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HomeMy WebLinkAboutWQ0006017_2022 Residual Annual Report_20230227 (2)Initial Review Reviewer Nathaniel.Thornburg Is this submittal an application? (Excluding additional information.) * Yes No If not an application what is the submittal type?* Annual Report Residual Annual Report Additional Information Other Annual Report Year* 2022 Permit Number (IR) * WQ0006017 Applicant/Permittee Town of Beaufort Email Notifications Does this need review by the hydrogeologist? * Yes No Regional Office Wilmington CO Reviewer Admin Reviewer Submittal Form Project Contact Information Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence. Name* Lysa Finnerty Email Address* LFinnerty@synagro.com Project Information ......................... Application/Document Type* New (Fee Required) Modification - Major (Fee Required) Renewal with Major Modification (Fee Required) Annual Report Additional Information Other Phone Number* 4105376150 Modification - Minor Renewal GW-59, NDMR, NDMLR, NDAR-1, N DAR-2 Residual Annual Report Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* Wastewater Irrigation High -Rate Infiltration Other Wastewater Reclaimed Water Closed -Loop Recycle Residuals Single -Family Residence Wastewater Other Irrigation Permit Number:* WQ0006017 Has Current Existing permit number Applicant/Permittee Address* 435 Williams Court, Ste 100, Baltimore, MD 21220 Facility Name* Town of Beaufort Class B Residuals Program Please provide comments/notes on your current submittal below. 2022 Annual Report for Town of Beaufort, NC At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here. (Application Form, Engineering Plans, Specifications, Calculations, Etc.) Beaufort NC 2022 Annual Report FINAL.pdf 4.07MB Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger than upload limit. * By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Submission Date 2/27/2023 435 Williams Court, Suite 100 Baltimore, MD 21220 www.synagro.com FEBRUARY 27, 2023 NCDEQ Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: 2022 Annual Report for Permit No. WQ0006017 Dear NCDEQ: SYNAGRO Synagro is submitting one electronic copy of the above referenced report on behalf of the Town of Beaufort, NC. If you have any questions or need additional information, please do not hesitate to contact Donovan Willis at (252) 728-7166 or Matthew Carter at 336-705-9886. Sincerely, 01171 Y--�m Derrick Shivar Environmental Compliance Manager Enclosures cc: Donovan Willis — Town of Beaufort Matthew Carter, Synagro YOUR PARTNER FORA CLEANER, GREENERWORLD TOWN OF BEAUFORT, NC RESIDUALS LAND APPLICATION PROGRAM Permit No. WQ0006017 2022 ANNUAL REPORT Town of Beaufort, NC Residuals Land Application Program 2022 Annual Report TABLE OF CONTENTS 1. Certification Form and Annual Operations Summary 2. Annual Residual Sampling Summary Forms and Residuals Analyses 3. Annual Land Application Field Summary Form 4. TCLP Analysis 5. Pathogen ReductionNector Attraction Reduction 6. Soil pH & Lime Application Records 7. Soil Analysis SECTION 1 ANNUAL LAND APPLICATION CERTIFICATION FORM Permitumber W00006017 County Carteret Year 2022 Facility acne (as shown on permit) Beaufort WWI'P—NPDF.S No. NCO021831 Land A Iication Operator Synagra Phonc# (336) 998-7150 Land api f ication of residuals as allowed by the above permit occurred during the past calendar year X S NO. If NO, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied, please a ach an explanation on how the residuals were handled. *Total n mber of application fields in permit. 2 *Total ber of fields utilized for land application during the year. I *TotalImber unt of dry tons applied during the year for all application sites. 68.64 *Total of acres utilized for land application during the year. 40.00 Facility was compliant during calendaryear 2022 with all conditions of the land application permit (including but not limited to items 1-13 be w) issued by the Division of Water Quality X YES NO. If no, pl ase provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pN was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3 ) copies of certified laboratory results arc attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in I SA NCAC 02T . 1105(a) or the Pollutant Loading Rates in 15A NCAC; 02T ,1 105(b) (Applicable to 40 CPR Part 503 regulated facilities). 7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CPR Part 503 regulated facilities). 8. All monitoring and reporting requirements in 15A NCAC 02T.1 111 were complied with (applicable to 40 CPR Part 503 regulated facilities). 9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. It. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit. 12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13. All buffer requirements as specified on the permit were maintained during each application of residuals, "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I gun a vgrrc that there are significant penalties for submitting false information, including; the possibility of fines and imprisonment for knowing violations." Perni4e Name and Title (type or print) Signal re ofPreparcr* Date (if dill rent from Permittee) ID. 2"41 Z :;: 7— //%'�.0W Signature of er tittee Date 2/01 /2023 nature ofLa Applier Date (if different from Permittec and Preparer) is defined in 40 CFR Part 503.9(r) and 15ANCAC 02T.1102 (26) DENR FORM ACF (12/2006) OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA ALL COUNTIES - ALL SITES DATE RANGE: 1/1/2022 - 12/31/2022 BEAUFORT,NC BEAUFORT, NC AEROBICALLY DIGESTED CAKE MONTH/YEAR May 2022 TOTAL Units Key: D - Dry Tons; G — Gallons; W — Wet Tons; Y — Cubic Yards Report Date: 1/27/2023 6:37:45 PM AMOUNT UNIT DRY TONS UNIT DRY METRIC TONS 500.00 Y 68.64 D 62.26 500.00 Y 68.64 D 62.26 SECTION 2 m LL d.' 4 a w C EY. � 0 LL m N 21 a R. F- ZIL c � m I 0 a ES N ❑ R. N C :Lu Q z C a� U z m o O "" Q LL OCf ❑ O z ca G1 i q ci m to Z a Z Q C! u ❑1 LLz c i T m c1Ov C) M r N N w cD N V 0 0 0 0 o Z Z Z z 40 Cl) Z� Ln� o� Z 2 c _a a b z O 7 0)z '0 � 1.3 j 'C m c E E n m .c o •Q1 a$ U U U' z U") R ►° ►-• dE z I w a A N k 0 j 0 ) 0 o L & LL 0 k \ z ƒ 8 G E g 8 8 7 S -It® q % 9 C3 \ � % � N 0 to 0p 0 PaceAnalyfical Report of Analysis Synagro 12701 Lancaster Hwy Pineville, NC 28134 Attention: Chris Wynne Project Name: Beaufort WWTP Lot Number:XA13016 Date Completed:02/08/2022 NIM�� Mr� 02/08/2022 3:54 PM Approved and released by: Project Manager II: Lucas Odom Q PCCRBp�� AAW 'ye I ANSI NdmlAccre00- Board eORft Al A C C R E D I T E D TESTING LABORATORY The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC. Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 Tel:803-791-9700 Fax:803-791-9111 www.pacelabs.com Page 1 of 7 PACE ANALYTICAL SERVICES, LLC SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative Synagro Lot Number: XA13016 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Where sampling is conducted by the client, results relate to the accuracy of the information provided, and as the samples are received. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace") Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or discussed below. Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2- dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7, Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal Coliform Colilert-18. Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight unless flagged with a "W" qualifier. If you have any questions regarding this report, please contact the Pace Project Manager listed on the cover page. The pH analysis associated with the sample(s) in this report was/were performed after the method recommended 15 minute holding time. Inorganic Metals Due to the low percent solids, the initial amount of the following samples is 3x greater than standard procedure: XA13016-001. The LOQ has been adjusted accordingly. Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 vvvvvv.pacelabs.com Page 2 of 7 Client:Synagro Laboratory ID:XA13016-001 Description: Beaufort WWTP Matrix: Solid Date Sampled:01/12/2022 1030 % Solids: 16.3 01/18/2022 0045 Date Received:01/13/2022 Inorganic non-metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (% Solids) SM 2540G 1 01/18/2022 0045 NBW 28681 1 350.1 (Ammonia - N ) 350.1 5 01/19/2022 2139 DAK 28766 1 (Nitrate - N ) 9056A 5 01/20/2022 2240 AAB 29256 3 (Nitrite - N ) 9056A 10 02/03/2022 0419 SUH 30794 1 (Phosphorus) 365.1 100 01/21/2022 1703 DMA 01/21/2022 1208 29127 1 (Soil pH meas) 9045D 1 01/17/2022 2203 NBW 28677 1 351.4 (TKN) 351.2 10 01/24/2022 1057 DMA 01/21/2022 1404 29104 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run % Solids SM 254OG 16.3 % 1 Ammonia - N (gas diffusion) 350.1 620 31 16 mg/kg 1 Nitrate - N (soluble) 9056A 1000 15 3.1 mg/kg 1 Nitrite - N (soluble) 9056A 260 12 6.1 mg/kg 3 Phosphorus 7723-14-0 365.1 22000 3100 610 mg/kg 1 Soil pH measured in water @ 20.7 ° C 9045D 6.2 su 1 TKN 351.2 42000 3100 1500 mg/kg 1 CVAA Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7471B 7471B 1 01/21/2022 0557 JAB2 01/21/2022 0141 28437 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7471B 0.99 0.49 0.12 mg/kg 1 ICP-AES Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3050B 601OD 1 01/19/2022 1323 JMH 01/19/2022 0051 28436 2 3050B 601OD 5 01/19/2022 1400 JMH 01/19/2022 0051 28436 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Aluminum 7429-90-5 6010D 8600 38 14 mg/kg 1 Arsenic 7440-38-2 6010D 12 1.4 0.47 mg/kg 1 Cadmium 7440-43-9 6010D 1.2 0.47 0.12 mg/kg 1 Calcium 7440-70-2 6010D 36000 2400 300 mg/kg 2 Chromium 7440-47-3 6010D 26 0.94 0.24 mg/kg 1 Copper 7440-50-8 6010D 630 4.7 2.1 mg/kg 2 Iron 7439-89-6 6010D 27000 9.4 4.3 mg/kg 1 Lead 7439-92-1 6010D 30 0.94 0.42 mg/kg 1 Magnesium 7439-95-4 6010D 4200 470 59 mg/kg 1 Manganese 7439-96-5 6010D 650 1.4 0.56 mg/kg 1 Molybdenum 7439-98-7 6010D 7.1 3.8 0.94 mg/kg 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 3 of 7 Client:Synagro Laboratory ID:XA13016-001 Description: Beaufort WWTP Matrix: Solid Date Sampled:01/12/2022 1030 % Solids: 16.3 01/18/2022 0045 Date Received:01/13/2022 ICP-AES Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3050B 6010D 1 01/19/2022 1323 JMH 01/19/2022 0051 28436 2 3050B 6010D 5 01/19/2022 1400 JMH 01/19/2022 0051 28436 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Nickel 7440-02-0 6010D 17 3.8 0.99 mg/kg 1 Potassium 7440-09-7 6010D 2200 470 59 mg/kg 1 Selenium 7782-49-2 6010D 6.0 1.9 0.77 mg/kg 1 Sodium 7440-23-5 6010D 3800 470 59 mg/kg 1 Zinc 7440-66-6 6010D 1200 24 5.9 mg/kg 2 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 4 of 7 Chain of Custody and Miscellaneous Documents Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 5 of 7 PACE ANALYTICAL SERVICES, LLC 0 z G 72 L) "Iz 371,1 aseei+j pue MO 1 � I '4dw. S 1 rn i} -34} Ir gd ON m WN OJEE%ft Nc�{�v �• �"' m t { CJ LL T V} S.} o m m E .' ra ;P. 'giry-I'P J11 I t3 tA V . � pp� 211, z _ - m � � y H d L1 ❑ - Q y �. t 00 5� C ao s,' F u H gr OL .4 � k 4 I I m I o � I n ` a p �� 121 `-ri C c eu !4Er m a 13 Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 6 of 7 dl5 A C � LL t E : E }. m I .w r F� CJ M. p Iwo L k .Q �r m J z W v o del 9Y c ` Lu IL 0 { yy m a 3 r•-y � rY q`I '9P C e ir XF S y u 13 _ �_p PACE ANALYTICAL SERVICES, LLC sarnplesReceiptchecklist (SRC)(MEUOIRc-1.51 R +ised;9f'9/201D Issurne AuLhori,-y; Pace MV - M-01 PagQ 1 of 1 Sample Receipt Checklist (SRQ :ient- Synyry Cnlr-rTtS Cted r`clutr; K5�' i +' i13+=022 l{lLi+: XA1301G Nllmrs at'reeei t: Pa 6 1 C jml; UPI. Lj rMP-x Lj OLl&er _ - — �Nu L- WL-rc rns#otvseals sort on LiseclK)jn:- • Yea Nc� NA 2. if mistod y W-A-As wore rpsznt, were the irract and unbrckcn r pH Strip ID., ]"A Come Sl.rip J f}_ 1"A . Te xd by. `A Original LemrwMtin-e upar r+xvi-x f Dffived (Gontgred) tempeFaturc c_pon receipt %Solid ShCl are-ip II): �L r.5 ;1.4 -%c. 'IA iNA aC NA jUA oC NA /XA a,( Mathac: �TrMp Lracure kllanir J❑¢,j;uinst Batt'"ems Tit; C,un IJ-3_ _ Ilk GLn Correct -on Facli�7: "C Mothod of uoulunt: 0 wet lee ❑ Ice Packs ❑ 13 . Ice ❑Nano ❑ Yes ❑ ]�lu ' �JMA 3. I[ Lcallperatitry of any tbblor exec eYlc l 6.ft�{.`. was P abed Manger ToL'a�eil'; Pfwl was Notified i : phdno ! ensail I fwuo-tr-f� re (cir� lr cmcj, Wes AJn NA 4, Js tlr 4ur�m•_rCia_ courier's packing sl= atLgcJicdta rhis torus' V Yrs Tdo 5. Wow proper cits5ody procedures (rcl:nquished,'recelved , fol=owt!j? M Y'ud, U Ma 6- W�knv mrnple IDs Eistcd twi the [:r.1C? M1'Ti M No _ 7- VkIc.� !;alnpJe. IDs Ii-,ted on all sample con miners? yc Al LJNO S"kFps co][cciian Gate 4, lime listed oCt Lf]¢ CC?CF - ❑d Yes 'No 9, l�.'as coilcotiout r1arCc lime listedcn all sample CorLuincls'J Yes No 10- Dicl all conta.irler [abe[ infbnHatii3n (JD, date, time} -&gene with IEu' Ct]C7 0 yes NO 11. Were LWLN tob4 pertormcd IMcd a,>I 113eCDC`.? 0 Yes ❑ No 12. Di d 3.11 falr pies A-rivi, in ells proper conlafri.ers for each test al1d,',k in goad conditicrl (Mlbfi-lceri, IvN an, etc.)? FA Yes LJ Nu 113. Was adsquam sample volumo Livai ialsla'I Ycs .� _ No 14. Were all sym�{+h� ples received L/a ds 1 e ho[dingtime or49 hours, whiclievrrr,(MICS first? Yes No 15_ Wcrz any sam ley conte"nein 1.1Lqsin&'0Xceess (63> Cie ano) sam ples Nne Ilstsa an COC'# 16- Foi, VOA and RSK-' 75 samp[eg, we-x� bubbieS present >;,pea.size" (V4'°or 15mm in diaini,, i) © Y43 ❑ NO ❑NA in any oFlhc V0A vfalt 4 I Yr.s 'No d NA _ 11. Were aft DR(Mil eFafWaul-ricnt %M pies recei•A4 at a PH of � 27 `r'vs _ N41 ;� A [ANA 113 '.Mare FLll cyanide samples rc=ived at a VH> i2 and mil Fain sam les rrL;tfv-.d at a pI•l i �? 19. Were ed I LLpp1jcqbJeNRy7 Ic}mnid&phenull�25,:IGGB_3 (= ,5mg L)SainpIr. 'r6.at' ❑ 'ys ❑Nq residual cHurina'I ❑ YL`' ❑ Na MNA 20. 1k'ero c1i=t rrmErWrequests (i-e- toqucstcd dilutions, MSIMSD desigrr,iicim. etc...) wrrruLly aanscrilied rronl the COC' into the camment seotaon in ijMS? 2 1 - wns tho Qnnre JIUMber Iis" on ILr G0F1taine1- label? If ves. Ounce k Y / No SLample 1'reservalion (Must be eoruplctod to. any mirnpie(S) un;r m-;L.y preserved or with headq- ,) sample() N. Uere received inrarmctly preerved snd were adiusted =car tingly in sainplL. mcOiv[rtg with Nn ItiL of cim1c vnc; JFi2SO 4l NR'03, NC4 tNaQH using 4R A; NA Tire vrprcaervaticn 14AA ]fmorc than one presomt[vo Es neuGed, pleases (lore in the MIU11 nLs below, Sample() NA were T=iv,d w ith 'xbb10s >G mist i_t dfumc;cr. Samplcs(s) NIL lhv m received with "1"RC > 0.5 rnWL (If 19 is APO Aad werc ai[.Lsted a"otding)y in sarripie rccaNing tvlL[t sodium thinsu.1Wc (Naas ) with Shc:rAy If), NA bnrcode Ial,Cls appli#r by- M02 Comments-. J)ace' ullL3+m Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 7 of 7 SECTION 3 N n � a a _U _ n m 5 o U U o O o w a ¢ a N ¢ m U F LLU pp, Q U) 0 w a to.0 Fyn w C9 4 a Q U U m N < m q1 'c o 0 xU ul O rn � N N W o Y 0 o 0 a E Ja N N 00 05 0 0 d o o 0 0 ~o n � Zc o 0 a © a o F E o O O O a d d " Z U Z Q na W o 0 Fi U) U c � M c z z C > Q Y � O a V 1 N L C6 o a o 0 fo z Q w � w w �d o (f) rn o u a Of Z O Z ❑ d U a z r a � ❑ Z � � U U d J 7 w w m m a z w 0 a v c5 to FCl) m o Z ❑ n '`a o 0 �D �D Z O E [~_7 0 c cK D ~ O b 4 7_ fn U n a n CK of U U) K O F C O O O r m J ❑ z w 0. w O ❑ to ❑ 2 u, v> w 0 0 cx 0 0 •t N O M- 1 7 m p N � CD rY =o 0 O � � N Cn N COU CD O J O d U o a a U .. o U > � ?' � � J dO ci in c d aa) 2 U w C a SECTION 4 SUMM111 ENVIRONMENTAL TECHN❑LOMZ3. INC Arraly0ca1 Laboralorfas February 03, 2022 Alex Fox Synagro 284 Boger Rd. Mocksville, NC 27028 TEL: FAX: RE: Beaufort WWTP Dear Alex Fox: Summit Environmental Technologies, Inc. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX.- (330) 253-4489 Wehsite: http://www.settek.com Order No.: 22010932 Summit Environmental Technologies, Inc. received 1 sample(s) on 1/14/2022 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, Jennifer Woolf Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 Arkansas 88-0735, California 2943, Colorado, Connecticut PH-0108, Florida NELAC E87688, Idaho OH00923, Illinois 200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988, Minnesota 1780279, Nevada OH009232020-1, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP CL0052, Oklahoma 2019-155, Oregon OH2O0001, Pennsylvania 011, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-19-16, Utah OH009232020-12, Virginia VELAP 10381, West Virginia 9957C Page 1 of 38 MM' Y Summit Environmental Technologies, Inc. Case Narrative SU3310 Win St. ENVIRONMENTAL TEC„HQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 wo#: 22010932 Arralyi9cal Laboralorlas TEL: (330) 253-8211 FAX.- (330) 253-4489 Wehsite: http://www.settek.com Date: 2/3/2022 CLIENT: Synagro Project: Beaufort WWTP WorkOrder Narrative: 22010932: This report in its entirety consists of the following documents: Cover Letter, Case Narrative, Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody, Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit Environmental Technologies, Inc., Work Order Number assigned to this report. Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program Analytes Report" for accredited analytes list. The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein. All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as "dry weight" using the "-dry" designation on the reporting units. This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any comments or problems with the analytical events associated with this report are noted below. Analytical Sequence Sample Notes: 22010932-OOIA TCLP-VOC-MSTR_8260D: Possible low bias for Tetrachloroethane due to low recovery in CCV. Adequate sensitivity demonstrated in Reporting Limit Check. 22010932-OOIA TCLP-SVOC_8270E: CCV exhibited high recovery for 2,4-Dinitrotoluene. Sample is ND for this analyte. 22010932-001a TCLP-SVOC-CPEST(808 I B): The Calibration Verification did not meet laboratory established acceptance criteria for Endrin, however associated LCS/MS/MSD all recovered within QC range. Analytical Sequence QC Notes: CCV VOC-MSTR NPW(8260): Possible low bias for Tetrachloroethane due to low recovery in CCV. Original Page 2 of 38 mm' y Summit Environmental Technologies, Inc. Case Narrative su3310 Win St. ENVIRONMENTAL TEC„HQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 wo#: 22010932 Arralyi9cal Laboralorlas TEL: (330) 253-8211 FAX.- (330) 253-4489 Wehsite: http://www.settek.com Date: 2/3/2022 CLIENT: Synagro Project: Beaufort WWTP Adequate sensitivity demonstrated in Reporting Limit Check LCS VOC-MSTR_NPW(8260): Possible low bias for Tetrachloroethane due to low recovery in CCV. Adequate sensitivity demonstrated in Reporting Limit Check. MB TCLP-VOC-MSTR TCLP(8260): Possible low bias for Tetrachloroethane due to low recovery in CCV. Adequate sensitivity demonstrated in Reporting Limit Check. CCV 40ppm SVOC-MSTR_S(8270): CCV exhibited high recoveries for several analytes. Associated samples are ND for these analytes. Surrogate outside recovery limits. Minimum method criterion of one surrogate within established recovery limits was met. 22010932-OOlAMS/1\4SD TCLP-SVOC-CPEST(8081B): P: RPD between confirmation column is greater than 40%. The Calibration Verification did not meet laboratory established acceptance criteria for Endrin, however associated LCS/MS/MSD all recovered within QC range. LCS-54572 TCLP-SVOC-CPEST(8081B): P: RPD between confirmation column is greater than 40%. Original Page 3 of 38 MM' Summit Environmental Technologies, In Qualifiers and Acronyms SU3310 Win S EkiwllOMM@NTALTECHN❑LOG{r,23.INC Cuyahoga Falls, Ohio442� WO#: 22010932 Arraly0cal Laboralorlas TEL: (330) 253-8211 FAX.- (330) 253-44E Wehsite: httn:11www.settek.co Date: 2/3/2022 These commonly used Qualifiers and Acronyms may or may not be present in this report. Qualifiers U The compound was analyzed for but was not detected. J The reported value is greater than the Method Detection Limit but less than the Reporting Limit. H The hold time for sample preparation and/or analysis was exceeded. D The result is reported from a dilution. E The result exceeded the linear range of the calibration or is estimated due to interference. MC The result is below the Minimum Compound Limit. The result exceeds the Regulatory Limit or Maximum Contamination Limit. in Manual integration was used to determine the area response. d Manual integration in which peak was deleted N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response. P The second column confirmation exceeded 25% difference. C The result has been confirmed by GC/MS. X The result was not confirmed when GUMS Analysis was performed. B/MB+ The analyte was detected in the associated blank. G The ICB or CCB contained reportable amounts of analyte. QC-/+ The CCV recovery failed low (-) or high (+). R/QDR The RPD was outside of accepted recovery limits. QL-/+ The LCS or LCSD recovery failed low (-) or high (+). QLR The LCS/LCSD RPD was outside of accepted recovery limits. QM-/+ The MS or MSD recovery failed low (-) or high (+). QMR The MS/MSD RPD was outside of accepted recovery limits. QV-/+ The ICV recovery failed low (-) or high (+). S The spike result was outside of accepted recovery limits. Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for additional information Acronyms ND Not Detected RL Reporting Limit QC Quality Control MDL Method Detection Limit MB Method Blank LOD Level of Detection LCS Laboratory Control Sample LOQ Level of Quantitation LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit QCS Quality Control Sample CRQL Contract Required Quantitation Limit DUP Duplicate PL Permit Limit MS Matrix Spike RegLvl Regulatory Limit MSD Matrix Spike Duplicate MCL Maximum Contamination Limit RPD Relative Percent Different MinCL Minimum Compound Limit ICV Initial Calibration Verification RA Reanalysis ICB Initial Calibration Blank RE Reextraction CCV Continuing Calibration Verification TIC Tentatively Identified Compound CCB Continuing Calibration Blank RT Retention Time PLC Reporting Limit Check CF Calibration Factor DF Dilution Factor RF Response Factor This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting. Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this list or for additional information regarding the use of these Qualifiers on reported data. Original Page 4 of 38 �� 1 � Summit Environmental Technologies, Inc. SU3310 Win St. ENVIROMMEWAL YECHNO ijULES. JNG, Cuyahoga Falls, Ohio 44223 Arraly0cal Laboralorlas TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: http://www.settek.com CLIENT: Synagro Project: Beaufort WWTP Lab SamplelD Client Sample ID 22010932-001 Beaufort WWTP Tag No Date Collected 1/13/2022 10:30:00 AM Workorder Sample Summary WO#: 22010932 03-Feb-22 Date Received Matrix 1/14/2022 10:25:00 AM Sludge Page 5 of 38 A Q+ z E* V 4 N N C Vl NO NO V V N O N N N N N N N 0 0 0 0 0 0 0 0 N O ul ul ul ul M 00 O O O O N N N N N N N N O O O O O O O O N N N N N N N N N N N N N N N N a a a a a a a O O O O O O O O O O O O O O O O O O O O O O O O O O O O N N N N N N N N N N N N N N O O O O O O O M M M M M M M N N N N N N N 0-i N N M ,M t O u U V] U .0 .0 W W W W W W W W co co 0 Q0 m m ca a_ SUMMIT Summit Environmental Technologies, Inc. 3310 Win St. ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223 Arralyt9cal Laboralorfas TEL: (330) 253-8211 FAX. (330) 253-4489 Website: http://�i,-"-m,.settek.coin Analytical Report (base report) WO#: 22010932 Date Reported: 2/3/2022 CLIENT: Synagro Tag Number: Matrix: SLUDGE Collection Date: 1/13/2022 10:30:00 AM Lab ID: 22010932-OOIA Project: Beaufort WWTP Client Sample ID Beaufort WWTP Analyses Result RL Qual Units DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW7470A SW7470A Analyst: KLC TCLP MERCURY ANALYSIS (SW1311/7470) TCLP Mercury ND 0.0100 mg/L 1 1/26/2022 3:57:00 PM METALS BY ICP/MS (EPA 6020B) SW6020 SW301 OA Analyst: DNS TCLP Arsenic ND 0.100 mg/L 40 1/26/2022 1:54:29 AM TCLP Cadmium ND 0.100 mg/L 40 1/26/2022 1:54:29 AM TCLP Chromium ND 0.100 mg/L 40 1/26/2022 1:54:29 AM TCLP Lead ND 0.100 mg/L 40 1/26/2022 1:54:29 AM TCLP Selenium ND 0.500 mg/L 40 1/26/2022 1:54:29 AM TCLP Silver ND 0.100 mg/L 40 1/26/2022 1:54:29 AM TCLP METALS, VOC, BNA, PEST, HERB -SOLID TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270) 1,4-Dichlorobenzene ND 2,4,5-Trichlorophenol ND 2,4,6-Trichlorophenol ND 2,4-Dinitrotoluene ND Cresols, Total ND Hexachloro-1,3-butadiene ND Hexachlorobenzene ND Hexachloroethane ND Nitrobenzene ND Pentachlorophenol ND Pyridine ND Surr: 2-Fluorophenol 103 Surr: Phenol-d6 102 Surr: Nitrobenzene-d5 82.6 Surr: 2,4,6-Tribromophenol 126 Surr: 2-Fluorobiphenyl 77.6 Surr: p-Terphenyl-d14 98.2 SW8270 SW351OC Analyst: SFG 0.200 mg/L 2 1/25/2022 8:27:00 PM 0.500 mg/L 2 1/25/2022 8:27:00 PM 0.500 mg/L 2 1/25/2022 8:27:00 PM 0.100 QC+ mg/L 2 1/25/2022 8:27:00 PM 10.0 mg/L 2 1/25/2022 8:27:00 PM 0.0400 mg/L 2 1/25/2022 8:27:00 PM 0.100 mg/L 2 1/25/2022 8:27:00 PM 0.200 mg/L 2 1/25/2022 8:27:00 PM 0.200 mg/L 2 1/25/2022 8:27:00 PM 0.500 mg/L 2 1/25/2022 8:27:00 PM 0.500 mg/L 2 1/25/2022 8:27:00 PM 10 - 157 %Rec 2 1/25/2022 8:27:00 PM 10 - 169 %Rec 2 1/25/2022 8:27:00 PM 32.1 - 130 %Rec 2 1/25/2022 8:27:00 PM 45.4 - 166 %Rec 2 1/25/2022 8:27:00 PM 35.7 - 130 %Rec 2 1/25/2022 8:27:00 PM 70 - 145 %Rec 2 1/25/2022 8:27:00 PM Qualifiers: B Analyte detected in the associated Method Blank H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. ND Not Detected P Second column confirmation exceeds R RPD outside accepted recovery limits E Value above quantitation range M Manual Integration used to determine area response N Tentatively identified compounds OG 1 PL Permit Limit Original RL Reporting Detection Limit Page 7 of 38 SUMMIT Summit Environmental Technologies, Inc. 3310 Win St. ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223 Arrafyt9caf Laboralorfas TEL: (330) 253-8211 FAX. (330) 253-4489 Website: http://�i,-"-m,.settek.coin Analytical Report (base report) WO#: 22010932 Date Reported: 2/3/2022 CLIENT: Synagro Tag Number: Matrix: SLUDGE Collection Date: 1/13/2022 10:30:00 AM Lab ID: 22010932-OOIA Project: Beaufort WWTP Client Sample ID Beaufort WWTP Analyses Result RL Qual Units DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8081 SW351OC Analyst: CSS TCLP PESTICIDES ANALYSIS (SW1311/8081) Chlordane, total ND 0.0250 mg/L 10 2/3/2022 7:20:00 AM Toxaphene ND 0.0500 mg/L 10 2/3/2022 7:20:00 AM Endrin ND 0.00500 mg/L 10 2/3/2022 7:20:00 AM gamma-BHC ND 0.00500 mg/L 10 2/3/2022 7:20:00 AM Heptachlor ND 0.00500 mg/L 10 2/3/2022 7:20:00 AM Heptachlor epoxide ND 0.00500 mg/L 10 2/3/2022 7:20:00 AM Methoxychlor ND 0.00500 mg/L 10 2/3/2022 7:20:00 AM Surr: TCMX 68.9 10 - 119 %Rec 10 2/3/2022 7:20:00 AM Surr: DCB 90.0 10 - 119 %Rec 10 2/3/2022 7:20:00 AM TCLP HERBICIDES BY EPA 8321B SW8321 Analyst: RIS 2,4-D ND 0.500 mg/L 50 1/31/2022 5:38:00 AM 2,4,5-TP ND 0.500 mg/L 50 1/31/2022 5:38:00 AM Surr: 2,4-Dichlorophenylacetic aci 98.0 70 - 130 %Rec 50 1/31/2022 5:38:00 AM TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8260 SW1311M Analyst: NAW TCLP VOLATILES ANALYSIS 1,1-Dichloroethene ND 0.250 mg/L 50 1/25/2022 4:45:00 AM 1,2-Dichloroethane ND 0.250 mg/L 50 1/25/2022 4:45:00 AM MEK ND 5.00 mg/L 50 1/25/2022 4:45:00 AM Benzene ND 0.250 mg/L 50 1/25/2022 4:45:00 AM Carbon tetrachloride ND 0.250 mg/L 50 1/25/2022 4:45:00 AM Chlorobenzene ND 2.50 mg/L 50 1/25/2022 4:45:00 AM Chloroform ND 0.250 mg/L 50 1/25/2022 4:45:00 AM Tetrachloroethene ND 0.250 QC- mg/L 50 1/25/2022 4:45:00 AM Trichloroethene ND 0.250 mg/L 50 1/25/2022 4:45:00 AM Vinyl chloride ND 0.100 mg/L 50 1/25/2022 4:45:00 AM Surr: 4-Bromofluorobenzene 98.1 70 - 130 %Rec 50 1/25/2022 4:45:00 AM Surr: Di brom ofl uorom ethane 103 70 - 130 %Rec 50 1/25/2022 4:45:00 AM Surr: Toluene-d8 103 70 - 130 %Rec 50 1/25/2022 4:45:00 AM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response MC Value is below Minimum Compound Limit. N Tentatively identified compounds ND Not Detected OG1 P Second column confirmation exceeds PL Permit Limit Original R RPD outside accepted recovery limits RL Reporting Detection Limit Page 8 of 38 MMIT Summit Environmental Technologies, Inc. Analytical Report SU3310 Win St. ENVIRONMENTAL TECHNOLOGIE-3, IRC Cuyahoga Falls, Ohio 44223 (base report) Arralyt9cal Laboralorfas TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 22010932 Website: http://www.settek.com Date Reported: 2/3/2022 CLIENT: Synagro Tag Number: Matrix: SLUDGE Collection Date: 1/13/2022 10:30:00 AM Lab ID: 22010932-OOIA Project: Beaufort WWTP Client Sample ID Beaufort WWTP Analyses Result RL Qual Units DF Date Analyzed RCI SW9014 Analyst: MS REACTIVE CYANIDE (9014/7.3.3.2)-SOLID Cyanide, Reactive ND 0.485 mg/Kg 1 1/19/20224:24:00 PM IGNITABILITY OF SOLIDS (SW-846: 1030) SW1030 Analyst: ALT Ignitability nonflammable mm/sec 1 1/26/2022 10:46:02 AM RCI SW9045D Analyst: ALT PH (SW9045D) pH 6.6 s.u.@17.6C 1 1/20/2022 1:58:57 PM RCI SW9034 Analyst: MS REACTIVE SULFIDE (9034)/7.3.4.2 Sulfide, Reactive ND 25.0 mg/Kg 1 1/19/20224:24:00 PM Qualifiers: B Analyte detected in the associated Method Blank H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. ND Not Detected P Second column confirmation exceeds R RPD outside accepted recovery limits E Value above quantitation range M Manual Integration used to determine area response N Tentatively identified compounds OG 1 PL Permit Limit Original RL Reporting Detection Limit Page 9 of 38 Summit Environmental Technologies, Inc. Accreditation Program SUMMIEF fr3310 Win St. Analv n tes Report ENwIROMMEWALYECHNOL.OG{r,S,INC Cuyahoga Falls, Ohio44223 J Y Arraly0cal Laboralorlas TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 22010932 Website: http://www.settek.com 03-Feb-22 Client: Synagro State: NW Project: Beaufort WWTP Program Name: NC_WW_SCM Sample ID Matrix Test Name Analyte Status 22010932-OOIA Sludge Ignitability of Solids (SW-846: 1030) Ignitability A Sludge Metals by ICP/MS (EPA 602013) Arsenic N Sludge Metals by ICP/MS (EPA 602013) Cadmium N Sludge Metals by ICP/MS (EPA 602013) Chromium N Sludge Metals by ICP/MS (EPA 602013) Lead N Sludge Metals by ICP/MS (EPA 602013) Selenium N Sludge Metals by ICP/MS (EPA 602013) Silver N Sludge pH (SW9045D) Hydrogen Ion (pH) A Sludge Reactive Cyanide (9014/7.3.3.2)-Solid Cyanide, Reactive U Sludge Reactive Sulfide (9034)/7.3.4.2 Sulfide, Reactive U Sludge TCLP Herbicides by EPA 8321B 2,4,5-TP A Sludge TCLP Herbicides by EPA 8321B 2,4-D A Sludge TCLP Mercury Analysis (SW1311/7470) Mercury A Sludge TCLP Pesticides Analysis (SW1311/8081) Chlordane, total A Sludge TCLP Pesticides Analysis (SW1311/8081) Endrin A Sludge TCLP Pesticides Analysis (SW1311/8081) gamma-BHC A Sludge TCLP Pesticides Analysis (SW1311/8081) Heptachlor A Sludge TCLP Pesticides Analysis (SW1311/8081) Heptachlor epoxide A Sludge TCLP Pesticides Analysis (SW1311/8081) Methoxychlor A Sludge TCLP Pesticides Analysis (SW1311/8081) Toxaphene A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 1,4-Dichlorobenzene A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4,5-Trichlorophenol A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4,6-Trichlorophenol A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4-Dinitrotoluene A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Cresols, Total A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachlorobenzene A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachlorobutadiene A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachloroethane A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Nitrobenzene A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Pentachlorophenol A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Pyridine A Sludge TCLP Volatiles Analysis 1,1-Dichloroethene A Original #1 Page 10 of 38 Summit Environmental Technologies, Inc. Accreditation Program SUMMIEF fr3310 Win St. Analv n tes Report ENVIROMMEWAL YECHHOL.OG{r,S, INC Cuyahoga Falls, Ohio 44223 J Y Arraly0cal Laboralorlas TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 22010932 Website: http://www.settek.com 03-Feb-22 Client: Synagro State: NW Project: Beaufort WWTP Program Name: NC_WW_SCM Sample ID Matrix Test Name Analyte Status 22010932-OOIA Sludge TCLP Volatiles Analysis 1,2-Dichloroethane A Sludge TCLP Volatiles Analysis 2-Butanone A Sludge TCLP Volatiles Analysis Benzene A Sludge TCLP Volatiles Analysis Carbon tetrachloride A Sludge TCLP Volatiles Analysis Chlorobenzene A Sludge TCLP Volatiles Analysis Chloroform A Sludge TCLP Volatiles Analysis Tetrachloroethene A Sludge TCLP Volatiles Analysis Trichloroethene A Sludge TCLP Volatiles Analysis Vinyl chloride A Original #1 Page 11 of 38 0 Fi U F� 0 E T r) a_ CD ry M L- M is M d rK z z 0- � � 75 N N CD N N M Ln E N N J � � L N N = Q U) E Q) 'N J d T � J Q U W 0 J E to r > M w O � � � Y IL U) 7 a co > Y H CO IL �o Z_ 0 IL 0 LO ao m � a N � N E _o co cn U Q O O O M M M O O O r- r- r- V CO N C o 0 m Cl Cl Cl U') U') U') 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 L6 Lfj 6 Lo Lo Lo Lo Lo N 0 0 0 0 0 0 0 0 0 0 o 0 0 Z Z Z Z Z Z Z Z Z Z C, C, C, v Ln Lon C C C 0 0 N O p 00 a o o 0 Z Z :Ea) E E c N N O O N N 0 0 U Oi OO N E o OP0 0 a)m o O o o v U U N 00 O O U O U i i i Q Q Y C O O E to (n (n N W aN m t :Ec 2 m 0 0 0 H H O 00 co O N Q) ca d � O c G N m C1 J Q1 � a rn n rn n M d zo zo c � in co n N N N N M In E N N J � � L _D O N = cl cl Q N E .N 3 a '• c J Q U u1 tm E N � > Uj Cl) � N Y a U O O o o co a 00 m U ? 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C.)Q C i i i i i i m � � � � � V V V V U N N N g N >. 07 07 07 07 07 07 r t\i t\i t\i 6 U 2 2 2 Z a a 00 co O ti m A U :C 75 a E J a- a U.)o rn to CO') d zo zo c � Tf in 75 N N a a N N E N N J � � L _D O N = cl cl a U) E E .N 3 a '• c J Q U w J C1 O � ri LO > M � N Y i a U CO N n a co � m U ? Y H N a- � z 0 U � J U H a � a N O Q) LO N a a .U. E m m Co U Q N O O LO U 00 O m R N m N N E o m c n C) a + + + + as as 0 V N O m m N N co U7 V O O O co m n N C2 LC2 - LC2 � m m m m � C2 U2 C2 Cfl N co co N m O O M N V O I'- � Ci CJ V C% Lx� O I-� U7 (6r-�— V C� N � O m I-- -,I- CO N N N U) — M N N N U7 I- co V M O V— N CP7 I- CP7 O O O CP7 CP7 N V C 6 CC) 6 c0 C 6 6 c0 O I-: c0 CC) 6 6 O2 O O2 r-� 00 I- O O O O O O O O O O O O 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 o co 0 0 0 0 0 0 0 0 0 0 0 0 O O O O O O O O O O O 0 0 0 0 0 0 0 0 0 0 0 0 O O Cf7 Cf7 O V A C%7 O O V V � 0 0 Cf7 Cf7 N V Cf7 O (A I� O Z O N V CA � � � (q CO l!7 CO CO (%7R (%7 I� � O O O O O O O O O O O O O O C= N N -O Q C NC NE N O 0 0 C o N L L C C 0 'O N:N C 0- 0- N CJ N N O N� Q O O O L O Q O O O-� O O O OL LL -0�_ V LL H i o O O O N O N d Z N N C1 U H I7 � to :E U U ) N C i i i i i i Cf7 co0 to N N (6 O 'O V V V V U O N N N T (n (n (n (n (n (n N N N O U 2 2 2 2 d d co M 4- 0 co m 0 0- A U :C O c G N Flo CJ J N a rn o rn n M d Z Z o C 0- in N N a a N N E N N J � � L _D O N = cl cl a U) E E .N 3 a '• C J Q U LU J C1 O � N LO > M � N Y i a U CO N n a co � m U ? Y H N a- � Z 0 U � J U H a � a 0 N (n O N LO N a a .U. E m m Co 0 Q N O O LO U O m R N m O O E o co Con a CJ CJ CJ CJ � O O O O O O O O O O O O m m m m m m m m m m m m CO CO � CO V O O CO N V N 0 0 0 0 0 0 0 N N rn v �Nf) O V O CEO co m m O 0 0 0 0 0 0 0 0 0 0 V N O N N CO N uO CO O CO m m n N u2 u7 v m m� v m7 V c2 c2 c2 v c2 2 22 N CO CO N m CO O m N V O I'- � O) m v Cv Lx� O I-� U7 (6� — V A N � O m I-- -,I- CO N N N U) — M N N N u7 V N N u7 I- V V I- m I- m M V N O V CO O O O O O O O O O O O O 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 o co 0 0 0 0 0 0 0 0 0 0 0 0 m------ O O O O O O O O O O O 0 0 0 0 0 0 0 0 0 0 0 0 O V V m Z O m N CO Z �f7 m N O1 CR CR � C CR CR O1 - O- O O O O O O O O O O O O O O O C N N O Q C NC N O N O 0 0 C o N L L C N C C 0 'O C r N C O- O- N 'o C co O C O QO O L OOQ O ff N -- O O -C "I- LL H i ON ON d Z N N Q U UUUCi i i i i iO � 0 co m co V V V V U 2 O O O N �, UJ UJ UJ UJ UJ UJ N N N O U 2 2 2 Z d d co M 4- 0 rn m C6 0- O c it N m a J to M � a ONO n 0L to rn n M d zo zo c IY Cl) 75 N N N N E N N J � � L _D N (6 cl cl Q N E .N 3 a '• c J Q U W J C1 M � N Y a I CO CO m O Ua co Y co a- � z 0 U U)al J H CJ m LO O) L O) a a .U. E m m Co U N N LO LO m m � a 0 o o fl >, E o m Co n a 0 0 0 O O O O O O cl cl cl z z z m a J to a ONO n 0L rn to CO') d zo zo c � IY in 75 N N N N E N N J � � L _2) co (6 0 cl a U) E 2 .N 3 a '• c J Q U W J C1 E O M Cl) Y a I U O Q) Uto > Y CO a- 0 z 0 U Q J Q al H CJ U v o J to O) a a .U. E m m Co CO N N LO U J J 0 o � o E o m i/) E)Q O O O CO N I-� O O O O � � � O O O 000 O O O O o 6 m v 0 0 0 O O O co M 4- 0 0 N ca O c it N m a J O a- a N CO 0L rn n M d zo zo c 0- Iin 75 n N N N N E N N J � � L _D U N = cl cl a U E E .N 3 a '• c J Q U u1 J C1 M � N Y a I CO CO m O U a m Y co a- Z 0 U U)al J H CJ m LO N L N a a .U. E m m Co U N N LO LO m m � a 0 o o fl >, E o m i/ U Q 0 0 0 0 0 0 0 0 0 0 0 0 v v v v v v O O O O O O O O O O O O 0 0 0 0 0 0 z z z z z z m a J n a- a N to 0L rn n M d zo zo c � IY in 75 n N N N N a �5 E N N J � � L _D U U = C6 C6 _ cl cl a U) E N E .3 a '• c J Q U u1 J C1 E O M E Cl) Y a I U O Q) U a co Y co a- Z 0 U Q J Q al H CJ U v o J L U a a .0 E m m Co U N N LO U J J 0 o � o E o m i/ U Q m m v Un v m o v C6 cl- r-� cli rn rn o rn rn rn 0 0 0 0 0 0 0 0 0 0 0 0 N N N N N N 0 0 0 0 0 0 0 0 0 0 0 0 v v v v v v O O O O O O O O O O O O E E E N o .� j Q U U -j co cn a a a a a a J J J J J J U U U U U U co M 4- 0 N ca 0- O c S N m a J N a N — 0L 00 rn n M d zo zo c in 75 n N N N N a co E N N J � � L _D U N = cl cl a U E E .N 3 a '• c J Q LU U J U O i M � N Y a I U N M O a m Y co a- Z 0 U � J al H CJ NLO U L N a a .U. E m m Co U Q O O U o 0 R N m o o E o m i/ U Q �f7 �f7 �f7 �f7 �f7 �f7 �f7 �f7 �f7 �f7 �f7 �f7 N U') Co O I- Co O m m m m O 0 0 0 0 0 0 0 0 0 0 0 0 O O O O N O O O O O O O N N E EE U 7 O .� > Q U U -j cin cn a a a a a a J J J J J J U U U U U U m a J M a- N CL rn n M d zo zo c IY in n N N N N a co E N N J C _D U U = C6 C6 cl cl a U) E E .N 3 a '• c J Q LU U J C1 E O U O i M Cl) Y a I U O Q) U a co Y N CO Z 0 U Q J Q al H CJ 0 LO U LO U a a .0 E m m Co U 0 Q O O U o 0 R N m 6 o o fl >, E o m i/ U Q 0 0 0 0 0 0 N N N N N N v CC! C m o m m � co� m rn rn . � � �f7 �f7 �f7 �f7 �f7 �f7 �f7 �f7 �f7 �f7 �f7 �f7 m O Co O N V N V 'j O O2 O m m O m O 0 0 0 0 0 0 0 0 0 0 0 0 O O O O N O O O O O O O N N o) N O I� ,- — — N E EE U 7 co O .� > Q U U -j i/) c/5 a a a a a a J J J J J J U U U U U U co M 4- 0 N N ca O c G N m a J O a- a Lc) n rn 00 M d Z Z o c in 75 O N N O N E N M J N L _D O N = cl cl Q N E .N 3 a '• c J Q LU U J C1 O � N L > M � N Y a U U N00 a a co m U ? Y H N a- Z 0 U � J U H a � a (n l N L N a a .V. E m m Co U W R O O M 0) w O O O N M b o o fl >, E o m Cn C) a a E Om N � O O �f7 L�2 �2 N N N O O O O O O O O O V Uf7 m m O N N O O O O O O O O O O O o 0 0 0 0 g 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 N �f7 �f7 �f7 �f7 �f7 O O O O O O 0 O O O O O O O O O O Z � m M coo co co Cd D O 0 0 0 O O O N X U o o m m -o c m m o O L C E N N 47 U W o1 2 2 m a J n a- Lc) n rn 00 to cn d Z Z o c [if in a O N N O N N M J N L _D O N = co (6 _ 0 cl Q N E .N 3 a '• c J Q LU ly- U J C1 O � N L > M Cl) Y a U U C9 co � a Fu co m Y H N a- -0 Z 0 U Q) J Q al H CJ 0 � U) le a a .V. E m m Co Cl) W R O O CN') O 7 O N M o o fl- � T E o m Co n C) a a � 0 0 0 0 0 0 m m m m m m O O o m rn CC) CC)rn 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Om N � O o0 �f7 N N N O O O O O O O O Cfl V (fl O— N O O cj O N O co co O VCC) 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 N �f7 �f7 �f7 �f7 �f7 O O O O O O 0 O O O O O O O O O O Q,zT CO N N O O O O O O O O O O O O O O O O 0 O O O O N Flo X U N O m _ U U m -o c m m o O 0 L C E N C/) C/) U W o) 2 2 co M 4- 0 cr) N ca O c it N m a J a- a LO 00 0� rn 00 M d zo zo c in n co O N N O N E N M J N L _D O N = cl cl Q N E .N 3 a '• c J Q LU U J C1 O � N L > M � N Y a U U N c a a co m —i coU ? Y H N a- Z O U J H CJ � a U v o J L N a a .V E m m Co U N n LO Cl) CO J J o o fl- � T E o m Co n a a a O O O O O m O O �2 �2 �2 �2 �2 �: �2 �2 O O O O O O O O co m Un Un m m m m 0 6 O O O O O O O O 0 0 0 0 0 0 0 CON 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 N �f7 �f7 �f7 �f7 �f7 O O O O O O O O O O O O O O O O O O O O O O O 0 O 0 0 0 0 0 m 0 0 C6 0 O O O O 0 O O O O 0 X U o o m m -o c m m o O n L C E N N 47 U W o1 2 2 m a J a- LO 00 � rn 00 CO') d zo zo c � [If in n 75 O N N O N E N CM J N L _D O N = co ( 0 cl Q N E .N 3 a '• c J Q LU ly- U J C1 O � N L > M Cl) Y a U U C9 co � a co m Y H N a- -0 Z 0 U Q) J U H a Q) a m LO Q) L O a a .V. E m m Co CO N n LO LO m m a o o fl- � T E o m Co n a m m Un m ccoo 0 0 0 0 0 0 0 N �f7 �f7 �f7 �f7 �f7 �f7 O O O O O O O O O O O O O O O O O O O O O O O O O O z z z z z z z m r 0 X U o o m Qco m U H E m m 0 L x0 C N N N 47 CO CO U H W 0) 2 2 co M 4- 0 N ca E / § \ _ u a § § CO ) § E 7 ƒ 3 O k § f 00 q 2 m q _ � _ � O c G N m a J m M � a rn rn n M d zo zo c in 75 n N N N N 45 45 E N N J C _D U N = cl cl Q N E .N 3 a '• c J Q U u1 a a a O 5 _ v > � N Y a a J O � H� n co 2 CO a- Z 0 U (D J U H a (D a Y L OJO LO L N a a .U. E m m Co U LO n LO LO 00 Cl) � a U U fl >, E o m i/ U Q O O N O O ii U U 2 a m a Im J a- a rn Cl) m n M d zo zo c � [If in 75 n N N N N E N N J � � L _D U N = cl cl Q N .N 3a '• c J Q U u1 a a a O 5 _ v > Cl) Y a a J O � H� n m 2 CO a- -0 Z 0 U (D J H CJ � a LO U v o J L U a a .U. E m m Co Cl) LO n LO J J 47 N 0- >, E o m i/ U Q O O O v 0 O m a J Q1 a- m rn rn n � M d zo zo c 0- � in 75 n N N N N 45 4) E N N J C _D U N = cl cl Q N 2.N 3a c J Q U u1 a a a O 5 _ v > n Cl) Y a a J O � H� I, m 2 CO a- Z 0 U Q) J Q CJ � a LO y � Q) L U a a .U. E m m Co U Q Cl) O O °D U o 0 R N m 6 47 N fl >, E o m il) C)Q N 6 rn O m a J Im LO a- O � rn rn rn n M d zo zo c � in co N N N N E N N J � � L _D U N = (6 (6 _ cl cl a U) E E .N 3 a c J Q U u1 a a a O 5 v > y_ n � N Y a a J O H� n m (� Y 2 m � -0 Z 0 U � J H CJ � a LO L N N a LO a .U. E m m Co U 0 CO Q M O O °D U o 0 R N m 6 U U 0- >, E o m i/) C)Q O N m m 0 O 26 U U 2 a J U P 00 M 0 � N own � O c6 0- Fi U F� 0 E J O d M 00 M is M d ry z z tT � � > 75 N N CD N N t0 t0 E N N J � � L N N = Q U) E E 'N J d T � J Q U LU 0 LO (n to N N a Q U E ca (6 CO 0 co ¢ M 0 00 U CY N N CO Q � E _o co cn U Q 00 co O ti N Q) ca d m a J M a- a N CO a' W LO M d o zo z C 75 cl a N N _ O N M J � L O N = cl cl Q N E.N 3a c J Q U u1 a e N N > C � � Y a �I Cl) co 2 fA o U 00 co O y a 70 Z 0 U N J U H a � a CM N co in Cl) N J � N a a .V. E m m Co O c ct r- O o � o rn O O O Uf7 N O Ci � O Nco L C N O p O p 00 0 0 0 E E c 0 0 O C/) C/) C/) m a J a- N CO a' W LO Cam') d zo zo C � [if C/) 75 N N _ O N E M J � L _D co C6 _ 0 cl a U) E 2 .N 3 a '• c J Q U u1 a e co N > C ) � Y a �I Cl) H fA O Q) U 00 > O> y a Z 0 U N J H CJ m N J M N Q a a .V. E m m Co CO O co rn r-� 6 6 rn rn rn U') o rn 7 7 7 C/) C/) C/) co M 0 co � N own � O c6 0- m a J LO a a a am i M d zo zo c 0- in n N O _ N Q1 E � J � L _D � N = cl cl a U E E .N 3 a c J Q U u1 Y C1 E 75 N > C D � Y a N Cl) �a co � 7 cU CO a- 70 zo 0 U (D J U H a (D a 01 O Y J Cl)N N a a .V. E m m Co U O c G N O rn V 0 cl z 0 a m (D �+ Q) N L" Qj C C co Co C m a J O a- a 0 0 am n M d zo zo c � [if in n N O _ N rn E J � L _D N N = cl cl a U E .N 3a '• c J Q U u1 tm Y tm E 75 CD N > C D � Y a N Cl) CD �Q co � 7 cU CO a- 70 zo 0 U CD J C H CJ 0) O co 01 N M_ N Of a a .V. E m m 00 U Q O O U o 0 s o � R N m 4) c N E o co i/ U Q v rn O O O rn O 0 O C6 m a J 01 a- 0 0 a- rn n M d zo zo c 0- � in n N O _ N rn E J � L _D � N = cl cl a U E 2 .N 3 a c J Q U u1 tm Y C1 E 75 N > C ) � Y a N CO a) > cU cA a- zo 0 U Q) J Q CJ a) O M_ Q) a a .V. E m m Co U 0 CO Q O O U o 0 s o 0 R N CO E o m i/) U Q 0 m rn rn Cf7 N �f7 Cri rn O O O rn co O N C6 m a J n a- 0 0 a- rn n M d zo zo c 0- in n N O _ N rn E � J � L _D N N = (6 (6 _ cl cl a U) E E .N 3 a c J Q U u1 Y C1 N N > C D � Y a N C/) � � 7 00) co U N Y a zo 0 U � J H CJ 01 O .. in a) N J � N a a .V. E m m Co U 00 O O O O rn V 0 co 6 CO Cl) CO co J J co 0� of Q) Q Q m E Q) c co >, Co Q) co co >1 U cn U Q U co M 0 m � N own � O c6 0- O c it N F a J n a- a a a am i M d o zo z c � in n Flo O _ N Q1 E � J � L _D � N = cl cl a U E E .N 3 a c J Q U u1 Y C1 E 75 N > C D � Y a N Cl) �a co � 7 cU CO a- Z 0 U (D J U H a (D a CO CO CO J J Q Q) 0- >, E o m i/) U Q F a Im 00 J o � a a a rn n M d o zo z c � [if in n N O _ N rn E � J � L _D N N = cl cl a U E E .N 3 a c J Q U u1 Y C1 E 75 N > C D � Y a N Cl) �a co � 7 cU CO a- Z 0 U (D J H CJ x U t � J 10 � m Q Q) E o m i/) U Q 00 N O O cl z 00 M 0 0 cr) � m O ca 0- O c i ct a J a rn n M d o zo z C 0- Tf C/) 75 a _ N G1 E � J � L _D N = cl cl a U E E .N 3 a > c J Q U w J C1 E 75 N > C D � Y a R N 7 a O (6 w 01 > y y a U Z 0 U (D J U H a (D a Cl) O Ut N cl z Q) U co Q) LD F a J LO r-) Im a rn n M d zo zo C � [If C/) 75 N rn E � J � L _D N N = cl cl a U) E E .N 3 a > c J Q U w J tm E 75 N > C D � Y a R -e N 7 a O (6 w 01 > y y a U Z 0 U (D J H CJ M in Cl) N J � a a .V. E m m Co CO M 00 O O Ut rn O O O N O Ut N N U m ry 6 LD U O c G N m a J a o a N rn i M d 0 z0 z C 0- n N O _ N Q1 E J L _D � N = cl cl a 0 E E .N 3 a >• c J Q U u1 at Y a) E 75 N > C D � Y a R Cl) N cn 7 'a O (6 rn > y y a U Z 0 U � J H CJ a 01 N Cl) Q) N a a .V. E m m Co U Q O O U o 0 M o U R N m Q Q) fl >, E 0 m Co n a v 0 rn O O N I- N m a J n � N rn n � M d z0 z0 C � [if C/) N O _ N rn E � J � L N N = cl cl a 0 E E .N 3 a > c J Q U u1 at Y a) N N > C D � Y a t5 Cl) � � N 7 a O (6 0)> Cl) y a U -0 Z 0 U � J U H a � a 0 Cl) N a a .V. E m m Co CO 0 Q O O U o 0 M o 0 R N m L 47 N 0- T E 0 co i/ U Q O co O O N I- N O N O O 00 M 0 N own � O c6 0- 0 E J CD d C,4 !L M is M IL z z Ir In F� m IN m O O O 2 a 00 co 0 co co m a_ O Ct S N a J Q1 a- N In 0' am i M d o zo z C CJ N O _ N O E N J � L cl cl a U E E .N 3 a c J Q U w U v �n V 7 N N to > C D � Y a LO O(U Q co Qj � 7 N Im > I Y C. CO a- � z 0 U U) J N .. d f) N 0 (U a a .V. E m m Co U a D O O M 0) w O O O N CO b N Ll N 0- >, E o m i/) U Q 0 CO O co co O O CO co F a J a N In a m i � M d zo zo C � [If C/) N O _ N O E N J � L (U (U = cl cl a U E E .N 3 a '• c J Q U w U N CW V 7 vi 75 N > C D � Y a LO Oj (U Q-e 7 I Y C. C0 a- � z 0 U J N .. d Cl) N 0 � � a a .V. E m m 00 a D Q O O 00 Ci O 0 � t o � R N CO L N (U 0- C T E o m i� U Q co m O O Co C6 a J N a N LO a m [-- to d zo zo C CJ 0� CO N O _ N O E N J C _D (U (U = cl cl a U E 2 .N 3 a c J Q U w U Q1 V 7 y N N > C ) � Y a LO a0 7 I Y C. N a- � z 0 U Q J Q CJ N .. in M J a a .V. E m m Co U le N_ G1 Cl) 13; N U CO J J N N 0- >, E o co i/) U Q O O 00 M 0 It � m ca o 0- F� 0 E J O d f� m r' M f� M is M d ry z z c � of C/) ry ry 0 N O _ N t0 E N J � L N N = Q N Q) 'N J d T � J a U LU V N N E E C Y IL U) O � w r > � 3 Y y a � Z 0 U J IL M V) Q1 M co U U J J E m m Co — C cn U a O co O r- LO N O O V N tb O oi T 21 00 co O LO co m O c i ct a J a- a 0 0000 0� m 00 M d o zo z c in 75 O _ N O E M J � L O ib _ N N _ cl cl a U E .N 3 a > c J Q U u1 J C1 E 75 N > C ) � Y a U C/) CO N d CM (6 00 > U �: Y H N a- Z 0 U N J H CJ � a m Cl) � a 0 o o E o m Co n a 0 co rn O O O s p p 0 Z z rn O U co U v a `" 1:1 6 V 5 V N N 75 a J N a 0 0000 0� m 00 CO') d zo zo c � [if in 75 o _ N O E M J � L O) co N _ cl cl a U) E 2 .N 3 a >• c J Q U u1 J C1 E 75 N > C � Y a U C/) Ct? N d M co 00 > U �: Y H N a- Z 0 U N J U H a � a CO CO CO J J 0 0 0 0 0- >, E o m i/ U Q co M 0 co m o ca 0- W s O � z I CC u .wCi�s u o It ll I !c RnWqmo jo ]igumN _. a c 9AnWU3nM LM"4l Wbrl- l *:XTU K �y 4 [Fi a at 9') % d m IS N is #p m oo } -1 14 15 N U V U IQ Ci U �7i 0 a� 0) m a - Page 37 of 38 Summit Environmental Technologies, Inc. SUMMIT 3310 Win St. ENVIRONMENTAL TECHN❑L4Ga1�S.IfiC Cuyahoga Falls, Ohio44223 Sample Log -In Check List Arrafocaf Laboralorias TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: http://`h,,",m,.settek.coin Client Name: SYN-NC-27028 Work Order Number: 22010932 RcptNo: 1 Logged by: Tegan A. Richards Completed By: Jacqueline Rasile Reviewed By: Jennifer Woolf 1/14/2022 10:25:00 AM 1/15/2022 6:18:42 PM 1/18/2022 11:29:27 AM Chain of Custody 1. Is Chain of Custody complete? Yes ❑d No ❑ Not Present ❑ 2. How was the sample delivered? UPS Lop In 3. Coolers are present? Yes ❑d No ❑ NA ❑ 4. Shipping container/cooler in good condition? Yes d❑ No ❑ Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present V No. Seal Date: Signed By: 5. Was an attempt made to cool the samples? Yes ❑d No ❑ NA ❑ 6. Were all samples received at a temperature of >0° C to 6.0°C Yes ❑d No ❑ NA ❑ 7. Sample(s) in proper container(s)? Yes ❑d No ❑ 8. Sufficient sample volume for indicated test(s)? Yes ❑d No ❑ 9. Are samples (except VOA and ONG) properly preserved? Yes ❑d No ❑ 10. Was preservative added to bottles? Yes ❑ No ❑d NA ❑ 11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm? Yes ❑ No ❑ No VOA Vials ❑� 12. Were any sample containers received broken? Yes ❑ No ❑d 13. Does paperwork match bottle labels? Yes No ❑ (Note discrepancies on chain of custody) 14. Are matrices correctly identified on Chain of Custody? Yes ❑d No ❑ 15. Is it clear what analyses were requested? Yes ❑d No ❑ 16. Were all holding times able to be met? Yes No ❑ (If no, notify customer for authorization.) Special Handling (if applicable) 17. Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA V Person Notified: Date: By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person Regarding: Client Instructions: 18. Additional remarks: Cooler Information Cooler No Temp °C Condition I Seal Intact Seal No Seal Date Signed By 1 10.0 Goodl Not Present Page 38 of 38 SECTION 5 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name Town of Beaufort WQ Permit Num her: WQ0006017 WWTP Nam Town of Beaufort WWTP NPDES Number: NCO02183 t MonitoringP rind: From 01/01/2022 To 12/31/2022 Pathogen Red uction (40 CFR 503,32115A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: All. I (time/temp) Alt. 2/S (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/l7 (I lo Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. fi (Equivalent to PFRP) if applicable o alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": CompoHeat Drying Heat Treatment Thermophilie Beta Rai Gamma Ray Pasteurization Class B: Alt. (1) Fecal ensity X Alt. (2) Process to Significantly Reduce Pathogens If applicable o alternative performed (Class B only) indieate "Process to Significantly Reduce Pathogens": Lime Stabil zation Air Drying Composting Aerobic Digestion Anaerobic Di estion rf nnni—M. 1. If loco A nr PI... R1 onm Wt tha f.11—ins mnnifnrirto rlul9• Parameter Allowable Level in Sludge Pathogen Density No. of frequency Sample Analytical Excee- of Type Technique Minimum Gco, Mean Maximum Units dences Analysis Fecal 2x 10 to Utc 61h MPN MPN/g Coliform power per gram of total solids <11400 309000 12100000 CFU/g 0 Annually Grab SM9222D- CPU MF 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Op ion/Alt. I Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS eduction) (40-day bench) (30-day bench) (Spec. 02 uptake) Op ion/Alt, 5 Option/Alt. 6 Option/Alt, 7 Option/Alt. 8 (14-Dai Aerobic) (AlkStabilization) (Drying — Stable) (Drying —Unstable) Op ion/Alt, 9 Option/Alt. 10 Injection) (Incorporation) )£ No vector attraction reduction alternatives were performed _ CERTIFICA TION STATEMENT (please check the appropriate statement) "I certi y, under penalty of law, that the pathogen requirements in 40 CFI( 503.32/ 15A NCAC 02T.1106 and the vector attraction X reducti n requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I ccrti y, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1 106 and the vector attraction reducti n requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met," (Please note if you check this statement attach an explan tion why you have not met one or both of the requirements.) "This determ nation has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel pri perly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. t m aware that there are significant penalties for false certification including fine and imprisonment." Donovan Wi lis, Public Utilities Director Todd Larson Operations Director Preparer Nar ic and Title (type or print) Land App ier Name and Title (if applicable) (type or print) r `r 1 /31 /2023 Signature oP reparer* Date Sign attire f Land Appl (if applicable) Date *Preparcr is defined in 40 CFR fart 503.9(r) and 15A NCAC 2T.1102 (26) Cameron Testing Services, Inc. Laboratory Report NC DENR#654 NC PHHS #37799 US EPA #NC01918 Client: Synagro CTS Prof. 2201-0083 DW Cert # 37799 roje:ct: Beaufort WWTP Regulatory Yes Sample Information C. Wynne „ 01/10/22 Received J. Cameron Date 01/10/22 Analyses and Results .. Lab ID Sample ID c Analyte Result = N m E Std. Methods g t3 ❑ :7. c ❑ Reference 2201- 01 -01 Sludge Gr Fec. Coliform-S 738000 CFUig 1ob00o 01/11/22 CSC 9222D - MF -02 98200 CFurg 98200 -03 <11400 CFUrg 114000 -04 759000 CFUlg 94900 -05 452000 CFurg 90400 -06 12100000 CFurg 97100 -07 78900 CFUIg 78900 Geomean 309000 2201- 01 -01 Sludge Or TS (%) 15.6 % 0.01 01/13/22 KJW 2540 G -TS -02 16.1 % 0.01 -03 14.5 % 0.01 -04 16.0 % 0.01 -05 15.5 % 0.01 -06 14.5 % 0,01 -07 15.7 i 0.01 Report Review Project Manager Date 219 S. Steele Str. 919-208-4240 Sanford NC 27330 chris@camerontesting.com � 0 k 0 0 c m U % \ E � \ L) \ o o ) 3 a Z32 \ \ o . 2 = ram 3 D § § 0 220 W )y u \o E _y FT \ �$ cu \ 2 } _ \ a VOA _ d g� E. G w a .0 e -1 . . . . . . % 41. \ \ � a e ® E . . . . ■ 2 d0G � . . . . . do3 � _ eO »1 j 0 .CL § xQm A J k geje 4- Zdwog co ) s . . . . . . . £. * �/ CL eL& � q / / %e§ % : 0) 0t ® / § O m....� § $ § \ 7 \ CL § ■ f � �N \ U ■ (L d — « E G \ k \ 0 \ \ SECTION 6 Agricultural Lime Application Log Year 2022 Project Beaufort Fields I I Soil I Lime Requirements Tons/Acre Date (state -county -site -field) I PH (from soil analysis) Applied A limed C R-07-3 B 1 5.41 1 1.OT I N/A N/A -Did not apply in 2022 *Lime will be applied when field conditions/cropping pattern permits SECTION 7 n / \ / & / = / = a 3 J @ \ O &0) 4 \ 0 'J o 3 CDL r C 2 o 2k\cn o 5 2 z z m z ! CO = o \ 2 \ \ \ § z \ J § 0 > u� >Mn - J « k \ CD NC N 7 _ 7 \ 2� N CO \ F { e % § m 04 0a k u p = = C r = G w amo 7 p m \\\ e = ' 0 \ / k § g / 2 7 & I # m m § _ LO 0 C C 00 ) % u u / cn 00 2 t R o \ _ � f ± E 0 CD (0 2 � # E CD 2 2 r u ? n z / \ 2 .boo LO Q r 2 w 6 ., E § 2 CD�0 / t CL \ § k \ 0 F k § 2 k / § 2 2 G \ _ C � CD) k \ � E u « R ƒ / 6 q $ 0�\ E § ' ® ' J u \ t / 2 M Q k F = Cl) \ CL u 0 G L \ 0 co \ n m ! / § 0 k \ \ k z my« 2 m w k 'j E = E { / �} 7 coo\ E& C / .\ / / E \ / y \ \ �E \ £ \k E k § / . E a / f Cl)LO -i (n N LL o 0 C N N w N a) y C y fC N i QN i O N (Q O _ E _ Q Q U E O a) O O y U a) U U co N O O U mE E X >, >, CL >, X X — a) a) a) U U N y c N N y N X a) a� a� a) y E aa) a? mco N cUi cUi N C) a) a) co O — y X O O O X O E O w N N O =°° o m- �, .—° O) C 0 U N � C �y L 0 (6 N>> N" a) E N .0 � L L .c O Q- j m W W CO Q M U (CO CO 6 (6 (wU O 0) (6 (6 0 O Z_ a) O Q Q �p X U `..' `..' Q U `..' c c 'O O O w .— C 'O X O O o N O X a) 0 0 O N C C N ++ O- 2)� L L zi O a) o o U U a) Q Q Q o E E E E C y C O U a s (n (n N— U C N Z o e \ Q Q m W 7 fA 1 al Z C C C C Q M O — Q U fA CC Q M M U U U W 2 `1 `1 2 2 2 2 2 2 Z Z Z O C. d d 0) 0) �i N N C O >> y U) m(B N a) Q O O Q N o L C C i �_ a) y a) .0 m O O 0 O� OLi N (B a-C U) a-+ U)O o N 7 "O Lo Lo a) U i i U (B O E ~ y C_ Q p O p= C a) n p 4 C O CD U) p p 7 -U L a) �. i �j 0+ C 0 U Zi OY (B r)CY a) y � a) C)-0 N U O (B U) N = O y oca O I E _ C i Z> O C Lo E a) a)C O y aLO) --I:- CY >a)N E U)_ 0 M U) U) O E a) n mU N m -p M C Q- a)O C N O ch O UO ) a O L a) 0 0 a) N U) y E U w C QQ O W O) C Lo a) -0 U) E Z L N -0 Q C fC 7 N i— L U i — O E — Z O O E U y U) N m N a) .E O N i (� O a .N >, i (A 3 C rz U) m U O O O N M E 73 O E E — y C L E > U)= V U U)N O (n U) d CO Va � (mN U C p y Q N M o m N zO a) m O CO C .E N N 0� a) o� O 415 r o Q N N a) rz a is N N C [� O L O N (B a) N (B z a E (B a) 0_ a) -0 _ a) Z U) t i O p U C E Q N M N Q m U) U) w o 0 3 '� a) — �Q d C E Q ; C: mO Q >, N U O ry�� co a) C L 0- OE LL UU> ,- cM a)YN OL W O O N CD p O m LL Oo Q XO ) w aw� zwO - > o a a) o a-0 O U D ow L C = O L > C a Q '� O U U)m m O N � a) a) .O � L _V w _' O N O C L x N= N U) m O 0 Q y M a) N N p� Q O m m CC n1N � (B C O O O U y m a)_ M QQ Mn Q Q a) E N E U) t C L D p M y o p C C a) m y a) w U a) o�� o o o �� �o m a) - aa)) Y Or (B O 'N C L 0) a) U Lp aa)) ° C O a) M C , a) U` O .0 C `� m U O o N U > d U C C 0+ C L O CE1 > 06 > CO O 0 EM a) WLE 0 -0 m 'a O N a) OI u) N p p C N> Ncm X a) > y _ U C U m L m E O E a) a) m L °� E m O a) U a) a) m y a) (B E> Z LLL �OO BBQ M