/06/2022
NIM�� Mr�
06/07/2022 6:15 PM
Approved and released by:
Project Manager II: Lucas Odom
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ANSI NdmlAccre00- Board
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A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 9

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: XE19004
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Inorganic Metals
The following samples were classified as biosolids therefore in order to ensure proper digestion they were
initially weighed out at around 3.0-3.5 grams: XE19004-001. The LOQ has been adjusted accordingly.
Inorganic Non -Metals
The method blank for prep batch 42781 contained the analyte total phosphate greater than the method
acceptance criteria. The associated samples contained detections for this analyte at concentrations
greater than 1 OX the value found in the method blank; therefore sample results are not impacted. The
data has been reported.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 9

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Synagro
Lot Number: XE19004
Sample Number Sample ID Matrix Date Sampled Date Received
001 FARMVILLE WWTP/ AERATION BASIN Solid 05/17/2022 1000 05/19/2022
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 9

Inorganic non-metals
Client:Synagro Laboratory ID:XE19004-001
Description: FARMVILLE WWTP/ AERATION BASIN Matrix: Solid
Date Sampled:05/17/2022 1000 % Solids: 4.34 05/23/2022 2318
Date Received:05/19/2022
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date
Batch
1 350.1
(Ammonia - N ) 350.1
10
05/27/2022 1035 CMM
42917
1
(Nitrate - N ) 353.2
1
06/02/2022 1900 KKP
43554
1
(Nitrite - N ) 353.2
1
06/02/2022 1900 KKP
43555
1
(Phosphorus) 365.1
50
05/26/2022 1717 DMA
05/24/2022 1315
42781
1
(Soil pH meas) 9045D
1
06/02/2022 1946 KKP
43695
1 351.4
(TKN) 351.2
2
05/28/2022 1607 DMA
05/24/2022 1224
42751
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Ammonia - N (gas diffusion)
350.1
6100 S
230
120
mg/kg
1
Nitrate - N (soluble)
353.2
8.4
4.6
0.62
mg/kg
1
Nitrite - N (soluble)
353.2
17
4.6
0.61
mg/kg
1
Phosphorus
7723-14-0 365.1
26000 B
5800
1200
mg/kg
1
Soil pH measured in water @
25.6 o C
9045D
7.1
su
1
TKN
351.2
45000 B
2300
1200
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 9

CVAA
Client:Synagro Laboratory ID:XE19004-001
Description: FARMVILLE WWTP/ AERATION BASIN Matrix: Solid
Date Sampled:05/17/2022 1000 % Solids: 4.34 05/23/2022 2318
Date Received:05/19/2022
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471 B 7471 B 1 05/24/2022 0730 JAB2 05/24/2022 0434 42401
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7471B 0.62 J 1.8 0.44 mg/kg 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 9

ICP-AES
Client:Synagro Laboratory ID:XE19004-001
Description: FARMVILLE WWTP/ AERATION BASIN Matrix: Solid
Date Sampled:05/17/2022 1000 % Solids: 4.34 05/23/2022 2318
Date Received:05/19/2022
Run Prep Method
1 3050B
Analytical Method Dilution Analysis Date Analyst
6010D 1 05/24/2022 0614 JMH
Prep Date Batch
05/20/2022 0933 42410
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
DL
Units
Run
Aluminum
7429-90-5
6010D
19000
130
50
mg/kg
1
Arsenic
7440-38-2
6010D
8.3
5.0
1.7
mg/kg
1
Cadmium
7440-43-9
6010D
1.6
J
1.7
0.42
mg/kg
1
Calcium
7440-70-2
6010D
15000
1700
210
mg/kg
1
Chromium
7440-47-3
6010D
42
3.4
0.84
mg/kg
1
Copper
7440-50-8
6010D
940
3.4
1.5
mg/kg
1
Iron
7439-89-6
6010D
48000
34
15
mg/kg
1
Lead
7439-92-1
6010D
48
3.4
1.5
mg/kg
1
Magnesium
7439-95-4
6010D
2700
1700
210
mg/kg
1
Manganese
7439-96-5
6010D
720
5.0
2.0
mg/kg
1
Molybdenum
7439-98-7
6010D
11
J
13
3.4
mg/kg
1
Nickel
7440-02-0
6010D
37
13
3.5
mg/kg
1
Potassium
7440-09-7
6010D
1500
J
1700
210
mg/kg
1
Selenium
7782-49-2
6010D
8.1
6.7
2.7
mg/kg
1
Sodium
7440-23-5
6010D
1000
J
1700
210
mg/kg
1
Zinc
7440-66-6
6010D
1200
17
4.2
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 9

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 9

PACE ANALYTICAL SERVICES, LLC
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 9
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corrwdy transcribed Rum the Me. into the uornmerp
YC3 +f No,' 4V the qu= nuir kr listed{ an the coaMincr lah:
Imple prCwe—fi ion (Must be crarr 0eted for any samplr(s) Jjtourrees.by pmv-
.ntple(f) NA Werx nrQiy iittiOrrpCt
sawplt� *�eiuk�g with K^ mL Of ci rcic -one: l 1 5O eiN{73, f [ 1, ] NOR r
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Comments..
ac
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: > 0.31n6}L (If # 19 is no) and worm
3hGaly ID:PA
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 9

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PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Chris Wynne
Project Name: Farmville VWVFP
Lot Number:XA12018
Date Completed:02/08/2022
NIM�� Mr�
02/08/2022 11:13 AM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: XA12018
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Inorganic Metals
Due to their matrix and low percent solids, the initial sample amount of the following samples is 3x greater
than standard procedure: XA12018-001. The LOQ has been adjusted accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 7

Client: Synagro Laboratory ID: XA12018-001
Description: Farmville WWTP Matrix: Solid
Date Sampled:01/10/2022 1045 % Solids: 9.49 01/13/2022 0152
Date Received: 01 /12/2022
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 2540G
1 01/13/2022 0152 NBW
28253
1 350.1
(Ammonia - N ) 350.1
5 01/19/2022 2217 DAK
28766
1
(Nitrate - N ) 9056A
5 01/20/2022 2154 AAB
29256
3
(Nitrite - N ) 9056A
5 02/03/2022 0356 SUH
30794
1
(Phosphorus) 365.1
50 01/17/2022 1528 DMA
01/13/2022 1127
28296
1
(Soil pH meas) 9045D
1 01/12/2022 2324 NEW
28252
1 351.4
(TKN) 351.2
2 01/24/2022 1045 DMA
01/21/2022 1404 29104
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
9.49
%
1
Ammonia - N (gas diffusion)
350.1
1400
53
27
mg/kg
1
Nitrate - N (soluble)
9056A
22 J
26
5.3
mg/kg
1
Nitrite - N (soluble)
9056A
140
11
5.3
mg/kg
3
Phosphorus
7723-14-0 365.1
13000
2600
530
mg/kg
1
Soil pH measured in water C)
19.4 ° C
9045D
6.5
su
1
TKN
351.2
18000 S
1100
530
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 01/13/2022 0831 JAB2
01/13/2022 0215
28257
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471 B
3.6
0.82
0.20
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 01/14/2022 1708 KSH2
01/14/2022 0035
28143
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
8700
67
25
mg/kg
1
Arsenic
7440-38-2 6010D
3.5
2.5
0.84
mg/kg
1
Cadmium
7440-43-9 6010D
0.70 J
0.84
0.21
mg/kg
1
Calcium
7440-70-2 6010D
5200
840
100
mg/kg
1
Chromium
7440-47-3 6010D
52
1.7
0.42
mg/kg
1
Copper
7440-50-8 6010D
240
1.7
0.76
mg/kg
1
Iron
7439-89-6 6010D
28000
17
7.6
mg/kg
1
Lead
7439-92-1 6010D
24
1.7
0.76
mg/kg
1
Magnesium
7439-95-4 6010D
1500
840
100
mg/kg
1
Manganese
7439-96-5 6010D
440
2.5
0.99
mg/kg
1
Molybdenum
7439-98-7 6010D
3.7 J
6.7
1.7
mg/kg
1
Nickel
7440-02-0 6010D
31
6.7
1.8
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range DL - Detection Limit Q - Surrogate failure
ND - Not detected at or above the DL N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% J - Estimated result < LOQ and > DL L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client: Synagro Laboratory ID: XA12018-001
Description: Farmville WWTP Matrix: Solid
Date Sampled:01/10/2022 1045 % Solids: 9.49 01/13/2022 0152
Date Received: 01 /12/2022
ICP-AES
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
6010D 1 01/14/2022 1708 KSH2
01/14/2022 0035
28143
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Potassium
7440-09-7 6010D
1500
840
100
mg/kg
1
Selenium
7782-49-2 6010D
1.7 J
3.4
1.4
mg/kg
1
Sodium
7440-23-5 6010D
720 J
840
100
mg/kg
1
Zinc
7440-66-6 6010D
630
8.4
2.1
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range DL - Detection Limit Q - Surrogate failure
ND - Not detected at or above the DL N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% J - Estimated result < LOQ and > DL L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services,
LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive
West Columbia, SC 29172
[phone] Fax [phone] www.pacelabs.com
Page 6 of 7
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PACE ANALYTICAL SERVICES, LLC
5amplcs Reculpt Checklist (511C) (MEODISC-151 Re.vi.wed:9fi9,+70an
.'rc'rlfhr 1 p ty_ age '. of 1
�Y�'� Is}uiri .xul}epri Pace �
ainple Reedpt Cbee Wist (SRC)
Client: Svn";ru Conlor incnecsp.ri hvl'Onta- .'RCr2 i 011:nG22 I nr#• NA12UIE
Ivli, ms of rcccip:: 1 f'�l.c 'Itcn: I I ;ll" FedT x OthrW;
i'es
}Jr.• 1. Wein! custody seat} p_esentonthe. cooler?
l'es
No , N.A'2. 1.'cwstadj seals'.vete pmvrit, wore #hey intact and unbroken?
pH Strip 10: R^ {'hlorineStrip JD: J" ... - Tcstcd by: ..-.
Original temperetwa upon re, e;pt r' Dcrived (Corected) leulpenature upon n uchpt °/:�3olid Snap -Cup ID'
1.4 3.w ef- NA INA oC NA 1 NA ,C NA INA oC
Mclhod: QTcmperature D=ank ❑kviInst I RYMes IR tswi la. 5 IR Gun Carrvction Factor: °C
M�Ihcul ofroolaitr. 17]Wellce ❑ Ice Pwks Q D ice ❑done
_
If temperwure of aft)' cooler exceeded 6-01T wa; Projecl h+ln rwgrr Notified?
I'M mras Nmtiflec by' ph<n iC I eraail f faoe-[o-Cate (uin:Iu 9 311)e}-
5fed Ll No
NA
4. Is [[ic commercial :.ow'ier's Wkino, slip.atr x hed a this form?
Yes
No
5- 'AVam prvprrcustody procedures (relirrquishi.;LVrcaoivcd) foliDwede
Yes
No
6. '7w' z; sump lc I Ds l isted nn the C)OM
x Yes
❑ No
7. 'Rlem siunple 1Ds J [stud on all parr p Ic -uonta [nerS7
8r orbs calLectiau dare R ri,rr� lislCd on the COC7
4�N
9, V,'� eo]lectian dare& tune lisieri rrn gI[sample crutainer�?
10. old3I1cartrurk.rIa1;eI inf{]rir,i,tl,n (ID, daft. time)a ee with [hr"COC?
I : , %Vfre fasts to b� ptrfvnmed limd oa the COC?
Yes
No'
[2- Did all Samples arrive hi the proper unnrdinm for each fest an:lor in gaad =dition
(iwhroken, lids on, e;o,)?
= Yes
Nl0
13_ a5 iY jequate sample volume avail*10
Yas
Tin
14- W= Hll 53rnples r meived within 4 tl,c holding time car 48 ltrrurq, whiclievcr comics i'irgt;j
Yes
� No
1$_ VJ any sanipics aooftalner3trissinlfexcrbs (circle. one) mnt•les Not kiw Uri COO?
Ely-
1:1 No
VINA
16- For VOA and RSK-175 stunpJes, were bu[;K4! prt;:4mt. !�-„peg-size Grtia-j ire ciamri r)
sn 311 oFlbe VOA vials? !
17, Wereal D ROlmetal _ uricnt sariiplcs rewi ved ArapH Df < 7?
J:jYes
N ro
,f NA
Yes
Na
NA
I S. Were a'.1 cyanide mrnpleE noosived.at s pf! :- 13 a_ cs sulftdosun plcsrcccivcdat a pr[1 > 9?
� Yes❑
_No
❑+f N�1
9. Were all applicable NH3 cyaai c�phetiGV625-1M08-? (-<q.5mg�t,) s;�mples tiw t)l'
re-.611.21 r.hlviinr'�
Dyes
❑ M
QNA
20- Werr. 4:limr ralnarks,Wqrtests (I-e- rugrjckt!d diluiian3, M4 VW5D designarinirs, etc,,,)
c3macdvlrfimr.-ribrri From theCOC inwthe eomment sec#ion in f,[MS7
yes
No
21- Was lb-, gum number lisrcd on the Ltffltxirwr lalx�? 1 f vrk Qiotki 0
Samplc Preservation (Misr he complend f�r any sarnp[e(s) Incorrectly f3Mmr-vL:J r with A=dspaee,)
Salnp-e(s) "n _ -- were receivcd incorrectly pr�sffved and were uslwd =!urdingly
In IaMple rilMi 7rlg with NA rnL ofcirc[e oye; 147SO4, HNO3, HCI, NaOH using SR J, NA
Time of pm-wrvufiun MA Jf rr:ore ;ham one prenirvative is needed, please note in U, tlomnlcals bi;low.
Sample(s) NA wea-e received wilt bubblrs>6 min in diarrictcr,
. ampl es{sj FA were jcveived with TRC > 0,5 ntyL (lf q l9 is pro }and wee
adjusted accordingly In sample rmciving with -odium thicsuliate (Na?S,()3) wit11 Sltcaly ]7} NA
SR b=ado leach appiiod by: JRC2 MC; OVC2r2022
Comments:
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

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SECTION 4

SUMM111
ENVIRONMENTAL TECHN❑LOMZ3. INC
Arraly0ca1 Laboralorfas
January 20, 2022
Chris Wynne
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL:
FAX:
RE: Farmville WWTP
Dear Chris Wynne:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
Order No.: 22010630
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/12/2022 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 2943, Colorado, Connecticut PH-0108, Florida NELAC E87688, Idaho 01100923, Illinois 200061, Indiana C-011-13, Kansas
E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988, Minnesota 1780279, Nevada 011009232020-1, New
Hampshire 2996, New Jersey 011006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP CL0052, Oklahoma
2019-155, Oregon 0112O0001, Pennsylvania 011, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-19-16, Utah 011009232020-12,
Virginia VELAP 10381, West Virginia 9957C
Page 1 of 37

SUMMIY Summit Environmental Technologies, Inc. Case Narrative
3310 Win St.
ENVIRONMENTAL TEC„HQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 wo#: 22010630
Arralyi9cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com Date: 1/20/2022
CLIENT: Synagro
Project: Farraville WWTP
WorkOrder Narrative:
22010630: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
22010630-OOIA TCLP-SVOC_8270E: CCV exhibited high recoveries for Hexachlorobenzene and
Hexachlorobutadiene. Sample is ND for these analytes.
22010630-OOIA MTL-TCLP-7(6010D): LCS-54357 exhibits high recovery for Silver. Sample is ND
for this analyte.
22010630-OOIA TCLP-VOC-MSTR 8260D: CCV exhibits high recovery for Vinyl chloride. Sample is
ND for this analyte.
22010630-001a TCLP-SVOC-CPEST(8081B): Bracketing CCVs and LCS-54350 exhibit high
recoveries for Heptachlor and Methoxychlor. Sample is ND for these analytes. P: RPD between
confirmation column is greater than 40%.
Original
Page 2 of 37

summly Summit Environmental Technologies, Inc. Case Narrative
3310 Win St.
ENVIRONMENTAL TEC„HQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 wo#: 22010630
Arralyi9cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com Date: 1/20/2022
CLIENT: Synagro
Project: Farraville WWTP
Analytical Sequence QC Notes:
CCV 40ppm SVOC-MSTR S(8270): CCV exhibited outlying recoveries for several analytes.
Associated samples may be biased accordingly. Surrogate outside recovery limits. Minimum method
criterion of one surrogate within established recovery limits was met.
LCS-54353 SVOC-BNA_TCLP(8270): Possible high bias for Hexachlorobenzene and
Hexachlorobutadiene due to high recoveries in CCV.
CCV VOC-MSTR_NPW(8260): CCV exhibits high recovery for Vinyl chloride. Associated samples
are ND for this analyte.
LCS VOC-MSTR NPW(8260): Possible high bias for Vinyl chloride due to high recovery in CCV.
LCS-54350 TCLP-SVOC-CPEST(8081B): LCS-54350 exhibits high recovery for Heptachlor.
Associated samples are ND for this analyte.
P: RPD between confirmation column is greater than 40%. Possible high bias for Heptachlor and
Methoxychlor due to high recoveries in bracketing CCVs.
MB-54350 TCLP-SVOC-CPEST(8081B): P: RPD between confirmation column is greater than 40%.
Original
Page 3 of 37

�� Summit Environmental Technologies, In Qualifiers and Acronyms
SU3310 Win S
EkiwllOMM@NTALTECHN❑LOG{r,S,INC Cuyahoga Falls, Ohio442� Wo#: 22010630
Arraly0cal Laboralorlas TEL: [phone] FAX.- (330) 253-446
Wehsite: httn:11www.settek.co Date: 1/20/2022
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
PLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 4 of 37

�� 1 � Summit Environmental Technologies, Inc.
SU3310 Win St.
ENVIRCNMEWAL YECHHOLOGNUS, JNC, Cuyahoga Falls, Ohio 44223
Analytical Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
CLIENT: Synagro
Project: Farmville WWTP
Lab SampleID Client Sample ID
22010630-001 Farmville WWTP
Tag No Date Collected
1/10/2022 11:00:00 AM
Workorder
Sample Summary
WO#: 22010630
20 Jan-22
Date Received Matrix
1/12/2022 10:30:00 AM Sludge
Page 5 of 37

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Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arralyt9cal Laboralorfas TEL: [phone] FAX. [phone]
Website: http://�i,-"-m,.settek.coin
Analytical Report
(base report)
WO#: 22010630
Date Reported: 1/20/2022
CLIENT:
Synagro Tag Number:
Matrix:
SLUDGE Collection Date: 1/10/2022 11:00:00 AM
Lab ID:
22010630-OOIA
Project:
Farmville WWTP
Client Sample ID Farmville WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury ND
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
ND
TCLP Badum(Ba)
ND
TCLP Cadmium(Cd)
ND
TCLP Chromium(Cr)
ND
TCLP Lead(Pb)
ND
TCLP Selenium(Se)
ND
TCLP Silver(Ag)
ND
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
ND
2,4, 5-Trichlorophenol
ND
2,4,6-Trichlorophenol
ND
2,4-Dinitrotoluene
ND
Cresols, Total
ND
Hexachloro-1,3-butadiene
ND
Hexachlorobenzene
ND
Hexachloroethane
ND
Nitrobenzene
ND
Pentachlorophenol
ND
Pyridine
ND
Surr: 2-Fluorophenol
77.8
Surr: Phenol-d6
81.5
Surr: Nitrobenzene-d5
60.4
Surr: 2,4,6-Tribromophenol
109
Surr: 2-Fluorobiphenyl
67.8
Surr: p-Terphenyl-d14
110
SW7470A SW7470A Analyst: KLC
0.00200 mg/L 1 1/14/2022 5:49:00 PM
SW6010 SW301OA Analyst: MSK
0.500
mg/L
1
1/18/2022 10:05:00 AM
5.00
mg/L
1
1/18/2022 10:05:00 AM
0.100
mg/L
1
1/18/2022 10:05:00 AM
0.200
mg/L
1
1/18/2022 10:05:00 AM
0.500
mg/L
1
1/18/2022 10:05:00 AM
0.0500
mg/L
1
1/18/2022 10:05:00 AM
0.500
QL+ mg/L
1
1/18/2022 10:05:00 AM
SW8270 SW351OC Analyst: SFG
0.200
mg/L
2
1/17/2022 7:29:00 PM
0.500
mg/L
2
1/17/2022 7:29:00 PM
0.500
mg/L
2
1/17/2022 7:29:00 PM
0.100
mg/L
2
1/17/2022 7:29:00 PM
10.0
mg/L
2
1/17/2022 7:29:00 PM
0.0400
QC+ mg/L
2
1/17/2022 7:29:00 PM
0.100
QC+ mg/L
2
1/17/2022 7:29:00 PM
0.200
mg/L
2
1/17/2022 7:29:00 PM
0.200
mg/L
2
1/17/2022 7:29:00 PM
0.500
mg/L
2
1/17/2022 7:29:00 PM
0.500
mg/L
2
1/17/2022 7:29:00 PM
10 - 157
%Rec
2
1/17/2022 7:29:00 PM
10 - 169
%Rec
2
1/17/2022 7:29:00 PM
32.1 - 130
%Rec
2
1/17/2022 7:29:00 PM
45.4 - 166
%Rec
2
1/17/2022 7:29:00 PM
35.7 - 130
%Rec
2
1/17/2022 7:29:00 PM
70 - 145
%Rec
2
1/17/2022 7:29:00 PM
Qualifiers: B
Analyte detected in the associated Method Blank
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
OG 1
PL Permit Limit Original
RL Reporting Detection Limit
Page 7 of 37

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arrafyt9caf Laboralorfas TEL: [phone] FAX. [phone]
Website: http://�i,-"-m,.settek.coin
Analytical Report
(base report)
WO#: 22010630
Date Reported: 1/20/2022
CLIENT:
Synagro Tag Number:
Matrix:
SLUDGE Collection Date: 1/10/2022 11:00:00 AM
Lab ID:
22010630-OOIA
Project:
Farmville WWTP
Client Sample ID Farmville WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8081
SW351OC Analyst: CSS
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total
ND
0.0250
mg/L
10
1/15/2022 4:13:00 PM
Toxaphene
ND
0.0500
mg/L
10
1/15/2022 4:13:00 PM
Endrin
ND
0.00500
mg/L
10
1/15/2022 4:13:00 PM
gamma-BHC
ND
0.00500
mg/L
10
1/15/2022 4:13:00 PM
Heptachlor
ND
0.00500
QL+ mg/L
10
1/15/2022 4:13:00 PM
Heptachlor epoxide
ND
0.00500
mg/L
10
1/15/2022 4:13:00 PM
Methoxychlor
ND
0.00500
QC+ mg/L
10
1/15/2022 4:13:00 PM
Surr: TCMX
80.1
10 - 119
%Rec
10
1/15/2022 4:13:00 PM
Surr: DCB
91.7
10 - 119
%Rec
10
1/15/2022 4:13:00 PM
TCLP HERBICIDES BY EPA 8321 B
SW8321
Analyst: TM
2,4-D
ND
0.500
mg/L
50
1/18/2022 8:36:00 PM
2,4,5-TP
ND
0.500
mg/L
50
1/18/2022 8:36:00 PM
Surr: 2,4-Dichlorophenylacetic aci
91.7
70 - 130
%Rec
50
1/18/2022 8:36:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260
SW1311M Analyst: SFG
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
0.250
mg/L
50
1/14/2022 4:14:00 PM
1,2-Dichloroethane
ND
0.250
mg/L
50
1/14/2022 4:14:00 PM
MEK
ND
5.00
mg/L
50
1/14/2022 4:14:00 PM
Benzene
ND
0.250
mg/L
50
1/14/2022 4:14:00 PM
Carbon tetrachloride
ND
0.250
mg/L
50
1/14/2022 4:14:00 PM
Chlorobenzene
ND
2.50
mg/L
50
1/14/2022 4:14:00 PM
Chloroform
ND
0.250
mg/L
50
1/14/2022 4:14:00 PM
Tetrachloroethene
ND
0.250
mg/L
50
1/14/2022 4:14:00 PM
Trichloroethene
ND
0.250
mg/L
50
1/14/2022 4:14:00 PM
Vinyl chloride
ND
0.100
QC+ mg/L
50
1/14/2022 4:14:00 PM
Surr: 4-Bromofluorobenzene
109
70 - 130
%Rec
50
1/14/2022 4:14:00 PM
Surr: Di brom ofl uorom ethane
93.4
70 - 130
%Rec
50
1/14/2022 4:14:00 PM
Surr: Toluene-d8
98.4
70 - 130
%Rec
50
1/14/2022 4:14:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified
compounds
ND Not Detected
OG1
P Second column confirmation
exceeds
PL Permit Limit
Original
R RPD outside accepted recovery
limits
RL Reporting Detection Limit
Page 8 of 37

MMIT
Summit Environmental Technologies, Inc. Analytical Report
SU3310 Win St.
ENVIRONMENTAL TECHNOLOGIE-3, IRC Cuyahoga Falls, Ohio 44223 (base report)
Arrafyt9caf Laboralorfas TEL: [phone] FAX.- [phone] WO#: 22010630
Website: http://www.settek.com Date Reported: 1/20/2022
CLIENT:
Synagro Tag Number:
Matrix:
SLUDGE Collection Date: 1/10/2022 11:00:00 AM
Lab ID:
22010630-OOIA
Project:
Farmville WWTP
Client Sample ID Farmville WWTP
Analyses
Result
RL Qual Units
DF
Date Analyzed
RCI
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive
ND
0.481 mg/Kg
1
1/18/2022 3:35:00 PM
IGNITABILITY OF SOLIDS (SW-846: 1030)
SW1030
Analyst: ALT
Ignitability nonflammable
mm/sec
1
1/18/2022 6:35:04 PM
PERCENT SOLIDS BY SM2540MOD
A2540B
Analyst: DHC
Percent Solids
7.46
%
1
1/18/2022 5:20:00 PM
RCI
SW9045D
Analyst: ALT
PH (SW9045D)
pH
6.6
s.u.@18.2C
1
1/18/2022 5:07:41 PM
RCI
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive
ND
25.0 mg/Kg
1
1/18/2022 3:35:00 PM
Qualifiers: B
Analyte detected in the associated Method Blank
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
OG 1
PL Permit Limit Original
RL Reporting Detection Limit
Page 9 of 37

Summit Environmental Technologies, Inc.
Accreditation
Program
MM'EF
frSU3310 Win St.
Analv n tes Report
ENwIROMMEWALYECHNOL.OG{r,S,INC
Cuyahoga Falls, Ohio44223
J
Y
ArralyVcal Laboralorlas
TEL: [phone] FAX.- [phone]
Wo#:
22010630
Wehsite: http://www.settek.com
20-Jan-22
Client: Synagro
State: NW
Project: Farmville WWTP
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
22010630-OOIA Sludge
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Sludge
Percent Solids by SM2540Mod
Percent Solids
N
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Sludge
TCLP Herbicides by EPA 8321B
2,4,5-TP
A
Sludge
TCLP Herbicides by EPA 8321B
2,4-D
A
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Version #2
Page 10 of 37

Summit Environmental Technologies, Inc.
Accreditation
Program
MM'EF
frSU3310 Win St.
Analv n tes Report
EMOROMMEWAL YECHHOL.OG{r,S,
INC Cuyahoga Falls, Ohio 44223
J
Y
ArralyVcal Laboralorlas
TEL: [phone] FAX.- [phone]
Wo#:
22010630
Wehsite: http://www.settek.com
20-Jan-22
Client: Synagro
State: NW
Project: Farmville WWTP
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
22010630-OOIA Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Sludge
TCLP Volatiles Analysis
1, 1 -Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chloroform
A
Sludge
TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge
TCLP Volatiles Analysis
Trichloroethene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
Version #2
Page 11 of 37

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Page 36 of 37

�� � � Summit Environmental Technologies, Inc.
SU3310 Win St.
ENVIRONMENTAL TECHNOLOQH�S.IfiC Cuyahoga Falls, Ohio44223 Sample Log -In Check List
Arrafocaf Laboralorias TEL: [phone] FAX.- [phone]
Website: http://`h,,",m,.settek.com
Client Name: SYN-NC-27028 Work Order Number: 22010630 RcptNo: 1
Logged by: Christina N. Jager 1/12/2022 10:30:00 AMr'
Completed By: Christina N. Jager 1/13/2022 3:06:01 PMdrx
Reviewed By: Jennifer Woolf 1/14/2022 10:40:02 AM
Chain of Custody
1. Is Chain of Custody complete? Yes ❑d No ❑ Not Present ❑
2. How was the sample delivered? UPS
Lop In
3. Coolers are present? Yes ❑d No ❑ NA ❑
4. Shipping container/cooler in good condition? Yes d❑ No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present V
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes ❑d No ❑ NA ❑
6. Were all samples received at a temperature of >0° C to 6.0°C Yes ❑d No ❑ NA ❑
7. Sample(s) in proper container(s)? Yes ❑d No ❑
8. Sufficient sample volume for indicated test(s)? Yes ❑d No ❑
g. Are samples (except VOA and ONG) properly preserved? Yes ❑d No ❑
10. Was preservative added to bottles? Yes ❑ No ❑d NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
❑
No ❑ No VOA Vials ❑�
12. Were any sample containers received broken?
Yes
❑
No ❑d
13. Does paperwork match bottle labels?
Yes
No ❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
❑d
No ❑
15. Is it clear what analyses were requested?
Yes
❑d
No ❑
16. Were all holding times able to be met?
Yes
No ❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
❑
No ❑ NA V
Person Notified: Date:
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Cooler Information
Cooler No
Temp °C
Condition
I Seal Intact
Seal No
Seal Date
Signed By
1
12.7
Goodl
Not Present
Page 37 of 37

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name. Town of Farmville WQ Permit Number: WQ0008778
811WTP Nanne: ToNS,in of Fari"vilie WWTP, Di ester Basin NPDES Number: NCO029572
Monitoring Period: From 01/01/22 To 12/31/22
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.( 106) - PIease indicate level achieved and alternative performed:
Class A:
Alt. I/A (tune/temp) Alt. 2/13 (Alk Treatment) Alt, 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt, 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class D:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
1rr--...t:.. L1.. ♦..101... A — VT... R' --W. fhn f.11-- n—Unv;nro rtafar
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean. Maximum Units
dences
Analysis
Fecal
2x10to tine 691
MPN
MPN/g
Coliform
power per gram
of total solids
91606
190000
508000
CFU/g
0
Annually
Grab
SM9222D
CFU
-MF
I000 MPN per gran' of
MPN/g
total solids (dreight)
Salmonella
3 MPN per 4 grams total
bacteria (inn
solids (dry «eight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt, 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Ark Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt, 9
(Injection)
Option/Alt.10
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32115A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33115A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32115A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (PIease note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
persolnrnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
David Hodgkins, Town Manager
Preparer Name and Ti a or print) Laud Applier Name and Title (if applicable) (type or print)
Signature of Prepares* Date Signature of Land Applier (if applicable)
Date
*Prepares is defined in 40 CFR Part 503.9(r) and t5A NCAC 2T.1102 (26)

Cameron Testing Services, Inc. Laboratory Report NC DENR #654
NC PHHS #37799
US EPA #NC01918
Client: Synagro CTS Proj. 1 2201-0060 DW Cert # 37799
Project: Farmville WWTP Regulatory Yes
Sample Information
Sampled C. Wynne Date 01/06/22 Received J. Cameron Date 01/06/22
Analyses and Results
E 2 d= y 8 Std. Methods
rLab1D Sample 1D M O `� Analyta Result c m ,E m
U c? .r ❑ c Reference
2201-0060 -01 3ludge Gr Fee. ColiformS 163000 CFUrg 40800 01/07/22 CSC 9222D - MF
-02 95800 CFU1g 24000
-03 508000 CFUig 39100
-04 423000 CFU,g 84700
-05 218000 CFurg 21800
-06 133000 CFUrg 22200
-07 91$00 CFulg 30500
Geomean 190000
2201-0060 -01 31udge Gr
TS (%) 8.01 %
%
0.01 01/11/22 KSW 2540 G -TS
-02
10. 3 %
%
0.01
-03
7.36%
/.
001
-04
3.99%
%
0101
-05
14.5%
%
o.oi
-06
14.6%
%
o.oi
-07
9.78%
%
0.01
Report
Review qX4
Project Manager Date
219 S. Steele Str. 919-208-4240
Sanford NC 27330 [e-mail] camerontesting.com

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SECTION 6

Agricultural Lime Application Log
Year 2022
Project Farmville
Fields Soil Lime Requirements Tons/Acre Date
(state -county -site -field) PH (from soil analysis) Applied A limed
PI-01-1 5.6 0.8T N/A
PI-01-2A 5.6 0.6T N/A
PI-01-6 5.7 0.7T N/A
N/A -Did not apply in 2022
*Lime will be applied when field conditions/cropping pattern permits

SECTION 7

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