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WQ0039924_2022 Residual Annual Report_20230223
Initial Review Reviewer Nathaniel.Thornburg Is this submittal an application? (Excluding additional information.) * Yes No If not an application what is the submittal type?* Annual Report Residual Annual Report Additional Information Other Annual Report Year* 2022 Permit Number (IR) * WQ0039924 Applicant/Permittee Marcal Cordova LLC Email Notifications Does this need review by the hydrogeologist? * Yes No Regional Office Fayetteville CO Reviewer Admin Reviewer Submittal Form Project Contact Information Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence. Name* Robert T. Branch Email Address* bbranch@branchrs.com Project Information ......................... Application/Document Type* New (Fee Required) Modification - Major (Fee Required) Renewal with Major Modification (Fee Required) Annual Report Additional Information Other Phone Number* 3363129007 Modification - Minor Renewal GW-59, NDMR, NDMLR, NDAR-1, N DAR-2 Residual Annual Report Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* Wastewater Irrigation High -Rate Infiltration Other Wastewater Reclaimed Water Closed -Loop Recycle Residuals Single -Family Residence Wastewater Other Irrigation Permit Number:* WQ0039924 Has Current Existing permit number Applicant/Permittee Address* 126 First Street Cordova, NC 28330 Facility Name* Marcal Cordova Class A Residuals Program Please provide comments/notes on your current submittal below. At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here. (Application Form, Engineering Plans, Specifications, Calculations, Etc.) Marcal NCDEQ 2022 AR final.pdf 9.94MB Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger than upload limit. * By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Submission Date 2/23/2023 2022 ANNUAL REPORT MARCAL CORDOVA, LLC (Formerly von Drehle Corporation) FIBER CLAY RESIDUAL CORDOVA, NORTH CAROLINA CLASS A PERMIT #WQ0039924 Prepared For: Marcal Cordova, LLC 126 First Street Cordova, N.C. 28330 Prepared By: Branch Residuals & Soils, LLC 1735 Heckle Blvd. Suite 103-291 Rock Hill SC, 29732 February 2023 BRANCH RESIDUALS & SO1LS, LLC 1735 Heckle Blvd, Suite 103-291, Rock Hill, SC 29732 PHONE (336) 312-9007 February 23, 2023 North Carolina Department of Environmental Quality Division of Water Resources 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Reference: 2022 CLASS A LAND APPLICATION ANNUAL REPORT Marcal Cordova, LLC. (Formerly von Drehle Corporation) Cordova, North Carolina Permit No. WQ0039924 BR&S Project No. 2014-110 Information Processing Unit: Branch Residuals & Soils is submitting all monitoring and reporting information as required in the referenced permit on behalf of Marcal Cordova, LLC for their facility in Cordova, North Carolina. This report includes: Distribution and Marketing Certification and Summary Form. Distributions were made from January through December during 2022. These distributions totaled 64,653.15 wet tons (24,893.03 dry tons). These applications were surface spread and incorporated into the soil. In December 2022 von Drehle Corporation was purchased by Marcal. The current facility is listed as Marcal Cordova LLC. Most of the activities for the year were performed as von Drehle Corporation. In addition, significant staff changes occurred in July 2022. Changes were made in both Facility ORC and Land Application ORC and are noted in the forms. If any further information is required regarding this land application program, please do not hesitate to contact me at (336) 312-9007. Sinc ely, Robert T. Branch, L.S.S. Land Application/Residuals Operator #15676 RTB Enclosures TABLE OF CONTENTS SECTION NO. TITLE Distribution and Marketing Certification and Summary Forms II Annual Residual Sampling Summary Form III Residual Analysis Lab Sheets IV Toxicity Characteristics Leaching Procedure (TCLP) Analysis Report V Pathogen and Vector Attraction Reduction Forms VI Pathogen and Vector Attraction Reduction Documentation DISTRIBUTION AND MARKETING CERTIFICATION AND SUMMARY FORM Iv U a 0 v 0 U h LUi imp W O W a 0 q 0 U (z A e I10 o C Q C Q C C C C Q C C q -- CA � o .o .o .o .o o .o .o .o40 a o 1 ^ O I: N O\ M O Ol� [t vl M M in [— M N S N M 0 [� O M �+ eC 'a 00 1.0 ON m l- V fV l— cn r- 110 p A N N [— Ln 00 G1 00 N W) C 40 y 0 a_ .0 U. O z y � V z �" o [� MN It CN O O N U M 1.0 ON M l- %O N .-. � Vl O M v1 't -0 N00 " Ln O 0 0 ---i n O C,, C 0 � N N cV N N N N N N — N^ o' N G t MO tz Q m 0 N M ON to M l� M N;I- 1-0 N G A .-- n G\ O'Id: M w! OO O\ M p M C y, G 00 �o ON " t- \D N -• V r v1 I O O� 0 M. in v� M N r 00 Wn C, N ID O y � G w h � C. a a K N cc Val G O cc G w IL F i Q R y L yy u a.. C4 a�i z tiE�oza �. Z, �L y/ay 4 A Z y y C � O X 0 ? ' A O E sQ O O cr tH U U R4 0 3 o c u . o Q N%' U • L x a m 0 L. 'a 0. 15 : u cu 4.1 c O O ccr Gn 0 > ca Q y U 0 c o L U i 4 � U 0 atu3b v 'O o ee v r CW 4 0.. ; N M ANNUAL RESIDUAL SAMPLING SUMMARY FORM 4 A4 3 a N G\ M O O 1 S �z3az r w a 3 W I 4 1 C a d. NGc\ 7 N R N O O O o (0V0 C N 00 [� Q 00 M z N �"� ,� V V V V cNr1 V V V N N � �'? N � Q O v, tn d• u. oo .0 M O N 00 n �p N •" � N V N � V m O CN N pQ `! cN•'1• en N C Q 7 d' C�i1 Vim', o N Z O C+i v N V 00 CN O Cl h C v�i v^ In ^ O O M M N O Cl! N Q z M kn 00 N N O �n �? N M V V N N O M O V V G R7 t� Q �"' eq NN CV N O 00 N 00 �7 O O O C CDcNrl N In M O C Q z C O O �_ O CC,',, -- V V N (V V el; V GM'� N o0 M V N 0 U Q N M Q M en n C O O _ N N O IDV n N V � V V C — M N M N Q N 7 N N N C d N O O O 00 00 N v N O z O Cy M ' i V' N o0 N V V V V [� V st � cq G N O x O M —. O p N C N —� O N N vN. V N c+i eV vi V N 00 M V � M K1 N r4 C N O n -» 00CD In C n Q Ct c0 l� � O C 00 O oll00 [� — N V N z M N In ct O N N oo N Cr- V N `p/' — M N N O wl O Co 5 C to O CD N V V N z M N O N V oM0 M V V N V -5iM d' N C Q 00 MO O OM F N z m O1 O M V O M O M M N M p N V W) 6 4- C� < C� Q Q Q Q Fr 0Nf 05 y Y M i-1 � �� � ' b � � • O 'U � N N � U O" '��jJ .� 'b cz i p" z N a C) N N LL U) U) c� G O LL z w N O F-' N U Q U z d G as L v U M tn x w C s 73 G "O L al a a ,r RESIDUAL ANALYSIS LAB SHEETS Waypoi ntNALYTICAL 1 /20/2022 Branch Residuals and Soils LLC Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill, SC, 29732 Ref: Analytical Testing Report Number: 22-012-0006 Project Description: Von Drehle 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Dear Bob Branch: Waypoint Analytical Virginia, Inc. received sample(s) on 1/12/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, TaWIT Mt (slvwy/ Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 6 (2) Waypoint ANALYTICAL Report Number: 22-012-0006 Client Project Description: Von Drehle 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Sample Summary Table Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 56210 Von Drehle Solids 01/11/2022 11:30 01/12/2022 SM-254OG WP MTN 56210 Von Drehle Solids 01/11/2022 11:30 01/12/2022 SM-4500-NH3C WP MTN 56210 Von Drehle Solids 01/11/2022 11:30 01/12/2022 SM-4500-NH3C-TKN WP MTN 56210 Von Drehle Solids 01/11/2022 11:30 01/12/2022 4500NO3F-2011 WP MTN 56210 Von Drehle Solids 01/11/2022 11:30 01/12/2022 6010D WP MTN 56210 Von Drehle Solids 01/11/2022 11:30 01/12/2022 SW-7471B WP MTN 56210 Von Drehle Solids 01/11/2022 11:30 01/12/2022 9045D WP MTN 56210 Von Drehle Solids 01/11/2022 11:30 01/12/2022 AOAC 955.01 WP MTN WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 2 of 6 Waypointo ANALYTICAL 46368 Branch Residuals and Soils LLC Project Von Drehle Bob Branch 1735 Heckle Blvd Information Suite 103-291 Rock Hill , SC 29732 Report Number: 22-012-0006 Lab No : 56210 Sample ID : Von Drehle 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Report Date : 01/20/2022 Received : 01/12/2022 TawlC m4 GtpT REPORTOFANALYSIS Pauric Mc Groary Ph.D., CPA Agronomist Matrix: Solids Sampled: 1/ 11/ 2022 11:30 Test Results Units MQL DF Date / Time Analyzed By Analytical Method Moisture 60.6 % 0.010 1 01/13/2216:31 FMM SM-2540G Potassium 70.6 mg/Kg - dry 25.4 1 01/15/22 19:06 TJS 6010D Calcium 181000 mg/Kg - dry 2540 20 01/17/22 18:42 TJS 6010D Sodium 596 mg/Kg - dry 63.5 1 01/15/22 19:06 TJS 6010D Aluminum 1810 mg/Kg - dry 12.7 1 01/15/22 19:06 TJS 6010D Nickel 3.35 mg/Kg - dry 0.634 1 01/15/22 19:06 TJS 6010D Arsenic <1.27 mg/Kg - dry 1.27 1 01/15/22 19:06 TJS 6010D Test Results Units MQL DF Date / Time By Analytical Analyzed Method pH 7.3 S.U. 1 01/19/22 15:02 DRS 9045D Total Solids 39.4 % 0.010 1 01/13/22 16:31 FMM SM-2540G Copper 36.0 mg/Kg - dry 1.27 1 01/15/22 19:06 TJS 6010D Lead <0.761 mg/Kg - dry 0.761 1 01/15/22 19:06 TJS 6010D Magnesium 2230 mg/Kg - dry 12.7 1 01/15/22 19:06 TJS 6010D Selenium 2.64 mg/Kg - dry 1.27 1 01/15/22 19:06 TJS 6010D Total Kjeldahl Nitrogen 6090 mg/Kg - dry 635 1 01/18/22 12:00 JPJ ;M-4500-NH3C-TKf Qualifiers/ B Analyte detected in blank Definitions H Beyond holding time DF Dilution Factor MQL Method Quantitation Limit Page 3 of 6 Waypointo ANALYTICAL 46368 Branch Residuals and Soils LLC Project Von Drehle Bob Branch 1735 Heckle Blvd Information Suite 103-291 Rock Hill , SC 29732 Report Number: 22-012-0006 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com REPORT OPANAL YSIS Report Date : 01/20/2022 Received : 01/12/2022 Taun,c ME &to"Ir Pauric Mc Groary Ph.D., CPA Agronomist Lab No : 56210 Sample ID : Von Drehle Matrix: Solids Sampled: 1/11/2022 11:30 Phosphorus 134 mg/Kg - dry 12.7 1 01/15/22 19:06 TJS 6010D Zinc 50.0 mg/Kg - dry 3.17 1 01/15/22 19:06 TJS 6010D Ammonia Nitrogen 269 mg/Kg - dry 254 1 01/18/22 14:00 JPJ SM-4500-NH3C Nitrate+Nitrite-N 13.3 mg/Kg - dry 11.7 1 01/18/22 15:26 ZBD 4500NO3F-2011 Cadmium <0.254 mg/Kg - dry 0.254 1 01/15/22 19:06 TJS 6010D Mercury <0.0398 mg/Kg - dry 0.0398 1 01/14/22 12:34 JW2 SW-7471B Calcium Carbonate Equivalent 48.6 % 0.1 1 01/19/22 06:35 DXT ACAC 955.01 Molybdenum 3.81 mg/Kg - dry 0.634 1 01/15/22 19:06 TJS 6010D Qualifiers/ B Analyte detected in blank Definitions H Beyond holding time DF Dilution Factor MQL Method Quantitation Limit Page 4 of 6 Waypoint(D ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Shipment Receipt Form Customer Number: 46368 Customer Name: Branch Residuals and Soils LLC Report Number: 22-012-0006 Shipping Method Fed Ex US Postal Lab • UPS Client Courier Other Thermometer ID: Shipping container/cooler uncompromised? • Yes No Number of coolers/boxes received F— 1 Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? _ Yes No • Not Present Chain of Custody (COC) present? 14 Yes No COC agrees with sample label(s)? t Yes No COC properly completed C' Yes No Samples in proper containers? #' Yes No Sample containers intact? CO, Yes No Sufficient sample volume for indicated test(s)? Yes No All samples received within holding time? Co Yes No Cooler temperature in compliance? Yes No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes No Water - Sample containers properly preserved Yes No • N/A Water - VOA vials free of headspace Yes No N/A Trip Blanks received with VOAs Yes No • N/A Soil VOA method 5035 — compliance criteria met Yes No • N/A High concentration container (48 hr) Low concentration EnCore samplers (48 hr) High concentration pre -weighed (methanol -14 d) Low cone pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? Yes • No Comments: Signature: Brandi Watson Date & Time: 01/12/2022 12:25:41 Page 5 of 6 9 3o 9 abPd O fl C. Op co E E_ E w rl i w n +v ra 0 2 N Z on vZ E v a�==va� E a S Q y O M 2 n Q — N U O O C 2 U 1+I p s C' L O � C L acr cc O Z Z Z r� LL ` r a d m > u u y C ' spilos% E Go 6 w _ E C OC K o w� w�y w o w w w �Nif N p o o - LL u O Lco KID a N-ZON/CON a ci ti �/ T N C 'N it d ,N-t,HN 'c _> n O w U d 'eN '6IN 'eD `IV uZ aS lN °w 6H *1 --C J gd`no'Po'sV 71r� a N Z O N v Z mti ,a, c co � a, � , o w m N a1!sodwo(J) jo gei(9) N ao` fl j i a we C Yl CL(�'��, c c O siauae3uo3 Jo jaquinN \ �1. cc is A uo T t oa = c i n O LCN C LL rCaL -U Z o d u O = C �m oL �c N s m a�. O co u O 4 coa e U U ° a CO � _ a c m > c O N a .5 w E O 00 L J *Ii C O O C t Q > LL } �e N Z n • } a0 u alY= N w O v � 2 U D Z % s ^+ Z o = w 2 co � a a NN +1+ .r p' waypoint_(2) ANALYTICAL 2/11 /2022 Branch Residuals and Soils LLC Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill, SC, 29732 Ref: Analytical Testing Report Number: 22-033-0004 Project Description: Von Drehle 2014-10 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Dear Bob Branch: Waypoint Analytical Virginia, Inc. received sample(s) on 2/2/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Tawfe M f Gfc'"r Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 7 (2) Waypoint. 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 22-033-0004 Client Project Description: Von Drehle 2014-10 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 56463 VD Solids 02/01/2022 14:04 02/02/2022 SM-2540G WP MTN 56463 VD Solids 02/O1/2022 14:04 02/02/2022 SM-4500-NH3C WP MTN 56463 VD Solids 02/O1/2022 14:04 02/02/2022 SM-4500-NH3C-TKN WP MTN 56463 VD Solids 02/O1/2022 14:04 02/02/2022 4500NO3F-2011 WP MTN 56463 VD Solids 02/O1/2022 14:04 02/02/2022 6010D WP MTN 56463 VD Solids 02/01/2022 14:04 02/02/2022 SW-7471B WP MTN 56463 VD Solids 02/01/2022 14:04 02/02/2022 9045D WP MTN 56463 VD Solids 02/O1/2022 14:04 02/02/2022 AOAC 955.01 WP MTN WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 2 of 7 0 Waypoint. 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46368 Branch Residuals and Soils LLC Project Von Drehle Bob Branch Report Date : 02/11/2022 1735 Heckle Blvd Information : 2014-10 Received : 02/02/2022 Suite 103-291 Rock Hill , SC 29732 l rc ply G10T Report Number: 22-033-0004 REPORT OPANALYSIS Pauric Mc Groary Ph.D., CPA Agronomist Lab No : 56463 Matrix: Solids Sample ID : VD Sampled: 2/1/2022 14:04 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Zinc Ammonia Nitrogen Nitrate+Nitrite-N Lead Mercury Selenium Calcium Carbonate Equivalent Test Total Kjeldahl Nitrogen Phosphorus Cadmium Molybdenum Analytical Method: SM-2540G Test Moisture 83.8 mg/Kg - dry 3.12 <249 mg/Kg - dry 249 <12.2 mg/Kg - dry 12.2 2.31 mg/Kg - dry 0.748 <0.0381 mg/Kg - dry 0.0381 <1.25 mg/Kg - dry 1.25 72.6 % 0.1 Results Units MQL 1 02/09/22 18:16 TJS 6010D 1 02/09/22 10:30 JPJ SM-4500-NH3C 1 02/09/22 15:01 ZBD 4500NO3F-2011 1 02/10/22 23:09 TJS 6010D 1 02/08/2217:30 JW2 SW-7471B 1 02/09/22 18:16 TJS 6010D 1 02/10/22 10:15 DXT AOAC 955.01 DF Date / Time By Analytical Analyzed Method 5460 mg/Kg - dry 623 1 02/09/22 09:30 JPJ ;M-4500-NH3C-TKr 137 mg/Kg - dry 12.5 1 02/09/22 18:16 TJS 6010D <0.249 mg/Kg - dry 0.249 1 02/09/22 18:16 TJS 6010D 4.66 mg/Kg - dry 0.623 1 02/09/22 18:16 TJS 6010D Results Units MQL DF Date / Time By Analytical Analyzed Batch 59.9 % 0.010 Qualifiers/ B Analyte detected in blank Definitions MQL Method Quantitation Limit 1 02/08/22 17:16 FMM L598301 DF Dilution Factor Page 3 of 7 Waypointo ANALYTICAL 46368 Branch Residuals and Soils LLC Project Von Drehle Bob Branch 1735 Heckle Blvd Information : 2014-10 Suite 103-291 Rock Hill , SC 29732 Report Number:22-033-0004 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com REPORT Of ANALYSIS Report Date : 02/11/2022 Received : 02/02/2022 Tawsc f �1001r Pauric Mc Groary Ph.D., CPA Agronomist Lab No : 56463 Sample ID: VD Matrix: Solids Sampled: 2/1/2022 14:04 Total Solids 40.1 % 0.010 1 02/08/22 17:16 FMM SM-2540G Potassium 66.1 mg/Kg - dry 24.9 1 02/10/22 23:09 TJS 6010D Calcium 180000 mg/Kg - dry 1250 10 02/10/22 23:14 TJS 6010D Magnesium 2240 mg/Kg - dry 12.5 1 02/09/22 18:16 TJS 6010D Sodium 658 mg/Kg - dry 62.3 1 02/09/22 18:16 TJS 6010D Aluminum 2390 mg/Kg - dry 12.5 1 02/09/22 18:16 TJS 6010D Copper 23.7 mg/Kg - dry 1.25 1 02/09/22 18:16 TJS 6010D Nickel 1.20 mg/Kg - dry 0.623 1 02/09/22 18:16 TJS 6010D Arsenic ¢ 1.25 mg/Kg - dry 1.25 1 02/09/22 18:16 TJS 6010D pH 7.0 S.U. 1 02/08/2215:46 DRS 9045D Qualifiers/ B Analyte detected in blank Definitions MQL Method Quantitation Limit DF Dilution Factor Page 4 of 7 Waypdlont(2) ANALYTICAL Client: Branch Residuals and Soils LLC Project: Von Drehle Lab Report Number: 22-033-0004 Date: 2/11 /2022 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com CASE NARRATIVE Metals Analysis Method 6010D Sample 56463 (VD) Analyte: Aluminum QC Batch No: 1-5986551598315 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 56463 Analyte: Calcium QC Batch No: 1-598925/1-598315 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 56463 Analyte: Potassium QC Batch No: 1-598925/1-598315 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 5 of 7 (2)W• 7621 Road, Richmond, 23237 ayPoint ain 80 -7 27 Main 804-743-9401 0Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Shipment Receipt Form Customer Number: 46368 Customer Name: Branch Residuals and Soils LLC Report Number: 22-033-0004 Shipping Method Fed Ex US Postal Lab Other • UPS Client Courier Thermometer ID: �— Shipping container/cooler uncompromised? (4; Yes No Number of coolers/boxes received F 1 Custody seals intact on shipping container/cooler? Yes No • Not Present Custody seals intact on sample bottles? Yes No • Not Present Chain of Custody (COC) present? Yes No COC agrees with sample label(s)? Yes No COC properly completed Yes No Samples in proper containers? Yes No Sample containers intact? • Yes No Sufficient sample volume for indicated test(s)? • Yes No All samples received within holding time? • Yes No Cooler temperature in compliance? • Yes No Cooler/Samples arrived at the laboratory on ice. • Yes No Samples were considered acceptable as cooling process had begun. Water - Sample containers properly preserved Yes No • N/A Water - VOA vials free of headspace Yes No • N/A Trip Blanks received with VOAs Yes No • N/A Soil VOA method 5035 — compliance criteria met Yes No • N/A High concentration container (48 hr) Low concentration EnCore samplers (48 hr) High concentration pre -weighed (methanol -14 d) Low cone pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? Yes • No Comments: Signature: Brandi Watson Date & Time: 02/02/2022 13:03:47 Page 6 of 7 L du L ODed O '0 E E E v _ c o u Y d �- p n1 O o 2 0 0 0 O 41 N fa O ry N n cl) Cp Q y Z W� � J ; NIr QU fJ ON SQ S °' 2 O e C i u p in C! �� O m z can z x x x u } c ;.-JOBz ` 1 0 x O i 1 G O 1 G W W l7 2_ L > G C J r _ N 0 v v > > i �= w vl u c a u �• L o 40 �. E E d cc d z Go s ca vvi / {{ r ^/� ;L o w G7 4` N 0lu E t� u° o r- ti / 1 a d❑� m c n c Q v � C_ O G 1 � C: .'�. Y ���.r 1 9 � �� i • W W W fo " GJ j u > > 7 O z z z m � O a S �� O v � at N v^ Vf � 'm a - al{sodwo(J) jo gej(E)) r z } a a ,- (AaN of jajaa) xijleVy y kc N c c 75 c u m N siauieluo:) jo jagwncc N � w ice � c N u a m c o c 0 nr o V O v % o n <6 _ Y 0 2 u 19 C p m T _ c A 0 y c — O L ate. �_ E c Y Y u V C. a � O j � a 0 J " v 0 E m ` c • •- 7 VYI } r E a a_ 0 n w a g m N E x r u R •— c • V C 0uJ L : - — :; "tij -` v } m u G a a 1 T m o Waypoint_(D ANALYTICAL 3/9/2022 Branch Residuals and Soils LLC Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill, SC, 29732 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Ref: Analytical Testing Report Number: 22-060-0014 Project Description: Von drehle Project# 2014-110 Dear Bob Branch: Waypoint Analytical Virginia, Inc. received sample(s) on 3/1/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, TOW,'c M C Goa"O Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 7 • • 7621 Whitepine Road, Richmond, VA 23237 Waypoint. Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 22-060-0014 Client Project Description: Von drehle Project# 2014-110 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 56880 VD Solids 56880 VD Solids 56880 VD Solids 56880 VD Solids 56880 VD Solids 56880 VD Solids 56880 VD Solids 56880 VD Solids WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN 02/28/2022 13:30 03/01/2022 02/28/2022 13:30 03/01/2022 02/28/2022 13:30 03/01/2022 02/28/2022 13:30 03/01/2022 02/28/2022 13:30 03/01/2022 02/28/2022 13:30 03/01/2022 02/28/2022 13:30 03/01/2022 02/28/2022 13:30 03/01/2022 SM-2540G WP MTN SM-4500-NH3C WP MTN SM-4500-NH3C-TKN WP MTN 4500NO3F-2011 WP MTN 6010D WP MTN SW-7471B WP MTN 9045D WP MTN AOAC 955.01 WP MTN Page 2 of 7 0 Waypoint. 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46368 Branch Residuals and Soils LLC Project Von drehle Bob Branch Report Date : 03/09/2022 1735 Heckle Blvd Information : Project# 2014-110 Received : 03/01/2022 Suite 103-291 Rock Hill , SC 29732 �Aw,c (i1� G10"I / Pauric Mc Groary Ph.D., CPA Report Number: 22-060-0014 REPORT Agronomist Lab No : 56880 Matrix: Solids Sample ID: VD Sampled: 2/28/2022 13:30 Test Results Units MOL DF Date / Time By Analytical Analyzed Method Moisture 61.3 % 0.010 1 03/03/2215:57 FMM SM-2540G Potassium 69.3 mg/Kg - dry 25.8 1 03/07/22 20:14 EAL 6010D Calcium 202000 mg/Kg - dry 2580 20 03/07/22 20:09 EAL 6010D Sodium 711 mg/Kg - dry 64.6 1 03/05/22 05:03 EAL 6010D Aluminum 1710 mg/Kg - dry 12.9 1 03/05/22 05:03 EAL 6010D Nickel 1.04 mg/Kg - dry 0.645 1 03/05/22 05:03 EAL 6010D Arsenic 1.71 mg/Kg - dry 1.29 1 03/05/22 05:03 EAL 6010D Test Results Units MQL DF Date / Time By Analytical Analyzed Method pH 7.7 s.u. 1 03/08/2215:09 DRS 9045D Total Solids 38.7 % 0.010 1 03/03/22 15:57 FMM SM-2540G Copper 22.7 mg/Kg - dry 1.29 1 03/05/22 05:03 EAL 6010D Lead 2.34 mg/Kg - dry 0.775 1 03/05/22 05:03 EAL 6010D Magnesium 1950 mg/Kg - dry 12.9 1 03/05/22 05:03 EAL 6010D Selenium 2.26 mg/Kg - dry 1.29 1 03/05/22 05:03 EAL 6010D Total Kjeldahl Nitrogen 3700 mg/Kg - dry 646 1 03/08/22 10:00 JPJ ;M-4500-NH3C-TKP Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit Page 3 of 7 Waypointo ANALYTICAL 46368 Branch Residuals and Soils LLC Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill , SC 29732 Report Number: 22-060-0014 Project Von drehle 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Information : Project# 2014-110 REPORT OFANALYSIS Report Date : 03/09/2022 Received : 03/01/2022 Towic W �10we.}/ Pauric Mc Groary Ph.D., CPA Agronomist Lab No : 56880 Sample ID : VD Matrix: Solids Sampled: 2/28/2022 13:30 Phosphorus 120 mg/Kg - dry 12.9 1 03/05/22 05:03 EAL 6010D Zinc 88.1 mg/Kg - dry 3.23 1 03/05/22 05:03 EAL 6010D Ammonia Nitrogen <258 mg/Kg - dry 258 1 03/08/22 14:37 JPJ SM-4500-NH3C Nitrate+Nitrite-N 23.7 mg/Kg - dry 12.6 1 03/08/22 14:31 ZBD 4500NO3F-2011 Cadmium <0.258 mg/Kg - dry 0.258 1 03/05/22 05:03 EAL 6010D Mercury <0.0348 mg/Kg - dry 0.0348 1 03/03/22 12:03 JW2 SW-7471B Calcium Carbonate Equivalent 45.2 % 0.1 1 03/07/22 09:15 DXT AOAC 955.01 Molybdenum 4.57 mg/Kg - dry 0.645 1 03/05/22 05:03 EAL 6010D Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit Page 4 of 7 Waypointo ANALYTICAL Client: Branch Residuals and Soils LLC Project: Von drehle Lab Report Number: 22-060-0014 Date: 3/8/2022 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com CASE NARRATIVE Metals Analysis Method 6010D Sample 99160 (1A) Analyte: Magnesium QC Batch No: L603214/L602543 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 99160 (1A) Analyte: Molybdenum QC Batch No: 1-603214/1-602543 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 99160 (1A) Analyte: Nickel QC Batch No: 1-603214/1-602543 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 99160 (1A) Analyte: Selenium QC Batch No: L603214/1-602543 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 5 of 7 Waypoint-Q) ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www,waypo i nta n a l ytica I. co m Shipment Receipt Form Customer Number: 46368 Customer Name: Branch Residuals and Soils LLC Report Number: 22-060-0014 Shipping Method Fed Ex US Postal Lab • UPS Client Courier Other Thermometer ID: Shipping container/cooler uncompromised? Yes No Number of coolers/boxes received 1 Custody seals intact on shipping container/cooler? Yes No 0 Not Present Custody seals intact on sample bottles? „ Yes No 16 Not Present Chain of Custody (COC) present? Yes No COC agrees with sample label(s)? Yes No COC properly completed Yes No Samples in proper containers? Yes No Sample containers intact?; Yes No Sufficient sample volume for indicated test(s)? Yes No All samples received within holding time? 6 Yes No Cooler temperature in compliance? it Yes No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes No Water - Sample containers properly preserved Yes No • N/A Water - VOA vials free of headspace Yes No • N/A Trip Blanks received with VOAs Yes No • N/A Soil VOA method 5035 — compliance criteria met Yes No • N/A High concentration container (48 hr) High concentration pre -weighed (methanol -14 d) Low concentration EnCore samplers (48 hr) Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? Comments: Yes • No Signature: Brandi Watson Date & Time: 03/01/2022 13:15:15 Page 6 of 7 L 4� L bard O a a a r. Q C 4E V N Z O O C v1 ri O I � N v Z ra`4o— Qn v ryxu a E CL W U M a N c Old0 2 _ a z z z x x u ` 0cc I a 3 cc cc N z z z L 2 = 'E j 0 m ,yf n N a ir1 a ❑CL ,�.. c o ��. ma a d •W CL — t r lu E a ¢ ¢ W E a E n n i m — w o " o y 'o t R va a E a ¢ E'• E E =� v O r d � ❑� i N d 'v G o G m v � � a Q CL CL j Q g lu lu ¢ E v J ©%fit% c e O O Z j � E -� w y^t } v a 00 > > > c a o Ny La Is A°�,J SL a a a a z z z `V m I atisodwo(�f jo gej(91 m (� ? i Yy T d d (AaM o3 jaya)j) xi7eyN J y N N CL E 17 c a _ m sjauiejuo3 jo jagwnN f H c c ` y J nC „'• C •� C D V c C c `v V � Q M a°� o u a --cp u Y, L ' H u — E E O a C CL � O N a m S z No\ J Q u z n aEi u U E '01 °o E a x Y c m �t y 0 T Q a WaypointNALYTICAL 4/6/2022 Branch Residuals and Soils LLC Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill, SC, 29732 Ref: Analytical Testing Report Number: 22-081-0014 Project Description: Von Drehle Project# 2014-110 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Dear Bob Branch: Waypoint Analytical Virginia, Inc. received sample(s) on 3/22/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, �awj•c M f G10" Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 7 (2) Waypoint. 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 22-081-0014 Client Project Description: Von Drehle Project# 2014-110 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 57238 VD Solids 03/21/2022 13:15 03/22/2022 SM-254OG WP MTN 57238 VD Solids 03/21/2022 13:15 03/22/2022 SM-4500-NH3C WP MTN 57238 VD Solids 03/21/2022 13:15 03/22/2022 SM-4500-NH3C-TKN WP MTN 57238 VD Solids 03/21/2022 13:15 03/22/2022 4500NO3F-2011 WP MTN 57238 VD Solids 03/21/2022 13:15 03/22/2022 6010D WP MTN 57238 VD Solids 03/21/2022 13:15 03/22/2022 SW-7471B WP MTN 57238 VD Solids 03/21/2022 13:15 03/22/2022 9045D WP MTN 57238 VD Solids 03/21/2022 13:15 03/22/2022 AOAC 955.01 WP MTN WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 2 of 7 0 Waypoint,7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46368 Branch Residuals and Soils LLC Project Von Drehle Bob Branch Report Date : 04/06/2022 1735 Heckle Blvd Information : Project# 2014-110 Received : 03/22/2022 Suite 103-291 Rock Hill , SC 29732 p Taw[( c MC Rio a� Pauric Mc Groary Ph.D., CPA Report Number: 22-081-0014 REPORT OFANALYSIS Agronomist Lab No : 57238 Matrix: Solids Sample ID: VD Sampled: 3/21/2022 13:15 Test Results Units MOL DF Date / Time By Analytical Analyzed Method Moisture 57.9 % 0.010 1 03/28/2216:47 FMM SM-254OG Total Kjeldahl Nitrogen 3800 mg/Kg - dry 594 1 03/29/22 11:00 JPJ ;M-4500-NH3C-TKP Potassium 84.3 mg/Kg - dry 23.8 1 03/31/22 00:13 EAL 6010D Calcium 208000 mg/Kg - dry 2380 20 03/29/22 18:52 TJS 6010D Sodium 549 mg/Kg - dry 59.4 1 03/29/22 04:22 EAL 6010D Aluminum 1950 mg/Kg - dry 11.9 1 03/29/22 04:22 TJS 6010D Manganese 40.9 mg/Kg - dry 1.19 1 03/29/22 04:22 EAL 6010D Zinc 67.0 mg/Kg - dry 2.97 1 03/29/22 04:22 EAL 6010D Nickel 1.00 mg/Kg - dry 0.593 1 03/29/22 04:22 EAL 6010D Lead 2.85 mg/Kg - dry 0.712 1 03/29/22 04:22 EAL 6010D Arsenic 1.94 mg/Kg - dry 1.19 1 03/29/22 04:22 EAL 6010D Calcium Carbonate Equivalent 25.3 % 0.1 1 04/05/22 11:26 DXT AOAC 955.01 Test Results Units MQL DF Date / Time By Analytical Analyzed Method pH 7.1 SM. 1 03/29/22 15:33 DRS 9045D Copper 28.3 mg/Kg - dry 1.19 1 03/29/22 04:22 EAL 6010D Selenium <1.19 mg/Kg - dry 1.19 1 03/29/22 04:22 EAL 6010D Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 3 of 7 Waypoint._ :, 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 °Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46368 Branch Residuals and Soils LLC Project Von Drehle Bob Branch Report Date : 04/06/2022 1735 Heckle Blvd Information : Project# 2014-110 Received : 03/22/2022 Suite 103-291 Rock Hill , SC 29732 q i awry �1 �ioP1� Pauric Mc Groary Ph.D., CPA Report Number: 22-081-0014 REPORT OFANALYSIS Agronomist Lab No : 57238 Matrix: Solids Sample ID: VD Sampled: 3/21/2022 13:15 Total Solids 42.1 % 0.010 1 03/28/22 16:47 FMM SM-254OG Phosphorus 122 mg/Kg - dry 11.9 1 03/29/22 04:22 EAL 6010D Sulfur 762 mg/Kg - dry 23.8 1 03/29/22 04:22 EAL 6010D Magnesium 2160 mg/Kg - dry 11.9 1 03/29/22 04:22 EAL 6010D Iron 1030 mg/Kg - dry 23.8 1 03/29/22 04:22 TJS 6010D Ammonia Nitrogen 382 mg/Kg - dry 238 1 03/29/22 15:00 JPJ SM-4500-NH3C Nitrate+Nitrite-N <11.9 mg/Kg - dry 11.9 1 03/29/22 13:58 ZBD 4500NO3F-2011 Cadmium <0.238 mg/Kg - dry 0.238 1 03/29/22 04:22 EAL 6010D Chromium 3.14 mg/Kg - dry 0.593 1 03/29/22 04:22 EAL 6010D Mercury 0.0605 mg/Kg - dry 0.0325 1 03/30/22 12:22 ZMT SW-7471B Molybdenum 5.13 mg/Kg - dry 0.593 1 03/29/22 04:22 EAL 6010D Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit Page 4 of 7 Waypoint(2) ANALYTICAL Client: Branch Residuals and Soils LLC Project: Von Drehle Lab Report Number: 22-081-0014 Date: 4/5/2022 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com CASE NARRATIVE Metals Analysis Method 6010D Sample 94622 Analyte: Aluminum QC Batch No: 1-607797/1-607031 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94622 Analyte: Iron QC Batch No: 1-607797/1-607031 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94622 Analyte: Lead QC Batch No: 1-607591/1-607031 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94087 (Frederick City) Analyte: Potassium QC Batch No: 1-608083/1-607764 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 5 of 7 • (2) Waypoir�t 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 1 Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Shipment Receipt Form Customer Number: 46368 Customer Name: Branch Residuals and Soils LLC Report Number: 22-081-0014 Shipping Method Fed Ex US Postal Lab Other • UPS Client Courier Thermometer ID: Shipping container/cooler uncompromised? 4, Yes No Number of coolers/boxes received F1 Custody seals intact on shipping container/cooler? Yes No 16 Not Present Custody seals intact on sample bottles? ) Yes No • Not Present Chain of Custody (COC) present? Yes No COC agrees with sample label(s)? Yes No COC properly completed j. Yes No Samples in proper containers? i6', Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test(s)? Yes No All samples received within holding time? Yes No Cooler temperature in compliance? • Yes No Cooler/Samples arrived at the laboratory on ice. • Yes No Samples were considered acceptable as cooling process had begun. Water - Sample containers properly preserved Yes No • N/A Water - VOA vials free of headspace Yes No 0 N/A Trip Blanks received with VOAs Yes No • N/A Soil VOA method 5035 — compliance criteria met Yes No • N/A High concentration container (48 hr) Low concentration EnCore samplers (48 hr) High concentration pre -weighed (methanol -14 d) Low cone pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? Yes 41 No Comments: Signature: Brandi Watson Date & Time: 03/22/2022 14:16:31 Page 6 of 7 6;o£GBee }\ k E \ \ \ k k ) \ \ § k Z f ( g&] mmCL zu� ao f}// an - 0 o - �§E}/ .�0__ ? § z I ) @ g g 0 Sa egm] ❑k �)} _ ! Wig) c §ri . - a. 2(/ �L E I !M 'a _ 7 7 - � E % � E E }\) lo MOD CL � ! g . a 3 ƒ }(_ % / C 7 z k k k) m k cc �a £ - ) ) z cc E. k�d=�m, i A,m,pti) x1ijew 2 ri E . _- m�� g @, _N �ix _ cr cc \ / . 7 . ƒ 7( fko E } Z _ - - k , g - ' £ } \� - . � } � � 2 _ z ( J | �}/ Ja )42 k I § ///ci - / � / � Waypointo ANALYTICAL 5/6/2022 Branch Residuals and Soils LLC Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill, SC, 29732 Ref: Analytical Testing 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointa nalytical.com Report Number: 22-117-0014 Project Description: Von Drehle 2014-110 Dear Bob Branch: Waypoint Analytical Virginia, Inc. received sample(s) on 4/27/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, T&WI c Mt &loam/ Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 8 0WaYPO*nt 7621 ain 80 -7 Road, Richmond, 27 -6446 Main 804-743 9401 *Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 22-117-0014 Client Project Description: Von Drehle 2014-110 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 57687 VD Solids 57687 VD Solids 57687 VD Solids 57687 VD Solids 57687 VD Solids 57687 VD Solids 57687 VD Solids 57687 VD Solids WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN 04/26/2022 13:30 04/27/2022 04/26/2022 13:30 04/27/2022 04/26/2022 13:30 04/27/2022 04/26/2022 13:30 04/27/2022 04/26/2022 13:30 04/27/2022 04/26/2022 13:30 04/27/2022 04/26/2022 13:30 04/27/2022 04/26/2022 13:30 04/27/2022 SM-2540G WP MTN SM-4500-NH3C WP MTN SM-4500-NH3C-TKN WP MTN 4500NO3F-2011 WP MTN 6010D WP MTN SW-7471B WP MTN 9045D WP MTN AOAC 955.01 WP MTN Page 2 of 8 Waypointo ANALYTICAL 46368 Branch Residuals and Soils LLC Project Von Drehle Bob Branch 1735 Heckle Blvd Information : 2014-110 Suite 103-291 Rock Hill , SC 29732 Report Number: 22-117-0014 Lab No : 57687 Sample ID: VD 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Report Date : 05/06/2022 Received : 04/27/2022 Taws( t G10wr REPORTOFANALY5I5 Pauric Mc Groary Ph.D., CPA Agronomist Matrix: Solids Sampled: 4/ 26/ 2022 13:30 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Moisture 59.7 % 0.010 1 04/29/2215:53 FMM SM-2540G Potassium 78.4 mg/Kg - dry 24.8 1 05/05/22 22:15 EAL 6010D Calcium 200000 mg/Kg - dry 6200 50 05/03/22 16:54 TJS 6010D Sodium 809 mg/Kg - dry 62.0 1 05/03/22 03:37 EAL 6010D Aluminum 1830 mg/Kg - dry 12.4 1 05/03/22 16:59 TJS 6010D Nickel <0.620 mg/Kg - dry 0.620 1 05/03/22 03:37 EAL 6010D Arsenic <1.24 mg/Kg - dry 1.24 1 05/03/22 03:37 EAL 6010D Test Results Units MQL DF Date / Time By Analytical Analyzed Method pH 7.6 S.U. 1 05/03/2215:18 DRS 9045D Total Solids 40.3 % 0.010 1 04/29/22 15:53 FMM SM-2540G Copper 30.5 mg/Kg - dry 1.24 1 05/03/22 03:37 EAL 6010D Lead 2.02 mg/Kg - dry 0.744 1 05/03/22 03:37 EAL 6010D Magnesium 2240 mg/Kg - dry 12.4 1 05/03/22 03:37 EAL 6010D Selenium <1.24 mg/Kg - dry 1.24 1 05/03/22 03:37 EAL 6010D Total Kjeldahl Nitrogen Qualifiers/ DF Dilution Factor Definitions 5860 mg/Kg - dry 620 1 05/05/22 13:00 JPJ >M-4500-NH3C-TKP MQL Method Quantitation Limit Page 3 of 8 Waypointo ANALYTICAL 46368 Branch Residuals and Soils LLC Project Von Drehle Bob Branch 1735 Heckle Blvd Information : 2014-110 Suite 103-291 Rock Hill , SC 29732 Report Number: 22-117-0014 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com REPORT OFANALYSIS Report Date : 05/06/2022 Received : 04/27/2022 Tawic mt (10T Pauric Mc Groary Ph.D., CPA Agronomist Lab No : 57687 Sample ID : VD Matrix: Solids Sampled: 4/26/2022 13:30 Phosphorus 126 mg/Kg - dry 12.4 1 05/03/22 03:37 TJS 6010D Zinc 71.0 mg/Kg - dry 3.10 1 05/03/22 03:37 EAL 6010D Ammonia Nitrogen <248 mg/Kg - dry 248 1 05/05/22 13:00 JPJ SM-4500-NH3C Nitrate+ N itrite-N <11.8 mg/Kg - dry 11.8 1 05/02/22 14:40 ZBD 4500NO3F-2011 Cadmium <0.248 mg/Kg - dry 0.248 1 05/03/22 16:59 TJS 6010D Mercury <0.342 mg/Kg - dry 0.342 1 05/02/22 14:12 ZMT SW-7471B Calcium Carbonate Equivalent 43.3 % 0.1 1 05/02/22 12:14 DXT AOAC 955.01 Molybdenum 3.52 mg/Kg - dry 0.620 1 05/03/22 03:37 EAL 6010D Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit Page 4 of 8 Waypoint.(2) ANALYTICAL Client: Branch Residuals and Soils LLC Project: Von Drehle Lab Report Number: 22-117-0014 Date: 5/6/2022 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com CASE NARRATIVE Metals Analysis Method 6010D Sample 94587 (Biosolids) Analyte: Aluminum QC Batch No: 1-614107/1-613524 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94587 (Biosolids) Analyte: Calcium QC Batch No: 1-613976/1-613524 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 57687 (VD) Analyte: Cadmium QC Batch No: 1-613976/1-613524 This analyte was analyzed at a dilution due to IEC interference/matrix interference. Sample 94587 (Biosolids) Analyte: Copper QC Batch No: 1-613976/1-613524 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94587 (Biosolids) Analyte: Phosphorus QC Batch No: 1-613976/1-613524 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94587 (Biosolids) Analyte: Zinc QC Batch No: L613976/L613524 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 85038 (SLR) Analyte: Potassium QC Batch No: 1-614676/1-614400 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Solids Total Mercury Analysis - CVAA Method 7471A Sample 99462 (Untreated Shatter Shield Plastic) Analyte: Mercury Page 5 of 8 Wayplpint(2)AYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° fax 804-271-6446 www.waypointanalytical.com QC Batch No: 1-613966/1-613596 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Page 6 of 8 (2) Waypoint 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Shipment Receipt Form Customer Number: 46368 Customer Name: Branch Residuals and Soils LLC Report Number: 22-117-0014 Shipping Method Fed Ex US Postal Lab Other • UPS Client Courier Thermometer ID: Shipping container/cooler uncompromised? Yes No Number of coolers/boxes received �1 Custody seals intact on shipping container/cooler? Yes No • Not Present Custody seals intact on sample bottles? 1 Yes No • Not Present Chain of Custody (COC) present? Yes No COC agrees with sample label(s)? • Yes No COC properly completed • Yes No Samples in proper containers? • Yes No Sample containers intact? • Yes No Sufficient sample volume for indicated test(s)? • Yes No All samples received within holding time? • Yes No Cooler temperature in compliance? • Yes No Cooler/Samples arrived at the laboratory on ice. • Yes No Samples were considered acceptable as cooling process had begun. Water - Sample containers properly preserved Yes No • N/A Water - VOA vials free of headspace Yes No 46 N/A Trip Blanks received with VOAs Yes No • N/A Soil VOA method 5035 — compliance criteria met Yes No • N/A High concentration container (48 hr) Low concentration EnCore samplers (48 hr) High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? Yes • No Comments: Signature: Brandi Watson Date & Time: 04/27/2022 07:55:35 Page 7 of 8 8 3o 8 abed O E � o` r'E 2 O C •� = m m p O O � o xa= c E N 2 g a x ° a a Z u v¢ v v m a v O o 7 O o o c p 0 na c V u Apr 0 0 C n 2 m Q 2 z x S 2 V r4 L 'u W - T G w N Q m V 0 %2 x_ W W W a a a Vf N VI IV91 w G E V Mama E o Q rr s I z G o it L O m E G E w E G E r p c L c m CL r. Cl. m 1 c a cu � a w V � n C c o m V Z E ))`+! O w f Y q E aj o` ¢ N m �y 1 rr. a a z a z a z z v Q At m n_ a7isodwo(�) �p geil9l m `s� � 0 a z C , I ,S (Aa)l of ja)aa) ruleW c a f L,) c c 7 7 siau!eluo}ojagwnN n m C r U .�. tt i �j J ,`•i r3 ~~ ` c ri > �Y CL `�` _ o _ C ✓J n ra ,a y c = c p c w a u c u �r a` a v w p d a E j Z �^ o m J i^ LL v 9 N Z 6 c Ct • �� m E LH G w h r — .1 m Waypointo ANALYTICAL 6/14/2022 Branch Residuals and Soils LLC Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill, SC, 29732 Ref: Analytical Testing Report Number: 22-153-0006 Project Description: 2014-110 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Dear Bob Branch: Waypoint Analytical Virginia, Inc. received sample(s) on 6/2/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 8 (2) Waypoint. 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 22-153-0006 Client Project Description: 2014-110 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 58186 VD Solids 58186 VD Solids 58186 VD Solids 58186 VD Solids 58186 VD Solids 58186 VD Solids 58186 VD Solids 58186 VD Solids WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN 05/31/2022 03:15 06/02/2022 05/31/2022 03:15 06/02/2022 05/31/2022 03:15 06/02/2022 05/31/2022 03:15 06/02/2022 05/31/2022 03:15 06/02/2022 05/31/2022 03:15 06/02/2022 05/31/2022 03:15 06/02/2022 05/31/2022 03:15 06/02/2022 SM-2540G WP MTN SM-4500-NH3C WP MTN SM-4500-NH3C-TKN WP MTN 4500NO3F-2011 WP MTN 6010D WP MTN SW-7471B WP MTN 9045D WP MTN AOAC 955.01 WP MTN Page 2 of 8 Waypointo ANALYTICAL 46368 Branch Residuals and Soils LLC Project 2014-110 Bob Branch 1735 Heckle Blvd Information Suite 103-291 Rock Hill , SC 29732 Report Number:22-153-0006 Lab No : 58186 Sample ID: VD 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Report Date : 06/14/2022 Received �y: 06/02/2022 TAWit I Gt"T REPORT OFANALYSIS Pauric Mc Groary Ph.D., CPA Agronomist Matrix: Solids Sampled: 5/31/2022 3:15 Test Results Units MQL DF Date / Time Analyzed By Analytical Method Moisture 56.8 % 0.010 1 06/07/2216:21 FMM SM-2540G Potassium 88.4 mg/Kg - dry 23.1 1 06/07/22 19:02 EAL 6010D Calcium 201000 mg/Kg - dry 2310 20 06/09/22 03:40 EAL 6010D Sodium 752 mg/Kg - dry 57.9 1 06/07/22 19:02 EAL 6010D Aluminum 2010 mg/Kg - dry 11.6 1 06/07/22 19:02 EAL 6010D Nickel 0.763 mg/Kg - dry 0.578 1 06/07/22 19:02 EAL 6010D Arsenic <1.16 mg/Kg - dry 1.16 1 06/07/22 19:02 EAL 6010D Test Results Units MQL DF Date / Time By Analytical Analyzed Method pH 7.3 S.U. 1 06/08/2215:21 DRS 9045D Total Solids 43.2 % 0.010 1 06/07/22 16:21 FMM SM-2540G Copper 24.3 mg/Kg - dry 1.16 1 06/07/22 19:02 EAL 6010D Lead 1.00 mg/Kg - dry 0.694 1 06/07/22 19:02 EAL 6010D Magnesium 2210 mg/Kg - dry 11.6 1 06/07/22 19:02 EAL 6010D Selenium <1.16 mg/Kg - dry 1.16 1 06/07/22 19:02 EAL 6010D Total Kjeldahl Nitrogen Qualifiers/ DF Dilution Factor Definitions 3750 mg/Kg - dry 579 1 06/14/22 11:30 ]P3 ;M-4500-NH3C-TKP MQL Method Quantitation Limit Page 3 of 8 Waypointo ANALYTICAL 46368 Branch Residuals and Soils LLC Project 2014-110 Bob Branch 1735 Heckle Blvd Information Suite 103-291 Rock Hill , SC 29732 Report Number:22-153-0006 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com REPORT Of ANAL YSIS Report Date : 06/14/2022 Received : 06/02/2022 Yawn M, �10wr Pauric Mc Groary Ph.D., CPA Agronomist Lab No : 58186 Sample ID: VD Matrix: Solids Sampled: 5/31/2022 3:15 Phosphorus 115 mg/Kg - dry 11.6 1 06/07/22 19:02 EAL 6010D Zinc 97.5 mg/Kg - dry 2.89 1 06/07/22 19:02 EAL 6010D Ammonia Nitrogen <231 mg/Kg - dry 231 1 06/14/22 14:30 JPJ SM-4500-NH3C Nitrate+Nitrite-N <11.0 mg/Kg - dry 11.0 1 06/07/22 14:55 ZBD 4500NO3F-2011 Cadmium <0.231 mg/Kg - dry 0.231 1 06/07/22 19:02 EAL 6010D Mercury <0.324 mg/Kg - dry 0.324 1 06/07/22 15:54 ZMT SW-7471B Calcium Carbonate Equivalent 48.9 % 0.1 1 06/09/22 12:45 DXT ACAC 955.01 Molybdenum 3.73 mg/Kg - dry 0.578 1 06/07/22 19:02 EAL 6010D Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 4 of 8 Waypointo ANALYTICAL Client: Branch Residuals and Soils LLC Project: 2014-110 Lab Report Number: 22-153-0006 Date: 6/14/2022 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com CASE NARRATIVE Metals Analysis Method 6010D Sample 90192 (WRC Topsoil (June)) Analyte: Aluminum QC Batch No: 1-620235/1-619916 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 90192 (WRC Topsoil (June)) Analyte: Aluminum QC Batch No: 1-620618/1-619916 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 90192 (WRC Topsoil (June)) Analyte: Calcium QC Batch No: 1-620618/1-619916 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 90192 (WRC Topsoil (June)) Analyte: Potassium QC Batch No: L620618/L619916 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 90192 (WRC Topsoil (June)) Analyte: Magnesium QC Batch No: 1-620235/1-619916 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 90192 (WRC Topsoil (June)) Analyte: Phosphorus QC Batch No: 1-620235/1-619916 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 90192 (WRC Topsoil (June)) Analyte: Lead QC Batch No: 1-620235/1-619916 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 90192 (WRC Topsoil (June)) Page 5 of 8 Waypoint(2) ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Analyte: Selenium QC Batch No: 1-620235/1-619916 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 6 of 8 (2) Waypoint 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 1 Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Shipment Receipt Form Customer Number: 46368 Customer Name: Branch Residuals and Solis LLC Report Number: 22-153-0006 Shipping Method Fed Ex US Postal Lab Other • UPS Client Courier Thermometer ID: I T Shipping container/cooler uncompromised? # Yes No Number of coolers/boxes received F1 Custody seals intact on shipping container/cooler? Yes No • Not Present Custody seals intact on sample bottles? Yes No • Not Present Chain of Custody (COC) present? • Yes No COC agrees with sample label(s)? Yes No COC properly completed Yes No Samples in proper containers? • Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test(s)? Yes No All samples received within holding time? • Yes No Cooler temperature in compliance? • Yes No Cooler/Samples arrived at the laboratory on ice. • Yes No Samples were considered acceptable as cooling process had begun. Water - Sample containers properly preserved Yes No • N/A Water - VOA vials free of headspace Yes No • N/A Trip Blanks received with VOAs Yes No • N/A Soil VOA method 5035 — compliance criteria met Yes No • N/A High concentration container (48 hr) Low concentration EnCore samplers (48 hr) High concentration pre -weighed (methanol -14 d) Low cone pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? Yes • No Comments: Signature: David Lennon Date & Time: 06/02/2022 11:46:51 Page 7 of 8 v� 0 .G � :i O O 6 co z n 00 3 m 1 a D n rl N ft z 2 T r cr 3 N S A m v v n o O a c n 7 O I A O IC '-�'� R Ch w w o a w pim v a n 3 o n? 10 ram'tj a o ro a ro 3 dlu G Number of Containers � �3T a Matrix (Refer to Key) z n. cr 21 0. eta c j 7 Z , w � ,�� 1 ' -, m (G)rab or (C)omposite r:: oFT �X 3� 2 2 2 p> 3 a z 1~~ _ 09 __ CL J m Z j ff 3 r_ 4 3 .% n1i1 M. a c // ,- ID j d N j{{j •� t� O O n ❑❑a I A m `gym 3 v C n; o l A N � c= e 3 3 c 3 c L� n _ - o z A A M A A A < m s c n c ro U a c. a = sa c 2 4 2 2 Dt s - 2 Ma n m D m rS.f 1A.f b Q d cA _ O . O N O O o p0� n O= w S A p n a G a 9 9 z N N V � ^ p Q1 N 2 C N n Z n Z b C n V N Lj O O O m s er n m A ra 3 - v� o o O c O O Page 8 of 8 WayPAoint . NALYTICAL 7/26/2022 Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill, SC, 29732 Ref: Analytical Testing Lab Report Number: 22-195-0047 Client Project Description: Von Dizehle Cordova, NC Project #2014-110 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Dear Mr. Bob Branch: Waypoint Analytical, LLC. received sample(s) on 7/14/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Randy Thomas Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 8 Waypointo ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2023 Arkansas State Program 88-0650 02/07/2023 California State Program 2904 06/30/2023 Florida State Program - NELAP E871157 06/30/2023 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2023 Illinois State Program - NELAP 200078 10/10/2022 Kentucky State Program 80215 06/30/2022 Kentucky State Program KY90047 12/31/2022 Louisiana State Program - NELAP LA037 12/31/2022 Louisiana State Program - NELAP 04015 06/30/2023 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2022 Pennsylvania State Program - NELAP 68-03195 05/31/2023 South Carolina State Program 84002 06/30/2022 Tennessee State Program 02027 02/11/2023 Texas State Program - NELAP T104704180 09/30/2022 Virginia State Program 00106 06/30/2023 Virginia State Program - NELAP 460181 09/14/2022 Page 1 of 1 00001122-195-0047 Page 2 of 8 (2) • 2790 Whitten Road, Memphis, TN 38133 Waypoint. Main 901.213.2400 ° Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 22-195-0047 Client Project Description: Von Dizehle Cordova, NC Project #2014-110 Lab No Client Sample ID 99086 VD Matrix Date Collected Date Received Solids 07/13/202213:00 07/14/2022 Page 3 of 8 WayplRint AYTICAL Client: Branch Residuals and Soils LLC Project: Von Dizehle Lab Report Number: 22-195-0047 Date: 7/25/2022 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com CASE NARRATIVE Metals Analysis Method 6010D Sample 86731 (SB27-2-4) Analyte: Aluminum QC Batch No: 1-628020/1-627265 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 86731 (SB27-2-4) Analyte: Arsenic QC Batch No: 1-627787/1-627265 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 86731 (SB27-2-4) Analyte: Iron QC Batch No: L627787/1-627265 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 86731 (SB27-2-4) Analyte: Potassium QC Batch No: 1-627787/1-627265 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 4 of 8 Waypoint. 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 1 Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 22972 Branch Residuals and Soils LLC Project Von Dizehle Mr. Bob Branch Report Date : 07/26/2022 1735 Heckle Blvd Information : Cordova, NC Received : 07/14/2022 Suite 103-291 Project #2014-110 Rock Hill , SC 29732 Report Number: 22-195-0047 REPORT OPANALYSIS Lab No : 99086 Sample ID : VD Matrix: Solids Sampled: 7/13/2022 13:00 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Neutralizing Value (%CCE) 28.1 % 0.1 1 07/20/22 16:34 DXT AOAC 955.01 Moisture 67.9 % 0.010 1 07/20/2216:09 FMM 2540G-2011 Ammonia Nitrogen 330 mg/Kg - dry 312 1 07/25/22 12:30 JPJ 4500NH3C-2011 Nitrate (NC3-N) <3.12 mg/Kg - dry 3.12 1 07/15/22 19:40 JCA 9056A Nitrite (NO2-N) <3.12 mg/Kg - dry 3.12 1 07/15/22 19:40 JCA 9056A Nitrate+Nitrite-N <3.12 mg/Kg - dry 3.12 1 07/15/22 19:40 9056A pH 7.8 SM. 1 07/21/2216:06 DRS 9045D Total Solids 32.1 % 0.010 1 07/20/22 16:09 FMM 2540G-2011 Total Kjeldahl Nitrogen 2830 mg/Kg - dry 458 1 07/19/22 12:36 CLP 4500NORGD-2011 Phosphorus 127 mg/Kg - dry 15.6 1 07/20/22 22:30 EAL 6010D Aluminum 1680 mg/Kg - dry 15.6 1 07/20/22 22:30 EAL 6010D Arsenic <1.56 mg/Kg - dry 1.56 1 07/20/22 22:30 EAL 6010D Cadmium <0.312 mg/Kg - dry 0.312 1 07/20/22 22:30 EAL 6010D Calcium 110000 mg/Kg - dry 779 5 07/21/22 13:21 EAL 6010D Copper 27.0 mg/Kg - dry 1.56 1 07/20/22 22:30 EAL 6010D Iron 1140 mg/Kg - dry 31.2 1 07/20/22 22:30 EAL 6010D Lead 2.08 mg/Kg - dry 0.934 1 07/20/22 22:30 EAL 6010D Magnesium 1440 mg/Kg - dry 15.6 1 07/20/22 22:30 EAL 6010D Mercury <0.452 mg/Kg - dry 0.452 1 07/21/22 16:32 JTR 7471A Molybdenum 3.64 mg/Kg - dry 0.778 1 07/20/22 22:30 EAL 6010D Nickel 2.08 mg/Kg - dry 0.778 1 07/20/22 22:30 EAL 6010D Potassium 66.7 mg/Kg - dry 31.2 1 07/20/22 22:30 EAL 6010D Selenium <1.56 mg/Kg - dry 1.56 1 07/20/22 22:30 EAL 6010D Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page S of 8 s 2790 Whitten Road, Memphis, TN 38133 Waypoint. Main 901.213.2400 ° Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 22972 Branch Residuals and Soils LLC Project Von Dizehle Mr. Bob Branch Report Date : 07/26/2022 1735 Heckle Blvd Information : Cordova, NC Received : 07/14/2022 Suite 103-291 Project #2014-110 Rock Hill , SC 29732 Report Number: 22-195-0047 REPORT OFANAL YSIS Lab No : 99086 Matrix: Solids Sample ID: VD Sampled: 7/13/2022 13:00 Test Results Units MOL DF Date / Time By Analytical Analyzed Method Sodium 595 mg/Kg - dry 77.9 1 07/20/22 22:30 EAL 6010D Zinc 93.8 mg/Kg - dry 3.89 1 07/20/22 22:30 EAL 6010D Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 6 of 8 (2) Waypoint 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 °Fax 901.21213.2440.2440 ANALYTICAL www.waypointanalytical.com Shipment Receipt Form Customer Number: 22972 Customer Name: Branch Residuals and Soils LLC Report Number: 22-195-0047 Shipping Method Fed Ex US Postal Lab Other • UPS Client Courier Thermometer ID: F102 Shipping container/cooler uncompromised? ( Yes No Number of coolers/boxes received F 1 Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? y' Yes No • Not Present Chain of Custody (COC) present? ib Yes No COC agrees with sample label(s)? 0 Yes No COC properly completed • Yes No Samples in proper containers? • Yes No Sample containers intact? • Yes No Sufficient sample volume for indicated test(s)? • Yes No All samples received within holding time? • Yes No Cooler temperature in compliance? • Yes No Cooler/Samples arrived at the laboratory on ice. • Yes No Samples were considered acceptable as cooling process had begun. Water - Sample containers properly preserved Yes No • N/A Water - VOA vials free of headspace Yes No • N/A Trip Blanks received with VOAs Yes No • N/A Soil VOA method 5035 — compliance criteria met Yes No 6 N/A High concentration container (48 hr) Low concentration EnCore samplers (48 hr) High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? Yes • No Comments: Signature: Makayla Weaver Date & Time: 07/14/2022 11:18:53 Page 7 of 8 0 - I = O c o E f= E iE E� r, t, O U t � vOi f N .Gi G G G m O o 2 O O o `•j fjl N N N \ N N N , � 6 4 S. S Y G tD nCLx`f £ n3 tt v v Q� v c00 p ° u 0 o N o o j y T v v x 2 2 x m m vO u .O O i •J. i 0 a N Q m v D W 4 V S_ W W T _I n z 0 z Vr _ �.ir m o rl 0 N G G 11 D Li? a E £ v °G z z Da> V t O A Y !- _N ° L y Ac O N G F- hfa H C- O C O L - U O A 1 cr ❑� •N y .. A �.t �1 m R u rs a � c Q _ 21 Q. a G 7 O n C m m E r i1) o o �1` T' G � A ✓ Ucc W W W cc o I n ti y Q Q Q ° m s� a 't al!sodwo(:)) jo gei(g) LJ Z a (AaH of ja;a8) xijleyy m N N N \l G n } Cis _ u`j c c V rs � svauiewo);ojagwnN ,I d rs m 'S c �=� O c LL rs „i O t luMC m n O m u m y = lu 4 G O a O f; E � � v0 O r `r, c E • C r -� W \ G > C�lJ v a_ �G c R G Z m Cam• �� r � %-t � n �., V u a` a` �,yl Page a of 8 Waypointo ANALYTICAL 8/4/2022 Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill, SC, 29732 Ref: Analytical Testing Lab Report Number: 22-207-0063 Client Project Description: Sludge Testing 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Dear Mr. Bob Branch: Waypoint Analytical, LLC. received sample(s) on 7/26/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, I M �Wwffl.! Randy Thomas Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 9 Waypointo ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2023 Arkansas State Program 88-0650 02/07/2023 California State Program 2904 06/30/2023 Florida State Program - NELAP E871157 06/30/2023 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2023 Illinois State Program - NELAP 200078 10/10/2022 Kentucky State Program 80215 06/30/2023 Kentucky State Program KY90047 12/31/2022 Louisiana State Program - NELAP LA037 12/31/2022 Louisiana State Program - NELAP 04015 06/30/2023 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2022 Pennsylvania State Program - NELAP 68-03195 05/31/2023 South Carolina State Program 84002 06/30/2022 Tennessee State Program 02027 02/11/2023 Texas State Program - NELAP T104704180 09/30/2022 Virginia State Program 00106 06/30/2023 Virginia State Program - NELAP 460181 09/14/2022 Page 1 of 1 00001/22-207-0063 Page 2 of 9 (!D2790 Whitten Road, Memphis, TN 38133 Waypoint Main 901.213.2400 ° Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 22-207-0063 Client Project Description: Sludge Testing Lab No Client Sample ID Matrix Date Collected Date Received 91259 VD Solids 07/25/202213:30 07/26/2022 Page 3 of 9 WYPOInt ANALYTICAL Client: Branch Residuals and Soils LLC Project: Sludge Testing Lab Report Number: 22-207-0063 Date: 8/4/2022 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalVtical.com CASE NARRATIVE Metals Analysis Method 6010D Sample 91854 (4-3A) Analyte: Aluminum QC Batch No: 1-629552/1-629101 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 91854 (4-3A) Analyte: Arsenic QC Batch No: 1-629552/1-629101 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 91854 (4-3A) Analyte: Calcium QC Batch No: 1-629798/1-629101 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 91854 (4-3A) Analyte: Cadmium QC Batch No: 1-629552/1-629101 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 91854 (4-3A) Analyte: Copper QC Batch No: 1-629552/1-629101 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 91854 (4-3A) Analyte: Iron QC Batch No: 1-629798/1-629101 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 91854 (4-3A) Analyte: Potassium QC Batch No: 1-629552/1-629101 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 4 of 9 Waypoint(2) ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Sample 91854 (4-3A) Analyte: Magnesium QC Batch No: 1-629552/1-629101 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 91854 (4-3A) Analyte: Manganese QC Batch No: 1-629552/1-629101 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 91854 (4-3A) Analyte: Sodium QC Batch No: 1-629552/1-629101 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 91854 (4-3A) Analyte: Nickel QC Batch No: 1-629552/1-629101 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 91854 (4-3A) Analyte: Lead QC Batch No: 1-629552/1-629101 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 91854 (4-3A) Analyte: Zinc QC Batch No: 1-629798/1-629101 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 5 of 9 Waypoint-0 ANALYTICAL 22972 Branch Residuals and Soils LLC Project Sludge Testing Mr. Bob Branch 1735 Heckle Blvd Information Suite 103-291 Rock Hill , SC 29732 Report Number:22-207-0063 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com REPORT OPANAL YSlS Report Date : 08/04/2022 Received : 07/26/2022 Lab No : 91259 Matrix: Solids Sample ID: VD Sampled: 7/25/2022 13:30 Test Results Units MOL DF Date / Time By Analytical Analyzed Method Neutralizing Value (%CCE) 68.3 % 0.1 1 08/03/22 09:48 DXT AOAC 955.01 Moisture 60.4 % 0.010 1 07/28/22 16:17 FMM 2540G-2011 Ammonia Nitrogen <253 mg/Kg - dry 253 1 08/02/22 14:30 JPJ 4500NH3C-2011 Nitrate (NO3-N) <2.53 mg/Kg - dry 2.53 1 07/27/22 15:49 JCA 9056A Nitrite (NO2-N) <2.53 mg/Kg - dry 2.53 1 07/27/22 15:49 JCA 9056A Nitrate+Nitrite-N <2.53 mg/Kg - dry 2.53 1 07/27/22 15:49 9056A Organic N 1659 mg/Kg - dry 530.3 1 07/29/22 10:41 CALCULATION pH 7.1 S.U. 1 08/01/2216:03 DRS 9045D Total Solids 39.6 % 0.010 1 07/28/22 16:17 FMM 254OG-2011 Total Volatile Solids 45.7 % 0.010 1 07/28/22 16:17 FMM 254OG-2011 Total Kjeldahl Nitrogen 1660 mg/Kg - dry 530 1 07/29/22 10:41 ANH 4500NORGD-2011 Phosphorus 123 mg/Kg - dry 12.6 1 07/29/22 18:20 TJS 6010D Aluminum 2160 mg/Kg - dry 12.6 1 07/29/22 18:20 TJS 6010D Arsenic <1.26 mg/Kg - dry 1.26 1 07/29/22 18:20 TJS 6010D Cadmium <0.253 mg/Kg - dry 0.253 1 07/29/22 18:20 TJS 6010D Calcium 192000 mg/Kg - dry 1260 10 08/01/22 14:07 TJS 6010D Copper 28.8 mg/Kg - dry 1.26 1 07/29/22 18:20 TJS 6010D Iron 917 mg/Kg - dry 25.3 1 07/29/22 18:20 TJS 6010D Lead 2.15 mg/Kg - dry 0.757 1 07/29/22 18:20 TJS 6010D Magnesium 2530 mg/Kg - dry 12.6 1 07/29/22 18:20 TJS 6010D Manganese 43.4 mg/Kg - dry 1.26 1 07/29/22 18:20 TJS 6010D Mercury <0.354 mg/Kg - dry 0.354 1 07/27/22 12:33 TJS 7471A Molybdenum 3.56 mg/Kg - dry 0.631 1 07/29/22 18:20 TJS 6010D Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 6 of 9 a2790 Whitten Road, Memphis, TN 38133 Waypoint Main 901.213.2400 ° Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 22972 Branch Residuals and Soils LLC Project Sludge Testing Mr. Bob Branch Report Date : 08/04/2022 1735 Heckle Blvd Information : Received : 07/26/2022 Suite 103-291 Rock Hill , SC 29732 Report Number : 22-207-0063 REPORT OFANALYSIS Lab No : 91259 Sample ID: VD Matrix: Solids Sampled: 7/25/2022 13:30 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Nickel 0.853 mg/Kg - dry 0.631 1 07/29/22 18:20 TJS 6010D Potassium 63.6 mg/Kg - dry 25.3 1 07/29/22 18:20 TJS 6010D Selenium <1.26 mg/Kg - dry 1.26 1 07/29/22 18:20 TJS 6010D Sodium 717 mg/Kg - dry 63.1 1 07/29/22 18:20 TJS 6010D Zinc 82.1 mg/Kg - dry 3.16 1 07/29/22 18:20 TJS 6010D Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit Page 7 of 9 (2) Waypoint 2790 Whitten Road, Memphis, .2440 Main 901.213.2400 * fax 901.21213.2440 ANALYTICAL www.waypointanalytical.corn Shipment Receipt Form Customer Number: 22972 Customer Name: Branch Residuals and Soils LLC Report Number: 22-207-0063 Shipping Method Fed Ex US Postal Lab Other • UPS Client Courier Thermometer ID: IT102 Shipping container/cooler uncompromised? 10 Yes No Number of coolers/boxes received 1 Custody seals intact on shipping container/cooler? ^ : Yes No • Not Present Custody seals intact on sample bottles? Yes No • Not Present Chain of Custody (COC) present? Yes No COC agrees with sample label(s)? • Yes No COC properly completed • Yes No Samples in proper containers? Yes No Sample containers intact? G Yes No Sufficient sample volume for indicated test(s)? • Yes No All samples received within holding time? 0 Yes No Cooler temperature in compliance? • Yes No Cooler/Samples arrived at the laboratory on ice. • Yes No Samples were considered acceptable as cooling process had begun. Water - Sample containers properly preserved Yes No • N/A Water - VOA vials free of headspace Yes No • N/A Trip Blanks received with VOAs Yes No • N/A Soil VOA method 5035 — compliance criteria met Yes No • N/A High concentration container (48 hr) Low concentration EnCore samplers (48 hr) High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? Yes • No Comments: Signature: Makayla Weaver Date & Time: 07/26/2022 11:07:52 Page 8 of 9 C E E E r= � i= z 0 O O 0 N N n N n u < oe= ax2r+ au C a E tt a a 0. v 4g v V p y x m G V L1 _ O O= O O N C 0 p, p O O O f0 2 U p X M U U 2 2 2 2 S S V a _ u F- Q Z z tJ t7 z (D is N 7Ci u u a E ILI E E a ac a cc w Z a > o v In In d E vi E r� iu E E Is � 7u L a ❑❑ d CC Q a iJ O to O O 27 a rni r, wif'-) lv ¢ f� u p �'�1, '«_. y W IJ ' !.� fit. F !T. /r'� �7 'Sy � l� a y !` 1 W W W E may\ a V > > > z z z no m v a a3isodwo(:)) jo gej(91 r13 E. ° Z il am z cc" (Aa)l of ja}aa) xuleyy J o- N c p E c c .. a m s�au�etiuo-i;o iagwnN Q, N z c � O h T \ N C cci 0 m t yi p m N a o A n, o - °' u a V O C p C > V V G C 7 d 'ao u -E w A " � O A rA n �o A > LL ��••e+ `V = 7 N r Z N v S u tu � iu a Page 9 Oi 9 WayPAoint_ NALYTICAL 8/29/2022 Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill, SC, 29732 Ref: Analytical Testing Lab Report Number: 22-229-0190 Client Project Description: Von Drehle Cordoxa, NC Project #2014-110 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Dear Mr. Bob Branch: Waypoint Analytical, LLC. received sample(s) on 8/17/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Jimmy R. Ferguson Assistant Technical Director Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 8 Waypointo ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2023 Arkansas State Program 88-0650 02/07/2023 California State Program 2904 06/30/2023 Florida State Program - NELAP E871157 06/30/2023 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2023 Illinois State Program - NELAP 200078 10/10/2022 Kentucky State Program 80215 06/30/2023 Kentucky State Program KY90047 12/31/2022 Louisiana State Program - NELAP LA037 12/31/2022 Louisiana State Program - NELAP 04015 06/30/2023 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2022 Pennsylvania State Program - NELAP 68-03195 05/31/2023 South Carolina State Program 84002 06/30/2022 Tennessee State Program 02027 02/11/2023 Texas State Program - NELAP T104704180 09/30/2022 Virginia State Program 00106 06/30/2023 Virginia State Program - NELAP 460181 09/14/2022 Page 1 of 1 0000V22-229-0190 Page 2 of 8 (2) 2790 Whitten Road, Memphis, TN 38133 Waypoint. Main 901.213.2400 ° Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 22-229-0190 Client Project Description: Von Drehle Cordoxa, NC Project #2014-110 Lab No Client Sample ID Matrix Date Collected Date Received 89522 VD Solids 08/16/202213:10 08/17/2022 Page 3 of 8 Waypointe ANALYTICAL Client: Branch Residuals and Soils LLC Project: Von Drehle Lab Report Number: 22-229-0190 Date: 8/29/2022 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com CASE NARRATIVE Metals Analysis Method 6010D Sample 58943 (Q3 sludge storage) Analyte: Potassium QC Batch No: 1-633858/1-633386 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 58943 (Q3 sludge storage) Analyte: Phosphorus QC Batch No: 1-633698/1-633386 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 4 of 8 Waypoint ANALYTICAL 22972 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 1 Fax 901.213.2440 www.waypointanalytical.com Branch Residuals and Soils LLC Project Von Drehle Mr. Bob Branch 1735 Heckle Blvd Information : Cordoxa, NC Suite 103-291 Project #2014-110 Rock Hill , SC 29732 Report Number: 22-229-0190 REPORiOFANALYSYS Report Date : 08/29/2022 Received : 08/17/2022 Lab No : 89522 Matrix: Solids Sample ID: VD Sampled: 8/16/2022 13:10 Test Results Units MOL DF Date / Time By Analytical Analyzed Method Neutralizing Value (%CCE) 41.7 % 0.1 1 08/25/22 13:42 DXT AOAC 955.01 Moisture 62.0 % 0.010 1 08/22/22 15:44 FMM 2540G-2011 Ammonia Nitrogen <263 mg/Kg - dry 263 1 08/24/22 11:00 JPJ 4500NH3C-2011 Nitrate (NO3-N) <2.63 mg/Kg - dry 2.63 1 08/18/22 17:17 SPJ 9056A Nitrite (NO2-N) <2.63 mg/Kg - dry 2.63 1 08/18/22 17:17 SPJ 9056A Nitrate+ N itrite-N <2.63 mg/Kg - dry 2.63 1 08/18/22 17:17 9056A Organic N 1239 mg/Kg - dry 873.7 1 08/19/22 12:49 CALCULATION pH 7.5 S.U. 1 08/23/2215:30 ADM 9045D Total Solids 38.0 % 0.010 1 08/22/22 15:44 FMM 2540G-2011 Total Volatile Solids 43.5 % 0.010 1 08/22/22 15:44 FMM 2540G-2011 Total Kjeldahl Nitrogen 1240 mg/Kg - dry 874 1 08/19/22 12:49 ANH 4500NORGD-2011 Phosphorus 139 mg/Kg - dry 13.2 1 08/24/22 12:33 EAL 6010D Aluminum 1920 mg/Kg - dry 13.2 1 08/24/22 12:33 EAL 6010D Arsenic <1.32 mg/Kg - dry 1.32 1 08/23/22 16:53 TJS 6010D Cadmium <0.263 mg/Kg - dry 0.263 1 08/23/22 16:53 TJS 6010D Calcium 188000 mg/Kg - dry 1320 10 08/24/22 12:28 EAL 6010D Copper 28.9 mg/Kg - dry 1.32 1 08/23/22 16:53 TJS 6010D Iron 1080 mg/Kg - dry 26.3 1 08/23/22 16:53 TJS 6010D Lead 1.47 mg/Kg - dry 0.789 1 08/23/22 16:53 TJS 6010D Magnesium 2450 mg/Kg - dry 13.2 1 08/23/22 16:53 TJS 6010D Manganese 40.5 mg/Kg - dry 1.32 1 08/23/22 16:53 TJS 6010D Mercury <0.413 mg/Kg - dry 0.413 1 08/19/22 11:23 TJS 7471A Molybdenum 3.97 mg/Kg - dry 0.657 1 08/23/22 16:53 TJS 6010D Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 5 of 8 s Waypoint. 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 1 Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 22972 Branch Residuals and Soils LLC Project Von Drehle Mr. Bob Branch Report Date : 08/29/2022 1735 Heckle Blvd Information : Cordoxa, NC Received : 08/17/2022 Suite 103-291 Project #2014-110 Rock Hill , SC 29732 Report Number : 22-229-0190 REPORTOPANALYSIS Lab No : 89522 Sample ID: VD Matrix: Solids Sampled: 8/16/2022 13:10 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Nickel 1.46 mg/Kg - dry 0.657 1 08/23/22 16:53 TIS 6010D Potassium 91.8 mg/Kg - dry 26.3 1 08/23/22 16:53 TIS 6010D Selenium <1.32 mg/Kg - dry 1.32 1 08/23/22 16:53 TIS 6010D Sodium 971 mg/Kg - dry 65.8 1 08/23/22 16:53 TIS 6010D Zinc 67.4 mg/Kg - dry 3.29 1 08/23/22 16:53 TIS 6010D Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 6 of 8 (2) Waypoint 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 °Fax 901.21213.2440.24A0 ANALYTICAL www.waypointanalytical.com Shipment Receipt Form Customer Number: 22972 Customer Name: Branch Residuals and Soils LLC Report Number: 22-229-0190 Shipping Method Fed Ex US Postal Lab Other • UPS Client Courier Thermometer ID: r137 Shipping container/cooler uncompromised? ,� Yes No Number of coolers/boxes received F__1 Custody seals intact on shipping container/cooler? Yes No • Not Present Custody seals intact on sample bottles? Yes No 0 Not Present Chain of Custody (COC) present? Yes No COC agrees with sample label(s)? • Yes No COC properly completed • Yes No Samples in proper containers? 6 Yes No Sample containers intact? • Yes No Sufficient sample volume for indicated test(s)? 4 Yes No All samples received within holding time? Yes No Cooler temperature in compliance? Yes No Cooler/Samples arrived at the laboratory on ice. Yes No Samples were considered acceptable as cooling process had begun. Water - Sample containers properly preserved Yes No • N/A Water - VOA vials free of headspace Yes No N/A Trip Blanks received with VOAs Yes No • N/A Soil VOA method 5035 — compliance criteria met Yes No • N/A High concentration container (48 hr) Low concentration EnCore samplers (48 hr) High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? Yes • No Comments: Signature: Hannah R. Brown Date & Time: '08/17/2022 15:57:05 Page 7 of 8 I IIIIII IIIII IIII BIIII CIIII IIIII ? �, 2022 IIII 111111 H11181111111111111111 - 3 o ar8nrt1 15 56 1� rE'- to is q c7 .o Q C N z N O N Z UV° uuxx L a� n? a v CL v v a n rnn x v v E O 41 3 L O o o e o 0 n p p U H ? s > �°,v°xZzxmX dj Y K ( 0 0 ' A O a w O 7 J 2 z n l7 l7 O a = to U. o a o v iIj V C c° u O! E E E s u a c�� z' L A t ` `o u, O Y E E 6+ E E E E a,v a .c O t o. "' N _ f cC Q O • O O 'a a, all C v m O: a • IL C `, c Z 0 2 ILD I --1 m o odwoO) jo gej)E)) v v m (ha)l ol iajaa) xpleW,r N K c c sjau!eluo) jo jagwnN n I 7E n c %A o ? u v a m c o c g L �i 0 0 m A o rn r z m i v c°-0 o , u E a v U a 5 C C v E a` y d E JI •^ o m T q O a ' c ¢ 3 Z - W u �Y.1.. m v m o E m _ _E' n 2 c � p a"i 2 d _ r- � =' •V 3 E .- Z - J m Page 8 of 8 WayPAoint NALYTICAL 9/30/2022 Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill, SC, 29732 Ref: Analytical Testing Lab Report Number: 22-264-0087 Client Project Description: Sludge Testing Von Drehle, Cordova NC Project #2014-110 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Dear Mr. Bob Branch: Waypoint Analytical, LLC. received sample(s) on 9/21/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a'—' symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Iry Randy Thomas Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 8 Waypoint ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2023 Arkansas State Program 88-0650 02/07/2023 California State Program 2904 06/30/2023 Florida State Program - NELAP E871157 06/30/2023 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2023 Illinois State Program - NELAP 200078 10/10/2023 Kentucky State Program 80215 06/30/2023 Kentucky State Program KY90047 12/31/2022 Louisiana State Program - NELAP LA037 12/31/2022 Louisiana State Program - NELAP 04015 06/30/2023 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2022 Pennsylvania State Program - NELAP 68-03195 05/31/2023 South Carolina State Program 84002 06/30/2.022 Tennessee State Program 02027 02/11/2023 Texas State Program - NELAP T104704180 09/30/2022 Virginia State Program 00106 06/30/2023 Virginia State Program - NELAP 460181 09/14/2023 Page 1 of 1 00001/22-264-0087 Page 2 of 8 (2) Waypoint. 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 22-264-0087 Client Project Description: Sludge Testing Von Drehle, Cordova NC Project #2014-110 Lab No Client Sample ID Matrix Date Collected Date Received 86436 VD Solids 09/20/202212:40 09/21/2022 Page 3 of 8 Waypoint'(2) ANALYTICAL Client: Branch Residuals and Soils LLC Project: Sludge Testing Lab Report Number: 22-264-0087 Date: 9/30/2022 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com CASE NARRATIVE Metals Analysis Method 6010D Sample 87284 (Frederick City) Analyte: Calcium QC Batch No: 1-640033/1-639345 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 87284 (Frederick City) Analyte: Iron QC Batch No: 1-639769/1-639345 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 87284 (Frederick City) Analyte: Potassium QC Batch No: 1-639769/1-639345 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 87284 (Frederick City) Analyte: Magnesium QC Batch No: L639769/1-639345 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Anions by Ion Chromatography Method 9056A Sample 86436 (VD) QC Batch No: 1-639836/1-639655 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Page 4 of 8 Waypointo ANALYTICAL 22972 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Branch Residuals and Soils LLC Project Sludge Testing Mr. Bob Branch 1735 Heckle Blvd Information : Von Drehle, Cordova NC Suite 103-291 Project #2014-110 Rock Hill , SC 29732 Report Number: 22-264-0087 REPORT OFANAL YSIS Report Date : 09/30/2022 Received : 09/21/2022 Lab No : 86436 Matrix: Solids Sample ID: VD Sampled: 9/20/2022 12:40 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Neutralizing Value (%CCE) 62.2 % 0.1 1 09/28/22 10:05 DXT AOAC 955.01 Moisture 63.1 % 0.010 1 09/23/22 16:43 FMM 2540G-2011 Ammonia Nitrogen 726 mg/Kg - dry 271 1 09/30/22 12:00 CLP 4500NH3C-2011 Nitrate (NO3-N) <27.1 mg/Kg - dry 27.1 10 09/27/22 03:27 MED 9056A Nitrite (NO2-N) <27.1 mg/Kg - dry 27.1 10 09/27/22 03:27 MED 9056A Nitrate+Nitrite-N <27.1 mg/Kg - dry 27.1 10 09/27/22 03:27 9056A Organic N <967.5 mg/Kg - dry 967.5 1 DH CALCULATION pH 7.2 S.U. 1 09/28/2216:02 SAR 9045D Total Solids 36.9 % 0.010 1 09/23/22 16:43 FMM 2540G-2011 Total Volatile Solids 47.4 % 0.010 1 09/23/22 16:43 FMM 2540G-2011 Total Kjeldahl Nitrogen <967 mg/Kg - dry 967 1 09/22/22 14:45 ANH 4500NORGD-2011 Phosphorus 156 mg/Kg - dry 13.6 1 09/27/22 20:18 EAL 6010D Aluminum 2100 mg/Kg - dry 13.6 1 09/27/22 20:18 EAL 6010D Arsenic <1.36 mg/Kg - dry 1.36 1 09/26/22 22:45 TJS 6010D Cadmium <0.271 mg/Kg - dry 0.271 1 09/26/22 22:45 TJS 6010D Calcium 179000 mg/Kg - dry 1360 10 09/27/22 20:12 EAL 6010D Copper 23.4 mg/Kg - dry 1.36 1 09/26/22 22:45 TJS 6010D Iron 1080 mg/Kg - dry 27.1 1 09/26/22 22:45 TJS 6010D Lead 1.59 mg/Kg - dry 0.813 1 09/26/22 22:45 TJS 6010D Magnesium 2280 mg/Kg - dry 13.6 1 09/26/22 22:45 TJS 6010D Manganese 39.6 mg/Kg - dry 1.36 1 09/27/22 20:18 EAL 6010D Mercury <0.415 mg/Kg - dry 0.415 1 09/23/22 11:17 TJS 7471A Molybdenum 3.41 mg/Kg - dry 0.677 1 09/26/22 22:45 TJS 6010D Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page S of 8 • Waypoint 2790 Whitten Road, Memphis, TN 38133 Main 901.213,2400 0 Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 22972 Branch Residuals and Soils LLC Project Sludge Testing Mr. Bob Branch Report Date : 09/30/2022 1735 Heckle Blvd Information : Von Drehle, Cordova NC Received : 09/21/2022 Suite 103-291 Project *2014-110 Rock Hill , SC 29732 Report Number: 22-264-0087 REPORTOFANALYSIS Lab No : 86436 Sample ID: VD Matrix: Solids Sampled: 9/20/2022 12:40 Test Results Units MOL DF Date / Time By Analytical Analyzed Method Nickel 0.864 mg/Kg - dry 0.677 1 09/26/22 22:45 TJS 6010D Potassium 62.3 mg/Kg - dry 27.1 1 09/26/22 22:45 TJS 6010D Selenium <1.36 mg/Kg - dry 1.36 1 09/26/22 22:45 TJS 6010D Sodium 867 mg/Kg - dry 67.8 1 09/26/22 22:45 TJS 6010D Zinc 99.2 mg/Kg - dry 3.39 1 09/26/22 22:45 EAL 6010D Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 6 of 8 (D 2790 Whitten Road, Memphis, Waypoint Main 901.213.2400 ' Fax 901.21213.2440.2440 ANALYTICAL www.waypointanalytical.com Shipment Receipt Form Customer Number: 22972 Customer Name: Branch Residuals and Soils LLC Report Number: 22-264-0087 Shipping Method Fed Ex US Postal Lab • UPS Client Courier Other Thermometer ID: VTO2 Shipping container/cooler uncompromised? 16 Yes No Number of coolers/boxes received I 1 Custody seals intact on shipping container/cooler? Yes No • Not Present Custody seals intact on sample bottles? _ Yes No • Not Present Chain of Custody (COC) present? ji Yes No COC agrees with sample label(s)? Yes No COC properly completed Yes No Samples in proper containers? (9, Yes No Sample containers intact? i/ Yes No Sufficient sample volume for indicated test(s)? • Yes No All samples received within holding time? 0 Yes No Cooler temperature in compliance? Yes No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes No Water - Sample containers properly preserved Yes No • N/A Water - VOA vials free of headspace Yes No • N/A Trip Blanks received with VOAs Yes No • N/A Soil VOA method 5035 — compliance criteria met Yes No • N/A High concentration container (48 hr) Low concentration EnCore samplers (48 hr) High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? Comments: Yes • No Signature: Makayla Weaver Date & Time: 09/21/2022 11:39:49 Page 7 of 8 0 p T E E E ^' a o P P p c] o l7 C O O Z G 0 ry o o N¢ m E Q r r t si v o O v v - T u Y T ~ u x z z x x x u Y — — ` x I D f0 0 CL W W W 0 z K tt z z 0 _ L LL j O a o � v •o 0-,� c 0 v G a E G E E V u u u m E z d o u � O 4 = 2 N R d C 'U t o n o Cl N A a ) 1- F ❑a C. �{ m c Q C 1;• v c. c d z m d Emom_ � � A cr E it C p Ira ", > U fu as ' z z G i, .1 f r� c cc u L C ai!sodWo'�1 io gei(E)1 Om C ,�\:1 > .. � (AaH of jajaa) zUieyV .o v t �'t S r N t o v n n c c c C m sjauietuo) jo jagwnN ." o ^ O ` n aLG r. c C ° s� O ' ` n J c ai E - , E O .-� •p r •p C 1 C T V a u a n` n a+ a E n O y j �• A J v > N t • > o � z o r. .n E E ' E u m E o ^ = C z Z r L Z WayPAoint NALYTICAL 10/31/2022 Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill, SC, 29732 Ref: Analytical Testing Lab Report Number: 22-292-0219 Client Project Description: Von Dretile Cordova, NC Project #2014-110 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Dear Mr. Bob Branch: Waypoint Analytical, LLC. received sample(s) on 10/19/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a' —'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Connie Cook Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 9 Waypointo ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2023 Arkansas State Program 88-0650 02/07/2023 California State Program 2904 06/30/2023 Florida State Program - NELAP E871157 06/30/2023 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2023 Illinois State Program - NELAP 200078 10/10/2023 Kentucky State Program 80215 06/30/2023 Kentucky State Program KY90047 12/31/2022 Louisiana State Program - NELAP LA037 12/31/2022 Louisiana State Program - NELAP 04015 06/30/2023 Mississippi State Program MS 02/11 /2023 North Carolina State Program 47701 07/31/2023 North Carolina State Program 415 12/31/2022 Pennsylvania State Program - NELAP 68-03195 05/31/2023 South Carolina State Program 84002 06/30/2022 Tennessee State Program 02027 02/11/2023 Texas State Program - NELAP T104704180 09/30/2022 Virginia State Program 00106 06/30/2023 Virginia State Program - NELAP 460181 09/14/2023 Page 1 of 1 00001)22-292-0219 Page 2 of 9 (2) Waypoint. 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 22-292-0219 Client Project Description: Von Dretile Cordova, NC Project #2014-110 Lab No Client Sample ID Matrix Date Collected Date Received 99349 VDI-7 Solids 10/18/202213:30 10/19/2022 Page 3 of 9 Waypoint(z) ANALYTICAL Client: Branch Residuals and Soils LLC Project: Von Dretile Lab Report Number: 22-292-0219 Date: 10/28/2022 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com CASE NARRATIVE Metals Analysis Method 6010D Sample 82178 (KCW-3-2) Analyte: Aluminum QC Batch No: 1-645267/1-644935 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 82178 (KCW-3-2) Analyte: Calcium QC Batch No: 1-645267/1-644935 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Sample 82178 (KCW-3-2) Analyte: Potassium QC Batch No: L645267/1-644935 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 82178 (KCW-3-2) Analyte: Molybdenum QC Batch No: 1-645267/1-644935 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 82178 (KCW-3-2) Analyte: Sodium QC Batch No: 1-645267/1-644935 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 82178 (KCW-3-2) Analyte: Selenium QC Batch No: L645267/1-644935 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 82178 (KCW-3-2) Analyte: Zinc QC Batch No: 1-645267/1-644935 Page 4 of 9 Waypigint(2)ANYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 5 of 9 Waypointo ANALYTICAL 22972 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Branch Residuals and Soils LLC Project Von Dretile Mr. Bob Branch 1735 Heckle Blvd Information : Cordova, NC Suite 103-291 Project #2014-110 Rock Hill , SC 29732 Report Number: 22-292-0219 REPORT OFANAL YSIS Report Date : 10/31/2022 Received : 10/19/2022 Lab No : 99349 Matrix: Solids Sample ID: VDI-7 Sampled: 10/18/2022 13:30 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Neutralizing Value (%CCE) 23.0 % 0.1 1 10/25/22 10:02 DXT AOAC 955.01 Moisture 63.8 % 0.010 1 10/24/2217:20 FMM 254OG-2011 Ammonia Nitrogen <276 mg/Kg - dry 276 1 10/26/22 15:00 JPJ 4500NH3C-2011 Nitrate (NO3-N) <27.6 mg/Kg - dry 27.6 10 10/20/22 19:29 SRJ 9056A Nitrite (NO2-N) <27.6 mg/Kg - dry 27.6 10 10/20/22 19:29 SRI 9056A Nitrate+Nitrite-N <27.6 mg/Kg - dry 27.6 10 10/20/22 19:29 9056A pH 7.8 S.U. 1 10/28/2214:02 SAR 9045D Total Solids 36.2 % 0.010 1 10/24/22 17:20 FMM 2540G-2011 Total Kjeldahl Nitrogen <912 mg/Kg - dry 912 1 10/24/22 16:03 ANH 4500NORGD-2011 Phosphorus 151 mg/Kg - dry 13.8 1 10/25/22 20:48 EAL 6010D Aluminum 2330 mg/Kg - dry 13.8 1 10/25/22 20:48 EAL 6010D Arsenic <1.38 mg/Kg - dry 1.38 1 10/25/22 20:48 EAL 6010D Cadmium <0.276 mg/Kg - dry 0.276 1 10/25/22 20:48 EAL 6010D Calcium 212000 mg/Kg - dry 2760 20 10/26/22 11:37 EAL 6010D Copper 32.3 mg/Kg - dry 1.38 1 10/25/22 20:48 EAL 6010D Lead 2.62 mg/Kg - dry 0.828 1 10/25/22 20:48 EAL 6010D Magnesium 2340 mg/Kg - dry 13.8 1 10/25/22 20:48 EAL 6010D Mercury <0.436 mg/Kg - dry 0.436 1 10/25/22 12:14 TJS 7471A Molybdenum 3.26 mg/Kg - dry 0.690 1 10/25/22 20:48 EAL 6010D Nickel 1.43 mg/Kg - dry 0.690 1 10/25/22 20:48 EAL 6010D Potassium 85.6 mg/Kg - dry 27.6 1 10/25/22 20:48 EAL 6010D Selenium <1.38 mg/Kg - dry 1.38 1 10/25/22 20:48 EAL 6010D Sodium 214 mg/Kg - dry 69.1 1 10/25/22 20:48 EAL 6010D Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 6 of 9 • Waypoint. ANALYTICAL 22972 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Branch Residuals and Soils LLC Project Von Dretile Mr. Bob Branch 1735 Heckle Blvd Information : Cordova, NC Suite 103-291 Project #2014-110 Rock Hill , SC 29732 Report Date : 10/31/2022 Received : 10/19/2022 Report Number: 22-292-0219 REPORrOFANALYSIS Lab No : 99349 Matrix: Solids Sample ID: VDI-7 Sampled: 10/18/2022 13:30 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Zinc Qualifiers/ DF Dilution Factor Definitions 66.9 mg/Kg - dry 3.45 1 10/25/22 20:48 EAL 6010D MQL Method Quantitation Limit Page 7 of 9 WayPAoint NALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Shipment Receipt Form Customer Number: 22972 Customer Name: Branch Residuals and Soils LLC Report Number: 22-292-0219 Shipping Method Fed Ex US Postal Lab Other 0 UPS Client Courier Thermometer ID: 102 Shipping container/cooler uncompromised? 4 Yes No Number of coolers/boxes received r 1 Custody seals intact on shipping container/cooler? Yes No 0 Not Present Custody seals intact on sample bottles? Yes No • Not Present Chain of Custody (COC) present? 46 Yes No COC agrees with sample label(s)? 16 Yes No COC properly completed Yes No Samples in proper containers? Yes No Sample containers intact? 66 Yes No Sufficient sample volume for indicated test(s)? Yes No All samples received within holding time? Yes No Cooler temperature in compliance? 46 Yes No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. • Yes No Water - Sample containers properly preserved Yes No • N/A Water - VOA vials free of headspace Yes No 0 N/A Trip Blanks received with VOAs Yes No 0 N/A Soil VOA method 5035 — compliance criteria met Yes No 46 N/A High concentration container (48 hr) Low concentration EnCore samplers (48 hr) High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? Yes • No Comments: Signature: Makayla Weaver Date & Time: 10/19/2022 16:49:56 Page 8 of 9 c ri F� o` E 4 O o vi p o z � o A G O i I N Z h u Q �' c =vv n C E 0° ro g a n °� a, u v vv v U u C p ,., g C Y be t7 S z S S S to 0 n 3 3 a 4.0 �- r J _ Q 2 Q 2 2 O N O O c r r u a v a cLi5 Ellz E _ + a en—C E v° n �Q O w u a v e L O y4r! a L cc 2❑� ► a 4 u21 G o 0 fi Q u E � oo� c 0AE , �' f 4 7u NN oC4'1 NaO AyYa c C aI a el g n a` apsodwo(7) JO gt1(9i z a a �n N (Aa)i 03 japti) x1i4eW ,11 �C7 a a, � g C snuiewo) }o jagwnry ,n z 1 C °i y � U Z 4 O rs a c O lea t 1 N_ o u 7g o u CL �+ 4 n ` C J Ccc en ~ Vf Y v 4 ► Z 2 o E z' 0 a^ `V E c m ZZ>\\\ 4 cv rage 7 oL 9 waypoint_(2) ANALYTICAL 12/9/2022 Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill, SC, 29732 Ref: Analytical Testing Lab Report Number: 22-326-0028 Client Project Description: Sludge Testing 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Dear Mr. Bob Branch: Waypoint Analytical, LLC. received sample(s) on 11/22/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Connie Cook Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 8 Waypointo ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID E�xiration Date Alabama State Program 40750 02/28/2023 Arkansas State Program 88-0650 02/07/2023 California State Program 2904 06/30/2023 Florida State Program - NELAP E871157 06/30/2023 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2023 Illinois State Program - NELAP 200078 10/10/2023 Kentucky State Program 80215 06/30/2023 Kentucky State Program KY90047 12/31/2022 Louisiana State Program - NELAP LA037 12/31/2022 Louisiana State Program - NELAP 04015 06/30/2023 Mississippi State Program MS 02/11 /2023 North Carolina State Program 47701 07/31/2023 North Carolina State Program 415 12/31/2022 Pennsylvania State Program - NELAP 68-03195 05/31/2023 South Carolina State Program 84002 06/30/2023 Tennessee State Program 02027 02/11/2023 Texas State Program - NELAP T104704180 09/30/2022 Virginia State Program 00106 06/30/2023 Virginia State Program - NELAP 460181 09/14/2023 Page 1 of 1 00001122-326-0028 Page 2 of 8 (0 Waypoint 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 1 Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 22-326-0028 Client Project Description: Sludge Testing Lab No Client Sample ID Matrix Date Collected Date Received 93773 VD Solids 11/21/202212:00 11/22/2022 Page 3 of 8 Waypointo ANALYTICAL Client: Branch Residuals and Soils LLC Project: Sludge Testing Lab Report Number: 22-326-0028 Date: 12/9/2022 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com CASE NARRATIVE Block Digestion and FIA Method 4500NORGD-2011 QC Batch No: L651411/1-650987 The MS/MSD recoveries are outside QC limits due to the level of analyte present in the parent sample relative to the spike level. RPD is based on the MS/MSD results and should be evaluated as laboratory duplicates. Metals Analysis Method 6010D Sample 93946 Analyte: Aluminum QC Batch No: 1-651373/1-651058 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 4 of 8 0 Waypoint ANALYTICAL 22972 Branch Residuals and Soils LLC Project Mr. Bob Branch 1735 Heckle Blvd Information Suite 103-291 Rock Hill , SC 29732 Report Number:22-326-0028 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Sludge Testing REPORT OFANAL YSIS Report Date : 12/09/2022 Received : 11/22/2022 Lab No : 93773 Matrix: Solids Sample ID: VD Sampled: 11/21/2022 12:00 Test Results Units MOL DF Date / Time By Analytical Analyzed Method Neutralizing Value (%CCE) 40.7 % 0.1 1 12/07/22 11:23 DXT AOAC 955.01 Moisture 65.4 % 0.010 1 11/28/2216:33 FMM 254OG-2011 Ammonia Nitrogen 630 mg/Kg - dry 289 1 12/01/22 16:10 JPJ 4500NH3C-2011 Nitrate (NO3-N) <289 mg/Kg - dry 289 100 11/23/22 18:37 SRJ 9056A Nitrite (NO2-N) <28.9 mg/Kg - dry 28.9 10 11/23/22 18:25 SRJ 9056A Nitrate+Nitrite-N <28.9 mg/Kg - dry 28.9 10 11/23/22 18:25 9056A pH 7.4 SM. 1 12/01/2215:03 DRS 9045D Total Solids 34.6 % 0.010 1 11/28/22 16:33 FMM 2540G-2011 Total Kjeldahl Nitrogen 1400 mg/Kg - dry 806 1 12/02/22 10:57 ANH 4500NORGD-2011 Phosphorus 112 mg/Kg - dry 14.5 1 12/01/22 00:55 JTR 6010D Aluminum 2110 mg/Kg - dry 14.5 1 12/01/22 00:55 JTR 6010D Arsenic <1.45 mg/Kg - dry 1.45 1 12/01/22 00:55 JTR 6010D Cadmium <0.289 mg/Kg - dry 0.289 1 12/01/22 00:55 JTR 6010D Calcium 183000 mg/Kg - dry 1450 10 12/01/22 19:12 TJS 6010D Copper 29.5 mg/Kg - dry 1.45 1 12/01/22 00:55 JTR 6010D Lead 3.99 mg/Kg - dry 0.867 1 12/01/22 00:55 JTR 6010D Magnesium 2560 mg/Kg - dry 14.5 1 12/01/22 00:55 JTR 6010D Mercury <0.451 mg/Kg - dry 0.451 1 11/29/22 12:47 FDS 7471A Molybdenum 3.27 mg/Kg - dry 0.722 1 12/01/22 00:55 JTR 6010D Nickel 0.921 mg/Kg - dry 0.722 1 12/01/22 00:55 JTR 6010D Potassium 79.8 mg/Kg - dry 28.9 1 12/01/22 00:55 JTR 6010D Selenium <1.45 mg/Kg - dry 1.45 1 12/01/22 00:55 JTR 6010D Sodium 618 mg/Kg - dry 72.3 1 12/01/22 00:55 JTR 6010D Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page S of 8 Waypointe ANALYTICAL 22972 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Branch Residuals and Soils LLC Project Sludge Testing Mr. Bob Branch 1735 Heckle Blvd Information Suite 103-291 Rock Hill , SC 29732 Report Date : 12/09/2022 Received : 11/22/2022 Report Number : 22-326-0028 REPORT OPANALYSIS Lab No : 93773 Matrix: Solids Sample ID: VD Sampled: 11/21/2022 12:00 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Zinc Qualifiers/ DF Dilution Factor Definitions 90.2 mg/Kg - dry 3.61 1 12/01/22 00:55 JTR 6010D MQL Method Quantitation Limit Page 6 of 8 (2) Waypoint 2790 Whitten Road, Memphis, Main 901.213.2400 0 Fax 901.21213.2440.2440 ANALYTICAL www.waypointanalytical.com Shipment Receipt Form Customer Number: 22972 Customer Name: Branch Residuals and Soils LLC Report Number: 22-326-0028 Shipping Method Fed Ex US Postal Lab Other UPS Client • Courier Thermometer ID: IT1102 Shipping container/cooler uncompromised? i, Yes No Number of coolers/boxes received F 1 Custody seals intact on shipping container/cooler? Yes No • Not Present Custody seals intact on sample bottles? Yes No • Not Present Chain of Custody (COC) present? • Yes No COC agrees with sample label(s)? :# Yes No COC properly completed * Yes No Samples in proper containers? • Yes No Sample containers intact? • Yes No Sufficient sample volume for indicated test(s)? • Yes No All samples received within holding time? • Yes No Cooler temperature in compliance? • Yes No Cooler/Samples arrived at the laboratory on ice. • Yes No Samples were considered acceptable as cooling process had begun. Water - Sample containers properly preserved Yes No • N/A Water - VOA vials free of headspace Yes No • N/A Trip Blanks received with VOAs Yes No • N/A Soil VOA method 5035 — compliance criteria met Yes No • N/A High concentration container (48 hr) Low concentration EnCore samplers (48 hr) High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? Yes • No Comments: Signature: Makayla Weaver Date & Time: 11/22/2022 12:27:53 Page 7 of 8 0 } E E E O a � = o f N d ✓ Y r O O U 0 O O p Z O © N � �., $ ♦♦ Z N t O v Z E r -- t fJt14 r I 1 w 3 > p u S p a s u _ ? .v rj r v S 2 V V Z S S S U - w C K ^O y > Z > > I O LL D 4_ a .G n ❑ p �_ i > _ n - - C z s c v E� E E a d C1 [ N ow•�-' � � M E E� E E L 4 s 'aa a > Q v O 0 0 Q r� N L C LZ J y C p .. y 7t' Li 1 i rI � V, E `U c p N d� C ! to W > W o N u R wi l IL a _< a Z a z cc a n I C7 C7 C9 alisodwo(�) jo gej(g) r E° z v u C (Aa)i of jalaa) xuleW J siauleluo) jo jagwnN W a rcc o I c £ � a N U ti .LU u o o M =� a ° E a a a O u ° ^ o R V •� } LL � N Z ° 6 E 4 o or- =4 — O a r \ 3Od ^ ,v E J N Z � � Page 8 of 8 TOXICITY CHARACTERISTICS LEACHING PROCEDURE (TCLP) ANALYSIS REPORT F"07— q1 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax eM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS inlo(ii;environn1e11talcltemists.conl Branch Residuals/Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill SC 29732 Attention: Bob Branch Date of Report: Feb 09, 2022 Customer PO #: Customer ID: 15060009 Report #: 2022-00648 Project ID: Sludge -von Drehle Lab ID Sample ID: Collect DaterTime Matrix Sampled by 22-01588 Site: Sludge 1/11/2022 11:30 AM Solid/Sludge Bob Branch Test Method Results Date Analyzed Chlordane (TCLP) SW-846 8081 B <0.02 mg/L 01/26/2022 Endrin (TCLP) SW-846 8081 B <0.0005 mg/L 01/26/2022 Heptachlor (TCLP) SW-846 8081 B <0.0005 mg/L 01/26/2022 Heptachlor epoxide (TCLP) SW-846 80816 <0.0005 mg/L 01/26/2022 Lindane (TCLP) SW-846 8081 B <0.0005 mg/L 01/26/2022 Methoxychlor (TCLP) SW-846 8081 B <0.0005 mg/L 01/26/2022 Toxaphene (TCLP) SW-846 8081 B <0.05 mg/L 01/26/2022 2,4,5-TP (TCLP) SW-846 8151 A <0.003 mg/L 01/27/2022 2,4-D (TCLP) SW-846 8151 A <0.003 mg/L 01/27/2022 1,4-Dichlorobenzene (TCLP) SW-846 8270 E <0.050 mg/L 01/28/2022 2,4,5-Trichlorophenol (TCLP) SW-846 8270 E <0.050 mg/L 01/28/2022 2,4,6-Trichlorophenol (TCLP) SW-846 8270 E <0.050 mg/L 01/28/2022 2,4-Dinitrotoluene (TCLP) SW-845 8270 E <0.050 mg/L 01/28/2022 Cresol (TCLP) SW-846 8270 E <0.050 mg/L 01/28/2022 Hexachloro-1,3-butadiene (TCLP) SW-846 8270 E <0.050 mg/L 01/28/2022 Hexachlorobenzene (TCLP) SW-846 8270 E <0.050 mg/L 01/28/2022 Hexachloroethane (TCLP) SW-846 8270 E <0.050 mg/L 01/28/2022 m + p-Cresol (TCLP) SW-846 8270 E <0.050 mg/L 01/28/2022 Nitrobenzene (TCLP) SW-846 8270 E <0.050 mg/L 01/28/2022 o-Cresol (TCLP) SW-846 8270 E <0.050 mg/L 01/28/2022 Pentachlorophenol (TCLP) SW-846 8270 E <0.050 mg/L 01/28/2022 Pyridine (TCLP) SW-846 8270 E <0.050 mg/L 01/28/2022 1,1-Dichloroethylene (TCLP) SW-846 Method 8260D <0.01 mg/L 01/19/2022 1,2-Dichloroethane (TCLP) SW-846 Method 8260D <0.01 mg/L 01/19/2022 Benzene (TCLP) SW-846 Method 8260D <0.01 mg/L 01/19/2022 Carbon Tetrachloride (TCLP) SW-846 Method 82600 <0.01 mg/L 01/19/2022 Report # 2022-00648 Page 1 of 2 41 Environmental Chemists, Inc. envirochem6602 Windmill I-Vay, Wilmu-igton, NC 28405 a 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Nlanteo, NC 27954 • 252.473.5702 Lab/Fax —.011111111 sM 255-A Wilrnington Highway Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infoCe.Penvironmentalc6emists.com Branch Residuals/Bob Branch Date of Report: Feb 09, 2022 1735 Heckle Blvd Suite 103-291 Customer PO #: Rock Hill SC 29732 Customer ID: 15060009 Attention: Bob Branch Report #: 2022-00648 Project ID: Sludge -von Drehle Chlorobenzene (TCLP) SW-846 Method 8260D <0.01 mg/L 01/19/2022 Chloroform (TCLP) SW-846 Method 8260D <0.01 mg/L 01/19/2022 Methyl ethyl ketone (TCLP) SW-846 Method 8260D <0.05 mg/L 01/19/2022 Tetrachloroethylene (TCLP) SW-846 Method 82600 <0.01 mg/L 01/19/2022 Trichloroethylene (TCLP) SW-846 Method 6260D <0.01 mg/L 01/19/2022 Vinyl Chloride (TCLP) SW-846 Method 8260D <0.01 mg/L 01/19/2022 RCI Ignitability EPA 1030 <0.8 mm/sec 01/17/2022 Cyanide SM 4500 CN D 1.36 mg/kg 01/20/2022 Sulfide SM 4500 S D 0.56 mg/kg 01/21/2022 pH SW 846 Method 9045D 7.87 units 01/24/2022 Result estimated. Analyzed out of 15 minutes hold time. TCLP Metals Arsenic EPA 200.7, Rev. 4.4,1994 <1.0 mg/L 01/26/2022 Barium EPA 200.7, Rev. 4.4,1994 <1.0 mg/L 01/26/2022 Cadmium EPA 200.7, Rev. 4.4, 1994 <1.0 mg/L 01/26/2022 Chromium EPA 200.7, Rev. 4.4,1994 <1.0 mg/L 01/26/2022 Lead EPA 200.7, Rev. 4.4, 1994 <1.0 mg/L 01/26/2022 Selenium EPA 200.7. Rev. 4A,1994 <1.0 mg/L 01/26/2022 Silver EPA 200.7, Rev. 4.4, 1094 <1.0 mg/L 01/26/2022 Mercury EPA 245.1 <0.0002 mg/L 01 /28/2022 Comment: Reviewed by: %lani Report #:: 2022-00648 Page 2 of 2 Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmington, NC 28405 910.392.0223 Sample Receipt Checklist Client: C (-E Yam! �U i� Date: 111 Ias Report Number.Qa ~ C)O 4 4 8 Receipt of sample: ECHEM Pickup 14 Client Delivery ❑ UPS ❑ Fed Ex ❑ Other ❑ ❑ YES ❑ NO N/A 1. Were custody seals present on the cooler? ❑ YES 10 NO N/A 2. If custody seals were present, were they intact/unbroken? Original temperature upon receipt °C Corrected temperature upon receipt oC How temperature taken: ❑ Temperature Blank V Against Bottles IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0 ❑ YES ❑ NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified? YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed? YES ❑ NO 5. Were sample ID's listed on the COU YES ❑ NO 6. Were samples ID's listed on sample containers? $1 YES ❑ NO 7. Were collection date and time listed on the COU YES ❑ NO 8. Were tests to be performed listed on the COU YES ❑ NO 9. Did samples arrive in proper containers for each test? YES ❑ NO 10. Did samples arrive in good condition for each test? YES ❑ NO 11. Was adequate sample volume available?' YES ❑ NO 12. Were samples received within proper holding time for requested tests? ❑ YES 10 NO 13. Were acid preserved samples received at a pH of <2? ❑ YES I0 NO 14. Were cyanide samples received at a pH >12? ❑ YES 10 NO 15. Were sulfide samples received at a pH >9? ❑ YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ** ❑ YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? ❑ YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H2SO4 HNO3 HCI NaOH Time of preservation: If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. Who was notified, date and time: Volatiles Sample(s) were received with headspace COMMENTS: DOC. QA.002 Rev 1 Ln CD a CD HN Z O C O t! O r in O! Q1 N E LL d M t u N tE O m o Om' E c c o C C W to V N CD O U. C to O ._ w W W" to 0 Z Z° a W W G O c.i LL O z V Z Q Z 0 U LU J J V r u w � W T (i ttl � � O w - z a 7 � I t2 w D H3HIO 1 a m Z OIHI 0 > Q HOVN V 41 CONH w LLu VOSZH d,OH 3NON x j I m3ewnN al evi E J 'lr6w m auPol43 G 42 (9 JO d) a a. (7 a a a a C7 Jouletuoc) I I 4ejJ Jo U�U(�U(9UC90000000000 allsodwo0 adh aidwag a m E d 40 H rr O c V N 4)• N to 0 i O � o � � � C w J 4) y a A e. E to I I PATHOGEN AND VECTOR ATTRACTION REDUCTION FORMS PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION The current permit, WQ0039924, does not have vector attraction requirements but does have Class A requirements for pathogens. These forms are marked to reflect these requirements. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) FacilityName: Marcal Cordova, LLC ( Formerly von Drehle Corp.) WQ Permit Number: WQ0039924 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 1/1/2022 To 1/31/2022 Pathoeen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/tent) ❑ r Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) L-J Alt.D (No Prior Test) O Process to Further Reduce Pathogens L.l If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment❑ Thermo hilic❑ Beta Ray ❑ Gainma Ray ❑ Pasteurization ❑ (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ Class B: jAlt. If applicable to alternative pefformed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ composting ❑ Aerobic Digestion 1 Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Numoer or Excee- Frequency of Analysis Sample Type na ica Tech- MinimumGeo. Mean MaximumUnits Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry wet ht Salmonella bacteria (in lieu of'fecal coliform) 3 MPN per 4 grams total solid (dry weight <_ 0.6 NA < 0.7 rams 0 Monthly Grab E682 Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.l (VS reduction) E�1 Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. O- uptake) El Alt. 5 (14-Day Aerobic) (7 Alt. 6 (Alk. Stabilization❑ Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) ❑ T. 9 (Injection) L.1 Alt. 10 (Incorporation) Ll No vector attraction reduction alternatives were performed El CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Mitchell Luckie, Systems En ineer ORC Preparer Name and Title (type or print) Signature of Preparer* Mr. Robert Branch Land Application ORC Land lier and Title (if applicable)(type or print) 2/23/23 2 23 Z 3 Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Marcal Cordova, LLC ( Formerly von Drehle Corp.) WQ Permit Number: WQ0039924 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 2/l/2022 To 2/28 2022 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/tetu) ❑ I Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) Alt.D (No Prior Test) ❑ Process to Further Reduce Patlto ens ❑21 If applicable to alternative performed (Class A only) indicate "I'mcess to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment❑ Thermo hilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: JAlt. (1) Fecal Density 01 Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ composting ❑ JAerobic Digestion lJ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in in Sludge Pathogen Density Numner or Excee- Frequency of Analysis y Sample Type Analytical Tech - nimip Minimum Geo. Mean aximu UnitsenrPIZ Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) MPN/ 4 Grams 0 Monthly Grab EPA 1682 Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry wei ht) _< 0.7 NA 1.3' Vector Attraction Reduction (I k NCAC 02T .1107) -Please indicate alternative performed: Alt.1 (VS reduction) F] Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ JAlt. 4 (Spec. OZ uptake) Alt. 5 (14-Day Aerobic) 1 1 Alt. 6 (Alk. Stabilization❑ Alt 7 (Drying - Stable) ❑ JAlt. 8 (Drying - Unstable) Alt. 9 (Injection) L 1 Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Mitchell Luckie, S stems En ineer ORC Mr. Robert Branch Land Application ORC_ _ Preparer Name and Title (type or print) Lan.d,ftplier a and Title (if applicable)(type or print) 2/23/23 Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Marcal Cordova, LLC ( Formerly von Drehle Corp.) WQ Permit Number: WQ0039924 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 3/l/2022 To 3/31/2022 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/tens) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testin) El A1t.D (No Prior Test) El to Further Reduce Pathens El If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment❑ Tliermo hilici I Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: JAlt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens CJ ........... If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Coinposting ❑ JAerobic Digestion ❑ Anaerobic Digestion El............ .............. If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge g Pathogen Density Number of Excee- Frequency of Analysis Y Sample Type Analytical Tech_ nioue Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry wei ht < 0.7 NA < 0.7 MPN/ 4 Grams I 0 Monthly I Grab I EPA 1 1682 Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. O, uptake) I I Alt. 5 (14-Day Aerobic) U Alt. 6 (Alk. Stabilization[] Alt 7 (Drying - Stable) ❑ JAIL. 8 (Drying - Unstable) Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." Li "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Mitchell Luckie, Systems Engineer ORC Mr. Robert Branch Land Application ORC Preparer Name and Title (type or print) L:O, ier a and Title (if applicable)(type or print) 2/23/23 Z %"L10 Signature of Preparer* Date §ignature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Marcal Cordova, LLC ( Formerly von Drehle Corp.) WQ Permit Number: WQ0039924 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 4/l/2022 To 4 30 2022 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (timehem) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) E A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogens LJ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 01 Heat Drying ❑ Heat Treatment❑ Thermo hilic❑ Beta Ray 01 Gamma Ray Ll Pasteurization ❑ —4— Class B: jAlt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Cl Air Drying ❑ composting ❑ jAerobic Digestion 1 Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Numner of Excee- nninof Frequency Analysis Sample Type na Ica Tech - Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Grab Salmonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry weight) < 0.6 NA < 0.6 4 GPams 0 Monthly 16N/ 82 Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ jAlt.4 (Spec. Oz uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization❑ Alt 7 (Drying- Stable) ❑ 1 Alt. 8 (Drying -Unstable) Ll Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed LD CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Mitchell Luckie, Systems Engineer ORC Preparer Name and Title (type or print) Signature of Preparer* Mr. Robert Branch Land Application ORC Land lie an e and Title (if applicable)(type or print) 2/23/23 �2 23 Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) bFENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Marcal Cordova, LLC ( Formerly von Drehle Corp.) WQ Permit Number: WQ0039924 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 5/l/2022 To 513l/2022 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/tent) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) El :. A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogens ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatmentg= Thermo hilic❑ Beta Ray ❑ Gatnma RN ❑ Pasteurization ❑ Class B: JAR. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ composting ❑ jAerobic Digestion[ I Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density um er of Excee- Frequency of Analysis Sample Type Analytical Tech - MinimumGeo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) <_ 0.6 NA < b.8 Grants 0 Monthly Grab E682 Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: t.1 (VS reduction) ❑ Alt. 2 (40-day bench) El Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. O, uptake) n t. 5 (14-Day Aerobic) ❑ LA Alt. 6 (Alk. Stabilization[] Alt 7 (Drying - Stable) El Alt. 8 (Drying - Unstable) , 1 . 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed Imo] CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Mitchell Luckie, Systems Engineer ORC Preparer Name and Title (type or print) Signature of Preparer* Mr. Robert Branch Land Application ORC Land �era and Title (if applicable)(type or print) 2/23/23 21319 Date ignature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Marcal Cordova, LLC ( Formerly von Drehle Corp.) WQ Permit Number: WQ0039924 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 6/1/2022 To 6'30'2022 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (tine/tein) ❑ Alt B (Al k Treatment) ❑ Alt. C (Prior Testing) El Mt.D (No Prior Test) ❑ Process to Further Reduce Pathogens ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment❑ Thermo hilic❑ Beta Ray ❑ Gamma Ra ❑ Pasteurization ❑ Class B: jAlt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": . • Lime Stabilization ❑ Air Drying ❑ comeosting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Numoer or Excee- Frequency of Analysis Sample Type Analytical Tech- inimu Geo. Mean axim Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry wei ht < 0.6 NA <- 0.8 ' MPN/ 4 Grams 0 I Monthly Grab • EPA 1682 Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) L Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ jAlt. 4 (Spec. OZ uptake) Alt. 5 (14-Day Aerobic) Ci Alt. 6 (Alk. Stabilization❑ Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC_ 02T .1107 have been met." _ ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Mitchell Luckie, Systems Engineer ORC Mr. Robert Branch Land Application ORC Preparer Name and Title (type or print) Land lier a and Title (if applicable)(type or print) �r 2/23/23 Z123 2 3 Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Marcal Cordova, LLC ( Formerly von Drehle Corp.) WQ Permit Number: WQ0039924 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 7/l/2022 To 7 31/2022 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/tern) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) t] Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogens ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment❑ Thermo hilic❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: jAlt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in in Sludge Pathogen Density Numner orl Excee- Frequency of Analysis Y Sample Type Analytical Tech - ninne Minimum Geo. Mean aximu Unitspnrpc Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry wei ht < 0.7 NA < 1.0 GPaii/is 0 Monthly Grab E682 Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. O, uptake) [7 Alt. 5 (14-Day Aerobic) (-1 Alt. 6 (Alk. Stabilization[] Alt 7 (Drying -Stable) ❑ Alt. 8 (Drying -Unstable) CI Alt. 9 (Injection) C7 Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed Cl CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Mitchell Luckie, Systems Engineer ORC Preparer Name and Title (type or print) Signature of Preparer* 2/23/23 Date Mr. Robert Branch Land Application ORC Land ier N e and Title (if applicable)(type or print) f 4/Z,?/2 Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Marcal Cordova, LLC ( Formerly von Drehle Corp.) WQ Permit Number: WQ0039924 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 8/l/2022 To 8/31/2022 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/tern) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testin) El Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogens ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment[]Thermo hilic❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density ❑ 1 Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Coniposting ❑ jAerobic Digestion U Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number, of Excee- Frequency of Analysis Sample Type Analytical Tech - ninue Minimum Geo. Mean Maximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry wei ht <_ 0.6 NA < 0.7 MPN/ 4 Grams 0 Monthly ' Grab EPA 1682 Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ IAIL 4 (Spec. O, uptake) ❑ Alt. 5 (14-Day Aerobic) i 1 Alt. 6 (Alk. Stabilization❑ Alt 7 (Drying- Stable) ❑ 1 Alt. 8 (Drying -Unstable) ❑ Alt. 9 (Injection) 7 Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed U CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr.Mitchell Luckie, Systems Engineer ORC Preparer Name and Title (type or print) Signature of Preparer* Mr. Robert Branch Land Application ORC Land lier a and Title (if applicable)(type or print) 2/23/23 ;4423 Date fignature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Marcal Cordova, LLC ( Formerly von Drehle Corp.) WQ Permit Number: WQ0039924 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 9/l/2022 To 9130'2022 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/tem) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) 0 A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogens ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Com ost ❑ Heat Drying ❑ Heat Treatment❑ Thermo hilic❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: JAlt. (1) Fecal Density 01 Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Com osting ❑ Aerobic Digestion L] Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density NumDer or denrprExcee- Frequency of Analysis Sample Type AnMyUc7a Tech- ni tip MinimumGeo. Mean MaximumUnits Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry wei ht < 0.7 NA <_ 0.8 /S 0 Monthly Grab E6g2 Vector Attraction Reduction (15 k NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) 1.I Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ JAlt. 4 (Spec. Oz uptake) f 7 Alt. 5 (14-Day Aerobic) Cl Alt. 6 (Alk. Stabilization❑ Alt 7 (Drying - Stable) ❑ JAR. 8 (Drying - Unstable) 0 Alt. 9 (Injection) I Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were erformed CJ CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." LJ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr.Mitchell Luckie, Systems Engineer ORC Preparer Name and Title (type or print) Signature of Preparer* Mr. Robert Branch Land Annlication ORC Land Tier N e Title (if applicable)(type or print) ,f 2/23/23 Wis�2 3 Date ignature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) FacilityName: Marcal Cordova, LLC ( Formerly von Drehle Corp.) WQ Permit Number: WQ0039924 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 10/1/2022 To 10/31/2022 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/tern) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) 1] A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogens ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Corn ost ❑ Heat Drying ❑ Heat Treatment❑ Thermo hilic[J Beta Ray ❑ 11 Gamma Ra ❑ Pasteurization ❑ Class B: ]Alt. _(I) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Patho ens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ jAerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the followin monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number or Excee- Frequency f Al i Sample Type Ana ytical Tech- nintip. Minimum Geo. Me Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN — CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry weight) < 0.6 NA < 0.7 MPN/ 4 Grams 0 Monthly Grab EPA 1682 Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. O, uptake) [ 7 Alt. 5 (14-Day Aerobic) rl Alt. 6 (Alk. Stabilization❑ Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) [ 1 Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed P1 CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the - Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Marcal Cordova, LLC ( Formerly von Drehle Corp.) WQ Permit Number: WQ0039924 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From l l/l/2022 To 11/30 2022 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/tent) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) El AIt.D (No Prior Test) ❑ Process to Further Reduce Pathogens ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Path ens": Compost 0 Heat Dryina ❑ Heat Treatment❑ Thermo hilicLl Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: JAlt. (1) Fecal Density 01 Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": . Lime Stabilization ❑ Air Drying ❑ Composting ❑ JAerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge g Pathogen Density Number of Excee- ennp.rof Frequency Analysis Y Sample Type Ana ytical Tech- ninue Minimum Geo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal 1coliform 3 MPN per 4 grams total solid (dry weight) <_ 0.6 NA < 0.'7 NQN/ 4 Grams 0 Monthly 1 Grab 1 1 EPA 1682 Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. O, uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization❑ Alt 7 (Drying - Stable) ❑ JAlt. 8 (Drying - Unstable) IJ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed Cl CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr.Mitchell Luckie, Systems Engineer ORC Preparer Name and Title (type or print) .- Signature of Preparer* Mr. Robert Branch Land Application ORC Land tier ne d Title (if applicable)(type or print) 2/23/23 2 2y/j.e Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Marcal Cordova, LLC ( Formerly von Drehle Corp.) WQ Permit Number: WQ0039924 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 12/1/2022 To 12/31/2022 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (tinie/tem) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) El Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogens ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment❑ Thermo hilic❑ Beta Ray ❑ Gamma Rav ❑ Pasteurization ❑ Class B: JAR. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Com ostin ❑ jAerobic Digestion[ l Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in in Sludge Pathogen Density Number of Excee- Frequency of Analysis Y Sample Type Wn—alytical Tech - ninm- Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry weight) < 0.7 NA 6.8 GPams 0 Monthly Grab PA E682 Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) D Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ jAlt. 4 (Spec. O, uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization❑ Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ' ' Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed Imo' CERTIFICATION STATEMENT (please check the appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the made under my ance designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr.Mitchell Luckie, Systems Engineer ORC Mr. Robert Branch Land Application ORC Preparer Name and Title (type or print) Land ier e d Title (if applicable)(type or print) 2/23/23 Signature of Preparer* Date 5ignature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) PATHOGEN AND VECTOR ATTRACTION REDUCTION DOCUMENTATION PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION DOCUMENTATION The current permit, WQ0039924, does not have vector attraction requirements but does have Class A requirements for pathogens. Documentation is attached to reflect these requirements. Marcal Cordova, LLC (Formerly von Drehle Corporation) Cordova, NC City of Rockingham IUP 0015 Jan-22 Biological Consulting Services h .......... 40 .......... UO ................ ................... ......................... . ... ..... V W o"O"'w ........ ...... . ............... ...... .................. ........ ........................ ......... ....... Ter... ... ....... ............. ::p F MrN r 2112238 12/28/21 < 0.07 :S 0.7 2112239 12/28/21 < 0.07 :s 0.7 2112240 12/28/21 < 0.07 < 0.7 2112241 12/28/21 :5 0.07 0.7 2112242 12/28/21 :S 0.07 < 0.7 2112243 12/28/21 < 0.07 0.7 244 12/28/21 < 0.07 < 0.6 Exceedances . ................. All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Monthly Pathogen and Vector Attraction Reduction Forms for Class A option. inc. BIOLOGICAL CONSULTING SERVICES OF NORTH FLORIDA, INC. December 28, 2021 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd. Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD1, VD2, VD3, VD4, VD5, VD6, VD7 BCS ID: 2112238, 2112239, 2112240, 2112241, 2112242, 2112243, 2112244 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Von Drehle Analysis Method Salmonella EPA 1682; BCS SOP MA (IS017025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, ?1 f I ltUL �- Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 2112238, 2112239, 2112240, 2112241, 2112242, 2112243, 2112244 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, A7-DHS:A7-0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES etaac..=.mram_ AM �' - � •' A<G AICCi i C tf Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD1 Sample Date/Time: December 21, 2021 13:21 BCS Sample ID: 2112238 Sample Description: Biosolid Date Received: December 22, 2021 11:35 Amount Submitted:100 mL BCS Bottle % Solids: 39.2 Amount Analyzed: 30.04 g Receipt Temperature: 1.1 deg C Preserved: Yes Analysis Start: December 22, 2021 12:30 Analysis Stop Date: December 28, 2021 10:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD2 Sample Date/Time: December 21, 2021 13:24 BCS Sample ID: 2112239 Sample Description: Biosolid Date Received: December 22, 2021 11:35 Amount Submitted:100 mL BCS Bottle % Solids: 39.7 Amount Analyzed: 30.10 g Receipt Temperature: 1.1 deg C Preserved: Yes Analysis Start: December 22, 2021 12:30 Analysis Stop Date: December 28, 2021 10:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 2112238, 2112239, 2112240, 2112241, 2112242, 2112243, 2112244 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD3 Sample Date/Time: December 21, 2021 13:18 BCS Sample ID: 2112240 Sample Description: Biosolid Date Received: December 22, 2021 11:35 Amount Submitted:100 mL BCS Bottle % Solids: 35.4 Amount Analyzed: 30.07 g Receipt Temperature: 1.1 deg C Preserved: Yes Analysis Start: December 22, 2021 12:30 Analysis Stop Date: December 28, 2021 10:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD4 Sample Date/Time: December 21, 2021 13:15 BCS Sample ID: 2112241 Sample Description: Biosolid Date Received: December 22, 2021 11:35 Amount Submitted:100 mL BCS Bottle % Solids: 38.8 Amount Analyzed: 29.93 g Receipt Temperature: 1.1 deg C Preserved: Yes Analysis Start: December 22, 2021 12:30 Analysis Stop Date: December 28, 2021 10:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2112238, 2112239, 2112240, 2112241, 2112242, 2112243, 2112244 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, A7-DHS:A7-0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL,, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES J%c s p11�j4B "'—~"' nc crrcor�cu Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD5 Sample Date/Time: December 21, 2021 13:27 BCS Sample ID: 2112242 Sample Description: Biosolid Date Received: December 22, 2021 11:35 Amount Submitted:100 mL BCS Bottle % Solids: 39.6 Amount Analyzed: 29.92 g Receipt Temperature: 1.1 deg C Preserved: Yes Analysis Start: December 22, 2021 12:30 Analysis Stop Date: December 28, 2021 10:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD6 Sample Date/Time: December 21, 2021 13:30 BCS Sample ID: 2112243 Sample Description: Biosolid Date Received: December 22, 2021 11:35 Amount Submitted:100 mL BCS Bottle % Solids: 39.5 Amount Analyzed: 29.96 g Receipt Temperature: 1.1 deg C Preserved: Yes Analysis Start: December 22, 2021 12:30 Analysis Stop Date: December 28, 2021 10:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 150.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2112238, 2112239, 2112240, 2112241, 2112242, 2112243, 2112244 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW. MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD7 Sample Date/Time: December 21, 2021 13:33 BCS Sample ID: 2112244 Sample Description: Biosolid Date Received: December 22, 2021 11:35 Amount Submitted:100 mL BCS Bottle % Solids: 40.8 Amount Analyzed: 29.96 g Receipt Temperature: 1.1 deg C Preserved: Yes Analysis Start: December 22, 2021 12:30 Analysis Stop Date: December 28, 2021 10:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 150.07 Salmonella MPN/mL sample analyzed Secondary Value: 0.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2112238, 2112239, 2112240, 2112241, 2112242, 2112243, 2112244 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924. ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Project: Von Drehle Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2112238, 2112239, 2112240, 2112241, 2112242, 2112243, 2112244 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES AII&B r 'i^ 1 wccncnr4cv I certify that I have examined and I am familiar with the information submitted herein. The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. Date: December 28, 2021 Page 7 of 8 Final Report BCS ID 2112238, 2112239, 2112240, 2112241, 2112242, 2112243, 2112244 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 1-2422, PADEP: 68-03950, AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES r•J. •.,1::`�` tlitx.,•lcacai'or: eQli� DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set (1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit & the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist forthe component. 13 The data are questionable because of improper laboratory or field protocols. L Off scale high. Actual value is known to be greater than value given. N Presumptive evidence forthe presence of material. There is an indication that the analyte is present, but the confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. L1 Indicates that the compound was analyzed for but not detected. The specified component was not detected. The reported value is the method detection limit. V Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that can be determined based on the volume. 7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client. Sterility can not be confirmed by BCS. # BCS Lab specific qualifier. See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2112238, 2112239, 2112240, 2112241, 2112242, 2112243, 2112244 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:A7-0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES v RP AAM a z Q C M) to L' I� M CJ _ O m (G X r• 3 4) .O ` M LL c j N J lL ti 0 U t4 'C N rn °i d y 0 .N (6 •r Y J Z d! N cn U M i Cj Y m d (D {- v G 0 G - G w o w u (sailddb aa3) lyl HSn21 _Q 9 to n USPOI •N g CM N N sisal NOdb-iU 9691 Hd3 N •p �- N PION Pue lsea,k H cn 0 N N Ix c M XX301 seuowopnesd m 7 N N N 7 Q N N ` GNo :o N C. N a XX301 sn0000aalu3 XX301 eliauol6a-1 N � N C ? PoUlaw 000 ellauol6a, L C m m (0dH) eualoeg luno0 aleid !loo '3 wJobll00 leloi )PIOC, dds ellemwleg ,� .x �C oc •(- �f enO ylulwlaH wjollloo leoa3 eipjeiJ V wnlpuodsoldfuO (`� d Q c sniin oualu3 algejnlin0 ry LLL — .1411oadsl O v w ti 0 CD Q T U) lL c.i Q u_ O la a E N = U � U CO U w .9 *k O 0 ML .a O .D U J E T- 0 3 U- rr, x Ls ialeM 6u14uuo JelemalseM jalem aoepn! pappe alelinsol4l wnipol p uopalloo le ainlejadwe C �1 n N z x U. r� [ u011391103 le . . ■■■■■■■ • . . ■...... ®Mmmmm®m■■ MM-- MOM 7 ^I , n, cn IA (n CL N �: QD rn i� ram. CD C m c y L E a Q N d E 0 C f0 �' U o Z d C N d E V L -C a `m E C n 44 z C. a F- E m U m N- kn N N c to cl '> > N m y N N U r i:4 u c m Li c a E E O U 0 Lo .n c� _ N W � paidweg awii N ti tYi 3 o No p ) N N N N i4 N � N paldweg oleo N m N w y N U C O Ce•�f, N d •U � M N d N L T In fn m U ;IQZ z 1 N U }b1J; C � Y O m o c a m E a >� y O O W Ud >% c01, cmi E C. 'a4) m f- N w 0 G L)a`a`_° E ECO P P O �V L O t E_ E_ 2 N m Of Marcal Cordova, LLC (Formerly von Drehle Corporation) Cordova, NC City of Rockingham IUP 0015 Feb-22 Biological Consulting Services .................................. -D ...... on Y:: ....... 2202011 2/5/22 < 0.07 :50.7 2202012 2/5/22 0.13 1.3 2202013 2/5/22 < 0.07 :5 0.7 2202014 2/5/22 :5 0.07 :s 0.7 2202015 2/5/22 < 0.07 :S 0.7 2202016 2/5/22 < 0.07 :s 0.7 2202017 2/5/22 :S 0.07 < 0.7 . . . . . . . . . . . . . . . . . . .. .......... .... Exceedances All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Monthly Pathogen and Vector Attraction Reduction Forms for Class A option. inc- BIOLOGICAL CONSULTING SERVICES OF NORTH FLORIDA, INC. February 09, 2022 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd. Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD1, VD2, VD3, VD4, VD5, VD6, VD7 BCS ID: 2202011, 2202012, 2202013, 2202014, 2202015, 2202016, 2202017 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Von Drehle Cordova NC Analysis Method Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 2202011, 2202012, 2202013, 2202014, 2202015, 2202016, 2202017 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW. MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 1-2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES I tla`A4B .......... Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD1 BCS Sample ID: 2202011 Date Received: February 02, 2022 9:38 Sample Date/Time: February 01, 2022 13:55 Sample Description: Biosolid Amount Submitted:100 mL bottle % Solids: 37.9 Amount Analyzed: 30.04 g Receipt Temperature: 5.3 deg C Preserved: Yes Analysis Start: February 02, 2022 10:55 Analysis Stop Date: February 05, 2022 10:00 Analyst: Kristin Baecher, M.S. Qualifier: U Primary Value: 150.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD2 Sample Date/Time: February 01, 2022 13:57 BCS Sample ID: 2202012 Sample Description: Biosolid Date Received: February 02, 2022 9:38 Amount Submitted:100 mL bottle % Solids: 40.6 Amount Analyzed: 30.06 g Receipt Temperature: 5.3 deg C Preserved: Yes Analysis Start: February 02, 2022 10:55 Analysis Stop Date: February 09, 2022 12:50 Analyst: Kristin Baecher, M.S. Qualifier: NONE Primary Value: 0.13 Salmonella MPN/mL sample analyzed Secondary Value: 1.3 Salmonella MPN/4 dry grams Analysis Notes: None Page 2 of 8 Final Report BCS ID 2202011, 2202012, 2202013, 2202014, 2202015, 2202016, 2202017 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES _t1�-MRAAA= � Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD3 Sample Date/Time: February 01, 2022 13:59 BCS Sample ID: 2202013 Sample Description: Biosolid Date Received: February 02, 2022 9:38 Amount Submitted:100 mL bottle % Solids: 40.0 Amount Analyzed: 30.01 g Receipt Temperature: 5.3 deg C Preserved: Yes Analysis Start: February 02, 2022 10:55 Analysis Stop Date: February 05, 2022 10:00 Analyst: Kristin Baecher, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD4 Sample Date/Time: February 01, 2022 14:02 BCS Sample ID: 2202014 Sample Description: Biosolid Date Received: February 02, 2022 9:38 Amount Submitted:100 mL bottle % Solids: 39.0 Amount Analyzed: 30.10 g Receipt Temperature: 5.3 deg C Preserved: Yes Analysis Start: February 02, 2022 10:55 Analysis Stop Date: February 05, 2022 10:00 Analyst: Kristin Baecher, M.S. Qualifier: U Primary Value: 150.07 Salmonella MPN/mL sample analyzed Secondary Value: 0.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2202011, 2202012, 2202013, 2202014, 2202015, 2202016, 2202017 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT SE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES AP&B •�/1 `` ,,<:,,:tom ` •t,�„t:d.t' era.u.cGwvurw+ ' .B. . Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD5 Sample Date/Time: February 01, 2022 14:04 BCS Sample ID: 2202015 Sample Description: Biosolid Date Received: February 02, 2022 9:38 Amount Submitted:100 mL bottle % Solids: 39.9 Amount Analyzed: 29.91 g Receipt Temperature: 5.3 deg C Preserved: Yes Analysis Start: February 02, 2022 10:55 Analysis Stop Date: February 05, 2022 10:00 Analyst: Kristin Baecher, M.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD6 Sample Date/Time: February 01, 2022 14:06 BCS Sample ID: 2202016 Sample Description: Biosolid Date Received: February 02, 2022 9:38 Amount Submitted:100 mL bottle % Solids: 39.6 Amount Analyzed: 30.10 g Receipt Temperature: 5.3 deg C Preserved: Yes Analysis Start: February 02, 2022 10:55 Analysis Stop Date: February 05, 2022 10:00 Analyst: Kristin Baecher, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 150.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2202011, 2202012, 2202013, 2202014, 2202015, 2202016, 2202017 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD7 Sample Date/Time: February 01, 2022 14:08 BCS Sample ID: 2202017 Sample Description: Biosolid Date Received: February 02, 2022 9:38 Amount Submitted:100 mL bottle % Solids: 37.2 Amount Analyzed: 30.03 g Receipt Temperature: 5.3 deg C Preserved: Yes Analysis Start: February 02, 2022 10:55 Analysis Stop Date: February 05, 2022 10:00 Analyst: Kristin Baecher, M.S. Qualifier: U Primary Value: 150.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS 10 2202011, 2202012, 2202013, 2202014, 2202015, 2202016, 2202017 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW. MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES liaczWA A1116 =,,i Client: Branch Residuals and Soils Project: Von Drehle Cordova NC Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2202011, 2202012, 2202013, 2202014, 2202015, 2202016, 2202017 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES "�;,. I51 T. i - wo ff;3c-nlRa . I certify that I have examined and I am familiar with the information submitted herein. The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 1702S, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. Date: February 09, 2022 Page 7 of 8 Final Report BCS ID 2202011, 2202012, 2202013, 2202014, 2202015, 2202016, 2202017 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES l$G�N{piAAM i-�� f GCrt LGit L u DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set (1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit & the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist for the component. J3 The data are questionable because of improper laboratory or field protocols. L Off scale high. Actual value is known to be greaterthan value given. N Presumptive evidence forthe presence of material. There is an indication thatthe analyte is present, but the confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. U Indicates that the compound was analyzed for but not detected. The specified component was not detected. The reported value is the method detection limit. V Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that can be determined based on the volume. 7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client. Sterility can not be confirmed by BCS. # BCS Lab specific qualifier. See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2202011, 2202012, 2202013, 2202014, 2202015, 2202016, 2202017 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ram'"—"`1 fcc nco a�cu 0 Z Q M' Lq } C W Oi C%I Ln M O M Li LL n N= rn c0i C � <3 CL —� Z O �. N EO U � M ❑ O U w 0 Nr O o U) U- U Q u_ O W Z E Nj- U U N U; co d W d o O ca ;a O s] V J O J LL U , Z X m U. I (seliddy a83) .LVI HsmAI Ualmol sisal UOdb-la 9191 V, plow pue Ise XX301 seuowopne XX3(31 sn3303OJ81 XX301 eilauot6 po4law 000 ellauoi6 (adH) eualoeg luno0 ap !100 Lw0I1100 lei +fr6 f dds ellauowl enO 4lulwl wioploo leo eipjeiE)g wnipuoasc sru!n ou91u3 elgejnlln0 x (aloj!o) l!oS/a6PnlSip!loso!I JaleM 6ul4u!jo JalemalseM jalem ooepn! 8£:6 ZZOZ/ZO/ZO PLOZOZZ ban siloS pue sienpisaa 4:)ueje I t i f0 y 0 pp C M C N pOj CO M W O LA f cm N N M O t N O N O N O N L3 > G N ep r N G N C N, N Nin N N CD N lA > N a N cu O M N O L O u c O L O soloed aol uazoIl / aoi pappe 9leilnso!41 wnipoS uo!loelloo le ainleiedwal uo11331103 le Hd paiallY PlalZI al!sodwo0 gejJ r' r r^ J podd14s sjauleluoo to 'oN �� •� paldweS awi.L ti� L, •a ^7 ., �} paldweS oleo r jy y fl a) 01 t—� C i d Of m 'C IQ E a a d 'a° Z � rn ,n o C _ �+� 0 E f� N '0 Q ca U d O c Z d a N v N 9 co y E` a 07 E "' Z ~ N N O O N O ❑ 10 O > N > 2to a a: cm a ct c ,cn V2 2' m tD m -0 V U C d Y O m D ti C d — V u m a cc a s Ci U l0 s ` CDtJd8 O n m E c a o 0 m E N 0 N O cic`.ai m 00 a m o_ D a .a ,v E a >_ 3 'o � `n `o (r w ,-. o E E N y N C t�J hf C c c -W,), mim 0 N 0 H C a a Marcal Cordova, LLC (Formerly von Drehle Corporation) Cordova, NC City of Rockingham IUP 0015 Mar-22 Biological Consulting Services lYIP�:.�� � er Sri1... `MPN 4 . 2203001 3/4/22 < 0.07 _ 2203002 3/4/22 < 0.07 < 0.7 2203003 3/4/22 < 0.07 < 0.7 2203004 3/4/22 < 0.07 < 0.7 2203005 3/4/22 < 0.07 < 0.7 2203006 3/4/22 < 0.07 < 0.7 2203007 3/4/22 < 0.07 < 0.7 Exceedances U All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Monthly Pathogen and Vector Attraction Reduction Forms for Class A option. inc. BIOLOGICAL CONSULTING SERVICES OF NORTH FLOR/DA, INC. March 04, 2022 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd. Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD1, VD2, VD3, VD4, VD5, VD6, VD7 BCS ID: 2203001, 2203002, 2203003, 2203004, 2203005, 2203006, 2203007 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Von Drehle Analysis Method Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, 1Vr�tG1 �LL Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 2203001, 2203002, 2203003, 2203004, 2203005, 2203006, 2203007 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 1-2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 140 to FAB Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD1 Sample Date/Time: February 28, 2022 12:52 BCS Sample ID: 2203001 Sample Description: Biosolid Date Received: March 01, 2022 9:49 Amount Submitted:100 mL BCS Bottle % Solids: 38.7 Amount Analyzed: 30.10 g Receipt Temperature: 2.0 deg C Preserved: Yes Analysis Start: March 01, 2022 10:50 Analysis Stop Date: March 04, 2022 10:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD2 Sample Date/Time: February 28, 2022 13:00 BCS Sample ID: 2203002 Sample Description: Biosolid Date Received: March 01, 2022 9:49 Amount Submitted:100 mL BCS Bottle % Solids: 38.4 Amount Analyzed: 30.08 g Receipt Temperature: 2.0 deg C Preserved: Yes Analysis Start: March 01, 2022 10:50 Analysis Stop Date: March 04, 2022 10:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 2203001, 2203002, 2203003, 2203004, 2203005, 2203006, 2203007 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 1,. ......... 8 Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD3 Sample Date/Time: February 28, 2022 13:02 BCS Sample ID: 2203003 Sample Description: Biosolid Date Received: March 01, 2022 9:49 Amount Submitted:100 mL BCS Bottle % Solids: 37.9 Amount Analyzed: 30.02 g Receipt Temperature: 2.0 deg C Preserved: Yes Analysis Start: March 01, 2022 10:50 Analysis Stop Date: March 04, 2022 10:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD4 Sample Date/Time: February 28, 2022 13:05 BCS Sample ID: 2203004 Sample Description: Biosolid Date Received: March 01, 2022 9:49 Amount Submitted:100 mL BCS Bottle % Solids: 38.9 Amount Analyzed: 30.00 g Receipt Temperature: 2.0 deg C Preserved: Yes Analysis Start: March 01, 2022 10:50 Analysis Stop Date: March 04, 2022 10:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2203001, 2203002, 2203003, 2203004, 2203005, 2203006, 2203007 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES I'lla-I+ a AF I B 7 Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD5 Sample Date/Time: February 28, 2022 13:07 BCS Sample ID: 2203005 Sample Description: Biosolid Date Received: March 01, 2022 9:49 Amount Submitted:100 mL BCS Bottle % Solids: 39.1 Amount Analyzed: 30.07 g Receipt Temperature: 2.0 deg C Preserved: Yes Analysis Start: March 01, 2022 10:50 Analysis Stop Date: March 04, 2022 10:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD6 Sample Date/Time: February 28, 2022 13:10 BCS Sample ID: 2203006 Sample Description: Biosolid Date Received: March 01, 2022 9:49 Amount Submitted:100 mL BCS Bottle % Solids: 38.1 Amount Analyzed: 30.00 g Receipt Temperature: 2.0 deg C Preserved: Yes Analysis Start: March 01, 2022 10:50 Analysis Stop Date: March 04, 2022 10:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 150.07 Salmonella MPN/mL sample analyzed Secondary Value: 150.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2203001, 2203002, 2203003, 2203004, 2203005, 2203006, 2203007 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422, PADEP: 68-03950, AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES AM o •: ncr:cu Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD7 Sample Date/Time: February 28, 2022 13:13 BCS Sample ID: 2203007 Sample Description: Biosolid Date Received: March 01, 2022 9:49 Amount Submitted:100 mL BCS Bottle % Solids: 39.0 Amount Analyzed: 30.10 g Receipt Temperature: 2.0 deg C Preserved: Yes Analysis Start: March 01, 2022 10:50 Analysis Stop Date: March 04, 2022 10:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2203001, 2203002, 2203003, 2203004, 2203005, 2203006, 2203007 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Project: Von Drehle Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2203001, 2203002, 2203003, 2203004, 2203005, 2203006, 2203007 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES A&B _ '� I certify that I have examined and I am familiar with the information submitted herein. The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. Date: March 04, 2022 Page 7 of 8 Final Report BCS ID 2203001, 2203002, 2203003, 2203004, 2203005, 2203006, 2203007 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES iilc+'i�iRPk`A96 - ' e DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set (1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit &the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist for the component. J3 The data are questionable because of improper laboratory or field protocols. L Off scale high. Actual value is known to be greater than value given. N Presumptive evidence for the presence of material. There is an indication that the analyte is present, but the confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. U Indicates that the compound was analyzed for but not detected. The specified component was not detected. The reported value is the method detection limit. V Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that can be determined based on the volume. 7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client. Sterility can not be confirmed by BCS. # BCS Lab specific qualifier. See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2203001, 2203002, 2203003, 2203004, 2203005, 2203006, 2203007 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES li$Gy,' Apg ! . ~ - � •. AC C...GG V �1 0 Z u a M } n � c~7 • � m � N M U 4 M o L U. 0 LL N J of 1- OC 2 N C: m 0 V c) a JZ C4.4 C, I 0 U0•co o v � c (L V � U. (sallddv aa-q) ltll ua�Mo� sisal aOdb-la 9LgL V plow pue lsE XX301 seuowopne XX3a1 sn00000jal XX3al ellauo16 po4law 000 ellau016 (OdH) eualoeg luno0 alE 11O3 wJOI!1O0 lei dds ellauowl 11 ! eA0 41u1w1i uLolgoo leo epe10 V wnlppoasa srulA oualu3 elgemlln0 (al31lo) N :o e � 0 h O N 9 j o roi cnY1 N o o H 00 m N ISN L O O❑ M O D o N N N th N N O N O m Ei r2 L L O C7 u c c m ` m r� � Jalem 6ulup(] �aleMalseM jalem aoeplis o Q :(Apeds) ja410 soloed aol uazoil / aol q r Urn Iv-Z u 00 (o m � p V -, E T-\ o J U`"•� 6- N im o p aFo pappe alellnsomi wnipos uogoa1IDD le amleaadwei uolioolioo le Hd pajally ple13 allsodwo0 gej0 �.+ SL Paddlys sjauleluoo to oN .. .-� paldweS awllUL Ri paldweS aleQ m y N 01 N i d d E Vi O m U '6 O = Z o N II m ` Q c a E l- m °7 E H o Z ~ CG M m N E 16 O N ❑ ' G N C N E%) G N CNI N O N VI G t i d U tY h L o o c t c ,a m to «Z fJ Z c d Y O C? - c E 5 c E O O > V 0 Y CD Ci a��tt to .0 V E 3 o m F' o aci O +' N Yl O o E E V-- E i=-:� w LL aO g a cn m 0 8 _E WE N O y o m c�� m m m `v 15 y j O N i�Vfv_ N d N O L C m m` N O N C1 CD C O R N F+ o N aj V C CL 9 O N N m d o rn o: tr tr L o u c �o m Marcal. Cordova, LLC (Formerly von Drehle Corporation) Cordova, NC City of Rockingham IUP 0015 Apr-22 Biological Consulting Services . . a ........... r mary. ........ Q ...... ..Mon air ella a W��. A .... ............ V N. 4JO M. pp 2203136 3/25/22 < 0.07 :5 0.6 2203137 3/25/22 < 0.07 < 0.6 2203138 3/25/22 < 0.07 < 0.6 2203139 3/25/22 :S 0.07 < 0.6 2203140 3/25/22 < 0.07 < 0.6 2203141 3/25/22 < 0.07 < 0.6 2203142 3/25/22 < 0.07 :5 0.6 ....... . . . . . . . . . . . Exceedances ........ .... All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Monthly Pathogen and Vector Attraction Reduction Forms for Class A option. inc. BIOLOGICAL CONSULTING SERVICES --,/ OF NORTH FLORIDA, INC. March 28, 2022 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd. Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD5, VD6, VD7, VD1, VD2, VD3, VD4 BCS ID: 2203136, 2203137, 2203138, 2203139, 2203140, 2203141, 2203142 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Von Drehle Cordova NC Analysis Method Salmonella EPA 1682; BCS SOP M-4 (1SO17025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 2203136, 2203137, 2203138, 2203139, 2203140, 2203141, 2203142 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 1$C rRp A J= r l AC G...LCii 1 t I> ...I;,iCftYu.;l..acu'd'e Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD5 Sample Date/Time: March 21, 2022 13:22 BCS Sample ID: 2203136 Sample Description: Biosolid Date Received: March 22, 2022 10:14 Amount Submitted:100 mL BCS Bottle % Solids: 43.7 Amount Analyzed: 29.91 g Receipt Temperature: 2.5 deg C Preserved: Yes Analysis Start: March 22, 2022 11:08 Analysis Stop Date: March 25, 2022 12:20 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 150.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD6 Sample Date/Time: March 21, 2022 13:26 BCS Sample ID: 2203137 Sample Description: Biosolid Date Received: March 22, 2022 10:14 Amount Submitted:100 mL BCS Bottle % Solids: 42.7 Amount Analyzed: 29.96 g Receipt Temperature: 2.5 deg C Preserved: Yes Analysis Start: March 22, 2022 11:08 Analysis Stop Date: March 25, 2022 12:20 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 2203136, 2203137, 2203138, 2203139, 2203140, 2203141, 2203142 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES lac=rs�a A nr.�i B Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD7 Sample Date/Time: March 21, 2022 13:30 BCS Sample ID: 2203138 Sample Description: Biosolid Date Received: March 22, 2022 10:14 Amount Submitted:100 mL BCS Bottle % Solids: 44.9 Amount Analyzed: 29.97 g Receipt Temperature: 2.5 deg C Preserved: Yes Analysis Start: March 22, 2022 11:08 Analysis Stop Date: March 25, 2022 12:20 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD1 Sample Date/Time: March 21, 2022 13:06 BCS Sample ID: 2203139 Sample Description: Biosolid Date Received: March 22, 2022 10:14 Amount Submitted:100 mL BCS Bottle % Solids: 43.6 Amount Analyzed: 29.96 g Receipt Temperature: 2.5 deg C Preserved: Yes Analysis Start: March 22, 2022 11:08 Analysis Stop Date: March 25, 2022 12:20 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Final Report BCS ID 2203136, 2203137, 2203138, 2203139, 2203140, 2203141, 2203142 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES A&B'IQI Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD2 Sample Date/Time: March 21, 2022 13:10 BCS Sample ID: 2203140 Sample Description: Biosolid Date Received: March 22, 2022 10:14 Amount Submitted:100 mL BCS Bottle % Solids: 45.4 Amount Analyzed: 30.00 g Receipt Temperature: 2.5 deg C Preserved: Yes Analysis Start: March 22, 2022 11:08 Analysis Stop Date: March 25, 2022 12:20 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD3 Sample Date/Time: March 21, 2022 13:14 BCS Sample ID: 2203141 Sample Description: Biosolid Date Received: March 22, 2022 10:14 Amount Submitted:100 mL BCS Bottle % Solids: 43.4 Amount Analyzed: 30.09 g Receipt Temperature: 2.5 deg C Preserved: Yes Analysis Start: March 22, 2022 11:08 Analysis Stop Date: March 25, 2022 12:20 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2203136, 2203137, 2203138, 2203139, 2203140, 2203141, 2203142 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES do AAB >: -I _ Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD4 Sample Date/Time: March 21, 2022 13:18 BCS Sample ID: 2203142 Sample Description: Biosolid Date Received: March 22, 2022 10:14 Amount Submitted:100 mL BCS Bottle % Solids: 45.3 Amount Analyzed: 30.00 g Receipt Temperature: 2.5 deg C Preserved: Yes Analysis Start: March 22, 2022 11:08 Analysis Stop Date: March 25, 2022 12:20 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 150.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2203136, 2203137, 2203138, 2203139, 2203140, 2203141, 2203142 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES �t c a At" ���. Client: Branch Residuals and Soils Project: Von Drehle Cordova NC Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2203136, 2203137, 2203138, 2203139, 2203140, 2203141, 2203142 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES >` i 2 #�F3GMRP1` I certify that I have examined and I am familiar with the information submitted herein. The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. Date: March 28, 2022 -' Page 7 of 8 Final Report BCS ID 2203136, 2203137, 2203138, 2203139, 2203140, 2203141, 2203142 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set (1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit &the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist forthe component. J3 The data are questionable because of improper laboratory orfield protocols. L Off scale high. Actual value is known to be greater than value given. N Presumptive evidence forthe presence of material. There is an indication that the analyte is present, but the confirmation requirement was not met. 0 Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. U Indicates that the compound was analyzed for but not detected. The specified component was not detected. The reported value is the method detection limit. V Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that can be determined based on the volume. 7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client. Sterility can not be confirmed by BCS. # BCS Lab specific qualifier. See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2203136, 2203137, 2203138, 2203139, 2203140, 2203141, 2203142 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT HE WRITTEN CONSENT OF BCS LABORATORIES JABs3C-tNRf` Co) } `° uti M CD X O cN U. B N LL m � C S: Off— ti a E —j � C U 7 O U W } 0 O F- w U U. O z U p 0 o _ o N F- 'ec F- ��' o W V CL cca U. LL 0 C,4 \, O cm � N vs v W d 0 v O CD B O „ O co -._.. 4 (sellddy aaj) iv.L HsnH U N C Ja410 N a°n � r c M o; N \ n Z Z V� (v ualnno� •N sisal 2lodb-18 S L9l t/d3 \ plow Pue lseaA N v d, N N m O 1° c r o Y ° XX341 seuowopnesci N Ql � Q N N O '' .t m? C C c E m XX3(11 sn0000aalu3 •p>0 N N N CA m n XX3al EIIOU01691 y N N c o t o (' `41 PoUlaw 000 eilauo!68-1 co m Y c ar3 8 (OdH) eual3e8 }unoo a)eld E E w a°, a+ s N wioploo lelol =Y fj' nCDo ° a7 al o m E dds el!auowleg l 0 eAO ulu!wlaH N wio;!loo leoa j elpjelE)'8 wn!puoasolam,, snnA 0118lu3 algeinllno lelo. :(A4!oeds) jayl( x (alono) poS/appn! Jpiloso!! jaleM 6u!)lu!j❑ JaleMalseM jaleM aoepn! soloed aoi ueza} / a: pappe ale}Inso!yl wn!po! uo!loolloo le amleaadwa. uoyoapoo le H paJall!j p1a!j allsodwoo gejE) V J padd!ys siau!eluoo }o •oN O C. pa!dweg aw!1 .3 1L �J Y � peldweS ale(] C y N rn - ay E a- m a m 0 � Z d c Lm 0 E 0 O z d N N m V o a a v r E (a a m y �' a E (6 a° N N r N n z F- E M �, ee►► r N O M p m ,� N 9 Q C r+ C fn O > o N d u N N w N N V N � L � u c u o c � m 00 FEE _ w c m A r N L > c; — u o w N LL r./1 m _ N N C a _O < a �° a. C m C T m M T o ,rJ .,j CQ N N N N I� .m C. ur ` c O 0 f0 a •Q 10 I o 131010 Marcal Cordova, LLC (Formerly von Drehle Corporation) Cordova, NC City of Rockingham IUP 0015 May-22 Services Lab# Date Analyzed Prim2ry Aue Salmonella iPN a ail P second:::::::.Value Salmonella a Ml'N e 4 grams D :. P... 2204209 5/4/22 < 0.07 < 0.6 2204210 5/4/22 < 0.07 < 0.6 2204211 5/4/22 < 0.07 < 0.7 2204212 5/4/22 < 0.07 < 0.7 2204213 5/4/22 < 0.07 < 0.8 2204214 5/4/22 < 0.07 < 0.6 2204215 5/4/22 T < 0.07 < 0.6 Exceedances Q All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Monthly Pathogen and Vector Attraction Reduction Forms for Class A option. Inc. BIOLOGICAL CONSULTING SERVICES OF- NORTH FLORIDA, INC. CO-- � May 04, 2022 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd. Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD1, VD2, VD3, VD4, VD5, VD6, VD7 BCS ID: 2204209, 2204210, 2204211, 2204212, 2204213, 2204214, 2204215 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Von Drehle Cordova NC Analysis Method Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 2204209, 2204210, 2204211, 2204212, 2204213, 2204214, 2204215 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES =ME3p`Ad= qqjll Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD1 Sample Date/Time: April 26, 2022 13:03 BCS Sample ID: 2204209 Sample Description: Biosolid Date Received: April 27, 2022 9:58 Amount Submitted:100 mL BCS Bottle % Solids: 40.7 Amount Analyzed: 30.02 g Receipt Temperature: 1.6 deg C Preserved: Yes Analysis Start: April 27, 2022 11:50 Analysis Stop Date: May 04, 2022 9:09 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD2 Sample Date/Time: April 26, 2022 13:06 BCS Sample ID: 2204210 Sample Description: Biosolid Date Received: April 27, 2022 9:58 Amount Submitted:100 mL BCS Bottle % Solids: 40.3 Amount Analyzed: 30.02 g Receipt Temperature: 1.6 deg C Preserved: Yes Analysis Start: April 27, 2022 11:50 Analysis Stop Date: May 04, 2022 9:09 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :90.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units r ogc c u, o Final Report BCS ID 2204209, 2204210, 2204211, 2204212, 2204213, 2204214, 2204215 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES #�$G�iy4RA`AAAB "�'•\�ncc..e rx r.0 u Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD3 Sample Date/Time: April 26, 2022 13:09 BCS Sample ID: 2204211 Sample Description: Biosolid Date Received: April 27, 2022 9:58 Amount Submitted:100 mL BCS Bottle % Solids: 39.2 Amount Analyzed: 30.05 g Receipt Temperature: 1.6 deg C Preserved: Yes Analysis Start: April 27, 2022 11:50 Analysis Stop Date: May 04, 2022 9:09 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD4 Sample Date/Time: April 26, 2022 13:12 BCS Sample ID: 2204212 Sample Description: Biosolid Date Received: April 27, 2022 9:58 Amount Submitted:100 mL BCS Bottle % Solids: 38.2 Amount Analyzed: 29.96 g Receipt Temperature: 1.6 deg C Preserved: Yes Analysis Start: April 27, 2022 11:50 Analysis Stop Date: May 04, 2022 9:09 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2204209, 2204210, 2204211, 2204212, 2204213, 2204214, 2204215 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 1-2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD5 Sample Date/Time: April 26, 2022 13:15 BCS Sample ID: 2204213 Sample Description: Biosolid Date Received: April 27, 2022 9:58 Amount Submitted:100 mL BCS Bottle % Solids: 32.2 Amount Analyzed: 30.10 g Receipt Temperature: 1.6 deg C Preserved: Yes Analysis Start: April 27, 2022 11:50 Analysis Stop Date: May 04, 2022 9:09 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.8 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD6 Sample Date/Time: April 26, 2022 13:18 BCS Sample ID: 2204214 Sample Description: Biosolid Date Received: April 27, 2022 9:58 Amount Submitted:100 mL BCS Bottle % Solids: 41.9 Amount Analyzed: 30.03 g Receipt Temperature: 1.6 deg C Preserved: Yes Analysis Start: April 27, 2022 11:50 Analysis Stop Date: May 04, 2022 9:09 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units r ZY u,o Final Report BCS ID 2204209, 2204210, 2204211, 2204212, 2204213, 2204214, 2204215 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES i Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD7 Sample Date/Time: April 26, 2022 13:21 BCS Sample ID: 2204215 Sample Description: Biosolid Date Received: April 27, 2022 9:58 Amount Submitted:100 mL BCS Bottle % Solids: 40.6 Amount Analyzed: 30.01 g Receipt Temperature: 1.6 deg C Preserved: Yes Analysis Start: April 27, 2022 11:50 Analysis Stop Date: May 04, 2022 9:09 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Final Report BCS ID 2204209, 2204210, 2204211, 2204212, 2204213, 2204214, 2204215 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES JFA IIsG�. Client: Branch Residuals and Soils Project: Von Drehle Cordova NC Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2204209, 2204210, 2204211, 2204212, 2204213, 2204214, 2204215 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ItA16 us.Fn I certify that I have examined and I am familiar with the information submitted herein. The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. ,l Signature of Laboratory Director/Authorized Rep. Date: May 04, 2022 Page 7 of 8 Final Report BCS ID 2204209, 2204210, 2204211, 2204212, 2204213, 2204214, 2204215 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES .l" .-.0 DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set (1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit & the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist forthe component. J3 The data are questionable because of improper laboratory orfield protocols. L Off scale high. Actual value is known to be greaterthan value given. N Presumptive evidence forthe presence of material. There is an indication that the analyte is present, but the confirmation requirement was not met. 0 Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. U Indicates that the compound was analyzed for but not detected. The specified component was not detected. The reported value is the method detection limit. V Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that can be determined based on the volume. ? Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client. Sterility can not be confirmed by BCS. # BCS Lab specific qualifier. See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2204209, 2204210, 2204211, 2204212, 2204213, 2204214, 2204215 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 0 Z F-I Kw M zA M �u } CO) � In al) N v ? 1 X c C> .O W' C.,) LL W ! cq ccCD U O (L1 N ti c0 � CO W (D 1— p N .' O - O 07 E O uj m U m 0 � a. to LL c 89:6 ZZOVLZ1b0 ZLZVOZZ VGA spog pue slenpisaa 4oueJg (sollddV aa=l)1-V.L HsnL I I I I :Jat11O sisal HOdb-j,iA 9L% Vd3i " plolN pue lseaA 0 N XX301 seuowopnasc{ � In i m XX3a1 s"33OOOJa)U_] *a f- N N 7 Q of a N{ c I 9 7 0 N elleuo!6a-1 9 7 N N N N XX3(11 N N d m P041ow OdD ellau016olj L o o L_ c (OdH) eualoeg lunoZ) aleldl m m Iloo '3I wJo;!100 Plod r f' :.-r /dds ellauowle5 N I enO 41u!w10H1 wJo}!loo ImmA e!pJe1O g wnlp!Jodsoldfu:Di snJ!n 3u9lu3 algemilno Ie1oJ O N m E E 0 U 0 m 0 z m J U > x (alono) I!osla6PEIS/p!lostng -y cl- --n LU Ja)eM 6unluuQ ! . 0 �y ry JalemalseM JaleM a3elJnsLL CD •` D "oed aol tiazoJ} / ani, r_ O u.l l'r {,7 PapPe alellnso!41 wn!poSi ' z - a 0 -y rn uo!laalloo le aJnie.todwe,L = C -- . U W z uo!loailoo le hd! v, ? -� c al!sodwoo ge1J I Gn �? — t c7i U J n U 1 Ln " " m 'E paddlt!s sJau!eluoo to •ohl �� r -- _ m to N N 3 J ___l �ti --, , I�t M !`� (•-.mot t"'' N ° d d c mc 3 v` dal m c `° E a o N Z 41 Q7 y to U m C E t Z d N E a` L d C E " N Z ly E m M N N a N C m N N d U c m m` j O N paldweS atu! l �� , % .J ''nJ N N - a poldwes 91e0 J m c O CL y 0 uj O V to ayi �, a - 2 .9 O O N 7 t ri �-'S f� I^ f'� � C N y '63 E 'd) cLi to O. � � M m O Z U C m Y O m } 11 V U "_ c a s E do0 figg! u u E_ t1 CL O 0 m 1' ? E " d N uCL(Lm " to O a .$ a I ` ❑ / (n Oj m � a E En o ,l 0 E E P a a Marcal Cordova, LLC (Formerly von Drehle Corporation) Cordova, NC City of Rockingham IUP 0015 Jun-22 Biological Consulting Services ................ na .. mar a ue: Almon 9::: ................. ...... ............... V- ifti. a con luk mon I ..... ... ......... ................ ..... ... ....... . ................ ....... ................ .............. ..................................... .... ........... ........ ........ ................. ................. ..... P..e .......... M ............ . ................ * ........ ............... ...... ..... ..... WN ....... M -am$: ..... ::per.. g.r ..Y ..... 2206031 6/4/22 < 0.07 < 0.6 2206002 6/4/22 < 0.07 < 0.6 2206003 6/4/22 < 0.07 :5 0.6 2206004 6/4/22 < 0.07 < 0.7 2206005 6/4/22 :5 0.07 :5 0.7 2206006 6/4/22 < 0.07 :5 0.8 2206007 6/4/22 < 0.07 :S 0.7 .................. ......... ................. ................................ ....................... Exceedances All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Monthly Pathogen and Vector Attraction Reduction Forms for Class A option. :inc. BIOLOGICAL CONSULTING SERVICES OF NORTH FLOR/DA, INC. June 06, 2022 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd. Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD 1, VD 2, VD 3, VD 4, VD 5, VD 6, VD 7 BCS ID: 2206001, 2206002, 2206003, 2206004, 2206005, 2206006, 2206007 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: 2014-110 Analysis Method Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 2206001, 2206002, 2206003, 2206004, 2206005, 2206006, 2206007 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, A7-DHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES A&B`1�FiG=NEi{A Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD 1 BCS Sample ID: 2206001 Date Received: June 01, 2022 10:25 Amount Analyzed: 30.10 g Analysis Start: June 01, 2022 11:50 Analyst: Robert Pimentel, B.S. Sample Date/Time: May 31, 2022 12:50 Sample Description: Biosolids Amount Submitted:100 mL BCS Bottle % Solids: 41.4 Receipt Temperature: 1.7 deg C Preserved: Yes Analysis Stop Date: June 04, 2022 9:00 Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD 2 BCS Sample ID: Date Received: Amount Analyzed Analysis Start: Analyst: 2206002 June 01, 2022 10:25 30.09 g June 01, 2022 11:50 Robert Pimentel, B.S. Sample Date/Time: May 31, 2022 12:53 Sample Description: Biosolids Amount Submitted:100 mL BCS Bottle % Solids: 46.9 Receipt Temperature: 1.7 deg C Preserved: Yes Analysis Stop Date: June 04, 2022 9:00 Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page t or 6 Final Report BCS ID 2206001, 2206002, 2206003, 2206004, 2206005, 2206006, 2206007 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ;ilt1:_I'AAw Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD 3 Sample Date/Time: May 31, 2022 12:56 BCS Sample ID: 2206003 Sample Description: Biosolids Date Received: June 01, 2022 10:25 Amount Submitted:100 mL BCS Bottle % Solids: 42.6 Amount Analyzed: 30.00 g Receipt Temperature: 1.7 deg C Preserved: Yes Analysis Start: June 01, 2022 11:50 Analysis Stop Date: June 04, 2022 9:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: _<0.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD 4 Sample Date/Time: May 31, 2022 13:00 BCS Sample ID: 2206004 Sample Description: Biosolids Date Received: June 01, 2022 10:25 Amount Submitted:100 mL BCS Bottle % Solids: 39.9 Amount Analyzed: 30.10 g Receipt Temperature: 1.7 deg C Preserved: Yes Analysis Start: June 01, 2022 11:50 Analysis Stop Date: June 04, 2022 9:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2206001, 2206002, 2206003, 2206004, 2206005, 2206006, 2206007 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES A16 ��- 1�3G.�NfRA c e u Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD 5 Sample Date/Time: May 31, 2022 13:03 BCS Sample ID: 2206005 Sample Description: Biosolids Date Received: June 01, 2022 10:25 Amount Submitted:100 mL BCS Bottle % Solids: 39.7 Amount Analyzed: 30.09 g Receipt Temperature: 1.7 deg C Preserved: Yes Analysis Start: June 01, 2022 11:50 Analysis Stop Date: June 04, 2022 9:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD 6 Sample Date/Time: May 31, 2022 13:06 BCS Sample ID: 2206006 Sample Description: Biosolids Date Received: June 01, 2022 10:25 Amount Submitted:100 mL BCS Bottle % Solids: 31.0 Amount Analyzed: 29.95 g Receipt Temperature: 1.7 deg C Preserved: Yes Analysis Start: June 01, 2022 11:50 Analysis Stop Date: June 04, 2022 9:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.8 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2206001, 2206002, 2206003, 2206004, 2206005, 2206006, 2206007 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES w�.All" Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD 7 Sample Date/Time: May 31, 2022 13:09 BCS Sample ID: 2206007 Sample Description: Biosolids Date Received: June 01, 2022 10:25 Amount Submitted:100 mL BCS Bottle % Solids: 39.1 Amount Analyzed: 29.97 g Receipt Temperature: 1.7 deg C Preserved: Yes Analysis Start: June 01, 2022 11:50 Analysis Stop Date: June 04, 2022 9:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 0.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2206001, 2206002, 2206003, 2206004, 2206005, 2206006, 2206007 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES >ll's�G=fNE(q' r� A ti C Client: Branch Residuals and Soils Project: 2014-110 Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2206001, 2206002, 2206003, 2206004, 2206005, 2206006, 2206007 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 1-2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Aw r ll3G-i44RFl I certify that I have examined and I am familiar with the information submitted herein. The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. Date: June 06, 2022 Page 7 of 8 Final Report BCS ID 2206001, 2206002, 2206003, 2206004, 2206005, 2206006, 2206007 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 1-2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES r. �= DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set (1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit & the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist for the component. J3 The data are questionable because of improper laboratory or field protocols. L Off scale high. Actual value is known to be greaterthan value given. N Presumptive evidence forthe presence of material. There is an indication that the analyte is present, but the confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. U Indicates that the compound was analyzed for but not detected. The specified component was not detected. The reported value is the method detection limit. V Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that can be determined based on the volume. 7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client. Sterility can not be confirmed by BCS. # BCS Lab specific qualifier. See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2206001, 2206002, 2206003, 2206004, 2206005, 2206006, 2206007 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 'WF h� y z O c N U (sallddy ead) lb'1 HsnH o :,aylt) gDZ z Q CD CAN �v'i N r Ual�wol 'l`J C I ( - sisal MC)d6-lid SL91. Vd3 y y 'p Cl)�! PIOW Pue }sea, is 0 m ^ A N 9 c N m Y 1 XX301 seuowopnesd M� W Q: �N M i y � Q N N Q ` co XX301 sn00000,alu3 � `' Cl. m of C fV A U C N V �1 °I + 7 ❑ O N N ❑ �p N d N -i XX301 ellau016a- as COS La. s \ a> e4 b L N —j ti 1 —`, y o o o a POt4l9w 000 e11au0160-1 O LL � �,, `� r r n (OdH) eualoeg 1un00 aleld O rn n co m` m` 9 N C o »: H CD I N E .� `.,f f0 W O N U f0 wo y- spy w,ol!1o018101 t� Z N o ^ry V 9❑ o o � o a Q% CI) 1 N N N . f ,Y �/ C� A U U E k f �7' J t;. dds epauowleS Uo �� v a Cy = C E H N tmll 0 enp ylwwlaH c 1-- V a a x „ w,ol!Ioo Ieoad ui c _ o co Ri - U t E 0 E E e!p,e!E) ig wnlpuodsoldti0 r d �' O W 0 t p P v 0 c sn"A oualu3 alge,nlln0 lelol O .; ° a ano) I!os/a6pnlg�P11oso! ,aert 6u!;uu o r2� y o 6 �' o N w u_ �J ,alemalsep/l 0 O r J �� o = C N N ,alert aoel,ng uL in N N s),ayl0 V a "ao1uazo,/ u. O W c=� m EL pappe olelinsw4l wn!pos uo!lOalloo le a,nle,edwal a E ;, r p �? U = V V� CD -' 1 Z R — u0!1001100 le Hd U W \ �; U. n n d c pa,all!:j Plaid o E •> "� 9 u, m r 4) m w al!sodwo0 �..� C N m ui 0_ O ��t \ ,- y" TO N O N cmN 'D a)d _ �� :1 .ti, 1 O a N CD ° E i= .�1 E padd!ys s,au!eluoa }o 'ON E �ti paldweg ew!1 ,.t> c CD t5 poldweg alea ' _ C in ` y N 01 E a ¢ Q Z y c _Q1 c O o N o C ' O c E m cn L un A ip 6) d 0 2 m O' u d o y '- m oo E a m y a M ❑ N g a N a �. N Z y F y N N r cn V✓� t� i ,� iC`�'� 5 Marcal Cordova, LLC (Formerly von Drehle Corporation) Cordova, NC City of Rockingham IUP 0015 Jul-22 Biological Consulting Services ................................................ .. .. . ..... U AW. ............... ....................... .................................. ......A . . . ... . . . ateAkWV"d .. . ...... ........................................ r mar V 'Ifiloh a::::::: .: - - A t1i"SA .................................... ............... .................. ............. ........................................ twond'Arvi a fti: diftoildit. VdSi .......... ........... .... ........................... ...... ... ................ .......... * ' ' P . . :: ... ---- ------------ ---- ' �4. ... ..... .. . . . -OW gy .... . ..... 2207109 7/19/22 :s 0.07 < 0.8 2207110 7/19/22 < 0.07 < 0.7 2207111 7/19/22 < 0.07 < 0.9 2207112 7/19/22 < 0.07 < 0.8 2207113 7/19/22 < 0.07 < 0.9 2207114 7/19/22 < 0.07 < 1.0 2207115 7/19/22 < 0.07 < 0.9 .................... .................. .................... .......... ................... .......... Exceedances All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Monthly Pathogen and Vector Attraction Reduction Forms for Class A option. a-N, inc. BIOLOGICAL CONSULTING SERVICES OF NORTH FLORIDA, INC. July 19, 2022 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd. Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD 1, VD 2, VD 3, VD 4, VD 5, VD 6, VD 7 BCS ID: 2207109, 2207110, 2207111, 2207112, 2207113, 2207114, 2207115 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Von Drehle Cordova NC Analysis Method Salmonella EPA 1682; BCS SOP M-4 (ISC17025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, r. I Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 . Final Report BCS ID 2207109, 2207110, 2207111, 2207112, 2207113, 2207114, 2207115 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 1-2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES AAW �.l..le.53'+x.iluuu.vw. Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD 1 Sample Date/Time: July 13, 2022 12:44 BCS Sample ID: 2207109 Sample Description: Biosolid Date Received: July 14, 2022 9:52 Amount Submitted:100 mL Bottle % Solids: 33.0 Amount Analyzed: 29.98 g Receipt Temperature: 3.0 deg C Preserved: Yes Analysis Start: July 14, 2022 10:20 Analysis Stop Date: July 19, 2022 10:40 Analyst: Erika DiPasquale, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.8 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD 2 BCS Sample ID Date Received Amount Analyzed 2207110 July 14, 2022 9:52 Sample Date/Time: July 13, 2022 12:46 Sample Description: Biosolid Amount Submitted:100 mL Bottle % Solids: 38.0 Receipt Temperature: 3.0 deg C Preserved: Yes Analysis Start: July 14, 2022 10:20 Analysis Stop Date: July 19, 2022 10:40 Analyst: Erika DiPasquale, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units 30.03 g Page 2 of 8 Final Report BCS ID 2207109, 2207110, 2207111, 2207112, 2207113, 2207114, 2207115 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES li#e-AhRPiAAAB i \ c c n k n• f n v Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD 3 BCS Sample ID: 2207111 Date Received: Amount Analyzed: Analysis Start: Analyst: July 14, 2022 9:52 30.10 g July 14, 2022 10:20 Erika DiPasquale, B.S. Sample Date/Time: July 13, 2022 12:48 Sample Description: Biosolid Amount Submitted:100 mL Bottle % Solids: 28.7 Receipt Temperature: 3.0 deg C Preserved: Yes Analysis Stop Date: July 19, 2022 10:40 Qualifier: U Primary Value: 150.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.9 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD 4 BCS Sample ID: 2207112 Date Received: July 14, 2022 9:52 Amount Analyzed: 30.00 g Sample Date/Time: July 13, 2022 12:51 Sample Description: Biosolid Amount Submitted:100 mL Bottle % Solids: 31.4 Receipt Temperature: 3.0 deg C Preserved: Yes Analysis Start: July 14, 2022 10:20 Analysis Stop Date: July 19, 2022 10:40 Analyst: Erika DiPasquale, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.8 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2207109, 2207110, 2207111, 2207112, 2207113, 2207114, 2207115 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 118CmNER/#AAw elpAblu ,44 /�\ Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD 5 BCS Sample ID: 2207113 Date Received: July 14, 2022 9:52 Amount Analyzed: 30.00 g Sample Date/Time: July 13, 2022 12:53 Sample Description: Biosolid Amount Submitted:100 mL Bottle % Solids: 29.1 Receipt Temperature: 3.0 deg C Preserved: Yes Analysis Start: July 14, 2022 10:20 Analysis Stop Date: July 19, 2022 10:40 Analyst: Erika DiPasquale, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.9 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD 6 Sample Date/Time: July 13, 2022 12:55 BCS Sample ID: 2207114 Sample Description: Biosolid Date Received: July 14, 2022 9:52 Amount Submitted:100 mL Bottle % Solids: 27.1 Amount Analyzed: 30.00 g Receipt Temperature: 3.0 deg C Preserved: Yes Analysis Start: July 14, 2022 10:20 Analysis Stop Date: July 19, 2022 10:40 Analyst: Erika DiPasquale, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :51.0 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2207109, 2207110, 2207111, 2207112, 2207113, 2207114, 2207115 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES li$C-MRA �A� e Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD 7 Sample Date/Time: July 13, 2022 12:57 BCS Sample ID: 2207115 Sample Description: Biosolid Date Received: July 14, 2022 9:52 Amount Submitted:100 mL Bottle % Solids: 29.1 Amount Analyzed: 30.01 g Receipt Temperature: 3.0 deg C Preserved: Yes Analysis Start: July 14, 2022 10:20 Analysis Stop Date: July 19, 2022 10:40 Analyst: Erika DiPasquale, B.S. Qualifier: U Primary Value: 150.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.9 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2207109, 2207110, 2207111, 2207112, 2207113, 2207114, 2207115 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES A Client: Branch Residuals and Soils Project: Von Drehle Cordova NC Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2207109, 2207110, 2207111, 2207112, 2207113, 2207114, 2207115 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:A7-0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ill)S3GaNiRA f I certify that I have examined and I am familiar with the information submitted herein. The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. 7' Date: July 19, 2022 Page 7 of 8 Final Report BCS ID 2207109, 2207110, 2207111, 2207112, 2207113, 2207114, 2207115 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOI IT THE WRITTEN CONSENT OF BCS LABORATORIES 11;pc' DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set (1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit & the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist forthe component. J3 The data are questionable because of improper laboratory orfield protocols. L Off scale high. Actual value is known to be greaterthan value given. N Presumptive evidence forthe presence of material. There is an indication that the analyte is present, butthe confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. U Indicates that the compound was analyzed for but not detected. The specified component was not detected. The reported value is the method detection limit. V Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that can be determined based on the volume. 7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client. Sterility can not be confirmed by BCS. # BCS Lab specific qualifier. See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2207109, 2207110, 2207111, 2207112, 2207113, 2207114, 2207115 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 1-2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES #c=iA19W 0 Z 11 C M CM u7 >- l � M m —04 M z cmC'. U! N M c, M LL G N '� U. : m = N d `J O z N �= G7 N to 0' U -r- N P` U CD,'cvn �. 7 m V {� 7 Y V d i+.1 o a m u. Lr- O U w 0 � O O U) LL U Q O w z E � = 0m UN co m w U N O O :n °n v J O LL zs:s zzozwrruo sutozz L QA _ slog pue sienp!saa goueis zs:s zzozuvuto v«Lozz 9 QA slog pue slenp!saa gauej 8 Ja410 ualmo� ••' _ 7 _ N O O j' 9) N C N . 9 N _ _ )! C N to A _ N C7 R d N m N _ _ =n )' N N I N O N i0 N cm > N i M N Ccl 7 , N N L CD r„ CD O �m -m rd. m m z° x m u_ S?,/ f�dds ellauot eAp glu!L !. wjo{!loo p e!p)e!E),g wn!puodsol sn.nA oualu3 alge)nllnJ 1 x (alono) I!osga5p6jyp!josol, jaleM 6u!Nuup jalemalseM Jajem aoejln'. sMaed aal uazal / a: pappe alejinso!gl wn!po, uo!loalloo le ainlejadwa uo!laalloo le H pa)a11!3 pla!zi al!sodwoJ gejE) padd!gs s)au!eluoo jo 'ON ■mmmm paldwes sw!1 * �- a ��� ✓ v, ,n v ti r paldwes ales '�{ --' `-- — - U ,L, U c d Y O m � rr C — to L C EC +. 0 tf) d 8 Zs d to 0 0 0, 0 O N N 0 'O ° ua`mx E E E v- L_ O WCo m LL (� a Marcal Cordova, LLC (Formerly von Drehle Corporation) Cordova, NC City of Rockingham IUP 0015 Aug-22 Biological Consulting Services C:: a Mon a::: ................ ....... .... ....... .... . lU::::e::::8i M: on; H'a.:: coinL:.:ar a ...........la ....... ...... ............... ....... ..... ...................... ......... ............... .... T .. ............ . ............ . ............ ..... NIP. . . ............ ............ . . :: . , PN :grow$: r-.Y...,:* 2207276 7/29/22 :5 0.07 < 0.6 2207277 7/29/22 < 0.07 :s 0.7 2207278 7/29/22 :S 0.07 :S 0.7 2207279 7/29/22 < 0.07 :50.7 2207280 7/29/22 < 0.07 :s 0.7 2207281 7/29/22 < 0.07 :s 0.7 2207282 7/29/22 < 0.07 :s 0.7 Exceedances All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Monthly Pathogen and Vector Attraction Reduction Forms for Class A option. inc. BIOLOGICAL CONSULTING SERVICES OF NORTH FLORIDA, INC. August 01, 2022 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd. Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD1, VD2, VD3, VD4, VD5, VD6, VD7 BCS ID: 2207276, 2207277, 2207278, 2207279, 2207280, 2207281, 2207282 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: 2014-110 Analysis Method Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, cif �,✓}v� � I'� 1.�L�✓� Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 2207276, 2207277, 2207278, 2207279, 2207280, 2207281, 2207282 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 1-2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ;= A �ti. wcc n.ccr�r.v Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD1 Sample Date/Time: July 25, 2022 13:02 BCS Sample ID: 2207276 Sample Description: Biosolid Date Received: July 26, 2022 9:53 Amount Submitted:100 mL Bottle % Solids: 42.8 Amount Analyzed: 30.10 g Receipt Temperature: 5.7 deg C Preserved: Yes Analysis Start: July 26, 2022 12:20 Analysis Stop Date: July 29, 2022 8:45 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD2 Sample Date/Time: July 25, 2022 13:04 BCS Sample ID: 2207277 Sample Description: Biosolid Date Received: July 26, 2022 9:53 Amount Submitted:100 mL Bottle % Solids: 37.6 Amount Analyzed: 30.07 g Receipt Temperature: 5.7 deg C Preserved: Yes Analysis Start: July 26, 2022 12:20 Analysis Stop Date: July 29, 2022 8:45 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 2207276, 2207277, 2207278, 2207279, 2207280, 2207281, 2207282 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES !li$C�IfAftA'M&B Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD3 BCS Sample ID: 2207278 Date Received: July 26, 2022 9:53 Amount Analyzed: 29.98 g Analysis Start: July 26, 2022 12:20 Analyst: Robert Pimentel, B.S. Sample Date/Time: July 25, 2022 13:07 Sample Description: Biosolid Amount Submitted:100 mL Bottle % Solids: 37.1 Receipt Temperature: 5.7 deg C Preserved: Yes Analysis Stop Date: July 30, 2022 9:00 Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD4 BCS Sample ID: 2207279 Date Received: July 26, 2022 9:53 Amount Analyzed Analysis Start: Analyst: 30.00 g July 26, 2022 12:20 Robert Pimentel, B.S. Sample Date/Time: July 25, 2022 13:10 Sample Description: Biosolid Amount Submitted:100 mL Bottle % Solids: 39.3 Receipt Temperature: 5.7 deg C Preserved: Yes Analysis Stop Date: July 30, 2022 9:00 Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2207276, 2207277, 2207278, 2207279, 2207280, 2207281, 2207282 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 14acz AP&B FCC !./ �„I;Vt;' ri ttM..lwuRAeore - Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD5 Sample Date/Time: July 25, 2022 13:14 BCS Sample ID: 2207280 Sample Description: Biosolid Date Received: July 26, 2022 9:53 Amount Submitted:100 mL Bottle % Solids: 39.1 Amount Analyzed: 30.10 g Receipt Temperature: 5.7 deg C Preserved: Yes Analysis Start: July 26, 2022 12:20 Analysis Stop Date: July 30, 2022 9:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 150.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD6 Sample Date/Time: July 25, 2022 13:16 BCS Sample ID: 2207281 Sample Description: Biosolid Date Received: July 26, 2022 9:53 Amount Submitted:100 mL Bottle % Solids: 38.4 Amount Analyzed: 30.09 g Receipt Temperature: 5.7 deg C Preserved: Yes Analysis Start: July 26, 2022 12:20 Analysis Stop Date: July 30, 2022 9:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2207276, 2207277, 2207278, 2207279, 2207280, 2207281, 2207282 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES I iKRl�4A I #M Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD7 Sample Date/Time: July 25, 2022 13:20 BCS Sample ID: 2207282 Sample Description: Biosolid Date Received: July 26, 2022 9:53 Amount Submitted:100 mL Bottle % Solids: 39.3 Amount Analyzed: 30.02 g Receipt Temperature: 5.7 deg C Preserved: Yes Analysis Start: July 26, 2022 12:20 Analysis Stop Date: July 30, 2022 9:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2207276, 2207277, 2207278, 2207279, 2207280, 2207281, 2207282 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT TH"EEWWRI17EN CONSENT OF BCS LABORATORIES IIy1G-NtAA1#AB Client: Branch Residuals and Soils Project: 2014-110 Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2207276, 2207277, 2207278, 2207279, 2207280, 2207281, 2207282 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES .,f, 5 �• .....'#,dam . I certify that I have examined and I am familiar with the information submitted herein. The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. Date: August 01, 2022 Page 7 of 8 Final Report BCS ID 2207276, 2207277, 2207278, 2207279, 2207280, 2207281, 2207282 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 1-2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 113G-tiiR{'At" DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received -without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set (1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit & the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist forthe component. J3 The data are questionable because of improper laboratory or field protocols. L Off scale high. Actual value is known to be greaterthan value given. N Presumptive evidence forthe presence of material. There is an indication thatthe analyte is present, but the confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. U Indicates that the compound was analyzed for but not detected. The specified component was not detected. The reported value is the method detection limit. V Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that can be determined based on the volume. 7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client. Sterility can not be confirmed by BCS. # BCS Lab specific qualifier. See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2207276, 2207277, 2207278, 2207279, 2207280, 2207281, 2207282 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 1-2422, PADEP: 68-03950, A7-DHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES A A ft B i�\: AG C n,KG1I r, u 0 z Q M T r I>- U M �=1 M W d N u, Cc,C.. V� CO O N cp 0 N J LL N s CD 0 m •N J z a� N 0 L) a W .,t V 12 O U W Y G 0 U LL O z U Cl 0- O - O = F- •gyp F m nvi o W 2 o - o. 0 a c m LL O � o � Q w o ,i t U 0) — 0 z N N W x U. U N O O S11 On 0 Cj h 3 o Ci �z o N LL v Q m c m ea U E 3 Z n. m o c cn o �p E 0 U ` a+ E c m O Z - °� ' a L d a E z IL l°' E m cn C N U £9=6 ZZOZ19ZILO ZBZLOZZ LOA sllog pue slenplsab yauejg (sa!lddy aaj) iVl Hsnm I N U lialmol N o _ c N �. a sisal UOdb-1Ll 919E Vd= _ > N N CA v }i>- PIOW Pue lsea� c cc N � "' v x f!1 M to N N . i o XX301 seuowopnasr c 9 o N c o m N XX301 sn0003ojalu3 R N N o m chi r XX301 ellauo!6a-1 > N N V i POy)aw 000 ellauo16e-1 m o m c c is y (OdH) eualoeg luno0 aleld � c a m w N Ol E !100 3 N a > v WJO}!I001e101 r°n � o o ) >� u u E J dds ellauowleg J �- }- n oo °f CL a o d m l' € h N N n 0 'D eA0 ylu!wlaH v o o N t� A- A. s° ' > N wj0)Iloo leoa j d N N CD CD e!p�e!g 8 wn!puodsoldti0 c IE E � snj!A 3!a9)u3 algemlln0 le)ol m • • `Cti :(Aj!oads) jayl0 O (alono) i!oS/ Beni P!loso!g y-- �3 r 9—' �� :} �) x e� m ti jaleM 6u!�luli0 c c o N N w JalemalseM o LL fn jalem ooepnS m c ,n N :(Apoads) jayl0 H Q; -a c h N m O s�laed ail uazOil / aOi y— -� .,_ l v O o N o°12 PaPPe alellnso!yi wrnpos �' N n a i uo!loapoo le ainlejadwal u a v ' c m uo!1391103 le Hd m` n a Zj paiall!j PIMA �(U m EEE apsodwo0 le tu �� gej0 0 r .1 c -0 m :ram. m (n r E E padd!ys sieu!eluoo to 'ON — cl DLD M paldw-6 ow!1 ,� n (j y N N Q 7 Q paldweg ale(] \ t o m :w n �L Nl c O n 7 > 61 i> Marcal Cordova, LLC (Formerly von Drehle Corporation) Cordova, NC City of Rockingham IUP 0015 Sep-22 Biological Consulting Services .............................. ... . .. . - Imar: .............. - ue:: a. onellic: .. ............. .... . ............ P ... .... ��r .Y ..... 22081571 8/23/22 :S 0.07 :50 .7 2208192 8/23/22 < 0.07 < 0.8 2208193 8/23/22 < 0.07 < 0.7 2208194 8/23/22 < 0.07 :5 0.7 2208195 8/23/22 < 0.07 < 0.8 2208196 %J 8/23/22 < 0.07 �5 0.7 2208197 8/23/22 :S 0.07 < 0.7 Exceedances ................. All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Monthly Pathogen and Vector Attraction Reduction Forms for Class A option. inc. BIOLOGICAL CONSULTING SERVICES f OF NORTH FLOR/DA, INC. August 23, 2022 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd. Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD1, VD2, VD3, VD4, VD5, VD6, VD7 BCS ID: 2208191, 2208192, 2208193, 2208194, 2208195, 2208196, 2208197 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: 2014-110 Analysis Method Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 2208191, 2208192, 2208193, 2208194, 2208195, 2208196, 2208197 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 1-2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES �• =lily: Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD1 Sample Date/Time: August 16, 2022 13:10 BCS Sample ID: '2208191 Sample Description: Biosolid Date Received: August 17, 2022 9:43 Amount Submitted:100 mL BCS Bottle % Solids: 39.0 Amount Analyzed: 30.03 g Receipt Temperature: 3.8 deg C Preserved: Yes Analysis Start: August 17, 2022 10:58 Analysis Stop Date: August 23, 2022 8:24 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD2 Sample Date/Time: August 16, 2022 13:05 BCS Sample ID: 2208192 Sample Description: Biosolid Date Received: August 17, 2022 9:43 Amount Submitted:100 mL BCS Bottle % Solids: 32.8 Amount Analyzed: 29.99 g Receipt Temperature: 3.8 deg C Preserved: Yes Analysis Start: August 17, 2022 10:58 Analysis Stop Date: August 23, 2022 8:24 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.8 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 2208191, 2208192, 2208193, 2208194, 2208195, 2208196, 2208197 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES lidNiRP[A&Bnit A«:k41 T k A Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD3 BCS Sample ID: 2208193 Date Received: August 17, 2022 9:43 Amount Analyzed: 30.00 g Analysis Start: August 17, 2022 10:58 Analyst: Robert Pimentel, B.S. Sample Date/Time: August 16, 2022 13:03 Sample Description: Biosolid Amount Submitted:100 mL BCS Bottle % Solids: 39.6 Receipt Temperature: 3.8 deg C Preserved: Yes Analysis Stop Date: August 23, 2022 8:24 Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 150.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD4 BCS Sample ID: 2208194 Date Received: August 17, 2022 9:43 Amount Analyzed: 30.10 g Analysis Start: August 17, 2022 10:58 Analyst: Robert Pimentel, B.S. Sample Date/Time: August 16, 2022 13:01 Sample Description: Biosolid Amount Submitted:100 mL BCS Bottle % Solids: 39.9 Receipt Temperature: 3.8 deg C Preserved: Yes Analysis Stop Date: August 23, 2022 8:24 Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2208191, 2208192, 2208193, 2208194, 2208195, 2208196, 2208197 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 41ac=1NEAP&B J:.l,,..l i.i•'',ti+u.:�altnaeoA< 9 Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD5 Sample Date/Time: August 16, 2022 12:59 BCS Sample ID: 2208195 Sample Description: Biosolid Date Received: August 17, 2022 9:43 Amount Submitted:100 mL BCS Bottle % Solids: 34.5 Amount Analyzed: 30.04 g Receipt Temperature: 3.8 deg C Preserved: Yes Analysis Start: August 17, 2022 10:58 Analysis Stop Date: August 23, 2022 8:24 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.8 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD6 Sample Date/Time: August 16, 2022 12:57 BCS Sample ID: 2208196 Sample Description: Biosolid Date Received: August 17, 2022 9:43 Amount Submitted:100 mL BCS Bottle % Solids: 37.8 Amount Analyzed: 29.99 g Receipt Temperature: 3.8 deg C Preserved: Yes Analysis Start: August 17, 2022 10:58 Analysis Stop Date: August 23, 2022 8:24 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2208191, 2208192, 2208193, 2208194, 2208195, 2208196, 2208197 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES tac->aAP6 �' `jr� � M1Cl ttCG3.4 L V Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD7 Sample Date/Time: August 16, 2022 12:55 BCS Sample ID: 2208197 Sample Description: Biosolid Date Received: August 17, 2022 9:43 Amount Submitted:100 mL BCS Bottle % Solids: 39.1 Amount Analyzed: 30.00 g Receipt Temperature: 3.8 deg C Preserved: Yes Analysis Start: August 17, 2022 10:58 Analysis Stop Date: August 23, 2022 8:24 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2208191, 2208192, 2208193, 2208194, 2208195, 2208196, 2208197 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES AM Client: Branch Residuals and Soils Project: 2014-110 Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2208191, 2208192, 2208193, 2208194, 2208195, 2208196, 2208197 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 11!i3G=i !..I;:VS,it,u.: ttltrarpn. '6 I certify that I have examined and I am familiar with the information submitted herein. The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method , however due to the inherent limitations of the methods, microorganisms may avoid detection.' BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. Date: August 23, 2022 Page 7 of 8 Final Report BCS ID 2208191, 2208192, 2208193, 2208194, 2208195, 2208196, 2208197 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 1lrG^i£?i AAB DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set (1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit & the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist for the component. J3 The data are questionable because of improper laboratory or field protocols. L Off scale high. Actual value is known to be greater than value given. N Presumptive evidence for the presence of material. There is an indication that the analyte is present, but the confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. U Indicates that the compound was analyzed for but not detected. The specified component was not detected. The reported value is the method detection limit. V Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that can be determined based on the volume. Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client. Sterility can not be confirmed by BCS. # BCS Lab specific qualifier. See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2208191, 2208192, 2208193, 2208194, 2208195, 2208196, 2208197 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:A7-0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 1t;C=ME{PiAi&B 0 Z Q M �❑ D � M m co CO O CO r ('. d O M LL oNU-ti LL 2 _ m E ,y Rf J z Q1 u U (n M .0 a C� C) \ "2 _ -� .r (�J CCU n� - m y °- W >T G1 Q C C 7 a A c A E a a c Q +, Z d ai D E to m U avi O t Z N d E a m L. O Q ro Z H N m co U WS ZZOZ/LL180 L6L80ZZ LaA sl!OS pue slenp!saa g3ueja 54*6 ZZOZ/L1,/80 96L8OZZ 9aA snot Due sienDisam u:)ueja (satlddy aaZIUVI Hsnu V z �� > sisal uodb-la SM bd3 plopy pue lsea/, Y m XX301seuowopnosd XX301 sn00000jalu3 XX301 ell9uo1681 POylaw oQo ellau01681 a a, w z CL V V Y E c a (odH) eualoeg lunoo aleld Q c w y > 1100 -3 U o m Z' '_' °' 0 0 N 0 61 0 LUJOPIOOlelol 0 dds epauowieg fi •- �- `r i- 1- '� `�° d o 0 m C E H d N _ eAO 41u!wl9H � F°' 0 a` a` wjo;!loo Ieoa3 ET e!pje!E)g wn!puodsoldtioE {= F Sru!A ou91u3 apemllno lelol Zi- t 0 :(f4pads) jaylo �J x m h 2 1!oS4pn--j /p!Ioso!g g T .T 7- �- ::_ is 00 0 jaleM 6u!%uua U- }alemalseM Jolem aoe�nS j u; c � g to to 00 /) ��"ieiadwa`' :(M!oads) sped aol uaza} / aol LI- •T- r y- , pappe alellnso!yl wrn OS uo!loapoo le aml U uogoapOo le Hd paIall!d NOW E a) apsodwoo E v padd!ys siau!eluoo;o 'ON ,= pa!dweS ow!1 N N SV pa!dweg ale(] i iGa C O Q' C t> \ c L V rA i� lC To i co N q t7 E> J y -E C� a i V C 10 m T YZ 0 o � C R � R N r N D O co N VI N Y N r co U o C a Of O Oro O > N _N N co O Marcal Cordova, LLC (Formerly von Drehle Corporation) Cordova, NC City of Rockingham IUP 0015 Oct-22 Biological Consulting Services . . . . . . . . . . . . . . . . . . . . . a. ei�. MaYzei . . . . . . . . . . . . . . . . . . . . . . . . . . MR 1 ... . ........ ... U Mon 6.10 ......... ....... ........... ................. ............................................................... . . .... ....... ............... . . . ............... ... ................. .... . .. ............ . .... ..... ............. ...... ..... . ..... 2209238 9/24/22 < 0.07 0.7 2209239 9/24/22 < 0.07 < 0.7 2209240 9/24/22 < 0.07 < 0.7 2209241 9/24/22 < 0.07 < 0.7 2209242 9/24/22 < 0.07 < 0.6 22092AI 1- 9/24/22 < 0.07 < 0.7 2209244 9/24/22 :5 0.07 :s 0.6 Exceedances All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Monthly Pathogen and Vector Attraction Reduction Forms for Class A option. inc. BIOLOGICAL CONSULTING SERVICES OF NORTH FLOR/DA, INC. September 26, 2022 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd. Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD1, VD2, VD3, VD4, VD5, VD6, VD7 BCS ID: 2209238, 2209239, 2209240, 2209241, 2209242, 2209243, 2209244 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Von Drehle Cordova NC Analysis Method Salmonella EPA 1682; BCS SOP M-4 (ISC17025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, 1 LL,� Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 2209238, 2209239, 2209240, 2209241, 2209242, 2209243, 2209244 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW. MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, A7-DHS:A7-0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 'if3r.`G-MRPa Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD1 Sample Date/Time: September 20, 2022 12:20 BCS Sample ID: 2209238 Sample Description: Biosolid Date Received: September 21, 2022 10:10 Amount Submitted:100 mL BCS Bottle % Solids: 35.6 Amount Analyzed: 30.09 g Receipt Temperature: 2.0 deg C Preserved: Yes Analysis Start: September 21, 2022 11:21 Analysis Stop Date: September 24, 2022 10:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 150.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD2 Sample Date/Time: September 20, 2022 12:24 BCS Sample ID: 2209239 Sample Description: Biosolid Date Received: September 21, 2022 10:10 Amount Submitted:100 mL BCS Bottle % Solids: 37.7 Amount Analyzed: 30.07 g Receipt Temperature: 2.0 deg C Preserved: Yes Analysis Start: September 21, 2022 11:21 Analysis Stop Date: September 24, 2022 10:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: _<0.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 2209238, 2209239, 2209240, 2209241, 2209242, 2209243, 2209244 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES is�r+'iiRP1A&B Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD3 Sample Date/Time: September 20, 2022 12:26 BCS Sample ID: 2209240 Sample Description: Biosolid Date Received: September 21, 2022 10:10 Amount Submitted:100 mL BCS Bottle % Solids: 38.1 Amount Analyzed: 30.08 g Analysis Start: September 21, 2022 11:21 Analyst: Robert Pimentel, B.S. Receipt Temperature: 2.0 deg C Preserved: Yes Analysis Stop Date: September 24, 2022 10:00 Qualifier: U Primary Value: 150.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD4 Sample Date/Time: September 20, 2022 12:32 BCS Sample ID: 2209241 Sample Description: Biosolid Date Received: September 21, 2022 10:10 Amount Submitted:100 mL BCS Bottle % Solids: 39.7 Amount Analyzed: 30.08 g Receipt Temperature: 2.0 deg C Preserved: Yes Analysis Start: September 21, 2022 11:21 Analysis Stop Date: September 24, 2022 10:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2209238, 2209239, 2209240, 2209241, 2209242, 2209243, 2209244 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 11e�MRA - *ed&AS AGCnkC•i S k. 19 (;,tt1 tf'•tu.;t WC.µ'u�e Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VDS Sample Date/Time: September 20, 2022 12:34 BCS Sample ID: 2209242 Sample Description: Biosolid Date Received: September 21, 2022 10:10 Amount Submitted:100 mL BCS Bottle % Solids: 41.0 Amount Analyzed: 30.01 g Receipt Temperature: 2.0 deg C Preserved: Yes Analysis Start: September 21, 2022 11:21 Analysis Stop Date: September 24, 2022 10:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit.for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD6 Sample Date/Time: September 20, 2022 12:38 BCS Sample ID: 2209243 Sample Description: Biosolid Date Received: September 21, 2022 10:10 Amount Submitted:100 mL BCS Bottle % Solids: 37.9 Amount Analyzed: 30.09 g Receipt Temperature: 2.0 deg C Preserved: Yes Analysis Start: September 21, 2022 11:21 Analysis Stop Date: September 24, 2022 10:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 150.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2209238, 2209239, 2209240, 2209241, 2209242, 2209243, 2209244 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, A7-DHS:A7-0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD7 Sample Date/Time: September 20, 2022 12:42 BCS Sample ID: 2209244 Sample Description: Biosolid Date Received: September 21, 2022 10:10 Amount Submitted:100 mL BCS Bottle % Solids: 40.2 Amount Analyzed: 30.09 g Receipt Temperature: 2.0 deg C Preserved: Yes Analysis Start: September 21, 2022 11:21 Analysis Stop Date: September 24, 2022 10:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2209238, 2209239, 2209240, 2209241, 2209242, 2209243, 2209244 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924. ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES tl &G=I4IR/AAw I. Client: Branch Residuals and Soils Project: Von Drehle Cordova NC Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical -Quantitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2209238, 2209239, 2209240, 2209241, 2209242, 2209243, 2209244 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES _ilac=_{yiR�a A &B ' •<c noo��cu I certify that I have examined and I am familiar with the information submitted herein. The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. Date: September 26, 2022 Page 7 of 8 Final Report BCS ID 2209238, 2209239, 2209240, 2209241, 2209242, 2209243, 2209244 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES AIjs`1G Nk�RPi r ' DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set (1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit & the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist for the component. J3 The data are questionable because of improper laboratory or field protocols. L Off scale high. Actual value is known to be greaterthan value given. N Presumptive evidence for the presence of material. There is an indication that the analyte is present, but the confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. U Indicates that the compound was analyzed for but not detected. The specified component was not detected. The reported value is the method detection limit. V Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that can be determined based on the volume. 7 Data are rejected 'and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client. Sterility can not be confirmed by BCS. # BCS Lab specific qualifier. See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2209238, 2209239, 2209240, 2209241, 2209242, 2209243, 2209244 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES s ilaC-MRA z° (sallddy aa3) .Ldl Hsna I I I L Ll c°n :�a410 Q M 'o 0 ualmol .N C co u7 L] � o i ro N N sisal HOdb-IH 9L9I Vd3 �p o M PIoW Pue 19e9,, in in m N N XX301seuowopnasd N c T c a m C)C- T m N !9 N XX301 sn00000J9lu3 N to N K f0 cm 'o J� N> N N N> N cm Cq N N M XX301 eilauol6a� O M LL. :� O1 N cm Po41aw 000 ellaua6a� •O J c H t N a;r N o N L. cc (0dH) eualoeg luno0 aleld � °�' 7 �} m` m m m` �O •N M n q ? r ll00'3 Z N r �. wMdlloO lelol `` ro• Ct dds ellauowles N C v en0 4lulwl8H wio}lloo leoad 0 p _ 0 o elpJelJ g wnlppodsoldti0 lE CL D sruln oualu3 algejnllnO lelol ❑ tih a '\J — :(Apoads) jayln Li LL O U W O 1- D U u_ O Z S U i K-, x (aloJlo) uosln pn'j pllosoll JaleM 6uhluu0 V T 3 J� lL jalemalseM jalem aoelJn! dsoloed ool uazoil / a- pappe alellnsol4l wnipo! Ill y uogoelloo le ainleiadwa E -,;i- p �ca�z d } v° c m Y 0 m tl c d E � _ c. � n Ucai in ai s O G ` 0 N at 511 0 R ►"' ua.mm E E= L: i= h r -- O LL C, "Z v rn Z OL OL ZZDZ/4Z160 uolloalloo 1e Hd N �� rn co m i�VZ60ZZ w w`'� �, u- Lan paJa11!3 MY w sllos pue slenplsaa 43ue'8 �.. ch 0 ` ' O V apsodwo0 "o 0 y 0 c eJ padd14s sJauleluoo to'ON • a • -rcr r paldwes awll 3 n ,., m J -G tl' c Paldweg olep � �'� r�; • ~rs � i _ „ •� m` L- m y N rn .n c E a m -v Q m +� m Z N m E in N m a .r t7 d C O N L •C o Z c •- 0! V •O G• _d 47 Q. H N � m °- eEa O m o Z E- E !n > N N C fa N N N tr d U O v C CD 0 N 9 0 m o veq N 0 w o N L > N N N N 61 O C tj N C t� 2 O) C t0 d a cn m o° U U m D � o O N <<. E Cs^ - .a v a7 t y .7 Q C cu cr Marcal Cordova, LLC (Formerly von Drehle Corporation) Cordova, NC City of Rockingham IUP 0015 Nov-22 Biological Consulting Services MAI. y a ue: C. ....... .............. . ............. . ..... :p-9 ;;N:*:4': Alm p 2210320 10/28/22 < 0.07 :S 0.7 2210321 10/28/22 < 0.07 :5 0.7 2210322 10/28/22 < 0.07 < 0.7 2210323 10/28/22 < 0.07 :S 0.6 2210324 10/28/22 < 0.07 < 0.7 2210325 10/28/22 < 0.07 < 0.7 2210326 10/28/22 :S 0.07 < 0.6 . . . . . . . . . . . . . . . . . . . . . ............ ............ Exceedances . All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Monthly Pathogen and Vector Attraction Reduction Forms for Class A option. 3inc. BIOLOGICAL CONSULTING SERVICES ✓ OF NORTH FLORIDA, INC. November 01, 2022 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd. Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD1, VD2, VD3, VD4, VD5, VD6, VD7 BCS ID: 2210320, 2210321, 2210322, 2210323, 2210324, 2210325, 2210326 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Von Drehle Cordova NC Analysis Method Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 2210320, 2210321, 2210322, 2210323, 2210324, 2210325, 2210326 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Paci Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD1 BCS Sample ID: 2210320 Date Received: October 25, 2022 9:56 Amount Analyzed: 3.01E+01 g Analysis Start: October 25, 2022 10:50 Analyst: Nelson Luque, B.S. Sample Date/Time: October 24, 2022 13:36 Sample Description: Biosolid Amount Submitted:100 mL BCS bottle % Solids: 36.5 Receipt Temperature: 0.2 deg C Preserved: Yes Analysis Stop Date: October 28, 2022 10:45 Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD2 BCS Sample ID: 2210321 Date Received: October 25, 2022 9:56 Amount Analyzed: 3.01E+01 g Analysis Start: October 25, 2022 10:50 Analyst: Nelson Luque, B.S. Sample Date/Time: October 24, 2022 13:39 Sample Description: Biosolid Amount Submitted:100mL BCS bottle % Solids: 36.6 Receipt Temperature: 0.2 deg C Preserved: Yes Analysis Stop Date: October 28, 2022 10:45 Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 2210320, 2210321, 2210322, 2210323, 2210324, 2210325, 2210326 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ti 5�/•�„ M� 'O HaG-MRA Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD3 BCS Sample ID: 2210322 Date Received: October 25, 2022 9:56 Amount Analyzed: 3.01E+01 g Analysis Start: October 25, 2022 10:50 Sample Date/Time: October 24, 2022 13:42 Sample Description: Biosolid Amount Submitted:100 mL BCS bottle % Solids: 37.3 Receipt Temperature: 0.2 deg Preserved: Yes Analysis Stop Date: October 28, 2022 10:45 Analyst: Nelson Luque, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mI- sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD4 BCS Sample ID: 2210323 Date Received: October 25, 2022 9:56 Amount Analyzed: 2.99E+01 g Analysis Start: October 25, 2022 10:50 Sample Date/Time: October 24, 2022 13:45 Sample Description: Biosolid Amount Submitted:100 mL BCS bottle % Solids: 42.2 Receipt Temperature: 0.2 deg Preserved: Yes Analysis Stop Date: October 28, 2022 10:45 Analyst: Nelson Luque, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mI- sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2210320, 2210321, 2210322, 2210323, 2210324, 2210325, 2210326 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD5 Sample Date/Time: October 24, 2022 13:48 BCS Sample ID: 2210324 Sample Description: Biosolid Date Received: October 25, 2022 9:56 Amount Submitted:100 mL BCS bottle % Solids: 36.6 Amount Analyzed: 2.99E+01 g Receipt Temperature: 0.2 deg C Preserved: Yes Analysis Start: October 25, 2022 10:50 Analysis Stop Date: October 28, 2022 10:45 Analyst: Nelson Luque, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD6 Sample Date/Time: October 24, 2022 13:51 BCS Sample ID: 2210325 Sample Description: Biosolid Date Received: October 25, 2022 9:56 Amount Submitted:100 mL BCS bottle % Solids: 35.7 Amount Analyzed: 2.99E+01 g Receipt Temperature: 0.2 deg C Preserved: Yes Analysis Start: October 25, 2022 10:50 Analysis Stop Date: October 28, 2022 10:45 Analyst: Nelson Luque, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2210320, 2210321, 2210322, 2210323, 2210324, 221032S, 2210326 BCS LABORATORIES, INC. — GAINESVILLE 4609 NVV 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES �iS3CA16 Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD7 Sample Date/Time: October 24, 2022 13:54 BCS Sample ID: 2210326 Sample Description: Biosolid Date Received: October 25, 2022 9:56 Amount Submitted:100 mL BCS bottle % Solids: 40.7 Amount Analyzed: 3.00E+01 g Receipt Temperature: 0.2 deg C Preserved: Yes Analysis Start: October 25, 2022 10:50 Analysis Stop Date: October 28, 2022 10:45 Analyst: Nelson Luque, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2210320, 2210321, 2210322, 2210323, 2210324, 2210325, 2210326 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL. WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES A&B Client: Branch Residuals and Soils Project: Von Drehle Cordova NC Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2210320, 2210321, 2210322, 2210323, 2210324, 2210325, 2210326 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 1-2422, PADEP: 68-03950, AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES JABll� I certify that I have examined and I am familiar with the information submitted herein. The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. Date: November 01, 2022 Page 7 of 8 Final Report BCS ID 2210320, 2210321, 2210322, 2210323, 2210324, 2210325, 2210326 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 1-2422, PADEP: 68-03950, AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES }i$E'1::1�F1 � -1� +ccnenrr c o ?` ........_.ass DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set (1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit &the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist for the component. J3 The data are questionable because of improper laboratory or field protocols. L Off scale high. Actual value is known to be greaterthan value given. N Presumptive evidence forthe presence of material. There is an indication thatthe analyte is present, butthe confirmation requirement was not met. 0 Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. u Indicates that the compound was analyzed for but not detected. The specified component was not detected. The reported value is the method detection limit. V Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that can be determined based on the volume. 7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client. Sterility can not be confirmed by BCS. # BCS Lab specific qualifier. See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2210320, 2210321, 2210322, 2210323, 2210324, 2210325, 2210326 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES I11ac.At" 0 Z C_ u� too � M m M 4 O M LL O y J LL � O �O U m SI ?� —� h M E ti in CA 0 T V o •,,finn Cn W � V A ^<i W (sa!iddy aaj) ldl ualmoJ .N slsai NOdb-.LH 9M dd3 plow pue lseaA XX3(]1seuowopnasd XX3(]1 sn0003aalu3 XX3(]1 eilauol6a-1 Po4law 0(30 ellau0160-1 ((]dH) eualoeg Juno(] aleld !103 '3 wJOJ!lo(] lelol : dds eilauowleS en0 ululwlDH wjoJ!loo IL-aad e!pje!Z) ig wn!puoasolamol 1 w a � c snjln oualu3 algeinlln(] lelo. M (tl ILL ja41( OU � x (aloj!o) l!os�l !loso!l uj sU �aleMalseM Cry � jalem ooepn<, 00 oft :(fq!oads) ja41( U- d U < U. O W y pappe alelInso!yl wn!po( = rn � p uo!loalloo le amlejedwa v U (� Z R uolioalioo le HI w�* M u. yt L' paall!j Plaid No �" apsodwo(] o p -0 -;li, Cj gejJ U J ,a 'ON padd!ys s-181-11eluoo Jo Qj t� paldweg awll peldweS ale(] i N 0 .y �N o1 1V E a C 10 f0 Z N � � � d c E m fn W •o y 0 w M Ua� 0 0 t 2 m a c wo � C ,a In Ea` m °1 �' E i° � N N m W Z d f E O M N N O o o A t� M N Q N D > v j N U,, d N N O a. u C q ow a O N C O N tII N N N fn N z y N C r Cry In N O! N N M N 7 Q O ONo V , C UI , N UI N N7 N_ coellN O O r t � U u u C m � m se:s ZZOZ/9Z/OL MOM LaA slog pue slenplsaa youeJg U� 15� � Z 1 d U } C m Y O Q V N V - Y C N tl 5 R r u to ISO P ad v p, o CCi m f' E N m m'0 �p5 m I-- � � � o k Udax 0 0 o O O N �...� +.. 4 N N 4) N C., Q' q r c m a H •� c 0 o in u a� C m � > > U U CD w F- P a a L y cr C CD w Mareal Cordova, LLC [Formerly von ❑rehle Corporation] Cordova, NC City of Rockingham IUP 0015 Dec-22 Biological Consulting Services iiaiiiii.......................................................:.............................................:................................. . to tial red'rmr' Y............... ;:e a m©ne1aSEca.riiar aXu . S ........................................................... . V alne Saymoriela Y...................................... .:.:.:.:.:::.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:..:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.::.:.:.:.:.:.:. :.......:.......:.......:.......:.......:......:............:................p.................................................................p............1 ' P i `sir: inl a 1N.T Nii er}. .. Y ..... ............ . 2211256 11/29/22 < 0.07 :S 0.7 2211257 11/29/22 < 0.07 < 0.8 2211258 11/29/22 < 0.07 < 0.8 2211259 11/29/22 0.07 0.80 2211260 11/29/22 < 0.07 < 0.7 2211261 11/29/22 < 0.07 < 0.7 2211262 11/29/22 < 0.07 :5 0.7 Exceedances All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Monthly Pathogen and Vector Attraction Reduction Forms for Class A option. inc, BIOLOGICAL CONSULTING SERVICES OF NORTH FLOR/DA, INC. December 02, 2022 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd. Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD1, VD2, VD3, VD4, VD5, VD6, VD7 BCS ID: 2211256, 2211257, 2211258, 2211259, 2211260, 2211261, 2211262 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Von Drehle Cordova NC Analysis Method Salmonella EPA 1682; BCS SOP M-4 (IS017025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 2211256, 2211257, 2211258, 2211259, 2211260, 2211261, 2211262 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL. WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES il�c=MtA r Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD1 Sample Date/Time: November 21, 2022 12:36 BCS Sample ID: 2211256 Sample Description: biosolid Date Received: November 22, 2022 9:50 Amount Submitted:100 mL BSC bottle % Solids: 38.3 Amount Analyzed: 2.99E+01 g Receipt Temperature: 4.0 deg C Preserved: Yes Analysis Start: November 22, 2022 10:05 Analysis Stop Date: November 29, 2022 10:00 Analyst: Nelson Luque, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD2 Sample Date/Time: November 21, 2022 12:39 BCS Sample ID: 2211257 Sample Description: biosolid Date Received: November 22, 2022 9:50 Amount Submitted:100 ml BSC bottle % Solids: 33.0 Amount Analyzed: 3.01E+01 g Receipt Temperature: 4.0 deg C Preserved: Yes Analysis Start: November 22, 2022 10:05 Analysis Stop Date: November 29, 2022 10:00 Analyst: Nelson Luque, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.8 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 2211256, 2211257, 2211258, 2211259, 2211260, 2211261, 2211262 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL. WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 1aC;i1AAJM R '_ ��•.= .. c e n c o: c o Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD3 Sample Date/Time: November 21, 2022 12:42 BCS Sample ID: 2211258 Sample Description: biosolid Date Received: November 22, 2022 9:50 Amount Submitted:100 ml BSC bottle % Solids: 33.4 Amount Analyzed: 3.01E+01 g Receipt Temperature: 4.0 deg C Preserved: Yes Analysis Start: November 22, 2022 10:05 Analysis Stop Date: November 29, 2022 10:00 Analyst: Nelson Luque, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: !90.8 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD4 Sample Date/Time: November 21, 2022 12:45 BCS Sample ID: 2211259 Sample Description: biosolid Date Received: November 22, 2022 9:50 Amount Submitted:100 ml BSC bottle % Solids: 36.8 Amount Analyzed: 2.99E+01 g Receipt Temperature: 4.0 deg C Preserved: Yes Analysis Start: November 22, 2022 10:05 Analysis Stop Date: December 01, 2022 12:00 Analyst: Nelson Luque, B.S. Qualifier: None Primary Value: 0.07 Salmonella MPN/mL sample analyzed Secondary Value: 0.8 Salmonella MPN/4 dry grams Analysis Notes: None Page 3 of 8 Final Report BCS ID 2211256, 2211257, 2211258, 2211259, 2211260, 2211261, 2211262 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES �lac_1 Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD5 BCS Sample ID: 2211260 Date Received: November 22, 2022 9:50 Amount Analyzed: 3.01E+01 g Analysis Start: November 22, 2022 10:05 Sample Date/Time: November 21, 2022 12:48 Sample Description: biosolid Amount Submitted:100 ml BSC bottle % Solids: 35.9 Receipt Temperature: 4.0 deg C Preserved: Yes Analysis Stop Date: November 29, 2022 10:00 Analyst: Nelson Luque, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD6 BCS Sample ID: 2211261 Date Received: November 22, 2022 9:50 Amount Analyzed: 3.00E+01 g Analysis Start: November 22, 2022 10:05 Analyst: Nelson Luque, B.S. Sample Date/Time: November 21, 2022 12:51 Sample Description: biosolid Amount Submitted:100 ml BSC bottle % Solids: 37.6 Receipt Temperature: 4.0 deg C Preserved: Yes Analysis Stop Date: November 29, 2022 10:00 Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2211256, 2211257, 2211258, 2211259, 2211260, 2211261, 2211262 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES A&Bilac:r�A Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD7 Sample Date/Time: November 21, 2022 12:54 BCS Sample ID: 2211262 Sample Description: biosolid Date Received: November 22, 2022 9:50 Amount Submitted:100 ml BSC bottle % Solids: 36.9 Amount Analyzed: 3.01E+01 g Receipt Temperature: 4.0 deg C Preserved: Yes Analysis Start: November 22, 2022 10:05 Analysis Stop Date: November 29, 2022 10:00 Analyst: Nelson Luque, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2211256, 2211257, 2211258, 2211259, 2211260, 2211261, 2211262 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW. MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES is lI$G_i�A Client: Branch Residuals and Soils Project: Von Drehle Cordova NC Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2211256, 2211257, 2211258, 2211259, 2211260, 2211261, 2211262 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE W` R1R,ITTEN CONSENT OF BCS LABORATORIES 4i3�>''A10AB c o I certify that I have examined and I am familiar with the information submitted herein. The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. Date: December 02, 2022 Page 7 of 8 Final Report BCS ID 2211256, 2211257, 2211258, 2211259, 2211260, 2211261, 2211262 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 1-2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 11C NSA B DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set (1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit & the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist for the component. J3 The data are questionable because of improper laboratory or field protocols. L Off scale high. Actual value is known to be greaterthan value given. N Presumptive evidence forthe presence of material. There is an indication that the analyte is present, but the confirmation requirement was not met. 0 Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. U Indicates that the compound was analyzed for but not detected. The specified component was not detected. The reported value is the method detection limit. V Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that can be determined based on the volume. 7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client. Sterility can not be confirmed by BCS. # BCS Lab specific qualifier. See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2211256, 2211257, 2211258, 2211259, 2211260, 2211261, 2211262 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 1-2422, PADEP: 68-03950, AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ,,,,.tab: 1i3C_I�EA110AB 4 O Z El a �u 'to- cn CM y ._ m G) cm M 0 r• O M L. O 4-1 LL r.- N 2 -� 0 t- m m •� ti M E J Z d tn U 0 to p 0 o - o !- a► O W v CL c W u c 0 x m L Iq ti (sa!Iddy eaj) IVI ! elmol sisal iIodb-j-8 S191. 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