WQ0000543_2022 Residual Annual Report_20230227 (2)

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * WQ0000543
Applicant/Permittee City of Sanford
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Raleigh
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Lysa Finnerty
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
4105376150
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0000543
Has Current Existing permit number
Applicant/Permittee Address*
435 Williams Court, Ste 100, Baltimore, MD 21220
Facility Name*
City of Sanford Class B Residuals Program
Please provide comments/notes on your current submittal below.
2022 Annual Report for City of Sanford, NC
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Sanford NC 2022 Annual Report FINAL.pdf 23.25MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/27/2023

435 Williams Court, Suite 100
Baltimore, MD 21220
www.synagro.com
FEBRUARY 27, 2023
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2022 Annual Report for Permit No. WQ0000543
Dear NCDEQ:
SYNAGRO
Synagro is submitting one electronic copy of the above referenced report on behalf of the City
of Sanford, NC.
If you have any questions or need additional information, please do not hesitate to contact Scott
Siletzky at [phone] or Ryan Copeland at [phone].
Sincerely,
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Ryan Copeland, Synagro
Scott Siletzky, City of Sanford
YOUR PARTNER FORA CLEANER, GREENERWORLD

CITY OF SANFORD
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0000543
2022 ANNUAL REPORT

City of Sanford, NC
Residuals Land Application Program
2022 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and Residuals
Analyses
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00000543 County Lee Year 2022
Facility Name (as shown on permit) Ci of Sanford WV4TP NPDFS No. N00024147
Land Application Operator Svnapro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO, If NO, skip Part A. and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation an how the residuals were handled.
Part A — Residuals Application Summ
Total number of application fields in the permit: 43
Total number of fields utilized for land application during the year: 24
Total amount of dry tons applied during the year for all application sites: 1055.78
Total number of acres utilized for land application during the year: 473.61
Part B = Annual Compliance Statement:
Facility was compliant during calendar year 2022 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO,
If no, please provide a written description why the facility was not compliam the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T A 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .11 I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations_
i t. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false inforrr�ation, including the possibility of fines and imprisonment for
knowingviolations." f! r 0 1
Hal Hggau -Public Cily Manager 1sC Z:5
Permittee Name and Title (type or print) SignaDoer e Cate
1s a3 vlrzo2=
Signature of Pre r• ate Si a of and plier Date
(if different from Permittee) (if different from Permittee and Preparer)
•Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 3/6/2022 - 3/31/2022
SANFORD,NC
SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
MONTH/YEAR
March 2022
TOTAL
Units Key: D - Dry Tons; G — Gallons; W — Wet Tons; Y — Cubic Yards
Report Date: 1/28/2023 1:35:43 PM
AMOUNT
UNIT
DRY TONS
UNIT
DRY METRIC TONS
496,000.00
G
105.90
D
96.05
496,000.00
G
105.90
D
96.05

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 4/1/2022 - 5/3/2022
SANFORD,NC
SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
MONTH/YEAR
April 2022
May 2022
IEel /_1I
Units Key: D - Dry Tons; G — Gallons; W — Wet Tons; Y — Cubic Yards
Report Date: 2/1/2023 5:06:24 PM
AMOUNT
UNIT
DRY TONS
UNIT
DRY METRIC TONS
1,103, 600.00
G
156.93
D
142.33
124,000.00
G
17.63
D
15.99
1.227.600.00
G
174.56
D
158.33

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 7/2/2022 - 8/9/2022
SANFORD,NC
SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
MONTH/YEAR
July 2022
August 2022
IEel /_1I
Units Key: D - Dry Tons; G — Gallons; W — Wet Tons; Y — Cubic Yards
Report Date: 1/28/2023 1:39:00 PM
AMOUNT
UNIT
DRY TONS
UNIT
DRY METRIC TONS
1,047,800.00
G
138.07
D
125.23
948,600.00
G
125.00
D
113.37
1,996,400.00
G
263.07
D
238.60

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 9/3/2022 - 12/31/2022
SANFORD,NC
SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
MONTH/YEAR
September 2022
October 2022
IEel /_1I
Units Key: D - Dry Tons; G — Gallons; W — Wet Tons; Y — Cubic Yards
Report Date: 1/28/2023 1:46:09 PM
AMOUNT
UNIT
DRY TONS
UNIT
DRY METRIC TONS
1,574,800.00
G
207.51
D
188.22
2,312,600.00
G
304.74
D
276.40
3.887.400.00
G
512.25
D
464.61

SECTION 2

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PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Chris Wynne
Project Name: Sanford VWVFP
Lot Number:XA05007
Date Completed:01/24/2022
NIM�� Mr�
01/24/2022 1:47 PM
Approved and released by:
Project Manager II: Lucas Odom
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A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 9

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: XA05007
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Inorganic Metals
Due to the matrix and low percent solids of the following samples, the initial sample amount is 3x greater
than standard procedure: XA05007-001. The LOQ has been adjusted accordingly.
Inorganic Non -Metals
The following sample was diluted due to the nature of the sample matrix for Nitrate and Nitrite: XA05007-
001. The LOQ has been elevated to reflect the dilution.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 9

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Synagro
Lot Number: XA05007
Sample Number Sample ID Matrix Date Sampled Date Received
001 Sanford WWTP Solid 01/04/2022 1330 01/05/2022
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 9

Inorganic non-metals
Client:Synagro Laboratory ID:XA05007-001
Description: Sanford WWTP Matrix: Solid
Date Sampled:01/04/2022 1330 % Solids: 5.12 01/12/2022 0029
Date Received:01/05/2022
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date
Batch
1 350.1
(Ammonia - N ) 350.1
25
01/12/2022 2127 DAK
28095
1
(Nitrate - N ) 9056A
5
01/20/2022 1634 AAB
29256
1
(Nitrite - N ) 9056A
5
01/20/2022 1634 AAB
29257
2
(Phosphorus) 365.1
50
01/13/2022 1550 DMA
01/06/2022 1459
27588
1
(Soil pH meas) 9045D
1
01/11/2022 2049 NBW
28081
1 351.4
(TKN) 351.2
5
01/20/2022 1024 DMA
01/12/2022 1125
28145
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Ammonia - N (gas diffusion)
350.1
6600
490
250
mg/kg
1
Nitrate - N (soluble)
9056A
11 J
49
9.8
mg/kg
1
Nitrite - N (soluble)
9056A
ND
20
9.8
mg/kg
1
Phosphorus
7723-14-0 365.1
30000
4900
980
mg/kg
2
Soil pH measured in water @
20.1 ° C
9045D
7.1
su
1
TKN
351.2
53000
4900
2400
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 9

CVAA
Client:Synagro Laboratory ID:XA05007-001
Description: Sanford WWTP Matrix: Solid
Date Sampled:01/04/2022 1330 % Solids: 5.12 01/12/2022 0029
Date Received:01/05/2022
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/10/2022 0757 JAB2 01/10/2022 0116 27833
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury
7439-97-6 7471B ND 1.5 0.36 mg/kg 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 9

ICP-AES
Client:Synagro Laboratory ID:XA05007-001
Description: Sanford WWTP Matrix: Solid
Date Sampled:01/04/2022 1330 % Solids: 5.12 01/12/2022 0029
Date Received:01/05/2022
Run Prep Method
1 3050B
Analytical Method Dilution Analysis Date Analyst
6010D 1 01/11/2022 1133 KSH2
Prep Date Batch
01/10/2022 0056 27840
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5
6010D
15000 S
120
47
mg/kg
1
Arsenic
7440-38-2
6010D
5.1
4.7
1.6
mg/kg
1
Cadmium
7440-43-9
6010D
1.4 J
1.6
0.39
mg/kg
1
Calcium
7440-70-2
6010D
15000
1600
190
mg/kg
1
Chromium
7440-47-3
6010D
34
3.1
0.78
mg/kg
1
Copper
7440-50-8
6010D
330
3.1
1.4
mg/kg
1
Iron
7439-89-6
6010D
15000
31
14
mg/kg
1
Lead
7439-92-1
6010D
18
3.1
1.4
mg/kg
1
Magnesium
7439-95-4
6010D
6000
1600
190
mg/kg
1
Manganese
7439-96-5
6010D
1300
4.7
1.8
mg/kg
1
Molybdenum
7439-98-7
6010D
17
12
3.1
mg/kg
1
Nickel
7440-02-0
6010D
31
12
3.3
mg/kg
1
Potassium
7440-09-7
6010D
6600
1600
190
mg/kg
1
Selenium
7782-49-2
6010D
5.9 J
6.2
2.5
mg/kg
1
Sodium
7440-23-5
6010D
2200
1600
190
mg/kg
1
Zinc
7440-66-6
6010D
720
16
3.9
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 9

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 9

PACE ANALYTICAL SERVICES. LLC
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10. Did
F"i Y es
NotL
1. A
ire togs to be perurrncd lisicd an the C-00?
0 Yr.-,
El No l
' 2- Di
(uo
all satuples arrive in the proper containers for each hest aridlor in 9*d €onditiun
uYy lids on, m)t
-
YcLJ
NQ
J. W
50nj ?IG V0113ma available?
Pri Yes
Ll No
A W
re all samples re:Pived within V the holditlgtlmaor48 hu-Prs, whicliever camest:ssl?
'r,
f No!
.. 5. W
a any satnpks oontaincrs Mr Sinw"o m (c ir;.lc ono) Samplm Not Mted an COc'
©'#: s
l
I-1� IY.-INA
'
in ar:u
:e, .acre IarrirYalefi preficn [re, {sif�" ( "fir {r�,n, i, cii x4+t rl
rrf Ilrn VOA vixlx?
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No: [Z]NA
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re. all DIZkVmelnNhitrient samplesreceived at a p--# of-:
Yea,
LJ No,
VNA
L 8- W
e all cyanide Ga np' as received at a pal > 12 and sulfide samples n4i uea AA u PH ` 9?
❑ Yw
❑ No
I
DMA
19. W
resi,lu
all applicable NWi�KRUcyanidephcnol 25. 1608.3( 0.5mWL)isarnplPs freegr
l c:sloriltie7
El Yes[' El No
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NA
r'emarkWee quesis {i.e. l egLw,Iird di[utisrr,Y,, "IM SD (Imi�,rllii,nn, rat,,,,)
ly tran` tibl 4 mom 1.1n CDC Info dte cormmvt w4ion in LJMS?
Yr,, ,N4
121- W.
is the n ooto num br-r listed on the container label'? If yes, Quom #
I
Se mple Pr-meivatiou (Must be
romp d fO.Y any samples) iIlcorrec ly Reserved Or V. W) he-RdspaCe'.)
$yfntplK(SJ
-n sarr,rle eiWfill g witlr NA _
Time of presef4'ation N A
Were reocivind inom-rcctly pTcwi- `Gd PiO wk;
L ocirc:e oua: H2S [ , NO3, ]-]CI, Na011 rsirg SR g 'NA
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if more than one pmertrative is needed, please nnie in the rt)mnmei
Ttdjtsstcd armordinAy -
1,5 bel w,
I
Sampl.M(sj NA__ _
wcry r:4z4ivcd with bubb[ca x
_
mm in dianie-r--
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wera received with TRC r D.5 m2VL (if # 19i
iv'irG w:t i wt'ivm thipsulfate 1,Na7LS3 with $heply IV, NA ..-..
� -- - — [)ate. 1151317Q2
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R bn=de lnbets applied by: �
Face Analytical Services, LLc (tormeny sneaiy tnwronmentai services, inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 9

0p
0
PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Chris Wynne
Project Name: Sanford VWVFP
Lot Number:XD08021
Date Completed:06/02/2022
NIM�� Mr�
06/03/2022 9:47 AM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: XD08021
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Inorganic Metals
The following samples were classified as a biosolid therefore they were weighed out at around 3.0 grams
to 4.0 grams to ensure proper digestion: -001. The LOQ has been adjusted accordingly.
Inorganic Non -Metals
Due to multiple QC failures, sample -001 required additional runs. The best run has been reported.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 7

Client: Synagro Laboratory ID: XD08021-001
Description: Sanford WWTP Matrix: Solid
Date Sampled: 04/06/2022 1330 % Solids: 3.41 04/13/2022 0031
)ate Received:04/08/2022
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 2540G
1 04/13/2022 0031 CVR
37943
1 350.1
(Ammonia - N ) 350.1
10 04/20/2022 1418 DRD
38502
3
(Nitrate - N ) 9056A
1 05/19/2022 1625 CAW
42428
3
(Nitrite - N ) 9056A
1 05/19/2022 1625 CAW
42431
1
(Phosphorus) 365.1
25 04/19/2022 1513 DMA
04/14/2022 1124
38098
1
(Soil pH meas) 9045D
1 04/15/2022 1444 NBW
38410
1 351.4
(TKN) 351.2
2 04/18/2022 1818 DMA
04/14/2022 1021
38097
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
3.41
%
1
Ammonia - N (gas diffusion)
350.1
13000
290
150
mg/kg
1
Nitrate - N (soluble)
9056A
37 H
15
2.9
mg/kg
3
Nitrite - N (soluble)
9056A
68 H
5.9
2.9
mg/kg
3
Phosphorus
7723-14-0 365.1
36000 S
3700
730
mg/kg
1
Soil pH measured in water C)
21 ° C
9045D
7.2
su
1
TKN
351.2
72000 B
2900
1500
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 04/18/2022 0424 JAB2
04/18/2022 0142
38298
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471 B
0.59 BJ
2.3
0.55
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601 OD
1 04/14/2022 0227 KSH2
04/12/2022 1109 37814
2 3050B
601 OD
1 04/15/2022 0209 JMH
04/12/2022 1109 37814
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
13000
190
70
mg/kg
1
Arsenic
7440-38-2 6010D
5.4 J
7.0
2.3
mg/kg
1
Cadmium
7440-43-9 6010D
1.4 J
2.3
0.59
mg/kg
1
Calcium
7440-70-2 6010D
14000
2300
290
mg/kg
1
Chromium
7440-47-3 6010D
36
4.7
1.2
mg/kg
1
Copper
7440-50-8 6010D
400
4.7
2.1
mg/kg
1
Iron
7439-89-6 6010D
14000 B
47
21
mg/kg
1
Lead
7439-92-1 6010D
25
4.7
2.1
mg/kg
1
Magnesium
7439-95-4 6010D
6000
2300
290
mg/kg
1
Manganese
7439-96-5 6010D
1400
7.0
2.8
mg/kg
1
Molybdenum
7439-98-7 6010D
30
19
4.7
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range DL - Detection Limit Q - Surrogate failure
ND - Not detected at or above the DL N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% J - Estimated result < LOQ and > DL L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client: Synagro Laboratory ID: XD08021-001
Description: Sanford WWTP Matrix: Solid
Date Sampled: 04/06/2022 1330 % Solids: 3.41 04/13/2022 0031
Date Received:04/08/2022
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 04/14/2022 0227 KSH2 04/12/2022 1109 37814
2 3050B 6010D 1 04/15/2022 0209 JMH 04/12/2022 1109 37814
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Nickel
7440-02-0
6010D
39
19
4.9
mg/kg
1
Potassium
7440-09-7
6010D
9400
2300
290
mg/kg
2
Selenium
7782-49-2
6010D
9.3
9.3
3.8
mg/kg
1
Sodium
7440-23-5
6010D
2100 J
2300
290
mg/kg
1
Zinc
7440-66-6
6010D
910
23
5.8
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range DL - Detection Limit Q - Surrogate failure
ND - Not detected at or above the DL N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% J - Estimated result < LOQ and > DL L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental
Services, Inc.)
106 Vantage Point Drive
West Columbia, SC 29172
[phone] Fax [phone]
www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
sarnples kdceipt ChFc4ist (SRc� (mtuolw L5I Revise(fV29/2020
- .ZAMJy M
Issuing Autho rity_ pac-_ kNV - WCOL Page Z Lr� 1
Sample Receipt Chec ict (SRC)
C rient- k :aRro
Cooler lnspcotcd �iy.+da#t: TC f 9411M,122 fro[ : }{DQtD02t
t:
P@ L C_l PA, ,�U 1 edEx Other;
pcariself
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cus44dseals u.erC resent were tl,ry 9�roi r[nd anbrnkerl?
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Chlodn: Strip ID: 11A Tested wn
1'Y;_.
C)riCina] tcLr.}e3LELu:1, upon recei]A l Derived (C-nToaed) tempmture uptsii rectiipT %Slbli� Snap -Cup In: 22-3
:+-8 13-5 cC NA j NA QC VA 1'1A eC. NA I NA nC — ..
Mctlad.. ❑-l-amperaturC
Blank `,n51 &Yale-, M Gun iD: 5 1, Crun Correction Factor_ 0 °C
,
'vict[rud of 400lanr ❑,� Wet lee LJ Xcc Packs Q Div .ce ❑ h one
Ycs ❑ Nu
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3. If Lmpmature Ofary a3l]ler.Fxcecded 6-.3'O, was Prajnrt [+Manager LNotr&d?
PM war Not;[%-d by; phone � r-mall i t �to-face (Circle aIIa)-
Yes Na
A
4. Ts the commercial courier's packtng 31ip 41Mched to tliis Form?
Yes Alaf
5. Were Proper r.wmfodymfur[s{relu[yui4h recaiwe }folloxec7
vr yes \T#
6. V4Fc:re simple Ms [fisted Cnr CFw- COC:?
J Yes NO
;. Wore sample 1T33 listed on all sunmple containnrs7
Ala
3. wn collection U= & tima IiMed c9i tlLe COG?
LVY
N�
9- Wei coilection date . tinse li5tcd on ail$amp]o cott
N,,
I&_ Did all cGinaineT NMI mrormmjm Lon (ID, date, Vme) agtee.vrth [be C.^
No
l 1. WLTO I'UNS to be perfrn-ntrd 1 isro:ri qn the COC?
ti P 12. Did all ,arnptes arrive in the p-Oper a ntalners for rwc test and!ar 1r, good cxrnditio,
(un>>n, [ids
0 Ya5 NCI l 3- Was adequate samplc vohirna avx.iiab[e?
-'es No lA. Wr" 3:1 samples recelv6d within h Jhe holding dnie or 48 hoLnfs, wilivIlover oome�; firsti—
Ycs Nu - 15. Were any samples containers nil5i:ngleacess (circle ago sLvripl4 Not lists bn CSC?
❑ Yvs, [IN" ❑, NA 10. Fnr VOA and KsK-l75 ;urnpies.3were habb1es pr2wFLf ="pea-siFe' (4T'av: limos in dirmlcter)
sn ariy oft1w VOA vials?
Na NA t t. We-e all DR OAr-etalm'nutri-m t sample., rxeived aL a pFr of < 2F
❑ Yr Nu NA 18, Were all amide sornplos rareiwed at a pH > -2 and suffice sauaplcs rime Ned at �t PH > 9?
❑ yes ❑ to N A' 1 arm all applicable N y FKNlq �nideJ lh no1e625, ! MI-3 (< 0.5mg(L) sana p[os freeif
rcn ldual Clllflrl h G`)
�] Yes 0h'o C-I]NA 20, lh'aeciientreanarlc�+rGyLr��ts{i-e-r�utstcddiluti�7ny, M�J�v]5D dcsignattorlti, cic.,,j
icormctily LtansoTibed from the WC: into the C 131MOF t Rr..:,tjon in LlMS2
Yes N 2-1,waSth' uots�,iM,hrrlisted ontl_G4unix.inerlRbC1?lfyes,ODUtC�
'simple P1Weruation (Must Ise enripleted fa:" LULy .sample(€] iftorrect:y preservcd or with hMspace-j
3.aM 1G45%F ". lva lC rcccIved [nrorroetly preserwtxi acid were agijii-�ted ac�vrditigiy
n wnplo r4ae.tv[nE with NA ruL of circle onc; H2904, HWO3, I u. NaOH usinS SR 4 NA
Circe of paw€ervmArm NA if more than one presotvULM is nmdVI, please n-LstL: in the ccmments belonu.
NA
_were .ocajved with bubb[cs �_6 mm in d:anizier.
•r �k-� _ WeM rccewed wi lh `1 RC: r 13 rng/L of # l9 is nv) and wCre
1=4Etcd aoconJiugjy in sample receivarg with sodium thiostllfhte (VazS;0.3) will 4ltealy ID-- NA
R barcode labels .4pslied by; TUC [c; 04M7124 2
Comments..
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

0p
0
PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Chris Wynne
Project Name: Sanford VWVFP
Lot Number:XG07030
Date Completed:07/27/2022
NIM�� Mr�
07/28/2022 11:05 AM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: XG07030
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Inorganic Metals
The following samples were classified as biosolids therefore they were initially weighed out at around 3.0-
4.0 grams to ensure proper digestion: XG07030-00. The LOQ has been adjusted accordingly.
Inorganic Non -Metals
The method blank for prep batch 47664 contained the analyte total phosphate greater than the method
acceptance criteria. The associated samples contained detections for this analyte at concentrations
greater than 1 OX the value found in the method blank; therefore sample results are not impacted. The
data has been reported.
The Nitrate/Nitrite method blank and LCS associated with the samples ran in a bracket that contained 11
injections. Per the SOP, no more than 10 injections shall be analyzed between CCV and CCB pairs.
Bracketing QC is passing and the data is not believed to be adversely affected.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 7

Client: Synagro Laboratory ID: XG07030-001
Description: Sanford WWTP Matrix: Solid
Date Sampled: 07/06/2022 1300 % Solids: 3.16 07/21/2022 2237
Date Received:07/07/2022
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 2540G
1 07/21/2022 2237 MJS2
48747
1 350.1
(Ammonia - N ) 350.1
50 07/19/2022 1202 CMM
47976
1
(Nitrate - N ) 353.2
5 07/20/2022 1355 KKP
47766
1
(Nitrite - N ) 353.2
1 07/20/2022 1330 KKP
47768
1
(Phosphorus) 365.1
25 07/18/2022 1558 DMA
07/12/2022 1324
47664
1
(Soil pH meas) 9045D
1 07/08/2022 1903 KKP
47564
1 351.4
(TKN) 351.2
2 07/13/2022 1843 DMA
07/12/2022 1200 47679
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
3.16
%
1
Ammonia - N (gas diffusion)
350.1
18000
1600
820
mg/kg
1
Nitrate - N (soluble)
353.2
1200 S
32
4.2
mg/kg
1
Nitrite - N (soluble)
353.2
160 S
6.3
0.83
mg/kg
1
Phosphorus
7723-14-0 365.1
30000
4000
790
mg/kg
1
Soil pH measured in water C)
25.7 ° C
9045D
7.5
su
1
TKN
351.2
61000
3200
1600
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 07/10/2022 1035 MRW2
07/10/2022 0654
47419
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471 B
1.1 J
2.5
0.61
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 07/13/2022 0734 JMH
07/11/2022 1541
47423
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
14000
190
73
mg/kg
1
Arsenic
7440-38-2 6010D
6.1 J
7.3
2.4
mg/kg
1
Cadmium
7440-43-9 6010D
1.8 J
2.4
0.61
mg/kg
1
Calcium
7440-70-2 6010D
16000
2400
300
mg/kg
1
Chromium
7440-47-3 6010D
53
4.9
1.2
mg/kg
1
Copper
7440-50-8 6010D
410
4.9
2.2
mg/kg
1
Iron
7439-89-6 6010D
20000
49
22
mg/kg
1
Lead
7439-92-1 6010D
24
4.9
2.2
mg/kg
1
Magnesium
7439-95-4 6010D
5900
2400
300
mg/kg
1
Manganese
7439-96-5 6010D
1600
7.3
2.9
mg/kg
1
Molybdenum
7439-98-7 6010D
21
19
4.9
mg/kg
1
Nickel
7440-02-0 6010D
40
19
5.1
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range DL - Detection Limit Q - Surrogate failure
ND - Not detected at or above the DL N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% J - Estimated result < LOQ and > DL L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client: Synagro Laboratory ID: XG07030-001
Description: Sanford WWTP Matrix: Solid
Date Sampled: 07/06/2022 1300 % Solids: 3.16 07/21/2022 2237
Date Received:07/07/2022
ICP-AES
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
6010D 1 07/13/2022 0734 JMH
07/11/2022 1541
47423
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Potassium
7440-09-7 6010D
11000
2400
300
mg/kg
1
Selenium
7782-49-2 6010D
5.1 J
9.7
3.9
mg/kg
1
Sodium
7440-23-5 6010D
2800
2400
300
mg/kg
1
Zinc
7440-66-6 6010D
990
24
6.1
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range DL - Detection Limit Q - Surrogate failure
ND - Not detected at or above the DL N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% J - Estimated result < LOQ and > DL L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
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Sample Receipt Checklist (SRC)
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Yrs Ntiu IWA 4, Js the wmrrLrrc;jAl "Llflvr'r 1packin& SHP aLLr hgdtp d1iR roan?
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Yoa Ntj G_ Wera: Fmp.Le iL)s listed on the COCA
c! Nc 7, Wem sample IDs Ilmd oil ail 4umplp conrLlfncrs?
Yes No I R. 1;ras collcctia l dale & times listed oa thr. CO
Yeo-s No 9_ 'Mis collection data& litnc listed on all sample cullilAiL:LTS"
Yes ❑ No 10, Did all c"incr IaheI infounation (ID, date, limo) agree with the Crc"?
YC5 NUl I _ Wert tests to be pal•formEd ILMW on the COC?
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aNA 16, For VOA and RSK-173 S4rrilplcs, Rr&t: bubbles FreiMt>"pea-s128"I,!/i"or Glum it dianlEter)
in,tl0r, i tiro VOA vials?
Yes
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>8uup le Pr*c,-ation (Must be cnrnple-ted for any mrr_pJe(s) iH; Wr ctE ' PreXr,,vd or -Lviih rrraispaoe-)
mELleis) "A vrc:cmucivef inconl3nilyprusurvedand wrrx,adjusCWaceaa•dirLgiv
samplo receiving with _�4 mL of circle onc: Hmcw, HNO3, I [Cl, NaO.11 using SR rf MA
ne of prcSCrYBtipn nr Ifmare thAr. one. p:, + a w ativc is need is plea; V not; jr. tl a commen is below.
n'PI "A were received widi bubbleF,>6mm ind�,.meter_
tnple:(s) W.} _ _worc rcmived with `l-RC > 0_5 mg/L(Ifuaq is120) anri +Aare
usted 20aor•dirlgly in sample n=:ving Lyjth radium thijl;ulfaw (Nk O.j) with Sboaly 1D, NA
baroode IAbels applied by: TKAit
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Page
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

0p
0
PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Adam Brigman
Project Name: Sanford VWVFP
Lot Number:XJ05043
Date Completed:11/01/2022
11/02/2022 5:28 PM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: XJ05043
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the matrix and low percent solid, the following sample has an initial weight that is 3x greater than
standard procedure: XJ05043-001. The LOQ has been adjusted accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 7

Client: Synagro Laboratory ID: XJ05043-001
Description: Sanford WWTP Matrix: Solid
Date Sampled:10/04/2022 1000 % Solids: 2.20 10/11/2022 2200
Date Received:10/05/2022
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 2540G
1 10/11/2022 2200 MJS2
56709
1 350.1
(Ammonia - N ) 350.1
50 10/19/2022 1650 CMM
57366
2
(Nitrate - N ) 353.2
10 10/20/2022 1824 KKP
58392
2
(Nitrite - N ) 353.2
10 10/20/2022 1824 KKP
57678
1
(Phosphorus) 365.1
25 10/08/2022 1459 DMA
10/07/2022 1400 56358
1
(Soil pH meas) 9045D
1 10/12/2022 1532 KKP
56841
1 351.4
(TKN) 351.2
2 10/07/2022 1846 DMA
10/06/2022 1447
56231
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 2540G
2.20
%
1
Ammonia - N (gas diffusion)
350.1
35000
2300
1200
mg/kg
1
Nitrate - N (soluble)
353.2
ND
91
12
mg/kg
2
Nitrite - N (soluble)
353.2
3900
91
12
mg/kg
2
Phosphorus
7723-14-0 365.1
46000
5700
1100
mg/kg
1
Soil pH measured in water @
21.4 ° C
9045D
7.8
su
1
TKN
351.2
89000
4500
2300
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 10/07/2022 1546 MRW2
10/07/2022 1138
55609
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471 B
1.1 J
3.6
0.87
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601 OD
1 10/18/2022 0121 JMH
10/07/2022 0714
56157
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 601OD
18000
290
110
mg/kg
1
Arsenic
7440-38-2 601OD
16
11
3.6
mg/kg
1
Cadmium
7440-43-9 601OD
2.7 J
3.6
0.90
mg/kg
1
Calcium
7440-70-2 601OD
20000
3600
450
mg/kg
1
Chromium
7440-47-3 601OD
84
7.2
1.8
mg/kg
1
Copper
7440-50-8 601OD
500
7.2
3.2
mg/kg
1
Iron
7439-89-6 601OD
25000
72
33
mg/kg
1
Lead
7439-92-1 601OD
33
7.2
3.2
mg/kg
1
Magnesium
7439-95-4 601OD
7300
3600
450
mg/kg
1
Manganese
7439-96-5 6010D
1800
11
4.2
mg/kg
1
Molybdenum
7439-98-7 6010D
22 J
29
7.2
mg/kg
1
Nickel
7440-02-0 6010D
55
29
7.5
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range DL - Detection Limit Q - Surrogate failure
ND - Not detected at or above the DL N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% J - Estimated result < LOQ and > DL L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client: Synagro Laboratory ID: XJ05043-001
Description: Sanford WWTP Matrix: Solid
Date Sampled:10/04/2022 1000 % Solids: 2.20 10/11/2022 2200
Date Received:10/05/2022
ICP-AES
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
6010D 1 10/18/2022 0121 JMH
10/07/2022 0714
56157
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Potassium
7440-09-7 601OD
12000
3600
450
mg/kg
1
Selenium
7782-49-2 601OD
8.6 J
14
5.8
mg/kg
1
Sodium
7440-23-5 601OD
3700
3600
450
mg/kg
1
Zinc
7440-66-6 601OD
1400
36
9.0
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range DL - Detection Limit Q - Surrogate failure
ND - Not detected at or above the DL N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% J - Estimated result < LOQ and > DL L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
DC#_7ikla; ENV-FRS++i-WCot-02S6%10 _SalTtpieSRereiptChedlWI'SK )
effective Date: EVV2G22
Sample Receipt Cheeldist (SRp
Client 5�1"'H ° C;oolerLn t rxcrll Jic LIc_ SF>s r 10.')51`H2,'. Lot#. 7CMb5�[3
f�9catls of reaeipT' ' Pact Clicut TJPS Fel;x Ot ier
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+I Yes -No 6. Were sample IDs listed on 6e COC and ali sample containers?
Yes Nu 7. Wa5; eollecdon date & titm lis3rtl OR-ffic Co C wixl All sa"Ple corltai.itc:rs?
Yes i*]o 3. Did �dl cutiLaiml latni ifl&Duxlikgl JD-. date, dtvic} a�•ec Ivid] Cite C'OC.'
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7Y—:m E To 112, Were alb p,llt tiles r0C6VCd vJ0jn'l2 the hOl:iiug time or 4g ltcxmis. wbiclieva conics lust'+
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Rim dprzsm-Vation 1f1TK rc il,$ri OJ3e PleSCINM ive is needed, please trote in t)hc C4mtllent5 below_
Saouple(sJ NP, were received Aitit bubbles >6 mtu iu dimurErx_
51LSL1(}1e5($} AA omre rmcivcd wi,i] TRH ] 0.5 L (• 419 is m?) and v
adjuswd arzordtngly ui smWk xeceMug with sadilnn tluoslAW'- (NMg7A) Wit>b U Aiigite ILA; v
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SECTION 4

SUMM111
ENVIRONMENTAL TECHN❑LOMZ3. INC
Arraly0ca1 Laboralorfas
January 14, 2022
Chris Wynne
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL:
FAX:
RE: Sanford WWTP
Dear Chris Wynne:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
Order No.: 22010178
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/5/2022 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 2943, Colorado, Connecticut PH-0108, Florida NELAC E87688, Idaho OH00923, Illinois 200061, Indiana C-OH-13, Kansas
E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988, Minnesota 1780279, Nevada OH009232020-1, New
Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP CL0052, Oklahoma
2019-155, Oregon OH2O0001, Pennsylvania 011, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-19-16, Utah OH009232020-12,
Virginia VELAP 10381, West Virginia 9957C
Page 1 of 36

MM' Y Summit Environmental Technologies, Inc. Case Narrative
SU3310 Win St.
ENVIRONMENTAL TEC„HQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 wo#: 22010178
Arralyi9cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com Date: 1/14/2022
CLIENT: Synagro
Project: Sanford WWTP
WorkOrder Narrative:
22010178: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
22010178-OOIA MTL-TCLP-7(6010D): LCS-54221 exhibits high recovery for Silver. Sample is ND
for this analyte.
22010178-OOIA TCLP-SVOC_8270E: CCV exhibits high recovery for Hexachlorobutadiene. Sample
is ND for this analyte. Possible low bias for Pyridine due to low recovery in CCV. Compound
demonstrated adequate instrument sensitivity in RLC.
Analytical Sequence QC Notes:
LCS-54221 Mtl-TCLP-7(6010): LCS-54221 exhibits high recovery for Silver. Associated samples are
ND for this analyte.
Original
Page 2 of 36

MM' Y Summit Environmental Technologies, Inc. Case Narrative
SU3310 Win St.
ENVIRONMENTAL TEC„HQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 wo#: 22010178
Arralyi9cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com Date: 1/14/2022
CLIENT: Synagro
Project: Sanford WWTP
LCS-54264 TCLP-SVOC-CPEST(8081B): P: RPD between confirmation column is greater than 40%.
CCV 40ppm SVOC-MSTR_S(8270): CCV exhibited high recovery for Hexachlorobutadiene.
Associated samples are ND for this analyte. CCV exhibited low recovery for Pyridine. Possible low
bias in associated samples for this analyte. Compound demonstrated adequate instrument sensitivity in
RLC.
MB-54320 SVOC-BNA_TCLP(8270): Possible low bias for Pyridine due to low recovery in CCV.
Compound demonstrated adequate instrument sensitivity in RLC.
LCS-54320 SVOC-BNA_TCLP(8270): Possible high bias for Hexachlorobutadiene due to high
recovery in CCV. Possible low bias for Pyridine due to low recovery in CCV. Compound demonstrated
adequate instrument sensitivity in RLC.
Original
Page 3 of 36

MM' Summit Environmental Technologies, In Qualifiers and Acronyms
SU3310 Win S
EkiwllOMM@NTALTECHN❑LOG{r,23.INC Cuyahoga Falls, Ohio442� WO#: 22010178
Arraly0cal Laboralorlas TEL: [phone] FAX.- (330) 253-44E
Wehsite: httn:11www.settek.co Date: 1/14/2022
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
PLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 4 of 36

�� 1 � Summit Environmental Technologies, Inc.
SU3310 Win St.
ENVIROMMEWAL YECHNO WULES, JNGG Cuyahoga Falls, Ohio 44223
Analytical Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
CLIENT: Synagro
Project: Sanford WWTP
Lab SampleID Client Sample ID
22010178-001 Sanford WWTP
Tag No Date Collected
1/4/2022 1:15:00 PM
Workorder
Sample Summary
WO#: 22010178
14 Jan-22
Date Received Matrix
1/5/2022 10:15:00 AM Sludge
Page 5 of 36

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SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arralyt9cal Laboralorfas TEL: [phone] FAX. [phone]
Website: http://�i,-"-m,.settek.coin
Analytical Report
(base report)
WO#: 22010178
Date Reported: 1/14/2022
CLIENT:
Synagro Tag Number:
Matrix:
SLUDGE Collection Date: 1/4/2022 1:15:00 PM
Lab ID:
22010178-OOIA
Project:
Sanford WWTP
Client Sample ID Sanford WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury ND
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
ND
TCLP Barium(Ba)
ND
TCLP Cadmium(Cd)
ND
TCLP Chromium(Cr)
ND
TCLP Lead(Pb)
ND
TCLP Selenium(Se)
ND
TCLP Silver(Ag)
ND
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
ND
2,4,5-Trichlorophenol
ND
2,4,6-Trichlorophenol
ND
2,4-Dinitrotoluene
ND
Cresols, Total
ND
Hexachloro-1,3-butadiene
ND
Hexachlorobenzene
ND
Hexachloroethane
ND
Nitrobenzene
ND
Pentachlorophenol
ND
Pyridine
ND
Surr: 2-Fluorophenol
80.6
Surr: Phenol-d6
87.2
Surr: Nitrobenzene-d5
65.1
Surr: 2,4,6-Tribromophenol
95.0
Surr: 2-Fluorobiphenyl
61.6
Surr: p-Terphenyl-d14
93.2
SW7470A SW7470A Analyst: KLC
0.00200 mg/L 1 1/7/20224:59:00 PM
SW6010 SW301OA Analyst: MSK
0.500
mg/L
1
1/10/2022 11:25:00
AM
5.00
mg/L
1
1/10/2022 11:25:00
AM
0.100
mg/L
1
1/10/2022 11:25:00
AM
0.200
mg/L
1
1/10/2022 11:25:00
AM
0.500
mg/L
1
1/10/2022 11:25:00
AM
0.0500
mg/L
1
1/10/2022 11:25:00
AM
0.500
QL+ mg/L
1
1/10/2022 11:25:00
AM
SW8270 SW351OC Analyst: SFG
0.200
mg/L
2
1/13/2022 7:46:00 PM
0.500
mg/L
2
1/13/2022 7:46:00 PM
0.500
mg/L
2
1/13/2022 7:46:00 PM
0.100
mg/L
2
1/13/2022 7:46:00 PM
10.0
mg/L
2
1/13/2022 7:46:00 PM
0.0400
QC+ mg/L
2
1/13/2022 7:46:00 PM
0.100
mg/L
2
1/13/2022 7:46:00 PM
0.200
mg/L
2
1/13/2022 7:46:00 PM
0.200
mg/L
2
1/13/2022 7:46:00 PM
0.500
mg/L
2
1/13/2022 7:46:00 PM
0.500
QC- mg/L
2
1/13/2022 7:46:00 PM
10 - 157
%Rec
2
1/13/2022 7:46:00 PM
10 - 169
%Rec
2
1/13/2022 7:46:00 PM
32.1 - 130
%Rec
2
1/13/2022 7:46:00 PM
45.4 - 166
%Rec
2
1/13/2022 7:46:00 PM
35.7 - 130
%Rec
2
1/13/2022 7:46:00 PM
70 - 145
%Rec
2
1/13/2022 7:46:00 PM
Qualifiers: B
Analyte detected in the associated Method Blank
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
OG 1
PL Permit Limit Original
RL Reporting Detection Limit
Page 7 of 36

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arrafyt9caf Laboralorfas TEL: [phone] FAX. [phone]
Website: http://�i,-"-m,.settek.coin
Analytical Report
(base report)
WO#: 22010178
Date Reported: 1/14/2022
CLIENT:
Synagro Tag Number:
Matrix:
SLUDGE Collection Date: 1/4/2022 1:15:00 PM
Lab ID:
22010178-OOIA
Project:
Sanford WWTP
Client Sample ID Sanford WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total
ND
Toxaphene
ND
Endrin
ND
gamma-BHC
ND
Heptachlor
ND
Heptachlor epoxide
ND
Methoxychlor
ND
Surr: TCMX
43.6
Surr: DCB
69.1
TCLP HERBICIDES BY EPA 8321B
2,4-D ND
2,4,5-TP ND
Surr: 2,4-Dichlorophenylacetic aci 96.6
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
1,2-Dichloroethane
ND
MEK
ND
Benzene
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroform
ND
Tetrachloroethene
ND
Trichloroethene
ND
Vinyl chloride
ND
Surr: 4-Bromofluorobenzene
96.6
Surr: Di brom ofl uorom ethane
101
Surr: Toluene-d8
101
SW8081 SW351OC Analyst: CSS
0.0250
mg/L
10
1/13/2022 12:25:00 AM
0.0500
mg/L
10
1/13/2022 12:25:00 AM
0.00500
mg/L
10
1/13/2022 12:25:00 AM
0.00500
mg/L
10
1/13/2022 12:25:00 AM
0.00500
mg/L
10
1/13/2022 12:25:00 AM
0.00500
mg/L
10
1/13/2022 12:25:00 AM
0.00500
mg/L
10
1/13/2022 12:25:00 AM
10 - 119
%Rec
10
1/13/2022 12:25:00 AM
10 - 119
%Rec
10
1/13/2022 12:25:00 AM
S W 8321
Analyst: RIS
0.500
mg/L
50
1/12/2022 12:20:00 AM
0.500
mg/L
50
1/12/2022 12:20:00 AM
70 - 130
%Rec
50
1/12/2022 12:20:00 AM
SW8260
SW1311M
Analyst: NAW
0.500
mg/L
100
1/7/2022 8:56:00 PM
0.500
mg/L
100
1/7/2022 8:56:00 PM
10.0
mg/L
100
1/7/2022 8:56:00 PM
0.500
mg/L
100
1/7/2022 8:56:00 PM
0.500
mg/L
100
1/7/2022 8:56:00 PM
5.00
mg/L
100
1/7/2022 8:56:00 PM
0.500
mg/L
100
1/7/2022 8:56:00 PM
0.500
mg/L
100
1/7/2022 8:56:00 PM
0.500
mg/L
100
1/7/2022 8:56:00 PM
0.200
mg/L
100
1/7/2022 8:56:00 PM
70 - 130
%Rec
100
1/7/2022 8:56:00 PM
70 - 130
%Rec
100
1/7/2022 8:56:00 PM
70 - 130
%Rec
100
1/7/2022 8:56:00 PM
Qualifiers: B
Analyte detected in the associated Method Blank
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
OG 1
PL Permit Limit Original
RL Reporting Detection Limit
Page 8 of 36

MMIT
Summit Environmental Technologies, Inc. Analytical Report
SU3310 Win St.
ENVIRONMENTAL TECHNOLOGIE-3, IRC Cuyahoga Falls, Ohio 44223 (base report)
Arralyt9cal Laboralorfas TEL: [phone] FAX.- [phone] WO#: 22010178
Website: http://www.settek.com Date Reported: 1/14/2022
CLIENT:
Synagro Tag Number:
Matrix:
SLUDGE Collection Date: 1/4/2022 1:15:00 PM
Lab ID:
22010178-OOIA
Project:
Sanford WWTP
Client Sample ID Sanford WWTP
Analyses
Result
RL Qual Units
DF
Date Analyzed
RCI
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive
ND
0.495 mg/Kg
1
1/10/2022 11:41:00 AM
IGNITABILITY OF SOLIDS (SW-846: 1030)
SW1030
Analyst: ALT
Ignitability nonflammable
mm/sec
1
1/7/2022 2:56:08 PM
PERCENT SOLIDS BY SM2540MOD
A2540B
Analyst: DHC
Percent Solids
4.38
%
1
1/10/2022 3:50:00 PM
RCI
SW9045D
Analyst: ALT
PH (SW9045D)
pH
6.9
s.u.@19.7C
1
1/7/20224:13:17 PM
RCI
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive
ND
25.0 mg/Kg
1
1/10/2022 11:41:00 AM
Qualifiers: B
Analyte detected in the associated Method Blank
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
OG 1
PL Permit Limit Original
RL Reporting Detection Limit
Page 9 of 36

Summit Environmental Technologies, Inc.
Accreditation
Program
SUMMIEF
fr3310 Win St.
Analv n tes Report
ENwIROMMEWALYECHNOL.OG{r,S,INC
Cuyahoga Falls, Ohio44223
J
Y
Arraly0cal Laboralorlas
TEL: [phone] FAX.- [phone]
Wo#:
22010178
Wehsite: http://www.settek.com
14 Jan-22
Client: Synagro
State: NW
Project: Sanford WWTP
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
22010178-OOIA Sludge
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Sludge
Percent Solids by SM2540Mod
Percent Solids
N
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Sludge
TCLP Herbicides by EPA 8321B
2,4,5-TP
A
Sludge
TCLP Herbicides by EPA 8321B
2,4-D
A
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Version #2
Page 10 of 36

Summit Environmental Technologies, Inc.
Accreditation
Program
SUMMIEF
fr3310 Win St.
Analv n tes Report
EMOROMMEWAL YECHHOL.OG{r,S,
INC Cuyahoga Falls, Ohio 44223
J
Y
Arraly0cal Laboralorlas
TEL: [phone] FAX.- [phone]
Wo#:
22010178
Wehsite: http://www.settek.com
14 Jan-22
Client: Synagro
State: NW
Project: Sanford WWTP
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
22010178-OOIA Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Sludge
TCLP Volatiles Analysis
1, 1 -Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chloroform
A
Sludge
TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge
TCLP Volatiles Analysis
Trichloroethene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
Version #2
Page 11 of 36

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Page 35 of 36

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHN❑L4Ga1�S.IfiC Cuyahoga Falls, Ohio44223 Sample Log -In Check List
Arrafocaf Laboralorias TEL: [phone] FAX.- [phone]
Website: http://`h,,",m,.settek.coin
Client Name: SYN-NC-27028 Work Order Number: 22010178 RcptNo: 1
Logged by: Jacqueline Rasile
Completed By: Jacqueline Rasile
Reviewed By: Jennifer Woolf
1/5/2022 10:15:00 AM
1/6/2022 12:51:42 PM
1/6/2022 1:47:07 PM
Chain of Custody
1. Is Chain of Custody complete? Yes ❑d No ❑ Not Present ❑
2. How was the sample delivered? FedEx
Lop In
3. Coolers are present? Yes ❑d No ❑ NA ❑
4. Shipping container/cooler in good condition? Yes d❑ No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present V
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes ❑d No ❑ NA ❑
6. Were all samples received at a temperature of >0° C to 6.0°C Yes ❑d No ❑ NA ❑
7. Sample(s) in proper container(s)?
Yes
❑d
No
❑
8. Sufficient sample volume for indicated test(s)?
Yes
❑d
No
❑
g. Are samples (except VOA and ONG) properly preserved?
Yes
❑d
No
❑
10. Was preservative added to bottles?
Yes
❑
No
❑d NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
❑
No
❑ No VOA Vials ❑�
12. Were any sample containers received broken?
Yes
❑
No
❑d
13. Does paperwork match bottle labels?
Yes
No
❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
❑d
No
❑
15. Is it clear what analyses were requested?
Yes
❑d
No
❑
16. Were all holding times able to be met?
Yes
No
❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
❑
No
❑ NA V
Person Notified: Date:
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Rec'd by Tegan Richards
Cooler Information
Cooler No
Temp °C
Condition
I Seal Intact
Seal No
Seal Date
Signed By
1
10.5
Goodl
Not Present
Page 36 of 36

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: _City of Sanford WQ Permit Number: WO0000543
WWTP Name: Big Buffalo WWTP NPDES Number: NCO024147
Monitoring Period; From 01/01/22 To 03/31/22
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1 I06) - Please indicate level achieved and alternative performed:
Class A:
Alt. I/A (time/temp) Alt. 21B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment ThermophiIic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annlicahle to ulternafivw —fnr .1 if 1— A — d`1., � n% .. ..�...,..�.., r..u.....:__ _ _�_.__
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Minimum Geo. Mean Maximum Units
Excec-
dences
of
Analysis
Type
Technique
Fecal
Coliform
2x 10 to the 61h
power per gram
of total solids
CFU
510000
693000
1360000
CFU/g
U
Quarterly
Grab
SM9222D
-MF
MPN
MPN/g
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 Lion/Alt. 1
Option/Alt.2
Option/Alt.3 Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/AIt. 5
(14-Day Aerobic)
Option/Alt. 6
(Alk Stabilization)
Option/Alt. 7 Option/Alt. 8
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement to 40 CFR 503,33/15A NCAC 02T.] 107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.I 106 and the vector attraction
reduction requirement to 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that them pathogen and vector attraction reduction requirements have
been met. I aaware that there are significant penalties for false certification including fine and imprisonment."
Scott Siletzky, WWTP Superintendent
Pr parer Name MTtlpe or print) Land Applier Name and Title (if applicable) (type or print)
a`i 15
Signature of Preparqof,-1 'Datt Signature of Land Applier (if applicable) Date
'Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1 102 (26)

Cameron Testing Services, Inc. Laboratory Report
NCDENR#654
NC PHHS #37799
US EPA #NC01918
Synagro
CTS Prof.
2201-0015
DW Cert # 37799
Proj13C :
Sanford WWTP
Regulatory
Yes
Sample Information
Sample
C. Wynne
Bate 01/04/22
Received
J.
Cameron Date
01/04/22
Analyses and Results
Lab ID
Sample ID
o m
;� o 2 Analyte
Result:
E
a `-
m
�' 4
Std. Methods
c� t?
_J
o
Reference
a
2201-0015
-01
3ludgE Gr Fec. Coliform-S
802000
CFu/g
72900
01/05/22 05C
9222D - MF
-02
527000
CFulg
65900
-03
510000
CFulg
63700
-04
515000
CFUlg
63300
-05
877000
CFUrg
73100
-06
1360000
CFUrg
64500
-07
577000
CFUrg
64100
Geomean
693000
2201-0015
-01
31udgE Gr TS (%)
4.60%
0.01
01/04/22 KW
2540 G -TS
-02
4.80%
0.01
-03
4.90%
0.01
-04
4.50%
0,0i
-05
4.50%
001
-06
4.60%
oot
-07
4.60%
0.01
Report
Review
Project Manager Date
219 S. Steele Str. 919-208-4240
Sanford NC 27330 [e-mail] camerontesting.com

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Sanford WQ Permit Number: WQ0000543
WWTP Name: Big Buffalo WWTP NPDES Number: NCO024147
Monitoring Period: From 04/01/22 To 06/30/22
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. VA (time/tomp) Alt. 2/8 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophiiic
Beta Ray Gamma Ray Pasteurization
Class H.
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class R only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
rr o .1 Dahl. 4n sa rri- A ri___ n.
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Minimum Geo. Mean Maximum Units
Excee-
dences
of
Analysis
Type
Technique
Fecal
Coliform
2x10to the 61'
power per gram
of total solids
CFU
530000
1030000
2060000
CFU/g
0
Quarterly
Grab
SM9222D
-MF
MPN
MPN/g
1000 MPN per gram of
%Mp''ra
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
Option/Alt. 3 Option/AIt. 4
(yS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(I 4-Day Aerobic)
(Alk Stabilization)
(Drying— Stable) (Drying --Unstable)
Option/Alt. 9
Option/Alt. 10
(injection)
(incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"1 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T_ 1106 and the vector attraction
X reduction requirement in 40 CPR 503.33/I5A NCAC 02T.1107 have been met."
"9 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel property gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Scott Siletzky, WWTP SuRRrintendent
Preparer Name and Title (type or print)
Signature of Prep DaFe
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Pan 503.9(r) and 15A NCAC 2T.1102 (26)

Cameron Testing Services, Inc. Laboratory Report
NC DENR 9654
NC PHHS #37799
US EPA #NC01918
Client:
Synagro CTS Proj.
22Q4_0025
DW Cert# 37799
Project:
Sanford WWTP Regulatory
Yes
Sample Information
Sampled
C. Wynne
Date 04/04/22 Received
J.
Cameron Date
04/04/22
Analyses and Results
Lab 1D
Sample ID
p
M E
p Analyte Result
E
y
a l=
U .�
Std. Methods
-�
c ❑ S
Reference
2204-0025
-01
' UCgE Gr Fec. Coliform-S 578000
CFU/9
578000
04/05/22 CSC
9222D - MF
-02
1070000
CFU7g
534000
-03
2060000
CFUrg
685000
-04
595000
CFU19
595000
-05
530000
CFUIg
530000
-06
1780000
CFurg
592000
-07
1750000
CFU/g
582000
Geomean 1030000
2204-0025 01
-01
Sludge Gr TS (%) 4.5
%
0,01
04/07/22 CSC
2540 G -TS
-02
4.5
%
001
-03
4.5
%
0.01
-04
4.5
%
0.01
-05
4.5
%
0.01
-06
4.4
%
0.01
-07
4.5
%
0.01
Report
Review
Project Manager I, Date r
oC!/C�5
219 S. Steele Str. 919-208-4240
Sanford NC 27330 Chris@.camerontesting.com

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Ci� ofSanford WQ Permit Number. WQ0000543
WWTP Name: Big Buffalo WWTP NPDES Number: NCO024147
Monitoring Period: From 07/0122 To 09/30/22
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt, I/A (time/temp) Alt. 21B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt, 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt, 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta stay Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class 8 only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Ir annlirahla fn 9t+arnnfiv., .,or£ .-.....d �C1...... ♦ ..-!`l...... ni _ _�_._ a_ r_n___.e__—__�___�_ _
Parameter
Allowable Level in Sludge
Pathogen Density
No_ of
Frequency
Sample
Analytical
Minimum Geo. Mean Maximum Units
Excee-
deuces
of
Analvsis
Type
Technique
Fecal
Coliform
2x10to the 601
power per gram
of total so I i ds
CM
99600
180000
447000
CPU/g
0
Quarterly
Grab
SM9222D
-MF
VTPN
MPN/g
1000 MPN per gram of
total solids (dry weight)
MPN/g
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed-
0 ption/Alt. 1
(VS reduction)
Option/Alt. 2
(40-day bench)
Option/Alt, 3 Option/Alt. 4
(30-day bench) X (Spec. 02 uptake)
0ption/Alt. 5
(14-Day Aerobic)
Option/Alt. 6
(Alk Stabilization)
Option/Alt. 7 Option/Alt. 8
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the ppathogen requirements in 40 CFR 503.32/15A NCAC 02T.] 106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Scott Siletzky, WWTP Superintendent
Preparer Name and Tit (type or print)
a Is 13
Signature of Prepar Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Cameron Testing Services, Inc. Laboratory Report NC DENR#654
NC PHHS #37799
US EPA #NC01918
Client: Synagro CTS Prof. 2208-0210 DWCert#37799
Project: Sanford VWVTP Regulatory Yes
Sample Information
Sampled C. Wynne Date 08/22/22 _Receives J. Cameron Date 0$I22122
Analyses and Results
;. E c '"�' y Std. Methods
Lab ID Sample ED o Analyte Result E ru ro
c� 1 Q S Reference
2208-0210 -01 3ludgE Gr Fec. Coliform-S 447000 CFUrg 112000 08/23/22 ERP 9222❑ - MF
-02 <113000 CFUrg 113000
-03 350000 CFUrg 117000
-04 110000 CFUrg 110000
-05 107000 CFUrg 107000
-06 304000 CFUrg 101000
-07 98600 CFUrg 98600
Geomean 180000
2208-0210 -01 Sludge Gr TS (%) 4.30% 0.01 08/23/22 ERP 2540 G -TS
-02 4.39% 0.01
-03 4.37% 0.01
-04 4.45% 0.01
-05 4.41 % 0.01
-06 4.39% 0.01
-07 4.39% 0.01
Report
Review D G 2 .. f CV rj
Project Manager Date 4 aV'T U D�
219 S. Steele Str, 919-208-4240
Sanford NC 27330 [e-mail]

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ANNUAL PATHOGLI AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: CityofSanford
WWTPName: _Big Buffalo WWTP
Monitoring Period: From 10/01/22
To 12/31/22
WQ Permit Number: WQ0000543
NPDES Number: NCO024147
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. I/A (timc/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/17 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class H:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If anntirnhln to altarnafiv narfnr A K'looa A ...-Rl ..w...-J......L- e.. n.....:....... _ .�_._.
Parameter
A]low•able Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Minimum Gco. Mean Maximum Units
Excec-
dences
of
Analysis
Type
Technique
Fecal
2x lO to the 6d,
CFU
23500
129000
386000
CFU/g
0
Quarterly
Grab
SM9222D
Coliform
power per gram
-MF
of total solids
MPN
MPN/g
1000 MPN per gram of
MPti/a
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying -- Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, raider penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
Xr reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met"
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement to 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Scott Siletzky, W WTP Superintendent
Preparer Name and Title( pe or print)
f � Is s3
Signature ofPreparer-45 4 ate
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and I5A NCAC 2T.1102 (26)

Cameron Testing Services, Inc. Laboratory Report NC DENR #654
NC PHHS #37799
US EPA #NC01918
Client: Synagro CTS Proj, 2210-0010 DW Carl # 37799
Project: Sanford WWTP Regulatory Yes
Sample Information
Sampled
C. Wynne
Date
10/03/22
Received
J.
Cameron
Date
10/03/22
Analyses and Results
Lab ID
Sample ID
P
L E
o
Analyte
Result
�
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ri "—'
m
T
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iv
,:
Std. Methods
c> t?
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Reference
2210-0010
-01
judge Gr
Fee. Coliform-S
199000
CFUIg
9940C
10/04/22
CSC
9222D - MF
-02
93000
CFUIg
4650C
-03
23500
CFUrg
2350C
-04
126000
CFUIg
126000
-05
386000
CFUrg
129000
-06
299000
CFUIg
150000
-07
<92200
CFurg
92200
Geomean
129000
2210-0010
-01
>iudge Gr
TS (%)
0.700%
0.01
10/03/22
CSC
2540 G -TS
-02
2,15%
0.01
-03
3.94%
0.01
-04
0.760%
0.01
-05
0.690%
0.01
-06
0.620%
0.01
-07
0.980%
001
Report
Review
Project Manager
Data
219 S, Steele Str. 919-208-4240
Sanford NC 27330 [e-mail]

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SECTION 6

Agricultural Lime Application Log
Year: 2022
Project: Sanford WWTP
Field
(state -county -site -field)
Soil
pH
Lime Requirement
(from soil analysis)
Tons/Acre
Applied
Date Applied
NC-CH-49-5
6.1
0.0
0.0
NC-CH-49-6
6.1
0.0
0.0
NC-CH-49-7
5.8
0.5
0.0
NC-CH-49-8
5.9
0.3
0.0
N C-C H-72-1
6.1
0.0
0.0
NC-CH-72-3
6.1
0.0
0.0
NC-CH-60-4
6.0
0.0
0.0
NC-CH-60-6
6.8
0.0
0.0
N C-C H-66-1
5.5
1.1
0.0
NC-CH-66-2
5.6
0.8
0.0
NC-CH-66-3
5.6
1.0
0.0
NC-CH-66-4
5.8
0.6
0.0
NC-CH-66-6
5.3
1.3
0.0
NC-CH-73-10
6.2
0.0
0.0
NC-CH-77-4
6.1
0.0
0.0
NC-CH-77-5
5.7
0.6
0.0
NC-CH-77-6
6.1
0.0
0.0
NC-CH-77-7
6.1
0.0
0.0
N C-C H-77-8A
6.0
0.0
0.0
NC-CH-77-8B
5.5
0.9
0.0
NC-CH-77-9
6.2
0.0
0.0
NC-CH-77-10
6.1
0.0
0.0
NC-CH-77-11
5.5
0.0
0.0
NC-CH-77-12
6.0
0.0
0.0
NC-CH-77-13
6.3
0.0
0.0
NC-CH-77-14
5.6
0.9
0.0
NC-CH-77-15
6.8
0.0
0.0
NC-CH-77-16
5.8
0.5
0.0
NC-CH-77-17
6.0
0.0
0.0
NC-CH-77-18
5.6
0.0
0.0
N C-C H-78-1
6.1
0.0
0.0
NC-CH-78-2
6.1
0.0
0.0
NC-CH-101-7
5.7
0.5
0.0
NC-CH-101-13
5.7
0.5
0.0
NC-CH-101-14
5.8
0.4
0.0
NC-CH-101-15
5.7
0.5
0.0

SECTION 7

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