WQ0012346_2022 Residual Annual Report_20230223 (2)

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * WQ0012346
Applicant/Permittee US MCB Camp Lejeune
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Wilmington
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Travis Voorhees
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
910-451-9518
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:* WQ0012346
Has Current Existing permit number
Applicant/Permittee Address* Commanding General ATTN:EMD 12 Post Lane Camp Lejeune, NC 28547-2540
Facility Name* US MCB Camp Lejeune Class A Residuals Program
Please provide comments/notes on your current submittal below.
Please see the attached annual report for Marine Corps Base Camp Lejeune. All comments are provided in the report cover letter.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2022 CAMP LEJEUNE CLASS A WASTEWATER
6.38MB
RESIDUALS APPLICATION ANNUAL REPORT.pdf
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/23/2023

CLASS "A" WASTEWATER RESIDUALS
APPLICATION ANNUAL REPORT
YEAR 2022
UNITED STATES
MARINE CORPS BASE
CAMP LEJEUNE, N. C.
PERMIT NO. WQ0012346
Enclosure (1)

CLASS "A" WASTEWATER
RESIDUALS APPLICATION ANNUAL
REPORT FOR THE YEAR 2022
MARINE CORPS BASE, CAMP
LEJEUNE PERMIT NO. WQ0012346
• Cover Letter.....................................................................
• Class A Annual Distribution and Marketing/Surface Disposal
Certification and Summary Form (Form DMSDF)........................
• Annual Residuals Sampling Summary Forms
(Forms RSSF & RSSF-B)......................................................
• Residuals Analysis Lab Sheets including TCLP Lab Sheets ...............
Annual Pathogen & Vector Attraction Reduction Forms
• (Form PVRF 2T) and Vector Attraction Reduction Lab Sheets .............
SECTION I
SECTION 2
SECTION 3
SECTION 4
SECTION 5

Application to Forested Sites
Application to TLZ Training Areas
°r Mir,.kvJ
Camp Lejeune Advanced Wastewater Treatment Plant Transferring Biosolids from Tanker to Applicator
ATAD Facility

SECTION 1
Cover Letter

UNITED STATES MARINE CORPS
MARINE CORPS INSTALLATIONS EAST —MARINE CORPS BASE
PSC BOX 20005
CAMP LEJEUNE NC 28542-0005
5090.20.1
G-F/BEMD
FEB 14 2023
Mr. Nathaniel Thornburg
North Carolina Department of
Environmental Quality
Division of Water Resources
Non -Discharge Permitting Branch
1617 Mail Service Center
Raleigh, North Carolina 27699 1617
Dear Mr. Thornburg:
In accordance with requirements of 15A NCAC 02T, enclosure (1)
forwards Marine Corps Base Camp Lejeune's (MCB CAMLEJ) Class "All
Wastewater Residuals Application Annual Report for the Year 2022.
The forms in this report were prepared by Charles "Sonny" Scozzari,
MCB CAMLEJ Wastewater and Land Application Supervisor, for the
Permittee Robert A. Lowder, Director, Environmental Management
Division (EMD) .
In the fourth quarter of 2022, two (2) Autothermal Thermophilic
Aerobic Digestor weekly residual sample results for pathogen
reduction were above the allowable fecal coliform density limit. MCB
CAMLEJ did not land apply any residuals with fecal analyses above the
allowable limit.
If you have any questions please contact Mr. Travis Voorhees,
Environmental Quality Branch, EMD, at [phone].
ncerelybnvi
r
R A. P.E.
Director,mental Management
By direct
the Commanding General
Enclosure: 1. Class "A" Wastewater Residuals Application
Annual Report Year 2022
Copy To:
File (ODI# 27391)

SECTION 2
Class A Distribution & Marketing/Surface
Disposal Certification & Summary Forms
(Form DMSDF)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0012346 FACILITY NAME: U.S. MARINE CORPS BASE CAMP LEJEUNE
PHONE: [phone]OX232 COUNTY: ONSLOW OPERATOR: CHARLES "SONNY" SCOZZARI
FACILITY TYPE (please check one): © Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
❑ Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes El No © —* If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Reci Tent Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
CAMLEJ AWWTP NCO063029
41.09
February
CAMLEJ AWWTP NCO063029
92.68
March
CAMLE] AWWTP NCO063029
23.87
April
CAMLEJ AWWTP NCO063029
16.33
May
CAMLEJ AWWTP NCO063029
8.05
June
CAMLEJ AWWTP NCO063029
43.21
July
CAMLEJ AWWTP NCO063029
56.49
August
CAMLEJ AWWTP NCO063029
65
September
CAMLE] AWWTP NCO063029
61.13
October
CAMLEJ AWWTP NCO063029
32.43
November
CAMLEJ AWWTP NCO063029
18.71
December
CAMLEJ AWWTP NCO063029
6.47
Total from FORM DMSDF (sup)
Totals:
I Annual (dry tons):
0
465.46
0
0
Amendments used: I Bulking A ent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)l 0
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit © Yes
(including but not limited to items 1-3 below) issued by the Division of Water Resources: © No P It No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2 All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources.
1. No contravention cif Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief ,ruq accurate and complete. I am aware that there are significant
penalties for submitting f information, including the possibility of fines and imprisonment fo owi violations."
ilk� 7 =116&1
`6 I. f Per t�/
ate Signatu f Preparer** Date
(if diff nt from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM DMSDF (1212006)

2022 Camp Lejeune Class A Residuals Application Report Sugar Water Report
TRAIN 1
TRAIN 2
TRAIN 3
TRAIN 4
DATE
A B
AMOUNT
DATE
A B
AMOUNT
DATE
A B
AMOUNT
DATE
A B
AMOUNT
1/5/2022
B
250 GAL
1/28/2022
B
250 GAL
4/6/2022
A
250 GAL
9/26/2022
A
250 GAL
2/2/2022
B
250 GAL
4/6/2022
B
250 GAL
9/26/2022
B
250 GAL
2/14/2022
B
250 GAL
4/13/2022
B
250 GAL
10/6/2022
A
250 GAL
2/28/2022
B
250 GAL
4/19/2022
A
250 GAL
10/6/2022
B
250 GAL
3/2/2022
B
250 GAL
4/19/2022
A
250 GAL
10/19/2022
A
250 GAL
10/6/2022
B
250 GAL
6/30/2022
B
250 GAL
10/19/2022
B
250 GAL
12/2/2022
A
250 GAL
7/13/2022
A
250 GAL
12/2/2022
A
250 GAL
12/8/2022
A
250 GAL
7/13/2022
B
250 GAL
12/2/2022
B
250 GAL
12/8/2022
A
250 GAL
12/8/2022
B
250 GAL

SECTION 3
Annual Residuals Sampling Summary Forms
(Forms RSSF & RSSF-B)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0012346
Facility Name:
Residual Source WQ # or
NPDES #:
U.S. MCB CAMP LEJEUNE
0401011 t
WWTP Name: Camp Lejeune Advanced WWTP
Residual Analvsis Data
Laboratory: 1) Camp Lejeune ELS
2) Environmental Chemists, Inc.
3)
4)
5)
II�
Parimit
ameter -
Conc.
_ -
Sampleor • •• Date
M
•
®M.M-.M.M
• .. -III
i i
®®'
��_-.-.■-___-,
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under
to assure that qu
penalties for sub
D
Signature ofyKeplim
law, that this document was prepared under my direction or supervision in accordance with a system designed
►onnel properly gathered and evaluated the information submitted. I am aware that there are significant
ie information, including the possibility of fines and imprisonment for knowing violations."
GZ
Date
defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF {12/2006}

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQOO 12346
Facility Name: U.S. MCB Camp Lejeune
Residual Source
NPDES # or WQ#:
NCO063029
WWTP Name: Camp Lejeune Advanced WWTP
Residual Analysis Data
Laboratory: 1) MCB Camp Lejeune ELS
2) Environmental Chemists, Inc.
3)
4)
5)
Parameter
(mg/kg)
Sample- or- Composite Date
®®®®-uuuuu,uuuuu,uuuuu,u.--uuuu�
KIM$
-Magnesium
Potassium
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties fqp<53mitting false information, including the possibility of fines and imprisonment for knowing violations."
id
Signature of P4arer bate
in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
111:1 g I a 101 mm I vwg = -,JjJ

SECTION 4
Residuals Analysis Lab Sheets
including TCLP Lab Sheets

TCLP Analysis Lab Sheets

[env7irochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
USMC Camp Lejeune
G-F/EMD/ECB -12 Post Lane
Camp Lejeune NC 28547
Attention: Lauren Acosta
Date of Report: Mar 15, 2022
Customer PO #:
Customer ID: 12060026
Report #: 2022-03388
Project ID: T4B
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-07985 Site: T413
2/22/2022
8:39 AM Solid/Sludge Julius Acosta
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
3.34 %
02/24/2022
Chlordane (TCLP)
SW-846 8081 B
<0.02 mg/L
02/28/2022
Endrin (TCLP)
SW-846 8081 B
<0.0005 mg/L
02/28/2022
Heptachlor (TCLP)
SW-846 8081 B
<0.0005 mg/L
02/28/2022
Heptachlor epoxide (TCLP)
SW-846 8081 B
<0.0005 mg/L
02/28/2022
Lindane (TCLP)
SW-846 8081 B
<0.0005 mg/L
02/28/2022
Methoxychlor (TCLP)
SW-846 8081 B
<0.0005 mg/L
02/28/2022
Toxaphene (TCLP)
SW-846 8081 B
<0.05 mg/L
02/28/2022
2,4,5-TP (TCLP)
SW-846 8151 A
<0.003 mg/L
03/02/2022
2,4-D (TCLP)
SW-846 8151 A
<0.003 mg/L
03/02/2022
1,4-Dichlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
03/01/2022
2,4,5-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
03/01/2022
2,4,6-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
03/01/2022
2,4-Dinitrotoluene (TCLP)
SW-846 8270 E
<0.050 mg/L
03/01/2022
Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
03/01/2022
Hexachloro-1,3-butadiene (TCLP)
SW-8468270E
<0.050mg/L
03/01/2022
Hexachlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
03/01/2022
Hexachloroethane (TCLP)
SW-846 8270 E
<0.050 mg/L
03/01/2022
m + p-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
03/01/2022
Nitrobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
03/01/2022
o-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
03/01/2022
Pentachlorophenol (TCLP)
SW-846 8270 E
<0.250 mg/L
03/01/2022
Pyridine (TCLP)
SW-846 8270 E
<0.050 mg/L
03/01/2022
1,1-Dichloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
03/02/2022
1,2-Dichloroethane (TCLP)
SW-846 Method 8260D
<0.01 mg/L
03/02/2022
Benzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
03/02/2022
Report #:: 2022-03388 Page 1 of 2

r-
77 1
• -
ANALYTICAL & CONSULTING CHEMISTS
USMC Camp Lejeune
G-F/EMD/ECB -12 Post Lane
Camp Lejeune NC 28547
Attention: Lauren Acosta
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Mar 15, 2022
Customer PO #:
Customer ID: 12060026
Report #: 2022-03388
Project ID: T4B
Carbon Tetrachloride (TCLP)
SW-846 Method 8260D
<0.01 mg/L
03/02/2022
Chlorobenzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
03/02/2022
Chloroform (TCLP)
SW-846 Method 8260D
<0.01 mg/L
03/02/2022
Methyl ethyl ketone (TCLP)
SW-846 Method 8260D
<0.05 mg/L
03/02/2022
Tetrachloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
03/02/2022
Trichloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
03/02/2022
Vinyl Chloride (TCLP)
SW-846 Method 8260D
<0.01 mg/L
03/02/2022
RCI
Cyanide
SM 4500 CN D-2016
1.60 mg/kg
03/01 /2022
Sulfide
SM 4500 S D
< 1.00 mg/kg
03/03/2022
Ignitability
SW 846 method 1010
>157 °F
03/07/2022
pH
SW 846 Method 9045D
8.70 units
03/14/2022
Result estimated. Analyzed out of
15 minutes hold time.
TCLP Metals
Arsenic
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
02/28/2022
Barium
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
02/28/2022
Cadmium
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
02/28/2022
Chromium
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
02/28/2022
Lead
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
02/28/2022
Selenium
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
02/28/2022
Silver
EPA 200.7, Rev.4.4, 1994
<1.Omg/L
02/28/2022
Mercury
EPA 245.1
<0.0002 mg/L
02/28/2022
Comment:
Reviewed by:
Report #:: 2022-03388 Page 2 of 2

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
9
qMM i R 10.392.0223
p e eceipt CheCKIISt
Client: ate:
Date: e�— Report Number: _ 2022- O 3 g
Receipt of sample: ECHEM Pickup Client Delivery ❑ UPS ❑
❑ YES ❑ NO FeclEx ❑ Other ❑
N/A I. Were custody seals present on the cooler?
❑ YES ❑ NO N/A . If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt
How temperature taken: ❑ Temperature Blank
IR Gun ID: Thomas Traceable S/N: 210835468 IR Gun Correct, ngFactoB c. 0
❑ YES ❑ NO 3. If temperature of cooler exceeded 6°C, was Project M r.
YES ElNO 4. Were proper custody procedures (relinquished/received) followefd?d7
YES ❑ NO 5. Were sample ID's listed on the COC?
YES ❑ NO 6. Were samples ID's listed on sample containers?
YES ❑ NO 7. Were collection date and time listed on the COC?
YES ❑ NO 8. Were tests to be performed listed on the COC?
YES ❑ NO 9. Did samples arrive in proper containers for each test?
YES ❑ NO 10. Did samples a -rive i -1 eoo i o�n iti�n ir-ir a�' —
Y�5 r, :es:?
'�' �❑ NO 11 �,�ras adequate sample V911.1me avai!ab!�?
P( YES ❑ NO 12. Were samples received within proper holding time for requested tests?
❑ YES ❑ NO 13. Were acid preserved samples received at a pH of <2?
❑ YES ❑ NO 14. Were cyanide samples received at a pH >12?
❑ YES ❑ NO 15. Were sulfide samples received at a pH >9?
❑ YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L?x
❑ YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any samples) incorrect)
Sample(s) y preserved or with headspace)
were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation; If more than one preservative is needed, notate in comments below
Not Notify customer service immediately for incorrectly preserved samples. Obtain anew sample or
-lotify the state lab if directed to analyzed by the customer. who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
'C
DOC. QA.002 Rev 1

6602
Wind
Way
ngton
ENVIRONMENTAL CHEMISTS, INC OFFICE: 9101-392-0223F'AX910-3 2� 4
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLFCTION AND CHAIN nF CIISTnDY
CLIENT: Commandina General
PROJECT NAME: Camp Lejeune MCB
REPORT NO: Z Z ^ O 3
ADDRESS: G-F/EMD/EQB/Environmental Lab
CONTACT NAME: Lauren Acosta
PO NO: Contract No. N4008519D8037
12 Post Lane
REPORT TO: Lauren Acosta
PHONEIFAX: 910-451-0020 (fax) 910-451-7195
Camp Lejeune NC 28547
COPY TO:
email: [e-mail]
Sampled By: ul'wS Ac_os+ct SAMPLE TYPE: I = Influent E = Effluent W = Well_ ST = Strpam_ Sn = Snil_ SI = Slurinp (lthor-
r
Sample Identification
Collection
m
E;
E>
w
m
a o
E
ci
m_
o
V
m
o �,
" E
ow
m m
g z
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
�,
Z
,
p
i
o
=
-_
o
_
a
o
rz2
-�Tl
SL
C
P
q p
/ O
TCLP - Volatile, Semi -volatile,
Pesticides Herbicides RCRA 8 metals
G
P
Reactivity, Corrosivity, Ignitability
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Transfer
Relinquished By:
DateTme
Rec ived By:
D te/Time
1
b%
:� s?�2
2.
O
rmNGrawre ep meceivea: a Acceptecl: Rejected: Resam Re uested:
Delivered B Received By: �Da ZZ Time:
Comments: TUR AROUND:

1ST QUARTER
Residuals Analysis lab Sheets

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
12 Post Lane, Camp Lejeune, NC 28547
Client:
FC Wastewater
Date of Report:
9 February 2022
Date Collected:
18 January 2022
Report No.:
2022-1-RESIDUALS
Date Received:
18 January 2022
Lab ID:
227, 94
Sample:
Quarterly Sludge
Collected By:
N. Droski
Sample ID: CROM
Date
Analyte
Results
Units
Method
Analyzed By
Analyzed
pH
8.06
SU
1/18/2022
SM 4500 H+ B
ELS
Nitrate
See Attached
Envirochem
Nitrogen
Sludge
See Attached
Envirochem
Residuals
NOTE:
Certi ied By:
L PUREN. CACOSTA

r a
cM
ANALYTICAL & CONSULTING CHEMISTS
USMC Camp Lejeune
G-F1;EMDIECB -12 Post Lane
Camp Lejeune NC 28547
Attention: Lauren Acosta
Lab ID Sample ID:
22-02631 Site: CROM Tank
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910,392.4424 Fax
710 Sowsertown Road, Mantea, NC 27954 - 252-473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
Vest Method
PAN
Used 30% Mineraltzabon Rate
SAR
Sludge Residuals
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Nitrate+N itrite-Nitrogen
Total Solids (%)
Ammonia Nitrogen
[e-mail]
Date of Report: Feb 08, 2022
Customer PO #:
Customer ID: 12060026
Report #: 2022-01084
Project ID: Sludge
Coliect DaterTime Matrix Sampled by
1/18/2022 9:03 AM Solid/Sludge Nicholas ❑roski
Calculation
Calculation
EPA 200.7, Rev. 4.4, 1994
EPA 200 7, Rev. 4.4, 1994
EPA 200.7. Rev, 4.4, 1994
EPA 200.7. Rev. 4.4. 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7. Rev 4.4. 1994
EPA 200.7. Rev. 4A. 1994
EPA 200.7. Rev. 4.4, 1994
EPA 200.7, Rev. 4A, 1994
EPA 200.7. Rev. 4 4, 199A
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4. 1994
EPA 200,7, Rev. 4.4. 1094
EPA 200.7_ Rev_ 4.4, 1994
EPA 353.2
SM 2540 8
SM 4500 NH3 C-2011
-total KI.eldahl Nitrogen (TKN) SM 4500 Norg B-2011
Total Phosphorous SM 4500 P [F-H]-2011
pH SW 846 Method 90451)
Result estimated. Analyzed out of 15 minutes hold time.
Results Date Analyzed
15900 mg/kg
O&U,
71300 mglkg
* 17.9 mg/kg
* 17.9 mg/kg
66800 mg/kg
25.4 mglkg
312 mglkg
< 17.9 mg/kg
2990 mg/kg
<17.9 mglkg
< 17.9 mglkg
3300 mg/kg
< 17.9 rng/kq
2220 mg/kg
1400 mg/kg
7.96 mg/kg
5.28 %
19300 mg/kg
40200 mglkg
53600 mglkg
8.14units
02/08/2022
02/08/2022
01/26/2022
01/26/2022
01/26/2022
01/26/2022
01/26/2022
01/26/2022
01/26/2022
01/26/2022
01/26/2022
01/26/2022
01/31/2022
01/31/2022
01 /31 /2022
01/26/2022
01/24/2022
01 /20/2022
01121 /2022
01/24/2022
01/26/2022
01 /24/2022
Mercury SV%J-9467471 B <0.362 mg/kg 01/28/2022
Reoort # 2022.01084 Page 1 or 2

Environmental Chemists, Inc.
envirvchem
ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910,347.5843 Lab/Fax
[e-mail]
USMC Camp Lejeune Date of Report: Feb 08, 2022
G-F/EM❑/ECB -12 Post Lane Customer PO #:
Camp Lejeune NC 28547 Customer ID: 12060026
Attention. Lauren Acosta Report #: 2022-01084
Project 1D: Sludge
Comment: Results, except ph and SAR, reported on a dry weight basis. pH and SAR reported on an as
received basis.
i
Reviewed by: al oaj
Report # . 2022-01084 Page 2 of 2

Environmental Chemist, Inc., Wilmington, NC Lab 494
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client: Date: Oc� Report Number:, C?)ojg
Receipt of sample: ECHEM PickuPA Client Delivery ❑ 1UPS ❑ FedEx ❑ Other ❑
❑ YES ❑ NO J0 N/A 1. Were custody seals present on the cooler?
❑ YES ❑ NO 1 Q0 N/A 2. if custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt °C
How temperature taken: ❑ Temperature Blank k? Against Bottles
1R Gun ID: Thomas Traceable S/N 1925116S7 IR Gun Correction Factor'C: 0.0
❑
YES
❑
NO
3.
If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
❑
NO
4.
Were proper custody procedures (relinquished/received) followed?
YES
❑
NO
5.
Were sample ID's listed on the CDC?
YES
❑
NO
6.
Were samples ID's listed on sample containers?
JO
YES
❑
NO
7.
Were collection date and time listed on the CDC?
YES
❑
NO
8.
Were tests to be performed listed on the CDC?
YES
❑
NO
9.
Did samples arrive in proper contalners For each test?
YES
❑
NO
10. Did samples arrive in good condition for each test?
YES
❑
NO
11.
Was adequate sample volume availableT
YES
❑
NO
12.
Were samples received within proper holding time for requested tests?
❑
YES
❑
NO
13. Were acid preserved samples received at a pH of <2?
❑
YES
❑
NO
14.
Were cyanide samples received at a pH ?12?
❑
YES
❑
NO
1S.
Were sulfide samples received at a pH >9?
❑
YES
❑
NO
16.
Were NH3/TICN/phenol received at a chlorine residual of E0.5 m/L? **
❑
YES
❑
NO
17.
Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑
YES
❑
NO
18.
Were orthophosphate Samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SOa HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. obtain a new sampie or
notify the state la if directed to analyzed by the customer. who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

NO 2W5
-fir A � wi'��a:•
ENVIRONMENTAL CHEMISTS, INC ❑FFCc 910-392-0223FiAX910-392-4424
s
r NCI) ENR: DWQ CERTIFICATION # 94 NCQHHS: OLS CERTIFICAT [0N # 3:.25 infaaenvirornmenta(chemists-com
Analytical & Consulting C"miss
COI I FCTION AHD CHAIN OF CUSTODY
CLIENT: Commanding Gerjeral
1PROJECT NAME: Camp Lejeune MCB
REPORT NO: a -- Q i OS
ADDRESS: G-FIEMDIEQBIEnvironmental Lab
CONTACT NAME: Lauren Acosta
PO NO:
12 Post Lane
I REPORT TO: Lauren Acosta
PHONEIFAX: gip 451_597
Camp Le9eune NC 28547
COPY TO:
ernail: [e-mail]
.ramnlprl Rv- 1i) e-,:, n 1, I'r7 5 SA RA PI C TYPF• I = Infli rant i` r Fffli zv nt W = WvII ST = Stream AC) c Snii SI = !Shjelei F2 [ lthAr-
Sample Identification
- Collection
m �,
W F❑
2
c
ra
=
a
w
a¢Qi
PRESERVATION
ANALYSIS REQIJESTEO
Date
Time
Temp
z
o
¢
o
u
CROM TANK
i �P- Lz
C'
swdce
C
2. r _11
�o f
x
Aiuminum. Arsenic, Cadmium, Chromium,
Capper, Lead, Magnesium, Molybdenum,
G
G
C
P
Nickel, Potassium, Sodium, Selenium, Zirc,
Mercury, Sludge, Nitrite_ Nitrate,
G
G
G
P
Nitrate -Nitrite, TKN, Total Solids/Soils &
Sludge, Ammonia. Total Phosphorus.
G
G
C
P
Calcium, SAR, PAN
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
"
G
G
C
P
G
G
Transfer
Relinquished By:
Datemme Received By:
Date7imp
1.
Z2 -0q 14
2.
r
. t 2 o a
s v
temperature
Delivered By:
Comments:
epted:
Received B
to reested:
141a-�Time:
TURNAROUND:

2ND QUARTER
Residuals Analysis Lab Sheets

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
12 Post Lane, Camp Lejeune, NC 28547
Client:
FC Wastewater
Date of Report:
28 April 2022
Date Collected:
5 April 2022
Report No.:
2022-2-RESIDUALS
Date Received:
5 April 2022
Lab ID:
227, 94
Sample:
Quarterly Sludge
Collected By:
J. Acosta
Sample ID: CROM
Date
Analyte
Results
Units
Method
Analyzed By
Analyzed
pH
8.79
SU
4/05/2022
SM 4500 H+ B
ELS
Nitrate
See Attached
Envirochem
Nitrogen
Sludge
See Attached
Envirochem
Residuals
NOTE: Crom tank was down for maintenance. Sample collected from T3B.
Certi ied By:
L PUREN. CACOSTA

F"ww' 0
- 71
s+a
ANALYTICAL & CONSULTING CHEMISTS
USMC Camp Lejeune
G-FIEMDIECB -12 Post Lane
Camp Lejeune NC 28547
Attention: Lauren Acosta
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.M3 Lab • 910.392.4424 Fax
710 Bovvsertoti}n Road, Manteo, NC 27954 • 252.473,5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info?a environmcn[alChcmisis.Cam
Date of Report: Apr 27, 2022
Customer PO #:
Customer Id: 12060026
Report #: 2022-06208
Project ID: T3B
Lab I❑ Sample ID: Collect Date/Time Matrix Sampled by
22-15069 Site: T38 4/5/2022 7.20 AM SolidlSiudge Julius Acosta
Test Method Results Date Analyzed
PAN Calwiat,on 29300 mg/kg 04/19/2022
Used 30°h Mineralization Rate.
SAR
Cafrulalion
0.580
04/19/2022
Nitrate Nitrogen (caic)
Nitrite Nitrogen
EPA 353.2
63.6 mg/kg
04/07/2022
Nitrate Nitrogen
subUaction Method
122 mglkg
04/19/2022
Sludge Residuals
Aluminum
EPA 200.7, Rev. 44, 1904
57800 mg/kg
04/14/2022
Arsenic
EPA 200 7, Rev. 4.4, 1994
<37A mg/kg
04/14/2022
Cadmium
EPA 2007_ Rev. 4.4, 1994
<37.4 mg/kg
04/14/2022
Calcium
EPA 200 7, Rev, 4.4. 1994
63600 mg/kg
04/14/2022
Chromium
EPA 200.7. Rev. 4.4, 1994
<37.4 mglkg
04/14/2022
Copper
EPA 200.7, Rev. 4.4, 1994
293 mglkg
040412022
Lead
EPA 200 7, Rev, 4.4, 1994
<37.4 mg/kg
04/ 1412022
Magnesium
EPA 200.7. Rev 4.4, 1994
5380 mg/kg
04/14/2022
Molybdenum
EPA 200.7, Rev. 4.4, 1994
<37 4 mg/kg
04/14/2022
Nickel
EPA200.7, Rev. 4.4. 1994
<37.4 mg/kg
04/14/2022
Potassium
EPA 200.7. Rev. 4.4, 1994
8310 mg/kg
04/14/2022
Selenium
EPA 200.7. Rev. J.4, 1994
<37,4 mglkg
04/14/2022
Sodium
EPA 200.7, Rev 4.4. 1994
3500 mg/kg
04/14/2022
Zinc
EPA 200.7, Rev 4 4, 1994
1570 mg/kg
04/14/2022
Nitrate+Nitrate-Nitrogen
EPA 3532
185mglkg
04/12/2022
Total Solids (%)
SM 2540 8
2.60 %
040712022
Ammonia Nitrogen
SM 4500 NH3 C-2011
35400 mg/kg
a4/07/2022
Totat Kjeldahl Nitrogen (TKN)
SM 4500 NofgB-2011
73400 mg/kg
04/07/2022
Total Phosphorus
SM 4500 P (F-H)-2011
56200 mg/kg
04/14/2022
Repon:. 2022.05208 Page 1 of 2

su
ANALYTICAL & CONSULTING CHEMISTS
USNIC Camp Lejeune
G-FIEMD/ECB -12 Post Lane
Camp Lejeune NC 28547
Attention: Lauren Acosta
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 9][1.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/ Fax
2S5•A Wilmington Highway, Jacksonville, NC 28540 • 910.347,5843 Lab/Fax
i ni`oru en.iranmen talchem i sls.com
Date of Report: Apr 27, 2022
Customer PO #:
Customer ID: 12060026
Report #: 2022-06208
Project ID: T38
pH SW 846 Method 9045D 9.03 units 04/12/2022
Result estimated. Analyzed out of 15 minutes hoki lime.
Mercury sw-B45 7471 s <0.638 mglkg 04l2512022
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis
Reviewed by:
Report 0 : 2022-G6208 Page 2 of 2

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client: U AA C-- Date: J' I Qa Report Number: A a U
Receipt of sample: ECHEM Pickup Client Delivery ❑
1UPS ❑ EedEx ❑ Other ❑
❑ YES
10 NO
N/A 1. Were custody seals present on the cooler?
❑ YES
10 NO
N/A 12, If custody seals were present, were they intact/unbroken?
Original temperature upon receipt ! . `C Corrected temperature upon receipt 'C
How temperature taken: ❑ Temperature Blank ❑ Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IA Gun Correction Pa{tor'C. 0.0
Cl YES
❑ NO
3- If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
❑ NO
4. Were proper custody procedures (relinquishedireceived) followed?
YES
© NO
S. Were sample ID's listed on the CDC?
YES
❑ NO
6_ Were samples ID's listed on sample containers?
YES
❑ NO
7. Were Collection date and time listed on the COC?
YES
❑ NO
8. Were tests to be performed listed on the COC?
YES
❑ NO
9. Did samples arrive in proper containers for each test?
YES
❑ NO
10 Did samples arrive in goad condition for each test?
YJ YES
❑ NO
11. Was adequate sample volume available?'
IL YES
❑ NO
12. Were samples received within proper holding time for requested tests?
❑ YES
❑ NO
13. Were acid preserved samples received at a pH of <27
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
0 YES
Cl NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑ NO
16, Were NH3/TKN/Phenol received at a chlorine residual of <O.5 m/L? "
❑ YES
❑ NO
17, Were Sulfide/Cyanide received at a Chlorine residual of <0.5 m/L?
❑ YES
❑ NO 118,
Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
' * Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(sj incorrectly preserved a with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one). HzSO, h NO3 HCl NaOH
Time of preservation; if more than one preservative is needed, notate in comments below
Note: Notify customer service Immediately for mcorrectiy preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC QA.002 Rev 1

Way
'- ENVIRONMENTAL CHEMISTS, INC OFFICE!9101-32-0223F'AX910-3 2-4424
G info nvironmentalchemists.com
Analytical & Consulting Chemists NCQFAll2 QWC CERTIFICATION # 94 NCOHHS: DLS Gt_RTiFICATEflN 37729
COLLECTION AND CHAIN OF CUSTODY
CLIENT: Comm ndin a
PROJECT NAME: Camp Lejeune MCB
REPORT NO: —0(0 �Q 8
ADDRESS: G-FIEMDIEQBIEnvironmental Late
CONTACT NAME: Lauren Acosta
PO NO:
12 Post Lane
REPORTTO: Lauren Acosta
PHONEIFAX: 91 451- 9 7
Camp Le eune NC 28547
1 COPY TO:
email: [e-mail]
Sampled By: A L1, SAMPLE TYPE_ I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL= Sludge, Other:
Sample Identification
�—
Collection
a
e s
a
v a
y
a
J z
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
x
i
N
s
"o
x
o
6Y
a
F
o
2
Y 5 7,
❑ 22a
C
P
,r(
�'7LI +
x
Aluminum, Arsenic, CadmiuWChromium,
Copper; Lead, Magnesium, Molybdenum.
G
G
C
P
Nickel; Potassium SodiumSelenium, Zinc,
Mercury, Sludge, Nitrite, Nitrate,
G
G
C
P
Nitrate-Nitrite,'TKN, Total Solids7Soils &
Sludge, Ammonia, Total Phosphorus;
G
G
C
P
Calcium, SAR, PAN
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Transfer
Relinquished By:
❑atelTme R eiv-d By:
DateMme
1.
3iOn alau JA
2.
Temperature when Received: 1.-1 • b Accepted: ected: ResarnpIT11r.
sted:
Delivered 8y: Received By: Hate: J� Time:
Comments: n k 1'2 !1 TURNAROUND:

3RD QUARTER
Residuals Analysis Lab Sheets

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
12 Post Lane, Camp Lejeune, NC 28547
Client:
FC Wastewater
Date of Report:
30 August 2022
Date Collected:
2 August 2022
Report No.:
2022-3-RESIDUALS
Date Received:
2 August 2022
Lab ID:
227, 94
Sample:
Quarterly Sludge
Collected By:
J. Acosta
Sample ID: CROM
Date
Analyte
Results
Units
Method
Analyzed By
Analyzed
pH
8.19
SU
8/02/2022
SM 4500 H+ B
ELS
Nitrate
See Attached
Envirochem
Nitrogen
Sludge
See Attached
Envirochem
Residuals
Certified By:
L 9�) �t—
UREND. ACOSTA

w w
,:M
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 e M0.347.5843 Lab/Fax
inf'o(ri cnviraaimentalchemists.com
USMC Camp Lejeune Date of Report: Aug 26, 2022
G-F/EMD/ECB -12 Post Lane Customer PD #: N4008519DB034
Camp Lejeune NC 28547 Customer ID: 1206002E
Attention: Lauren Acosta Report #: 2022-14791
Project ID: Crom Tank
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-36070 Site: CRAM Tank 8/2/2022 7 52 AM Solid/Sludge Acosta Julius
Test Method Results Date Analyzed
PAN Calculation 814 mglkg 08/26/2022
Used 301Io Mineralization Rafe
SAP
Calculation
0.670
08/26/202 2
Sludge Residuals
Aluminum
EPA 200 7 Rev 4 4 1994
61500 mg/kg
08/23/2022
Calcium
EPA 2007 Rev 4 4 1994
46300 mg/kg
08/23/2022
Copper
EPA 200 7 Rev 4 4 1994
356 mglkg
08/23/2022
Potassium
EPA 200 7, Rev 4 4. 1994
7110 mglkg
08/23/2022
Arsenic
EPA 200S. Rev 54 1994
<18.1 mglkg
08/16/2022
Cadmium
EPA 2005 Rev 54 1994
<18.1 mglkg
08/16/2022
Chromium
EPA 2008 Rev 54 1994
24.4mglkg
08/16/2022
Lead
EPA 200 8 Rev 54 1094
t 18.1 mg/kg
08/16/2022
Magnesium
EPA 2008 Rev 54.1994
4900mglkg
08/17/2022
Molybdenum
EPA 200 0. Rev 54. 1994
<18.1 mg/kg
08/16/2022
Nickel
EPA 2008. Rev 54 1994
¢18.1 mglkg
08/16/2022
Selenium
EPA 200B, Rav 54 1994
<18.1 mglkg
08/16/2022
Sodium
EPA 200 8 Rev 5 4 1994
3480 mg/kg
08/17/2022
Zinc
EPA 200 8 Rev 54 1994
1550 mg/kg
08/16/2022
Nitrate+Nitrite-Nitrogen
EPA 353 2
49.5 mg/kg
08/08/2022
Total Solids (%)
SM 2540 s
2.70 %
08105/2022
Ammonia Nitrogen
SM 4500 NH3 C-2011
41000 mglkg
08/08/2022
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg a-2011
73000 mglkg
08/05/2022
Total Phosphorus
SM 4500 P (F-rt)-2011
49500 mglkg
08/17/2022
PH
SW 846 Method 0045a
8.47 units
08/16/2022
Result estimated Analyzed out of
15 minutes hold time.
Mercury
sw-1346 7471 a
<0.6 mg/kg
08/16/2022
Report N 2022-14791 Page T of 2

Environmental Chemists, Inc.
,ZnvirocheM
ANALYTICAL & CONSULTING CHEWSTS
USMC Camp Lejeune
G-FIEMDIECB -12 Post Lane
Camp Lejeune NC 28547
Attention: Lauren Acosta
6602 Windmill Way, Wilmington, NC 2$405 . 910.392.0223 Lab 1 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 + 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
infoL environmentalchemists.com
Date of Report: Aug 26, 2022
Customer PO M N4008519D8034
Customer ID: 12060026
Report #: 2022-14791
Project ID: Crom Tank
Comment: Results, except pH and SAR, reported on a dry weight basis. SAR and pH reported on an as
received basis.
Reviewed by: [r-
Repprt # 2022-14791 Page 2 of 2

Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Ciient:LJl�t`� Date: 3 Ju Report Number: ,_J .)
Receipt of sample; ECHEM Pickup Client Delivery 0
JUPS ❑ FeclEx ❑ Other ❑
❑ YES ❑ NO
11 N/A
1. Were custody seals present on the cooler?
❑ YES ID NO
N/A
2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt -C Corrected temperature upon receipt °C
How temperature taken: ❑ Temperature Blank Against Bottles
IR Gun ID: Thomas Traceable S/N 192511G57 IR Gun Correction Factor °C: 0,0
❑ YES
❑ NO
3. if temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
k] YES
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
K YES
❑ NO
S. Were sample ID's listed on the COC?
YES
❑ NO
6. Were samples ID's listed on sample containers?
YES
❑ NO
7. Were collection date and time listed on the COC?
YES
❑ NO
S. Were tests to be performed listed on the COC?
YES
13 NO
9. Did samples arrive in proper containers for each test?
1� YES
yp YES
❑ NO
❑ NO
10. Did samples arrive in good condition for each test?
11. Was adequate sample volume available?"
UL YES
❑ NO
U. Were Samples received within proper holding time for requested tests?
❑ YES
❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14. Were cyanide samples received at a pH a12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑ No
16, Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES
❑ NO
17. Were Sulfide/Cyanide received a t a chlorine residual of t0.5 m/L?
❑ YES
❑ NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and retarded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Samples) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCl NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtaln a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

602 Windmill Way Wilmington, NC 284
ENVIRONMENTAL CHEMISTS, I N C OFFICE 910-392-023 FAX [phone]
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@_environmentalchemists.com
COLLECTION AND CHAIN OF CUSTODY
CLIENT: Comm ndin G
PROJECT NAME: Camp Lejeune MCB
REPORT NO: a���,C-1 r,,
ADDRESS: G-PEMO/EQB/Environmental Late
CONTACT NAME: Lauren Acosta
PO NO: n ra'& r b-
�HD
12 Post Lane
REPORT TO: Lauren Acosta
PHONEIFAX 91 451- 5 7
Camp Le'eune NC 28547
ICOPY TO:
email: lauren.acosta@usmc,mil
Sampled ILf I . v S -Lj SAMPLE TYPE: I = Influent. E = Effluent, W = Well, ST = Stream, SO = Soil. SL = Sludge. Other:
Sample Identification
Collection
0. E1
a
w
O p
e
n
_
C C7
`o
6
n
= E
�+
C Jj
m
go_
2
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
N
Q
a
o
i
CROM TANK
8
SUMCE
C
P
■ U
x
Aluminum, Arsenic, Cadmium, Chromium,
Copper, Lead, Magnesium, molybdenum,
G
C
P
Nickel, Potassium, Sodium, Selenium, Zinc,
Mercury, Sludge, Nitrite, Nitrate,
G
G
C
P
Nitrate -Nitrite, TKN, Total 5olidslSails &
Sludge, Ammonia, Total Phosphorus,
G
G
C
P
Calcium, SAR, PAN
G
G
C
P
G
G
C
P
GI
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Transfer
Relinquished By:
Dater.rime
ec ived By:
D terfime
2.
Temperature when Received: t3 • 1 Accepted: V Rej ted: Resamp a uested:
Aess� � z
Delivered By:rG [ Received By: Date Time
Comments: TLIR AROUND:

4TH QUARTER
Residuals Analysis Lab Sheets

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
12 Post Lane, Camp Lejeune, NC 28547
Client:
FC Wastewater
Date of Report:
14 November 2022
Date Collected:
5 October 2022
Report No.:
2022-4-RESIDUALS
Date Received:
5 October 2022
Lab ID:
227, 94
Sample:
Quarterly Sludge
Collected By:
J. Acosta
Sample ID: CROM
Date
Analyte
Results
Units
Method
Analyzed By
Analyzed
pH
6.99
SU
10/05/2022
SM 4500 H+ B
ELS
Nitrate
See Attached
Envirochem
Nitrogen
Sludge
See Attached
Envirochem
Residuals
Certified By:
L 9�) �t—
UREND. ACOSTA

F"WWT -', '�7
ANALYTICAL & CONSULTING CHEMISTS
IJSMC Camp Lejeune
G-FIEMD/EC B -12 Post Lane
Camp Lejeune NC 28547
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
755-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
in [e-mail]
Date of Report: Nov 11, 2022
Customer PO #:
Report #: 2022-19833
Customer ID: 12060026
Project ID: Cron Tank
Late ID Sample ID: Collect DatelTime Matrix Sampled by
22-48705 Site: CROM Tank 10/5/2022 7 45 AM SolidlSludge J. Acosta
Test Method Results Date Analyzed
PAN
Calculation
21300 mg/kg
11/11/2022
Used 30% Mineralization Rate.
SAR
Calculation
25.4
11 /11 /2022
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4,4, 1994
66100 mg/kg
11/09/2022
Arsenic
EPA200.7, Rev.4.4, 1994
13.9 mglkg
11/09/2022
Cadmium
EPA 200.7. Rev- 4.4. 1994
<9.24 mg/kg
11/0912022
Calcium
EPA 200.7, Rev, 4.A, 1994
46300 mg/kg
11/09/2022
Chromium
EPA 200.7, Rev .4.4, 1994
22-0 mg/kg
11/09/2022
Copper
EPA 200.7. Rev. 4.4, 1994
347 mg/kg
11/09/2022
Lead
EPA 2007._ Rev- 4.4. 1994
17.1 mglkg
11/09/2022
Magnesium
EPA 200.7, Rev- 4.4,1994
4580 mg/kg
11/09/2022
Molybdenum
EPA 200.7, Rev. 4.4,1994
<9.24 mg/kg
11/09/2022
N ickel
EPA 200.7. Rev. 4A.1994
16.0 mg/kg
11/09/2022
Potassium
EPA 200.7, Rev. 4.4. 1994
7050 mg/kg
11/09/2022
Selenium
EPA 200.7. Rev. 4.4, 1994
<9,24 mg/kg
11/09/2022
Sodium
EPA 200.7. Rev 4.4, 1994
3560 mglkg
11/09/2022
Zinc
EPA 200.7, Rev. 4.4, 1994
1650 mg/kg
11/09/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2
20.3 mglkg
10/10/2022
Total Solids (%)
sM 2540 s
2.75 %
10/10/2022
Ammonia Nitrogen
SM4500 NH3 C-201 t
37800 mg/kg
10/06/2022
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
70200 mg/kg
10/06/2022
Total Phosphorus
SM4500 P cF-Hy-2011
67800 mg/kg
10/13/2022
pH
sw 846 Method 90451]
8.55 units
10/20/2022
Result estimated. Analyzed out of 15
minutes hold time.
Mercury
sW-845 7471 a
<0.702 mglkq
11101/2022
Comment: Results, except pH, reported on a dry weight basis.
pH reported on an as received basis.
Reviewed by: HL a
� -
Report # 2022-19B33 Page 1 of 1

Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way
Wilmington, NC 28405
910.392.02 23
Sample Receipt Checklist
Client: IKS lll� Date:10 Jr �4 Report Number: _ 2022_ 198 _3,3
Receipt of sample: ECHFM Pickup
Client Deliverer ❑
UPS ❑ FeC1FY ❑ Other ❑
❑ YES
❑ 1d0
19 N/A 1.
Were custody seals present on the cooler?
❑ YE5
❑ N❑
N/A 2.
If custody seals were present, were they intact/unbroken?
Original temperature upon receipt
°C Corrected temperature upon receipt °C
How temperature taken:
❑ Temperature Blank W Against Bottles
IR Gun ID: Thomas Traceable S/ld 192511657 IR Gun Correction Factor- °C: ❑A
YES
❑ NO
3.
If temperature of cooler exceeded FC, was Project Mgr./QA notified?
E� YES
❑ NO
4_
Were proper custody procedures (relinquished/received) €ol}owed?
® YES
❑ NO
5.
Were sample 1D's listed on the COC?
U YES
❑ NO
6.
Were samples ID's listed on sample containers?
R YES
❑ NO
7.
Were collection date and time listed on the COC?
1� YES
❑ NO
8.
Were tests to be performed listed on the COC?
® YES
❑ NO
9.
Did samples arrive in proper containers for each test?
YES
❑ NO
10,
aid samples arrive in good condition for each test?
D� YES
10 NO
❑ NO
111,
12.
Was adequate sample volume available?'
Were samples received within proper holding time for requested tests?
❑' YES
❑ YES
❑ NO
13.
Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14.
Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15.
Were sulfide samples received at a pH >9?
❑ YES
❑ NO
16.
Were NH3/TKN/Phenol received at a chlorine residual of <0.5 in/L?
❑ YES
Cl NO
17.
Were Sulfide/Cyanide received at a chlorine residual ofc0.5 m/L?
❑ YES
❑ NO
18.
Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
Bacteria samples are checked for Chlorine at time of analysis and recorded on the benciisheet.
Sample Preservation:
sample(s)
by adding (Circle one):
Time of preservation:
{Must be completed for any samples) incorrectly preserved or with headspace)
were received incorrectly preserved and were adjusted accordingly
H2S0; HNO3 H0 NaOH
If more than one preservative is needed, notate in comments below
Note: NonFy customer service imrneJ ately for incorrectly preserved samp'es, ❑bta n a new samale or
notify the state lab it direrted to analyzed by the customer. Who was notified, date and time:
Voiatiles Sample(s)
were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

602
ill Way
► - Rt
ENVIRONMENTAL CHEMISTS, INC OFFICE994-392.023FAX 910-NC
24424$
Analytical $Consult ng Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
CLIENT: Commanding Geneull
PROJECT NAME: Camp Lejeune MCB
REPORT NO: a— 19955
ADDRESS: G-FIEMDJEQB/Environmental Lab
CONTACT NAME: Lauren Acosta
PO NO: l�� rapt No. Nq�(9 D
12 Post Lane
REPORT TO: Lauren Acosta
PHONE/FAX- 910451-5977
Camp Le eune NC 28547
COPY TO:
email: [e-mail]
Sarni led By: cUs SAMPLE TYPE: I = Influent, E = Effluent, W = Well, 5T = Stream, SO = Soil, 5L = Sludge, Other:
;�
Sample Identification
Collection
rm a
n
S
a
o
a
t
c c7
`o
0 a
Q
c
M.
kE
�
Q us
m
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
*
N
a
❑
z
CRaM TANK
i° �' �^'"
b� `��
C
P
4g-��,
x
Aluminum. Arsenic, Cadmium, Chromium,
Copper, Lead, Magnesium, Molybdenum,
G
P
Nickel, Potassium, Sodium, Selenium, Zinc,
Mercury, Sludge, Nitrite, Nitrate,
G
G
C
P
Nitrate -Nitrite, TKN, Total solids/Sails &
Sludge. Ammonia, Total Phosphorus,
GG
C
P
Calcium, SAR, PAN
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
{
G
G
Transfer
Relinquished By:
Dateriime
JReceived By:
Datef7ime
1.
i7 7 -b
z.
4
r 1-
Temperature w ec "v ,Accepted: );Icted: Resample R qu steel:
Delivered By Received By: _ Date: Time:
Comments: TURNA OUND:

SECTION 5
Annual Pathogen &Vector Attraction
Reduction Forms (Form PVRF 2T)
and Vector Attraction Reduction Lab
Sheets

1ST QUARTER
Pathogen and Vector Attraction Reduction Form
and Lab Sheets

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: U.S. MCB CAMP LEJEUNE WQ Permit Number: WQ0012346
WWTP Name: Camp Lejeune Advanced WWTP
NPDES Number: NCO063029
Monitoring Period: From l/l/2022 To 3/31/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp)❑
Alt B (Alk Treatment) ❑
I Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
1 Process to Further Reduce Pathogens❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑ Heat Treatment ❑
Thermophilic 0
Beta Ray ❑
Gamma Ray ❑ Pasteurization ❑
Class B:
Alt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑ Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g y
Number of
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -
ni ue
Minimu
Geo. Mean
aximun-
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
2.82
5.42
18.56
MPN/
Gam
0
Weekly
Grab
Sm
922 CE
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.l (VS reduction)
❑
Alt. 2 (40-day bench)
❑
Alt. 3 (30-day bench)❑
Alt. 4 (Spec. Oz uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization
❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
Alt. 10 (Incorporation)
❑
No vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Charles Scozzari Supe , WW/Land App Charles Scozzari Sur.94sor, WW/Land App
Preparer Name n itle (t a or print) Land Applier Natgie nd T' e (if applicable)(type or print)
3
Signat f Preparer* applicable)
is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/20061

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 02/07/2022
Report No.: 2022-JAN ATAD Lab ID: 227
Sample ID:
T2B
Date Collected:
01/04/2022
Collected By:
WILLIAMS
Time Collected:
0753
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.08
01/04/2022
SM 2540 G
ALB
o Volatile Solids
50.15
o
01/04/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
01/04/2022
Collected By:
WILLIAMS
Time Collected:
0753
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.35
01/04/2022
SM 2540 G
ALB
o Volatile Solids
60.38
o
01/04/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
01/04/2022
Collected By:
WILLIAMS
Time Collected:
0753
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.62
%
01/04/2022
SM 2540 G
ALB
o Volatile Solids
64.54
o
01/04/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 1 of 7

Sample ID:
CROM
Date Collected:
01/04/2022
Collected By:
WILLIAMS
Time Collected:
0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.34
o
01/04/2022
SM 2540 G
ALB
o Volatile Solids
48.69
o
01/04/2022
SM 2540 G
ALB
Fecal Coliforms
5.41
MPN/gram
01/04/2022
SM 9221 C E
ALB
Sample ID:
T2B
Date Collected:
01/06/2022
Collected By:
RUBERTE
Time Collected:
0805
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.04
1/11/2022
SM 2540 G
DES
o Volatile Solids
50.73
%
1/11/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
01/06/2022
Collected By:
RUBERTE
Time Collected:
0805
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.16
%
1/11/2022
SM 2540 G
DES
o Volatile Solids
57.41
%
1/11/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
1 1/11/2022
Collected By:
DROSKI
Time Collected:
0753
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.95
%
1/11/2022
SM 2540 G
DES
o Volatile Solids
2.90
%
1/11/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 2 of 7

Sample ID:
T4B
Date Collected:
1 1/11/2022
Collected By:
DROSKI
Time Collected:
0753
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.90
%
1/11/2022
SM 2540 G
DES
o Volatile Solids
55.75
%
1/11/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
1 1/11/2022
Collected By:
DROSKI
Time Collected:
0753
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.33
1/11/2022
SM 2540 G
DES
o Volatile Solids
63.16
%
1/11/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
1 1/11/2022
Collected By:
DROSKI
Time Collected:
0854
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.57
%
1/11/2022
SM 2540 G
DES
o Volatile Solids
51.23
%
1/11/2022
SM 2540 G
DES
Fecal Coliforms
7.06
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
1 1/13/2022
Collected By:
RUBERTE
Time Collected:
0755
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.05
o
01/18/2022
SM 2540 G
ALB
o Volatile Solids
49.18
o
01/18/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 3 of 7

Sample ID:
T4B
Date Collected:
1 1/13/2022
Collected By:
RUBERTE
Time Collected:
0755
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.12
o
01/18/2022
SM 2540 G
ALB
o Volatile Solids
54.69
o
01/18/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
1/18/2022
Collected By:
DROSKI
Time Collected:
0807
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.32
o
01/18/2022
SM 2540 G
ALB
o Volatile Solids
47.14
o
01/18/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3A
Date Collected:
1 1/18/2022
Collected By:
DROSKI
Time Collected:
0807
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.54
%
01/18/2022
SM 2540 G
ALB
o Volatile Solids
58.81
o
01/18/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
1/18/2022
Collected By:
DROSKI
Time Collected:
0807
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.02
%
01/18/2022
SM 2540 G
ALB
o Volatile Solids
53.58
o
01/18/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 4 of 7

Sample ID:
CROM
Date Collected:
1 1/18/2022
Collected By:
DROSKI
Time Collected:
0837
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
5.14
o
01/18/2022
SM 2540 G
ALB
o Volatile Solids
45.28
o
01/18/2022
SM 2540 G
ALB
Fecal Coliforms
3.50
MPN/gram
01/18/2022
SM 9221 C E
ALB
Sample ID:
T2B
Date Collected:
01/19/2022
Collected By:
DROSKI
Time Collected:
0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
NOT ANALYZED
o
SM 2540 G
% Volatile Solids
NOT ANALYZED
o
SM 2540 G
Fecal Coliforms
4.17
MPN/gram
01/19/2022
SM 9221 C E
LA
Sample ID:
T2B
Date Collected:
1 1/20/2022
Collected By:
DROSKI
Time Collected:
0658
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.39
%
1/25/2022
SM 2540 G
ALB
o Volatile Solids
48.51
%
1/25/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3A
Date Collected:
1/20/2022
Collected By:
DROSKI
Time Collected:
0658
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.27
%
1/25/2022
SM 2540 G
ALB
o Volatile Solids
56.54
%
1/25/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 5 of 7

Sample ID:
T4B
Date Collected:
1 1/20/2022
Collected By:
DROSKI
Time Collected:
0658
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.00
%
1/25/2022
SM 2540 G
ALB
o Volatile Solids
53.48
%
1/25/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
1/20/2022
Collected By:
DROSKI
Time Collected:
0658
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.76
%
1/25/2022
SM 2540 G
ALB
o Volatile Solids
68.79
%
1/25/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
1 1/25/2022
Collected By:
DROSKI
Time Collected:
0731
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.38
%
1/25/2022
SM 2540 G
ALB
o Volatile Solids
53.97
%
1/25/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
1/25/2022
Collected By:
DROSKI
Time Collected:
0731
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
7.48
%
1/25/2022
SM 2540 G
ALB
o Volatile Solids
68.09
%
1/25/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 6 of 7

Sample ID:
CROM
Date Collected:
1 1/25/2022
Collected By:
DROSKI
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.56
%
1/25/2022
SM 2540 G
ALB
o Volatile Solids
48.05
%
1/25/2022
SM 2540 G
ALB
Fecal Coliforms
5.06
MPN/gram
1/25/2022
SM 2540 G
ALB
Sample ID:
T3B
Date Collected:
1/27/2022
Collected By:
DROSKI
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.71
%
1/27/2022
SM 2540 G
DES
o Volatile Solids
53.19
%
1/27/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4A
Date Collected:
1 1/27/2022
Collected By:
DROSKI
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.05
%
1/27/2022
SM 2540 G
DES
o Volatile Solids
65.29
%
1/27/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Certified By:
L REN D. ACOSTA
Page 7 of 7

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 03/07/2022
Report No.: 2022-FEB ATAD Lab ID: 227
Sample ID:
T4A
Date Collected:
02/01/2022
Collected By:
DROSKI
Time Collected:
0710
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.95
02/01/2022
SM 2540 G
ALB
o Volatile Solids
60.98
%
02/01/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
02/01/2022
Collected By:
DROSKI
Time Collected:
0710
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.73
02/01/2022
SM 2540 G
ALB
o Volatile Solids
51.06
%
02/01/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
02/01/2022
Collected By:
DROSKI
Time Collected:
0710
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.69
%
02/01/2022
SM 2540 G
ALB
o Volatile Solids
59.45
%
02/01/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 1 of 7

Sample ID:
CROM
Date Collected:
02/01/2022
Collected By:
DROSKI
Time Collected:
0721
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.96
%
02/01/2022
SM 2540 G
ALB
o Volatile Solids
47.06
%
02/01/2022
SM 2540 G
ALB
Fecal Coliforms
5.05
MPN/gram
02/01/2022
SM 9221 C E
ALB
Sample ID:
T3B
Date Collected:
02/03/2022
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.72
02/03/2022
SM 2540 G
ALB
o Volatile Solids
51.66
%
02/03/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
02/03/2022
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.80
%
02/03/2022
SM 2540 G
ALB
o Volatile Solids
59.39
%
02/03/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
02/03/2022
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
5.23
%
02/03/2022
SM 2540 G
ALB
o Volatile Solids
61.22
%
02/03/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 2 of 7

Sample ID:
T3B
Date Collected:
02/08/2022
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.70
%
02/08/2022
SM 2540 G
DES
o Volatile Solids
50.49
%
02/08/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
02/08/2022
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.66
02/08/2022
SM 2540 G
DES
o Volatile Solids
58.11
%
02/08/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
02/08/2022
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.11
%
02/08/2022
SM 2540 G
DES
o Volatile Solids
65.39
%
02/08/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
02/08/2022
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.03
%
02/08/2022
SM 2540 G
DES
o Volatile Solids
46.62
%
02/08/2022
SM 2540 G
DES
Fecal Coliforms
4.47
MPN/gram
SM 9221 C E
Page 3 of 7

Sample ID:
T3B
Date Collected:
02/10/2022
Collected By:
WILLIAMS
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.42
%
02/10/2022
SM 2540 G
ALB
o Volatile Solids
51.44
%
02/10/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
02/10/2022
Collected By:
WILLIAMS
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.35
%
02/10/2022
SM 2540 G
ALB
o Volatile Solids
55.84
%
02/10/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
02/10/2022
Collected By:
WILLIAMS
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.47
%
02/10/2022
SM 2540 G
ALB
o Volatile Solids
66.47
%
02/10/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
02/15/2022
Collected By:
WILLIAMS
Time Collected:
0948
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.25
%
02/15/2022
SM 2540 G
ALB
o Volatile Solids
51.13
%
02/15/2022
SM 2540 G
ALB
Fecal Coliforms
5.54
MPN/gram
02/15/2022
SM 9221 C E
ALB
Page 4 of 7

Sample ID:
T4B
Date Collected:
02/15/2022
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.03
%
02/15/2022
SM 2540 G
ALB
o Volatile Solids
54.66
%
02/15/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
02/15/2022
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.27
%
02/15/2022
SM 2540 G
ALB
o Volatile Solids
66.38
%
02/15/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
02/15/2022
Collected By:
WILLIAMS
Time Collected:
0855
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
6.38
%
02/15/2022
SM 2540 G
ALB
o Volatile Solids
42.94
%
02/15/2022
SM 2540 G
ALB
Fecal Coliforms
2.82
MPN/gram
02/15/2022
SM 9221 C E
ALB
Sample ID:
T3B
Date Collected:
02/17/2022
Collected By:
ACOSTA
Time Collected:
0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.26
%
02/17/2022
SM 2540 G
ALB
o Volatile Solids
51.10
%
02/17/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 5 of 7

Sample ID:
T4B
Date Collected:
02/17/2022
Collected By:
ACOSTA
Time Collected:
0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.33
%
02/17/2022
SM 2540 G
ALB
o Volatile Solids
54.82
%
02/17/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
02/22/2022
Collected By:
WILLIAMS
Time Collected:
0710
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.38
%
02/22/2022
SM 2540 G
ALB
o Volatile Solids
51.67
%
02/22/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
02/22/2022
Collected By:
RUBERTE
Time Collected:
0827
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.15
%
02/22/2022
SM 2540 G
ALB
o Volatile Solids
53.22
%
02/22/2022
SM 2540 G
ALB
Fecal Coliforms
5.71
MPN/gram
02/22/2022
SM 9221 C E
ALB
Sample ID:
FEED
Date Collected:
02/22/2022
Collected By:
WILLIAMS
Time Collected:
0710
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.63
%
02/22/2022
SM 2540 G
ALB
o Volatile Solids
68.02
%
02/22/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 6 of 7

Sample ID:
T3B
Date Collected:
02/24/2022
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.93
%
03/01/2022
SM 2540 G
ALB
o Volatile Solids
52.31
%
03/01/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
02/24/2022
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.09
%
03/01/2022
SM 2540 G
ALB
o Volatile Solids
52.68
%
03/01/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
02/24/2022
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.24
%
03/01/2022
SM 2540 G
ALB
o Volatile Solids
68.58
%
03/01/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Certified By:
L REN D. ACOSTA
Page 7 of 7

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 04/04/2022
Report No.: 2022-MAR ATAD Lab ID: 227
Sample ID:
TIB
Date Collected:
03/01/2022
Collected By:
RUBERTE
Time Collected:
0741
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.85
03/01/2022
SM 2540 G
ALB
o Volatile Solids
48.71
%
03/01/2022
SM 2540 G
ALB
Fecal Coliforms
3.71
MPN/gram
03/01/2022
SM 9221 C E
LA
Sample ID:
T2B
Date Collected:
03/01/2022
Collected By:
RUBERTE
Time Collected:
0742
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.35
03/01/2022
SM 2540 G
ALB
o Volatile Solids
48.96
%
03/01/2022
SM 2540 G
ALB
Fecal Coliforms
5.37
MPN/gram
03/01/2022
SM 9221 C E
LA
Sample ID:
T3B
Date Collected:
03/01/2022
Collected By:
RUBERTE
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.20
%
03/01/2022
SM 2540 G
ALB
o Volatile Solids
53.45
%
03/01/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 1 of 9

Sample ID:
T4B
Date Collected:
03/01/2022
Collected By:
RUBERTE
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.19
%
03/01/2022
SM 2540 G
ALB
o Volatile Solids
56.87
%
03/01/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
03/01/2022
Collected By:
RUBERTE
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.77
03/01/2022
SM 2540 G
ALB
o Volatile Solids
68.95
%
03/01/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
03/03/2022
Collected By:
DROSKI
Time Collected:
0751
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.29
%
03/03/2022
SM 2540 G
ALB/DES
o Volatile Solids
52.35
%
03/03/2022
SM 2540 G
ALB/DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
03/03/2022
Collected By:
DROSKI
Time Collected:
0751
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.57
%
03/03/2022
SM 2540 G
ALB/DES
o Volatile Solids
56.87
%
03/03/2022
SM 2540 G
ALB/DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 2 of 9

Sample ID:
T3B
Date Collected:
03/08/2022
Collected By:
DROSKI
Time Collected:
0719
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.08
%
03/08/2022
SM 2540 G
ALB
o Volatile Solids
55.62
%
03/08/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
03/08/2022
Collected By:
DROSKI
Time Collected:
0719
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.03
03/08/2022
SM 2540 G
ALB
o Volatile Solids
54.32
%
03/08/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
03/08/2022
Collected By:
DROSKI
Time Collected:
0719
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
5.02
%
03/08/2022
SM 2540 G
ALB
o Volatile Solids
63.72
%
03/08/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
TIB
Date Collected:
03/08/2022
Collected By:
DROSKI
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
5.10
%
03/08/2022
SM 2540 G
ALB
o Volatile Solids
47.58
%
03/08/2022
SM 2540 G
ALB
Fecal Coliforms
3.53
MPN/gram
03/08/2022
SM 9221 C E
ALB
Page 3 of 9

Sample ID:
T2B
Date Collected:
03/08/2022
Collected By:
DROSKI
Time Collected:
0724
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
1.02
%
03/08/2022
SM 2540 G
ALB
o Volatile Solids
57.99
%
03/08/2022
SM 2540 G
ALB
Fecal Coliforms
17.14
MPN/gram
03/08/2022
SM 9221 C E
ALB
Sample ID:
T3B
Date Collected:
03/10/2022
Collected By:
RUBERTE
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.96
%
03/10/2022
SM 2540 G
ALB
o Volatile Solids
55.24
%
03/10/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
03/10/2022
Collected By:
RUBERTE
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.06
%
03/10/2022
SM 2540 G
ALB
o Volatile Solids
53.95
%
03/10/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
03/15/2022
Collected By:
DROSKI
Time Collected:
0726
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.96
%
03/15/2022
SM 2540 G
ALB
o Volatile Solids
55.38
%
03/15/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 4 of 9

Sample ID:
T4B
Date Collected:
03/15/2022
Collected By:
DROSKI
Time Collected:
0726
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.89
%
03/15/2022
SM 2540 G
ALB
o Volatile Solids
55.78
%
03/15/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
03/15/2022
Collected By:
DROSKI
Time Collected:
0726
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
5.68
%
03/15/2022
SM 2540 G
ALB
o Volatile Solids
68.26
%
03/15/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
TIB
Date Collected:
03/15/2022
Collected By:
DROSKI
Time Collected:
0732
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.99
%
03/15/2022
SM 2540 G
ALB
o Volatile Solids
46.52
%
03/15/2022
SM 2540 G
ALB
Fecal Coliforms
3.61
MPN/gram
3/15/2022
SM 9221 C E
ALB
Sample ID:
T2B
Date Collected:
03/15/2022
Collected By:
DROSKI
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
0.96
%
03/15/2022
SM 2540 G
ALB
o Volatile Solids
54.88
%
03/15/2022
SM 2540 G
ALB
Fecal Coliforms
18.56
MPN/gram
3/15/2022
SM 9221 C E
ALB
Page 5 of 9

Sample ID:
T3B
Date Collected:
03/17/2022
Collected By:
RUBERTE
Time Collected:
0755
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.86
%
03/17/2022
SM 2540 G
ALB
o Volatile Solids
55.64
%
03/17/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
03/17/2022
Collected By:
RUBERTE
Time Collected:
0755
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.88
%
03/17/2022
SM 2540 G
ALB
o Volatile Solids
55.07
%
03/17/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
03/22/2022
Collected By:
RUBERTE
Time Collected:
0820
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.03
%
03/22/2022
SM 2540 G
ALB
o Volatile Solids
54.66
%
03/22/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
03/22/2022
Collected By:
RUBERTE
Time Collected:
0820
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.00
%
03/22/2022
SM 2540 G
ALB
o Volatile Solids
53.60
%
03/22/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 6 of 9

Sample ID:
FEED
Date Collected:
03/22/2022
Collected By:
RUBERTE
Time Collected:
0820
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.56
%
03/22/2022
SM 2540 G
ALB
o Volatile Solids
67.24
%
03/22/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T1B
Date Collected:
03/22/2022
Collected By:
RUBERTE
Time Collected:
0825
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
6.14
%
03/22/2022
SM 2540 G
ALB
o Volatile Solids
45.74
%
03/22/2022
SM 2540 G
ALB
Fecal Coliforms
2.93
MPN/gram
03/22/2022
SM 9221 C E
ALB
Sample ID:
T2B
Date Collected:
03/22/2022
Collected By:
RUBERTE
Time Collected:
0824
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.20
%
03/22/2022
SM 2540 G
ALB
o Volatile Solids
48.71
%
03/22/2022
SM 2540 G
ALB
Fecal Coliforms
4.29
MPN/gram
03/22/2022
SM 9221 C E
ALB
Sample ID:
T3B
Date Collected:
03/24/2022
Collected By:
DROSKI
Time Collected:
0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.90
%
03/24/2022
SM 2540 G
DES
o Volatile Solids
55.16
%
03/24/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 7 of 9

Sample ID:
T4B
Date Collected:
03/24/2022
Collected By:
DROSKI
Time Collected:
0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.92
%
03/24/2022
SM 2540 G
DES
o Volatile Solids
54.47
%
03/24/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
03/29/2022
Collected By:
RUBERTE
Time Collected:
0807
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
6.16
%
03/29/2022
SM 2540 G
ALB
o Volatile Solids
47.60
%
03/29/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
TIB
Date Collected:
03/29/2022
Collected By:
ACOSTA
Time Collected:
0803
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.08
%
03/29/2022
SM 2540 G
ALB
o Volatile Solids
49.49
%
03/29/2022
SM 2540 G
ALB
Fecal Coliforms
8.65
MPN/gram
03/29/2022
SM 9221 C E
ALB
Sample ID:
T2B
Date Collected:
03/29/2022
Collected By:
ACOSTA
Time Collected:
0802
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
1.96
%
03/29/2022
SM 2540 G
ALB
o Volatile Solids
50.98
%
03/29/2022
SM 2540 G
ALB
Fecal Coliforms
9.18
MPN/gram
03/29/2022
SM 9221 C E
ALB
Page 8 of 9

Sample ID:
T3B
Date Collected:
03/29/2022
Collected By:
RUBERTE
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.84
%
03/29/2022
SM 2540 G
ALB
o Volatile Solids
53.59
%
03/29/2022
SM 2540 G
ALB
Fecal Coliforms
6.34
MPN/gram
03/29/2022
SM 9221 C E
ALB
Sample ID:
T4B
Date Collected:
03/29/2022
Collected By:
RUBERTE
Time Collected:
0802
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.71
%
03/29/2022
SM 2540 G
ALB
o Volatile Solids
52.21
%
03/29/2022
SM 2540 G
ALB
Fecal Coliforms
4.85
MPN/gram
03/29/2022
SM 9221 C E
ALB
Sample ID:
T3B
Date Collected:
03/31/2022
Collected By:
DROSKI
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.83
%
03/31/2022
SM 2540 G
DES
o Volatile Solids
54.19
%
03/31/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
03/31/2022
Collected By:
DROSKI
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.88
%
03/31/2022
SM 2540 G
DES
o Volatile Solids
54.24
%
03/31/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Certified By:
L REN D. ACOSTA
Page 9 of 9

REPORT NO. 2022 BSQTRI
Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 02/23/2022
Report No.: 2022 BSQTRI Lab ID: 227
Date Collected: 01/20/2022 Time Collected: 0800 Collected By: I DES
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.54
%
1/25/2022
SM 2540 G
ALB
B-S
o Volatile Solids
49.75
%
1/25/2022
SM 2540 G
ALB
B-S DUP
o Total Solids
1.54
%
1/25/2022
SM 2540 G
ALB
B-S DUP
o Volatile Solids
49.90
%
1/25/2022
SM 2540 G
ALB
QUALITY CONTROL - 01/20/2022
B-S/B-S DUP
Average
%RPD
o Total Solids
1.54 %
0 %
o Volatile Solids
49.83 %
0.3 %
Date Collected: 01/25/2022 Time Collected: 0922 Collected By: I ALB
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.57
%
1/27/2022
SM 2540 G
DES
B-S
o Volatile Solids
49.04
%
1/27/2022
SM 2540 G
DES
B-S DUP
o Total Solids
1.54
%
1/27/2022
SM 2540 G
DES
B-S DUP
o Volatile Solids
49.43
%
1/27/2022
SM 2540 G
DES
QUALITY CONTROL - 01/25/2022
B-S/B-S DUP
Average
%RPD
o Total Solids
1.56 %
1.9 %
o Volatile Solids
57.30 %
0.8 %
Page 1 of 3

REPORT NO. 2022 BSQTRI
Date Collected: 02/01/2022 Time Collected: 0910 Collected By: I ALB
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.40
%
02/01/2022
SM 2540 G
ALB
B-S
o Volatile Solids
48.29
%
02/01/2022
SM 2540 G
ALB
B-S DUP
o Total Solids
1.40
%
02/01/2022
SM 2540 G
ALB
B-S DUP
o Volatile Solids
48.15
%
02/01/2022
SM 2540 G
ALB
QUALITY CONTROL - 02/01/2022
B-S/B-S DUP
Average
%RPD
o Total Solids
1.40
0 %
o Volatile Solids
48.22 %
0.3 %
Date Collected: 02/08/2022 Time Collected: 1232 Collected By: I DES
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.35
%
02/08/2022
SM 2540 G
DES
B-S
o Volatile Solids
48.25
%
02/08/2022
SM 2540 G
DES
B-S DUP
o Total Solids
1.40
%
02/08/2022
SM 2540 G
DES
B-S DUP
o Volatile Solids
48.21
%
02/08/2022
SM 2540 G
DES
QUALITY CONTROL - 02/08/2022
B-S/B-S DUP
Average
%RPD
o Total Solids
1.38 %
3.6 %
o Volatile Solids
48.23 %
0.1 %
Page 2 of 3

REPORT NO. 2022 BSQTRI
Date Collected: 02/15/2022 Time Collected: 0740 Collected By: I ALB
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.37
02/15/2022
SM 2540 G
ALB
B-S
o Volatile Solids
47.46
02/15/2022
SM 2540 G
ALB
B-S DUP
o Total Solids
1.37
%
02/15/2022
SM 2540 G
ALB
B-S DUP
o Volatile Solids
47.54
%
02/15/2022
SM 2540 G
ALB
QUALITY CONTROL - 02/15/2022
B-S/B-S DUP
Average
%RPD
o Total Solids
1.37 %
0 %
o Volatile Solids
47.50 %
0.2 %
Date Collected: 02/18/2022 Time Collected: 0730 Collected By: I ALB
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.42
%
02/22/2022
SM 2540 G
ALB
B-S
o Volatile Solids
48.71
%
02/22/2022
SM 2540 G
ALB
B-S DUP
o Total Solids
1.43
%
02/22/2022
SM 2540 G
ALB
B-S DUP
o Volatile Solids
48.85
02/22/2022
SM 2540 G
ALB
QUALITY CONTROL - 02/18/2022
B-S/B-S DUP
Average
%RPD
o Total Solids
1.43 %
0.7 %
o Volatile Solids
48.78 %
0.3 %
*B-S: BENCH -SCALE
6-WEEK VOLATILE SOLIDS REDUCTION 2.1 El
Certified By:
L REN D. ACOSTA
Page 3 of 3

MCB CAMLEJ ELS
ATAD BENCH -SCALE VOLATILE SOLIDS REDUCTION ANALYSIS
Sample Date
Sample ID
Temp
(°C)
DO
(mg/L)
% TS
% VS
% VS Avg
Analyst
1/20/2022
BENCH
15.1
9.91
1.54
49.75
49.83
ALB
BENCH-DUP
1.54
49.90
1/25/2022
BENCH
11.2
10.09
1.57
49.04
49.24
DES
BENCH-DUP
1.54
49.43
2/1/2022
BENCH
19.8
6.78
1.40
48.29
48.22
ALB
BENCH-DUP
1.40
48.15
2/8/2022
BENCH
18.3
10.2
1.35
48.25
48.23
DES
BENCH-DUP
1.40
48.21
2/15/2022
BENCH
12.9
9.75
1.37
47.46
47.50
ALB
BENCH-DUP
1.37
47.54
2/18/2022
BENCH
23.7
I
7.73
1
1.42
48.71
48.78
ALB
BENCH-DUP
1.43
48.85
INITIAL VS (%) 49.83 VS
2.1%
FINAL VS (%) 48.78 REDUCTION
VS REDUCTION = (INITIAL VS - FINAL VS) / INITIAL VS X 100
*VS REDUCTION MUST BE < 15% TO MEET VECTOR ATTRACTION REDUCTION REQUIREMENTS
REV. 01 /2020

2ND QUARTER
Pathogen and Vector Attraction Reduction Form
and Lab Sheets

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: U.S. MCB CAMP LEJEUNE
WWTP Name: Camp Lejeune Advanced WWTP
WQ Permit Number:
NPDES Number:
Monitoring Period: From 4/l/2022 To 6/30/2022
WQ0012346
NCO063029
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) 0
1 Alt B (Alk Treatment) ❑ I Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) Q
I ' Process to Further Reduce Pathogens❑
If applicable to alternative performed (Class A
only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic 0
Beta Ray ' ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Allowable Level
Patho en Densit
g y
Number o
Frequency
Sample
Analytical
Parameter
in Sludge
Excee-
dences
of Analysis
Type
Tech -
nique
Minimum
Geo. Mean
aximuni
Units
2 x 10 to the
MPN
6th power
per gram of
Fecal Coliform
total solids
CFU
1000 mpn per gram
SM
of total solid (dry
5.79
9.64
110
0
Weekly
Grab
weight)
Gram/
9221 E
Salmonella bacteria
3 MPN per 4 grams
(in lieu of fecal
total solid (dry
coliform)
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction)
❑
Alt. 2 (40-day bench)
❑
Alt. 3 (30-day bench) 0
Wt. 4 (Spec. Oz uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization
❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
Alt. 10 (Incorporation)
❑
No vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Charles Scozzari Sue so , /Land A
Preparer Name a tl type or print)
Signature
Charles Scozzari Supervisor, WW/Land App
Land Applier WAeAnd jitle (if applicable)(type or print)
Date Signatg4of Land Applier (if applicable)
is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 05/02/2022
Report No.: 2022-APR ATAD Lab ID: 227
Sample ID:
T4B
Date Collected:
04/05/2022
Collected By:
ACOSTA
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.04
04/05/2022
SM 2540 G
ALB
o Volatile Solids
55.78
%
04/05/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
04/05/2022
Collected By:
ACOSTA
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.30
04/05/2022
SM 2540 G
ALB
o Volatile Solids
67.46
%
04/05/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
04/05/2022
Collected By:
ACOSTA
Time Collected:
0718
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.76
%
04/05/2022
SM 2540 G
ALB
o Volatile Solids
52.97
%
04/05/2022
SM 2540 G
ALB
Fecal Coliforms
6.52
MPN/gram
04/05/2022
SM 9221 C E
DES
Page 1 of 8

Sample ID:
T3B
Date Collected:
04/07/2022
Collected By:
ACOSTA
Time Collected:
0713
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.18
%
04/07/2022
SM 2540 G
DES
o Volatile Solids
66.44
%
04/07/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
04/07/2022
Collected By:
ACOSTA
Time Collected:
0713
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.12
04/07/2022
SM 2540 G
DES
o Volatile Solids
57.77
%
04/07/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2A
Date Collected:
04/12/2022
Collected By:
ACOSTA
Time Collected:
0727
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.37
%
04/12/2022
SM 2540 G
DES
o Volatile Solids
57.52
%
04/12/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
04/12/2022
Collected By:
ACOSTA
Time Collected:
0727
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.03
%
04/12/2022
SM 2540 G
DES
o Volatile Solids
64.55
%
04/12/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 2 of 8

Sample ID:
T4B
Date Collected:
04/12/2022
Collected By:
ACOSTA
Time Collected:
0727
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.97
%
04/12/2022
SM 2540 G
DES
o Volatile Solids
55.55
%
04/12/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
04/12/2022
Collected By:
ACOSTA
Time Collected:
0727
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.82
04/12/2022
SM 2540 G
DES
o Volatile Solids
69.19
%
04/12/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
04/12/2022
Collected By:
ACOSTA
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.11
%
04/12/2022
SM 2540 G
DES
o Volatile Solids
50.15
%
04/12/2022
SM 2540 G
DES
Fecal Coliforms
5.79
MPN/gram
04/12/2022
SM 9221 C E
DES
Sample ID:
BNR
Date Collected:
04/12/2022
Collected By:
ACOSTA
Time Collected:
0727
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.00
%
04/12/2022
SM 2540 G
DES
o Volatile Solids
46.64
%
04/12/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 3 of 8

Sample ID:
T2A
Date Collected:
04/14/2022
Collected By:
ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.35
%
04/19/2022
SM 2540 G
DES/ALB
o Volatile Solids
66.03
%
04/19/2022
SM 2540 G
DES/ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
04/14/2022
Collected By:
ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.91
%
04/19/2022
SM 2540 G
DES/ALB
o Volatile Solids
63.41
%
04/19/2022
SM 2540 G
DES/ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
04/14/2022
Collected By:
ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.04
%
04/19/2022
SM 2540 G
DES/ALB
o Volatile Solids
54.63
%
04/19/2022
SM 2540 G
DES/ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2A
Date Collected:
04/19/2022
Collected By:
WILLIAMS
Time Collected:
0723
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.73
%
04/19/2022
SM 2540 G
DES/ALB
o Volatile Solids
64.85
%
04/19/2022
SM 2540 G
DES/ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 4 of 8

Sample ID:
T3B
Date Collected:
04/19/2022
Collected By:
WILLIAMS
Time Collected:
0723
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.85
%
04/19/2022
SM 2540 G
DES/ALB
o Volatile Solids
60.80
%
04/19/2022
SM 2540 G
DES/ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
04/19/2022
Collected By:
WILLIAMS
Time Collected:
0723
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.03
%
04/19/2022
SM 2540 G
DES/ALB
o Volatile Solids
54.54
%
04/19/2022
SM 2540 G
DES/ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
04/19/2022
Collected By:
WILLIAMS
Time Collected:
0723
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.63
%
04/19/2022
SM 2540 G
DES/ALB
o Volatile Solids
66.50
%
04/19/2022
SM 2540 G
DES/ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
04/19/2022
Collected By:
WILLIAMS
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.50
%
04/19/2022
SM 2540 G
DES/ALB
o Volatile Solids
52.05
%
04/19/2022
SM 2540 G
DES/ALB
Fecal Coliforms
7.20
MPN/gram
04/19/2022
SM 9221 C E
DES
Page 5 of 8

Sample ID:
T2A
Date Collected:
04/21/2022
Collected By:
ACOSTA
Time Collected:
0820
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.75
%
04/21/2022
SM 2540 G
DES
o Volatile Solids
62.19
%
04/21/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
04/21/2022
Collected By:
ACOSTA
Time Collected:
0820
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.03
%
04/21/2022
SM 2540 G
DES
o Volatile Solids
60.13
%
04/21/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
04/21/2022
Collected By:
ACOSTA
Time Collected:
0820
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.10
%
04/21/2022
SM 2540 G
DES
o Volatile Solids
55.48
%
04/21/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
04/26/2022
Collected By:
ACOSTA
Time Collected:
0755
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.89
%
04/26/2022
SM 2540 G
DES
o Volatile Solids
55.70
%
04/26/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 6 of 8

Sample ID:
T3B
Date Collected:
04/26/2022
Collected By:
ACOSTA
Time Collected:
0755
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.24
%
04/26/2022
SM 2540 G
DES
o Volatile Solids
57.33
%
04/26/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
04/26/2022
Collected By:
ACOSTA
Time Collected:
0755
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.38
%
04/26/2022
SM 2540 G
DES
o Volatile Solids
59.08
%
04/26/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
04/26/2022
Collected By:
ACOSTA
Time Collected:
0755
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.41
%
04/26/2022
SM 2540 G
DES
o Volatile Solids
70.39
%
04/26/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
04/26/2022
Collected By:
ACOSTA
Time Collected:
0804
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.56
%
04/26/2022
SM 2540 G
DES
o Volatile Solids
54.15
%
04/26/2022
SM 2540 G
DES
Fecal Coliforms
7.03
MPN/gram
04/26/2022
SM 9221 C E
ALB
Page 7 of 8

Sample ID:
T2B
Date Collected:
04/28/2022
Collected By:
ACOSTA
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.29
%
04/28/2022
SM 2540 G
DES
o Volatile Solids
56.27
%
04/28/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
04/28/2022
Collected By:
ACOSTA
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.23
%
04/28/2022
SM 2540 G
DES
o Volatile Solids
60.08
%
04/28/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
04/28/2022
Collected By:
ACOSTA
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.15
%
04/28/2022
SM 2540 G
DES
o Volatile Solids
59.58
%
04/28/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Certified By:
L REN D. ACOSTA
Page 8 of 8

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 06/03/2022
Report No.: 2022-MAY ATAD Lab ID: 227
Sample ID:
T2B
Date Collected:
05/03/2022
Collected By:
DROSKI
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.15
05/03/2022
SM 2540 G
ALB
o Volatile Solids
55.44
%
05/03/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
05/03/2022
Collected By:
DROSKI
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.14
05/03/2022
SM 2540 G
ALB
o Volatile Solids
57.92
%
05/03/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4A
Date Collected:
05/03/2022
Collected By:
DROSKI
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.70
%
05/03/2022
SM 2540 G
ALB
o Volatile Solids
67.30
%
05/03/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
05/03/2022
SM 9221 C E
Page 1 of 9

Sample ID:
FEED
Date Collected:
05/03/2022
Collected By:
DROSKI
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.24
%
05/03/2022
SM 2540 G
ALB
o Volatile Solids
68.77
%
05/03/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
05/03/2022
Collected By:
DROSKI
Time Collected:
0751
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.56
05/03/2022
SM 2540 G
ALB
o Volatile Solids
54.11
%
05/03/2022
SM 2540 G
ALB
Fecal Coliforms
58.59
MPN/gram
05/03/2022
SM 9221 C E
ALB
Sample ID:
T2B
Date Collected:
05/05/2022
Collected By:
DROSKI
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.21
%
05/05/2022
SM 2540 G
ALB
o Volatile Solids
55.65
%
05/05/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
05/05/2022
Collected By:
DROSKI
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.28
%
05/05/2022
SM 2540 G
ALB
o Volatile Solids
60.27
%
05/05/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 2 of 9

Sample ID:
T4A
Date Collected:
05/05/2022
Collected By:
DROSKI
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.51
%
05/05/2022
SM 2540 G
ALB
o Volatile Solids
67.81
%
05/05/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
05/10/2022
Collected By:
DROSKI
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.23
05/10/2022
SM 2540 G
GS/ALB
o Volatile Solids
54.09
%
05/10/2022
SM 2540 G
GS/ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
05/10/2022
Collected By:
DROSKI
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.05
%
05/10/2022
SM 2540 G
GS/ALB
o Volatile Solids
57.27
%
05/10/2022
SM 2540 G
GS/ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
05/10/2022
Collected By:
DROSKI
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.18
%
05/10/2022
SM 2540 G
GS/ALB
o Volatile Solids
57.47
%
05/10/2022
SM 2540 G
GS/ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 3 of 9

Sample ID:
FEED
Date Collected:
05/10/2022
Collected By:
DROSKI
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.31
%
05/10/2022
SM 2540 G
GS/ALB
o Volatile Solids
67.16
%
05/10/2022
SM 2540 G
GS/ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
05/10/2022
Collected By:
DROSKI
Time Collected:
0727
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.86
%
05/10/2022
SM 2540 G
GS/ALB
o Volatile Solids
52.26
%
05/10/2022
SM 2540 G
GS/ALB
Fecal Coliforms
6.29
MPN/gram
05/10/2022
SM 9221 C E
ALB
Sample ID:
T2B
Date Collected:
05/12/2022
Collected By:
DROSKI
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.27
%
05/12/2022
SM 2540 G
GS
o Volatile Solids
53.70
%
05/12/2022
SM 2540 G
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3A
Date Collected:
05/12/2022
Collected By:
DROSKI
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.01
%
05/12/2022
SM 2540 G
GS
o Volatile Solids
64.91
%
05/12/2022
SM 2540 G
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 4 of 9

Sample ID:
T4B
Date Collected:
05/12/2022
Collected By:
DROSKI
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.08
%
05/12/2022
SM 2540 G
GS
o Volatile Solids
56.84
%
05/12/2022
SM 2540 G
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
BNR
Date Collected:
05/12/2022
Collected By:
DROSKI
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.02
%
05/12/2022
SM 2540 G
GS
o Volatile Solids
43.10
%
05/12/2022
SM 2540 G
GS
Fecal Coliforms
110
MPN/gram
05/12/2022
SM 9221 C E
GS
Sample ID:
T2B
Date Collected:
1 5/17/2022
Collected By:
DROSKI
Time Collected:
0723
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.10
%
5/17/2022
SM 2540 G
GS/LA
o Volatile Solids
55.15
%
5/17/2022
SM 2540 G
GS/LA
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3A
Date Collected:
5/17/2022
Collected By:
DROSKI
Time Collected:
0723
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.54
%
5/17/2022
SM 2540 G
GS/LA
o Volatile Solids
61.35
%
5/17/2022
SM 2540 G
GS/LA
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 5 of 9

Sample ID:
T4B
Date Collected:
1 5/17/2022
Collected By:
DROSKI
Time Collected:
0723
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.97
%
5/17/2022
SM 2540 G
GS/LA
o Volatile Solids
55.29
%
5/17/2022
SM 2540 G
GS/LA
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
5/17/2022
Collected By:
DROSKI
Time Collected:
0723
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.72
%
5/17/2022
SM 2540 G
GS/LA
o Volatile Solids
63.53
%
5/17/2022
SM 2540 G
GS/LA
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
1 5/17/2022
Collected By:
DROSKI
Time Collected:
0734
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.79
%
5/17/2022
SM 2540 G
GS/LA
o Volatile Solids
51.73
%
5/17/2022
SM 2540 G
GS/LA
Fecal Coliforms
6.45
MPN/gram
5/17/2022
SM 9221 C E
ALB
Sample ID:
T2B
Date Collected:
5/19/2022
Collected By:
DROSKI
Time Collected:
0728
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.06
%
5/19/2022
SM 2540 G
GS
o Volatile Solids
55.13
%
5/19/2022
SM 2540 G
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 6 of 9

Sample ID:
T4B
Date Collected:
1 5/19/2022
Collected By:
DROSKI
Time Collected:
0728
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.04
%
5/19/2022
SM 2540 G
GS
o Volatile Solids
55.75
%
5/19/2022
SM 2540 G
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
5/24/2022
Collected By:
DROSKI
Time Collected:
0728
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.91
%
05/24/2022
SM 2540 G
ALB
o Volatile Solids
56.96
%
05/24/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
1 5/24/2022
Collected By:
DROSKI
Time Collected:
0728
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.90
%
05/24/2022
SM 2540 G
ALB
o Volatile Solids
57.51
%
05/24/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
5/24/2022
Collected By:
DROSKI
Time Collected:
0728
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.93
%
05/24/2022
SM 2540 G
ALB
o Volatile Solids
62.08
%
05/24/2022
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 7 of 9

Sample ID:
CROM
Date Collected:
1 5/24/2022
Collected By:
DROSKI
Time Collected:
0741
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.56
%
05/24/2022
SM 2540 G
ALB
o Volatile Solids
54.22
%
05/24/2022
SM 2540 G
ALB
Fecal Coliforms
7.00
MPN/gram
5/24/2022
SM 9221 C E
ALB
Sample ID:
T2B
Date Collected:
5/26/2022
Collected By:
DROSKI
Time Collected:
0732
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.89
%
05/26/2022
SM 2540 G
ALB/DES
o Volatile Solids
58.33
%
05/26/2022
SM 2540 G
ALB/DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
1 5/26/2022
Collected By:
DROSKI
Time Collected:
0732
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.90
%
05/26/2022
SM 2540 G
ALB/DES
o Volatile Solids
59.17
%
05/26/2022
SM 2540 G
ALB/DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
5/31/2022
Collected By:
DROSKI
Time Collected:
0731
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.85
%
05/31/2022
SM 2540 G
GS/DES
o Volatile Solids
56.19
%
05/31/2022
SM 2540 G
GS/DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 8 of 9

Sample ID:
T4B
Date Collected:
1 5/31/2022
Collected By:
DROSKI
Time Collected:
0731
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.98
%
05/31/2022
SM 2540 G
GS/DES
o Volatile Solids
53.53
%
05/31/2022
SM 2540 G
GS/DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
5/31/2022
Collected By:
DROSKI
Time Collected:
0731
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
6.49
%
05/31/2022
SM 2540 G
GS/DES
o Volatile Solids
58.27
%
05/31/2022
SM 2540 G
GS/DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
1 5/31/2022
Collected By:
DROSKI
Time Collected:
0747
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.63
%
05/31/2022
SM 2540 G
GS/DES
o Volatile Solids
51.70
%
05/31/2022
SM 2540 G
GS/DES
Fecal Coliforms
6.82
MPN/gram
05/31/2022
SM 9221 C E
GS
Certified By:
L REN D. ACOSTA
Page 9 of 9

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 07/01/2022
Report No.: 2022-JUN ATAD Lab ID: 227
Sample ID:
T3A
Date Collected:
06/02/2022
Collected By:
DROSKI
Time Collected:
0704
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.37
06/02/2022
SM 2540 B
ALB/DES
o Volatile Solids
62.29
%
06/02/2022
SM 2540 B
ALB/DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
06/02/2022
Collected By:
DROSKI
Time Collected:
0704
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.78
06/02/2022
SM 2540 B
ALB/DES
o Volatile Solids
57.54
%
06/02/2022
SM 2540 B
ALB/DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
06/07/2022
Collected By:
RUBERTE
Time Collected:
0714
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.24
%
06/08/2022
SM 2540 B
ALB
o Volatile Solids
58.28
%
06/08/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 1 of 7

Sample ID:
T4B
Date Collected:
06/07/2022
Collected By:
RUBERTE
Time Collected:
0714
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.89
%
06/08/2022
SM 2540 B
ALB
o Volatile Solids
57.53
%
06/08/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
06/07/2022
Collected By:
RUBERTE
Time Collected:
0714
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.93
06/08/2022
SM 2540 B
ALB
o Volatile Solids
63.75
%
06/08/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
06/07/2022
Collected By:
ACOSTA
Time Collected:
0720
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.52
%
06/08/2022
SM 2540 B
ALB
o Volatile Solids
55.32
%
06/08/2022
SM 2540 B
ALB
Fecal Coliforms
7.11
MPN/gram
06/07/2022
SM 9221 C E
ALB
Sample ID:
T3B
Date Collected:
06/09/2022
Collected By:
DROSKI
Time Collected:
0727
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.19
%
06/09/2022
SM 2540 B
DES
o Volatile Solids
56.88
%
06/09/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 2 of 7

Sample ID:
T4B
Date Collected:
06/09/2022
Collected By:
DROSKI
Time Collected:
0727
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.97
%
06/09/2022
SM 2540 B
DES
o Volatile Solids
56.73
%
06/09/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3A
Date Collected:
06/14/2022
Collected By:
ACOSTA
Time Collected:
0709
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.79
06/14/2022
SM 2540 B
ALB
o Volatile Solids
61.50
%
06/14/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
06/14/2022
Collected By:
ACOSTA
Time Collected:
0709
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.04
%
06/14/2022
SM 2540 B
ALB
o Volatile Solids
55.68
%
06/14/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
06/14/2022
Collected By:
ACOSTA
Time Collected:
0709
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.36
%
06/14/2022
SM 2540 B
ALB
o Volatile Solids
62.14
%
06/14/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 3 of 7

Sample ID:
CROM
Date Collected:
06/14/2022
Collected By:
ACOSTA
Time Collected:
0714
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.53
%
06/14/2022
SM 2540 B
ALB
o Volatile Solids
54.15
%
06/14/2022
SM 2540 B
ALB
Fecal Coliforms
7.09
MPN/gram
06/14/2022
SM 9221 C E
ALB
Sample ID:
T3A
Date Collected:
06/16/2022
Collected By:
J. ACOSTA
Time Collected:
0645
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.72
%
06/16/2022
SM 2540 B
ALB
o Volatile Solids
59.82
%
06/16/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
06/16/2022
Collected By:
J. ACOSTA
Time Collected:
0645
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.19
%
06/16/2022
SM 2540 B
ALB
o Volatile Solids
55.16
%
06/16/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
06/21/2022
Collected By:
J. ACOSTA
Time Collected:
0717
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.47
%
06/21/2022
SM 2540 B
DES/ALB
o Volatile Solids
55.45
%
06/21/2022
SM 2540 B
DES/ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 4 of 7

Sample ID:
T4B
Date Collected:
06/21/2022
Collected By:
J. ACOSTA
Time Collected:
0717
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.06
%
06/21/2022
SM 2540 B
DES/ALB
o Volatile Solids
54.23
%
06/21/2022
SM 2540 B
DES/ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
06/21/2022
Collected By:
J. ACOSTA
Time Collected:
0717
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
5.25
%
06/21/2022
SM 2540 B
DES/ALB
o Volatile Solids
60.55
%
06/21/2022
SM 2540 B
DES/ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
06/21/2022
Collected By:
J. ACOSTA
Time Collected:
0723
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.48
%
06/21/2022
SM 2540 B
DES/ALB
o Volatile Solids
53.31
%
06/21/2022
SM 2540 B
DES/ALB
Fecal Coliforms
7.26
MPN/gram
06/21/2022
SM 9221 C E
LA
Sample ID:
T3B
Date Collected:
06/23/2022
Collected By:
DROSKI
Time Collected:
0716
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.64
%
06/23/2022
SM 2540 B
GS
o Volatile Solids
51.71
%
06/23/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 5 of 7

Sample ID:
T4B
Date Collected:
06/23/2022
Collected By:
DROSKI
Time Collected:
0716
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.18
%
06/23/2022
SM 2540 B
GS
o Volatile Solids
52.50
%
06/23/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
06/28/2022
Collected By:
J. ACOSTA
Time Collected:
0651
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.76
%
06/28/2022
SM 2540 B
ALB
o Volatile Solids
60.16
%
06/28/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
06/28/2022
Collected By:
J. ACOSTA
Time Collected:
0651
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.52
%
06/28/2022
SM 2540 B
ALB
o Volatile Solids
51.06
%
06/28/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
06/28/2022
Collected By:
J. ACOSTA
Time Collected:
0651
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.26
%
06/28/2022
SM 2540 B
ALB
o Volatile Solids
51.12
%
06/28/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 6 of 7

Sample ID:
CROM
Date Collected:
06/28/2022
Collected By:
J. ACOSTA
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.64
%
06/28/2022
SM 2540 B
ALB
o Volatile Solids
2.62
%
06/28/2022
SM 2540 B
ALB
Fecal Coliforms
6.84
MPN/gram
06/28/2022
SM 9221 C E
ALB
Sample ID:
T3B
Date Collected:
06/30/2022
Collected By:
J. ACOSTA
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.53
%
06/30/2022
SM 2540 B
ALB
o Volatile Solids
54.44
%
06/30/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
06/30/2022
Collected By:
J. ACOSTA
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.21
%
06/30/2022
SM 2540 B
ALB
o Volatile Solids
53.26
%
06/30/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Certified By:
L REN D. ACOSTA
Page 7 of 7

REPORT NO. 2022 BSQTR2
Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 05/18/2022
Report No.: 2022 BSQTR2 Lab ID: 227
Date Collected: 04/11/2022 Time Collected: 0730 Collected By: I ALB
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.91
%
04/12/2022
SM 2540 G
DES
B-S
o Volatile Solids
52.45
%
04/12/2022
SM 2540 G
DES
B-S DUP
o Total Solids
1.91
%
04/12/2022
SM 2540 G
DES
B-S DUP
o Volatile Solids
52.24
%
04/12/2022
SM 2540 G
DES
QUALITY CONTROL - 04/11/2022
B-S/B-S DUP
Average
%RPD
o Total Solids
1.91 %
0 %
o Volatile Solids
52.35 %
0.4 %
Date Collected: 04/18/2022 Time Collected: 1310 Collected By: I ALB
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.72
%
04/19/2022
SM 2540 G
DES/ALB
B-S
o Volatile Solids
51.98
%
04/19/2022
SM 2540 G
DES/ALB
B-S DUP
o Total Solids
1.71
%
04/19/2022
SM 2540 G
DES/ALB
B-S DUP
o Volatile Solids
52.06
%
04/19/2022
SM 2540 G
DES/ALB
QUALITY CONTROL - 04/19/2022
B-S/B-S DUP
Average
%RPD
o Total Solids
1.72 %
0.6 %
o Volatile Solids
52.02 %
0.2 %
Page 1 of 3

REPORT NO. 2022 BSQTR2
Date Collected: 4/25/2022 Time Collected: 1 1451 Collected By: I ALB
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.53
%
04/26/2022
SM 2540 G
DES
B-S
o Volatile Solids
51.67
%
04/26/2022
SM 2540 G
DES
B-S DUP
o Total Solids
1.54
%
04/26/2022
SM 2540 G
DES
B-S DUP
o Volatile Solids
51.58
%
04/26/2022
SM 2540 G
DES
QUALITY CONTROL - 04/25/2022
B-S/B-S DUP
Average
%RPD
o Total Solids
1.54
0.6 %
o Volatile Solids
51.63 %
0.2 %
Date Collected: 05/02/2022 Time Collected: 0736 Collected By: I DES
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.62
%
05/03/2022
SM 2540 G
ALB
B-S
o Volatile Solids
51.06
%
05/03/2022
SM 2540 G
ALB
B-S DUP
o Total Solids
1.63
%
05/03/2022
SM 2540 G
ALB
B-S DUP
o Volatile Solids
50.89
%
05/03/2022
SM 2540 G
ALB
QUALITY CONTROL - 05/02/2022
B-S/B-S DUP
Average
%RPD
o Total Solids
1.63 %
0.6 %
o Volatile Solids
50.98 %
0.3 %
Page 2 of 3

REPORT NO. 2022 BSQTR2
Date Collected: 05/10/2022 Time Collected: 0927 Collected By: I ALB
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.66
%
05/10/2022
SM 2540 G
ALB
B-S
o Volatile Solids
45.16
%
05/10/2022
SM 2540 G
ALB
B-S DUP
o Total Solids
1.69
%
05/10/2022
SM 2540 G
ALB
B-S DUP
o Volatile Solids
44.41
%
05/10/2022
SM 2540 G
ALB
QUALITY CONTROL - 05/10/2022
B-S/B-S DUP
Average
%RPD
o Total Solids
1.68 %
1.8 %
o Volatile Solids
44.79 %
1.7 %
*B-S: BENCH -SCALE
6-WEEK VOLATILE SOLIDS REDUCTION 14.4 $
Certified By:
LAkJREN D. ACOSTA
Page 3 of 3

MCB CAMLEJ ELS
ATAD BENCH -SCALE VOLATILE SOLIDS REDUCTION ANALYSIS
Sample Date
Sample ID
Temp
C
DO
m /L
% TS
% VS
% VS Avg
Analyst
4/11/2022
BENCH
15.7
7 6
1.91
52.45
52.35
DES
BENCH-DUP
1.91
52.24
4/18/2022
BENCH
19.9
5.1
1.72
51.98
52.02
DES/ALB
BENCH-DUP
1.71
52.06
4/25/2022
BENCH
21.7
7.4
1.53
51.67
51.63
BENCH-DUP
1.54
51.58
5/2/2022
BENCH
22.5
6.4
1.62
51.06
50.98
BENCH-DUP
1.63
50.89
5/10/2022
BENCH
18.5
6.2
1.66
45.16
44.79
BENCH-DUP
1.69
44.41
INITIAL VS (%) 52.35 VS
FINAL VS (%) 44.79 REDUCTION 14.4%
VS REDUCTION = (INITIAL VS - FINAL VS) / INITIAL VS X 100
*VS REDUCTION MUST BE < 15% TO MEET VECTOR ATTRACTION REDUCTION REQUIREMENTS
REV. 01 /2020

3RD QUARTER
Pathogen and Vector Attraction Reduction Form
and Lab Sheets

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: U.S. MCB CAMP LEJEUNE WQ Permit Number: WQ0012346
WWTP Name: Camp Lejeune Advanced WWTP
NPDES Number: NCO063029
Monitoring Period: From 7/l/2022 To 9/30/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) 0
Alt B (Alk Treatment) ElAlt.
C (Prior Testing) ❑
A1t.D (No Prior Test)
I Process to Further Reduce Pathogens 0
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑ Heat Treatment ❑
Thenmophilic 2
Beta Ray ❑
Gamma Ray ❑ Pasteurization ❑
Class B: 171t.
(1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in Sludge
Patho en DenSlt
g y
Number of
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -
niciue
Minimum
Geo. Mean
Maximud
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
6.38
7.18
16.51
Gram/
0
Weekly
Grab
SM
922 CE
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction)
❑
Alt. 2 (40-day bench)
❑
Alt. 3 (30-day bench) 0
jAlt. 4 (Spec. OZ uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization
❑
Alt 7 (Drying - Stable) ❑Alt.
8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
Alt. 10 (Incorporation)
❑
No vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Charles Scozzari Su Ervis , WW/Land
Preparer Name Sid triti,p,ftype or print)
Signature
c/
Charles Scozzari
%kisor, WW/Land A
Land Applier N,#J�d Title (if applicable)(type or print)
61
of Land Applier (if applicable)
ate
is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T /,A 02 (26)
DENR FORM PVRF 02T (12/2006)

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 08/09/2022
Report No.: 2022-JUL ATAD Lab ID: 227
Sample ID:
T3B
Date Collected:
07/05/2022
Collected By:
WILLIAMS
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.44
07/05/2022
SM 2540 B
ALB/DES
o Volatile Solids
54.00
%
07/05/2022
SM 2540 B
ALB/DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
07/05/2022
Collected By:
WILLIAMS
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.15
07/05/2022
SM 2540 B
ALB/DES
o Volatile Solids
54.02
%
07/05/2022
SM 2540 B
ALB/DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
07/05/2022
Collected By:
WILLIAMS
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.48
%
07/05/2022
SM 2540 B
ALB/DES
o Volatile Solids
61.00
%
07/05/2022
SM 2540 B
ALB/DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 1 of 7

Sample ID:
CROM
Date Collected:
07/05/2022
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
1.09
%
07/05/2022
SM 2540 B
ALB/DES
o Volatile Solids
60.35
%
07/05/2022
SM 2540 B
ALB/DES
Fecal Coliforms
16.51
MPN/gram
07/05/2022
SM 9221 C E
ALB
Sample ID:
T3B
Date Collected:
07/07/2022
Collected By:
DROSKI
Time Collected:
0720
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.54
07/07/2022
SM 2540 B
ALB
o Volatile Solids
53.07
%
07/07/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
07/07/2022
Collected By:
DROSKI
Time Collected:
0720
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.24
%
07/07/2022
SM 2540 B
ALB
o Volatile Solids
52.89
%
07/07/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM (TS)
Date Collected:
07/07/2022
Collected By:
DROSKI
Time Collected:
0720
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.59
%
07/07/2022
SM 2540 B
ALB
o Volatile Solids
53.10
%
07/07/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 2 of 7

Sample ID:
T3B
Date Collected:
07/12/2022
Collected By:
DROSKI
Time Collected:
0708
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.74
%
07/12/2022
SM 2540 B
DES
o Volatile Solids
53.33
%
07/12/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
07/12/2022
Collected By:
DROSKI
Time Collected:
0708
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.31
07/12/2022
SM 2540 B
DES
o Volatile Solids
52.68
%
07/12/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
07/12/2022
Collected By:
DROSKI
Time Collected:
0708
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.44
%
07/12/2022
SM 2540 B
DES
o Volatile Solids
60.82
%
07/12/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
07/12/2022
Collected By:
DROSKI
Time Collected:
0718
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.64
%
07/12/2022
SM 2540 B
DES
o Volatile Solids
53.00
%
07/12/2022
SM 2540 B
DES
Fecal Coliforms
6.79
MPN/gram
07/12/2022
SM 9221 C E
DES
Page 3 of 7

Sample ID:
T3B
Date Collected:
07/14/2022
Collected By:
WILLIAMS
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.89
%
07/14/2022
SM 2540 B
GS
o Volatile Solids
50.97
%
07/14/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
07/14/2022
Collected By:
WILLIAMS
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.50
%
07/14/2022
SM 2540 B
GS
o Volatile Solids
51.73
%
07/14/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
07/14/2022
Collected By:
WILLIAMS
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.45
%
07/14/2022
SM 2540 B
GS
o Volatile Solids
58.22
%
07/14/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
07/19/2022
Collected By:
J. ACOSTA
Time Collected:
0630
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.90
%
07/21/2022
SM 2540 B
ALB
o Volatile Solids
58.70
%
07/21/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 4 of 7

Sample ID:
T3B
Date Collected:
07/19/2022
Collected By:
J. ACOSTA
Time Collected:
0630
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.46
%
07/21/2022
SM 2540 B
ALB
o Volatile Solids
50.49
%
07/21/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
07/19/2022
Collected By:
J. ACOSTA
Time Collected:
0630
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.26
%
07/21/2022
SM 2540 B
ALB
o Volatile Solids
49.60
%
07/21/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
07/19/2022
Collected By:
J. ACOSTA
Time Collected:
0630
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.65
%
07/21/2022
SM 2540 B
ALB
o Volatile Solids
51.05
%
07/21/2022
SM 2540 B
ALB
Fecal Coliforms
6.79
MPN/gram
07/19/2022
SM 9221 C E
DES
Sample ID:
T3B
Date Collected:
07/21/2022
Collected By:
RUBERTE
Time Collected:
0712
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.50
%
07/21/2022
SM 2540 B
ALB
o Volatile Solids
51.72
%
07/21/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 5 of 7

Sample ID:
T4B
Date Collected:
07/21/2022
Collected By:
RUBERTE
Time Collected:
0712
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.24
%
07/21/2022
SM 2540 B
ALB
o Volatile Solids
49.65
%
07/21/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
07/26/2022
Collected By:
J. ACOSTA
Time Collected:
0705
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.95
%
07/26/2022
SM 2540 B
ALB
o Volatile Solids
54.33
%
07/26/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
07/26/2022
Collected By:
J. ACOSTA
Time Collected:
0705
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.61
%
07/26/2022
SM 2540 B
ALB
o Volatile Solids
59.72
%
07/26/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
07/26/2022
Collected By:
J. ACOSTA
Time Collected:
0717
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.75
%
07/26/2022
SM 2540 B
ALB
o Volatile Solids
51.28
%
07/26/2022
SM 2540 B
ALB
Fecal Coliforms
6.52
MPN/gram
07/26/2022
SM 9221 C E
DES
Page 6 of 7

Sample ID:
T3B
Date Collected:
07/28/2022
Collected By:
J. ACOSTA
Time Collected:
0620
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.74
%
08/02/2022
SM 2540 B
ALB
o Volatile Solids
51.99
%
08/02/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Certified By:
LP&REN D. ACOSTA
Page 7 of 7

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 09/08/2022
Report No.: 2022-AUG ATAD Lab ID: 227
Sample ID:
FEED
Date Collected:
08/02/2022
Collected By:
J. ACOSTA
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.06
%
08/02/2022
SM 2540 B
ALB
o Volatile Solids
58.65
%
08/02/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
08/02/2022
Collected By:
J. ACOSTA
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.65
%
08/02/2022
SM 2540 B
ALB
o Volatile Solids
50.57
%
08/02/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
08/02/2022
Collected By:
J. ACOSTA
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.73
%
08/02/2022
SM 2540 B
LA
o Volatile Solids
52.35
%
08/02/2022
SM 2540 B
LA
Fecal Coliforms
6.59
MPN/gram
08/02/2022
SM 9221 C E
GS
Page 1 of 5

Sample ID:
T3B
Date Collected:
08/04/2022
Collected By:
J. ACOSTA
Time Collected:
0820
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.71
%
08/04/2022
SM 2540 B
ALB
o Volatile Solids
51.30
%
08/04/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
08/09/2022
Collected By:
J. ACOSTA
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.50
%
08/09/2022
SM 2540 B
DES
o Volatile Solids
60.09
%
08/09/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
08/09/2022
Collected By:
J. ACOSTA
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.69
%
08/09/2022
SM 2540 B
DES
o Volatile Solids
51.82
%
08/09/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
08/09/2022
Collected By:
J. ACOSTA
Time Collected:
0755
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.71
%
08/09/2022
SM 2540 B
DES
o Volatile Solids
51.97
%
08/09/2022
SM 2540 B
DES
Fecal Coliforms
6.64
MPN/gram
08/09/2022
SM 9221 C E
DES
Page 2 of 5

Sample ID:
T3B
Date Collected:
08/11/2022
Collected By:
J. ACOSTA
Time Collected:
0635
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.05
%
08/16/2022
SM 2540 B
ALB
o Volatile Solids
50.74
%
08/16/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
08/16/2022
Collected By:
RUBERTE
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.75
%
08/16/2022
SM 2540 B
ALB
o Volatile Solids
50.10
%
08/16/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
08/16/2022
Collected By:
RUBERTE
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.98
%
08/16/2022
SM 2540 B
ALB
o Volatile Solids
58.34
%
08/16/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
08/16/2022
Collected By:
RUBERTE
Time Collected:
0738
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.74
08/16/2022
SM 2540 B
ALB
o Volatile Solids
50.55
%
08/16/2022
SM 2540 B
ALB
Fecal Coliforms
6.57
MPN/gram
08/16/2022
SM 9221 C E
ALB
Page 3 of 5

Sample ID:
T3B
Date Collected:
08/18/2022
Collected By:
J. ACOSTA
Time Collected:
0748
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.90
%
08/23/2022
SM 2540 B
ALB
o Volatile Solids
54.46
%
08/23/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
08/23/2022
Collected By:
J. ACOSTA
Time Collected:
0645
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.24
08/23/2022
SM 2540 B
ALB
o Volatile Solids
60.10
%
08/23/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
08/23/2022
Collected By:
J. ACOSTA
Time Collected:
0645
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.37
%
08/23/2022
SM 2540 B
ALB
o Volatile Solids
52.43
%
08/23/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
08/23/2022
Collected By:
J. ACOSTA
Time Collected:
0702
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.31
%
08/23/2022
SM 2540 B
ALB
o Volatile Solids
52.77
%
08/23/2022
SM 2540 B
ALB
Fecal Coliforms
7.79
MPN/gram
08/23/2022
SM 9221 C E
ALB
Page 4of5

Sample ID:
T2B
Date Collected:
08/25/2022
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.24
%
08/30/2022
SM 2540 B
ALB
o Volatile Solids
50.45
%
08/30/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
08/30/2022
Collected By:
J. ACOSTA
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.20
08/30/2022
SM 2540 B
ALB
o Volatile Solids
50.48
%
08/30/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
08/30/2022
Collected By:
J. ACOSTA
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.28
%
08/30/2022
SM 2540 B
ALB
o Volatile Solids
59.51
%
08/30/2022
SM 2540 B
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
08/30/2022
Collected By:
J. ACOSTA
Time Collected:
0708
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.72
08/30/2022
SM 2540 B
ALB
o Volatile Solids
50.29
%
08/30/2022
SM 2540 B
ALB
Fecal Coliforms
6.62
MPN/gram
08/30/2022
SM 9221 C E
ALB
Certified By:
L REN D. ACOSTA
Page 5 of 5

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 10/06/2022
Report No.: 2022-SEP ATAD Lab ID: 227
Sample ID:
T2B
Date Collected:
09/01/2022
Collected By:
J. ACOSTA
Time Collected:
0625
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.97
09/07/2022
SM 2540 B
GS
o Volatile Solids
57.72
%
09/07/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
09/06/2022
Collected By:
J. ACOSTA
Time Collected:
0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.21
09/07/2022
SM 2540 B
GS
o Volatile Solids
59.87
%
09/07/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
09/06/2027
Collected By:
J. ACOSTA
Time Collected:
0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.42
%
09/07/2022
SM 2540 B
GS
o Volatile Solids
52.34
%
09/07/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 1 of 6

Sample ID:
CROM
Date Collected:
09/06/2022
Collected By:
J. ACOSTA
Time Collected:
0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.80
%
09/07/2022
SM 2540 B
GS
o Volatile Solids
50.31
%
09/07/2022
SM 2540 B
GS
Fecal Coliforms
6.4
MPN/gram
09/06/2022
SM 9221 C E
ALB
Sample ID:
T2B
Date Collected:
09/08/2022
Collected By:
J. ACOSTA
Time Collected:
0628
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.80
09/13/2022
SM 2540 B
GS/DES
o Volatile Solids
51.19
%
09/13/2022
SM 2540 B
GS/DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
09/13/2022
Collected By:
J. ACOSTA
Time Collected:
0643
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.13
%
09/13/2022
SM 2540 B
GS/DES
o Volatile Solids
59.04
%
09/13/2022
SM 2540 B
GS/DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
09/13/2022
Collected By:
J. ACOSTA
Time Collected:
0643
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.79
%
09/13/2022
SM 2540 B
GS/DES
o Volatile Solids
51.57
%
09/13/2022
SM 2540 B
GS/DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 2 of 6

Sample ID:
CROM
Date Collected:
09/13/2022
Collected By:
J. ACOSTA
Time Collected:
0701
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.82
%
09/13/2022
SM 2540 B
GS/DES
o Volatile Solids
49.46
%
09/13/2022
SM 2540 B
GS/DES
Fecal Coliforms
6.38
MPN/gram
09/13/2022
SM 9221 C E
GS/DES
Sample ID:
T2B
Date Collected:
09/15/2022
Collected By:
J. ACOSTA
Time Collected:
0640
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.64
09/20/2022
SM 2540 B
GS
o Volatile Solids
51.38
%
09/20/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
09/20/2022
Collected By:
J. ACOSTA
Time Collected:
0746
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.55
%
09/20/2022
SM 2540 B
GS
o Volatile Solids
59.27
%
09/20/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
09/20/2022
Collected By:
J. ACOSTA
Time Collected:
0746
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.72
%
09/20/2022
SM 2540 B
GS
o Volatile Solids
48.85
%
09/20/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 3 of 6

Sample ID:
CROM
Date Collected:
09/20/2022
Collected By:
J. ACOSTA
Time Collected:
0739
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.69
%
09/20/2022
SM 2540 B
GS
o Volatile Solids
49.50
%
09/20/2022
SM 2540 B
GS
Fecal Coliforms
6.69
MPN/gram
09/20/2022
SM 9221 C E
LA
Sample ID:
T2B
Date Collected:
09/22/2022
Collected By:
J. ACOSTA
Time Collected:
0630
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.50
%
09/27/2022
SM 2540 B
GS
o Volatile Solids
52.29
%
09/27/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3A
Date Collected:
09/22/2022
Collected By:
J. ACOSTA
Time Collected:
0630
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.57
%
09/27/2022
SM 2540 B
GS
o Volatile Solids
58.95
%
09/27/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
09/27/2022
Collected By:
J. ACOSTA
Time Collected:
0630
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.25
%
09/27/2022
SM 2540 B
GS
o Volatile Solids
58.70
%
09/27/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 4 of 6

Sample ID:
T2B
Date Collected:
09/27/2022
Collected By:
J. ACOSTA
Time Collected:
0630
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.58
%
09/27/2022
SM 2540 B
GS
o Volatile Solids
51.03
%
09/27/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3A
Date Collected:
09/27/2022
Collected By:
J. ACOSTA
Time Collected:
0630
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.46
%
09/27/2022
SM 2540 B
GS
o Volatile Solids
56.05
%
09/27/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
09/27/2022
Collected By:
J. ACOSTA
Time Collected:
0738
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.68
%
09/27/2022
SM 2540 B
GS
o Volatile Solids
49.76
%
09/27/2022
SM 2540 B
GS
Fecal Coliforms
6.72
MPN/gram
09/27/2022
SM 9221 C E
DES
Sample ID:
T2B
Date Collected:
09/29/2022
Collected By:
J. ACOSTA
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.47
%
10/05/2022
SM 2540 B
DES
o Volatile Solids
50.87
%
10/05/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 5 of 6

Sample ID:
T3A
Date Collected:
09/29/2022
Collected By:
J. ACOSTA
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.32
%
10/05/2022
SM 2540 B
DES
o Volatile Solids
54.36
%
10/05/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Certified By:
LP&REN D. ACOSTA
Page 6 of 6

REPORT NO. 2022 BSQTR3
Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 09/12/2022
Report No.: 2022 BSQTR3 Lab ID: 227
Date Collected: 08/03/2022 Time Collected: 1246 Collected By: I ALB
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
2.03
%
08/04/2022
SM 2540 B
ALB
B-S
o Volatile Solids
51.04
%
08/04/2022
SM 2540 B
ALB
B-S DUP
o Total Solids
2.04
%
08/04/2022
SM 2540 B
ALB
B-S DUP
o Volatile Solids
51.18
%
08/04/2022
SM 2540 B
ALB
QUALITY CONTROL - 08/03/2022
B-S/B-S DUP
Average
%RPD
o Total Solids
2.04 %
0.5 %
o Volatile Solids
51.11 %
0.3 %
Date Collected: 08/08/2022 Time Collected: 0815 Collected By: I ALB
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.89
%
08/09/2022
SM 2540 B
DES/LA
B-S
o Volatile Solids
52.12
%
08/09/2022
SM 2540 B
DES/LA
B-S DUP
o Total Solids
1.90
%
08/09/2022
SM 2540 B
DES/LA
B-S DUP
o Volatile Solids
51.96
%
08/09/2022
SM 2540 B
DES/LA
QUALITY CONTROL - 08/08/2022
B-S/B-S DUP
Average
%RPD
o Total Solids
1.90 %
0.5 %
o Volatile Solids
52.04 %
0.3 %
Page 1 of 3

REPORT NO. 2022 BSQTR3
Date Collected: 08/15/2022 Time Collected: 0851 Collected By: I GS
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.84
%
08/16/2022
SM 2540 B
ALB
B-S
o Volatile Solids
51.57
%
08/16/2022
SM 2540 B
ALB
B-S DUP
o Total Solids
1.83
%
08/16/2022
SM 2540 B
ALB
B-S DUP
o Volatile Solids
50.55
%
08/16/2022
SM 2540 B
ALB
QUALITY CONTROL - 08/15/2022
B-S/B-S DUP
Average
%RPD
o Total Solids
1.84
0.5 %
o Volatile Solids
51.44 %
0.5 %
Date Collected: 08/22/2022 Time Collected: 0758 Collected By: I ALB
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.69
%
08/23/2022
SM 2540 B
ALB
B-S
o Volatile Solids
52.94
%
08/23/2022
SM 2540 B
ALB
B-S DUP
o Total Solids
1.69
%
08/23/2022
SM 2540 B
ALB
B-S DUP
o Volatile Solids
52.91
%
08/23/2022
SM 2540 B
ALB
QUALITY CONTROL - 08/22/2022
B-S/B-S DUP
Average
%RPD
o Total Solids
1.69 %
0.0 %
o Volatile Solids
52.93 %
0.1 %
Page 2 of 3

REPORT NO. 2022 BSQTR3
Date Collected: 08/29/2022 Time Collected: 0817 Collected By: I ALB
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.60
%
08/30/2022
SM 2540 B
ALB
B-S
o Volatile Solids
50.68
%
08/30/2022
SM 2540 B
ALB
B-S DUP
o Total Solids
1.61
%
08/30/2022
SM 2540 B
ALB
B-S DUP
o Volatile Solids
51.05
%
08/30/2022
SM 2540 B
ALB
QUALITY CONTROL - 08/29/2022
B-S/B-S DUP
Average
%RPD
o Total Solids
1.61 %
0.6 %
o Volatile Solids
50.87 %
0.7 %
Date Collected: 09/06/2022 Time Collected: 0815 Collected By: I ALB
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.53
%
09/07/2022
SM 2540 B
GS
B-S
o Volatile Solids
52.83
%
09/07/2022
SM 2540 B
GS
B-S DUP
o Total Solids
1.54
%
09/07/2022
SM 2540 B
GS
B-S DUP
o Volatile Solids
52.73
%
09/07/2022
SM 2540 B
GS
QUALITY CONTROL - 09/06/2022
B-S/B-S DUP
Average
%RPD
o Total Solids
1.54 %
0.7 %
o Volatile Solids
52.78 %
0.2 %
*B-S: BENCH -SCALE
6-WEEK VOLATILE SOLIDS REDUCTION -3.3 %
Certified By:
L RE�ACOSTA
Page 3 of 3

MCB CAMLEJ ELS
ATAD BENCH -SCALE VOLATILE SOLIDS REDUCTION ANALYSIS
Sample Date
Sample ID
Tom p
(m O
% TS
% VS
% VS Avg
Analyst
8/3/2022
BENCH
21.1
6.50
2.03
51.04
51.11
ALB
BENCH-DUP
2.04
51.18
8/8/2022
BENCH
21.2
6.28
1.89
52.12
52.04
DES
BENCH-DUP
1.90
51.96
8/15/2022
BENCH
21.2
2.41
1.84
51.57
51.44
ALB
BENCH-DUP
1.83
51.31
8/22/2022
BENCH
21.7
6.9
1.69
52.94
52.93
ALB
BENCH-DUP
1.69
52.91
8/29/2022
BENCH
21.7
8.45
1.60
50.68
50.87
ALB
BENCH-DUP
1.61
51.05
9/6/2022
BENCH
21.7
8.13
1
1.53
52.83
52.78
ALB
BENCH-DUP 1
1.54
52.73
INITIAL VS (%) 51.11 VS
-3.3%
FINAL VS (%) 52.78 REDUCTION
VS REDUCTION = (INITIAL VS - FINAL VS) / INITIAL VS X 100
*VS REDUCTION MUST BE < 15% TO MEET VECTOR ATTRACTION REDUCTION REQUIREMENTS
REV. 01 /2020

4TH QUARTER
Pathogen and Vector Attraction Reduction Form
and Lab Sheets

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: U.S. MCB CAMP LEJEUNE WQ Permit Number: WQ0012346
WWTP Name: Camp Lejeune Advanced WWTP
Monitoring Period: From 10/1/2022 To
NPDES Number: NCO063029
12/31 /2022
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) 21D Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
I Process to Further Reduce Pathogens r❑
If applicable to alternative performed (Class A
only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic 21
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
JAlt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B
only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
I Composting ❑ Aerobic Digestion ❑
Anaerobic Digestion ❑
- -- -- - - ---- - - - ---- - ---- -- .. .
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g y
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
n alyt►caI
Tech -
nioue
inimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
5.43
27.96
4163 *
gam/
2
Weekly
Grab
SM
922 CE
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
I weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been Md.!
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Charles Scozzar' upeyvisor, WW/Land App Charles Scozzarjervisor, WW/Land App
Preparer Naqf(an4 itle (type or print)
of
Land Applier N
.12
713'-
ate Si2nature/f[Lai
Title (if applicable)(type or print)
G
Applier (if applicable) ate
is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
* Note: Please see cover letter for explanation on pathogen density.
DENR FORM PVRF 02T (12/2006)

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 11/14/2022
Report No.: 2022-OCT ATAD Lab ID: 227
Sample ID:
T2B
Date Collected:
10/04/2022
Collected By:
J. ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.42
10/05/2022
SM 2540 B
DES
o Volatile Solids
51.21
%
10/05/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
10/04/2022
Collected By:
J. ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.53
10/05/2022
SM 2540 B
DES
o Volatile Solids
52.59
%
10/05/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
10/04/2022
Collected By:
J. ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.37
%
10/05/2022
SM 2540 B
DES
o Volatile Solids
58.99
%
10/05/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 1 of 7

Sample ID:
CROM
Date Collected:
10/04/2022
Collected By:
J. ACOSTA
Time Collected:
0747
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.67
%
10/05/2022
SM 2540 B
DES
o Volatile Solids
49.95
%
10/05/2022
SM 2540 B
DES
Fecal Coliforms
6.74
MPN/gram
10/05/2022
SM 9221 C E
LA
Sample ID:
T2B
Date Collected:
10/06/2022
Collected By:
J. ACOSTA
Time Collected:
0645
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.34
10/11/2022
SM 2540 B
DES
o Volatile Solids
51.50
%
10/11/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
10/06/2022
Collected By:
J. ACOSTA
Time Collected:
0645
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.32
%
10/11/2022
SM 2540 B
DES
o Volatile Solids
53.38
%
10/11/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
10/11/2022
Collected By:
WILLIAMS
Time Collected:
0650
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.60
%
10/11/2022
SM 2540 B
DES
o Volatile Solids
50.27
%
10/11/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 2 of 7

Sample ID:
T3B
Date Collected:
10/11/2022
Collected By:
WILLIAMS
Time Collected:
0650
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.06
%
10/11/2022
SM 2540 B
DES
o Volatile Solids
52.31
%
10/11/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
10/11/2022
Collected By:
WILLIAMS
Time Collected:
0650
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.88
10/11/2022
SM 2540 B
DES
o Volatile Solids
60.23
%
10/11/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
10/11/2022
Collected By:
WILLIAMS
Time Collected:
0705
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.69
%
10/11/2022
SM 2540 B
DES
o Volatile Solids
60.43
%
10/11/2022
SM 2540 B
DES
Fecal Coliforms
6.69
MPN/gram
10/11/2022
SM 9221 C E
DES
Sample ID:
T3B
Date Collected:
10/13/2022
Collected By:
EJ RUBERTE
I Time Collected:
0710
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.59
%
10/20/2022
SM 2540 B
DES
o Volatile Solids
51.97
%
10/20/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 3 of 7

Sample ID:
T2B
Date Collected:
10/13/2022
Collected By:
EJ RUBERTE
I Time Collected:
0710
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.71
%
10/20/2022
SM 2540 B
DES
o Volatile Solids
52.23
%
10/20/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
10/18/2022
Collected By:
J ACOSTA
Time Collected:
0654
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.55
%
10/20/2022
SM 2540 B
DES
o Volatile Solids
61.45
%
10/20/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
10/18/2022
Collected By:
J ACOSTA
Time Collected:
0654
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.69
%
10/20/2022
SM 2540 B
DES
o Volatile Solids
51.98
%
10/20/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
10/18/2022
Collected By:
J ACOSTA
Time Collected:
0654
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.99
%
10/20/2022
SM 2540 B
DES
o Volatile Solids
49.83
%
10/20/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 4 of 7

Sample ID:
CROM
Date Collected:
10/18/2022
Collected By:
J ACOSTA
Time Collected:
0706
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.70
%
10/20/2022
SM 2540 B
DES
o Volatile Solids
50.29
%
10/20/2022
SM 2540 B
DES
Fecal Coliforms
6.67
MPN/gram
10/18/2022
SM 9221 C E
LA
Sample ID:
T3B
Date Collected:
10/20/2022
Collected By:
J. ACOSTA
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.49
%
10/25/2022
SM 2540 B
DES
o Volatile Solids
53.71
%
10/25/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
10/20/2022
Collected By:
J. ACOSTA
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.79
%
10/25/2022
SM 2540 B
DES
o Volatile Solids
52.83
%
10/25/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
10/25/2022
Collected By:
J. ACOSTA
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.69
%
10/25/2022
SM 2540 B
DES
o Volatile Solids
51.84
%
10/25/2022
SM 2540 B
DES
Fecal Coliforms
5.43
MPN/gram
10/25/2022
SM 9221 C E
DES
Page 5 of 7

Sample ID:
FEED
Date Collected:
10/25/2022
Collected By:
J. ACOSTA
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.88
%
10/26/2022
SM 2540 B
DES
o Volatile Solids
61.75
%
10/26/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
10/25/2022
Collected By:
J. ACOSTA
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.73
%
10/26/2022
SM 2540 B
DES
o Volatile Solids
52.20
%
10/26/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4A
Date Collected:
10/25/2022
Collected By:
J. ACOSTA
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.53
%
10/26/2022
SM 2540 B
DES
o Volatile Solids
61.58
%
10/26/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
10/25/2022
Collected By:
J. ACOSTA
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.74
%
10/26/2022
SM 2540 B
DES
o Volatile Solids
50.79
%
10/26/2022
SM 2540 B
DES
Fecal Coliforms
6.57
MPN/gram
10/25/2022
SM 9221 C E
DES
Page 6 of 7

Sample ID:
T3B
Date Collected:
10/27/2022
Collected By:
DES
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.22
%
10/27/2022
SM 2540 B
DES
o Volatile Solids
51.77
%
10/27/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
10/27/2022
Collected By:
DES
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.65
%
10/27/2022
SM 2540 B
DES
o Volatile Solids
50.93
%
10/27/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4A
Date Collected:
10/27/2022
Collected By:
DES
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.47
%
10/27/2022
SM 2540 B
DES
o Volatile Solids
61.18
%
10/27/2022
SM 2540 B
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Certified By:
L REN D. ACOSTA
Page 7 of 7

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 12/02/2022
Report No.: 2022-NOV ATAD Lab ID: 227
Sample ID:
T2B
Date Collected:
11/01/2022
Collected By:
M. SHIVAR
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.23
11/01/2022
SM 2540 B
GS
o Volatile Solids
53.87
%
11/01/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
11/01/2022
Collected By:
M. SHIVAR
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.86
11/01/2022
SM 2540 B
GS
o Volatile Solids
49.67
%
11/01/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
11/01/2022
Collected By:
M. SHIVAR
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.93
%
11/01/2022
SM 2540 B
GS
o Volatile Solids
62.28
%
11/01/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 1 of 7

Sample ID:
CROM
Date Collected:
11/01/2022
Collected By:
M. SHIVAR
Time Collected:
0752
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.82
%
11/01/2022
SM 2540 B
GS
o Volatile Solids
50.93
%
11/01/2022
SM 2540 B
GS
Fecal Coliforms
6.38
MPN/gram
11/01/2022
SM 9221 C E
GS
Sample ID:
T2B
Date Collected:
11/03/2022
Collected By:
E. RUBERTE
I Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.00
11/03/2022
SM 2540 B
GS
o Volatile Solids
49.15
%
11/03/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
11/03/2022
Collected By:
E. RUBERTE
I Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.24
%
11/03/2022
SM 2540 B
GS
o Volatile Solids
52.54
%
11/03/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
11/08/2022
Collected By:
M. SHIVAR
Time Collected:
0757
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.67
%
11/08/2022
SM 2540 B
GS
o Volatile Solids
61.21
%
11/08/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 2 of 7

Sample ID:
T2B
Date Collected:
11/08/2022
Collected By:
M. SHIVAR
Time Collected:
0757
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.14
%
11/08/2022
SM 2540 B
GS
o Volatile Solids
51.12
%
11/08/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
11/08/2022
Collected By:
M. SHIVAR
Time Collected:
0757
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.22
11/08/2022
SM 2540 B
GS
o Volatile Solids
52.15
%
11/08/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
11/08/2022
Collected By:
M. SHIVAR
Time Collected:
0836
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.84
%
11/08/2022
SM 2540 B
GS
o Volatile Solids
50.08
%
11/08/2022
SM 2540 B
GS
Fecal Coliforms
6.80
MPN/gram
11/08/2022
SM 9221 C E
DES
Sample ID:
T2B
Date Collected:
11/10/2022
Collected By:
J. ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.19
%
11/16/2022
SM 2540 B
GS
o Volatile Solids
52.17
%
11/16/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 3 of 7

Sample ID:
T3B
Date Collected:
11/10/2022
Collected By:
J. ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.71
%
11/16/2022
SM 2540 B
GS
o Volatile Solids
51.21
%
11/16/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
11/15/2022
Collected By:
J. ACOSTA
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.75
%
11/17/2022
SM 2540 B
GS
o Volatile Solids
31.92
%
11/17/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
11/15/2022
Collected By:
J. ACOSTA
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.94
%
11/17/2022
SM 2540 B
GS
o Volatile Solids
50.48
%
11/17/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
11/15/2022
Collected By:
J. ACOSTA
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.31
%
11/17/2022
SM 2540 B
GS
o Volatile Solids
50.63
%
11/17/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 4 of 7

Sample ID:
CROM
Date Collected:
11/17/2022
Collected By:
J. ACOSTA
Time Collected:
0758
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.95
%
11/17/2022
SM 2540 B
GS
o Volatile Solids
50.09
%
11/17/2022
SM 2540 B
GS
Fecal Coliforms
6.00
MPN/gram
11/17/2022
SM 9221 C E
GS
Sample ID:
T2B
Date Collected:
11/17/2022
Collected By:
J. ACOSTA
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.78
%
11/21/2022
SM 2540 B
GS
o Volatile Solids
54.00
%
11/21/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
11/17/2022
Collected By:
J. ACOSTA
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.95
%
11/21/2022
SM 2540 B
GS
o Volatile Solids
49.70
%
11/21/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
11/22/2022
Collected By:
M. SHIVAR
Time Collected:
0720
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.01
%
11/22/2022
SM 2540 B
GS
o Volatile Solids
48.76
%
11/22/2022
SM 2540 B
GS
Fecal Coliforms
5.97
MPN/gram
11/22/2022
SM 9221 C E
GS
Page 5 of 7

Sample ID:
T2B
Date Collected:
11/22/2022
Collected By:
M. SHIVAR
Time Collected:
0705
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.55
%
11/22/2022
SM 2540 B
GS
o Volatile Solids
51.56
%
11/22/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
11/22/2022
Collected By:
M. SHIVAR
Time Collected:
0705
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.44
%
11/22/2022
SM 2540 B
GS
o Volatile Solids
51.03
%
11/22/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
11/22/2022
Collected By:
M. SHIVAR
Time Collected:
0705
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.46
%
11/22/2022
SM 2540 B
GS
o Volatile Solids
60.14
%
11/22/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
11/29/2022
Collected By:
J. ACOSTA
Time Collected:
0807
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.76
%
11/29/2022
SM 2540 B
GS
o Volatile Solids
49.71
%
11/29/2022
SM 2540 B
GS
Fecal Coliforms
6.51
MPN/gram
11/29/2022
SM 9221 C E
GS
Page 6 of 7

Sample ID:
FEED
Date Collected:
11/29/2022
Collected By:
J. ACOSTA
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.97
%
11/29/2022
SM 2540 B
GS
o Volatile Solids
61.85
%
11/29/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
11/29/2022
Collected By:
J. ACOSTA
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.25
%
11/29/2022
SM 2540 B
GS
o Volatile Solids
53.58
%
11/29/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
11/29/2022
Collected By:
J. ACOSTA
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.40
%
11/29/2022
SM 2540 B
GS
o Volatile Solids
49.20
%
11/29/2022
SM 2540 B
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Certified By:
L REN D. ACOSTA
Page 7 of 7

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 01/05/2023
Report No.: 2022-DEC ATAD Lab ID: 227
Sample ID:
T2B
Date Collected:
12/l/2022
Collected By:
M. SHIVAR
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.19
12/l/2022
SM 2540 G
GS
o Volatile Solids
51.44
%
12/l/2022
SM 2540 G
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
12/l/2022
Collected By:
M. SHIVAR
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.25
12/l/2022
SM 2540 G
GS
o Volatile Solids
49.32
%
12/l/2022
SM 2540 G
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
12/6/2022
Collected By:
J. ACOSTA
Time Collected:
0721
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
5.03
%
12/6/2022
SM 2540 G
DES
o Volatile Solids
48.42
%
12/6/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 1 of 8

Sample ID:
T2B
Date Collected:
12/6/2022
Collected By:
J. ACOSTA
Time Collected:
0721
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.95
%
12/6/2022
SM 2540 G
DES
o Volatile Solids
55.74
%
12/6/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
12/6/2022
Collected By:
J. ACOSTA
Time Collected:
0721
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.20
12/6/2022
SM 2540 G
DES
o Volatile Solids
52.74
%
12/6/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
12/6/2022
Collected By:
J. ACOSTA
Time Collected:
0747
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.30
%
12/6/2022
SM 2540 G
DES
o Volatile Solids
52.83
%
12/6/2022
SM 2540 G
DES
Fecal Coliforms
7.79
MPN/gram
12/6/2022
SM 9221 C E
DES
Sample ID:
FEED
Date Collected:
12/8/2022
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.87
%
12/8/2022
SM 2540 G
DES
o Volatile Solids
63.49
%
12/8/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 2 of 8

Sample ID:
T2B
Date Collected:
12/8/2022
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.17
%
12/8/2022
SM 2540 G
DES
o Volatile Solids
51.76
%
12/8/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
12/8/2022
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.94
12/8/2022
SM 2540 G
DES
o Volatile Solids
55.26
%
12/8/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
12/13/2022
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.83
%
12/13/2022
SM 2540 G
DES
o Volatile Solids
61.59
%
12/13/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
12/13/2022
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.05
%
12/13/2022
SM 2540 G
DES
o Volatile Solids
56.30
%
12/13/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 3 of 8

Sample ID:
T3B
Date Collected:
12/13/2022
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.06
%
12/13/2022
SM 2540 G
DES
o Volatile Solids
49.71
%
12/13/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
12/13/2022
Collected By:
WILLIAMS
Time Collected:
1030
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.12
%
12/13/2022
SM 2540 G
DES
o Volatile Solids
53.15
%
12/13/2022
SM 2540 G
DES
Fecal Coliforms
2547
MPN/gram
12/13/2022
SM 9221 C E
DES
Sample ID:
T2B
Date Collected:
12/15/2022
Collected By:
M. SHIVAR
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.17
%
12/15/2022
SM 2540 G
DES
o Volatile Solids
58.60
%
12/15/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
12/15/2022
Collected By:
M. SHIVAR
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.11
%
12/15/2022
SM 2540 G
DES
o Volatile Solids
50.90
%
12/15/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 4 of 8

Sample ID:
CROM
Date Collected:
12/15/2022
Collected By:
M. SHIVAR
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.20
%
12/15/2022
SM 2540 G
DES
o Volatile Solids
54.90
%
12/15/2022
SM 2540 G
DES
Fecal Coliforms
4163
MPN/gram
12/15/2022
SM 9221 C E
DES
Sample ID:
T2A
Date Collected:
12/19/2022
Collected By:
M. SHIVAR
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.20
%
12/20/2022
SM 2540 G
DES
o Volatile Solids
57.95
%
12/20/2022
SM 2540 G
DES
Fecal Coliforms
240
MPN/gram
12/19/2022
SM 9221 C E
DES
Sample ID:
T2B
Date Collected:
12/19/2022
Collected By:
M. SHIVAR
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.16
%
12/20/2022
SM 2540 G
DES
o Volatile Solids
57.69
%
12/20/2022
SM 2540 G
DES
Fecal Coliforms
6.33
MPN/gram
12/19/2022
SM 9221 C E
DES
Sample ID:
CROM
Date Collected:
12/19/2022
Collected By:
M. SHIVAR
Time Collected:
0753
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.19
%
12/20/2022
SM 2540 G
DES
o Volatile Solids
55.36
%
12/20/2022
SM 2540 G
DES
Fecal Coliforms
596
MPN/gram
12/19/2022
SM 9221 C E
DES
Page 5 of 8

Sample ID:
FEED
Date Collected:
12/20/2022
Collected By:
M. SHIVAR
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.94
%
12/20/2022
SM 2540 G
DES
o Volatile Solids
64.11
%
12/20/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
12/20/2022
Collected By:
M. SHIVAR
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.07
%
12/20/2022
SM 2540 G
DES
o Volatile Solids
55.43
%
12/20/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
12/20/2022
Collected By:
M. SHIVAR
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.04
%
12/20/2022
SM 2540 G
DES
o Volatile Solids
49.13
%
12/20/2022
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
12/23/2022
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.02
%
12/27/2022
SM 2540 G
LA
o Volatile Solids
54.91
%
12/27/2022
SM 2540 G
LA
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 6 of 8

Sample ID:
T3B
Date Collected:
12/23/2022
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.00
%
12/27/2022
SM 2540 G
LA
o Volatile Solids
48.37
%
12/27/2022
SM 2540 G
LA
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
12/27/2022
Collected By:
M. SHIVAR
Time Collected:
0844
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.11
%
12/27/2022
SM 2540 G
LA
o Volatile Solids
45.60
%
12/27/2022
SM 2540 G
LA
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
12/27/2022
Collected By:
M. SHIVAR
Time Collected:
0844
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.97
%
12/27/2022
SM 2540 G
LA
o Volatile Solids
48.53
%
12/27/2022
SM 2540 G
LA
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
12/27/2022
Collected By:
M. SHIVAR
Time Collected:
0844
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.50
%
12/27/2022
SM 2540 G
LA
o Volatile Solids
62.86
%
12/27/2022
SM 2540 G
LA
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 7 of 8

Sample ID:
CROM
Date Collected:
12/27/2022
Collected By:
M. SHIVAR
Time Collected:
0857
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
1.96
%
12/27/2022
SM 2540 G
LA
o Volatile Solids
53.87
%
12/27/2022
SM 2540 G
LA
Fecal Coliforms
480
MPN/gram
12/27/2022
SM 9221 C E
LA
Sample ID:
T2B
Date Collected:
12/29/2022
Collected By:
M. SHIVAR
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.22
%
01/03/2023
SM 2540 G
GS
o Volatile Solids
57.84
o
01/03/2023
SM 2540 G
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
12/29/2022
Collected By:
M. SHIVAR
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.10
%
01/03/2023
SM 2540 G
GS
o Volatile Solids
47.21
o
01/03/2023
SM 2540 G
GS
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Certified By:
L REN D. ACOSTA
Page 8 of 8

REPORT NO. 2022 BSQTR4
Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 12/02/2022
Report No.: 2022 BSQTR4 Lab ID: 227
Date Collected: 10/28/2022 Time Collected: 0700 Collected By: I GS
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
2.04
%
11/01/2022
SM 2540 G
GS
B-S
o Volatile Solids
51.50
%
11/01/2022
SM 2540 G
GS
B-S DUP
o Total Solids
2.11
%
11/01/2022
SM 2540 G
GS
B-S DUP
o Volatile Solids
50.20
%
11/01/2022
SM 2540 G
GS
QUALITY CONTROL - 10/28/2022
B-S/B-S DUP
Average
%RPD
o Total Solids
2.08 %
3.4 %
o Volatile Solids
50.85 %
2.6 %
Date Collected: 11/01/2022 Time Collected: 1040 Collected By: I GS
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.79
%
11/03/2022
SM 2540 G
GS
B-S
o Volatile Solids
50.04
%
11/03/2022
SM 2540 G
GS
B-S DUP
o Total Solids
1.79
%
11/03/2022
SM 2540 G
GS
B-S DUP
o Volatile Solids
50.43
%
11/03/2022
SM 2540 G
GS
QUALITY CONTROL - 11/01/2022
B-S/B-S DUP
Average
%RPD
o Total Solids
1.79 %
0.0 %
o Volatile Solids
50.24 %
0.8 %
Page 1 of 3

REPORT NO. 2022 BSQTR4
Date Collected: 11/08/2022 Time Collected: 0810 Collected By: I GS
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.39
%
11/08/2022
SM 2540 G
GS
B-S
o Volatile Solids
50.17
%
11/08/2022
SM 2540 G
GS
B-S DUP
o Total Solids
1.38
%
11/08/2022
SM 2540 G
GS
B-S DUP
o Volatile Solids
51.24
%
11/08/2022
SM 2540 G
GS
QUALITY CONTROL - 11/08/2022
B-S/B-S DUP
Average
%RPD
o Total Solids
1.39
0.7 %
o Volatile Solids
50.71 %
2.1 %
Date Collected: 11/15/2022 Time Collected: 0830 Collected By: I DES
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.26
%
11/16/2022
SM 2540 G
GS
B-S
o Volatile Solids
51.01
%
11/16/2022
SM 2540 G
GS
B-S DUP
o Total Solids
1.34
%
11/16/2022
SM 2540 G
GS
B-S DUP
o Volatile Solids
49.03
%
11/16/2022
SM 2540 G
GS
QUALITY CONTROL - 11/15/2022
B-S/B-S DUP
Average
%RPD
o Total Solids
1.30 %
6.2 %
o Volatile Solids
50.02 %
4.0 %
Page 2 of 3

REPORT NO. 2022 BSQTR4
Date Collected: 11/22/2022 Time Collected: 1000 Collected By: I DES
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.07
%
11/22/2022
SM 2540 G
GS
B-S
o Volatile Solids
47.53
%
11/22/2022
SM 2540 G
GS
B-S DUP
o Total Solids
1.15
%
11/22/2022
SM 2540 G
GS
B-S DUP
o Volatile Solids
45.93
%
11/22/2022
SM 2540 G
GS
QUALITY CONTROL - 11/22/2022
B-S/B-S DUP
Average
%RPD
o Total Solids
1.11 %
7.2 %
o Volatile Solids
46.73 %
3.4 %
Date Collected: 11/29/2022 Time Collected: 0850 Collected By: I GS
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.00
%
11/29/2022
SM 2540 G
GS
B-S
o Volatile Solids
48.67
%
11/29/2022
SM 2540 G
GS
B-S DUP
o Total Solids
1.00
%
11/29/2022
SM 2540 G
GS
B-S DUP
o Volatile Solids
48.42
%
11/29/2022
SM 2540 G
GS
QUALITY CONTROL - 11/29/2022
B-S/B-S DUP
Average
%RPD
o Total Solids
1.00 %
0 %
o Volatile Solids
48.55 %
0.5 %
*B-S: BENCH -SCALE
6-WEEK VOLATILE SOLIDS REDUCTION 4.5 %
Certified By:
L RE�ACOSTA
Page 3 of 3

MCB CAMLEJ ELS
ATAD BENCH -SCALE VOLATILE SOLIDS REDUCTION ANALYSIS
Sample Date
Sample ID
Tom p
(m O)
% TS
% VS
% VS Avg
Analyst
10/28/2022
BENCH
19.4
9.04
2.04
51.5
50.85
GS
BENCH-DUP
2.11
50.2
ll/l/2022
BENCH
2O.4
6.22
1.79
50.04
50.24
GS
BENCH-DUP
1.79
50.43
11/8/2022
BENCH
19.0
6.21
1.39
50.17
50.71
GS
BENCH-DUP
1.38
51.24
11/15/2022
BENCH
19.6
8.95
1.26
51.01
50.02
GS
BENCH-DUP
1.34
49.03
11/22/2022
BENCH
19.5
9.14
1.07
47.53
46.73
CS
BENCH-DUP
1.15
45.93
11/29/2022
BENCH
19.4
9.04
1.00
48.67
48.55
CS
BENCH-DUP 1
1.00
48.42
INITIAL VS (%) 50.85 VS
4.5%
FINAL VS (%) 48.55 REDUCTION
VS REDUCTION = (INITIAL VS - FINAL VS) / INITIAL VS X 100
*VS REDUCTION MUST BE < 15% TO MEET VECTOR ATTRACTION REDUCTION REQUIREMENTS
REV. 01 /2020