NC0026051_Pretreatment_Annual_Report_20230228

Pretreatment Annual Report
POTW: Durham County Triangle WWTP
NPDES #: NC0026051
WWTP: Triangle Wastewater Treatment Plant
Reporting Period: January 1, 2022 to December 31, 2022
Person to contact
Regarding this report: Amy Moore
Phone#: [phone]
I certify that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel
properly gather and evaluate the information submitted. Based upon my inquiry of the
person or persons who manage the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and
belief, true, accurate and complete.
o Jai laoa
Stephanie Brixey Date
Deputy Director of E&ES/ OTW Director

Pretreatment Annual Report
POTW: Durham County Triangle WWTP
NPDES #: NC0026051
WWTP: Triangle Wastewater Treatment Plant
Reporting Period: January 1,2022 to December 31, 2022
Person to contact
Regarding this report: Amy Moore
Phone#: [phone]
I certify that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel
properly gather and evaluate the information submitted. Based upon my inquiry of the
person or persons who manage the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and
belief,true, accurate and complete.
Amy Mo D to
Laboratory& Compliance Manager

DURHAM COUNTY
PRETREATMENT ANNUAL REPORT
NARRATIVE
GENERAL PROGRAM INFORMATION:
Durham County submitted revisions to the Enforcement Response Plan (ERP) on
February 11, 2020, in response to the Dental Amalgam Rule, that was approved February
13, 2020. Durham County submitted a revision of the Long Term Monitoring Plan
(LTMP) to the Division on September 5, 2013, that was approved by the Division on
October 8, 2013. Durham County submitted a revision of the Sewer Use Ordinance
(SUO) to the Division on December 18, 2012. A letter was received from the Division
on January 28, 2013, requesting additional information. The additional information was
submitted March 21, 2013 and approved by the Division on April 3, 2013. The Industrial
Waste Survey (IWS) was submitted to the Division on March 31, 2021. The Division
requested additional information that was submitted on May 3, 2021. The IWS was
approved by the Division on May 5, 2021. Durham County submitted a revision of the
Headwork's Analysis (HWA) on March 16, 2018, that was approved by the Division on
May 2, 2018.
The "Pretreatment Program Info Database" sheet for Durham County contained multiple
errors. The errors have been highlighted and detailed in the attached document titled
"2302 Durham_County_highlighted corrections". NPDES permit number NCO026051
was effective on October 1, 2022 and will expire on April 30, 2027. Durham County and
the Triangle Wastewater Treatment Plant has 14 SIU's and 13 CIU's. The allocation table
submitted to the Division in October 2022 with the Cintas permit renewal titled "AT
221031 Cintas Renewal" has a % Design mgd SIU permitted as 12 and Permitted SILT
flow(mgd) as 1.4405.
The attached SNC summary emailed to Durham County on January 20, 2023, contains
multiple errors. Cintas, DC-037, does not have a history of SNC. United Therapeutics,
DC-053, was in SNC for acetone in the second semiannual period of 2020 only.
Phononic, DC-075, was in SNC for reporting in the first semiannual period of 2015 and
nickel for the first semiannual period of 2022. PowerSecure, DC-095, was in SNC for
reporting in the first semiannual period of 2020 and the second semiannual period of
2021. Aurobindo, DC-089, was in SNC for acetone for the second semiannual period of
2019.
GENERAL PERMIT INFORMATION:
During the reporting period the following Industrial User Permits were issued, modified,
or renewed:

• AstraZeneca, IUP DC-078 was renewed with an effective date of January 1, 2022.
The permit was received by the Division of Environmental Quality for streamline
review on December 29, 2021 and approved on February 23, 2022.
• Biogen, IUP DC-080 was modified with an effective date of August 1, 2022. The
permit was received by the Division for streamline review on July 27, 2022 and
approved on September 29, 2022.
• Cintas, IUP DC-037 permit application for renewal was received by Durham
County on May 6, 2022. The permit was renewed with an effective date of
November 2, 2022. The permit was received by the Division for streamline
review on December 14, 2022 and approved on January 13, 2023.
• Cree, IUP DC-076 was modified to reflect a name change, to Wolfspeed Durham,
with an effective date of August 23, 2022. The permit was received by the
Division for streamline review on September 27, 2022 and approved on
November 8, 2022.
• Cree RTP, IUP DC-040 was modified to reflect a name change to Wolfspeed RTP
with an effective date of August 23, 2022. The permit was received by the
Division for streamline review on September 27, 2022, and approved November
8, 2022.
• PowerSecure, IUP DC-095 was modified with an effective date of June 1, 2022.
The permit was modified for flow reporting requirements, the requirement for a
certified operator to maintain the pretreatment units and to require a pretreatment
system log. The permit was received by the Division for streamline review on
May 31, 2022 and was approved on July 26, 2022.
SIU INFORMATION:
1. AstraZeneca (IUP DC-078) — AstraZeneca was issued a Notice of Violation on
February 21, 2023 for failure to monitor for low-level mercury in the second
semi-annual period of 2022. The Notice of Violation was issued in accordance
with the ERP.
2. Aurobindo USA (IUP DC-089)—No permit violations occurred at this facility.
3. Biogen (IUP DC-080) — No permit violations occurred at this facility. Biogen
submitted an Authorization to Construct letter on August 22, 2022 to install a new
flow meter. Durham County granted the ATC on September 15, 2022. The new
bubbler flow meter was installed and calibrated on September 28, 2022.
4. Cintas (IUP DC-037) — Cintas was issued a Notice of Violation on May 3, 2022
for late reporting of the monthly flow for February 2022. February 2022 flow

report was received on April 7, 2022. Cintas was issued a Notice of Violation on
February 16, 2023 for failure to sample chloride for the second semi-annual
period of 2022. Cintas was issued a Notice of Violation on February 22, 2023 for
exceeding the monthly limit of oil and grease (polar) for the month of December
2022. The Notices of Violation were issued in accordance with the ERP.
S. Micross (IUP DC-085)—No permit violations occurred at this facility
6. MP Pharma Services (IUP DC-114) — MP Pharma Services, Inc. exceeded the
monthly flow for January-March 2022. A Notice of Violation was not issued for
January-March 2022 because it was determined by the flow meter manufacturer
that the magnetic flow meter was giving erroneous reading due to the low flow
through the pipe and meter. Flow meter readings were compared against water
meter reading for the site to confirm the manufacturer assessment. The
manufacturer reset the flow meter and MP Pharma Services returned to
compliance. Durham County received a letter from MP Pharma Services on
March 7, 2022 detailing the non-compliance and corrective action.
7. Phononic (IUP DC-075) — Phononic was issued a Notice of Violation on June
16, 2022 for failure to monitor monthly parameters for bismuth, nickel and
tellurium in April 2022. Phononic was issued a Notice of Violation on August 31,
2022 for exceeding the monthly limit of nickel for April-June 2022. Phononic was
in Significant Noncompliance for violating the Technical Review Criteria for the
first semi-annual period of 2022. Phononic was issued a Notice of Violation on
October 17, 2022 for late reporting of August 2022 monthly parameters, and
exceeding the monthly limit for flow for July through September. Phononic was
issued a Notice of Violation on October 17, 2022 for exceeding the monthly limit
for nickel in July and August 2022. Phononic responded to all violations and
conducted all required sampling. Phononic hired a consultant to address the nickel
violations and increased nickel monitoring to return to compliance for the second
semi-annual period of 2022. Phononic optimized the nickel filtration unit by
adding bone char to absorb nickel and reduce nickel in the discharge. Phononic is
collaborating with the property owner and Durham County Utilities to address the
increased monthly average flow. The Notices of Violation were issued in
accordance with the ER-P.
8. PowerSecure (IUP DC-095)—No permit violations occurred at this facility.
9. SCM Metal (IUP DC-005)—No permit violations occurred at this facility.
10. Tergus Pharma, IUP (DC-115) — Tergus Pharma was issued a Notice of
Violation for late reporting of April 2022 monthly average flow on June 16, 2022.
Tergus Pharma was issued a Notice of Violation on February 16, 2022 for late
reporting of November and December 2022 monthly average flow. The Notices of
Violation were issued in accordance with the ER-P.

11. TriPharm Services (IUP DC-106) — TriPharm Services was issued a Notice of
Violation on May 3, 2022 for late reporting of February and March flow.
TriPharm hired a consulting firm to troubleshoot the discrepancies between
incoming water usage and discharge flow. The City of Durham was not charging
for all incoming water. TriPharm has purchased additional flow capacity. The
Notice of Violation was issued in accordance with the ERP.
12. United Therapeutics (IUP DC-053) — No permit violations occurred at this
facility.
13. Wolfspeed Durham (IUP DC-0761 — No permit violations occurred at this
facility.
14. Wolfspeed RTP (IUP DC-040) No permit violations occurred at this facility.
WASTE REDUCTION ACTIVITIES:
The Triangle Wastewater Treatment Plant participates in the following waste reduction
activities:
1. Recycling of plastic, glass, aluminum, newspaper and corrugated cardboard.
2. Recycling of used pens, markers, mechanical pencils, highlighters, scotch tape
dispensers and cores, and ink jet cartridges.
3. Recycling of used batteries.
4. Secondary containment for bulk storage of chemicals.
5. Recycling of used oil.
6. Reduction of paper generation.
7. Reduction of power consumption via automation. Logic controls are present that
operates the rotors used for aeration as well as the intensity of the Ultraviolet
Disinfection System.
Permit applications and inspection reports were reviewed for industrial waste reduction
activities information. The codes used in Part V, Waste Reduction Information of the
Industrial Waste Survey and Permit Application are used here. A copy of the code and
description is attached for reference.
Indusia Name Code or description of waste reduction activity
AstraZeneca None
Aurobindo W 19, W34, W36, W55, W62, W71
Biogen W 13, W33, W34, W36, W39, W99
Cintas W 13

Micross W21, W23, W33, W34, W36
MP Pharma None
Phononic W21, W33, W52, W67
PowerSecure W 13, W24, W31, W32, W33, W34, W36, W52
SCM W39
Tergus Pharma None
TriPharm Services W 13, W21, W24, W31, W32, W36, W39, W52, W54, W62
United Therapeutics W21, W24, W25, W33, W34, W36, W52, W54, W55
Wolfspeed Durham W24, W32, W33, W34, W36, W51, W54, W55, W67
Wolfspeed RTP W24, W32, W33, W34, W36, W51, W54, W55
WASTE REDUCTION CODES:
W 13 Improved maintenance scheduling recordkee in , or procedures
W 14 Changed production schedule to minimize equipment and feedstock
changeovers
W 19 Other changes in operating ractices (explain briefly in comments
W21 Instituted procedures to ensure that materials do not stay in inventory
beyond shelf-life
W22 Began to test outdated material-continue to use if still effective
W23 Eliminated shelf-life requirements for stable materials
W24 Instituted better labeling procedures
W25 Instituted clearinghouse to exchange materials that would otherwise
be discarded
W29 Other changes in Inventory control(explain briefly in comments)
W31 Improved storage or stacking procedures
W32 Improved procedures for loading, unloading and transfer operations
W33 Installed overflow alarms or automatic shutoff valves
W34 Installed secondary containment
W35 Installed vapor recovery systems

W36 Implemented inspection or monitoring program of potential spill or
leak sources
W39 Others ill and leak prevention(explain briefly in comments
W41 Increased purity of raw materials
W42 Substituted raw materials
W49 Other raw material modifications (explain briefly in comments
W51 Instituted recirculation within a process
W52 Modified equipment, layout, or piping
W53 Use of a different process catalyst
W54 Instituted better controls on operating bulk containers to minimize
discarding of empty containers
W55 Changed from small volume containers to bulk containers to
minimize discarding of empty containers
W58 Other process modifications (explain briefly in comments)
W59 Modified stripping/cleaning equipment
W60 Changed to mechanical stripping/cleaning devices (from solvents or
other materials
W61 Changed to aqueous cleaners from solvents or other materials)
W62 Reduced the number of solvents used to make waste more amenable
to recycling
W63 Modified containment procedures for cleaning units
W64 Improved draining procedures
W65 I Redesigned parts racks to reduce drag out
W66 Modified or installed rinses stems
W67 Improved rinse equipment design
W68 Improved rinse equipment operation
W71 Other cleaning and degreasing operation(explain briefly in
comments
W72 Modified spray systems orequipment
W73 Substituted coating materials used
W74 Improved application techniques
W75 Changed from spray to others stem
W78 Other surface preparation and finishing (explain briefly in comments
W81 Changed product specifications
W82 Modified design or composition of product
W83 I Modified packaging

W89 Other product modifications (explain briefly in comments)
W99 Other(specify in comments
ADDITIONAL INFORMATION:
Phononic was in SNC for exceeding the Technical Review Criteria for nickel in the first
semi-annual period of 2022.
bioMASON, Durham County local IUP number DCL-106, was in Significant
Noncompliance for failure to sample for the second semi-annual period of 2022.
The Public Notice and Proof of publication in The Herald Sun is included with this
submittal.

Pretreatment Program Info Database printed on: 1/19/2023
for Program Name Durham County IWC %at 7Q10 100.00
WWTP Name Triangle Stream Information
Program Approval Date 07/06/1995 7Q10 Flow cfs/mgd 0 / 0.00
Pretreatment Status 1Q10 Flow cfs/mgd 0.00 / 0.00
Full Stream Classification ws-iv
Region RRO Basin Number CPF05
County Durham Receiving Stream Name NORTHEAST CREEK
NPDES Number NC0026051
NPDES Effective Date Last PAR Rec 02/28/2022 PAR Due Date03/01/2023 mercury
12/01/2011 1631
NPDES Expire Date Current Fiscal 03/04/2020 required
p� 04/30/2016 Year PCI Done
POTW is Primary WWTP TRUE Last Audit on 09/15/2021 Audit Year Nex125/26 yes
Design Flow mgd 12.0000 % Design mgd is SIU permitted 13.17 Permitted SIU flow(mgd) [Pt_SIU) 1.58051
WWTP SIU's 13 Program SIUs 13
WWTP CIU's 11 Program CIUs 111 HWA LTMP IWS SUO ERP
date Inactive Date Next Due 04/01/2023 05/04/2026
Date Received by DWR 03/16/2018 09/05/2013 03/31/2021 12/20/2012 02/11/2020
Date Approved 05/02/2018 10/08/2013 05/05/2021 04/03/2013 02/13/2020
Adopt Date Required
Date Adopted 03/11/2013
01
Info in this Box from Pt Contacts
Date Date Date
PT—Pro Attended Attended Attended
Formal Name g.Prime Phonel ext Fax HWA Wksp UP Wksp PAR Wksp
Ms. Stephanie Brixey 1 919-560-9034 L 1919-544-8590 11 6/22/2011 1 1/23/2007
[e-mail] Deputy Director of E&ES/POTW 15926 NC Hwy 55 E IFT713
Ms.Amy Moore Prim 919-560-9035 L 1919-544-8590 11 2/9/2012 1 4/18/2012 1 1/19/2012
[e-mail] LABORATORY&COMPLIANCE
Ms. Laura Melton 919-560-9042 919-544-8590
[e-mail] Pretreatment Project Coordinator 15926 Highway 55 East 27713
Pretreatment Related NOVs from DWQ DWR Central Office Contact JPretreatment Staff
3/24/2004 PAR-failure to enforce-nov/orders for SNC DWR Regional Contact ICheng Zhang

hist
IIVV REPORT
Durham County
2016 2017 2018 2019 2020 2021 2022
1st half 2nd half 1st half 2nd half 1st half 2nd half 1st half 12nd half 1st half 12nd half 1st half 2nd half 1st half 12nd half
Cintas Corporation PreviousNames:
IUP# DC-037 Pipe# 001 SIU Word Description:
laundry,Industrial
IUP Status:Active
Mercury
Oil Grease
United Therapeutics Corporation PreviousNames:
IUP# DC-053 Pipe# 001 SIU Word Description:
Subpart D&E
IUP Status:Active
Acetone I I I Ix X I X XI X
pH I I I I I I I
Phononic PreviousNames:
IUP# DC-075 Pipe# 001 SIU Word Description:
Subpart A
IUP Status:Active
Reporting
Aurobindo Pharma USA PreviousNames:
IUP# DC-089 Pipe# 001 SIU Word Description:
439 D+E
IUP Status:Active
Acetone I I I Ix I I I
PowerSecure PreviousNames:
IUP# DC-095 Pipe# 001 SIU Word Description:
metal finisher
IUP Status:Active
Reporting I I I I X I Ix I
An'X'in a semi-annual period indicates snc for the period for the respective parameter.
This information is compiled from man
PRINTED ON: 1/19/2023 p Y sources,and has not been verified. PAGE 37
Contact the local pretreatment coordinator or state pretreatment staff if errors are noted.

Chapter 9, PAR Guidance
Pretreatment Performance Summary (PPS)
1. Pretreatment Town Name. Durham County
2. "Pri mary" N PDES N umber NC00 26051 TorCol
lu n
or Non D i scharge Permit#if applicable=> use only
EPA
WENDB
3. PAR begin Date, pl ease enter 01/01/yy or 07/01/yy 3. => 1/1/2022 PSSD
4. PAR end Date, pleaseenter 06/30/yy or 12/31/yy 4. => 12/31/2022 PSED
5. Total number of SI Us, i ncl udes Cl Us 5. => 14 SIUs
6. Number of Cl Us 6. => 13 Clus
7. Enter the Higher Number, either (7a) or (7b) here=> 0 NOIN
7a. Number of SI Us not sampled by POTW 7a. => 0
7b. Number of SIUs not inspected by POTW 7b. => 0
8. Number of SlUswith no IUP, or with an expired IUP 8. => 0 NOCM
9. Total Number of SIUs in SNC due to either I U Reporting violations or
IUP Limit violations. To avoid double counting some SlUs
Enter ( 9a+ 9b) - 9c here=> 1 PSNC
Enter the Number of SI Us in SNC for :
9a. I U Reporti ng vi of ati ons 9a. => 0 M SNC
9b. IUP Limit violations 9b. => 1 SNPS
9c. Both I U Reporti ng & L i mi t vi of ati ons 9c. => 0
1o. Number of SlUsin SNC due to I Reporting violations
that were not sampled or i nspected by POTW 10. => 0 SNIN
11. Number of SIUs in SNC dueto violation of 11. => 0 SSNC
Compl i ance Schedul a due dates
12. Number NOVs, NNCs, AOs, or similar assesed to SIUs 12. => 12 FENF
13. Number Civi I or Cri mi nal Penalti es assessed to SI Us 13. => 0 JUDI
14. Number of SIUs included in public notice 14. => 1 SVPU
15. Number of SlUsfrom which penal ti es col I ected 15. => 0 IUPN
16. Total A mount of Ci vi I Penal ti es Col I ected 16. => $ 0.00
17. Total N umber of SI Us on a compl i ance schedul e 17. => 0 SOCS
Foot Notes: AO Administrative Order NOV Noticeof Violation
CIU Categorical Industrial User PAR Pretreatment Annual Report
CO Consent Order POTW Public Operated Treatment Works
IUP Industrial User Pretreatment Permit SIU Significant Industrial User
NNC Noticeof Non-Compliance SNC significant Non-Compliance,formerly RNC

Public Notice
Durham County in accordance with Federal and State Regulations, is hereby giving public notice.
Listed below are users in significant noncompliance with national pretreatment regulations (40
CFR Part 403), state pretreatment regulations (15 NCAC 2H.0900), or local pretreatment
regulations during January 2022 through December 2022.
Phononic,located at 800 Capitola Drive,Suite 7,and regulated by significant industrial user permit
number DC-075 was in status of significant noncompliance for exceeding the Technical Review
Criteria for nickel in the first semiannual period of January through June 2022. A written
notification titled "Notice of Violation"was sent to the user's authorized representative requiring
them to notify the County of the cause of the violation. Phononic increased monitoring for nickel
and optimized the nickel treatment process to return to compliance.
bioMASON, located at 12 TW Alexander Drive, Building 200, Suite B, and regulated by local
industrial user permit number DCL-102 was in status of significant noncompliance for failure to
self-monitor for the second semiannual period of July through December 2022. A written
notification titled"Notice of Violation"was sent to the user's authorized representative requiring
them to notify the County of the cause of the violation.

or this notice will be NOTICE TO CREDITORS Wake County, Raleigh, North Caroli �pao ous c�sn Rooms wm,sh.—a
i ,recovery.Debtors na, for TERMINATION OF PARENTAL Bathroom Living,Dining and Kitchen
e asked to make im- The undersigned,having qualified as 919-949-4022 175.00 i
I.This the 6th dayof Executor of the Estate of Jarmila Hel- RIGHTS. Weekly,125.00 Deposit with
en McMullen,of Wake County,North This the 23 of February 2023.
Juliana Borbas,the tY Utilities included
'authorized to receive Carolina, hereby notifies all persons, VELASOUFZ&ASSOCIATES
�I assets belonging to fines and corporations having claims Jul!ssa F. Garcia, Esq. Attorney for
g 9 against the estate of said decedent to Plaintiff, 107 North Church St.-Ste. 200 !
Group PLLC, 3020 exhibit them to the undersigned,on or 200, Durham, NC 27701, 919-765-
't' lDarh= V. ryTCT
before May 16,2023,or this notice will 5645. „ Veranda Whiffed School�age ate 201 Durham, NC be pleaded in bar of recovery.All IPL0111277
Per Feb 28,Mar 21 2023 Housing For Persons 62 years o
sons,fines and corporations indebted and up
023 to the said estate are requested to
make immediate payment to the un- I _. ._.__. Studio,1,&2 Bedroom Apartments
dersigned. NOTICE TO CREDITORS j
English Labrador Re- For More Information, Contact us
ALL PERSONS, firms and corpora- frievers Monday-Friday 9am-5pm!
Barbara L.Wadsworth,Executor tions having claims against Charles 6 beautiful males left. $1400-1600
b23,as Administrator c/o Charles N.Griffin,III Moseley Lowe, deceased, of Wake Sire is a senior hunter and certified Call:[phone]
es all persons,firms Kirschbaum,Nanney,Keenan&Grid- County,N.C.,are notified to exhibit the therapy dog.Dam loyal pet.AKC lim- Email: verandawhitted @cahecman
a them to the under- fin,PA. same to the undersigned on or before ited registration. Please call or text agement.com +
ptice will be pleaded P.O.Box 19766 (May 31,2023),or this notice will be 9194644385.
;ate will please make Raleigh,NC 27619-9766 pleaded in bar of recovery.Debtors of TDD Relay#711
IPLO109604 the decedent are asked to make'Im- Chihuahuas 910-986-8097 This institution is an equal opportu-
Feb 14,21,28,Mar 7 2023 mediate payment. This February 28, nity provider
P,Esquire at Kennon 2023.
127707 Rone Patrick Lowe Jr (919I680-8900
NOTICE TO CREDITORS 501 Truitt Drive,Elon,NC 27244
All persons, firths and corporations IPLO111394
having claims against MARLON AR- Feb 28,Mar 7,1.4,21 2023
RINGTON WILLIAMS, DECEASED, of (k 12Y
Durham County, are noticed to ex-
',oximatey 55,972 net hiblt the same to the undersigned on NORTH CAROLINA I -
py as 38,848 square or before May 15,2023,or this notice DURHAM COUNTY ouxz.HOUSING
'easily accessible lo- along with the appropriate general NOTICE TO CREDITORS OPPORTUNITY
C 27603 is preferred. statute will be pleaded in bar of re- The undersigned,having qualified on
d. Possession date aovery. Debtors of the deceased are the 23rd day of February 2023,as Ad-
asked time for proposals asked to make immediate payment. ministrator CTA of the Estate of Lois Isa
ions,proposal forms This the 14th day of February 2023. Lloyd Dezem aka Lois Marie Dezem Puppies born 11-23-22; ready to ForSilk
All correspondence should be to the deceased,of Durham County, North go; black,cream,apricot boys and
Estate of Marlon Arrington Williams, Carolina, does hereby notify all per- girls;purebred,no AKC;dew claws
c/o Florence A.Bowen,Attorney,P.O. sons, firms and corporations having removed,natural tail;$400 call or txt y 5 O 11bilb. -!Qa
Box 51263,Durham,NC 27717. claims against said Estate to exhibit 919-415-9406. = l
IPLO109649 them to the undersigned on or be- -OC6ar1 View Trailer for sale of
Feb 14,21,28,Mar 7 2023 fore the 28th day of May 2023,or this Oceanfront Court
m at:
Notice will be pleaded in bar of their �' 1996 Oakwood 14 X 60 for sale.
' recovery.All persons indebted to said Located on lot G2 Oceanfront Court.
Notice to Creditors-Estate of Estate will please make immediate [e-mail]$t 90,000
Arlene Fischer Jones payment to the undersigned.
This 28th day of February 2023
ALL PERSONS, firms and corpora- Cynthia Browning,Administrator CTA Directory
tions having claims against Arlene Estate of Lois Lloyd Dezem aka Lois
Fischer Jones, deceased, of Wake Marie Dezem 4
County,NC,are notified to exhibit the Julia G.Henry,Esquire }�p�
same to the undersigned on or before l Kennon Craver,PLLC
May 18, 2023 or this notice will be 4011 University Drive,Suite 300 Golden Retriever Puppies AKC AKC
pleaded in bar of recovery.Debtors of Durham North Carolina 27707 Golden Retriever puppies, ready to POND WORK
the decedent are asked to make im- IPLO111423 go,born 12-28-22,females,$600,call FILL IN SWIMMING POOLS
mediate payment.This the 14th day of Feb 28,Mar 7,14,21 2023 910-375-0815 February,2023.Carole Jones Magee, - ALSO FISH PONDS
- SO FISH
PONDS
Personal Representative, in c/o Ash- v Ready Now,Beautiful Miniature
2252
ley Kevitt,Attorney,at Carolina Family Public Notice Schnauzers
Estate Planning, 201 Commonwealth Miniature Schnauzers are the perfect SWIMMING POOL DEMOLITION
Court,Suite 100,Cary,NC 27511. Durham County in accordance with pet small, hypoallergenic, energetic, Mobfles,Bams,House Demolition
IPLO109689 Federal and State Regulations, is family dogs, great for small or large www•bobcatvinnie.com
h Campus Feb 14,21,28,Mar 7 2023 hereby giving public notice. Listed settings-beautiful colors-Serious in- 919.761.7192
below are users in significant non- quiries only to great homes! $1500
compliance with national pretreatment 252-567-8115 or HHSchnauzers.com FIREWOOD
NOTICE TO CREDITORS regulations (40 CFR Part 403), state
ALL PERSONS, firms and corpora- pretreatment regulations (15 NCAC WE DELIVER
'Jommunity Engage- tions having claims against James 2H.0900), or local pretreatment reg-
.ulations during January 2022 through 919-201-37 I
"Jim" Schaefer, deceased, of Wake
I,at 2:00 P.M.,East- December 2022.
'p Conference Room, County,N.C.,are notified to exhibit the Phononic, located at 800 Capitola DRIVEWAY WORK
same to the undersigned on or be- eg g_ GRAVEL DRIVEWAYS
ham,North Carolina Drive,Suite 7,and r ulated y si b
land date. fore(6/6/2023),or this notice will be nificant industrial user permit number PRIVATE ROADS
pleaded in bar of recovery.Debtors of DC-075 was in status of significant
the decedent are asked to make im- Volden
• PARKING LOTS
am Time,on March noncompliance for exceeding the1 i�' TRACTOR GRADING
!Conference Room, mediate payment. This February 28, Technical Review Criteria for nickel in
ith Carolina 27701. 2023• the first semiannual period of January 919-201-3711
Yvonne Schaefer,Executor
lZoom using the link through June 2022.A written notifica- riever Pups
1700 Fairing View Way,Fuquay-Varf- tion title"Notice of Violation"was sent AKC,Vet checked, 1st shot,wormed,
ORnBJemozTIpWV- na,NC 27526 to the user's authorized representative champ line,$1,500.434-728-3403 JtltlkiT(>i 8I11tS
IPLO111592 requiring them to notify the County of
Feb 28,Mar 7,14,21 2023 the cause of the violation. Phononic _- Debris Removal Junk and yard de-
be obtained from increased monitoring for nickel and T si bris hauling.Clean out storage build-
it!es at httpsl/www. optimized the nickel treatment pro- 4 7 ings.Natural areas thinning/ mulch.
/bid-opportunities. NOTICE TO CREDITORS cess to return to compliance. Durham,Orange,Person,Granville.Call
Idenda without reg- ALL PERSONS, firms and corpora- bioMASON,located at 12 TW Alexan- 919 682 9067 call/text 919 667 4626
Feeive email notifica- tions having claims against Barbara der Drive,Building 200,Suite B,and
1Dfvision,Proposers S.Bailey,deceased,of Wake County, regulated by local industrial user per- ++
N.C.,are notified to exhibit the same mR number DCL-102 was in status of i► ) '41 tAMMU&MA 1 WAp f 4
to the undersigned on or before May significant noncompliance for failure 42 r in part,such pro- 23rd, 2023, or this notice will be to self-monitor for the second semian-
Tree service Tree trimming or complete
If the County. pleaded in bar of recovery. Debtors nual period of Julynot through December AussieDoodle Pups,triendly,10 wks, removal.Storm clean up.Stump grind-
immediate the decedent are asked to make of Violation"
atin"written notification to th title"Notice M/F,$900,l yr health guar,all shots/ ing Durham,Orange,Person,Granville
immediate payment. This 21 st day of of Violation"was sent to the user's au- worming,MtOlive,9192231894 call 919 682 9067 call/text 919 667
February,2023. thorized representative requiring them 4626
Betty Harrell,Executor,8300 Edwards to notify the County of the cause of the
Road,Castalia,NC,27816 violation.
IPLO109982 IPLO111519 - -
Feb 21,28,Mar 7,14 2023 Feb 28 2023 NEWSOBSERVER.COMf

Beaufort Gazette The Herald-Pock Hill el Nuevo Herald-Miami Sun News-Myrtle Beach
Belleville ■ Durham
Bellingham Herald Idaho Statesman Raleigh News&Obserwer The Telegraph-Macon
Bradenton Herald Island Packet The Olympian San Luis Obispo
AW,WICLATCHY Centre Daily Times Kansas City Star Sacramento Bee Th-City Herald
Charlotte Obser%er Lexington Herald-Leader Fort Worth Star-Telegram Wichita Eagle
Columbus Ledger-Enquirer Merced Sun- r_
Fresno Bee Miami Herald Sun Herald-Biloxi
AFFIDAVIT OF PUBLICATION
Account It Order Number Identification Order PO Amount Cols Depth
36398 388169 Print Legal Ad-IPL01115190-IPLO111519 $136.50 1 41 L
Attention: STATE OF NORTH CAROLINA
DURHAM COUNTY ENGINEERING-UTILITY DIVISION COUNTY OF WAKE,COUNTY OF DURHAM
5926 HWY 55 EAST Before the undersigned,a Notary Public of Dallas
DURHAM,NC 27713 County,Texas,duly commissioned and authorized to
administer oaths,affirmations,etc.,personally
appeared Tara Pennington,who being duly sworn or
affirmed,according to law,cloth depose and say that he
Public Notice or she is Accounts Receivable Specialist of the News&
Observer Publishing Company,a corporation organized
Durham County in accordance with Federal and State Regulations, is and doing business under the Laws of the State of North
hereby giving public notice. Listed Carolina,and publishing a newspaper known as The
below are users t significant non-
compliance with national pretreatment News&Observer,Wake and State aforesaid,the said
regulations (40 CFR Part 403), state newspaper in which such notice,paper,document,or
pretreatment regulations (15 NCAC legal advertisement was published was,at the time of
2H.0900), or local pretreatment reg-
ulations during January 2022 through each and every such publication,a newspaper meeting
December 20
Phononic, located at 800 Capitola q all of the requirements and qualifications of Section 1-
Drive,Suite 7,and regulated by sig- ; 597 of the General Statutes of North Carolina and was a
nificant industrial user permit number qualified newspaper within the meaning of Section 1 597
DC-075 was in status of significant q a p p g
noncompliance for exceeding the of the General Statutes of North Carolina,and that as
Technical Review Criteria for nickel in the first semiannual period of January such he or she makes this affidavit;and is familiar with
through June 2022.A written notifica- the books,files and business of said corporation and by
tion title"Notice of Violation"was sent to the user's authorized representative reference to the files of said publication the attached
requiring them to notify the County of advertisement for DURHAM COUNTY ENGINEERING-
the cause of the violation. Phononic increased monitoring for nickel and UTILITY DIVISION was inserted in the aforesaid
optimized the nickel treatment pro- newspaper on dates as follows:
cess to return to compliance.
biolVASON,located at 12 TW Alexan-
der Drive,Building 200,Suite B,and
regulated by local industrial user per-
mit number DCL-102 was in status of
significant noncompliance for failure
to self-monitor for the second semian-
nual period of July through December
2022.A written notification title"Notice
of Violation"was sent to the user's au-
thorized representative requiring them
to notify the County of the cause of the
violation. f
IPL0111519 � �^
Feb 28 2023
C4 V
I certify or declare)under penalty of perjury that the
foregoing is true and correct.
S± WI:*44-e r
Notary Public in and for the state of Texas,residing in
Dallas County
STEPHANIE HATCHER
4-'
=• My hlataly 10#133534406
., F*res January 14,2026
Extra charge for lost or duplicate affidavits.
Legal document please do not destroy!

TWWTP Allocation Table Printed: 11/4/2022, 3:05 PM
Allocation Table Page 1 of 5
Headworks last approved: 05/02/18
Allocation Table updated: 10/31/22
Permits last modified: 08/23/22
POTW=> TriangleWWTP
NPDES#=> NCO026051
FLOW BC
Industry Type Renewal Modification Date Permit Limits Permit
IUP INDUSTRY NAMES Permit Pipe of Effective Effective Permit Conc.
Count (please list alphabeticly) number number I ndustry Date Date Expi res M GD 9al/da m
1 AstraZeneca Pharmaceuticals DC-078 001 439 D&E Pharmaceutical 01/01/22 12/31/26 0.0020 2,000
2 Aurobindo USA DC-089 001 439 D&E Pharmaceutical 10/09/19 12/01/21 10/08/24 0.0390 39,000
3 Bio en DC-080 001 439 C,D&E Pharmaceutical 08/24/20 10/01/21 08/23/25 0.1250 125,000
4 Cintas DC-037 001 Full Service Laundry Facility 11/02/22 11/01/27 0.1000 100,000
5 Wolf speed Durham 008, 009 DC-076 469 Semi Conductor Mfg. 08/01/19 08/23/23 07/31/24 0.59101 591,000
Wolfspeed Durham 008 008 Combined Discharge) monitor
Wolf speed Durham 009 009 Combined Discharge) monitor
Wolfspeed Durham 013 013 433 Metal Finisher 0.0300 monitor
6 Wolf speed RTP DC-040 012 469 Semi Conductor Mf g. 08/01/19 08/23/22 07/31/24 0.3290 329,000
7 MP Pharma DC-114 001 439 D Pharmaceutical 08/09/21 08/08/24 0.0020 2,000
8 M i cross Advanced DC-085 001 469 E R&D Semiconductor 10/21/19 10/20/24 0.0750 75,000
9 Phononic DC-075 001 469 A Semi Conductor Mf g. 03/08/18 03/06/23 0.0200 20,000
10 PowerSecure DC-095 001 433 Metal Finisher 11/13/19 06/01/22 11/12/24 0.0060 6,000
11 SCM Metals DC-005 001 471.104A Powder Former 07/01/21 06/30/26 0.0500 50,000
12 Tri Pharm DC-106 001 439 D&E Pharmaceutical 10/18/20 10/17/23 0.0050 5,000
13 Tergus Pharma DC-115 001 439 D&E Pharmaceutical 12/27/21 12/26/23 0.0065 6,500
14 United Therapeutics DC-053 001 Combined Discharge) 05/25/20 09/01/21 05/24/25 0.0600 60,000
Column Totals=> 1.4405 1,410,500
Basis=> N PDES
MAHL from HWA (Ibs/day) => NPDES Permitted Flow=> 12.0000
U ncontrol I abl e L oadi ng(I bs/day) => 5.3100
Total AlIowablefor Industry(MAIL) (Ibs/day) => 6.6900
Total Permitted to Industry(Ibs/day) => 1.4405
MAIL left(Ibs/day) => 5.2495
Percent Allow. Ind. (MAIL) still available(%) => 78.5%
Percent MAHL still available(%) => 43.7%
5 Percent M A H L I bs/d => r:�0,6000

TWWTP Allocation Table Printed: 11/4/2022, 3:05 PM
Allocation Table Page 2 of 5
Headworks last approved: 05/02/18
Allocation Table updated: 10/31/22
Permits last modified: 08/23/22
POTW=> TriangleWWTP
NPDES#=> NC0026051
)D TSS Ammonia Arsenic Cadmium Chromium
Industry Limits Permit Limits Permit Limits Permit Limits Permit Limits Permit Limits
1 U P INDUSTRY NAMES Permit Pi pe L oad Conc. L oad Conc. L oad Conc. L oad Conc. L oad Conc. L oad
Count (please list alphabeticly) number number I bs/da m /I I bs/d m /I I bs/d m /I I bs/d m /I I bs/d m /I I bs/day
1 AstraZeneca Pharmaceuti cal s DC-078 001
2 Aurobindo USA DC-089 001 monitor monitor monitor monitor
3 Bio en DC-080 001 monitor monitor monitor monitor
4 Cintas DC-037 001 monitor monitor monitor monitor, monitor
5 Wolfspeed Durham 008, 009 DC-076
Wolfspeed Durham 008 008 monitor monitor monitor
Wolfspeed Durham 009 009
Wolfspeed Durham 013 013 0.0700 0.0175 1.7100 0.4278
6 Wolfspeed RTP DC-040 012 monitor monitor monitor monitor
7 M P Pharma DC-114 001
8 MicrossAdvanced DC-085 001 monitor monitor
9 Phononic DC-075 001
10 PowerSecure DC-095 001 0.0700 0.0035 1.7100 0.0856
11 SCM Metals DC-005 001 monitor monitor
12 TriPharm DC-106 001 monitor monitor monitor monitor E_=1
13 Tergus Pharma DC-115 001 monitor Imonitor monitor monitor monitor
14 United Therapeutics DC-053 001 monitor monitor I monitor I monitor
Column Totals=> 1 0 0 1 0 1 0.00001 0.0210 1 0.5134
Stream Stream Stream
Ba§s=> Design Design Design Std Std Std
M A H L from H WA (1 bs/day) _> 20016 25020 2502.00 0.8962 0.2987 4.8465
U ncontrol I ab1 e L oadi ng(I bs/day) _> 8281 9964 1306.42 0.1329 0.0133 0.1771
Total AlIowablefor Industry(MAIL) (Ibs/day) _> 11735 15056 1195.58 0.7633 0.2854 4.6694
Total Permitted to Industry(Ibs/day) _> 0 0 0.00 0.0000 0.0210 0.5134
MAIL left(Ibstday) _> 11735 15056 1195.58 0.7633 0.2644 4.1560
Percent A I I ow. I nd. (M A I L) sti I I avai I ab1 e(%) _> 100.0% 100.0% 100.0% 100.0% 92.6% 89.0%
Percent M A H L st i I I avai I abl e(%) _> 58.6% 60.2% 47.8% 85.2% 88.5% 85.8%
5 Percent M A H L I bstd => 1001 1251 125.10 0.0448 0.0149 0.2423

TWWTP Allocation Table Printed: 11/4/2022, 3:05 PM
Allocation Table Page 3 of 5
Headworks last approved: 05/02/18
Allocation Table updated: 10/31/22
Permits last modified: 08/23/22
POTW=> TriangleWWTP
NPDES#=> NC0026051
Copper Cyanide Lead Mercury Molybdenum
Industry Permit Limits Permit Limits Permit Limits Permit Limits Permit Limits
IUP INDUSTRY NAMES Permit Pipe Conc. Load Conc. Load Conc. Load Conc. Load Conc. Load
Count (please list alphabeticly) number number m /I I bs/da m I I bs/da m /I I bs/da m /I I bs/da m /I I bs/da
1 AstraZeneca Pharmaceuti cal s DC-078 001 0.000142 0.000002
2 Aurobindo USA DC-089 001 monitor monitor 0.000142 0.000046 monitor
3 Bio en DC-080 001 0.0400 0.0417 0.000142 0.000148 monitor
4 Cintas DC-037 001 monitor, monitor, 0.000142 0.000118 monitor
5 Wolfspeed Durham 008, 009 DC-076 0.000142 0.000700
Wolfspeed Durham 008 008 monitor monitor monitor monitor monitor
Wolfspeed Durham 009 009 monitor monitor monitor
Wolfspeed Durham 013 013 2.0700 0.5179 0.6500 0.1626 0.4300 0.1076
6 Wolfspeed RTP DC-040 012 monitorl monitor 0.000142 0.000390 monitor
7 M P Pharma DC-114 001 0.000142 0.000002
8 MicrossAdvanced DC-085 001 monitor monitor monitor 0.000142 0.000089 monitor
9 Phononic DC-075 001 0.000142 0.000024 monitor
10 PowerSecure DC-095 001 1 2.0700 0.1036 0.50001 0.0250 0.4300 0.02151 0.000142 0.000007 monitor,
11 SCM Metals DC-005 001 0.5000 0.2085 0.0300 0.0125 0.1000 0.04171 0.000142 0.0000591 monitor
12 Tri Pharm DC-106 001 0.000142 0.000006 monitor
13 Tergus Pharma DC-115 001 monitor monitor monitor 0.000142 0.000008 monitor
14 United Therapeutics DC-053 001 monitor 0.000142 0.000071 monitor
Column Totals=> 0.8300 0.2419 0.1708 0.001670 0.0000
AS/Nit/TF Stream Stream Sludge
Ba§s=> inhibition Std Std NPDES Ceiling HASL
M A H L from H WA (I bs/day) _> 23.6589 0.7950 3.1596 0.025829 22.9553
U ncontrol I abi e L oadi ng(I bs/day) _> 1.9308 0.0221 0.1949 0.003543 0.3366
Total AlIowablefor Industry(MAIL) (Ibs/day) _> 21.7281 0.7728 2.9647 0.022286 22.6188
Total Permitted to Industry(Ibs/day) _> 0.8300 0.2419 0.1708 0.001670 0.0000
MAIL left(Ibs/day) _> 20.8981 0.5310 2.7939 0.020616 22.6188
Percent AIIow. Ind. (MAIL) stiII avaiIabie(%) _> 96.2% 68.7% 94.2% 92.5% 100.0%
Percent M AH L sti I I avai I abl e(%) _> 88.3% 66.8% 88.4% 79.8% 98.5%
5 Percent M A H L I bs/d => 1.1829 0.0397 0.1580 0.001291 1.1478

TWWTP Allocation Table Printed: 11/4/2022, 3:05 PM
Allocation Table Page 4 of 5
Headworks last approved: 05/02/18
Allocation Table updated: 10/31/22
Permits last modified: 08/23/22
POTW=> TriangleWWTP
NPDES#=> NC0026051
Nickel Selenium Silver Zinc Total Nitrogen
Industry Permit Limits Permit Limits Permit Limits Permit Limits Permit Limits
IUP INDUSTRY NAMES Permit Pipe Conc. Load Conc. Load Conc. Load Conc. Load Conc. Load
Count (please list alphabeticly) number number m /I I bs/da m /I I bs/da m /I I bs/da m /I I bs/da m /I I bs/day
1 AstraZeneca Pharmaceuti cal s DC-078 001
2 Aurobindo USA DC-089 001 monitor monitor
3 Bio en DC-080 001 monitor monitor
4 Cintas I DC-037 001 monitor monitor monitor monitor
5 Wolfspeed Durham 008, 009 DC-076
Wolfspeed Durham 008 008 monitor monitor monitor monitor monitor
Wolfspeed Durham 009 009
Wolfspeed Durham 013 013 2.3800 0.5955 0.2400 0.0600 1.4800 0.3703
6 Wolfspeed RTP DC-040 012 monitor monitor I monitor monitorl monitor
7 M P Pharma DC-114 001
8 MicrossAdvanced DC-085 001 monitor monitor monitor monitor
9 Phononic DC-075 001 0.0200
10 PowerSecure DC-095 001 1.0000 0.0500 0.2400 0.0120 1.4800 0.0741
11 SCM Metals DC-005 001 monitor monitor monitor monitor
12 TriPharm DC-106 001 1 monitor monitor
13 Tergus Pharma DC-115 001 monitor monitor monitor monitor monitor
14 United Therapeutics DC-053 001 monitor monitor
Column Totals=> 0.6655 0.00001 0.0721 0.4444 0.00
u ge
Ceiling AS/Nit/TF AS/Nit/TF
Ba§s=> Stream Std HASL inhibition inhibition Design
M A H L from H WA (I bs/day) _> 2.4843 0.4219 12.3224 49.2894 4003.2000
U ncontrol I abl e L oadi ng(I bs/day) _> 0.3321 0.0930 0.0443 18.1304 1988.6492
Total AlIowablefor Industry(MAIL) (Ibs/day) _> 2.1522 0.3289 12.2781 31.1590 2014.55
Total Permitted to Industry(Ibs/day) _> 0.6655 0.0000 0.0721 0.4444 0.00
MAIL left(Ibs/day) _> 1.4867 0.3289 12.2060 30.7146 2014.55
Percent A I I ow. I nd. (M A I L) sti I I avai I abl e(%) _> 69.1 % 100.0% 99.4% 98.6% 100.0%
Percent M A H L st i I I avai I abl e(%) _> 59.8% 78.0% 99.1 % 62.3% 50.3%
5 Percent M A H L I bs/d => 0.1242 0.0211 0.6161 2.4645 200.16

TWWTP Allocation Table Printed: 11/4/2022, 3:05 PM
Allocation Table Page 5 of 5
Headworks last approved: 05/02/18
Allocation Table updated: 10/31/22
Permits last modified: 08/23/22
POTW=> TriangleWWTP
NPDES#=> NC0026051
Total Phos. Chloride Fluoride
Industry Permit Limits Permit Limits Permit Limits
IUP INDUSTRY NAMES Permit Pipe Conc. Load Conc. Load Conc. Load
Count (please list alphabeticly) number number m /I I bs/da m /I I bs/da m /I I bs/da
1 AstraZeneca Pharmaceuti cal s DC-078 001
2 Aurobindo USA DC-089 001 monitor monitor monitor
3 Bio en DC-080 001 monitor monitor monitor
4 Cintas DC-037 001 monitor monitor monitor
5 Wolfspeed Durham 008, 009 DC-076 1 7.0000 34.5026
Wolfspeed Durham 008 008 monitor monitor monitor
Wolfspeed Durham 009 009 monitor monitor
Wolfspeed Durham 013 013
6 Wolfspeed RTP DC-040 012 monitor monitor 7.0000 19.2070
7 M P Pharma DC-114 001
8 MicrossAdvanced DC-085 001 monitor monitor 6.0000 3.7530
9 Phononic DC-075 001
10 PowerSecure DC-095 001
11 SCM Metals DC-005 001 monitor monitor monitor
12 TriPharm DC-106 001 monitor monitor monitor
13 Tergus Pharma DC-115 001 monitor monitor monitor
14 United Therapeutics DC-053 001 monitor monitor monitor
Column Totals 4_� 0.00 0.0000 57.4626
Ba§s=> Design Stream Std NPDES
M A H L from H WA (I bs/day) _> 650.00 16179.5562 100.3290
U ncontrol I abl e L oadi ng(I bs/day) _> 238.92 3844.2251 31.7881
Total AlIowablefor Industry(MAIL) (Ibs/day) _> 411.08 12335.3311 68.5409
Total Permitted to Industry(Ibs/day) _> 0.00 0.0000 57.4626
MAIL left(Ibstday) _> 411.08 12335.3311 11.0783
Percent Allow. Ind. (MAIL) still available(%) _> 100.0% 100.0% 16.2%
Percent M A H L st i I I avai I abl e(%) _> 63.2% 76.2% 11.0%
5 Percent M A H L I bs/d => 32.5000 808.9778 5.0164

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Acetone
02/09/2022 S AstraZeneca020922Se1 0.794 /20.7 mg/L /
f
Feb 2022 Week 2 0.794 / mg/L /
Feb 2022 Average 0.794 /8.2 mg/L /
2022 Quarter 1 0.794 / mg/L /
2022 1 st 6 Months(Avg) 0.794 / mg/L /
2022 lst6...(Max) 0.794 / mg/L /
2022 lst6...(Min) 0.794 / mg/L /
2022 lst6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2022 S AstraZeneca0122F1ow 0.000102 / MGD /
02/28/2022 S AstrraZeneca0222F1ow 0.000068 / MGD /
03/31/2022 S AstraZeneca0322FIow 0.000071 / MGD /
04/30/2022 S AstraZeneca0422FIow 0.000174 / MGD /
05/31/2022 S AstraZeneca0522FIow 0.000225 / MGD /
06/30/2022 S AstraZeneca0622FIow 0.000102 / MGD /
Jan 2022 Week 4 0.000102 / MGD /
Feb 2022 Week 4 0.000068 / MGD /
Mar 2022 Week 4 0.000071 / MGD /
Apr 2022 Week 4 0.000174 / MGD /
May 2022 Week 4 0.000225 / MGD /
Jun 2022 Week 4 0.000102 / MGD /
Jan 2022 Average 0.000102 /0.002 MGD /
Feb 2022 Average 0.000068 /0.002 MGD /
Mar 2022 Average 0.000071 /0.002 MGD /
Apr 2022 Average 0.000174 /0.002 MGD /
May 2022 Average 0.000225 /0.002 MGD /
Jun 2022 Average 0.000102 /0.002 MGD /
2022 Quarter 1 0.00008 / MGD /
2022 Quarter 2 0.000167 / MGD /
2022 1 st 6 Months(Avg) 0.000124 / MGD /
2022 lst6...(Max) 0.000225 / MGD /
Friday,February 17,2023 5:51:55PM *Indicates Violation **Indicates TRC Violation Page 1 of 5

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Average Flow for Month
2022 lst6...(Min) 0.000068 / MGD /
2022 lst6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
COD
02/09/2022 S AstraZeneca02O922Sel 194 / mg/L /
f
04/19/2022 P AstraZeneca041922P0 15 / mg/L /
TW
Feb 2022 Week 2 194 / mg/L /
Apr 2022 Week 3 15 / mg/L /
Feb 2022 Average 194 / mg/L /
Apr 2022 Average 15 / mg/L /
2022 Quarter 1 194 / mg/L /
2022 Quarter 2 15 / mg/L /
2022 1 st 6 Months(Avg) 104.5 / mg/L /
2022 1st 6...(Max) 194 / mg/L /
2022 1st 6...(Min) 15 / mg/L /
2022 1st6...(Count) 2
Sample Date SampleID Result/Limit Mass/Limit
Ethyl acetate
02/09/2022 S AstraZeneca020922Se1 < 0.01 /20.7 mg/L < /
f
Feb 2022 Week 2 < 0.01 / mg/L < /
Feb 2022 Average < 0.01 /8.2 mg/L < /
2022 Quarter 1 < 0.01 / mg/L < /
2022 1 st 6 Months(Avg) < 0.01 / mg/L < /
2022 lst6...(Max) < 0.01 / mg/L < /
2022 lst6...(Min) < 0.01 / mg/L < /
2022 1st 6...(Count) 1 / /
Friday,February 17,2023 5:51:55PM *Indicates Violation **Indicates TRC Violation Page 2 of 5

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
02/09/2022 S AstraZeneca020922Se1 < 0.01 /20.7 mg/L < /
f
Feb 2022 Week 2 < 0.01 / mg/L < /
Feb 2022 Average < 0.01 /8.2 mg/L < /
2022 Quarter 1 < 0.01 / mg/L < /
2022 1 st 6 Months(Avg) < 0.01 / mg/L < /
2022 lst6...(Max) < 0.01 / mg/L < /
2022 lst6...(Min) < 0.01 / mg/L < /
2022 1st 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
02/09/2022 S AstraZeneca02O922Sel 0.000004 /0.000142 mg/L /
f
04/19/2022 P AstraZeneca041922PO 0.000006 /0.000142 mg/L /
TWHg
Feb 2022 Week 2 0.000004 / mg/L /
Apr 2022 Week 3 0.000006 / mg/L /
Feb 2022 Average 0.000004 / mg/L /
Apr 2022 Average 0.000006 / mg/L /
2022 Quarter 1 0.000004 / mg/L /
2022 Quarter 2 0.000006 / mg/L /
2022 1 st 6 Months(Avg) 0.000005 / mg/L /
2022 1st6...(Max) 0.000006 / mg/L /
2022 lst6...(Min) 0.000004 / mg/L /
2022 1st6...(Count) 2
Friday,February 17,2023 5:51:55PM *Indicates Violation **Indicates TRC Violation Page 3 of 5

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
02/09/2022 S AstraZeneca02O922Sel < 0.01 /3.0 mg/L < /
f
Feb 2022 Week 2 < 0.01 / mg/L < /
Feb 2022 Average < 0.01 /0.7 mg/L < /
2022 Quarter 1 < 0.01 / mg/L < /
2022 1 st 6 Months(Avg) < 0.01 / mg/L < /
2022 lst6...(Max) < 0.01 / mg/L < /
2022 lst6...(Min) < 0.01 / mg/L < /
2022 1st 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
02/09/2022 S AstraZeneca02O922Sel < 0.01 /20.7 mg/L < /
f
Feb 2022 Week 2 < 0.01 /8.2 mg/L < /
Feb 2022 Average < 0.01 / mg/L < /
2022 Quarter 1 < 0.01 / mg/L < /
2022 1 st 6 Months(Avg) < 0.01 / mg/L < /
2022 1st 6...(Max) < 0.01 / mg/L < /
2022 1st 6...(Min) < 0.01 / mg/L < /
2022 1st 6...(Count) 1
Friday,February 17,2023 5:51:55PM *Indicates Violation **Indicates TRC Violation Page 4 of 5

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
pH
02/09/2022 S AstraZeneca02O922Sel 7.3 /6.0-10.0 SU /
f
04/19/2022 P AstraZeneca041922PO 6.7 /6.0-10.0 SU /
TW
Feb 2022 Week 2 7.3 / SU /
Apr 2022 Week 3 6.7 / SU /
Feb 2022 Average 7.3 / SU /
Apr 2022 Average 6.7 / SU /
2022 Quarter 1 7.3 / SU /
2022 Quarter 2 6.7 / SU /
2022 1 st 6 Months(Avg) 7 / SU /
2022 lst6...(Max) 7.3 / SU /
2022 lst6...(Min) 6.7 / SU /
2022 lst6...(Count) 2
■
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Friday,February 17,2023 5:51:55PM *Indicates Violation **Indicates TRC Violation Page 5 of 5

Aurobindo USA
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Acetone
02/10/2022 P Aurobindo021022POT < 0.025 /5.59 mg/L < /
W
03/08/2022 S Aurobindo030822Se1f 0.928 /5.59 mg/L /
Feb 2022 Week 2 < 0.025 / mg/L < /
Mar 2022 Week 2 0.928 / mg/L /
Feb 2022 Average < 0.025 /2.21 mg/L < /
Mar 2022 Average 0.928 /2.21 mg/L /
2022 Quarter 1 < 0.477 / mg/L < /
2022 1 st 6 Months(Avg) < 0.477 / mg/L < /
2022 lst6...(Max) 0.928 / mg/L /
2022 lst6...(Min) < 0.025 / mg/L < /
2022 lst6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
02/10/2022 P Aurobindo021022POT 4.9 / mg/L /
W
03/08/2022 S Aurobindo03O822Self 14.5 / mg/L /
Feb 2022 Week 2 4.9 / mg/L /
Mar 2022 Week 2 14.5 / mg/L /
Feb 2022 Average 4.9 / mg/L /
Mar 2022 Average 14.5 / mg/L /
2022 Quarter 1 9.7 / mg/L /
2022 1 st 6 Months(Avg) 9.7 / mg/L /
2022 1st 6...(Max) 14.5 / mg/L /
2022 1st 6...(Min) 4.9 / mg/L /
2022 1st 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/19/2022 S Aurobindo0122F1ow 0.004263 / MGD /
02/17/2022 S Aurobindo0222F1ow 0.003622 / MGD /
03/16/2022 S Aurobindo0322F1ow 0.00463 / MGD /
04/30/2022 S Aurobindo0422F1ow 0.004184 / MGD /
Friday,February 17,2023 5:57:38PM *Indicates Violation **Indicates TRC Violation Page 1 of 12

Aurobindo USA
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Average Flow for Month
05/18/2022 S Aurobindo0522F1ow 0.005013 / MGD /
06/15/2022 S Aurobindo0622F1ow 0.00473 / MGD /
Jan 2022 Week 3 0.004263 / MGD /
Feb 2022 Week 3 0.003622 / MGD /
Mar 2022 Week 3 0.00463 / MGD /
Apr 2022 Week 4 0.004184 / MGD /
May 2022 Week 3 0.005013 / MGD /
Jun 2022 Week 3 0.00473 / MGD /
Jan 2022 Average 0.004263 /0.039 MGD /
Feb 2022 Average 0.003622 /0.039 MGD /
Mar 2022 Average 0.00463 /0.039 MGD /
Apr 2022 Average 0.004184 /0.039 MGD /
May 2022 Average 0.005013 /0.039 MGD /
Jun 2022 Average 0.00473 /0.039 MGD /
2022 Quarter 1 0.004172 / MGD /
2022 Quarter 2 0.004642 / MGD /
2022 1 st 6 Months(Avg) 0.004407 / MGD /
2022 lst6...(Max) 0.005013 / MGD /
2022 lst6...(Min) 0.003622 / MGD /
2022 1st 6...(Count) 6
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
BOD
02/10/2022 P Aurobindo021022POT 168 / mg/L /
W
03/08/2022 S Aurobindo03O822Self 46 / mg/L /
Feb 2022 Week 2 168 / mg/L /
Mar 2022 Week 2 46 / mg/L /
Feb 2022 Average 168 / mg/L /
Mar 2022 Average 46 / mg/L /
2022 Quarter 1 107 / mg/L /
2022 1 st 6 Months(Avg) 107 / mg/L /
2022 lst6...(Max) 168 / mg/L /
2022 lst6...(Min) 46 / mg/L /
Friday,February 17,2023 5:57:38PM *Indicates Violation **Indicates TRC Violation Page 2 of 12

Aurobindo USA
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
BOD
2022 lst6...(Count) 2
Sample Date SampleID Result/Limit Mass/Limit
Cadmium
02/10/2022 P Aurobindo021022POT < 0.00008 / mg/L < /
W
03/08/2022 S Aurobindo03O822Self < 0.00008 / mg/L < /
Feb 2022 Week 2 < 0.00008 / mg/L < /
Mar 2022 Week 2 < 0.00008 / mg/L < /
Feb 2022 Average < 0.00008 / mg/L < /
Mar 2022 Average < 0.00008 / mg/L < /
2022 Quarter 1 < 0.00008 / mg/L < /
2022 1 st 6 Months(Avg) < 0.00008 / mg/L < /
2022 lst6...(Max) < 0.00008 / mg/L < /
2022 lst6...(Min) < 0.00008 / mg/L < /
2022 lst6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
02/10/2022 P Aurobindo021022POT 30.8 / mg/L /
W
03/08/2022 S Aurobindo03O822Self 40 / mg/L /
Feb 2022 Week 2 30.8 / mg/L /
Mar 2022 Week 2 40 / mg/L /
Feb 2022 Average 30.8 / mg/L /
Mar 2022 Average 40 / mg/L /
2022 Quarter 1 35.4 / mg/L /
2022 1 st 6 Months(Avg) 35.4 / mg/L /
2022 lst6...(Max) 40 / mg/L /
2022 lst6...(Min) 30.8 / mg/L /
2022 lst6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
COD
02/10/2022 P Aurobindo021022POT 376 / mg/L /
W
03/08/2022 S Aurobindo03O822Self 203 / mg/L /
Feb 2022 Week 2 376 / mg/L /
Mar 2022 Week 2 203 / mg/L /
Feb 2022 Average 376 / mg/L /
Mar 2022 Average 203 / mg/L /
2022 Quarter 1 289.5 / mg/L /
Friday,February 17,2023 5:57:38PM *Indicates Violation **Indicates TRC Violation Page 3 of 12

Aurobindo USA
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
COD
2022 1 st 6 Months(Avg) 289.5 / mg/L /
2022 lst6...(Max) 376 / mg/L /
2022 lst6...(Min) 203 / mg/L /
2022 lst6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
02/10/2022 P Aurobindo021022POT 0.037 / mg/L /
W
03/08/2022 S Aurobindo03O822Self 0.024 / mg/L /
Feb 2022 Week 2 0.037 / mg/L /
Mar 2022 Week 2 0.024 / mg/L /
Feb 2022 Average 0.037 / mg/L /
Mar 2022 Average 0.024 / mg/L /
2022 Quarter 1 0.031 / mg/L /
2022 1 st 6 Months(Avg) 0.031 / mg/L /
2022 lst6...(Max) 0.037 / mg/L /
2022 lst6...(Min) 0.024 / mg/L /
2022 lst6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
02/10/2022 P Aurobindo021022POT < 0.003 / mg/L < /
W
03/08/2022 S Aurobindo030822Se1f < 0.003 / mg/L < /
Feb 2022 Week 2 < 0.003 / mg/L < /
Mar 2022 Week 2 < 0.003 / mg/L < /
Feb 2022 Average < 0.003 / mg/L < /
Mar 2022 Average < 0.003 / mg/L < /
2022 Quarter 1 < 0.003 / mg/L < /
2022 1 st 6 Months(Avg) < 0.003 / mg/L < /
2022 lst6...(Max) < 0.003 / mg/L < /
2022 1st 6...(Min) < 0.003 / mg/L < /
2022 1st 6...(Count) 2 / /
Sample Date SampleID Result/Limit Mass/Limit
Ethyl acetate
02/10/2022 P Aurobindo021022POT 0.027 15.59 mg/L /
W
03/08/2022 S Aurobindo03O822Self < 0.005 /5.59 mg/L < /
Feb 2022 Week 2 0.027 / mg/L /
Mar 2022 Week 2 < 0.005 / mg/L < /
Friday,February 17,2023 5:57:38PM *Indicates Violation **Indicates TRC Violation Page 4 of 12

Aurobindo USA
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Ethyl acetate
Feb 2022 Average 0.027 /2.21 mg/L /
Mar 2022 Average < 0.005 /2.21 mg/L < /
2022 Quarter 1 < 0.016 / mg/L < /
2022 1 st 6 Months(Avg) < 0.016 / mg/L < /
2022 lst6...(Max) 0.027 / mg/L /
2022 lst6...(Min) < 0.005 / mg/L < /
2022 1st 6...(Count) 2
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Fluoride
02/10/2022 P Aurobindo021022POT 0.63 / mg/L /
W
03/08/2022 S Aurobindo03O822Self 0.7 / mg/L /
Feb 2022 Week 2 0.63 / mg/L /
Mar 2022 Week 2 0.7 / mg/L /
Feb 2022 Average 0.63 / mg/L /
Mar 2022 Average 0.7 / mg/L /
2022 Quarter 1 0.67 / mg/L /
2022 1 st 6 Months(Avg) 0.67 / mg/L /
2022 lst6...(Max) 0.7 / mg/L /
2022 lst6...(Min) 0.63 / mg/L /
2022 lst6...(Count) 2
Sample Date SampleID Result/Limit Mass/Limit
Isopropyl acetate
02/10/2022 P Aurobindo021022POT < 0.005 /5.59 mg/L < /
W
03/08/2022 S Aurobindo030822Se1f < 0.005 /5.59 mg/L < /
Feb 2022 Week 2 < 0.005 / mg/L < /
Mar 2022 Week 2 < 0.005 / mg/L < /
Feb 2022 Average < 0.005 /2.21 mg/L < /
Mar 2022 Average < 0.005 /2.21 mg/L < /
2022 Quarter 1 < 0.005 / mg/L < /
2022 1 st 6 Months(Avg) < 0.005 / mg/L < /
Friday,February 17,2023 5:57:38PM *Indicates Violation **Indicates TRC Violation Page 5 of 12

Aurobindo USA
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Isopropyl acetate
2022 lst6...(Max) < 0.005 / mg/L < /
2022 lst6...(Min) < 0.005 / mg/L < /
2022 lst6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Mercury-LL
03/08/2022 S Aurobindo03O822Self 0.000052 /0.000142 mg/L /
05/09/2022 P Aurobindo05O922POT 0.00001 /0.000142 mg/L /
WHg
Mar 2022 Week 2 0.000052 / mg/L /
May 2022 Week 2 0.00001 / mg/L /
Mar 2022 Average 0.000052 / mg/L /
May 2022 Average 0.00001 / mg/L /
2022 Quarter 1 0.000052 / mg/L /
2022 Quarter 2 0.00001 / mg/L /
2022 1 st 6 Months(Avg) 0.000031 / mg/L /
2022 lst6...(Max) 0.000052 / mg/L /
2022 lst6...(Min) 0.00001 / mg/L /
2022 lst6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Methylene Chloride
02/10/2022 P Aurobindo021022POT < 0.003 /0.81 mg/L < /
W
03/08/2022 S Aurobindo030822Se1f < 0.005 /0.81 mg/L < /
Feb 2022 Week 2 < 0.003 / mg/L < /
Friday,February 17,2023 5:57:38PM *Indicates Violation **Indicates TRC Violation Page 6 of 12

Aurobindo USA
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
Methylene Chloride
Mar 2022 Week 2 < 0.005 / mg/L < /
Feb 2022 Average < 0.003 /0.18 mg/L < /
Mar 2022 Average < 0.005 /0.18 mg/L < /
2022 Quarter 1 < 0.004 / mg/L < /
2022 1 st 6 Months(Avg) < 0.004 / mg/L < /
2022 lst6...(Max) < 0.005 / mg/L < /
2022 lst6...(Min) < 0.003 / mg/L < /
2022 lst6...(Count) 2
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Molybdenum
02/10/2022 P Aurobindo021022POT < 0.001 / mg/L < /
W
03/08/2022 S Aurobindo03O822Self < 0.001 / mg/L < /
Feb 2022 Week 2 < 0.001 / mg/L < /
Mar 2022 Week 2 < 0.001 / mg/L < /
Feb 2022 Average < 0.001 / mg/L < /
Mar 2022 Average < 0.001 / mg/L < /
2022 Quarter 1 < 0.001 / mg/L < /
2022 1 st 6 Months(Avg) < 0.001 / mg/L < /
2022 lst6...(Max) < 0.001 / mg/L < /
2022 lst6...(Min) < 0.001 / mg/L < /
2022 lst6...(Count) 2
Sample Date SampleID Result/Limit Mass/Limit
n-Amyl acetate
02/10/2022 P Aurobindo021022POT < 0.005 /5.59 mg/L < /
W
03/08/2022 S Aurobindo030822Se1f < 0.005 /5.59 mg/L < /
Feb 2022 Week 2 < 0.005 / mg/L < /
Mar 2022 Week 2 < 0.005 / mg/L < /
Feb 2022 Average < 0.005 /2.21 mg/L < /
Mar 2022 Average < 0.005 /2.21 mg/L < /
2022 Quarter 1 < 0.005 / mg/L < /
Friday,February 17,2023 5:57:38PM *Indicates Violation **Indicates TRC Violation Page 7 of 12

Aurobindo USA
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
n-Amyl acetate
2022 1 st 6 Months(Avg) < 0.005 / mg/L < /
2022 lst6...(Max) < 0.005 / mg/L < /
2022 lst6...(Min) < 0.005 / mg/L < /
2022 lst6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
02/10/2022 P Aurobindo021022POT 0.9 / mg/L /
W
03/08/2022 S Aurobindo03O822Self 0.8 / mg/L /
Feb 2022 Week 2 0.9 / mg/L /
Mar 2022 Week 2 0.8 / mg/L /
Feb 2022 Average 0.9 / mg/L /
Mar 2022 Average 0.8 / mg/L /
2022 Quarter 1 0.8 / mg/L /
2022 1 st 6 Months(Avg) 0.8 / mg/L /
2022 lst6...(Max) 0.9 / mg/L /
2022 lst6...(Min) 0.8 / mg/L /
2022 lst6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
02/10/2022 P Aurobindo021022POT 17.2 / mg/L /
W
03/08/2022 S Aurobindo030822Se1f 26.2 / mg/L /
Feb 2022 Week 2 17.2 / mg/L /
Mar 2022 Week 2 26.2 / mg/L /
Feb 2022 Average 17.2 / mg/L /
Mar 2022 Average 26.2 / mg/L /
2022 Quarter 1 21.7 / mg/L /
2022 1 st 6 Months(Avg) 21.7 / mg/L /
2022 lst6...(Max) 26.2 / mg/L /
2022 1st 6...(Min) 17.2 / mg/L /
2022 1st 6...(Count) 2 / /
Friday,February 17,2023 5:57:38PM *Indicates Violation **Indicates TRC Violation Page 8 of 12

Aurobindo USA
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Oil&Grease,Total
02/10/2022 P Aurobindo021022POT 9.6 /200 mg/L /
W
03/08/2022 S Aurobindo030822Se1f 8.8 /200 mg/L /
Feb 2022 Week 2 9.6 / mg/L /
Mar 2022 Week 2 8.8 / mg/L /
Feb 2022 Average 9.6 / mg/L /
Mar 2022 Average 8.8 / mg/L /
2022 Quarter 1 9.2 / mg/L /
2022 1 st 6 Months(Avg) 9.2 / mg/L /
2022 lst6...(Max) 9.6 / mg/L /
2022 lst6...(Min) 8.8 / mg/L /
2022 lst6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
02/10/2022 P Aurobindo021022POT 8.9 /6.0-10.0 SU /
W
03/08/2022 S Aurobindo03O822Self 8.5 /6.0-10.0 SU /
Feb 2022 Week 2 8.9 / SU /
Mar 2022 Week 2 8.5 / SU /
Feb 2022 Average 8.9 / SU /
Mar 2022 Average 8.5 / SU /
2022 Quarter 1 8.7 / SU /
2022 1 st 6 Months(Avg) 8.7 / SU /
2022 1st 6...(Max) 8.9 / SU /
2022 1st 6...(Min) 8.5 / SU /
2022 1st6...(Count) 2
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Friday,February 17,2023 5:57:38PM *Indicates Violation **Indicates TRC Violation Page 9 of 12

Aurobindo USA
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Temperature
02/10/2022 P Aurobindo021022POT 14 /66 °C /
W
03/08/2022 S Aurobindo030822Se1f 17 /66 °C /
Feb 2022 Week 2 14 / °C /
Mar 2022 Week 2 17 / °C /
Feb 2022 Average 14 / °C /
Mar 2022 Average 17 / °C /
2022 Quarter 1 15.5 / °C /
2022 1 st 6 Months(Avg) 15.5 / °C /
2022 lst6...(Max) 17 / °C /
2022 lst6...(Min) 14 / °C /
2022 lst6...(Count) 2
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
02/10/2022 P Aurobindo021022POT 16.3 / mg/L /
W
03/08/2022 S Aurobindo03O822Self 25.4 / mg/L /
Feb 2022 Week 2 16.3 / mg/L /
Mar 2022 Week 2 25.4 / mg/L /
Feb 2022 Average 16.3 / mg/L /
Mar 2022 Average 25.4 / mg/L /
2022 Quarter 1 20.85 / mg/L /
2022 1st 6 Months(Avg) 20.85 / mg/L /
2022 1st 6...(Max) 25.4 / mg/L /
2022 1st 6...(Min) 16.3 / mg/L /
2022 1st 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
02/10/2022 P Aurobindo021022POT 3.51 / mg/L /
W
03/08/2022 S Aurobindo030822Se1f 3.43 / mg/L /
Feb 2022 Week 2 3.51 / mg/L /
Mar 2022 Week 2 3.43 / mg/L /
Friday,February 17,2023 5:57:38PM *Indicates Violation **Indicates TRC Violation Page 10 of 12

Aurobindo USA
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Total Phosphorus
Feb 2022 Average 3.51 / mg/L /
Mar 2022 Average 3.43 / mg/L /
2022 Quarter 1 3.47 / mg/L /
2022 1 st 6 Months(Avg) 3.47 / mg/L /
2022 lst6...(Max) 3.51 / mg/L /
2022 lst6...(Min) 3.43 / mg/L /
2022 lst6...(Count) 2 / /
Sample Date SampleID Result/Limit Mass Mmit
TSS
02/10/2022 P Aurobindo021022POT 87 / mg/L /
W
03/08/2022 S Aurobindo03O822Self 74 / mg/L /
Feb 2022 Week 2 87 / mg/L /
Mar 2022 Week 2 74 / mg/L /
Feb 2022 Average 87 / mg/L /
Mar 2022 Average 74 / mg/L /
2022 Quarter 1 80.5 / mg/L /
2022 1 st 6 Months(Avg) 80.5 / mg/L /
2022 lst6...(Max) 87 / mg/L /
2022 lst6...(Min) 74 / mg/L /
2022 lst6...(Count) 2
Sample Date SampleID Result/Limit Mass/Limit
VOC
02/10/2022 P Aurobindo021022POT 0.027 / mg/L /
W
03/08/2022 S Aurobindo03O822Self 0.928 / mg/L /
Feb 2022 Week 2 0.027 / mg/L /
Mar 2022 Week 2 0.928 / mg/L /
Feb 2022 Average 0.027 / mg/L /
Mar 2022 Average 0.928 / mg/L /
2022 Quarter 1 0.4775 / mg/L /
2022 1 st 6 Months(Avg) 0.4775 / mg/L /
2022 lst6...(Max) 0.928 / mg/L /
2022 lst6...(Min) 0.027 / mg/L /
2022 lst6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
02/10/2022 P Aurobindo021022POT 0.087 / mg/L /
W
Friday,February 17,2023 5:57:38PM *Indicates Violation **Indicates TRC Violation Page 11 of 12

Aurobindo USA
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Zinc
03/08/2022 S Aurobindo03O822Self 0.089 / mg/L /
Feb 2022 Week 2 0.087 / mg/L /
Mar 2022 Week 2 0.089 / mg/L /
Feb 2022 Average 0.087 / mg/L /
Mar 2022 Average 0.089 / mg/L /
2022 Quarter 1 0.088 / mg/L /
2022 1 st 6 Months(Avg) 0.088 / mg/L /
2022 lst6...(Max) 0.089 / mg/L /
2022 Ist6...(Min) 0.087 / mg/L /
2022 Ist 6...(Count) 2 / /
Friday,February 17,2023 5:57:38PM *Indicates Violation **Indicates TRC Violation Page 12 of 12

Biogen
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
Acetone
02/23/2022 P Biogen022322POTW 0.0712 / 12.19 mg/L 0.0367 / lbs/day
Feb 2022 Week 4 0.0712 / mg/L 0.0367 / lbs/day
Feb 2022 Average 0.0712 /4.83 mg/L 0.0367 / lbs/day
2022 Quarter 1 0.0712 / mg/L 0.0367 / lbs/day
2022 1 st 6 Months(Avg) 0.0712 / mg/L 0.0367 / lbs/day
2022 lst6...(Max) 0.0712 / mg/L 0.0367 / lbs/day
2022 1st6...(Min) 0.0712 / mg/L 0.0367 / lbs/day
2022 1st6...(Count) 1 / 1 /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Ammonia
02/08/2022 S Biogen02O822Self 5.12 / mg/L 3.4605 / lbs/day
02/23/2022 P Biogen022322POTW 4.5 / mg/L 2.3197 / lbs/day
Feb 2022 Week 2 5.12 / mg/L 3.4605 / lbs/day
Feb 2022 Week 4 4.5 / mg/L 2.3197 / lbs/day
Feb 2022 Average 4.81 / mg/L 2.8901 / lbs/day
2022 Quarter 1 4.81 / mg/L 2.8901 / lbs/day
2022 1 st 6 Months(Avg) 4.81 / mg/L 2.8901 / lbs/day
2022 lst6...(Max) 5.12 / mg/L 3.4605 / lbs/day
2022 lst6...(Min) 4.5 / mg/L 2.3197 / lbs/day
2022 lst6...(Count) 2 / 2 /
Sample Date SampleID Result/Limit Mass/Limit
Average Flow for Month
01/31/2022 S Biogen0122F1ow 0.067241 / MGD /
02/28/2022 S Biogen0222F1ow 0.064582 / MGD /
03/31/2022 S Biogen0322F1ow 0.058076 / MGD /
04/30/2022 S Biogen0422F1ow 0.097893 / MGD /
05/31/2022 S Biogen0522F1ow 0.137413 / MGD /
06/30/2022 S Biogen0622F1ow 0.144726 / MGD /
Jan 2022 Week 4 0.067241 / MGD /
Feb 2022 Week 4 0.064582 / MGD /
Mar 2022 Week 4 0.058076 / MGD /
Wednesday,February 22,2023 12:00:14PM *Indicates Violation **Indicates TRC Violation Page 1 of 10

Biogen
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Average Flow for Month
Apr 2022 Week 4 0.097893 / MGD /
May 2022 Week 4 0.137413 / MGD /
Jun 2022 Week 4 0.144726 / MGD /
Jan 2022 Average 0.067241 / MGD /
Feb 2022 Average 0.064582 / MGD /
Mar 2022 Average 0.058076 / MGD /
Apr 2022 Average 0.097893 / MGD /
May 2022 Average 0.137413 / MGD /
Jun 2022 Average 0.144726 / MGD /
2022 Quarter 1 0.0633 / MGD /
2022 Quarter 2 0.126677 / MGD /
2022 1 st 6 Months(Avg) 0.094989 / MGD /
2022 lst6...(Max) 0.144726 / MGD /
2022 lst6...(Min) 0.058076 / MGD /
2022 lst6...(Count) 6
Sample Date SamplelD Result/Limit Mass/Limit
BOD
02/08/2022 S Biogen02O822Self 210 / mg/L 141.933 / lbs/day
02/23/2022 P Biogen022322POTW 178 / mg/L 91.758 / lbs/day
Feb 2022 Week 2 210 / mg/L 141.933 / lbs/day
Feb 2022 Week 4 178 / mg/L 91.758 / lbs/day
Feb 2022 Average 194 / mg/L 116.846 / lbs/day
2022 Quarter 1 194 / mg/L 116.846 / lbs/day
2022 1 st 6 Months(Avg) 194 / mg/L 116.846 / lbs/day
2022 lst6...(Max) 210 / mg/L 141.933 / lbs/day
2022 lst6...(Min) 178 / mg/L 91.758 / lbs/day
2022 lst6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
02/09/2022 S Biogen02O922Self 66.3 / mg/L 37.7494 / lbs/day
02/23/2022 P Biogen022322POTW 265 / mg/L 136.6063 / lbs/day
Feb 2022 Week 2 66.3 / mg/L 37.7494 / lbs/day
Feb 2022 Week 4 265 / mg/L 136.6063 / lbs/day
Feb 2022 Average 165.65 / mg/L 87.1778 / lbs/day
2022 Quarter 1 165.65 / mg/L 87.1778 / lbs/day
2022 1 st 6 Months(Avg) 165.65 / mg/L 87.1778 / lbs/day
2022 lst6...(Max) 265 / mg/L 136.6063 / lbs/day
2022 lst6...(Min) 66.3 / mg/L 37.7494 / lbs/day
2022 lst6...(Count) 2 / 2 /
Wednesday,February 22,2023 12:00:14PM *Indicates Violation **Indicates TRC Violation Page 2 of 10

Biogen
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
COD
02/08/2022 S Biogen02O822Self 559 / mg/L 377.81 / lbs/day
02/23/2022 P Biogen022322POTW 205 / mg/L 105.68 / lbs/day
Feb 2022 Week 2 559 / mg/L 377.81 / lbs/day
Feb 2022 Week 4 205 / mg/L 105.68 / lbs/day
Feb 2022 Average 382 / mg/L 241.74 / lbs/day
2022 Quarter 1 382 / mg/L 241.74 / lbs/day
2022 1 st 6 Months(Avg) 382 / mg/L 241.75 / lbs/day
2022 lst6...(Max) 559 / mg/L 377.81 / lbs/day
2022 lst6...(Min) 205 / mg/L 105.68 / lbs/day
2022 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
02/08/2022 S Biogen02O822Self < 0.002 /0.05 mg/L < 0.001014 / lbs/day
02/23/2022 P Biogen022322POTW < 0.003 /0.05 mg/L < 0.001289 / lbs/day
Feb 2022 Week 2 < 0.002 / mg/L < 0.001014 / lbs/day
Feb 2022 Week 4 < 0.003 / mg/L < 0.001289 / lbs/day
Feb 2022 Average < 0.002 /0.04 mg/L < 0.001151 / lbs/day
2022 Quarter 1 < 0.002 / mg/L < 0.001151 / lbs/day
2022 1 st 6 Months(Avg) < 0.002 / mg/L < 0.001151 / lbs/day
2022 lst6...(Max) < 0.003 / mg/L < 0.001289 / lbs/day
2022 lst6...(Min) < 0.002 / mg/L < 0.001014 / lbs/day
2022 lst6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Diroximel fumarate
03/08/2022 S Biogen03O822SelfDRF < 0.013 / mg/L < 0 / lbs/day
05/18/2022 S Biogen051822SelfDRF < 0.013 / mg/L < /
Mar 2022 Week 2 < 0.013 / mg/L < 0 /
May 2022 Week 3 < 0.013 / mg/L < /
Mar 2022 Average < 0.013 / mg/L < 0 /
May 2022 Average < 0.013 / mg/L < /
2022 Quarter 1 < 0.013 / mg/L < 0 /
Wednesday,February 22,2023 12:00:14PM *Indicates Violation **Indicates TRC Violation Page 3 of 10

Biogen
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Diroximel fumarate
2022 Quarter 2 < 0.013 / mg/L < /
2022 1 st 6 Months(Avg) < 0.013 / mg/L < 0 /
2022 lst6...(Max) < 0.013 / mg/L < 0 /
2022 lst6...(Min) < 0.013 / mg/L < /
2022 lst6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
02/23/2022 P Biogen022322POTW < 0.0025 / 12.19 mg/L < 0.0013 / lbs/day
Feb 2022 Week 4 < 0.0025 / mg/L < 0.0013 / lbs/day
Feb 2022 Average < 0.0025 /4.83 mg/L < 0.0013 / lbs/day
2022 Quarter 1 < 0.0025 / mg/L < 0.0013 / lbs/day
2022 1 st 6 Months(Avg) < 0.0025 / mg/L < 0.0013 / lbs/day
2022 lst6...(Max) < 0.0025 / mg/L < 0.0013 / lbs/day
2022 lst6...(Min) < 0.0025 / mg/L < 0.0013 / lbs/day
2022 lst6...(Count) I / 1 /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
02/09/2022 S Biogen02O922Self 0.92 / mg/L 0.5227 / lbs/day
02/23/2022 P Biogen022322POTW 0.88 / mg/L 0.4536 / lbs/day
Feb 2022 Week 2 0.92 / mg/L 0.5227 / lbs/day
Feb 2022 Week 4 0.88 / mg/L 0.4536 / lbs/day
Feb 2022 Average 0.9 / mg/L 0.4882 / lbs/day
2022 Quarter 1 0.9 / mg/L 0.4882 / lbs/day
2022 1 st 6 Months(Avg) 0.90 / mg/L 0.4882 / lbs/day
2022 lst6...(Max) 0.92 / mg/L 0.5227 / lbs/day
2022 lst6...(Min) 0.88 / mg/L 0.4536 / lbs/day
2022 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
02/23/2022 P Biogen022322POTW < 0.0025 / 12.19 mg/L < 0.0013 / lbs/day
Wednesday,February 22,2023 12:00:14PM *Indicates Violation **Indicates TRC Violation Page 4 of 10

Biogen
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Isopropyl acetate
Feb 2022 Week 4 < 0.0025 / mg/L < 0.0013 / lbs/day
Feb 2022 Average < 0.0025 /4.83 mg/L < 0.0013 / lbs/day
2022 Quarter 1 < 0.0025 / mg/L < 0.0013 / lbs/day
2022 1 st 6 Months(Avg) < 0.0025 / mg/L < 0.0013 / lbs/day
2022 lst6...(Max) < 0.0025 / mg/L < 0.0013 / lbs/day
2022 lst6...(Min) < 0.0025 / mg/L < 0.0013 / lbs/day
2022 1st 6...(Count) 1 / 1 /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Mercury-LL
02/08/2022 S Biogen02O822Self 0.000007 /0.000142 mg/L /
02/22/2022 P Biogen022222POTWH 0.000002 /0.000142 mg/L /
9
Feb 2022 Week 2 0.000007 / mg/L /
Feb 2022 Week 4 0.000002 / mg/L /
Feb 2022 Average 0.000005 / mg/L /
2022 Quarter 1 0.000005 / mg/L /
2022 1 st 6 Months(Avg) 0.000005 / mg/L /
2022 lst6...(Max) 0.000007 / mg/L /
2022 lst6...(Min) 0.000002 / mg/L /
2022 lst6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Methylene Chloride
02/23/2022 P Biogen022322POTW < 0.003 / 1.77 mg/L < 0.001289 / lbs/day
Feb 2022 Week 4 < 0.003 / mg/L < 0.001289 / lbs/day
Wednesday,February 22,2023 12:00:14PM *Indicates Violation **Indicates TRC Violation Page 5 of 10

Biogen
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Methylene Chloride
Feb 2022 Average < 0.003 /0.41 mg/L < 0.001289 / lbs/day
2022 Quarter 1 < 0.003 / mg/L < 0.001289 / lbs/day
2022 1 st 6 Months(Avg) < 0.003 / mg/L < 0.001289 / lbs/day
2022 lst6...(Max) < 0.003 / mg/L < 0.001289 / lbs/day
2022 lst6...(Min) < 0.003 / mg/L < 0.001289 / lbs/day
2022 1st 6...(Count) 1 / 1 /
■
Sample Count: 1 Months Sampled: l Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result l Limit Mass l Limit
Molybdenum
02/23/2022 P Biogen022322POTW < 0.001 / mg/L < 0.0005 / lbs/day
Feb 2022 Week 4 < 0.001 / mg/L < 0.0005 / lbs/day
Feb 2022 Average < 0.001 / mg/L < 0.0005 / lbs/day
2022 Quarter 1 < 0.001 / mg/L < 0.0005 / lbs/day
2022 1 st 6 Months(Avg) < 0.001 / mg/L < 0.0005 / lbs/day
2022 lst6...(Max) < 0.001 / mg/L < 0.0005 / lbs/day
2022 lst6...(Min) < 0.001 / mg/L < 0.0005 / lbs/day
2022 lst6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
02/23/2022 P Biogen022322POTW < 0.003 / 12.19 mg/L < 0.0013 / lbs/day
Feb 2022 Week 4 < 0.003 / mg/L < 0.0013 / lbs/day
Feb 2022 Average < 0.003 /4.83 mg/L < 0.0013 / lbs/day
2022 Quarter 1 < 0.003 / mg/L < 0.0013 / lbs/day
2022 1 st 6 Months(Avg) < 0.003 / mg/L < 0.0013 / lbs/day
2022 lst6...(Max) < 0.003 / mg/L < 0.0013 / lbs/day
2022 lst6...(Min) < 0.003 / mg/L < 0.0013 / lbs/day
2022 lst6...(Count) 1 / 1 /
Wednesday,February 22,2023 12:00:14PM *Indicates Violation **Indicates TRC Violation Page 6 of 10

Biogen
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
02/23/2022 P Biogen022322POTW 0.8 / mg/L 0.423 / lbs/day
Feb 2022 Week 4 0.8 / mg/L 0.423 / lbs/day
Feb 2022 Average 0.8 / mg/L 0.423 / lbs/day
2022 Quarter 1 0.8 / mg/L 0.423 / lbs/day
2022 1 st 6 Months(Avg) 0.8 / mg/L 0.423 / lbs/day
2022 lst6...(Max) 0.8 / mg/L 0.423 / lbs/day
2022 lst6...(Min) 0.8 / mg/L 0.423 / lbs/day
2022 lst6...(Count) 1 / 1 /
Sample Date SampleID Result/Limit Mass/Limit
Nitrogen,Total
02/08/2022 S Biogen02O822Self 30.6 / mg/L 20.682 / lbs/day
02/23/2022 P Biogen022322POTW 13.9 / mg/L 7.165 / lbs/day
Feb 2022 Week 2 30.6 / mg/L 20.682 / lbs/day
Feb 2022 Week 4 13.9 / mg/L 7.165 / lbs/day
Feb 2022 Average 22.25 / mg/L 13.924 / lbs/day
2022 Quarter 1 22.25 / mg/L 13.924 / lbs/day
2022 1 st 6 Months(Avg) 22.25 / mg/L 13.924 / lbs/day
2022 lst6...(Max) 30.6 / mg/L 20.682 / lbs/day
2022 lst6...(Min) 13.9 / mg/L 7.165 / lbs/day
2022 lst6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
02/08/2022 S Biogen02O822Self 3.9 /200 mg/L /
02/23/2022 P Biogen022322POTW < 2.5 /200 mg/L < /
Feb 2022 Week 2 3.9 / mg/L /
Feb 2022 Week 4 < 2.5 / mg/L < /
Feb 2022 Average < 3.2 / mg/L < /
2022 Quarter 1 < 3.2 / mg/L < /
2022 1 st 6 Months(Avg) < 3.2 / mg/L < /
2022 lst6...(Max) 3.9 / mg/L /
2022 lst6...(Min) < 2.5 / mg/L < /
Wednesday,February 22,2023 12:00:14PM *Indicates Violation **Indicates TRC Violation Page 7 of 10

Biogen
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Oil&Grease,Total
2022 lst6...(Count) 2
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
pH
02/08/2022 S Biogen02O822Self 7.44 /5.5- 10.5 SU /
02/23/2022 P Biogen022322POTW 7.5 /5.5- 10.5 SU /
Feb 2022 Week 2 7.44 / SU /
Feb 2022 Week 4 7.5 / SU /
Feb 2022 Average 7.47 / SU /
2022 Quarter 1 7.47 / SU /
2022 1 st 6 Months(Avg) 7.47 / SU /
2022 lst6...(Max) 7.5 / SU /
2022 lst6...(Min) 7.44 / SU /
2022 lst6...(Count) 2
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Temperature
02/08/2022 S Biogen02O822Self 21.9 /66 °C /
02/23/2022 P Biogen022322POTW 20 /66 °C /
Feb 2022 Week 2 21.9 / °C /
Feb 2022 Week 4 20 / °C /
Feb 2022 Average 21 / °C /
2022 Quarter 1 21 / °C /
2022 1 st 6 Months(Avg) 21.0 / °C /
2022 lst6...(Max) 21.9 / °C /
Wednesday,February 22,2023 12:00:14PM *Indicates Violation **Indicates TRC Violation Page 8 of 10

Biogen
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
Temperature
2022 lst6...(Min) 20 / °C /
2022 lst6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
TKN
02/23/2022 P Biogen022322POTW 13.1 / mg/L 6.753 / lbs/day
Feb 2022 Week 4 13.1 / mg/L 6.753 / lbs/day
Feb 2022 Average 13.1 / mg/L 6.753 / lbs/day
2022 Quarter 1 13.1 / mg/L 6.753 / lbs/day
2022 1 st 6 Months(Avg) 13.1 / mg/L 6.753 / lbs/day
2022 lst6...(Max) 13.1 / mg/L 6.753 / lbs/day
2022 lst6...(Min) 13.1 / mg/L 6.753 / lbs/day
2022 lst6...(Count) 1 / 1 /
Sample Date SampleID Result/Limit Mass/Limit
Total Phosphorus
02/08/2022 S Biogen02O822Self 9.28 / mg/L 6.2721 / lbs/day
02/23/2022 P Biogen022322POTW 4.18 / mg/L 2.1548 / lbs/day
Feb 2022 Week 2 9.28 / mg/L 6.2721 / lbs/day
Feb 2022 Week 4 4.18 / mg/L 2.1548 / lbs/day
Feb 2022 Average 6.73 / mg/L 4.2134 / lbs/day
2022 Quarter 1 6.73 / mg/L 4.2134 / lbs/day
2022 1 st 6 Months(Avg) 6.73 / mg/L 4.2134 / lbs/day
2022 lst6...(Max) 9.28 / mg/L 6.2721 / lbs/day
2022 lst6...(Min) 4.18 / mg/L 2.1548 / lbs/day
2022 lst6...(Count) 2 / 2 /
Sample Date SampleID Result/Limit Mass/Limit
TSS
02/08/2022 S Biogen02O822Self 610 / mg/L 412.282896 / lbs/day
02/23/2022 P Biogen022322POTW 316 / mg/L 162.896546 / lbs/day
Feb 2022 Week 2 610 / mg/L 412.282896 / lbs/day
Feb 2022 Week 4 316 / mg/L 162.896546 / lbs/day
Wednesday,February 22,2023 12:00:14PM *Indicates Violation **Indicates TRC Violation Page 9 of 10

Biogen
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
TSS
Feb 2022 Average 463 / mg/L 287.589721 / lbs/day
2022 Quarter 1 463 / mg/L 287.589721 / lbs/day
2022 1 st 6 Months(Avg) 463 / mg/L 287.59 / lbs/day
2022 lst6...(Max) 610 / mg/L 412.282896 / lbs/day
2022 lst6...(Min) 316 / mg/L 162.896546 / lbs/day
2022 1st6...(Count) 2 / 2 /
Sample Date SampleID Result/Limit Mass/Limit
Zinc
02/09/2022 S Biogen02O922Self 1.18 / mg/L 0.671859 / lbs/day
02/23/2022 P Biogen022322POTW 1.189 / mg/L 0.612924 / lbs/day
Feb 2022 Week 2 1.18 / mg/L 0.671859 / lbs/day
Feb 2022 Week 4 1.189 / mg/L 0.612924 / lbs/day
Feb 2022 Average 1.185 / mg/L 0.642391 / lbs/day
2022 Quarter 1 1.185 / mg/L 0.642391 / lbs/day
2022 1 st 6 Months(Avg) 1.185 / mg/L 0.642391 / lbs/day
2022 lst6...(Max) 1.189 / mg/L 0.671859 / lbs/day
2022 lst6...(Min) 1.18 / mg/L 0.612924 / lbs/day
2022 lst6...(Count) 2 / 2 /
Wednesday,February 22,2023 12:00:14PM *Indicates Violation **Indicates TRC Violation Page 10 of 10

Cintas Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
Aluminum
06/15/2022 S Cintas061522Self 0.71 / mg/L 0.277074 / lbs/day
Jun 2022 Week 3 0.71 / mg/L 0.277074 / lbs/day
Jun 2022 Average 0.71 / mg/L 0.277074 / lbs/day
2022 Quarter 2 0.71 / mg/L 0.277074 / lbs/day
2022 1 st 6 Months(Avg) 0.71 / mg/L 0.277074 / lbs/day
2022 lst6...(Max) 0.71 / mg/L 0.277074 / lbs/day
2022 lst6...(Min) 0.71 / mg/L 0.277074 / lbs/day
2022 1st6...(Count) 1 / 1 /
Sample Date SampleID Result/Limit Mass/Limit
Ammonia
01/11/2022 P CintaS011122POTW 1.9 / mg/L 0.9522 / lbs/day
01/12/2022 S CintaS011222Self 3.4 / mg/L 1.9093 / lbs/day
02/22/2022 S Cintas022222Self 17.8 / mg/L 7.0105 / lbs/day
03/18/2022 S Cintas031822Self 7.9 / mg/L 4.0322 / lbs/day
04/05/2022 S Cintas04O522Self 1.5 / mg/L 0.6484 / lbs/day
05/03/2022 S Cintas05O322Self 1.3 / mg/L 0.71 / lbs/day
06/15/2022 S Cintas061522Self 4.71 / mg/L 1.8381 / lbs/day
Jan 2022 Week 2 2.65 / mg/L 1.4307 / lbs/day
Feb 2022 Week 4 17.8 / mg/L 7.0105 / lbs/day
Mar 2022 Week 3 7.9 / mg/L 4.0322 / lbs/day
Apr 2022 Week 1 1.5 / mg/L 0.6484 / lbs/day
May 2022 Week 1 1.3 / mg/L 0.71 / lbs/day
Jun 2022 Week 3 4.71 / mg/L 1.8381 / lbs/day
Jan 2022 Average 2.65 / mg/L 1.4307 / lbs/day
Feb 2022 Average 17.8 / mg/L 7.0105 / lbs/day
Mar 2022 Average 7.9 / mg/L 4.0322 / lbs/day
Apr 2022 Average 1.5 / mg/L 0.6484 / lbs/day
May 2022 Average 1.3 / mg/L 0.71 / lbs/day
Jun 2022 Average 4.71 / mg/L 1.8381 / lbs/day
2022 Quarter 1 7.75 / mg/L 3.4761 / lbs/day
2022 Quarter 2 2.5 / mg/L 1.0655 / lbs/day
2022 1 st 6 Months(Avg) 5.50 / mg/L 2.4430 / lbs/day
2022 lst6...(Max) 17.8 / mg/L 7.0105 / lbs/day
2022 lst6...(Min) 1.3 / mg/L 0.6484 / lbs/day
2022 lst6...(Count) 7 / 7 /
Sample Date SampleID Result/Limit Mass/Limit
Average Flow for Month
01/31/2022 S Cintas0122F1ow 0.051832 /0.180 MGD /
02/28/2022 S Cintas0222F1ow 0.058604 /0.180 MGD /
03/31/2022 S Cintas0322F1ow 0.053285 /0.180 MGD /
Wednesday,February 22,2023 1:31:24PM *Indicates Violation **Indicates TRC Violation Page 1 of 17

Cintas Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
04/30/2022 S Cintas0422F1ow 0.049801 /0.180 MGD /
05/31/2022 S Cintas0522F1ow 0.047875 /0.180 MGD /
06/30/2022 S Cintas0622F1ow 0.051973 /0.180 MGD /
Jan 2022 Week 4 0.051832 / MGD /
Feb 2022 Week 4 0.058604 / MGD /
Mar 2022 Week 4 0.053285 / MGD /
Apr 2022 Week 4 0.049801 / MGD /
May 2022 Week 4 0.047875 / MGD /
Jun 2022 Week 4 0.051973 / MGD /
Jan 2022 Average 0.051832 /0.120 MGD /
Feb 2022 Average 0.058604 /0.120 MGD /
Mar 2022 Average 0.053285 /0.120 MGD /
Apr 2022 Average 0.049801 /0.120 MGD /
May 2022 Average 0.047875 /0.120 MGD /
Jun 2022 Average 0.051973 /0.120 MGD /
2022 Quarter 1 0.054574 / MGD /
2022 Quarter 2 0.049883 / MGD /
2022 1 st 6 Months(Avg) 0.052228 / MGD /
2022 lst6...(Max) 0.058604 / MGD /
2022 lst6...(Min) 0.047875 / MGD /
2022 lst6...(Count) 6
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
BOD
01/11/2022 P CintaS011122POTW 342 / mg/L 171.399 / lbs/day
01/12/2022 S CintaS011222Self 352 / mg/L 197.665 / lbs/day
02/10/2022 P Cintas021022POTW 405 / mg/L /
02/22/2022 S Cintas022222Self 288 / mg/L 113.428 / lbs/day
03/15/2022 P Cintas031522POTW 1270 / mg/L /
03/18/2022 S Cintas031822Self 401 / mg/L 204.674 / lbs/day
04/05/2022 S Cintas04O522Self 351 / mg/L 151.73 / lbs/day
04/26/2022 P Cintas042622POTW 935 / mg/L /
05/03/2022 S Cintas05O322Self 300 / mg/L 163.851 / lbs/day
05/24/2022 P Cintas052422POTW 497 / mg/L /
Wednesday,February 22,2023 1:31:24PM *Indicates Violation **Indicates TRC Violation Page 2 of 17

Cintas Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
BOD
06/09/2022 P Cintas06O922POTW 496 / mg/L /
06/15/2022 S Cintas061522Self 438 / mg/L 170.927 / lbs/day
06/21/2022 P Cintas062122POTW 626 / mg/L /
Jan 2022 Week 2 347 / mg/L 184.532 / lbs/day
Feb 2022 Week 2 405 / mg/L /
Feb 2022 Week 4 288 / mg/L 113.428 / lbs/day
Mar 2022 Week 3 835.5 / mg/L 204.674 / lbs/day
Apr 2022 Week 1 351 / mg/L 151.73 / lbs/day
Apr 2022 Week 4 935 / mg/L /
May 2022 Week 1 300 / mg/L 163.851 / lbs/day
May 2022 Week 4 497 / mg/L /
Jun 2022 Week 2 496 / mg/L /
Jun 2022 Week 3 532 / mg/L 170.927 / lbs/day
Jan 2022 Average 347 / mg/L 184.532 / lbs/day
Feb 2022 Average 346.5 / mg/L 113.428 / lbs/day
Mar 2022 Average 835.5 / mg/L 204.674 / lbs/day
Apr 2022 Average 643 / mg/L 151.73 / lbs/day
May 2022 Average 398.5 / mg/L 163.851 / lbs/day
Jun 2022 Average 520 / mg/L 170.927 / lbs/day
2022 Quarter 1 509.7 / mg/L 171.792 / lbs/day
2022 Quarter 2 520.4 / mg/L 162.169 / lbs/day
2022 1 st 6 Months(Avg) 515.5 / mg/L 167.668 / lbs/day
2022 1st6...(Max) 1270 / mg/L 204.674 / lbs/day
2022 1st6...(Min) 288 / mg/L /
2022 1st 6...(Count) 13 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
06/15/2022 S Cintas061522Self < 0.005 / mg/L < 0.001951 / lbs/day
Jun 2022 Week 3 < 0.005 / mg/L < 0.001951 / lbs/day
Jun 2022 Average < 0.005 / mg/L < 0.001951 / lbs/day
2022 Quarter 2 < 0.005 / mg/L < 0.001951 / lbs/day
2022 1 st 6 Months(Avg) < 0.005 / mg/L < 0.001951 / lbs/day
2022 lst6...(Max) < 0.005 / mg/L < 0.001951 / lbs/day
2022 lst6...(Min) < 0.005 / mg/L < 0.001951 / lbs/day
2022 lst6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
01/11/2022 P CintasOI1122POTW 95 / mg/L 47.6109 / lbs/day
02/22/2022 S Cintas022222Self 95.7 / mg/L 37.6913 / lbs/day
Jan 2022 Week 2 95 / mg/L 47.6109 / lbs/day
Wednesday,February 22,2023 1:31:24PM *Indicates Violation **Indicates TRC Violation Page 3 of 17

Cintas Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
Chloride
Feb 2022 Week 4 95.7 / mg/L 37.6913 / lbs/day
Jan 2022 Average 95 / mg/L 47.6109 / lbs/day
Feb 2022 Average 95.7 / mg/L 37.6913 / lbs/day
2022 Quarter 1 95.35 / mg/L 42.6511 / lbs/day
2022 1 st 6 Months(Avg) 95.35 / mg/L 42.6511 / lbs/day
2022 lst6...(Max) 95.7 / mg/L 47.6109 / lbs/day
2022 lst6...(Min) 95 / mg/L 37.6913 / lbs/day
2022 lst6...(Count) 2 / 2 /
Sample Date SampleID Result/Limit Mass/Limit
Chromium
01/12/2022 S CintaS011222Self 0.017 / mg/L 0.009546 / lbs/day
02/22/2022 S Cintas022222Self 0.006 / mg/L 0.002166 / lbs/day
03/18/2022 S Cintas031822Self 0.007 / mg/L 0.003522 / lbs/day
04/05/2022 S Cintas04O522Self < 0.003 / mg/L < 0.001081 / lbs/day
05/03/2022 S Cintas05O322Self < 0.003 / mg/L < 0.001365 / lbs/day
06/15/2022 S Cintas061522Self < 0.005 / mg/L < 0.001951 / lbs/day
Jan 2022 Week 2 0.017 / mg/L 0.009546 / lbs/day
Feb 2022 Week 4 0.006 / mg/L 0.002166 / lbs/day
Mar 2022 Week 3 0.007 / mg/L 0.003522 / lbs/day
Apr 2022 Week 1 < 0.003 / mg/L < 0.001081 / lbs/day
May 2022 Week 1 < 0.003 / mg/L < 0.001365 / lbs/day
Jun 2022 Week 3 < 0.005 / mg/L < 0.001951 / lbs/day
Jan 2022 Average 0.017 / mg/L 0.009546 / lbs/day
Feb 2022 Average 0.006 / mg/L 0.002166 / lbs/day
Mar 2022 Average 0.007 / mg/L 0.003522 / lbs/day
Apr 2022 Average < 0.003 / mg/L < 0.001081 / lbs/day
May 2022 Average < 0.003 / mg/L < 0.001365 / lbs/day
Jun 2022 Average < 0.005 / mg/L < 0.001951 / lbs/day
2022 Quarter 1 0.01 / mg/L 0.005078 / lbs/day
2022 Quarter 2 < 0.003 / mg/L < 0.001466 / lbs/day
2022 1 st 6 Months(Avg) < 0.007 / mg/L < 0.003272 / lbs/day
2022 lst6...(Max) 0.017 / mg/L 0.009546 / lbs/day
2022 lst6...(Min) < 0.003 / mg/L < 0.001081 / lbs/day
2022 lst6...(Count) 6 / 6 /
Sample Date SampleID Result/Limit Mass/Limit
Copper
01/12/2022 S CintasO11222Self 0.15 / mg/L 0.084232 / lbs/day
02/22/2022 S Cintas022222Self 0.066 / mg/L 0.025994 / lbs/day
03/18/2022 S Cintas031822Self 0.079 / mg/L 0.040322 / lbs/day
04/05/2022 S CintasO4O522Self 0.044 / mg/L 0.01902 / lbs/day
Wednesday,February 22,2023 1:31:24PM *Indicates Violation **Indicates TRC Violation Page 4 of 17

Cintas Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Copper
05/03/2022 S Cintas05O322Self 0.041 / mg/L 0.022393 / lbs/day
06/15/2022 S Cintas061522Self 0.073 / mg/L 0.028488 / lbs/day
Jan 2022 Week 2 0.15 / mg/L 0.084232 / lbs/day
Feb 2022 Week 4 0.066 / mg/L 0.025994 / lbs/day
Mar 2022 Week 3 0.079 / mg/L 0.040322 / lbs/day
Apr 2022 Week 1 0.044 / mg/L 0.01902 / lbs/day
May 2022 Week 1 0.041 / mg/L 0.022393 / lbs/day
Jun 2022 Week 3 0.073 / mg/L 0.028488 / lbs/day
Jan 2022 Average 0.15 / mg/L 0.084232 / lbs/day
Feb 2022 Average 0.066 / mg/L 0.025994 / lbs/day
Mar 2022 Average 0.079 / mg/L 0.040322 / lbs/day
Apr 2022 Average 0.044 / mg/L 0.01902 / lbs/day
May 2022 Average 0.041 / mg/L 0.022393 / lbs/day
Jun 2022 Average 0.073 / mg/L 0.028488 / lbs/day
2022 Quarter 1 0.098 / mg/L 0.050183 / lbs/day
2022 Quarter 2 0.053 / mg/L 0.0233 / lbs/day
2022 1 st 6 Months(Avg) 0.076 / mg/L 0.036742 / lbs/day
2022 lst6...(Max) 0.15 / mg/L 0.084232 / lbs/day
2022 lst6...(Min) 0.041 / mg/L 0.019020 / lbs/day
2022 lst6...(Count) 6 / 6 /
Sample Date SampleID Result/Limit Mass/Limit
Fluoride
01/11/2022 P CintaS011122POTW 0.73 / mg/L 0.3659 / lbs/day
01/12/2022 S Cintas011222Self < 0.05 / mg/L < 0.0281 / lbs/day
02/22/2022 S Cintas022222Self < 0.05 / mg/L < 0.0197 / lbs/day
03/18/2022 S Cintas031822Self 0.22 / mg/L 0.1123 / lbs/day
04/05/2022 S Cintas04O522Self 0.42 / mg/L 0.1816 / lbs/day
05/03/2022 S Cintas05O322Self 0.78 / mg/L 0.426 / lbs/day
06/15/2022 S Cintas061522Self < 0.05 / mg/L < 0.0195 / lbs/day
Jan 2022 Week 2 < 0.39 / mg/L < 0.197 / lbs/day
Feb 2022 Week 4 < 0.05 / mg/L < 0.0197 / lbs/day
Mar 2022 Week 3 0.22 / mg/L 0.1123 / lbs/day
Apr 2022 Week 1 0.42 / mg/L 0.1816 / lbs/day
May 2022 Week 1 0.78 / mg/L 0.426 / lbs/day
Jun 2022 Week 3 < 0.05 / mg/L < 0.0195 / lbs/day
Jan 2022 Average < 0.39 / mg/L < 0.197 / lbs/day
Feb 2022 Average < 0.05 / mg/L < 0.0197 / lbs/day
Mar 2022 Average 0.22 / mg/L 0.1123 / lbs/day
Apr 2022 Average 0.42 / mg/L 0.1816 / lbs/day
May 2022 Average 0.78 / mg/L 0.426 / lbs/day
Jun 2022 Average < 0.05 / mg/L < 0.0195 / lbs/day
Wednesday,February 22,2023 1:31:24PM *Indicates Violation **Indicates TRC Violation Page 5 of 17

Cintas Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
Fluoride
2022 Quarter 1 < 0.26 / mg/L < 0.1315 / lbs/day
2022 Quarter 2 < 0.42 / mg/L < 0.209 / lbs/day
2022 1 st 6 Months(Avg) < 0.33 / mg/L < 0.1647 / lbs/day
2022 lst6...(Max) 0.78 / mg/L 0.4260 / lbs/day
2022 lst6...(Min) < 0.05 / mg/L < 0.0195 / lbs/day
2022 lst6...(Count) 7 / 7 /
Sample Date SampleID Result/Limit Mass/Limit
Lead
01/12/2022 S CintaS011222Self 0.025 / mg/L 0.014039 / lbs/day
02/22/2022 S Cintas022222Self 0.011 / mg/L 0.004332 / lbs/day
03/18/2022 S Cintas031822Self 0.013 / mg/L 0.006635 / lbs/day
04/05/2022 S Cintas04O522Self 0.0092 / mg/L 0.003977 / lbs/day
05/03/2022 S Cintas05O322Self < 0.0025 / mg/L < 0.001365 / lbs/day
06/15/2022 S Cintas061522Self < 0.0125 / mg/L < 0.004878 / lbs/day
Jan 2022 Week 2 0.025 / mg/L 0.014039 / lbs/day
Feb 2022 Week 4 0.011 / mg/L 0.004332 / lbs/day
Mar 2022 Week 3 0.013 / mg/L 0.006635 / lbs/day
Apr 2022 Week 1 0.0092 / mg/L 0.003977 / lbs/day
May 2022 Week 1 < 0.0025 / mg/L < 0.001365 / lbs/day
Jun 2022 Week 3 < 0.0125 / mg/L < 0.004878 / lbs/day
Jan 2022 Average 0.025 / mg/L 0.014039 / lbs/day
Feb 2022 Average 0.011 / mg/L 0.004332 / lbs/day
Mar 2022 Average 0.013 / mg/L 0.006635 / lbs/day
Apr 2022 Average 0.0092 / mg/L 0.003977 / lbs/day
May 2022 Average < 0.0025 / mg/L < 0.001365 / lbs/day
Jun 2022 Average < 0.0125 / mg/L < 0.004878 / lbs/day
2022 Quarter 1 0.0163 / mg/L 0.008335 / lbs/day
2022 Quarter 2 < 0.0081 / mg/L < 0.003407 / lbs/day
2022 1 st 6 Months(Avg) < 0.0122 / mg/L < 0.005871 / lbs/day
2022 lst6...(Max) 0.025 / mg/L 0.014039 / lbs/day
2022 lst6...(Min) < 0.0025 / mg/L < 0.001365 / lbs/day
2022 lst6...(Count) 6 / 6 /
Sample Date SampleID Result/Limit Mass/Limit
Mercury-LL
01/10/2022 P CintasOI1022POTWH 0.000027 /0.000142 mg/L /
g
01/12/2022 S Cintas011222Self < 0 /0.000142 mg/L < /
Jan 2022 Week 2 < 0.000013 / mg/L < /
Jan 2022 Average < 0.000013 / mg/L < /
2022 Quarter 1 < 0.000013 / mg/L < /
Wednesday,February 22,2023 1:31:24PM *Indicates Violation **Indicates TRC Violation Page 6 of 17

Cintas Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Mercury-LL
2022 1 st 6 Months(Avg) < 0.000013 / mg/L < /
2022 lst6...(Max) 0.000027 / mg/L /
2022 lst6...(Min) < 0.000000 / mg/L < /
2022 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
01/12/2022 S Cintas011222Self 0 / mg/L 0.0213 / lbs/day
02/22/2022 S Cintas022222Self 0 / mg/L 0.0055 / lbs/day
03/18/2022 S Cintas031822Self 0 / mg/L 0.0107 / lbs/day
04/05/2022 S Cintas04O522Self 0 / mg/L 0.0099 / lbs/day
05/03/2022 S CintaS050322Self 0 / mg/L 0.0034 / lbs/day
06/15/2022 S Cintas061522Self < 0 / mg/L < 0.0078 / lbs/day
Jan 2022 Week 2 0 / mg/L 0.0213 / lbs/day
Feb 2022 Week 4 0 / mg/L 0.0055 / lbs/day
Mar 2022 Week 3 0 / mg/L 0.0107 / lbs/day
Apr 2022 Week 1 0 / mg/L 0.0099 / lbs/day
May 2022 Week 1 0 / mg/L 0.0034 / lbs/day
Jun 2022 Week 3 < 0 / mg/L < 0.0078 / lbs/day
Jan 2022 Average 0 / mg/L 0.0213 / lbs/day
Feb 2022 Average 0 / mg/L 0.0055 / lbs/day
Mar 2022 Average 0 / mg/L 0.0107 / lbs/day
Apr 2022 Average 0 / mg/L 0.0099 / lbs/day
May 2022 Average 0 / mg/L 0.0034 / lbs/day
Jun 2022 Average < 0 / mg/L < 0.0078 / lbs/day
2022 Quarter 1 0 / mg/L 0.0125 / lbs/day
2022 Quarter 2 < 0 / mg/L < 0.007 / lbs/day
2022 1 st 6 Months(Avg) < 0.0 / mg/L < 0.0098 / lbs/day
2022 lst6...(Max) 0.0 / mg/L 0.0213 / lbs/day
2022 lst6...(Min) 0.0 / mg/L 0.0034 / lbs/day
2022 Ist6...(Count) 6 / 6 /
Wednesday,February 22,2023 1:31:24PM *Indicates Violation **Indicates TRC Violation Page 7 of 17

Cintas Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Nickel
01/12/2022 S CintasOI1222Self 0.025 / mg/L 0.014039 / lbs/day
02/22/2022 S Cintas022222Self 0.013 / mg/L 0.00512 / lbs/day
03/18/2022 S Cintas031822Self 0.017 / mg/L 0.008677 / lbs/day
04/05/2022 S CintasO4O522Self 0.015 / mg/L 0.006484 / lbs/day
05/03/2022 S Cintas05O322Self 0.01 / mg/L 0.005462 / lbs/day
06/15/2022 S Cintas061522Self 0.022 / mg/L 0.008585 / lbs/day
Jan 2022 Week 2 0.025 / mg/L 0.014039 / lbs/day
Feb 2022 Week 4 0.013 / mg/L 0.00512 / lbs/day
Mar 2022 Week 3 0.017 / mg/L 0.008677 / lbs/day
Apr 2022 Week 1 0.015 / mg/L 0.006484 / lbs/day
May 2022 Week 1 0.01 / mg/L 0.005462 / lbs/day
Jun 2022 Week 3 0.022 / mg/L 0.008585 / lbs/day
Jan 2022 Average 0.025 / mg/L 0.014039 / lbs/day
Feb 2022 Average 0.013 / mg/L 0.00512 / lbs/day
Mar 2022 Average 0.017 / mg/L 0.008677 / lbs/day
Apr 2022 Average 0.015 / mg/L 0.006484 / lbs/day
May 2022 Average 0.01 / mg/L 0.005462 / lbs/day
Jun 2022 Average 0.022 / mg/L 0.008585 / lbs/day
2022 Quarter 1 0.0183 / mg/L 0.009279 / lbs/day
2022 Quarter 2 0.0157 / mg/L 0.006844 / lbs/day
2022 1 st 6 Months(Avg) 0.017 / mg/L 0.008061 / lbs/day
2022 lst6...(Max) 0.025 / mg/L 0.014039 / lbs/day
2022 lst6...(Min) 0.01 / mg/L 0.005120 / lbs/day
2022 1st 6...(Count) 6 / 6 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
01/11/2022 P CintaS011122POTW < 0.1 / mg/L < 0.025 / lbs/day
01/12/2022 S Cintas011222Self 0.1 / mg/L 0.032 / lbs/day
02/22/2022 S Cintas022222Self 0.2 / mg/L 0.075 / lbs/day
03/18/2022 S Cintas031822Self 0.1 / mg/L 0.071 / lbs/day
04/05/2022 S Cintas04O522Self 0.1 / mg/L 0.026 / lbs/day
05/03/2022 S Cintas05O322Self < 0 / mg/L < 0.011 / lbs/day
06/15/2022 S Cintas061522Self < 0 / mg/L < 0.008 / lbs/day
Jan 2022 Week 2 < 0.1 / mg/L < 0.029 / lbs/day
Feb 2022 Week 4 0.2 / mg/L 0.075 / lbs/day
Mar 2022 Week 3 0.1 / mg/L 0.071 / lbs/day
Apr 2022 Week 1 0.1 / mg/L 0.026 / lbs/day
May 2022 Week 1 < 0 / mg/L < 0.011 / lbs/day
Jun 2022 Week 3 < 0 / mg/L < 0.008 / lbs/day
Jan 2022 Average < 0.1 / mg/L < 0.029 / lbs/day
Feb 2022 Average 0.2 / mg/L 0.075 / lbs/day
Wednesday,February 22,2023 1:31:24PM *Indicates Violation **Indicates TRC Violation Page 8 of 17

Cintas Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Nitrate-Nitrite
Mar 2022 Average 0.1 / mg/L 0.071 / lbs/day
Apr 2022 Average 0.1 / mg/L 0.026 / lbs/day
May 2022 Average < 0 / mg/L < 0.011 / lbs/day
Jun 2022 Average < 0 / mg/L < 0.008 / lbs/day
2022 Quarter 1 < 0.1 / mg/L < 0.051 / lbs/day
2022 Quarter 2 < 0 / mg/L < 0.015 / lbs/day
2022 1st 6 Months(Avg) < 0.1 / mg/L < 0.035 / lbs/day
2022 lst6...(Max) 0.2 / mg/L 0.075 / lbs/day
2022 lst6...(Min) < 0.0 / mg/L < 0.008 / lbs/day
2022 1st 6...(Count) 7 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
01/11/2022 P CintasOl1122POTW 17.2 / mg/L 8.62 / lbs/day
02/22/2022 S Cintas022222Self 61.1 / mg/L 24.064 / lbs/day
03/18/2022 S Cintas031822Self 44.1 / mg/L 22.509 / lbs/day
04/05/2022 S Cintas04O522Self 16.9 / mg/L 7.306 / lbs/day
05/03/2022 S Cintas05O322Self 11.3 / mg/L 6.172 / lbs/day
06/15/2022 S Cintas061522Self 47.3 / mg/L 18.459 / lbs/day
Jan 2022 Week 2 17.2 / mg/L 8.62 / lbs/day
Feb 2022 Week 4 61.1 / mg/L 24.064 / lbs/day
Apr 2022 Week 1 16.9 / mg/L 7.306 / lbs/day
Mar 2022 Week 3 44.1 / mg/L 22.509 / lbs/day
May 2022 Week 1 11.3 / mg/L 6.172 / lbs/day
Jun 2022 Week 3 47.3 / mg/L 18.459 / lbs/day
Jan 2022 Average 17.2 / mg/L 8.62 / lbs/day
Feb 2022 Average 61.1 / mg/L 24.064 / lbs/day
Mar 2022 Average 44.1 / mg/L 22.509 / lbs/day
Apr 2022 Average 16.9 / mg/L 7.306 / lbs/day
May 2022 Average 11.3 / mg/L 6.172 / lbs/day
Jun 2022 Average 47.3 / mg/L 18.459 / lbs/day
2022 Quarter 1 40.8 / mg/L 18.398 / lbs/day
2022 Quarter 2 25.17 / mg/L 10.645 / lbs/day
2022 1 st 6 Months(Avg) 32.98 / mg/L 14.522 / lbs/day
2022 lst6...(Max) 61.1 / mg/L 24.064 / lbs/day
2022 lst6...(Min) 11.3 / mg/L 6.172 / lbs/day
2022 lst6...(Count) 6 / 6 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,HEM(Polar)
01/11/2022 P CintasOI1122POTW < 2.5 / 100 mg/L < 1.252918 / lbs/day
01/12/2022 S CintasOI1222Self < 2.5 / 100 mg/L < 1.403872 / lbs/day
Wednesday,February 22,2023 1:31:24PM *Indicates Violation **Indicates TRC Violation Page 9 of 17

Cintas Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Oil&Grease,HEM(Polar)
02/22/2022 S Cintas022222Self 10.2 / 100 mg/L 4.017251 / lbs/day
03/18/2022 S Cintas031822Self 24.1 / 100 mg/L 12.300833 / lbs/day
04/05/2022 S CintasO4O522Self 6.9 / 100 mg/L 2.982724 / lbs/day
05/03/2022 S Cintas05O322Self < 2.5 / 100 mg/L < 1.365425 / lbs/day
06/15/2022 S Cintas061522Self 72.1 / 100 mg/L 28.136685 / lbs/day
Jan 2022 Week 2 < 2.5 / mg/L < 1.328395 / lbs/day
Feb 2022 Week 4 10.2 / mg/L 4.017251 / lbs/day
Mar 2022 Week 3 24.1 / mg/L 12.300833 / lbs/day
Apr 2022 Week 1 6.9 / mg/L 2.982724 / lbs/day
May 2022 Week 1 < 2.5 / mg/L < 1.365425 / lbs/day
Jun 2022 Week 3 72.1 / mg/L 28.136685 / lbs/day
Jan 2022 Average < 2.5 / mg/L < 1.328395 / lbs/day
Feb 2022 Average 10.2 / mg/L 4.017251 / lbs/day
Mar 2022 Average 24.1 / mg/L 12.300833 / lbs/day
Apr 2022 Average 6.9 / mg/L 2.982724 / lbs/day
May 2022 Average < 2.5 / mg/L < 1.365425 / lbs/day
Jun 2022 Average 72.1 / mg/L 28.136685 / lbs/day
2022 Quarter 1 < 9.8 / mg/L < 4.743719 / lbs/day
2022 Quarter 2 < 27.2 / mg/L < 10.828278 / lbs/day
2022 1 st 6 Months(Avg) < 17.3 / mg/L < 7.35139 / lbs/day
2022 lst6...(Max) 72.1 / mg/L 28.136685 / lbs/day
2022 lst6...(Min) < 2.5 / mg/L < 1.252918 / lbs/day
2022 lst6...(Count) 7 / 7 /
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Oil&Grease,SGT-HEM(Non-Polar)
01/11/2022 P CintaS011122POTW < 2.5 / 100 mg/L < 1.2529 / lbs/day
01/12/2022 S Cintas011222Self < 2.5 / 100 mg/L < 1.4039 / lbs/day
02/22/2022 S Cintas022222Self < 2.5 / 100 mg/L < 0.9846 / lbs/day
03/18/2022 S Cintas031822Self 6.3 / 100 mg/L 3.2156 / lbs/day
04/05/2022 S Cintas04O522Self < 2.5 / 100 mg/L < 1.0807 / lbs/day
05/03/2022 S Cintas05O322Self < 2.5 / 100 mg/L < 1.3654 / lbs/day
06/15/2022 S Cintas061522Self 11.3 / 100 mg/L 4.4098 / lbs/day
Jan 2022 Week 2 < 2.5 / mg/L < 1.3284 / lbs/day
Wednesday,February 22,2023 1:31:24PM *Indicates Violation **Indicates TRC Violation Page 10 of 17

Cintas Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,SGT-HEM(Non-Polar)
Feb 2022 Week 4 < 2.5 / mg/L < 0.9846 / lbs/day
Mar 2022 Week 3 6.3 / mg/L 3.2156 / lbs/day
Apr 2022 Week 1 < 2.5 / mg/L < 1.0807 / lbs/day
May 2022 Week 1 < 2.5 / mg/L < 1.3654 / lbs/day
Jun 2022 Week 3 11.3 / mg/L 4.4098 / lbs/day
Jan 2022 Average < 2.5 / mg/L < 1.3284 / lbs/day
Feb 2022 Average < 2.5 / mg/L < 0.9846 / lbs/day
Mar 2022 Average 6.3 / mg/L 3.2156 / lbs/day
Apr 2022 Average < 2.5 / mg/L < 1.0807 / lbs/day
May 2022 Average < 2.5 / mg/L < 1.3654 / lbs/day
Jun 2022 Average 11.3 / mg/L 4.4098 / lbs/day
2022 Quarter 1 < 3.5 / mg/L < 1.7142 / lbs/day
2022 Quarter 2 < 5.4 / mg/L < 2.2853 / lbs/day
2022 1 st 6 Months(Avg) < 4.3 / mg/L < 1.9590 / lbs/day
2022 lst6...(Max) 11.3 / mg/L 4.4098 / lbs/day
2022 lst6...(Min) < 2.5 / mg/L < 0.9846 / lbs/day
2022 1st6...(Count) 7 / 7 /
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
01/11/2022 P CintaS011122POTW 7.2 /6.0-10.5 SU /
01/12/2022 S Cintas011222Self 6.7 /6.0-10.5 SU /
02/22/2022 S Cintas022222Self 7.2 /6.0-10.5 SU /
03/18/2022 S Cintas031822Self 7.2 /6.0-10.5 SU /
04/05/2022 S Cintas04O522Self 7.3 /6.0-10.5 SU /
05/03/2022 S Cintas05O322Self 7.3 /6.0-10.5 SU /
06/15/2022 S Cintas061522Self 7.4 /6.0-10.5 SU /
Jan 2022 Week 2 6.95 / SU /
Feb 2022 Week 4 7.2 / SU /
Mar 2022 Week 3 7.2 / SU /
Apr 2022 Week 1 7.3 / SU /
May 2022 Week 1 7.3 / SU /
Jun 2022 Week 3 7.4 / SU /
Jan 2022 Average 6.95 / SU /
Wednesday,February 22,2023 1:31:24PM *Indicates Violation **Indicates TRC Violation Page 11 of 17

Cintas Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
pH
Feb 2022 Average 7.2 / SU /
Mar 2022 Average 7.2 / SU /
Apr 2022 Average 7.3 / SU /
May 2022 Average 7.3 / SU /
Jun 2022 Average 7.4 / SU /
2022 Quarter 1 7.08 / SU /
2022 Quarter 2 7.33 / SU /
2022 1 st 6 Months(Avg) 7.19 / SU /
2022 lst6...(Max) 7.4 / SU /
2022 lst6...(Min) 6.7 / SU /
2022 lst6...(Count) 7
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
01/11/2022 P CintaS011122POTW 20 /66 °C /
01/12/2022 S CintaS011222Self 25.7 /66 °C /
02/22/2022 S Cintas022222Self 26.9 /66 °C /
03/18/2022 S Cintas031822Self 27.9 /66 °C /
04/05/2022 S Cintas040522Se1f 31.9 /66 °C /
05/03/2022 S Cintas050322Se1f 30.8 /66 °C /
06/15/2022 S Cintas061522Self 37.9 /66 °C /
Jan 2022 Week 2 22.9 / °C /
Feb 2022 Week 4 26.9 / °C /
Mar 2022 Week 3 27.9 / °C /
Apr 2022 Week 1 31.9 / °C /
May 2022 Week 1 30.8 / °C /
Jun 2022 Week 3 37.9 / °C /
Jan 2022 Average 22.9 / °C /
Feb 2022 Average 26.9 / °C /
Mar 2022 Average 27.9 / °C /
Apr 2022 Average 31.9 / °C /
May 2022 Average 30.8 / °C /
Jun 2022 Average 37.9 / °C /
2022 Quarter 1 25.1 / °C /
Wednesday,February 22,2023 1:31:24PM *Indicates Violation **Indicates TRC Violation Page 12 of 17

Cintas Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Temperature
2022 Quarter 2 33.5 / °C /
2022 1 st 6 Months(Avg) 28.7 / °C /
2022 lst6...(Max) 37.9 / °C /
2022 lst6...(Min) 20 / °C /
2022 lst6...(Count) 7
■
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
01/11/2022 P CintaS011122POTW 17.2 / mg/L 8.62 / lbs/day
02/10/2022 P Cintas021022POTW 20.7 / mg/L /
03/15/2022 P Cintas031522POTW 42.2 / mg/L /
03/18/2022 S Cintas031822Self 44 / mg/L 22.458 / lbs/day
04/05/2022 S Cintas04O522Self 16.9 / mg/L 7.306 / lbs/day
04/26/2022 P Cintas042622POTW 33 / mg/L /
05/03/2022 S Cintas050322Self 11.3 / mg/L 6.172 / lbs/day
05/24/2022 P CintaS052422POTW 38 / mg/L /
06/09/2022 P Cintas06O922POTW 66.9 / mg/L /
06/15/2022 S Cintas061522Self 47.3 / mg/L 18.459 / lbs/day
06/21/2022 P Cintas062122POTW 36.1 / mg/L /
Jan 2022 Week 2 17.2 / mg/L 8.62 / lbs/day
Feb 2022 Week 2 20.7 / mg/L /
Mar 2022 Week 3 43.1 / mg/L 22.458 / lbs/day
Apr 2022 Week 1 16.9 / mg/L 7.306 / lbs/day
Apr 2022 Week 4 33 / mg/L /
May 2022 Week 1 11.3 / mg/L 6.172 / lbs/day
May 2022 Week 4 38 / mg/L /
Jun 2022 Week 2 66.9 / mg/L /
Jun 2022 Week 3 41.7 / mg/L 18.459 / lbs/day
Jan 2022 Average 17.2 / mg/L 8.62 / lbs/day
Feb 2022 Average 20.7 / mg/L /
Mar 2022 Average 43.1 / mg/L 22.458 / lbs/day
Apr 2022 Average 24.95 / mg/L 7.306 / lbs/day
May 2022 Average 24.65 / mg/L 6.172 / lbs/day
Jun 2022 Average 50.1 / mg/L 18.459 / lbs/day
Wednesday,February 22,2023 1:31:24PM *Indicates Violation **Indicates TRC Violation Page 13 of 17

Cintas Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
TKN
2022 Quarter 1 31.03 / mg/L 15.539 / lbs/day
2022 Quarter 2 35.64 / mg/L 10.645 / lbs/day
2022 1 st 6 Months(Avg) 33.96 / mg/L 12.603 / lbs/day
2022 lst6...(Max) 66.9 / mg/L 22.458 / lbs/day
2022 lst6...(Min) 11.3 / mg/L /
2022 lst6...(Count) 11 / 5 /
Sample Date SampleID Result/Limit Mass/Limit
Total Petroleum Hydrocarbon
01/12/2022 S CintaS011222Self < 2.5 / mg/L < 1.404 / lbs/day
Jan 2022 Week 2 < 2.5 / mg/L < 1.404 / lbs/day
Jan 2022 Average < 2.5 / mg/L < 1.404 / lbs/day
2022 Quarter 1 < 2.5 / mg/L < 1.404 / lbs/day
2022 1 st 6 Months(Avg) < 2.5 / mg/L < 1.404 / lbs/day
2022 lst6...(Max) < 2.5 / mg/L < 1.404 / lbs/day
2022 lst6...(Min) < 2.5 / mg/L < 1.404 / lbs/day
2022 lst6...(Count) 1 / 1 /
Sample Date Sample-ID Result/Limit Mass/Limit
Total Phosphorus
01/11/2022 P CintasOI1122POTW 1.72 / mg/L 0.862 / lbs/day
01/12/2022 S CintasO11222Self 1.5 / mg/L 0.8423 / lbs/day
02/10/2022 P Cintas021022POTW 1.78 / mg/L /
02/22/2022 S Cintas022222Self 5.6 / mg/L 2.2055 / lbs/day
03/15/2022 P Cintas031522POTW 3.99 / mg/L /
03/18/2022 S Cintas031822Self 4.3 / mg/L 2.1948 / lbs/day
04/05/2022 S CintasO4O522Self 1.1 / mg/L 0.4755 / lbs/day
04/26/2022 P Cintas042622POTW 4 / mg/L /
05/03/2022 S Cintas05O322Self 1 / mg/L 0.5462 / lbs/day
05/24/2022 P Cintas052422POTW 7.29 / mg/L /
06/09/2022 P Cintas06O922POTW 3 / mg/L /
06/15/2022 S Cintas061522Self 4.7 / mg/L 1.8342 / lbs/day
06/21/2022 P Cintas062122POTW 2.21 / mg/L /
Jan 2022 Week 2 1.61 / mg/L 0.8522 / lbs/day
Feb 2022 Week 2 1.78 / mg/L /
Feb 2022 Week 4 5.6 / mg/L 2.2055 / lbs/day
Mar 2022 Week 3 4.145 / mg/L 2.1948 / lbs/day
Apr 2022 Week 1 1.1 / mg/L 0.4755 / lbs/day
Apr 2022 Week 4 4 / mg/L /
May 2022 Week 1 1 / mg/L 0.5462 / lbs/day
May 2022 Week 4 7.29 / mg/L /
Jun 2022 Week 2 3 / mg/L /
Wednesday,February 22,2023 1:31:24PM *Indicates Violation **Indicates TRC Violation Page 14 of 17

Cintas Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Total Phosphorus
Jun 2022 Week 3 3.455 / mg/L 1.8342 / lbs/day
Jan 2022 Average 1.61 / mg/L 0.8522 / lbs/day
Feb 2022 Average 3.69 / mg/L 2.2055 / lbs/day
Mar 2022 Average 4.145 / mg/L 2.1948 / lbs/day
Apr 2022 Average 2.55 / mg/L 0.4755 / lbs/day
May 2022 Average 4.145 / mg/L 0.5462 / lbs/day
Jun 2022 Average 3.303 / mg/L 1.8342 / lbs/day
2022 Quarter 1 3.148 / mg/L 1.5262 / lbs/day
2022 Quarter 2 3.329 / mg/L 0.9519 / lbs/day
2022 1 st 6 Months(Avg) 3.245 / mg/L 1.2801 / lbs/day
2022 lst6...(Max) 7.29 / mg/L 2.2055 / lbs/day
2022 lst6...(Min) 1 / mg/L /
2022 lst6...(Count) 13 / 7 /
Sample Date SampleID Result/Limit Mass/Limit
TSS
01/11/2022 P CintaS011122POTW 145 / mg/L 72.669256 / lbs/day
01/12/2022 S Cintas011222Self 177 / mg/L 99.394152 / lbs/day
02/10/2022 P Cintas021022POTW 240 / mg/L /
02/22/2022 S Cintas022222Self 174 / mg/L 68.52958 / lbs/day
03/15/2022 P Cintas031522POTW 252 / mg/L /
03/18/2022 S Cintas031822Self 162 / mg/L 82.686096 / lbs/day
04/05/2022 S Cintas04O522Self 136 / mg/L 58.789928 / lbs/day
04/26/2022 P Cintas042622POTW 786 / mg/L /
05/03/2022 S Cintas05O322Self 66 / mg/L 36.047215 / lbs/day
05/24/2022 P Cintas052422POTW 256 / mg/L /
06/09/2022 P Cintas06O922POTW 298 / mg/L /
06/15/2022 S Cintas061522Self 164 / mg/L 64.000226 / lbs/day
06/21/2022 P Cintas062122POTW 520 / mg/L /
Jan 2022 Week 2 161 / mg/L 86.031704 / lbs/day
Feb 2022 Week 2 240 / mg/L /
Feb 2022 Week 4 174 / mg/L 68.52958 / lbs/day
Mar 2022 Week 3 207 / mg/L 82.686096 / lbs/day
Apr 2022 Week 1 136 / mg/L 58.789928 / lbs/day
Apr 2022 Week 4 786 / mg/L /
May 2022 Week 1 66 / mg/L 36.047215 / lbs/day
May 2022 Week 4 256 / mg/L /
Jun 2022 Week 2 298 / mg/L /
Jun 2022 Week 3 342 / mg/L 64.000226 / lbs/day
Jan 2022 Average 161 / mg/L 86.031704 / lbs/day
Feb 2022 Average 207 / mg/L 68.52958 / lbs/day
Mar 2022 Average 207 / mg/L 82.686096 / lbs/day
Wednesday,February 22,2023 1:31:24PM *Indicates Violation **Indicates TRC Violation Page 15 of 17

Cintas Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
TSS
Apr 2022 Average 461 / mg/L 58.789928 / lbs/day
May 2022 Average 161 / mg/L 36.047215 / lbs/day
Jun 2022 Average 327.3 / mg/L 64.000226 / lbs/day
2022 Quarter 1 191.7 / mg/L 80.819771 / lbs/day
2022 Quarter 2 318 / mg/L 52.945789 / lbs/day
2022 1 st 6 Months(Avg) 259.7 / mg/L 68.8738 / lbs/day
2022 lst6...(Max) 786 / mg/L 99.394152 / lbs/day
2022 1st6...(Min) 66 / mg/L /
2022 1st 6...(Count) 13 / 7 /
Sample Date SampleID Result/Limit Mass/Limit
VOC
01/12/2022 S CintaS011222Self < 0.001 / mg/L < /
Jan 2022 Week 2 < 0.001 / mg/L < /
Jan 2022 Average < 0.001 / mg/L < /
2022 Quarter 1 < 0.001 / mg/L < /
2022 1 st 6 Months(Avg) < 0.001 / mg/L < /
2022 lst6...(Max) < 0.001 / mg/L < /
2022 lst6...(Min) < 0.001 / mg/L < /
2022 lst6...(Count) 1
Sample Date SampleID Result/Limit Mass/Limit
Zinc
01/12/2022 S CintasO11222Self 1.4 / mg/L 0.786168 / lbs/day
02/22/2022 S Cintas022222Self 0.75 / mg/L 0.295386 / lbs/day
03/18/2022 S Cintas031822Self 0.81 / mg/L 0.41343 / lbs/day
04/05/2022 S CintasO4O522Self 0.7 / mg/L 0.302595 / lbs/day
05/03/2022 S Cintas05O322Self 0.66 / mg/L 0.360472 / lbs/day
06/15/2022 S Cintas061522Self 0.58 / mg/L 0.226342 / lbs/day
Jan 2022 Week 2 1.4 / mg/L 0.786168 / lbs/day
Feb 2022 Week 4 0.75 / mg/L 0.295386 / lbs/day
Mar 2022 Week 3 0.81 / mg/L 0.41343 / lbs/day
Apr 2022 Week 1 0.7 / mg/L 0.302595 / lbs/day
May 2022 Week 1 0.66 / mg/L 0.360472 / lbs/day
Jun 2022 Week 3 0.58 / mg/L 0.226342 / lbs/day
Jan 2022 Average 1.4 / mg/L 0.786168 / lbs/day
Feb 2022 Average 0.75 / mg/L 0.295386 / lbs/day
Mar 2022 Average 0.81 / mg/L 0.41343 / lbs/day
Apr 2022 Average 0.7 / mg/L 0.302595 / lbs/day
May 2022 Average 0.66 / mg/L 0.360472 / lbs/day
Jun 2022 Average 0.58 / mg/L 0.226342 / lbs/day
2022 Quarter 1 0.987 / mg/L 0.498328 / lbs/day
Wednesday,February 22,2023 1:31:24PM *Indicates Violation **Indicates TRC Violation Page 16 of 17

Cintas Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Zinc
2022 Quarter 2 0.647 / mg/L 0.29647 / lbs/day
2022 1 st 6 Months(Avg) 0.817 / mg/L 0.397399 / lbs/day
2022 lst6...(Max) 1.4 / mg/L 0.786168 / lbs/day
2022 lst6...(Min) 0.58 / mg/L 0.226342 / lbs/day
2022 Ist 6...(Count) 6 / 6 /
Wednesday,February 22,2023 1:31:24PM *Indicates Violation **Indicates TRC Violation Page 17 of 17

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: '001
Sample Date Sample-ID Result/Limit Mass/Limit
Aluminum
01/19/2022 S Micross011922Self 0.078 / mg/L /
01/25/2022 P Micross012522POTW 0.013 / mg/L /
Jan 2022 Week 3 0.078 / mg/L /
Jan 2022 Week 4 0.013 / mg/L /
Jan 2022 Average 0.046 / mg/L /
2022 Quarter 1 0.046 / mg/L /
2022 1 st 6 Months(Avg) 0.046 / mg/L /
2022 lst6...(Max) 0.078 / mg/L /
2022 lst6...(Min) 0.013 / mg/L /
2022 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
01/19/2022 S Micross011922Self 4.5 / mg/L /
01/25/2022 P MicrossOl2522POTW 2.8 / mg/L /
Jan 2022 Week 3 4.5 / mg/L /
Jan 2022 Week 4 2.8 / mg/L /
Jan 2022 Average 3.65 / mg/L /
2022 Quarter 1 3.65 / mg/L /
2022 1 st 6 Months(Avg) 3.65 / mg/L /
2022 lst6...(Max) 4.5 / mg/L /
2022 lst6...(Min) 2.8 / mg/L /
2022 lst6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2022 S Micross0122F1ow 0.024119 /0.100 MGD /
02/28/2022 S Micross0222F1ow 0.02528 /0.100 MGD /
03/30/2022 S Micross0322F1ow 0.029667 /0.100 MGD /
04/30/2022 S Micross0422F1ow 0.040061 /0.100 MGD /
05/31/2022 S Micross0522F1ow 0.035281 /0.100 MGD /
06/30/2022 S Micross0622F1ow 0.041131 /0.100 MGD /
Jan 2022 Week 4 0.024119 / MGD /
Feb 2022 Week 4 0.02528 / MGD /
Mar 2022 Week 4 0.029667 / MGD /
Apr 2022 Week 4 0.040061 / MGD /
May 2022 Week 4 0.035281 / MGD /
Jun 2022 Week 4 0.041131 / MGD /
Jan 2022 Average 0.024119 /0.075 MGD /
Feb 2022 Average 0.02528 /0.075 MGD /
Mar 2022 Average 0.029667 /0.075 MGD /
Apr 2022 Average 0.040061 /0.075 MGD /
Tuesday,February 21,2023 2:37:46PM *Indicates Violation **Indicates TRC Violation Page 1 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SampleID Result/Limit Mass/Limit
Average Flow for Month
May 2022 Average 0.035281 /0.075 MGD /
Jun 2022 Average 0.041131 /0.075 MGD /
2022 Quarter 1 0.026355 / MGD /
2022 Quarter 2 0.038824 / MGD /
2022 1 st 6 Months(Avg) 0.032590 / MGD /
2022 lst6...(Max) 0.041131 / MGD /
2022 Ist6...(Min) 0.024119 / MGD /
2022 Ist 6...(Count) 6
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Chloride
01/19/2022 S MicrossO11922Self 24 / mg/L /
01/25/2022 P MicrossOl2522POTW 25.4 / mg/L /
Jan 2022 Week 3 24 / mg/L /
Jan 2022 Week 4 25.4 / mg/L /
Jan 2022 Average 24.7 / mg/L /
2022 Quarter 1 24.7 / mg/L /
2022 1 st 6 Months(Avg) 24.7 / mg/L /
2022 lst6...(Max) 25.4 / mg/L /
2022 lst6...(Min) 24 / mg/L /
2022 lst6...(Count) 2
Sample Date SampleID Result/Limit Mass/Limit
Chromium
01/19/2022 S Micross011922Self 0.004 / mg/L /
01/25/2022 P Micross012522POTW < 0.001 / mg/L < /
Jan 2022 Week 3 0.004 / mg/L /
Jan 2022 Week 4 < 0.001 / mg/L < /
Jan 2022 Average < 0.003 / mg/L < /
2022 Quarter 1 < 0.003 / mg/L < /
2022 1 st 6 Months(Avg) < 0.003 / mg/L < /
2022 lst6...(Max) 0.004 / mg/L /
2022 Ist6...(Min) < 0.001 / mg/L < /
Tuesday,February 21,2023 2:37:46PM *Indicates Violation **Indicates TRC Violation Page 2 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
2022 1st 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Copper
01/19/2022 S Micross011922Self 0.046 / mg/L /
01/25/2022 P Micross012522POTW 0.026 / mg/L /
Jan 2022 Week 3 0.046 / mg/L /
Jan 2022 Week 4 0.026 / mg/L /
Jan 2022 Average 0.036 / mg/L /
2022 Quarter 1 0.036 / mg/L /
2022 1 st 6 Months(Avg) 0.036 / mg/L /
2022 lst6...(Max) 0.046 / mg/L /
2022 lst6...(Min) 0.026 / mg/L /
2022 lst6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
01/19/2022 S Micross011922Self 0.007 / mg/L /
Jan 2022 Week 3 0.007 / mg/L /
Jan 2022 Average 0.007 / mg/L /
2022 Quarter 1 0.007 / mg/L /
2022 1 st 6 Months(Avg) 0.007 / mg/L /
2022 lst6...(Max) 0.007 / mg/L /
2022 lst6...(Min) 0.007 / mg/L /
2022 lst6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
01/19/2022 S MicrossO11922Self 1.1 / mg/L /
01/25/2022 P MicrossO12522POTW 1 / mg/L /
Jan 2022 Week 3 1.1 / mg/L /
Jan 2022 Week 4 1 / mg/L /
Jan 2022 Average 1.05 / mg/L /
2022 Quarter 1 1.05 / mg/L /
2022 1 st 6 Months(Avg) 1.05 / mg/L /
2022 lst6...(Max) 1.1 / mg/L /
2022 lst6...(Min) 1 / mg/L /
2022 lst6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Lead
Tuesday,February 21,2023 2:37:46PM *Indicates Violation **Indicates TRC Violation Page 3 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SampleID Result/Limit Mass/Limit
Lead
01/19/2022 S Micross011922Self 0.0103 / mg/L /
Jan 2022 Week 3 0.0103 / mg/L /
Jan 2022 Average 0.0103 / mg/L /
2022 Quarter 1 0.0103 / mg/L /
2022 1 st 6 Months(Avg) 0.0103 / mg/L /
2022 lst6...(Max) 0.0103 / mg/L /
2022 lst6...(Min) 0.0103 / mg/L /
2022 lst6...(Count) 1
Sample Date SampleID Result/Limit Mass/Limit
Mercury-LL
01/07/2022 S Micross010722Se1fHg 0.000003 /0.000142 mg/L /
05/09/2022 P Micross05O922POTW 0.000006 /0.000142 mg/L /
Hg
Jan 2022 Week 1 0.000003 / mg/L /
May 2022 Week 2 0.000006 / mg/L /
Jan 2022 Average 0.000003 / mg/L /
May 2022 Average 0.000006 / mg/L /
2022 Quarter 1 0.000003 / mg/L /
2022 Quarter 2 0.000006 / mg/L /
2022 1 st 6 Months(Avg) 0.000005 / mg/L /
2022 lst6...(Max) 0.000006 / mg/L /
2022 lst6...(Min) 0.000003 / mg/L /
2022 lst6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Molybdenum
01/19/2022 S Micross011922Self 0.031 / mg/L /
Jan 2022 Week 3 0.031 / mg/L /
Jan 2022 Average 0.031 / mg/L /
2022 Quarter 1 0.031 / mg/L /
2022 1 st 6 Months(Avg) 0.031 / mg/L /
2022 lst6...(Max) 0.031 / mg/L /
2022 lst6...(Min) 0.031 / mg/L /
Tuesday,February 21,2023 2:37:46PM *Indicates Violation **Indicates TRC Violation Page 4 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
2022 1st 6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
01/19/2022 S Micross011922Self 0.0046 / mg/L /
01/25/2022 P Micross012522POTW 0.0019 / mg/L /
Jan 2022 Week 3 0.0046 / mg/L /
Jan 2022 Week 4 0.0019 / mg/L /
Jan 2022 Average 0.0033 / mg/L /
2022 Quarter 1 0.0033 / mg/L /
2022 1 st 6 Months(Avg) 0.0033 / mg/L /
2022 lst6...(Max) 0.0046 / mg/L /
2022 lst6...(Min) 0.0019 / mg/L /
2022 lst6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
01/19/2022 S Micross011922Self 0.9 / mg/L /
01/25/2022 P Micross012522POTW 1.4 / mg/L /
Jan 2022 Week 3 0.9 / mg/L /
Jan 2022 Week 4 1.4 / mg/L /
Jan 2022 Average 1.2 / mg/L /
2022 Quarter 1 1.2 / mg/L /
2022 1 st 6 Months(Avg) 1.2 / mg/L /
2022 lst6...(Max) 1.4 / mg/L /
2022 1st6...(Min) 0.9 / mg/L /
2022 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
01/25/2022 P Micross012522POTW 11.3 / mg/L /
Jan 2022 Week 4 11.3 / mg/L /
Jan 2022 Average 11.3 / mg/L /
2022 Quarter 1 11.3 / mg/L /
2022 1 st 6 Months(Avg) 11.3 / mg/L /
2022 lst6...(Max) 11.3 / mg/L /
2022 lst6...(Min) 11.3 / mg/L /
2022 lst6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
Tuesday,February 21,2023 2:37:46PM *Indicates Violation **Indicates TRC Violation Page 5 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: '001
Sample Date Sample-ID Result/Limit Mass/Limit
Oil&Grease,Total
01/19/2022 S Micross011922Self < 2.5 /200 mg/L < /
01/25/2022 P Micross012522POTW < 2.5 /200 mg/L < /
Jan 2022 Week 3 < 2.5 / mg/L < /
Jan 2022 Week 4 < 2.5 / mg/L < /
Jan 2022 Average < 2.5 / mg/L < /
2022 Quarter 1 < 2.5 / mg/L < /
2022 1 st 6 Months(Avg) < 2.5 / mg/L < /
2022 lst6...(Max) < 2.5 / mg/L < /
2022 lst6...(Min) < 2.5 / mg/L < /
2022 lst6...(Count) 2
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Organic Compounds
01/19/2022 S Micross011922Self 0.004 / mg/L /
Jan 2022 Week 3 0.004 / mg/L /
Jan 2022 Average 0.004 / mg/L /
2022 Quarter 1 0.004 / mg/L /
2022 1 st 6 Months(Avg) 0.004 / mg/L /
2022 lst6...(Max) 0.004 / mg/L /
2022 lst6...(Min) 0.004 / mg/L /
2022 lst6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
pH
01/07/2022 S Micross010722SelfHg 7 /5.5-10.5 SU /
01/19/2022 S Micross011922Self 7.1 /5.5-10.5 SU /
01/25/2022 P Micross012522POTW 7.2 /5.5-10.5 SU /
Jan 2022 Week 1 7 / SU /
Jan 2022 Week 3 7.1 / SU /
Jan 2022 Week 4 7.2 / SU /
Jan 2022 Average 7.1 / SU /
2022 Quarter 1 7.1 / SU /
2022 1 st 6 Months(Avg) 7.1 / SU /
Tuesday,February 21,2023 2:37:46PM *Indicates Violation **Indicates TRC Violation Page 6 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
pH
2022 lst6...(Max) 7.2 / SU /
2022 lst6...(Min) 7 / SU /
2022 lst6...(Count) 3 / /
Sample Count: 3 Months Sampled: 1 Weeks Sampled: 3 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Silver
01/19/2022 S Micross011922Self 0.0004 / mg/L /
Jan 2022 Week 3 0.0004 / mg/L /
Jan 2022 Average 0.0004 / mg/L /
2022 Quarter 1 0.0004 / mg/L /
2022 1 st 6 Months(Avg) 0.0004 / mg/L /
2022 lst6...(Max) 0.0004 / mg/L /
2022 lst6...(Min) 0.0004 / mg/L /
2022 lst6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
01/07/2022 S Micross010722SelfHg 16.6 /66 °C /
01/19/2022 S Micross011922Self 13.3 /66 °C /
01/25/2022 P Micross012522POTW 17 /66 °C /
Jan 2022 Week 1 16.6 / °C /
Jan 2022 Week 3 13.3 / °C /
Jan 2022 Week 4 17 / °C /
Jan 2022 Average 15.6 / °C /
2022 Quarter 1 15.6 / °C /
2022 1 st 6 Months(Avg) 15.6 / °C /
2022 lst6...(Max) 17 / °C /
2022 lst6...(Min) 13.3 / °C /
2022 lst6...(Count) 3
Tuesday,February 21,2023 2:37:46PM *Indicates Violation **Indicates TRC Violation Page 7 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: '001
Sample Count: 3 Months Sampled: 1 Weeks Sampled: 3 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Tin
01/19/2022 S Micross011922Self 0.020500000 / mg/L /
Jan 2022 Week 3 0 / mg/L /
Jan 2022 Average 0 / mg/L /
2022 Quarter 1 0 / mg/L /
2022 1 st 6 Months(Avg) 0 / mg/L /
2022 lst6...(Max) 0 / mg/L /
2022 1st6...(Min) 0 / mg/L /
2022 1st6...(Count) 1
Sample Date SampleLD Result/Limit Mass/Limit
TKN
01/19/2022 S MicrossO11922Self 8.2 / mg/L /
01/25/2022 P MicrossOl2522POTW 9.87 / mg/L /
Jan 2022 Week 3 8.2 / mg/L /
Jan 2022 Week 4 9.87 / mg/L /
Jan 2022 Average 9.04 / mg/L /
2022 Quarter 1 9.04 / mg/L /
2022 1 st 6 Months(Avg) 9.04 / mg/L /
2022 lst6...(Max) 9.87 / mg/L /
2022 lst6...(Min) 8.2 / mg/L /
2022 lst6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
01/19/2022 S Micross011922Self 5.6 / mg/L /
Jan 2022 Week 3 5.6 / mg/L /
Jan 2022 Average 5.6 / mg/L /
2022 Quarter 1 5.6 / mg/L /
2022 1 st 6 Months(Avg) 5.6 / mg/L /
2022 lst6...(Max) 5.6 / mg/L /
2022 1st6...(Min) 5.6 / mg/L /
2022 1st6...(Count) 1 / /
Tuesday,February 21,2023 2:37:46PM *Indicates Violation **Indicates TRC Violation Page 8 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
VOC
01/19/2022 S Micross011922Self 0.0031 / mg/L /
Jan 2022 Week 3 0.0031 / mg/L /
Jan 2022 Average 0.0031 / mg/L /
2022 Quarter 1 0.0031 / mg/L /
2022 1 st 6 Months(Avg) 0.0031 / mg/L /
2022 lst6...(Max) 0.0031 / mg/L /
2022 1st6...(Min) 0.0031 / mg/L /
2022 1st6...(Count) 1 / /
Sample Date SampleID Result/Limit Mass/Limit
Zinc
01/19/2022 S Micross011922Self 0.661 / mg/L /
Jan 2022 Week 3 0.661 / mg/L /
Jan 2022 Average 0.661 / mg/L /
2022 Quarter 1 0.661 / mg/L /
2022 1 st 6 Months(Avg) 0.661 / mg/L /
2022 lst6...(Max) 0.661 / mg/L /
2022 lst6...(Min) 0.661 / mg/L /
2022 lst6...(Count) 1
Tuesday,February 21,2023 2:37:46PM *Indicates Violation **Indicates TRC Violation Page 9 of 9

MP Pharma Services, Inc.
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
02/23/2022 S MPPharma022322Se < 0.013 / 20.7 mg/L < /
if
06/13/2022 P MPPhanna06l322P < 0.025 / 20.7 mg/L < /
OTW
Feb 2022 Week 4 < 0.013 / mg/L < /
Jun 2022 Week 2 < 0.025 / mg/L < /
Feb 2022 Average < 0.013 / 8.2 mg/L < /
Jun 2022 Average < 0.025 / 8.2 mg/L < /
2022 Quarter 1 < 0.013 / mg/L < /
2022 Quarter 2 < 0.025 / mg/L < /
2022 1 st 6 Months(Avg) < 0.019 / mg/L < /
2022 lst6...(Max) < 0.025 / mg/L < /
2022 lst6...(Min) < 0.013 / mg/L < /
2022 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2022 S MPPharma0122F1ow 0.036194 / MGD /
02/28/2022 S MPPhanna0222F1ow 0.032877 / MGD /
04/01/2022 S MPPharrna0322Flow 0.01643 / MGD /
04/30/2022 S MPPharrna0422Flow 0.001364 / MGD /
05/31/2022 S MPPharma0522Flow 0.001641 / MGD /
06/30/2022 S MPPharma0622F1ow 0.001785 / MGD /
Jan 2022 Week 4 0.036194 / MGD /
Apr 2022 Week 1 0.01643 / MGD /
Feb 2022 Week 4 0.032877 / MGD /
Apr 2022 Week 4 0.001364 / MGD /
May 2022 Week 4 0.001641 / MGD /
Jun 2022 Week 4 0.001785 / MGD /
Jan 2022 Average 0.036194 / 0.002 MGD * /
Feb 2022 Average 0.032877 / 0.002 MGD * /
Apr 2022 Average 0.008897 / 0.002 MGD * /
May 2022 Average 0.001641 / 0.002 MGD /
Jun 2022 Average 0.001785 / 0.002 MGD /
2022 Quarter 1 0.034536 / MGD /
2022 Quarter 2 0.005305 / MGD /
2022 1 st 6 Months(Avg) 0.015049 / MGD /
2022 lst6...(Max) 0.036194 / MGD /
Tuesday,February 21,2023 10:56:35PM *Indicates Violation **Indicates TRC Violation Page 1 of 4

MP Pharma Services, Inc.
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
2022 1st 6...(Min) 0.001364 / MGM /
2022 lst6...(Count) 6
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
02/23/2022 S MPPharma022322Se < 0.05 / 20.7 mg/L < /
if
06/13/2022 P MPPharma06l322P < 0.005 / 20.7 mg/L < /
OTW
Feb 2022 Week 4 < 0.05 / mg/L < /
Jun 2022 Week 2 < 0.005 / mg/L < /
Feb 2022 Average < 0.05 / 8.2 mg/L < /
Jun 2022 Average < 0.005 / 8.2 mg/L < /
2022 Quarter 1 < 0.05 / mg/L < /
2022 Quarter 2 < 0.005 / mg/L < /
2022 1 st 6 Months(Avg) < 0.028 / mg/L < /
2022 lst6...(Max) < 0.05 / mg/L < /
2022 lst6...(Min) < 0.005 / mg/L < /
2022 lst6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
02/23/2022 S MPPharma022322Se < 0.05 / 20.7 mg/L < /
if
06/13/2022 P MPPhartna06l322P < 0.005 / 20.7 mg/L < /
OTW
Feb 2022 Week 4 < 0.05 / mg/L < /
Jun 2022 Week 2 < 0.005 / mg/L < /
Feb 2022 Average < 0.05 / 8.2 mg/L < /
Jun 2022 Average < 0.005 / 8.2 mg/L < /
2022 Quarter 1 < 0.05 / mg/L < /
2022 Quarter 2 < 0.005 / mg/L < /
2022 1 st 6 Months(Avg) < 0.028 / mg/L < /
2022 lst6...(Max) < 0.05 / mg/L < /
2022 lst6...(Min) < 0.005 / mg/L < /
2022 lst6...(Count) 2 / /
Tuesday,February 21,2023 10:56:35PM *Indicates Violation **Indicates TRC Violation Page 2 of 4

MP Pharma Services, Inc.
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
06/13/2022 P MPPharrna06l322P < 0.000001 / 0.000142 mg/L < /
OTWHg
Jun 2022 Week 2 < 0.000001 / mg/L < /
Jun 2022 Average < 0.000001 / mg/L < /
2022 Quarter 2 < 0.000001 / mg/L < /
2022 1 st 6 Months(Avg) < 0.000001 / mg/L < /
2022 1st 6...(Max) < 0.000001 / mg/L < /
2022 1st6...(Min) < 0.000001 / mg/L < /
2022 lst6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
06/13/2022 P MPPharma06l322P < 0.005 / 3.0 mg/L < /
OTW
Jun 2022 Week 2 < 0.005 / mg/L < /
Jun 2022 Average < 0.005 / 0.7 mg/L < /
2022 Quarter 2 < 0.005 / mg/L < /
2022 1 st 6 Months(Avg) < 0.005 / mg/L < /
2022 lst6...(Max) < 0.005 / mg/L < /
2022 lst6...(Min) < 0.005 / mg/L < /
2022 lst6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
02/23/2022 S MPPharrna022322Se < 0.025 / 20.7 mg/L < /
if
06/13/2022 P MPPharma061322P < 0.005 / 20.7 mg/L < /
OTW
Feb 2022 Week 4 < 0.025 / mg/L < /
Jun 2022 Week 2 < 0.005 / mg/L < /
Feb 2022 Average < 0.025 / 8.2 mg/L < /
Jun 2022 Average < 0.005 / 8.2 mg/L < /
2022 Quarter 1 < 0.025 / mg/L < /
2022 Quarter 2 < 0.005 / mg/L < /
2022 1 st 6 Months(Avg) < 0.015 / mg/L < /
2022 lst6...(Max) < 0.025 / mg/L < /
2022 lst6...(Min) < 0.005 / mg/L < /
2022 1st 6...(Count) 2
Tuesday,February 21,2023 10:56:35PM *Indicates Violation **Indicates TRC Violation Page 3 of 4

MP Pharma Services, Inc.
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
PH
02/23/2022 S MPPharma022322Se 7.53 / 6.0-10.0 Su /
if
Feb 2022 Week 4 7.53 / Su /
Feb 2022 Average 7.53 / Su /
2022 Quarter 1 7.53 / su /
2022 1 st 6 Months(Avg) 7.53 / su /
2022 1st 6...(Max) 7.53 / su /
2022 1st 6...(Min) 7.53 / Su /
2022 lst6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
02/23/2022 S MPPharma022322Se 21.6 / 66 °C /
if
Feb 2022 Week 4 21.6 / °C /
Feb 2022 Average 21.6 / °C /
2022 Quarter 1 21.6 / °C /
2022 1 st 6 Months(Avg) 21.6 / °C /
2022 lst6...(Max) 21.6 / °C /
2022 lst6...(Min) 21.6 / °C /
2022 lst6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
VOC
02/23/2022 S MPPharrna022322Se 0.0065 / mg/L /
if
Feb 2022 Week 4 0.0065 / mg/L /
Feb 2022 Average 0.0065 / mg/L /
2022 Quarter 1 0.0065 / mg/L /
2022 1 st 6 Months(Avg) 0.0065 / mg/L /
2022 lst6...(Max) 0.0065 / mg/L /
2022 1st 6...(Min) 0.0065 / mg/L /
2022 lst6...(Count) 1
Tuesday,February 21,2023 10:56:35PM *Indicates Violation **Indicates TRC Violation Page 4 of 4

Phononic
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Average Flow for Month
01/31/2022 S Phononic0122F1ow 0.016172 / MGD /
02/28/2022 S Phononic0222F1ow 0.01768 / MGD /
03/31/2022 S Phononic0322F1ow 0.014415 / MGD /
04/30/2022 S Phononic0422F1ow 0.032 / MGD /
05/31/2022 S Phononic0522F1ow 0.032 / MGD /
06/30/2022 S Phononic0622F1ow 0.025 / MGD /
Jan 2022 Week 4 0.016172 / MGD /
Feb 2022 Week 4 0.01768 / MGD /
Mar 2022 Week 4 0.014415 / MGD /
Apr 2022 Week 4 0.032 / MGD /
May 2022 Week 4 0.032 / MGD /
Jun 2022 Week 4 0.025 / MGD /
Jan 2022 Average 0.016172 /0.020 MGD /
Feb 2022 Average 0.01768 /0.020 MGD /
Mar 2022 Average 0.014415 /0.020 MGD /
Apr 2022 Average 0.032 /0.020 MGD * /
May 2022 Average 0.032 /0.020 MGD * /
Jun 2022 Average 0.025 /0.020 MGD * /
2022 Quarter 1 0.016089 / MGD /
2022 Quarter 2 0.029667 / MGD /
2022 1 st 6 Months(Avg) 0.022878 / MGD /
2022 lst6...(Max) 0.032 / MGD /
2022 lst6...(Min) 0.014415 / MGD /
2022 lst6...(Count) 6
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 3 50.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Bismuth
01/17/2022 S Phononic011722Self 0.039 / mg/L /
02/16/2022 S Phononic021622Self 0.022 / mg/L /
03/10/2022 P Phononic031022POT < 0.05 / mg/L < /
W
03/17/2022 S Phononic031722Self 0.049 / mg/L /
06/23/2022 S Phononic062322Self 0.022 / mg/L /
Jan 2022 Week 3 0.039 / mg/L /
Tuesday,February 28,2023 10:46:44AM *Indicates Violation **Indicates TRC Violation Page 1 of 5

Phononic
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Bismuth
Feb 2022 Week 3 0.022 / mg/L /
Mar 2022 Week 2 < 0.05 / mg/L < /
Mar 2022 Week 3 0.049 / mg/L /
Jun 2022 Week 4 0.022 / mg/L /
Jan 2022 Average 0.039 / mg/L /
Feb 2022 Average 0.022 / mg/L /
Mar 2022 Average < 0.05 / mg/L < /
Jun 2022 Average 0.022 / mg/L /
2022 Quarter 1 < 0.04 / mg/L < /
2022 Quarter 2 0.022 / mg/L /
2022 1 st 6 Months(Avg) < 0.036 / mg/L < /
2022 lst6...(Max) < 0.05 / mg/L < /
2022 lst6...(Min) 0.022 / mg/L /
2022 lst6...(Count) 5
Sample Date SampleID Result/Limit Mass/Limit
Mercury-LL
03/10/2022 P Phononic031022POT 0.000001 /0.000142 mg/L /
WHg
Mar 2022 Week 2 0.000001 / mg/L /
Mar 2022 Average 0.000001 / mg/L /
2022 Quarter 1 0.000001 / mg/L /
2022 1 st 6 Months(Avg) 0.000001 / mg/L /
2022 lst6...(Max) 0.000001 / mg/L /
2022 lst6...(Min) 0.000001 / mg/L /
2022 lst6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Molybdenum
01/17/2022 S Phononic011722Self < 0.003 / mg/L < 0.0002 / lbs/day
03/10/2022 P Phononic031022POT 0.002 / mg/L 0.0005 / lbs/day
W
Jan 2022 Week 3 < 0.003 / mg/L < 0.0002 / lbs/day
Mar 2022 Week 2 0.002 / mg/L 0.0005 / lbs/day
Tuesday,February 28,2023 10:46:44AM *Indicates Violation **Indicates TRC Violation Page 2 of 5

Phononic
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Molybdenum
Jan 2022 Average < 0.003 / mg/L < 0.0002 / lbs/day
Mar 2022 Average 0.002 / mg/L 0.0005 / lbs/day
2022 Quarter 1 < 0.002 / mg/L < 0.0004 / lbs/day
2022 1 st 6 Months(Avg) < 0.002 / mg/L < 0.0004 / lbs/day
2022 lst6...(Max) < 0.003 / mg/L < 0.0005 / lbs/day
2022 lst6...(Min) 0.002 / mg/L 0.0002 / lbs/day
2022 lst6...(Count) 2 / 2 /
Sample Date SampleID Result/Limit Mass/Limit
Nickel
01/17/2022 S Phononic0I1722Self 0.147 / mg/L 0.013697 / 0.02 lbs/day
02/16/2022 S Phononic021622Self < 0.0025 / mg/L < 0.000511 / 0.02 lbs/day
03/10/2022 P Phononic031022POT 0.0854 / mg/L 0.022006 / 0.02 lbs/day *
W
03/17/2022 S Phononic031722Se1f 1.8 / mg/L 0.463826 / 0.02 lbs/day * *
06/23/2022 S Phononic062322Self 0.174 / mg/L 0.036279 / 0.02 lbs/day * *
Jan 2022 Week 3 0.147 / mg/L 0.013697 / lbs/day
Feb 2022 Week 3 < 0.0025 / mg/L < 0.000511 / lbs/day
Mar 2022 Week 2 0.0854 / mg/L 0.022006 / lbs/day
Mar 2022 Week 3 1.8 / mg/L 0.463826 / lbs/day
Jun 2022 Week 4 0.174 / mg/L 0.036279 / lbs/day
Jan 2022 Average 0.147 / mg/L 0.013697 / lbs/day
Feb 2022 Average < 0.0025 / mg/L < 0.000511 / lbs/day
Mar 2022 Average 0.9427 / mg/L 0.242916 / lbs/day
Jun 2022 Average 0.174 / mg/L 0.036279 / lbs/day
2022 Quarter 1 < 0.5087 / mg/L < 0.12501 / lbs/day
2022 Quarter 2 0.174 / mg/L 0.036279 / lbs/day
2022 1 st 6 Months(Avg) < 0.4418 / mg/L < 0.107264 / lbs/day
2022 lst6...(Max) 1.8 / mg/L 0.463826 / lbs/day
2022 lst6...(Min) < 0.0025 / mg/L < 0.000511 / lbs/day
2022 Ist 6...(Count) 5 / 5 /
Sample Count: 5 Months Sampled: 4 Weeks Sampled: 5 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 3 60.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 2 40.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
PH
Tuesday,February 28,2023 10:46:44AM *Indicates Violation **Indicates TRC Violation Page 3 of 5

Phononic
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
pH
01/17/2022 S Phononic011722Self 6.5 /5.5-10 SU /
03/10/2022 P Phononic031022POT 6.8 /5.5-10 SU /
W
Jan 2022 Week 3 6.5 / SU /
Mar 2022 Week 2 6.8 / SU /
Jan 2022 Average 6.5 / SU /
Mar 2022 Average 6.8 / SU /
2022 Quarter 1 6.65 / SU /
2022 1 st 6 Months(Avg) 6.65 / SU /
2022 lst6...(Max) 6.8 / SU /
2022 lst6...(Min) 6.5 / SU /
2022 lst6...(Count) 2
Sample Count: 2 Months Sampled: 2 ' Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Tellurium
01/17/2022 S Phononic011722Self 0.507 / mg/L /
02/16/2022 S Phononic021622Self 0.065 / mg/L /
03/10/2022 P Phononic031022POT 0.29 / mg/L /
W
03/17/2022 S Phononic031722Self 0.07 / mg/L /
06/23/2022 S Phononic062322Self 0.057 / mg/L /
Jan 2022 Week 3 0.507 / mg/L /
Feb 2022 Week 3 0.065 / mg/L /
Mar 2022 Week 2 0.29 / mg/L /
Mar 2022 Week 3 0.07 / mg/L /
Jun 2022 Week 4 0.057 / mg/L /
Jan 2022 Average 0.507 / mg/L /
Feb 2022 Average 0.065 / mg/L /
Mar 2022 Average 0.18 / mg/L /
Jun 2022 Average 0.057 / mg/L /
2022 Quarter 1 0.233 / mg/L /
2022 Quarter 2 0.057 / mg/L /
2022 1st 6 Months(Avg) 0.198 / mg/L /
2022 1st 6...(Max) 0.507 / mg/L /
2022 1st 6...(Min) 0.057 / mg/L /
Tuesday,February 28,2023 10:46:44AM *Indicates Violation **Indicates TRC Violation Page 4 of 5

Phononic
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Tellurium
2022 1st 6...(Count) 5
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
01/17/2022 S Phononic011722Self 20.7 / °C /
03/10/2022 P Phononic031022POT 15 / °C /
W
Jan 2022 Week 3 20.7 / °C /
Mar 2022 Week 2 15 / °C /
Jan 2022 Average 20.7 / °C /
Mar 2022 Average 15 / °C /
2022 Quarter 1 17.9 / °C /
2022 1 st 6 Months(Avg) 17.9 / °C /
2022 lst6...(Max) 20.7 / °C /
2022 lst6...(Min) 15 / °C /
2022 lst6...(Count) 2
Tuesday,February 28,2023 10:46:44AM *Indicates Violation **Indicates TRC Violation Page 5 of 5

PowerSecure
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Aluminum
03/23/2022 P PowerSecure032322P 4.87 / mg/L /
OTW
03/30/2022 S PowerSecure033022Se 2.6 / mg/L /
if
Mar 2022 Week 4 3.735 / mg/L /
Mar 2022 Average 3.735 / mg/L /
2022 Quarter 1 3.735 / mg/L /
2022 1 st 6 Months(Avg) 3.735 / mg/L /
2022 lst6...(Max) 4.87 / mg/L /
2022 lst6...(Min) 2.6 / mg/L /
2022 lst6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2022 S PowerSecure0122F1ow 0 / MGD /
02/28/2022 S PowerSecure0222F1ow 0.001068 / MGD /
03/31/2022 S PowerSecure0322F1ow 0.000457 / MGD /
04/30/2022 S PowerSecure0422F1ow 0.000092 / MGD /
05/31/2022 S PowerSecure0522F1ow 0.000071 / MGD /
06/30/2022 S PowerSecure0622F1ow 0.00009 / MGD /
Jan 2022 Week 4 0 / MGD /
Feb 2022 Week 4 0.001068 / MGD /
Mar 2022 Week 4 0.000457 / MGD /
Apr 2022 Week 4 0.000092 / MGD /
May 2022 Week 4 0.000071 / MGD /
Jun 2022 Week 4 0.00009 / MGD /
Jan 2022 Average 0 /0.006 MGD /
Feb 2022 Average 0.001068 /0.006 MGD /
Mar 2022 Average 0.000457 /0.006 MGD /
Apr 2022 Average 0.000092 /0.006 MGD /
May 2022 Average 0.000071 /0.006 MGD /
Jun 2022 Average 0.00009 /0.006 MGD /
2022 Quarter 1 0.000508 / MGD /
2022 Quarter 2 0.000084 / MGD /
2022 1st 6 Months(Avg) 0.000296 / MGD /
2022 1st 6...(Max) 0.001068 / MGD /
2022 1st 6...(Min) 0 / MGD /
2022 1st 6...(Count) 6
Tuesday,February 21,2023 2:40:01PM *Indicates Violation **Indicates TRC Violation Page 1 of 9

PowerSecure
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
03/23/2022 P PowerSecure032322P < 0.00008 /0.11 mg/L < /
OTW
03/30/2022 S PowerSecure033022Se < 0.0005 /0.11 mg/L < /
if
Mar 2022 Week 4 < 0.00029 / mg/L < /
Mar 2022 Average < 0.00029 /0.07 mg/L < /
2022 Quarter 1 < 0.00029 / mg/L < /
2022 1 st 6 Months(Avg) < 0.00029 / mg/L < /
2022 lst6...(Max) < 0.0005 / mg/L < /
2022 lst6...(Min) < 0.00008 / mg/L < /
2022 lst6...(Count) 2
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
02/11/2022 S PowerSecure02lI22Se 1740 / mg/L /
if
03/23/2022 P PowerSecure032322P 1960 / mg/L /
OTW
03/30/2022 S PowerSecure033022Se 1570 / mg/L /
if
Feb 2022 Week 2 1740 / mg/L /
Mar 2022 Week 4 1765 / mg/L /
Feb 2022 Average 1740 / mg/L /
Mar 2022 Average 1765 / mg/L /
2022 Quarter 1 1756.67 / mg/L /
2022 1st 6 Months(Avg) 1756.67 / mg/L /
2022 lst6...(Max) 1960 / mg/L /
2022 Ist6...(Min) 1570 / mg/L /
Tuesday,February 21,2023 2:40:01PM *Indicates Violation **Indicates TRC Violation Page 2 of 9

PowerSecure
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Chloride
2022 1st 6...(Count) 3
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
03/23/2022 P PowerSecure032322P < 0.001 /2.77 mg/L < /
OTW
03/30/2022 S PowerSecure033022Se < 0.003 /2.77 mg/L < /
if
Mar 2022 Week 4 < 0.002 / mg/L < /
Mar 2022 Average < 0.002 / 1.71 mg/L < /
2022 Quarter 1 < 0.002 / mg/L < /
2022 1 st 6 Months(Avg) < 0.002 / mg/L < /
2022 1st 6...(Max) < 0.003 / mg/L < /
2022 1st 6...(Min) < 0.001 / mg/L < /
2022 1st 6...(Count) 2
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Copper
03/23/2022 P PowerSecure032322P 0.174 /3.38 mg/L /
OTW
03/30/2022 S PowerSecure033022Se 0.322 /3.38 mg/L /
if
Mar 2022 Week 4 0.248 / mg/L /
Mar 2022 Average 0.248 /2.07 mg/L /
2022 Quarter 1 0.248 / mg/L /
2022 1 st 6 Months(Avg) 0.248 / mg/L /
2022 lst6...(Max) 0.322 / mg/L /
2022 1st 6...(Min) 0.174 / mg/L /
2022 1st 6...(Count) 2 / /
Tuesday,February 21,2023 2:40:01PM *Indicates Violation **Indicates TRC Violation Page 3 of 9

PowerSecure
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
03/23/2022 P PowerSecure032322P < 0.003 /0.60 mg/L < /
OTW
03/30/2022 S PowerSecure033022Se < 0.004 /0.60 mg/L < /
if
Mar 2022 Week 4 < 0.003 / mg/L < /
Mar 2022 Average < 0.003 10.50 mg/L < /
2022 Quarter 1 < 0.003 / mg/L < /
2022 1 st 6 Months(Avg) < 0.003 / mg/L < /
2022 lst6...(Max) < 0.004 / mg/L < /
2022 lst6...(Min) < 0.003 / mg/L < /
2022 lst6...(Count) 2
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Lead
03/23/2022 P PowerSecure032322P < 0.0003 /0.69 mg/L < /
OTW
03/30/2022 S PowerSecure033022Se < 0.0025 /0.69 mg/L < /
if
Mar 2022 Week 4 < 0.0014 / mg/L < /
Mar 2022 Average < 0.0014 /0.43 mg/L < /
2022 Quarter 1 < 0.0014 / mg/L < /
2022 1 st 6 Months(Avg) < 0.0014 / mg/L < /
2022 lst6...(Max) < 0.0025 / mg/L < /
2022 lst6...(Min) < 0.0003 / mg/L < /
2022 lst6...(Count) 2 / /
Tuesday,February 21,2023 2:40:01PM *Indicates Violation **Indicates TRC Violation Page 4 of 9

PowerSecure
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury
03/30/2022 S PowerSecure033022Se < 0 /0.000142 mg/L < /
if
Mar 2022 Week 4 < 0 / mg/L < /
Mar 2022 Average < 0 / mg/L < /
2022 Quarter 1 < 0 / mg/L < /
2022 1 st 6 Months(Avg) < 0.00000 / mg/L < /
2022 lst6...(Max) < 0.00000 / mg/L < /
2022 lst6...(Min) < 0.00000 / mg/L < /
2022 1st 6...(Count) 1
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
06/13/2022 P PowerSecure061322P 0.000003 / mg/L /
OTWHg
Jun 2022 Week 2 0.000003 / mg/L /
Jun 2022 Average 0.000003 / mg/L /
2022 Quarter 2 0.000003 / mg/L /
2022 1st 6 Months(Avg) 0.000003 / mg/L /
2022 1st 6...(Max) 0.000003 / mg/L /
2022 1st 6...(Min) 0.000003 / mg/L /
2022 1st 6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
03/30/2022 S PowerSecure033022Se 0.027 / mg/L /
if
Mar 2022 Week 4 0.027 / mg/L /
Tuesday,February 21,2023 2:40:01PM *Indicates Violation **Indicates TRC Violation Page 5 of 9

PowerSecure
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Molybdenum
Mar 2022 Average 0.027 / mg/L /
2022 Quarter 1 0.027 / mg/L /
2022 1 st 6 Months(Avg) 0.027 / mg/L /
2022 lst6...(Max) 0.027 / mg/L /
2022 lst6...(Min) 0.027 / mg/L /
2022 lst6...(Count) 1
Sample Date SampleID Result/Limit Mass/Limit
Nickel
03/23/2022 P PowerSecure032322P 0.138 / 1.30 mg/L /
OTW
03/30/2022 S PowerSecure033022Se 0.171 / 1.30 mg/L /
if
Mar 2022 Week 4 0.1545 / mg/L /
Mar 2022 Average 0.1545 / 1.00 mg/L /
2022 Quarter 1 0.1545 / mg/L /
2022 1st 6 Months(Avg) 0.1545 / mg/L /
2022 1st 6...(Max) 0.171 / mg/L /
2022 1st 6...(Min) 0.138 / mg/L /
2022 1st 6...(Count) 2
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
02/11/2022 S PowerSecure021122Se 7.8 /6.0-10.0 SU /
if
03/23/2022 P PowerSecure032322P 8.7 /6.0-10.0 SU /
OTW
03/30/2022 S PowerSecure033022Se 8.6 /6.0-10.0 SU /
if
Feb 2022 Week 2 7.8 / SU /
Mar 2022 Week 4 8.65 / SU /
Feb 2022 Average 7.8 / SU /
Mar 2022 Average 8.65 / SU /
2022 Quarter 1 8.37 / SU /
2022 1 st 6 Months(Avg) 8.37 / SU /
Tuesday,February 21,2023 2:40:01PM *Indicates Violation **Indicates TRC Violation Page 6 of 9

PowerSecure
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
pH
2022 lst6...(Max) 8.7 / SU /
2022 lst6...(Min) 7.8 / SU /
2022 lst6...(Count) 3 / /
Sample Count: 3 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Silver
03/23/2022 P PowerSecure032322P < 0.0003 /0.43 mg/L < /
OTW
03/30/2022 S PowerSecure033022Se < 0.0025 /0.43 mg/L < /
if
Mar 2022 Week 4 < 0.0014 / mg/L < /
Mar 2022 Average < 0.0014 /0.24 mg/L < /
2022 Quarter 1 < 0.0014 / mg/L < /
2022 1 st 6 Months(Avg) < 0.0014 / mg/L < /
2022 1st 6...(Max) < 0.0025 / mg/L < /
2022 1st 6...(Min) < 0.0003 / mg/L < /
2022 1st 6...(Count) 2
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
02/11/2022 S PowerSecure021122Se 20.5 /66 °C /
if
03/23/2022 P PowerSecure032322P 20 /66 °C /
OTW
03/30/2022 S PowerSecure033022Se 21.5 /66 °C /
if
Feb 2022 Week 2 20.5 / °C /
Tuesday,February 21,2023 2:40:01PM *Indicates Violation **Indicates TRC Violation Page 7 of 9

PowerSecure
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Temperature
Mar 2022 Week 4 20.8 / °C /
Feb 2022 Average 20.5 / °C /
Mar 2022 Average 20.8 / °C /
2022 Quarter 1 20.7 / °C /
2022 1 st 6 Months(Avg) 20.7 / °C /
2022 lst6...(Max) 21.5 / °C /
2022 lst6...(Min) 20 / °C /
2022 lst6...(Count) 3
Sample Count: 3 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
TTO
03/30/2022 S PowerSecure033022Se < 0.0002 /2.13 mg/L < /
if
Mar 2022 Week 4 < 0.0002 / mg/L < /
Mar 2022 Average < 0.0002 / mg/L < /
2022 Quarter 1 < 0.0002 / mg/L < /
2022 1 st 6 Months(Avg) < 0.0002 / mg/L < /
2022 lst6...(Max) < 0.0002 / mg/L < /
2022 lst6...(Min) < 0.0002 / mg/L < /
2022 1st 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Zinc
03/23/2022 P PowerSecure032322P 0.198 /2.61 mg/L /
OTW
03/30/2022 S PowerSecure033022Se 0.275 /2.61 mg/L /
if
Tuesday,February 21,2023 2:40:01PM *Indicates Violation **Indicates TRC Violation Page 8 of 9

PowerSecure
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Zinc
Mar 2022 Week 4 0.237 / mg/L /
Mar 2022 Average 0.237 / 1.48 mg/L /
2022 Quarter 1 0.237 / -9/1-
2022 1 st 6 Months(Avg) 0.237 / -9/1-
2022 lst6...(Max) 0.275 / mg/L /
2022 Ist6...(Min) 0.198 / mg/L /
2022 1st 6...(Count) 2
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Tuesday,February 21,2023 2:40:01PM *Indicates Violation **Indicates TRC Violation Page 9 of 9

SCM Metal Products, Inc.
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
01/14/2022 S SCM011422Self 3.9 / mg/L 0.6424 / lbs/day
Jan 2022 Week 2 3.9 / mg/L 0.6424 / lbs/day
Jan 2022 Average 3.9 / mg/L 0.6424 / lbs/day
2022 Quarter 1 3.9 / mg/L 0.6424 / lbs/day
2022 1 st 6 Months(Avg) 3.9 / mg/L 0.6424 / lbs/day
2022 lst6...(Max) 3.9 / mg/L 0.6424 / lbs/day
2022 lst6...(Min) 3.9 / mg/L 0.6424 / lbs/day
2022 lst 6...(Count) I / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2022 S SCM0122F1ow 0.010805 / 0.080 MGD /
02/28/2022 S SCM0222171ow 0.010077 / 0.080 MGD /
03/31/2022 S SCM0322171ow 0.010653 / 0.080 MGD /
04/30/2022 S SCM0422171ow 0.009959 / 0.080 MGD /
05/31/2022 S SCM0522171ow 0.012173 / 0.080 MGD /
06/30/2022 S SCM0622171ow 0.013765 / 0.080 MGD /
Jan 2022 Week 4 0.010805 / MGD /
Feb 2022 Week 4 0.010077 / MGD /
Mar 2022 Week 4 0.010653 / MGD /
Apr 2022 Week 4 0.009959 / MGD /
May 2022 Week 4 0.012173 / MGD /
Jun 2022 Week 4 0.013765 / MGD /
Jan 2022 Average 0.010805 / 0.050 MGD /
Feb 2022 Average 0.010077 / 0.050 MGD /
Mar 2022 Average 0.010653 / 0.050 MGD /
Apr 2022 Average 0.009959 / 0.050 MGD /
May 2022 Average 0.012173 / 0.050 MGD /
Jun 2022 Average 0.013765 / 0.050 MGD /
2022 Quarter 1 0.010512 / MGD /
2022 Quarter 2 0.011966 / MGD /
2022 1 st 6 Months(Avg) 0.011239 / MGD /
2022 1st 6...(Max) 0.013765 / MGD /
2022 lst6...(Min) 0.009959 / MGD /
2022 lst6...(Count) 6 / /
Tuesday,February 21,2023 7:37:34PM *Indicates Violation **Indicates TRC Violation Page 1 of 8

SCM Metal Products, Inc.
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
01/14/2022 S SCM011422Self < 0.0005 / mg/L < 0.000082 / lbs/day
04/20/2022 S SCM042022Self < 0.0005 / mg/L < 0.000062 / lbs/day
Jan 2022 Week 2 < 0.0005 / mg/L < 0.000082 / lbs/day
Apr 2022 Week 3 < 0.0005 / mg/L < 0.000062 / lbs/day
Jan 2022 Average < 0.0005 / mg/L < 0.000082 / lbs/day
Apr 2022 Average < 0.0005 / mg/L < 0.000062 / lbs/day
2022 Quarter 1 < 0.0005 / mg/L < 0.000082 / lbs/day
2022 Quarter 2 < 0.0005 / mg/L < 0.000062 / lbs/day
2022 1 st 6 Months(Avg) < 0.0005 / mg/L < 0.000072 / lbs/day
2022 lst6...(Max) < 0.0005 / mg/L < 0.000082 / lbs/day
2022 lst6...(Min) < 0.0005 / mg/L < 0.000062 / lbs/day
2022 lst6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
01/14/2022 S SCM011422Self 19.7 / mg/L 3.245 / lbs/day
Jan 2022 Week 2 19.7 / mg/L 3.245 / lbs/day
Jan 2022 Average 19.7 / mg/L 3.245 / lbs/day
2022 Quarter 1 19.7 / mg/L 3.245 / lbs/day
2022 1 st 6 Months(Avg) 19.7 / mg/L 3.2451 / lbs/day
2022 lst6...(Max) 19.7 / mg/L 3.2450 / lbs/day
2022 lst6...(Min) 19.7 / mg/L 3.2450 / lbs/day
2022 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
01/14/2022 S SCM011422Self 0.055 / 0.75 mg/L 0.00901 / lbs/day
04/20/2022 S SCM042022Self 0.09 / 0.75 mg/L 0.011228 / lbs/day
05/05/2022 P SCM050522POTW 0.055 / 0.75 mg/L 0.006602 / lbs/day
Jan 2022 Week 2 0.055 / mg/L 0.00901 / lbs/day
Apr 2022 Week 3 0.09 / mg/L 0.011228 / lbs/day
May 2022 Week 1 0.055 / mg/L 0.006602 / lbs/day
Jan 2022 Average 0.055 / 0.50 mg/L 0.00901 / lbs/day
Apr 2022 Average 0.09 / 0.50 mg/L 0.011228 / lbs/day
May 2022 Average 0.055 / 0.50 mg/L 0.006602 / lbs/day
2022 Quarter 1 0.055 / mg/L 0.00901 / lbs/day
2022 Quarter 2 0.073 / mg/L 0.008915 / lbs/day
Tuesday,February 21,2023 7:37:34PM *Indicates Violation **Indicates TRC Violation Page 2 of 8

SCM Metal Products, Inc.
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Copper
2022 1 st 6 Months(Avg) 0.067 / mg/L 0.008947 / lbs/day
2022 lst6...(Max) 0.090 / mg/L 0.011228 / lbs/day
2022 lst6...(Min) 0.055 / mg/L 0.006602 / lbs/day
2022 lst6...(Count) 3 / 3 /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
05/05/2022 P SCM050522POTW < 0.003 / 0.04 mg/L < 0.0003 / lbs/day
May 2022 Week I < 0.003 / mg/L < 0.0003 / lbs/day
May 2022 Average < 0.003 / 0.03 mg/L < 0.0003 / lbs/day
2022 Quarter 2 < 0.003 / mg/L < 0.0003 / lbs/day
2022 1 st 6 Months(Avg) < 0.003 / mg/L < 0.000300 / lbs/day
2022 lst6...(Max) < 0.003 / mg/L < 0.000300 / lbs/day
2022 lst6...(Min) < 0.003 / mg/L < 0.000300 / lbs/day
2022 lst6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
01/14/2022 S SCM011422Self 0.73 / mg/L 0.1202 / lbs/day
Jan 2022 Week 2 0.73 / mg/L 0.1202 / lbs/day
Jan 2022 Average 0.73 / mg/L 0.1202 / lbs/day
2022 Quarter 1 0.73 / mg/L 0.1202 / lbs/day
2022 1 st 6 Months(Avg) 0.73 / mg/L 0.1202 / lbs/day
2022 lst6...(Max) 0.73 / mg/L 0.1202 / lbs/day
2022 lst6...(Min) 0.73 / mg/L 0.1202 / lbs/day
2022 Ist 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Lead
01/14/2022 S SCM011422Self 0.0057 / 0.20 mg/L 0.000939 / lbs/day
04/20/2022 S SCM042022Self < 0.0025 / 0.20 mg/L < 0.000312 / lbs/day
05/05/2022 P SCM050522POTW 0.0009 / 0.20 mg/L 0.000107 / lbs/day
Jan 2022 Week 2 0.0057 / mg/L 0.000939 / lbs/day
Apr 2022 Week 3 < 0.0025 / mg/L < 0.000312 / lbs/day
May 2022 Week 1 0.0009 / mg/L 0.000107 / lbs/day
Jan 2022 Average 0.0057 / 0.10 mg/L 0.000939 / lbs/day
Tuesday,February 21,2023 7:37:34PM *Indicates Violation **Indicates TRC Violation Page 3 of 8

SCM Metal Products, Inc.
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
Lead
Apr 2022 Average < 0.0025 / 0.10 mg/L < 0.000312 / lbs/day
May 2022 Average 0.0009 / 0.10 mg/L 0.000107 / lbs/day
2022 Quarter 1 0.0057 / mg/L 0.000939 / lbs/day
2022 Quarter 2 < 0.0017 / mg/L < 0.000209 / lbs/day
2022 1 st 6 Months(Avg) < 0.0030 / mg/L < 0.000453 / lbs/day
2022 lst6...(Max) 0.0057 / mg/L 0.000939 / lbs/day
2022 lst6...(Min) 0.0009 / mg/L 0.000107 / lbs/day
2022 lst6...(Count) 3 / 3 /
Sample Date SampleID Result/Limit Mass/Limit
Mercury-LL
01/14/2022 S SCM011422Self 0.000001 / 0.000142 mg/L /
Jan 2022 Week 2 0.000001 / mg/L /
Jan 2022 Average 0.000001 / mg/L /
2022 Quarter 1 0.000001 / mg/L /
2022 1 st 6 Months(Avg) 0.000001 / mg/L /
2022 lst6...(Max) 0.000001 / mg/L /
2022 lst6...(Min) 0.000001 / mg/L /
2022 1st 6...(Count) 1
Sample Date SampleID Result/Limit Mass/Limit
Molybdenum
01/14/2022 S SCM011422Self < 0.003 / mg/L < 0.0004 / lbs/day
04/20/2022 S SCM042022Self < 0.003 / mg/L < 0.0003 / lbs/day
Jan 2022 Week 2 < 0.003 / mg/L < 0.0004 / lbs/day
Apr 2022 Week 3 < 0.003 / mg/L < 0.0003 / lbs/day
Jan 2022 Average < 0.003 / mg/L < 0.0004 / lbs/day
Apr 2022 Average < 0.003 / mg/L < 0.0003 / lbs/day
2022 Quarter 1 < 0.003 / mg/L < 0.0004 / lbs/day
2022 Quarter 2 < 0.003 / mg/L < 0.0003 / lbs/day
2022 1 st 6 Months(Avg) < 0.003 / mg/L < 0.0004 / lbs/day
2022 lst6...(Max) < 0.003 / mg/L < 0.0004 / lbs/day
2022 lst6...(Min) < 0.003 / mg/L < 0.0003 / lbs/day
2022 1st6...(Count) 2 / 2 /
Tuesday,February 21,2023 7:37:34PM *Indicates Violation **Indicates TRC Violation Page 4 of 8

SCM Metal Products, Inc.
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
01/14/2022 S SCM011422Self < 0.0025 / mg/L < 0.000412 / lbs/day
04/20/2022 S SCM042022Self < 0.0025 / mg/L < 0.000312 / lbs/day
Jan 2022 Week 2 < 0.0025 / mg/L < 0.000412 / lbs/day
Apr 2022 Week 3 < 0.0025 / mg/L < 0.000312 / lbs/day
Jan 2022 Average < 0.0025 / mg/L < 0.000412 / lbs/day
Apr 2022 Average < 0.0025 / mg/L < 0.000312 / lbs/day
2022 Quarter 1 < 0.0025 / mg/L < 0.000412 / lbs/day
2022 Quarter 2 < 0.0025 / mg/L < 0.000312 / lbs/day
2022 1 st 6 Months(Avg) < 0.0025 / mg/L < 0.000362 / lbs/day
2022 lst6...(Max) < 0.0025 / mg/L < 0.000412 / lbs/day
2022 lst6...(Min) < 0.0025 / mg/L < 0.000312 / lbs/day
2022 lst6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
01/14/2022 S SCM011422Self 0.3 / mg/L 0.056 / lbs/day
Jan 2022 Week 2 0.3 / mg/L 0.056 / lbs/day
Jan 2022 Average 0.3 / mg/L 0.056 / lbs/day
2022 Quarter 1 0.3 / mg/L 0.056 / lbs/day
2022 1 st 6 Months(Avg) 0.3 / mg/L 0.056 / lbs/day
2022 lst6...(Max) 0.3 / mg/L 0.056 / lbs/day
2022 lst6...(Min) 0.3 / mg/L 0.056 / lbs/day
2022 lst6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
01/14/2022 S SCM011422Self 7.8 / mg/L 1.285 / lbs/day
Jan 2022 Week 2 7.8 / mg/L 1.285 / lbs/day
Jan 2022 Average 7.8 / mg/L 1.285 / lbs/day
2022 Quarter 1 7.8 / mg/L 1.285 / lbs/day
2022 1 st 6 Months(Avg) 7.8 / mg/L 1.285 / lbs/day
2022 lst6...(Max) 7.8 / mg/L 1.285 / lbs/day
2022 lst6...(Min) 7.8 / mg/L 1.285 / lbs/day
2022 1st6...(Count) I / 1 /
Tuesday,February 21,2023 7:37:34PM *Indicates Violation **Indicates TRC Violation Page 5 of 8

SCM Metal Products, Inc.
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
01/14/2022 S SCM011422Self < 2.5 / 200 mg/L < /
Jan 2022 Week 2 < 2.5 / mg/L < /
Jan 2022 Average < 2.5 / mg/L < /
2022 Quarter 1 < 2.5 / mg/L < /
2022 1 st 6 Months(Avg) < 2.5 / mg/L < /
2022 lst6...(Max) < 2.5 / mg/L < /
2022 lst6...(Min) < 2.5 / mg/L < /
2022 lst6...(Count) 1
Sample Date SampleID Result/Limit Mass/Limit
PH
01/14/2022 S SCM011422Self 6.78 / 6.0-10.5 Su /
04/20/2022 S SCM042022Self 8.3 / 6.0-10.5 su /
05/05/2022 P SCM050522POTW 7.1 / 6.0-10.5 Su /
Jan 2022 Week 2 6.78 / Su /
Apr 2022 Week 3 8.3 / su /
May 2022 Week 1 7.1 / Su /
Jan 2022 Average 6.78 / su /
Apr 2022 Average 8.3 / Su /
May 2022 Average 7.1 / Su /
2022 Quarter 1 6.78 / su /
2022 Quarter 2 7.7 / Su /
2022 1 st 6 Months(Avg) 7.39 / Su /
2022 lst6...(Max) 8.3 / Su /
2022 lst6...(Min) 6.78 / Su /
2022 lst6...(Count) 3
Sample Date SamplelD Result/Limit Mass/Limit
Selenium
01/14/2022 S SCM011422Self < 0.005 / mg/L < 0.000824 / lbs/day
04/20/2022 S SCM042022Self < 0.005 / mg/L < 0.000624 / lbs/day
Jan 2022 Week 2 < 0.005 / mg/L < 0.000824 / lbs/day
Apr 2022 Week 3 < 0.005 / mg/L < 0.000624 / lbs/day
Jan 2022 Average < 0.005 / mg/L < 0.000824 / lbs/day
Apr 2022 Average < 0.005 / mg/L < 0.000624 / lbs/day
2022 Quarter 1 < 0.005 / mg/L < 0.000824 / lbs/day
2022 Quarter 2 < 0.005 / mg/L < 0.000624 / lbs/day
Tuesday,February 21,2023 7:37:34PM *Indicates Violation **Indicates TRC Violation Page 6 of 8

SCM Metal Products, Inc.
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Selenium
2022 1 st 6 Months(Avg) < 0.005 / mg/L < 0.000724 / lbs/day
2022 lst6...(Max) < 0.005 / mg/L < 0.000824 / lbs/day
2022 lst6...(Min) < 0.005 / mg/L < 0.000624 / lbs/day
2022 lst6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
01/14/2022 S SCM011422Self 11.3 / 66 °C /
04/20/2022 S SCM042022Self 21.7 / 66 °C /
05/05/2022 P SCM050522POTW 21 / 66 °C /
Jan 2022 Week 2 11.3 / °C /
Apr 2022 Week 3 21.7 / °C /
May 2022 Week 1 21 / °C /
Jan 2022 Average 11.3 / °C /
Apr 2022 Average 21.7 / °C /
May 2022 Average 21 / °C /
2022 Quarter 1 11.3 / °C /
2022 Quarter 2 21.4 / °C /
2022 1 st 6 Months(Avg) 18 / °C /
2022 lst6...(Max) 21.7 / °C /
2022 lst6...(Min) 11.3 / °C /
2022 lst6...(Count) 3
Sample Date SamplelD Result/Limit Mass/Limit
TKN
01/14/2022 S SCM011422Self 7.5 / mg/L 1.235 / lbs/day
Jan 2022 Week 2 7.5 / mg/L 1.235 / lbs/day
Jan 2022 Average 7.5 / mg/L 1.235 / lbs/day
2022 Quarter 1 7.5 / mg/L 1.235 / lbs/day
2022 1st 6 Months(Avg) 7.5 / mg/L 1.235 / lbs/day
2022 lst6...(Max) 7.5 / mg/L 1.235 / lbs/day
2022 1st 6...(Min) 7.5 / mg/L 1.235 / lbs/day
2022 lst6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
Tuesday,February 21,2023 7:37:34PM *Indicates Violation **Indicates TRC Violation Page 7 of 8

SCM Metal Products, Inc.
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
Total Phosphorus
01/14/2022 S SCM011422Self 1.3 / mg/L 0.2141 / lbs/day
Jan 2022 Week 2 1.3 / mg/L 0.2141 / lbs/day
Jan 2022 Average 1.3 / mg/L 0.2141 / lbs/day
2022 Quarter 1 1.3 / mg/L 0.2141 / lbs/day
2022 1 st 6 Months(Avg) 1.3 / mg/L 0.2141 / lbs/day
2022 lst6...(Max) 1.3 / mg/L 0.2141 / lbs/day
2022 lst6...(Min) 1.3 / mg/L 0.2141 / lbs/day
2022 1st6...(Count) I / 1 /
Sample Date SampleID Result/Limit Mass/Limit
VOC
01/14/2022 S SCM011422Self < 0.0125 / mg/L < /
Jan 2022 Week 2 < 0.0125 / mg/L < /
Jan 2022 Average < 0.0125 / mg/L < /
2022 Quarter 1 < 0.0125 / mg/L < /
2022 1 st 6 Months(Avg) < 0.0125 / mg/L < /
2022 lst6...(Max) < 0.0125 / mg/L < /
2022 lst6...(Min) < 0.0125 / mg/L < /
2022 1st 6...(Count) 1
Sample Date SampleID Result/Limit Mass/Limit
Zinc
01/14/2022 S SCM011422Self 0.532 / mg/L 0.087633 / lbs/day
04/20/2022 S SCM042022Self 0.427 / mg/L 0.053332 / lbs/day
Jan 2022 Week 2 0.532 / mg/L 0.087633 / lbs/day
Apr 2022 Week 3 0.427 / mg/L 0.053332 / lbs/day
Jan 2022 Average 0.532 / mg/L 0.087633 / lbs/day
Apr 2022 Average 0.427 / mg/L 0.053332 / lbs/day
2022 Quarter 1 0.532 / mg/L 0.087633 / lbs/day
2022 Quarter 2 0.427 / mg/L 0.053332 / lbs/day
2022 1 st 6 Months(Avg) 0.480 / mg/L 0.070483 / lbs/day
2022 lst6...(Max) 0.532 / mg/L 0.087633 / lbs/day
2022 lst6...(Min) 0.427 / mg/L 0.053332 / lbs/day
2022 Ist 6...(Count) 2 / 2 /
Tuesday,February 21,2023 7:37:34PM *Indicates Violation **Indicates TRC Violation Page 8 of 8

Tereus Pharma
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
05/27/2022 P Tergus052722POTW < 0.025 /20.7 mg/L < /
May 2022 Week 4 < 0.025 / mg/L < /
May 2022 Average < 0.025 /8.2 mg/L < /
2022 Quarter 2 < 0.025 / mg/L < /
2022 1 st 6 Months(Avg) < 0.025 / mg/L < /
2022 lst6...(Max) < 0.025 / mg/L < /
2022 lst6...(Min) < 0.025 / mg/L < /
2022 lst6...(Count) 1
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Arsenic
03/22/2022 S Tergus032222Self < 0.0015 / mg/L < /
05/27/2022 P Tergus052722POTW < 0.001 / mg/L < /
Mar 2022 Week 4 < 0.0015 / mg/L < /
May 2022 Week 4 < 0.001 / mg/L < /
Mar 2022 Average < 0.0015 / mg/L < /
May 2022 Average < 0.001 / mg/L < /
2022 Quarter 1 < 0.0015 / mg/L < /
2022 Quarter 2 < 0.001 / mg/L < /
2022 1 st 6 Months(Avg) < 0.0013 / mg/L < /
2022 lst6...(Max) < 0.0015 / mg/L < /
2022 lst6...(Min) < 0.001 / mg/L < /
2022 lst6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2022 S Tergus0122F1ow 0.000167 / MGD /
02/28/2022 S Tergus0222F1ow 0.000039 / MGD /
03/31/2022 S Tergus0322F1ow 0.000048 / MGD /
04/30/2022 S Tergus0422F1ow 0.00006 / MGD /
05/31/2022 S Tergus0522F1ow 0.000037 / MGD /
06/30/2022 S Tergus0622F1ow 0.000125 / MGD /
Jan 2022 Week 4 0.000167 / MGD /
Tuesday,February 28,2023 10:50:14AM *Indicates Violation **Indicates TRC Violation Page 1 of 13

Tereus Pharma
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Feb 2022 Week 4 0.000039 / MGD /
Mar 2022 Week 4 0.000048 / MGD /
Apr 2022 Week 4 0.00006 / MGD /
May 2022 Week 4 0.000037 / MGD /
Jun 2022 Week 4 0.000125 / MGD /
Jan 2022 Average 0.000167 / MGD /
Feb 2022 Average 0.000039 / MGD /
Mar 2022 Average 0.000048 / MGD /
Apr 2022 Average 0.00006 / MGD /
May 2022 Average 0.000037 / MGD /
Jun 2022 Average 0.000125 / MGD /
2022 Quarter 1 0.000085 / MGD /
2022 Quarter 2 0.000074 / MGD /
2022 1 st 6 Months(Avg) 0.000079 / MGD /
2022 lst6...(Max) 0.000167 / MGD /
2022 lst6...(Min) 0.000037 / MGD /
2022 1st 6...(Count) 6
Sample Date SamplelD Result/Limit Mass/Limit
BOD
03/22/2022 S Tergus032222Self 723 / mg/L /
05/27/2022 P Tergus052722POTW 154 / mg/L /
Mar 2022 Week 4 723 / mg/L /
May 2022 Week 4 154 / mg/L /
Mar 2022 Average 723 / mg/L /
May 2022 Average 154 / mg/L /
2022 Quarter 1 723 / mg/L /
2022 Quarter 2 154 / mg/L /
2022 1 st 6 Months(Avg) 438.5 / mg/L /
2022 lst6...(Max) 723 / mg/L /
2022 lst6...(Min) 154 / mg/L /
2022 lst6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
03/22/2022 S Tergus032222Self < 0.00025 / mg/L < /
05/27/2022 P Tergus052722POTW < 0.00008 / mg/L < /
Mar 2022 Week 4 < 0.00025 / mg/L < /
May 2022 Week 4 < 0.00008 / mg/L < /
Mar 2022 Average < 0.00025 / mg/L < /
May 2022 Average < 0.00008 / mg/L < /
2022 Quarter 1 < 0.00025 / mg/L < /
Tuesday,February 28,2023 10:50:14AM *Indicates Violation **Indicates TRC Violation Page 2 of 13

Tereus Pharma
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Cadmium
2022 Quarter 2 < 0.00008 / mg/L < /
2022 1 st 6 Months(Avg) < 0.00016 / mg/L < /
2022 lst6...(Max) < 0.00025 / mg/L < /
2022 lst6...(Min) < 0.00008 / mg/L < /
2022 lst6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
03/22/2022 S Tergus032222Self 10.6 / mg/L /
05/27/2022 P Tergus052722POTW 13.8 / mg/L /
Mar 2022 Week 4 10.6 / mg/L /
May 2022 Week 4 13.8 / mg/L /
Mar 2022 Average 10.6 / mg/L /
May 2022 Average 13.8 / mg/L /
2022 Quarter 1 10.6 / mg/L /
2022 Quarter 2 13.8 / mg/L /
2022 1 st 6 Months(Avg) 12.2 / mg/L /
2022 lst6...(Max) 13.8 / mg/L /
2022 lst6...(Min) 10.6 / mg/L /
2022 lst6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
03/22/2022 S Tergus032222Self < 0.003 / mg/L < /
05/27/2022 P Tergus052722POTW 0.004 / mg/L /
Mar 2022 Week 4 < 0.003 / mg/L < /
May 2022 Week 4 0.004 / mg/L /
Mar 2022 Average < 0.003 / mg/L < /
May 2022 Average 0.004 / mg/L /
2022 Quarter 1 < 0.003 / mg/L < /
2022 Quarter 2 0.004 / mg/L /
2022 1 st 6 Months(Avg) < 0.003 / mg/L < /
2022 lst6...(Max) 0.004 / mg/L /
2022 lst6...(Min) < 0.003 / mg/L < /
2022 lst6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
03/22/2022 S Tergus032222Self 0.825 / mg/L /
05/27/2022 P Tergus052722POTW 0.097 / mg/L /
Mar 2022 Week 4 0.825 / mg/L /
Tuesday,February 28,2023 10:50:14AM *Indicates Violation **Indicates TRC Violation Page 3 of 13

Tereus Pharma
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Copper
May 2022 Week 4 0.097 / mg/L /
Mar 2022 Average 0.825 / mg/L /
May 2022 Average 0.097 / mg/L /
2022 Quarter 1 0.825 / mg/L /
2022 Quarter 2 0.097 / mg/L /
2022 1 st 6 Months(Avg) 0.461 / mg/L /
2022 lst6...(Max) 0.825 / mg/L /
2022 lst6...(Min) 0.097 / mg/L /
2022 1st 6...(Count) 2 / /
Sample Date SampleID Result/Limit Mass/Limit
Cyanide
03/22/2022 S Tergus032222Self < 0.001 / mg/L < /
05/27/2022 P Tergus052722POTW < 0.003 / mg/L < /
Mar 2022 Week 4 < 0.001 / mg/L < /
May 2022 Week 4 < 0.003 / mg/L < /
Mar 2022 Average < 0.001 / mg/L < /
May 2022 Average < 0.003 / mg/L < /
2022 Quarter 1 < 0.001 / mg/L < /
2022 Quarter 2 < 0.003 / mg/L < /
2022 1 st 6 Months(Avg) < 0.002 / mg/L < /
2022 lst6...(Max) < 0.003 / mg/L < /
2022 lst6...(Min) < 0.001 / mg/L < /
2022 lst6...(Count) 2
Sample Date SampleID Result/Limit Mass/Limit
Ethyl acetate
05/27/2022 P Tergus052722POTW < 0.003 /20.7 mg/L < /
May 2022 Week 4 < 0.003 / mg/L < /
May 2022 Average < 0.003 /8.2 mg/L < /
2022 Quarter 2 < 0.003 / mg/L < /
2022 1 st 6 Months(Avg) < 0.003 / mg/L < /
2022 lst6...(Max) < 0.003 / mg/L < /
2022 lst6...(Min) < 0.003 / mg/L < /
2022 lst6...(Count) 1 / /
Tuesday,February 28,2023 10:50:14AM *Indicates Violation **Indicates TRC Violation Page 4 of 13

Tereus Pharma
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
03/22/2022 S Tergus032222Self 0.64 / mg/L /
05/27/2022 P Tergus052722POTW 0.6 / mg/L /
Mar 2022 Week 4 0.64 / mg/L /
May 2022 Week 4 0.6 / mg/L /
Mar 2022 Average 0.64 / mg/L /
May 2022 Average 0.6 / mg/L /
2022 Quarter 1 0.64 / mg/L /
2022 Quarter 2 0.6 / mg/L /
2022 1 st 6 Months(Avg) 0.62 / mg/L /
2022 lst6...(Max) 0.64 / mg/L /
2022 lst6...(Min) 0.6 / mg/L /
2022 lst6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
05/27/2022 P Tergus052722POTW < 0.003 /20.7 mg/L < /
May 2022 Week 4 < 0.003 / mg/L < /
May 2022 Average < 0.003 /8.2 mg/L < /
2022 Quarter 2 < 0.003 / mg/L < /
2022 1 st 6 Months(Avg) < 0.003 / mg/L < /
2022 lst6...(Max) < 0.003 / mg/L < /
2022 lst6...(Min) < 0.003 / mg/L < /
2022 lst6...(Count) 1
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Tuesday,February 28,2023 10:50:14AM *Indicates Violation **Indicates TRC Violation Page 5 of 13

Tereus Pharma
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Lead
03/22/2022 S Tergus032222Self 0.0374 / mg/L /
05/27/2022 P Tergus052722POTW 0.0006 / mg/L /
Mar 2022 Week 4 0.0374 / mg/L /
May 2022 Week 4 0.0006 / mg/L /
Mar 2022 Average 0.0374 / mg/L /
May 2022 Average 0.0006 / mg/L /
2022 Quarter 1 0.0374 / mg/L /
2022 Quarter 2 0.0006 / mg/L /
2022 1 st 6 Months(Avg) 0.019 / mg/L /
2022 lst6...(Max) 0.0374 / mg/L /
2022 lst6...(Min) 0.0006 / mg/L /
2022 lst6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
03/22/2022 S Tergus032222Self < 0.000001 /0.000142 mg/L < /
05/27/2022 P Tergus052722POTWH 0.000003 /0.000142 mg/L /
9
Mar 2022 Week 4 < 0.000001 / mg/L < /
May 2022 Week 4 0.000003 / mg/L /
Mar 2022 Average < 0.000001 / mg/L < /
May 2022 Average 0.000003 / mg/L /
2022 Quarter 1 < 0.000001 / mg/L < /
2022 Quarter 2 0.000003 / mg/L /
2022 1 st 6 Months(Avg) < 0.000002 / mg/L < /
2022 lst6...(Max) 0.000003 / mg/L /
2022 lst6...(Min) < 0.000001 / mg/L < /
2022 lst6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
05/27/2022 P Tergus052722POTW < 0.003 /3.0 mg/L < /
May 2022 Week 4 < 0.003 / mg/L < /
May 2022 Average < 0.003 /0.7 mg/L < /
Tuesday,February 28,2023 10:50:14AM *Indicates Violation **Indicates TRC Violation Page 6 of 13

Tereus Pharma
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
2022 Quarter 2 < 0.003 / mg/L < /
2022 1 st 6 Months(Avg) < 0.003 / mg/L < /
2022 lst6...(Max) < 0.003 / mg/L < /
2022 lst6...(Min) < 0.003 / mg/L < /
2022 lst6...(Count) 1
Sample Count: 1 Months Sampled: l Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
03/22/2022 S Tergus032222Self < 0.003 / mg/L < /
05/27/2022 P Tergus052722POTW < 0.001 / mg/L < /
Mar 2022 Week 4 < 0.003 / mg/L < /
May 2022 Week 4 < 0.001 / mg/L < /
Mar 2022 Average < 0.003 / mg/L < /
May 2022 Average < 0.001 / mg/L < /
2022 Quarter 1 < 0.003 / mg/L < /
2022 Quarter 2 < 0.001 / mg/L < /
2022 1 st 6 Months(Avg) < 0.002 / mg/L < /
2022 lst6...(Max) < 0.003 / mg/L < /
2022 lst6...(Min) < 0.001 / mg/L < /
2022 lst6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
05/27/2022 P Tergus052722POTW < 0.003 /20.7 mg/L < /
May 2022 Week 4 < 0.003 / mg/L < /
May 2022 Average < 0.003 /8.2 mg/L < /
2022 Quarter 2 < 0.003 / mg/L < /
2022 1 st 6 Months(Avg) < 0.003 / mg/L < /
2022 lst6...(Max) < 0.003 / mg/L < /
2022 lst6...(Min) < 0.003 / mg/L < /
2022 lst6...(Count) 1 / /
Tuesday,February 28,2023 10:50:14AM *Indicates Violation **Indicates TRC Violation Page 7 of 13

Tereus Pharma
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
03/22/2022 S Tergus032222Self 0.0511 / mg/L /
05/27/2022 P Tergus052722POTW 0.011 / mg/L /
Mar 2022 Week 4 0.0511 / mg/L /
May 2022 Week 4 0.011 / mg/L /
Mar 2022 Average 0.0511 / mg/L /
May 2022 Average 0.011 / mg/L /
2022 Quarter 1 0.0511 / mg/L /
2022 Quarter 2 0.011 / mg/L /
2022 1 st 6 Months(Avg) 0.0311 / mg/L /
2022 lst6...(Max) 0.0511 / mg/L /
2022 lst6...(Min) 0.011 / mg/L /
2022 lst6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
03/22/2022 S Tergus032222Self 0.4 / mg/L /
05/27/2022 P Tergus052722POTW 0.2 / mg/L /
Mar 2022 Week 4 0.4 / mg/L /
May 2022 Week 4 0.2 / mg/L /
Mar 2022 Average 0.4 / mg/L /
May 2022 Average 0.2 / mg/L /
2022 Quarter 1 0.4 / mg/L /
2022 Quarter 2 0.2 / mg/L /
2022 1 st 6 Months(Avg) 0.3 / mg/L /
2022 lst6...(Max) 0.4 / mg/L /
2022 lst6...(Min) 0.2 / mg/L /
2022 lst6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
03/22/2022 S Tergus032222Self 2.03 / mg/L /
05/27/2022 P Tergus052722POTW 3.96 / mg/L /
Mar 2022 Week 4 2.03 / mg/L /
Tuesday,February 28,2023 10:50:14AM *Indicates Violation **Indicates TRC Violation Page 8 of 13

Tereus Pharma
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
Nitrogen,Total
May 2022 Week 4 3.96 / mg/L /
Mar 2022 Average 2.03 / mg/L /
May 2022 Average 3.96 / mg/L /
2022 Quarter 1 2.03 / mg/L /
2022 Quarter 2 3.96 / mg/L /
2022 1 st 6 Months(Avg) 3.00 / mg/L /
2022 lst6...(Max) 3.96 / mg/L /
2022 lst6...(Min) 2.03 / mg/L /
2022 1st 6...(Count) 2
SampleDate SampleID Result/Limit Mass/Limit
Oil&Grease,Total
03/22/2022 S Tergus032222Self 17.4 /200 mg/L /
05/27/2022 P Tergus052722POTW 5.4 /200 mg/L /
Mar 2022 Week 4 17.4 / mg/L /
May 2022 Week 4 5.4 / mg/L /
Mar 2022 Average 17.4 / mg/L /
May 2022 Average 5.4 / mg/L /
2022 Quarter 1 17.4 / mg/L /
2022 Quarter 2 5.4 / mg/L /
2022 1 st 6 Months(Avg) 11.4 / mg/L /
2022 lst6...(Max) 17.4 / mg/L /
2022 lst6...(Min) 5.4 / mg/L /
2022 lst6...(Count) 2
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
pH
03/22/2022 S Tergus032222Self 8.8 /6.0-10.0 SU /
05/27/2022 P Tergus052722POTW 6.5 /6.0-10.0 SU /
Mar 2022 Week 4 8.8 / SU /
May 2022 Week 4 6.5 / SU /
Mar 2022 Average 8.8 / SU /
May 2022 Average 6.5 / SU /
Tuesday,February 28,2023 10:50:14AM *Indicates Violation **Indicates TRC Violation Page 9 of 13

Tereus Pharma
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
pH
2022 Quarter 1 8.8 / SU /
2022 Quarter 2 6.5 / SU /
2022 1 st 6 Months(Avg) 7.65 / SU /
2022 lst6...(Max) 8.8 / SU /
2022 lst6...(Min) 6.5 / SU /
2022 1st 6...(Count) 2
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result l Limit Mass l Limit
Selenium
03/22/2022 S Tergus032222Self < 0.0013 / mg/L < /
05/27/2022 P Tergus052722POTW < 0.0005 / mg/L < /
Mar 2022 Week 4 < 0.0013 / mg/L < /
May 2022 Week 4 < 0.0005 / mg/L < /
Mar 2022 Average < 0.0013 / mg/L < /
May 2022 Average < 0.0005 / mg/L < /
2022 Quarter 1 < 0.0013 / mg/L < /
2022 Quarter 2 < 0.0005 / mg/L < /
2022 1 st 6 Months(Avg) < 0.0009 / mg/L < /
2022 lst6...(Max) < 0.0013 / mg/L < /
2022 lst6...(Min) < 0.0005 / mg/L < /
2022 lst6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Silver
03/22/2022 S Tergus032222Self < 0.0005 / mg/L < /
05/27/2022 P Tergus052722POTW < 0.0003 / mg/L < /
Mar 2022 Week 4 < 0.0005 / mg/L < /
May 2022 Week 4 < 0.0003 / mg/L < /
Mar 2022 Average < 0.0005 / mg/L < /
May 2022 Average < 0.0003 / mg/L < /
2022 Quarter 1 < 0.0005 / mg/L < /
2022 Quarter 2 < 0.0003 / mg/L < /
2022 1 st 6 Months(Avg) < 0.0004 / mg/L < /
Tuesday,February 28,2023 10:50:14AM *Indicates Violation **Indicates TRC Violation Page 10 of 13

Tereus Pharma
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Silver
2022 lst6...(Max) < 0.0005 / mg/L < /
2022 lst6...(Min) < 0.0003 / mg/L < /
2022 lst6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
03/22/2022 S Tergus032222Self 25.5 /66 °C /
05/27/2022 P Tergus052722POTW 27 /66 °C /
Mar 2022 Week 4 25.5 / °C /
May 2022 Week 4 27 / °C /
Mar 2022 Average 25.5 / °C /
May 2022 Average 27 / °C /
2022 Quarter 1 25.5 / °C /
2022 Quarter 27 / °C /
2022 1 st 6 Months(Avg) 26.3 / °C /
2022 lst6...(Max) 27 / °C /
2022 lst6...(Min) 25.5 / °C /
2022 lst6...(Count) 2
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
03/22/2022 S Tergus032222Self 1.66 / mg/L /
05/27/2022 P Tergus052722POTW 3.77 / mg/L /
Mar 2022 Week 4 1.66 / mg/L /
May 2022 Week 4 3.77 / mg/L /
Mar 2022 Average 1.66 / mg/L /
May 2022 Average 3.77 / mg/L /
2022 Quarter 1 1.66 / mg/L /
2022 Quarter 2 3.77 / mg/L /
2022 1 st 6 Months(Avg) 2.72 / mg/L /
2022 lst6...(Max) 3.77 / mg/L /
2022 lst6...(Min) 1.66 / mg/L /
2022 lst6...(Count) 2 / /
Tuesday,February 28,2023 10:50:14AM *Indicates Violation **Indicates TRC Violation Page 11 of 13

Tereus Pharma
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
Total Phosphorus
03/22/2022 S Tergus032222Self 3.42 / mg/L /
05/27/2022 P Tergus052722POTW 7.72 / mg/L /
Mar 2022 Week 4 3.42 / mg/L /
May 2022 Week 4 7.72 / mg/L /
Mar 2022 Average 3.42 / mg/L /
May 2022 Average 7.72 / mg/L /
2022 Quarter 1 3.42 / mg/L /
2022 Quarter 2 7.72 / mg/L /
2022 1 st 6 Months(Avg) 5.57 / mg/L /
2022 lst6...(Max) 7.72 / mg/L /
2022 lst6...(Min) 3.42 / mg/L /
2022 lst6...(Count) 2 / /
Sample Date SampleID Result/Limit Mass Mmit
TSS
03/22/2022 S Tergus032222Self 7.2 / mg/L /
05/27/2022 P Tergus052722POTW 8 / mg/L /
Mar 2022 Week 4 7.2 / mg/L /
May 2022 Week 4 8 / mg/L /
Mar 2022 Average 7.2 / mg/L /
May 2022 Average 8 / mg/L /
2022 Quarter 1 7.2 / mg/L /
2022 Quarter 2 8 / mg/L /
2022 1 st 6 Months(Avg) 7.6 / mg/L /
2022 lst6...(Max) 8 / mg/L /
2022 lst6...(Min) 7.2 / mg/L /
2022 lst6...(Count) 2 / /
Sample Date SampleID Result/Limit Mass/Limit
VOC
05/27/2022 P Tergus052722POTW 0.998 / mg/L /
May 2022 Week 4 0.998 / mg/L /
May 2022 Average 0.998 / mg/L /
2022 Quarter 2 0.998 / mg/L /
2022 1 st 6 Months(Avg) 0.998 / mg/L /
2022 lst6...(Max) 0.998 / mg/L /
2022 lst6...(Min) 0.998 / mg/L /
2022 lst6...(Count) 1 / /
Sample Date SampleID Result/Limit Mass/Limit
Zinc
Tuesday,February 28,2023 10:50:14AM *Indicates Violation **Indicates TRC Violation Page 12 of 13

Tereus Pharma
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
03/22/2022 S Tergus032222Self 1.07 / mg/L /
05/27/2022 P Tergus052722POTW 0.417 / mg/L /
Mar 2022 Week 4 1.07 / mg/L /
May 2022 Week 4 0.417 / mg/L /
Mar 2022 Average 1.07 / mg/L /
May 2022 Average 0.417 / mg/L /
2022 Quarter 1 1.07 / mg/L /
2022 Quarter 2 0.417 / mg/L /
2022 1 st 6 Months(Avg) 0.744 / mg/L /
2022 lst6...(Max) 1.07 / mg/L /
2022 Ist6...(Min) 0.417 / mg/L /
2022 Ist 6...(Count) 2 / /
Tuesday,February 28,2023 10:50:14AM *Indicates Violation **Indicates TRC Violation Page 13 of 13

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
05/05/2022 P TriPharnt050522PO < 0.025 / 5.44 mg/L < 0.0012 / lbs/day
TW
May 2022 Week 1 < 0.025 / mg/L < 0.0012 / lbs/day
May 2022 Average < 0.025 / 2.15 mg/L < 0.0012 / lbs/day
2022 Quarter 2 < 0.025 / mg/L < 0.0012 / lbs/day
2022 1 st 6 Months(Avg) < 0.025 / mg/L < 0.0012 / lbs/day
2022 1st 6...(Max) < 0.025 / mg/L < 0.0012 / lbs/day
2022 lst6...(Min) < 0.025 / mg/L < 0.0012 / lbs/day
2022 lst6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
03/08/2022 S TriPharm03O822Self < 0.05 / mg/L < /
05/05/2022 P TriPharm050522PO 0.3 / mg/L 0.0139 / lbs/day
TW
Mar 2022 Week 2 < 0.05 / mg/L < /
May 2022 Week 1 0.3 / mg/L 0.0139 / lbs/day
Mar 2022 Average < 0.05 / mg/L < /
May 2022 Average 0.3 / mg/L 0.0139 / lbs/day
2022 Quarter 1 < 0.05 / mg/L < /
2022 Quarter 2 0.3 / mg/L 0.0139 / lbs/day
2022 1 st 6 Months(Avg) < 0.18 / mg/L < 0.0139 / lbs/day
2022 lst6...(Max) 0.3 / mg/L 0.0139 / lbs/day
2022 lst6...(Min) < 0.05 / mg/L < /
2022 1st6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2022 S TriPharm0122F1ow 0.006694 / MGD /
02/28/2022 S TriPharm0222F1ow 0.007957 / MGD /
03/31/2022 S TriPharm0322F1ow 0.007401 / MGD /
04/30/2022 S TriPharm0422F1ow 0.00774 / MGD /
05/31/2022 S TriPharm0522FIow 0.004312 / MGD /
06/30/2022 S TriPharm0622F1ow 0.004167 / MGD /
Jan 2022 Week 4 0.006694 / MGD /
Feb 2022 Week 4 0.007957 / MGD /
Mar 2022 Week 4 0.007401 / MGD /
Apr 2022 Week 4 0.00774 / MGD /
Tuesday,February 21,2023 10:18:05PM *Indicates Violation **Indicates TRC Violation Page 1 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
May 2022 Week 4 0.004312 / MGD /
Jun 2022 Week 4 0.004167 / MGD /
Jan 2022 Average 0.006694 / 0.005 MGD * /
Feb 2022 Average 0.007957 / 0.005 MGD * /
Mar 2022 Average 0.007401 / 0.005 MGD * /
Apr 2022 Average 0.00774 / 0.005 MGD * /
May 2022 Average 0.004312 / 0.005 MGD /
Jun 2022 Average 0.004167 / 0.005 MGD /
2022 Quarter 1 0.007351 / MGD /
2022 Quarter 2 0.005406 / MGD /
2022 1 st 6 Months(Avg) 0.006379 / MGD /
2022 lst6...(Max) 0.007957 / MGD /
2022 lst6...(Min) 0.004167 / MGD /
2022 lst6...(Count) 6
Sample Date SamplelD Result/Limit Mass/Limit
BOD
03/08/2022 S TriPharn103O822Self 5.3 / mg/L /
05/05/2022 P TriPharm050522PO 3.1 / mg/L 0.143 / lbs/day
TW
Mar 2022 Week 2 5.3 / mg/L /
May 2022 Week 1 3.1 / mg/L 0.143 / lbs/day
Mar 2022 Average 5.3 / mg/L /
May 2022 Average 3.1 / mg/L 0.143 / lbs/day
2022 Quarter 1 5.3 / mg/L /
2022 Quarter 2 3.1 / mg/L 0.143 / lbs/day
2022 1 st 6 Months(Avg) 4.2 / mg/L 0.143 / lbs/day
2022 lst6...(Max) 5.3 / mg/L 0.143 / lbs/day
2022 lst6...(Min) 3.1 / mg/L /
2022 1st 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
03/08/2022 S TriPharm030822Self < 0.00008 / mg/L < /
05/05/2022 P TriPharrn050522PO < 0.00008 / mg/L < 0.000003 / lbs/day
TW
Mar 2022 Week 2 < 0.00008 / mg/L < /
May 2022 Week 1 < 0.00008 / mg/L < 0.000003 / lbs/day
Tuesday,February 21,2023 10:18:05PM *Indicates Violation **Indicates TRC Violation Page 2 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
Cadmium
Mar 2022 Average < 0.00008 / mg/L < /
May 2022 Average < 0.00008 / mg/L < 0.000003 / lbs/day
2022 Quarter 1 < 0.00008 / mg/L < /
2022 Quarter 2 < 0.00008 / mg/L < 0.000003 / lbs/day
2022 1 st 6 Months(Avg) < 0.00008 / mg/L < 0.000003 / lbs/day
2022 lst6...(Max) < 0.00008 / mg/L < 0.000003 / lbs/day
2022 lst6...(Min) < 0.00008 / mg/L < /
2022 1st6...(Count) 2 / I /
Sample Date SampleID Result/Limit Mass/Limit
Chloride
03/08/2022 S TriPharm03O822Self 12 / mg/L /
05/05/2022 P TriPharm050522P0 12 / mg/L 0.554 / lbs/day
TW
Mar 2022 Week 2 12 / mg/L /
May 2022 Week 1 12 / mg/L 0.554 / lbs/day
Mar 2022 Average 12 / mg/L /
May 2022 Average 12 / mg/L 0.554 / lbs/day
2022 Quarter 1 12 / mg/L /
2022 Quarter 2 12 / mg/L 0.554 / lbs/day
2022 1 st 6 Months(Avg) 12 / mg/L 0.5540 / lbs/day
2022 lst6...(Max) 12 / mg/L 0.5540 / lbs/day
2022 lst6...(Min) 12 / mg/L /
2022 lst6...(Count) 2 / 1 /
Sample Date SampleID Result/Limit Mass/Limit
COD
03/08/2022 S TriPharm030822Self < 7.5 / mg/L < /
05/05/2022 P TriPhar1n050522P0 30 / mg/L 1.39 / lbs/day
TW
Mar 2022 Week 2 < 7.5 / mg/L < /
May 2022 Week 1 30 / mg/L 1.39 / lbs/day
Mar 2022 Average < 7.5 / mg/L < /
May 2022 Average 30 / mg/L 1.39 / lbs/day
2022 Quarter 1 < 7.5 / mg/L < /
2022 Quarter 2 30 / mg/L 1.39 / lbs/day
2022 1 st 6 Months(Avg) < 18.8 / mg/L < 1.39 / lbs/day
2022 lst6...(Max) 30 / mg/L 1.39 / lbs/day
Tuesday,February 21,2023 10:18:05PM *Indicates Violation **Indicates TRC Violation Page 3 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
COD
2022 1st 6...(Min) < 7.5 / mg/L < /
2022 lst6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
05/05/2022 P TriPhann05O522PO < 0.003 / mg/L < 0.000115 / lbs/day
TW
May 2022 Week 1 < 0.003 / mg/L < 0.000115 / lbs/day
May 2022 Average < 0.003 / mg/L < 0.000115 / lbs/day
2022 Quarter 2 < 0.003 / mg/L < 0.000115 / lbs/day
2022 1 st 6 Months(Avg) < 0.003 / mg/L < 0.000115 / lbs/day
2022 lst6...(Max) < 0.003 / mg/L < 0.000115 / lbs/day
2022 lst6...(Min) < 0.003 / mg/L < 0.000115 / lbs/day
2022 lst6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
05/05/2022 P TriPharm050522P0 < 0.005 / 5.44 mg/L < 0.0002 / lbs/day
TW
May 2022 Week 1 < 0.005 / mg/L < 0.0002 / lbs/day
May 2022 Average < 0.005 / 2.15 mg/L < 0.0002 / lbs/day
2022 Quarter 2 < 0.005 / mg/L < 0.0002 / lbs/day
2022 1 st 6 Months(Avg) < 0.005 / mg/L < 0.0002 / lbs/day
2022 lst6...(Max) < 0.005 / mg/L < 0.0002 / lbs/day
2022 1st 6...(Min) < 0.005 / mg/L < 0.0002 / lbs/day
2022 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
03/08/2022 S TriPharm030822Se1f 0.32 / mg/L /
05/05/2022 P TriPharm050522P0 0.74 / mg/L 0.0342 / lbs/day
TW
Mar 2022 Week 2 0.32 / mg/L /
May 2022 Week 1 0.74 / mg/L 0.0342 / lbs/day
Mar 2022 Average 0.32 / mg/L /
May 2022 Average 0.74 / mg/L 0.0342 / lbs/day
2022 Quarter 1 0.32 / mg/L /
2022 Quarter 2 0.74 / mg/L 0.0342 / lbs/day
Tuesday,February 21,2023 10:18:05PM *Indicates Violation **Indicates TRC Violation Page 4 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
2022 1 st 6 Months(Avg) 0.53 / mg/L 0.0342 / lbs/day
2022 lst6...(Max) 0.74 / mg/L 0.0342 / lbs/day
2022 lst6...(Min) 0.32 / mg/L /
2022 lst6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
05/05/2022 P TriPharm050522PO < 0.005 / 5.44 mg/L < 0.0002 / lbs/day
TW
May 2022 Week 1 < 0.005 / mg/L < 0.0002 / lbs/day
May 2022 Average < 0.005 / 2.15 mg/L < 0.0002 / lbs/day
2022 Quarter 2 < 0.005 / mg/L < 0.0002 / lbs/day
2022 1 st 6 Months(Avg) < 0.005 / mg/L < 0.0002 / lbs/day
2022 lst6...(Max) < 0.005 / mg/L < 0.0002 / lbs/day
2022 lst6...(Min) < 0.005 / mg/L < 0.0002 / lbs/day
2022 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
03/07/2022 S TriPharrn03O722Self 0.000002 / 0.000142 mg/L /
Hg
05/04/2022 P TriPharrn05O422PO 0.000001 / 0.000142 mg/L /
TWHg
Mar 2022 Week 1 0.000002 / mg/L /
May 2022 Week 1 0.000001 / mg/L /
Mar 2022 Average 0.000002 / mg/L /
May 2022 Average 0.000001 / mg/L /
2022 Quarter 1 0.000002 / mg/L /
2022 Quarter 0.000001 / mg/L /
2022 1 st 6 Months(Avg) 0.000002 / mg/L /
2022 lst6...(Max) 0.000002 / mg/L /
2022 1st 6...(Min) 0.000001 / mg/L /
2022 lst6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
05/05/2022 P TriPharm05O522PO < 0.003 / 0.78 mg/L < 0.000115 / lbs/day
TW
Tuesday,February 21,2023 10:18:05PM *Indicates Violation **Indicates TRC Violation Page 5 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
May 2022 Week 1 < 0.003 / mg/L < 0.000115 / lbs/day
May 2022 Average < 0.003 / 0.18 mg/L < 0.000115 / lbs/day
2022 Quarter 2 < 0.003 / mg/L < 0.000115 / lbs/day
2022 1 st 6 Months(Avg) < 0.003 / mg/L < 0.000115 / lbs/day
2022 lst6...(Max) < 0.003 / mg/L < 0.000115 / lbs/day
2022 lst6...(Min) < 0.003 / mg/L < 0.000115 / lbs/day
2022 lst6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
03/08/2022 S TriPharm030822Self < 0.001 / mg/L < /
05/05/2022 P TriPhann05O522PO < 0.001 / mg/L < 0 / lbs/day
TW
Mar 2022 Week 2 < 0.001 / mg/L < /
May 2022 Week 1 < 0.001 / mg/L < 0 / lbs/day
Mar 2022 Average < 0.001 / mg/L < /
May 2022 Average < 0.001 / mg/L < 0 / lbs/day
2022 Quarter 1 < 0.001 / mg/L < /
2022 Quarter 2 < 0.001 / mg/L < 0 / lbs/day
2022 1 st 6 Months(Avg) < 0.001 / mg/L < 0.0000 / lbs/day
2022 lst6...(Max) < 0.001 / mg/L < 0.0000 / lbs/day
2022 lst6...(Min) < 0.001 / mg/L < /
2022 1st6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
05/05/2022 P TriPharm050522PO < 0.005 / 5.44 mg/L < 0.0002 / lbs/day
TW
May 2022 Week 1 < 0.005 / mg/L < 0.0002 / lbs/day
May 2022 Average < 0.005 / 2.15 mg/L < 0.0002 / lbs/day
2022 Quarter 2 < 0.005 / mg/L < 0.0002 / lbs/day
2022 1 st 6 Months(Avg) < 0.005 / mg/L < 0.0002 / lbs/day
2022 lst6...(Max) < 0.005 / mg/L < 0.0002 / lbs/day
2022 lst6...(Min) < 0.005 / mg/L < 0.0002 / lbs/day
2022 1st 6...(Count) 1 / 1 /
Tuesday,February 21,2023 10:18:05PM *Indicates Violation **Indicates TRC Violation Page 6 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
03/08/2022 S TriPhar1n03O822Self 1 / mg/L /
05/05/2022 P TriPharrn05O522PO 2 / mg/L 0.092 / lbs/day
TW
Mar 2022 Week 2 1 / mg/L /
May 2022 Week 1 2 / mg/L 0.092 / lbs/day
Mar 2022 Average 1 / mg/L /
May 2022 Average 2 / mg/L 0.092 / lbs/day
2022 Quarter 1 1 / mg/L /
2022 Quarter 2 2 / mg/L 0.092 / lbs/day
2022 1 st 6 Months(Avg) 1.5 / mg/L 0.092 / lbs/day
2022 1st6...(Max) 2.0 / mg/L 0.092 / lbs/day
2022 1st 6...(Min) 1.0 / mg/L /
2022 lst6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
03/08/2022 S TriPharm030822Self 1.25 / mg/L /
05/05/2022 P TriPharm05O522PO 2.54 / mg/L 0.117 / lbs/day
TW
Mar 2022 Week 2 1.25 / mg/L /
May 2022 Week 1 2.54 / mg/L 0.117 / lbs/day
Mar 2022 Average 1.25 / mg/L /
May 2022 Average 2.54 / mg/L 0.117 / lbs/day
2022 Quarter 1 1.25 / mg/L /
2022 Quarter 2 2.54 / mg/L 0.117 / lbs/day
2022 1 st 6 Months(Avg) 1.90 / mg/L 0.117 / lbs/day
2022 lst6...(Max) 2.54 / mg/L 0.117 / lbs/day
2022 lst6...(Min) 1.25 / mg/L /
2022 lst6...(Count) 2 / 1 /
Sample Date SampleID Result/Limit Mass/Limit
pH
03/08/2022 S TriPharm03O822Self 7.2 / 5.5-10.5 su /
05/05/2022 P TriPharm050522PO 7.1 / 5.5-10.5 su /
TW
Mar 2022 Week 2 7.2 / su /
May 2022 Week 1 7.1 / Su /
Mar 2022 Average 7.2 / Su /
Tuesday,February 21,2023 10:18:05PM *Indicates Violation **Indicates TRC Violation Page 7 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
PH
May 2022 Average 7.1 / su /
2022 Quarter 1 7.2 / SU /
2022 Quarter 2 7.1 / su /
2022 1 st 6 Months(Avg) 7.15 / su /
2022 lst6...(Max) 7.2 / su /
2022 1st 6...(Min) 7.1 / su /
2022 lst6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
03/08/2022 S TriPharm03O822Self 20 / 66 °C /
05/05/2022 P TriPhann05O522PO 28 / 66 °C /
TW
Mar 2022 Week 2 20 / °C /
May 2022 Week 1 28 / °C /
Mar 2022 Average 20 / °C /
May 2022 Average 28 / °C /
2022 Quarter 1 20 / °C /
2022 Quarter 28 / °C /
2022 1 st 6 Months(Avg) 24 / °C /
2022 1st 6...(Max) 28 / °C /
2022 lst6...(Min) 20 / °C /
2022 lst6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
TKN
03/08/2022 S TriPhann03O822Self 0.26 / mg/L /
05/05/2022 P TriPharn1050522PO 0.55 / mg/L 0.025 / lbs/day
TW
Mar 2022 Week 2 0.26 / mg/L /
May 2022 Week 1 0.55 / mg/L 0.025 / lbs/day
Mar 2022 Average 0.26 / mg/L /
May 2022 Average 0.55 / mg/L 0.025 / lbs/day
2022 Quarter 1 0.26 / mg/L /
2022 Quarter 2 0.55 / mg/L 0.025 / lbs/day
2022 1 st 6 Months(Avg) 0.41 / mg/L 0.025 / lbs/day
2022 lst6...(Max) 0.55 / mg/L 0.025 / lbs/day
2022 lst6...(Min) 0.26 / mg/L /
Tuesday,February 21,2023 10:18:05PM *Indicates Violation **Indicates TRC Violation Page 8 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
TKN
2022 1st 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
03/08/2022 S TriPhar1n03O822Self 0.226 / mg/L /
05/05/2022 P TriPharm05O522PO 0.475 / mg/L 0.0219 / lbs/day
TW
Mar 2022 Week 2 0.226 / mg/L /
May 2022 Week 1 0.475 / mg/L 0.0219 / lbs/day
Mar 2022 Average 0.226 / mg/L /
May 2022 Average 0.475 / mg/L 0.0219 / lbs/day
2022 Quarter 1 0.226 / mg/L /
2022 Quarter 2 0.475 / mg/L 0.0219 / lbs/day
2022 1 st 6 Months(Avg) 0.351 / mg/L 0.0219 / lbs/day
2022 lst6...(Max) 0.475 / mg/L 0.0219 / lbs/day
2022 lst6...(Min) 0.226 / mg/L /
2022 lst6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
TSS
03/08/2022 S TriPhann03O822Se1f < 1.6 / mg/L < /
05/05/2022 P TriPharm05O522PO < 1.5 / mg/L < 0.066947 / lbs/day
TW
Mar 2022 Week 2 < 1.6 / mg/L < /
May 2022 Week 1 < 1.5 / mg/L < 0.066947 / lbs/day
Mar 2022 Average < 1.6 / mg/L < /
May 2022 Average < 1.5 / mg/L < 0.066947 / lbs/day
2022 Quarter 1 < 1.6 / mg/L < /
2022 Quarter 2 < 1.5 / mg/L < 0.066947 / lbs/day
2022 1 st 6 Months(Avg) < 1.5 / mg/L < 0.066947 / lbs/day
2022 lst6...(Max) < 1.6 / mg/L < 0.066947 / lbs/day
2022 lst6...(Min) < 1.5 / mg/L < /
2022 1st6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
03/08/2022 S TriPhann03O822Self 0.019 / mg/L /
Tuesday,February 21,2023 10:18:05PM *Indicates Violation **Indicates TRC Violation Page 9 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
VOC
05/05/2022 P TriPharrn050522PO < 0.025 / mg/L < /
TW
Mar 2022 Week 2 0.019 / mg/L /
May 2022 Week 1 < 0.025 / mg/L < /
Mar 2022 Average 0.019 / mg/L /
May 2022 Average < 0.025 / mg/L < /
2022 Quarter 1 0.019 / mg/L /
2022 Quarter 2 < 0.025 / mg/L < /
2022 1st 6 Months(Avg) < 0.022 / mg/L < /
2022 lst6...(Max) < 0.025 / mg/L < /
2022 lst6...(Min) 0.019 / mg/L /
2022 1st 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
03/08/2022 S TriPharm03O822Self 0.089 / mg/L /
05/05/2022 P TriPharrn05O522PO 0.277 / mg/L 0.012789 / lbs/day
TW
Mar 2022 Week 2 0.089 / mg/L /
May 2022 Week 1 0.277 / mg/L 0.012789 / lbs/day
Mar 2022 Average 0.089 / mg/L /
May 2022 Average 0.277 / mg/L 0.012789 / lbs/day
2022 Quarter 1 0.089 / mg/L /
2022 Quarter 2 0.277 / mg/L 0.012789 / lbs/day
2022 1 st 6 Months(Avg) 0.183 / mg/L 0.012789 / lbs/day
2022 lst6...(Max) 0.277 / mg/L 0.012789 / lbs/day
2022 1st 6...(Min) 0.089 / mg/L /
2022 lst6...(Count) 2 / 1 /
Tuesday,February 21,2023 10:18:05PM *Indicates Violation **Indicates TRC Violation Page 10 of 10

United Therapeutics Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
02/02/2022 S UTP1020222Self 2.7 / mg/L 0.6537 / lbs/day
03/11/2022 P UTP1031122POTW 2.6 / mg/L /
Feb 2022 Week 1 2.7 / mg/L 0.6537 / lbs/day
Mar 2022 Week 2 2.6 / mg/L /
Feb 2022 Average 2.7 / mg/L 0.6537 / lbs/day
Mar 2022 Average 2.6 / mg/L /
2022 Quarter 1 2.65 / mg/L 0.6537 / lbs/day
2022 1 st 6 Months(Avg) 2.65 / mg/L 0.6537 / lbs/day
2022 lst6...(Max) 2.7 / mg/L 0.6537 / lbs/day
2022 lst6...(Min) 2.6 / mg/L /
2022 lst6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2022 S UTP10122F1ow 0.027 / MGD /
02/28/2022 S UTP10222F1ow 0.024 / MGD /
03/31/2022 S UTP10322F1ow 0.022 / MGD /
04/30/2022 S UTP10422F1ow 0.023 / MGD /
05/31/2022 S UTP10522F1ow 0.026 / MGD /
06/30/2022 S UTP10622F1ow 0.031 / MGD /
Jan 2022 Week 4 0.027 / MGD /
Feb 2022 Week 4 0.024 / MGD /
Mar 2022 Week 4 0.022 / MGD /
Apr 2022 Week 4 0.023 / MGD /
May 2022 Week 4 0.026 / MGD /
Jun 2022 Week 4 0.031 / MGD /
Jan 2022 Average 0.027 / MGD /
Feb 2022 Average 0.024 / MGD /
Mar 2022 Average 0.022 / MGD /
Apr 2022 Average 0.023 / MGD /
May 2022 Average 0.026 / MGD /
Jun 2022 Average 0.031 / MGD /
2022 Quarter 1 0.024333 / MGD /
2022 Quarter 2 0.026667 / MGD /
2022 1 st 6 Months(Avg) 0.0255 / MGD /
2022 lst6...(Max) 0.031 / MGD /
2022 lst6...(Min) 0.022 / MGD /
Tuesday,February 21,2023 10:26:41PM *Indicates Violation **Indicates TRC Violation Pagel of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
2022 1st 6...(Count) 6
Sample Date SamplelD Result/Limit Mass/Limit
BOD
02/02/2022 S UTP1020222Self 52.4 / mg/L 12.687 / lbs/day
03/11/2022 P UTP1031122POTW 78.5 / mg/L /
Feb 2022 Week 1 52.4 / mg/L 12.687 / lbs/day
Mar 2022 Week 2 78.5 / mg/L /
Feb 2022 Average 52.4 / mg/L 12.687 / lbs/day
Mar 2022 Average 78.5 / mg/L /
2022 Quarter 1 65.5 / mg/L 12.687 / lbs/day
2022 1 st 6 Months(Avg) 65.5 / mg/L 12.687 / lbs/day
2022 lst6...(Max) 78.5 / mg/L 12.687 / lbs/day
2022 1st 6...(Min) 52.4 / mg/L /
2022 lst6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
02/02/2022 S UTP1020222Self < 0.0005 / mg/L < 0.000121 / lbs/day
Feb 2022 Week 1 < 0.0005 / mg/L < 0.000121 / lbs/day
Feb 2022 Average < 0.0005 / mg/L < 0.000121 / lbs/day
2022 Quarter 1 < 0.0005 / mg/L < 0.000121 / lbs/day
2022 1 st 6 Months(Avg) < 0.0005 / mg/L < 0.000121 / lbs/day
2022 lst6...(Max) < 0.0005 / mg/L < 0.000121 / lbs/day
2022 lst6...(Min) < 0.0005 / mg/L < 0.000121 / lbs/day
2022 1st6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
02/02/2022 S UTP1020222Self 29.8 / mg/L 7.2149 / lbs/day
03/11/2022 P UTP1031122POTW 25 / mg/L /
Feb 2022 Week 1 29.8 / mg/L 7.2149 / lbs/day
Mar 2022 Week 2 25 / mg/L /
Feb 2022 Average 29.8 / mg/L 7.2149 / lbs/day
Mar 2022 Average 25 / mg/L /
2022 Quarter 1 27.4 / mg/L 7.2149 / lbs/day
Tuesday,February 21,2023 10:26:41PM *Indicates Violation **Indicates TRC Violation Page 2 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
2022 1 st 6 Months(Avg) 27.4 / mg/L 7.2149 / lbs/day
2022 lst6...(Max) 29.8 / mg/L 7.2149 / lbs/day
2022 lst6...(Min) 25 / mg/L /
2022 lst6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
COD
02/02/2022 S UTP1020222Self 208 / mg/L 50.36 / lbs/day
03/11/2022 P UTP1031122POTW 177 / mg/L /
Feb 2022 Week 1 208 / mg/L 50.36 / lbs/day
Mar 2022 Week 2 177 / mg/L /
Feb 2022 Average 208 / mg/L 50.36 / lbs/day
Mar 2022 Average 177 / mg/L /
2022 Quarter 1 192.5 / mg/L 50.36 / lbs/day
2022 1 st 6 Months(Avg) 192.5 / mg/L 50.36 / lbs/day
2022 lst6...(Max) 208 / mg/L 50.36 / lbs/day
2022 lst6...(Min) 177 / mg/L /
2022 lst6...(Count) 2 / 1 /
Sample Date SamplelD Result l Limit Mass l Limit
Cyanide
03/11/2022 P UTP1031122POTW < 0.003 / mg/L < /
Mar 2022 Week 2 < 0.003 / mg/L < /
Mar 2022 Average < 0.003 / mg/L < /
2022 Quarter 1 < 0.003 / mg/L < /
2022 1 st 6 Months(Avg) < 0.003 / mg/L < /
2022 lst6...(Max) < 0.003 / mg/L < /
2022 lst6...(Min) < 0.003 / mg/L < /
2022 lst6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
02/02/2022 S UTP1020222Self 0.49 / mg/L 0.1186 / lbs/day
Feb 2022 Week 1 0.49 / mg/L 0.1186 / lbs/day
Feb 2022 Average 0.49 / mg/L 0.1186 / lbs/day
2022 Quarter 1 0.49 / mg/L 0.1186 / lbs/day
Tuesday,February 21,2023 10:26:41PM *Indicates Violation **Indicates TRC Violation Page 3 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
2022 1 st 6 Months(Avg) 0.49 / mg/L 0.1186 / lbs/day
2022 lst6...(Max) 0.49 / mg/L 0.1186 / lbs/day
2022 lst6...(Min) 0.49 / mg/L 0.1186 / lbs/day
2022 lst6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
02/02/2022 S UTP1020222Self 0.000001 / 0.000142 mg/L /
03/10/2022 P UTP1031022POTW 0.000024 / 0.000142 mg/L /
Hg
Feb 2022 Week 1 0.000001 / mg/L /
Mar 2022 Week 2 0.000024 / mg/L /
Feb 2022 Average 0.000001 / mg/L /
Mar 2022 Average 0.000024 / mg/L /
2022 Quarter 1 0.000013 / mg/L /
2022 1 st 6 Months(Avg) 0.000013 / mg/L /
2022 lst6...(Max) 0.000024 / mg/L /
2022 lst6...(Min) 0.000001 / mg/L /
2022 1st6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
02/02/2022 S UTP1020222Self < 0.003 / mg/L < 0.0006 / lbs/day
Feb 2022 Week I < 0.003 / mg/L < 0.0006 / lbs/day
Feb 2022 Average < 0.003 / mg/L < 0.0006 / lbs/day
2022 Quarter 1 < 0.003 / mg/L < 0.0006 / lbs/day
2022 1 st 6 Months(Avg) < 0.003 / mg/L < 0.0006 / lbs/day
2022 lst6...(Max) < 0.003 / mg/L < 0.0006 / lbs/day
2022 lst6...(Min) < 0.003 / mg/L < 0.0006 / lbs/day
2022 lst6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
02/02/2022 S UTP1020222Self 0.6 / mg/L 0.136 / lbs/day
03/11/2022 P UTP1031122POTW 0.8 / mg/L /
Feb 2022 Week 1 0.6 / mg/L 0.136 / lbs/day
Mar 2022 Week 2 0.8 / mg/L /
Tuesday,February 21,2023 10:26:41PM *Indicates Violation **Indicates TRC Violation Page 4 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
Feb 2022 Average 0.6 / mg/L 0.136 / lbs/day
Mar 2022 Average 0.8 / mg/L /
2022 Quarter 1 0.7 / mg/L 0.136 / lbs/day
2022 1 st 6 Months(Avg) 0.7 / mg/L 0.136 / lbs/day
2022 lst6...(Max) 0.8 / mg/L 0.136 / lbs/day
2022 1st 6...(Min) 0.6 / mg/L /
2022 lst6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
02/02/2022 S UTP1020222Self 14.4 / mg/L 3.486 / lbs/day
03/11/2022 P UTP1031122POTW 11.3 / mg/L /
Feb 2022 Week 1 14.4 / mg/L 3.486 / lbs/day
Mar 2022 Week 2 11.3 / mg/L /
Feb 2022 Average 14.4 / mg/L 3.486 / lbs/day
Mar 2022 Average 11.3 / mg/L /
2022 Quarter 1 12.85 / mg/L 3.486 / lbs/day
2022 1 st 6 Months(Avg) 12.85 / mg/L 3.486 / lbs/day
2022 lst6...(Max) 14.4 / mg/L 3.486 / lbs/day
2022 lst6...(Min) 11.3 / mg/L /
2022 1st6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
02/02/2022 S UTP1020222Self < 2.5 / 200 mg/L < /
03/11/2022 P UTP1031122POTW 6.2 / 200 mg/L /
Feb 2022 Week I < 2.5 / mg/L < /
Mar 2022 Week 2 6.2 / mg/L /
Feb 2022 Average < 2.5 / mg/L < /
Mar 2022 Average 6.2 / mg/L /
2022 Quarter I < 4.35 / mg/L < /
2022 1 st 6 Months(Avg) < 4.35 / mg/L < /
2022 lst6...(Max) 6.2 / mg/L /
2022 lst6...(Min) < 2.5 / mg/L < /
2022 lst6...(Count) 2
Tuesday,February 21,2023 10:26:41PM *Indicates Violation **Indicates TRC Violation Page 5 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
PH
02/02/2022 S UTP1020222Self 7.7 / 5.5-10.0 Su /
03/11/2022 P UTP1031122POTW 7 / 5.5-10.0 Su /
Feb 2022 Week 1 7.7 / su /
Mar 2022 Week 2 7 / su /
Feb 2022 Average 7.7 / su /
Mar 2022 Average 7 / Su /
2022 Quarter 1 7.35 / Su /
2022 1 st 6 Months(Avg) 7.35 / su /
2022 lst6...(Max) 7.7 / su /
2022 lst6...(Min) 7 / Su /
2022 1st 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
02/02/2022 S UTP1020222Self 16.5 / 66 °C /
03/11/2022 P UTP1031122POTW 17 / 66 °C /
Feb 2022 Week 1 16.5 / °C /
Mar 2022 Week 2 17 / °C /
Feb 2022 Average 16.5 / °C /
Mar 2022 Average 17 / °C /
2022 Quarter 1 16.8 / °C /
2022 1 st 6 Months(Avg) 16.8 / °C /
2022 lst6...(Max) 17 / °C /
2022 1st 6...(Min) 16.5 / °C /
2022 lst6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
TKN
02/02/2022 S UTP1020222Self 13.9 / mg/L 3.365 / lbs/day
03/11/2022 P UTP1031122POTW 10.5 / mg/L /
Feb 2022 Week 1 13.9 / mg/L 3.365 / lbs/day
Mar 2022 Week 2 10.5 / mg/L /
Feb 2022 Average 13.9 / mg/L 3.365 / lbs/day
Mar 2022 Average 10.5 / mg/L /
2022 Quarter 1 12.2 / mg/L 3.365 / lbs/day
2022 1 st 6 Months(Avg) 12.2 / mg/L 3.365 / lbs/day
2022 lst6...(Max) 13.9 / mg/L 3.365 / lbs/day
Tuesday,February 21,2023 10:26:41PM *Indicates Violation **Indicates TRC Violation Page 6 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
TKN
2022 1st 6...(Min) 10.5 / mg/L /
2022 lst6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
02/02/2022 S UTP1020222Self 2 / mg/L 0.4842 / lbs/day
03/11/2022 P UTP1031122POTW 0.146 / mg/L /
Feb 2022 Week 1 2 / mg/L 0.4842 / lbs/day
Mar 2022 Week 2 0.146 / mg/L /
Feb 2022 Average 2 / mg/L 0.4842 / lbs/day
Mar 2022 Average 0.146 / mg/L /
2022 Quarter 1 1.073 / mg/L 0.4842 / lbs/day
2022 1 st 6 Months(Avg) 1.073 / mg/L 0.4842 / lbs/day
2022 lst6...(Max) 2 / mg/L 0.4842 / lbs/day
2022 lst6...(Min) 0.146 / mg/L /
2022 lst6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
TSS
02/02/2022 S UTP1020222Self 46.9 / mg/L 11.354968 / lbs/day
03/11/2022 P UTP1031122POTW 52 / mg/L /
Feb 2022 Week 1 46.9 / mg/L 11.354968 / lbs/day
Mar 2022 Week 2 52 / mg/L /
Feb 2022 Average 46.9 / mg/L 11.354968 / lbs/day
Mar 2022 Average 52 / mg/L /
2022 Quarter 1 49.5 / mg/L 11.354968 / lbs/day
2022 1 st 6 Months(Avg) 49.5 / mg/L 11.355 / lbs/day
2022 lst6...(Max) 52 / mg/L 11.354968 / lbs/day
2022 lst 6...(Min) 46.9 / mg/L /
2022 1st6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
02/02/2022 S UTP1020222Self 0.0504 / mg/L /
Feb 2022 Week 1 0.0504 / mg/L /
Feb 2022 Average 0.0504 / mg/L /
Tuesday,February 21,2023 10:26:41PM *Indicates Violation **Indicates TRC Violation Page 7 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
VOC
2022 Quarter 1 0.0504 / mg/L /
2022 1 st 6 Months(Avg) 0.0504 / mg/L /
2022 lst6...(Max) 0.0504 / mg/L /
2022 lst6...(Min) 0.0504 / mg/L /
2022 lst6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
02/02/2022 S UTP1020222Self 0.24 / mg/L 0.058106 / lbs/day
Feb 2022 Week 1 0.24 / mg/L 0.058106 / lbs/day
Feb 2022 Average 0.24 / mg/L 0.058106 / lbs/day
2022 Quarter 1 0.24 / mg/L 0.058106 / lbs/day
2022 1 st 6 Months(Avg) 0.24 / mg/L 0.058106 / lbs/day
2022 lst6...(Max) 0.24 / mg/L 0.058106 / lbs/day
2022 lst6...(Min) 0.24 / mg/L 0.058106 / lbs/day
2022 lst6...(Count) 1 / 1 /
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 002
Sample Date SampleID Result/Limit Mass/Limit
Acetone
02/02/2022 S UTP2020222Self 0.135 / 20.7 mg/L /
03/11/2022 P UTP2031122POTW 0.215 / 20.7 mg/L /
Feb 2022 Week 1 0.135 / mg/L /
Mar 2022 Week 2 0.215 / mg/L /
Feb 2022 Average 0.135 / 8.2 mg/L /
Mar 2022 Average 0.215 / 8.2 mg/L /
2022 Quarter 1 0.175 / mg/L /
2022 1 st 6 Months(Avg) 0.175 / mg/L /
2022 lst6...(Max) 0.215 / mg/L /
2022 lst6...(Min) 0.135 / mg/L /
2022 1st6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
Tuesday,February 21,2023 10:26:41PM *Indicates Violation **Indicates TRC Violation Page 8 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 002
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
02/02/2022 S UTP2020222Self < 0.05 / 20.7 mg/L < /
03/11/2022 P UTP2031122POTW < 0.01 / 20.7 mg/L < /
Feb 2022 Week 1 < 0.05 / mg/L < /
Mar 2022 Week 2 < 0.01 / mg/L < /
Feb 2022 Average < 0.05 / 8.2 mg/L < /
Mar 2022 Average < 0.01 / 8.2 mg/L < /
2022 Quarter 1 < 0.03 / mg/L < /
2022 1 st 6 Months(Avg) < 0.03 / mg/L < /
2022 lst6...(Max) < 0.05 / mg/L < /
2022 lst6...(Min) < 0.01 / mg/L < /
2022 1st 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
02/02/2022 S UTP2020222Self < 0.05 / 20.7 mg/L < /
03/11/2022 P UTP2031122POTW < 0.01 / 20.7 mg/L < /
Feb 2022 Week 1 < 0.05 / mg/L < /
Mar 2022 Week 2 < 0.01 / mg/L < /
Feb 2022 Average < 0.05 / 8.2 mg/L < /
Mar 2022 Average < 0.01 / 8.2 mg/L < /
2022 Quarter 1 < 0.03 / mg/L < /
2022 1 st 6 Months(Avg) < 0.03 / mg/L < /
2022 1st6...(Max) < 0.05 / mg/L < /
2022 lst6...(Min) < 0.01 / mg/L < /
2022 lst6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Methyl Chloride
02/02/2022 S UTP2020222Self < 0.001 / mg/L < /
Feb 2022 Week 1 < 0.001 / mg/L < /
Feb 2022 Average < 0.001 / mg/L < /
2022 Quarter 1 < 0.001 / mg/L < /
2022 1 st 6 Months(Avg) < 0.001 / mg/L < /
2022 lst6...(Max) < 0.001 / mg/L < /
2022 lst6...(Min) < 0.001 / mg/L < /
2022 1st6...(Count) 1
Tuesday,February 21,2023 10:26:41PM *Indicates Violation **Indicates TRC Violation Page 1 of 2

United Therapeutics Corporation
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 002
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
03/11/2022 P UTP2031122POTW < 0.01 / 3.0 mg/L < /
Mar 2022 Week 2 < 0.01 / mg/L < /
Mar 2022 Average < 0.01 / 0.7 mg/L < /
2022 Quarter 1 < 0.01 / mg/L < /
2022 1 st 6 Months(Avg) < 0.01 / mg/L < /
2022 lst6...(Max) < 0.01 / mg/L < /
2022 lst6...(Min) < 0.01 / mg/L < /
2022 lst6...(Count) 1
Sample Date SampleID Result/Limit Mass/Limit
n-Amyl acetate
02/02/2022 S UTP2020222Self < 0.025 / 20.7 mg/L < /
03/11/2022 P UTP2031122POTW < 0.01 / 20.7 mg/L < /
Feb 2022 Week 1 < 0.025 / mg/L < /
Mar 2022 Week 2 < 0.01 / mg/L < /
Feb 2022 Average < 0.025 / 8.2 mg/L < /
Mar 2022 Average < 0.01 / 8.2 mg/L < /
2022 Quarter 1 < 0.018 / mg/L < /
2022 1 st 6 Months(Avg) < 0.018 / mg/L < /
2022 lst6...(Max) < 0.025 / mg/L < /
2022 lst6...(Min) < 0.01 / mg/L < /
2022 lst6...(Count) 2
Tuesday,February 21,2023 10:26:41PM *Indicates Violation **Indicates TRC Violation Page 2 of 2

Wolfspeed Durham
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Aluminum
03/13/2022 S CreeP8031322Self 0.38 / mg/L /
04/25/2022 S CreeP8042522Self 0.36 / mg/L /
Mar 2022 Week 2 0.38 / mg/L /
Apr 2022 Week 4 0.36 / mg/L /
Mar 2022 Average 0.38 / mg/L /
Apr 2022 Average 0.36 / mg/L /
2022 Quarter 1 0.38 / mg/L /
2022 Quarter 2 0.36 / mg/L /
2022 1 st 6 Months(Avg) 0.37 / mg/L /
2022 lst6...(Max) 0.38 / mg/L /
2022 lst6...(Min) 0.36 / mg/L /
2022 lst6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
01/25/2022 P CreeP8012522POT 20.2 / mg/L /
W
03/13/2022 S CreeP8031322Self 19.3 / mg/L /
04/25/2022 S CreeP8042522Self 21.8 / mg/L /
06/21/2022 S CreeP8062122Self 23.8 / mg/L /
Jan 2022 Week 4 20.2 / mg/L /
Mar 2022 Week 2 19.3 / mg/L /
Apr 2022 Week 4 21.8 / mg/L /
Jun 2022 Week 3 23.8 / mg/L /
Jan 2022 Average 20.2 / mg/L /
Mar 2022 Average 19.3 / mg/L /
Apt-2022 Average 21.8 / mg/L /
Jun 2022 Average 23.8 / mg/L /
2022 Quarter 1 19.75 / mg/L /
2022 Quarter 2 22.8 / mg/L /
2022 1 st 6 Months(Avg) 21.28 / mg/L /
2022 lst6...(Max) 23.8 / mg/L /
2022 lst6...(Min) 19.3 / mg/L /
2022 lst6...(Count) 4
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Tuesday,February 21,2023 10:29:34PM *Indicates Violation **Indicates TRC Violation Page 1 of 11

Wolfspeed Durham
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2022 S CreeP80122F1ow 0.350807 / MGD /
02/28/2022 S CreeP80222F1ow 0.387606 / MGD /
03/31/2022 S CreeP80322Flow 0.395291 / MGD /
04/30/2022 S CreeP80422F1ow 0.392799 / MGD /
05/31/2022 S CreeP80522F1ow 0.394134 / MGD /
06/30/2022 S CreeP80622F1ow 0.397642 / MGD /
Jan 2022 Week 4 0.350807 / MGD /
Feb 2022 Week 4 0.387606 / MGD /
Mar 2022 Week 4 0.395291 / MGD /
Apr 2022 Week 4 0.392799 / MGD /
May 2022 Week 4 0.394134 / MGD /
Jun 2022 Week 4 0.397642 / MGD /
Jan 2022 Average 0.350807 / MGD /
Feb 2022 Average 0.387606 / MGD /
Mar 2022 Average 0.395291 / MGD /
Apr 2022 Average 0.392799 / MGD /
May 2022 Average 0.394134 / MGD /
Jun 2022 Average 0.397642 / MGD /
2022 Quarter 1 0.377901 / MGD /
2022 Quarter 2 0.394858 / MGD /
2022 1st 6 Months(Avg) 0.38638 / MGD /
2022 lst6...(Max) 0.397642 / MGD /
2022 lst6...(Min) 0.350807 / MGD /
2022 1st6...(Count) 6 / /
Sample Date SampleLD ResultlLimit Mass/Limit
Barium
03/13/2022 S CreeP8031322Self 0.022 / mg/L /
Mar 2022 Week 2 0.022 / mg/L /
Mar 2022 Average 0.022 / mg/L /
2022 Quarter 1 0.022 / mg/L /
2022 1 st 6 Months(Avg) 0.022 / mg/L /
2022 1st 6...(Max) 0.022 / mg/L /
2022 lst6...(Min) 0.022 / mg/L /
2022 lst6...(Count) 1
Tuesday,February 21,2023 10:29:34PM *Indicates Violation **Indicates TRC Violation Page 2 of 11

Wolfspeed Durham
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
03/13/2022 S CreeP8031322Self < 0.0005 / mg/L < /
Mar 2022 Week 2 < 0.0005 / mg/L < /
Mar 2022 Average < 0.0005 / mg/L < /
2022 Quarter 1 < 0.0005 / mg/L < /
2022 1 st 6 Months(Avg) < 0.0005 / mg/L < /
2022 lst6...(Max) < 0.0005 / mg/L < /
2022 lst6...(Min) < 0.0005 / mg/L < /
2022 lst6...(Count) 1
Sample Date SampleID Result/Limit Mass/Limit
Chloride
01/25/2022 P CreeP8012522POT 142 / mg/L /
W
03/13/2022 S CreeP8031322Self 133 / mg/L /
04/25/2022 S CreeP8042522Self 129 / mg/L /
06/21/2022 S CreeP8062122Self 170 / mg/L /
Jan 2022 Week 4 142 / mg/L /
Mar 2022 Week 2 133 / mg/L /
Apr 2022 Week 4 129 / mg/L /
Jun 2022 Week 3 170 / mg/L /
Jan 2022 Average 142 / mg/L /
Mar 2022 Average 133 / mg/L /
Apr 2022 Average 129 / mg/L /
Jun 2022 Average 170 / mg/L /
2022 Quarter 1 137.5 / mg/L /
2022 Quarter 2 149.5 / mg/L /
2022 1 st 6 Months(Avg) 143.5 / mg/L /
2022 lst6...(Max) 170 / mg/L /
2022 lst6...(Min) 129 / mg/L /
2022 1st 6...(Count) 4
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
03/13/2022 S CreeP8031322Self < 0.003 / mg/L < /
Mar 2022 Week 2 < 0.003 / mg/L < /
Mar 2022 Average < 0.003 / mg/L < /
2022 Quarter 1 < 0.003 / mg/L < /
Tuesday,February 21,2023 10:29:34PM *Indicates Violation **Indicates TRC Violation Page 3 of 11

Wolfspeed Durham
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
2022 1 st 6 Months(Avg) < 0.003 / mg/L < /
2022 lst6...(Max) < 0.003 / mg/L < /
2022 lst6...(Min) < 0.003 / mg/L < /
2022 lst6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
03/13/2022 S CreeP8031322Self 0.038 / mg/L /
04/25/2022 S CreeP8042522Self 0.36 / mg/L /
Mar 2022 Week 2 0.038 / mg/L /
Apr 2022 Week 4 0.36 / mg/L /
Mar 2022 Average 0.038 / mg/L /
Apr 2022 Average 0.36 / mg/L /
2022 Quarter 1 0.038 / mg/L /
2022 Quarter 2 0.36 / mg/L /
2022 1 st 6 Months(Avg) 0.199 / mg/L /
2022 lst6...(Max) 0.36 / mg/L /
2022 lst6...(Min) 0.038 / mg/L /
2022 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Lintit Mass/Limit
Cyanide
01/25/2022 P CreeP8012522POT < 0.003 / mg/L < /
W
03/13/2022 S CreeP8031322Self < 0.004 / mg/L < /
Jan 2022 Week 4 < 0.003 / mg/L < /
Mar 2022 Week 2 < 0.004 / mg/L < /
Jan 2022 Average < 0.003 / mg/L < /
Mar 2022 Average < 0.004 / mg/L < /
2022 Quarter 1 < 0.003 / mg/L < /
2022 1 st 6 Months(Avg) < 0.003 / mg/L < /
2022 lst6...(Max) < 0.004 / mg/L < /
2022 1st 6...(Min) < 0.003 / mg/L < /
2022 1st 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
Tuesday,February 21,2023 10:29:34PM *Indicates Violation **Indicates TRC Violation Page 4 of 11

Wolfspeed Durham
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
01/25/2022 P CreeP8012522POT 2.09 / mg/L /
W
03/13/2022 S CreeP8031322Self 2.3 / mg/L /
Jan 2022 Week 4 2.09 / mg/L /
Mar 2022 Week 2 2.3 / mg/L /
Jan 2022 Average 2.09 / mg/L /
Mar 2022 Average 2.3 / mg/L /
2022 Quarter 1 2.2 / mg/L /
2022 1 st 6 Months(Avg) 2.20 / mg/L /
2022 lst6...(Max) 2.3 / mg/L /
2022 lst6...(Min) 2.09 / mg/L /
2022 1st 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Lead
03/13/2022 S CreeP8031322Self < 0.0025 / mg/L < /
Mar 2022 Week 2 < 0.0025 / mg/L < /
Mar 2022 Average < 0.0025 / mg/L < /
2022 Quarter 1 < 0.0025 / mg/L < /
2022 1 st 6 Months(Avg) < 0.0025 / mg/L < /
2022 lst6...(Max) < 0.0025 / mg/L < /
2022 lst6...(Min) < 0.0025 / mg/L < /
2022 lst6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
01/25/2022 P CreeP8012522POT 0.000008 / mg/L /
WHg
03/13/2022 S CreeP8031322Self 0.000025 / mg/L /
04/25/2022 S CreeP8042522Self 0.000003 / mg/L /
05/11/2022 P CreeP8051122POT 0.000006 / mg/L /
WHg
Jan 2022 Week 4 0.000008 / mg/L /
Mar 2022 Week 2 0.000025 / mg/L /
Apr 2022 Week 4 0.000003 / mg/L /
May 2022 Week 2 0.000006 / mg/L /
Jan 2022 Average 0.000008 / mg/L /
Mar 2022 Average 0.000025 / mg/L /
Tuesday,February 21,2023 10:29:34PM *Indicates Violation **Indicates TRC Violation Page 5 of 11

Wolfspeed Durham
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SampleID Result/Limit Mass/Limit
Mercury-LL
Apr 2022 Average 0.000003 / mg/L /
May 2022 Average 0.000006 / mg/L /
2022 Quarter 1 0.000016 / mg/L /
2022 Quarter 2 0.000005 / mg/L /
2022 1 st 6 Months(Avg) 0.000010 / mg/L /
2022 lst 6...(Max) 0.000025 / mg/L /
2022 lst6...(Min) 0.000003 / mg/L /
2022 lst6...(Count) 4 / /
Sample Date SampleID Result/Limit Mass/Limit
Molybdenum
03/13/2022 S CreeP8031322Self 0.3 / mg/L /
Mar 2022 Week 2 0.3 / mg/L /
Mar 2022 Average 0.3 / mg/L /
2022 Quarter 1 0.3 / mg/L /
2022 1 st 6 Months(Avg) 0.3 / mg/L /
2022 lst6...(Max) 0.3 / mg/L /
2022 lst6...(Min) 0.3 / mg/L /
2022 1st 6...(Count) 1
Sample Date SampleID Result/Limit Mass/Limit
Nickel
03/13/2022 S CreeP8031322Self < 0.0025 / mg/L < /
Mar 2022 Week 2 < 0.0025 / mg/L < /
Mar 2022 Average < 0.0025 / mg/L < /
2022 Quarter 1 < 0.0025 / mg/L < /
2022 1 st 6 Months(Avg) < 0.0025 / mg/L < /
2022 lst6...(Max) < 0.0025 / mg/L < /
2022 lst6...(Min) < 0.0025 / mg/L < /
2022 lst6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
01/25/2022 P CreeP8012522POT 2.8 / mg/L /
W
Jan 2022 Week 4 2.8 / mg/L /
Jan 2022 Average 2.8 / mg/L /
Tuesday,February 21,2023 10:29:34PM *Indicates Violation **Indicates TRC Violation Page 6 of 11

Wolfspeed Durham
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
2022 Quarter 1 2.8 / mg/L /
2022 1 st 6 Months(Avg) 2.8 / mg/L /
2022 lst6...(Max) 2.8 / mg/L /
2022 lst6...(Min) 2.8 / mg/L /
2022 lst6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
01/25/2022 P CreeP8012522POT 31.2 / mg/L /
W
03/13/2022 S CreeP8031322Self 30 / mg/L /
04/25/2022 S CreeP8042522Self 28.5 / mg/L /
06/21/2022 S CreeP8062122Self 35.96 / mg/L /
Jan 2022 Week 4 31.2 / mg/L /
Mar 2022 Week 2 30 / mg/L /
Apr 2022 Week 4 28.5 / mg/L /
Jun 2022 Week 3 35.96 / mg/L /
Jan 2022 Average 31.2 / mg/L /
Mar 2022 Average 30 / mg/L /
Apr 2022 Average 28.5 / mg/L /
Jun 2022 Average 35.96 / mg/L /
2022 Quarter 1 30.6 / mg/L /
2022 Quarter 2 32.23 / mg/L /
2022 1 st 6 Months(Avg) 31.42 / mg/L /
2022 lst6...(Max) 35.96 / mg/L /
2022 lst6...(Min) 28.5 / mg/L /
2022 lst6...(Count) 4
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
01/25/2022 P CreeP8012522POT < 2.5 / mg/L < /
W
03/13/2022 S CreeP8031322Self < 2.5 / mg/L < /
Jan 2022 Week 4 < 2.5 / mg/L < /
Mar 2022 Week 2 < 2.5 / mg/L < /
Jan 2022 Average < 2.5 / mg/L < /
Mar 2022 Average < 2.5 / mg/L < /
2022 Quarter 1 < 2.5 / mg/L < /
Tuesday,February 21,2023 10:29:34PM *Indicates Violation **Indicates TRC Violation Page 7 of 11

Wolfspeed Durham
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
2022 1 st 6 Months(Avg) < 2.5 / mg/L < /
2022 lst6...(Max) < 2.5 / mg/L < /
2022 lst6...(Min) < 2.5 / mg/L < /
2022 lst6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
pH
01/25/2022 P CreeP8012522POT 9.2 / 5.0-10.5 su /
W
03/13/2022 S CreeP8031322Self 9.4 / 5.0-10.5 su /
Jan 2022 Week 4 9.2 / su /
Mar 2022 Week 2 9.4 / Su /
Jan 2022 Average 9.2 / su /
Mar 2022 Average 9.4 / su /
2022 Quarter 1 9.3 / Su /
2022 1 st 6 Months(Avg) 9.3 / Su /
2022 lst6...(Max) 9.4 / su /
2022 lst6...(Min) 9.2 / su /
2022 1st6...(Count) 2
Sample Date SampleID Result/Limit Mass/Limit
Selenium
03/13/2022 S CreeP8031322Self < 0.005 / mg/L < /
Mar 2022 Week 2 < 0.005 / mg/L < /
Mar 2022 Average < 0.005 / mg/L < /
2022 Quarter 1 < 0.005 / mg/L < /
2022 1 st 6 Months(Avg) < 0.005 / mg/L < /
2022 lst6...(Max) < 0.005 / mg/L < /
2022 lst6...(Min) < 0.005 / mg/L < /
2022 lst6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
Silver
03/13/2022 S CreeP8031322Self < 0.0025 / mg/L < /
Mar 2022 Week 2 < 0.0025 / mg/L < /
Mar 2022 Average < 0.0025 / mg/L < /
2022 Quarter 1 < 0.0025 / mg/L < /
Tuesday,February 21,2023 10:29:34PM *Indicates Violation **Indicates TRC Violation Page 8 of 11

Wolfspeed Durham
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SampleID Result/Limit Mass/Limit
Silver
2022 1 st 6 Months(Avg) < 0.0025 / mg/L < /
2022 lst6...(Max) < 0.0025 / mg/L < /
2022 lst6...(Min) < 0.0025 / mg/L < /
2022 lst6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
01/25/2022 P CreeP8012522POT 20 / 66 °C /
W
03/13/2022 S CreeP8031322Self 22.5 / 66 °C /
Jan 2022 Week 4 20 / °C /
Mar 2022 Week 2 22.5 / °C /
Jan 2022 Average 20 / °C /
Mar 2022 Average 22.5 / °C /
2022 Quarter 1 21.3 / °C /
2022 1 st 6 Months(Avg) 21.3 / °C /
2022 lst6...(Max) 22.5 / °C /
2022 lst6...(Min) 20 / °C /
2022 1st6...(Count) 2
Sample Date SampleID Result/Limit Mass/Limit
TKN
01/25/2022 P CreeP8012522POT 28.4 / mg/L /
W
03/13/2022 S CreeP8031322Self 24.4 / mg/L /
Jan 2022 Week 4 28.4 / mg/L /
Mar 2022 Week 2 24.4 / mg/L /
Jan 2022 Average 28.4 / mg/L /
Mar 2022 Average 24.4 / mg/L /
2022 Quarter 1 26.4 / mg/L /
2022 1 st 6 Months(Avg) 26.4 / mg/L /
2022 lst6...(Max) 28.4 / mg/L /
2022 lst6...(Min) 24.4 / mg/L /
2022 lst6...(Count) 2
Sample Date SampleID Result/Limit Mass/Limit
Total Phosphorus
Tuesday,February 21,2023 10:29:34PM *Indicates Violation **Indicates TRC Violation Page 9 of 11

Wolfspeed Durham
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
01/25/2022 P CreeP8012522POT 1.54 / mg/L /
W
03/13/2022 S CreeP8031322Self 1.7 / mg/L /
04/25/2022 S CreeP8042522Self 1.7 / mg/L /
06/21/2022 S CreeP8062122Self 1.24 / mg/L /
Jan 2022 Week 4 1.54 / mg/L /
Mar 2022 Week 2 1.7 / mg/L /
Apr 2022 Week 4 1.7 / mg/L /
Jun 2022 Week 3 1.24 / mg/L /
Jan 2022 Average 1.54 / mg/L /
Mar 2022 Average 1.7 / mg/L /
Apr 2022 Average 1.7 / mg/L /
Jun 2022 Average 1.24 / mg/L /
2022 Quarter 1 1.62 / mg/L /
2022 Quarter 2 1.47 / mg/L /
2022 1 st 6 Months(Avg) 1.545 / mg/L /
2022 1st 6...(Max) 1.7 / mg/L /
2022 lst6...(Min) 1.24 / mg/L /
2022 lst6...(Count) 4
Sample Date SamplelD Result/Limit Mass/Limit
VOC
03/13/2022 S CreeP8031322Self 0.895 / mg/L /
04/25/2022 S CreeP8042522Self 1.075 / mg/L /
06/21/2022 S CreeP8062122Self 0.65 / mg/L /
Mar 2022 Week 2 0.895 / mg/L /
Apt-2022 Week 4 1.075 / mg/L /
Jun 2022 Week 3 0.65 / mg/L /
Mar 2022 Average 0.895 / mg/L /
Apr 2022 Average 1.075 / mg/L /
Jun 2022 Average 0.65 / mg/L /
2022 Quarter 1 0.895 / mg/L /
2022 Quarter 2 0.8625 / mg/L /
2022 1 st 6 Months(Avg) 0.8733 / mg/L /
2022 lst6...(Max) 1.075 / mg/L /
2022 lst6...(Min) 0.65 / mg/L /
2022 lst6...(Count) 3
Tuesday,February 21,2023 10:29:34PM *Indicates Violation **Indicates TRC Violation Page 10 of 11

Wolfspeed Durham
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
03/13/2022 S CreeP8031322Self 0.5 / mg/L /
Mar 2022 Week 2 0.5 / mg/L /
Mar 2022 Average 0.5 / mg/L /
2022 Quarter 1 0.5 / mg/L /
2022 1 st 6 Months(Avg) 0.5 / mg/L /
2022 lst6...(Max) 0.5 / mg/L /
2022 lst6...(Min) 0.5 / mg/L /
2022 lst6...(Count) 1
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2022 S CreeP90122F1ow 0.047128 / MGD /
02/28/2022 S CreeP90222F1ow 0.045305 / MGD /
03/31/2022 S CreeP90322F1ow 0.053726 / MGD /
04/30/2022 S CreeP90422F1ow 0.064201 / MGD /
05/31/2022 S CreeP90522Flow 0.054131 / MGD /
06/30/2022 S CreeP90622F1ow 0.048657 / MGD /
Jan 2022 Week 4 0.047128 / MGD /
Feb 2022 Week 4 0.045305 / MGD /
Mar 2022 Week 4 0.053726 / MGD /
Apr 2022 Week 4 0.064201 / MGD /
May 2022 Week 4 0.054131 / MGD /
Jun 2022 Week 4 0.048657 / MGD /
Jan 2022 Average 0.047128 / MGD /
Feb 2022 Average 0.045305 / MGD /
Mar 2022 Average 0.053726 / MGD /
Apr 2022 Average 0.064201 / MGD /
May 2022 Average 0.054131 / MGD /
Jun 2022 Average 0.048657 / MGD /
2022 Quarter 1 0.04872 / MGD /
2022 Quarter 2 0.055663 / MGD /
2022 1 st 6 Months(Avg) 0.052191 / MGD /
2022 lst6...(Max) 0.064201 / MGD /
2022 lst6...(Min) 0.045305 / MGD /
Tuesday,February 21,2023 10:29:34PM *Indicates Violation **Indicates TRC Violation Page 11 of 11

Wolfspeed Durham
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
2022 1st 6...(Count) 6
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
03/13/2022 S CreeP9031322Self 15.1 / mg/L /
Mar 2022 Week 2 15.1 / mg/L /
Mar 2022 Average 15.1 / mg/L /
2022 Quarter 1 15.1 / mg/L /
2022 1 st 6 Months(Avg) 15.1 / mg/L /
2022 lst6...(Max) 15.1 / mg/L /
2022 lst6...(Min) 15.1 / mg/L /
2022 lst6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
Copper
03/13/2022 S CreeP9031322Self 0.02 / mg/L /
04/25/2022 S CreeP9042522Self 0.02 / mg/L /
Mar 2022 Week 2 0.02 / mg/L /
Apr 2022 Week 4 0.02 / mg/L /
Mar 2022 Average 0.02 / mg/L /
Apr 2022 Average 0.02 / mg/L /
2022 Quarter 1 0.02 / mg/L /
2022 Quarter 2 0.02 / mg/L /
2022 1 st 6 Months(Avg) 0.02 / mg/L /
2022 lst6...(Max) 0.02 / mg/L /
2022 lst6...(Min) 0.02 / mg/L /
2022 1st 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
01/25/2022 P CreeP9012522POT 0.64 / mg/L /
W
03/13/2022 S CreeP9031322Self 2.2 / mg/L /
Jan 2022 Week 4 0.64 / mg/L /
Mar 2022 Week 2 2.2 / mg/L /
Jan 2022 Average 0.64 / mg/L /
Mar 2022 Average 2.2 / mg/L /
Tuesday,February 21,2023 10:29:34PM *Indicates Violation **Indicates TRC Violation Pagel of 3

Wolfspeed Durham
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
2022 Quarter 1 1.42 / mg/L /
2022 1 st 6 Months(Avg) 1.42 / mg/L /
2022 lst6...(Max) 2.2 / mg/L /
2022 lst6...(Min) 0.64 / mg/L /
2022 lst6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
01/25/2022 P CreeP9012522POT 0.000011 / mg/L /
WHg
03/13/2022 S CreeP9031322Self 0.000022 / mg/L /
04/25/2022 S CreeP9042522Self 0.000003 / mg/L /
05/11/2022 P CreeP9051122POT 0.000005 / mg/L /
WHg
Jan 2022 Week 4 0.000011 / mg/L /
Mar 2022 Week 2 0.000022 / mg/L /
Apr 2022 Week 4 0.000003 / mg/L /
May 2022 Week 2 0.000005 / mg/L /
Jan 2022 Average 0.000011 / mg/L /
Mar 2022 Average 0.000022 / mg/L /
Apr 2022 Average 0.000003 / mg/L /
May 2022 Average 0.000005 / mg/L /
2022 Quarter 1 0.000016 / mg/L /
2022 Quarter 2 0.000004 / mg/L /
2022 1 st 6 Months(Avg) 0.000010 / mg/L /
2022 lst6...(Max) 0.000022 / mg/L /
2022 lst6...(Min) 0.000003 / mg/L /
2022 lst6...(Count) 4
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
01/25/2022 P CreeP9012522POT < 0.001 / mg/L < /
W
Jan 2022 Week 4 < 0.001 / mg/L < /
Jan 2022 Average < 0.001 / mg/L < /
2022 Quarter 1 < 0.001 / mg/L < /
2022 1 st 6 Months(Avg) < 0.001 / mg/L < /
2022 lst6...(Max) < 0.001 / mg/L < /
Tuesday,February 21,2023 10:29:34PM *Indicates Violation **Indicates TRC Violation Page 2 of 3

Wolfspeed Durham
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
2022 1st 6...(Min) < 0.001 / mg/L < /
2022 lst6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
01/25/2022 P CreeP9012522POT < 2.5 / mg/L < /
W
03/13/2022 S CreeP9031322Self 7.1 / mg/L /
Jan 2022 Week 4 < 2.5 / mg/L < /
Mar 2022 Week 2 7.1 / mg/L /
Jan 2022 Average < 2.5 / mg/L < /
Mar 2022 Average 7.1 / mg/L /
2022 Quarter 1 < 4.8 / mg/L < /
2022 1 st 6 Months(Avg) < 4.8 / mg/L < /
2022 lst6...(Max) 7.1 / mg/L /
2022 lst6...(Min) < 2.5 / mg/L < /
2022 lst6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
pH
01/25/2022 P CreeP9012522POT 7.1 / 5.0-10.5 Su /
W
03/13/2022 S CreeP9031322Self 7 / 5.0-10.5 su /
Jan 2022 Week 4 7.1 / su /
Mar 2022 Week 2 7 / su /
Jan 2022 Average 7.1 / Su /
Mar 2022 Average 7 / Su /
2022 Quarter 1 7.1 / Su /
2022 1 st 6 Months(Avg) 7.05 / su /
2022 1st 6...(Max) 7.1 / Su /
2022 lst6...(Min) 7 / Su /
2022 lst6...(Count) 2
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: All
Tuesday,February 21,2023 10:29:34PM *Indicates Violation **Indicates TRC Violation Page 3 of 3

Wolfspeed Durham
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: All
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2022 S Cree0122F1ow 0.398645 / 0.600 MGD /
02/28/2022 S Cree0222F1ow 0.486969 / 0.600 MGD /
03/31/2022 S Cree0322F1ow 0.449017 / 0.600 MGD /
04/30/2022 S Cree0422Flow 0.457 / 0.600 MGD /
05/31/2022 S Cree0522Flow 0.448265 / 0.600 MGD /
06/30/2022 S Cree0622F1ow 0.446157 / 0.600 MGD /
Jan 2022 Week 4 0.398645 / MGD /
Feb 2022 Week 4 0.486969 / MGD /
Mar 2022 Week 4 0.449017 / MGD /
Apr 2022 Week 4 0.457 / MGD /
May 2022 Week 4 0.448265 / MGD /
Jun 2022 Week 4 0.446157 / MGD /
Jan 2022 Average 0.398645 / 0.451 MGD /
Feb 2022 Average 0.486969 / 0.451 MGD * /
Mar 2022 Average 0.449017 / 0.451 MGD /
Apr 2022 Average 0.457 / 0.451 MGD * /
May 2022 Average 0.448265 / 0.451 MGD /
Jun 2022 Average 0.446157 / 0.451 MGD /
2022 Quarter 1 0.444877 / MGD /
2022 Quarter 2 0.450474 / MGD /
2022 1 st 6 Months(Avg) 0.447676 / MGD /
2022 lst6...(Max) 0.486969 / MGD /
2022 lst6...(Min) 0.398645 / MGD /
2022 1st6...(Count) 6 / /
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 013
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2022 S CreePl30l22F1ow 0.00071 / MGD /
02/28/2022 S CreeP130222F1ow 0.00015 / MGD /
03/31/2022 S CreeP130322Flow 0.00297 / MGD /
04/30/2022 S CreeP130422F1ow 0.00376 / MGD /
05/31/2022 S CreeP13053122Self 0.0055 / MGD /
05/31/2022 S CreeP130522F1ow 0.000333 / MGD /
06/30/2022 S CreeP130622F1ow 0.000255 / MGD /
Tuesday,February 21,2023 10:29:34PM *Indicates Violation **Indicates TRC Violation Page 1 of 1

Wolfspeed Durham
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 013
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Jan 2022 Week 4 0.00071 / MGD /
Feb 2022 Week 4 0.00015 / MGD /
Mar 2022 Week 4 0.00297 / MGD /
Apr 2022 Week 4 0.00376 / MGD /
May 2022 Week 4 0.002917 / MGD /
Jun 2022 Week 4 0.000255 / MGD /
Jan 2022 Average 0.00071 / 0.030 MGD /
Feb 2022 Average 0.00015 / 0.030 MGD /
Mar 2022 Average 0.00297 / 0.030 MGD /
Apr 2022 Average 0.00376 / 0.030 MGD /
May 2022 Average 0.002917 / 0.030 MGD /
Jun 2022 Average 0.000255 / 0.030 MGD /
2022 Quarter 1 0.001277 / MGD /
2022 Quarter 2 0.002462 / MGD /
2022 1 st 6 Months(Avg) 0.001954 / MGD /
2022 lst6...(Max) 0.0055 / MGD /
2022 lst6...(Min) 0.00015 / MGD /
2022 lst6...(Count) 7 / /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
03/13/2022 S CreeP13031322Self < 0.0005 / 0.11 mg/L < /
Mar 2022 Week 2 < 0.0005 / mg/L < /
Mar 2022 Average < 0.0005 / 0.07 mg/L < /
2022 Quarter 1 < 0.0005 / mg/L < /
2022 1 st 6 Months(Avg) < 0.0005 / mg/L < /
2022 lst6...(Max) < 0.0005 / mg/L < /
2022 1st 6...(Min) < 0.0005 / mg/L < /
2022 1st 6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
03/13/2022 S CreeP13031322Self < 0.003 / 2.77 mg/L < /
05/11/2022 P CreeP13051122POT 0.005 / 2.77 mg/L /
W
Mar 2022 Week 2 < 0.003 / mg/L < /
May 2022 Week 2 0.005 / mg/L /
Tuesday,February 21,2023 10:29:34PM *Indicates Violation **Indicates TRC Violation Page 1 of 4

Wolfspeed Durham
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 013
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
Mar 2022 Average < 0.003 / 1.71 mg/L < /
May 2022 Average 0.005 / 1.71 mg/L /
2022 Quarter 1 < 0.003 / mg/L < /
2022 Quarter 2 0.005 / mg/L /
2022 1 st 6 Months(Avg) < 0.004 / mg/L < /
2022 lst6...(Max) 0.005 / mg/L /
2022 lst6...(Min) < 0.003 / mg/L < /
2022 lst6...(Count) 2 / /
Sample Date SampleID Result/Limit Mass/Limit
Copper
03/13/2022 S CreeP13031322Self < 0.003 / 3.38 mg/L < /
05/11/2022 P CreeP13051122POT 0.016 / 3.38 mg/L /
W
06/21/2022 S CreeP13062122Self < 0.003 / 3.38 mg/L < /
Mar 2022 Week 2 < 0.003 / mg/L < /
May 2022 Week 2 0.016 / mg/L /
Jun 2022 Week 3 < 0.003 / mg/L < /
Mar 2022 Average < 0.003 / 2.07 mg/L < /
May 2022 Average 0.016 / 2.07 mg/L /
Jun 2022 Average < 0.003 / 2.07 mg/L < /
2022 Quarter 1 < 0.003 / mg/L < /
2022 Quarter 2 < 0.009 / mg/L < /
2022 1 st 6 Months(Avg) < 0.007 / mg/L < /
2022 lst6...(Max) 0.016 / mg/L /
2022 lst6...(Min) < 0.003 / mg/L < /
2022 lst6...(Count) 3 / /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
03/13/2022 S CreeP13031322Self < 0.004 / 1.20 mg/L < /
05/11/2022 P CreeP13051122POT < 0.003 / 1.20 mg/L < /
W
Mar 2022 Week 2 < 0.004 / mg/L < /
May 2022 Week 2 < 0.003 / mg/L < /
Mar 2022 Average < 0.004 / 0.65 mg/L < /
May 2022 Average < 0.003 / 0.65 mg/L < /
2022 Quarter 1 < 0.004 / mg/L < /
Tuesday,February 21,2023 10:29:34PM *Indicates Violation **Indicates TRC Violation Page 2 of 4

Wolfspeed Durham
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 013
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
2022 Quarter 2 < 0.003 / mg/L < /
2022 1 st 6 Months(Avg) < 0.003 / mg/L < /
2022 lst6...(Max) < 0.004 / mg/L < /
2022 lst6...(Min) < 0.003 / mg/L < /
2022 lst6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Lead
03/13/2022 S CreeP13031322Self < 0.0025 / 0.69 mg/L < /
05/11/2022 P CreeP13051122POT < 0.0003 / 0.69 mg/L < /
W
Mar 2022 Week 2 < 0.0025 / mg/L < /
May 2022 Week 2 < 0.0003 / mg/L < /
Mar 2022 Average < 0.0025 / 0.43 mg/L < /
May 2022 Average < 0.0003 / 0.43 mg/L < /
2022 Quarter 1 < 0.0025 / mg/L < /
2022 Quarter 2 < 0.0003 / mg/L < /
2022 1 st 6 Months(Avg) < 0.0014 / mg/L < /
2022 lst6...(Max) < 0.0025 / mg/L < /
2022 1st 6...(Min) < 0.0003 / mg/L < /
2022 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
03/13/2022 S CreeP13031322Self < 0.0025 / 3.98 mg/L < /
05/11/2022 P CreeP13051122POT 5.33 / 3.98 mg/L
W
05/23/2022 S CreeP13052322Self 0.005 / 3.98 mg/L /
05/25/2022 S CreeP13052522Self 0.0168 / 3.98 mg/L /
05/27/2022 S CreeP13052722Self 0.0296 / 3.98 mg/L /
Mar 2022 Week 2 < 0.0025 / mg/L < /
May 2022 Week 2 5.33 / mg/L /
May 2022 Week 4 0.0171 / mg/L /
Mar 2022 Average < 0.0025 / 2.38 mg/L < /
May 2022 Average 1.3454 / 2.38 mg/L /
2022 Quarter 1 < 0.0025 / mg/L < /
2022 Quarter 2 1.3454 / mg/L /
2022 1 st 6 Months(Avg) < 1.0768 / mg/L < /
Tuesday,February 21,2023 10:29:34PM *Indicates Violation **Indicates TRC Violation Page 3 of 4

Wolfspeed Durham
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 013
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
2022 lst6...(Max) 5.33 / mg/L /
2022 lst6...(Min) < 0.0025 / mg/L < /
2022 lst6...(Count) 5 / /
Sample Date SamplelD Result/Limit Mass/Limit
Silver
03/13/2022 S CreeP13031322Self < 0.0025 / 0.43 mg/L < /
05/11/2022 P CreeP13051122POT < 0.0003 / 0.43 mg/L < /
W
Mar 2022 Week 2 < 0.0025 / mg/L < /
May 2022 Week 2 < 0.0003 / mg/L < /
Mar 2022 Average < 0.0025 / 0.24 mg/L < /
May 2022 Average < 0.0003 / 0.24 mg/L < /
2022 Quarter 1 < 0.0025 / mg/L < /
2022 Quarter 2 < 0.0003 / mg/L < /
2022 1 st 6 Months(Avg) < 0.0014 / mg/L < /
2022 lst6...(Max) < 0.0025 / mg/L < /
2022 lst6...(Min) < 0.0003 / mg/L < /
2022 1st6...(Count) 2 / /
Sample Date SampleID Result/Limit Mass/Limit
Zinc
03/13/2022 S CreeP13031322Self < 0.005 / 2.61 mg/L < /
05/11/2022 P CreeP13051122POT 0.1 / 2.61 mg/L /
W
Mar 2022 Week 2 < 0.005 / mg/L < /
May 2022 Week 2 0.1 / mg/L /
Mar 2022 Average < 0.005 / 1.48 mg/L < /
May 2022 Average 0.1 / 1.48 mg/L /
2022 Quarter 1 < 0.005 / mg/L < /
2022 Quarter 2 0.1 / mg/L /
2022 1 st 6 Months(Avg) < 0.053 / mg/L < /
2022 lst6...(Max) 0.1 / mg/L /
2022 lst6...(Min) < 0.005 / mg/L < /
2022 1st 6...(Count) 2
Tuesday,February 21,2023 10:29:34PM *Indicates Violation **Indicates TRC Violation Page 4 of 4

Wolfspeed RTP
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Aluminum
03/16/2022 S CreeRTPP12031622 < 0.05 / mg/L < /
Self
04/25/2022 S CreeRTPP12042522 0.39 / mg/L /
Self
Mar 2022 Week 3 < 0.05 / mg/L < /
Apr 2022 Week 4 0.39 / mg/L /
Mar 2022 Average < 0.05 / mg/L < /
Apr 2022 Average 0.39 / mg/L /
2022 Quarter 1 < 0.05 / mg/L < /
2022 Quarter 2 0.39 / mg/L /
2022 1 st 6 Months(Avg) < 0.22 / mg/L < /
2022 lst6...(Max) 0.39 / mg/L /
2022 lst6...(Min) < 0.05 / mg/L < /
2022 1st 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
02/22/2022 P CreeRTPP12022222 0.5 / mg/L /
POTW
03/16/2022 S CreeRTPP12031622 3.4 / mg/L /
Self
Feb 2022 Week 4 0.5 / mg/L /
Mar 2022 Week 3 3.4 / mg/L /
Feb 2022 Average 0.5 / mg/L /
Mar 2022 Average 3.4 / mg/L /
2022 Quarter 1 1.95 / mg/L /
2022 1 st 6 Months(Avg) 1.95 / mg/L /
2022 lst6...(Max) 3.4 / mg/L /
2022 lst6...(Min) 0.5 / mg/L /
2022 1st 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Arsenic
03/16/2022 S CreeRTPP12031622 < 0.005 / mg/L < /
Self
Mar 2022 Week 3 < 0.005 / mg/L < /
Mar 2022 Average < 0.005 / mg/L < /
2022 Quarter 1 < 0.005 / mg/L < /
2022 1 st 6 Months(Avg) < 0.005 / mg/L < /
Tuesday,February 21,2023 10:46:OOPM *Indicates Violation **Indicates TRC Violation Page 1 of 11

Wolfspeed RTP
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Arsenic
2022 lst6...(Max) < 0.005 / mg/L < /
2022 lst6...(Min) < 0.005 / mg/L < /
2022 lst6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
O1/30/2022 S CreeRTPP120122F10 0.057652 / 0.469 MGD /
w
02/28/2022 S CreeRTPP120222Flo 0.066597 / 0.469 MGD /
w
03/31/2022 S CreeRTPP120322F10 0.066742 / 0.469 MGD /
w
04/30/2022 S CreeRTPP120422F10 0.064639 / 0.469 MGD /
w
05/31/2022 S CreeRTPP120522F10 0.064007 / 0.469 MGD /
w
06/30/2022 S CreeRTPP120622F10 0.054848 / 0.469 MGD /
w
Jan 2022 Week 4 0.057652 / MGD /
Feb 2022 Week 4 0.066597 / MGD /
Mar 2022 Week 4 0.066742 / MGD /
Apr 2022 Week 4 0.064639 / MGD /
May 2022 Week 4 0.064007 / MGD /
Jun 2022 Week 4 0.054848 / MGD /
Jan 2022 Average 0.057652 / 0.329 MGD /
Feb 2022 Average 0.066597 / 0.329 MGD /
Mar 2022 Average 0.066742 / 0.329 MGD /
Apr 2022 Average 0.064639 / 0.329 MGD /
May 2022 Average 0.064007 / 0.329 MGD /
Jun 2022 Average 0.054848 / 0.329 MGD /
2022 Quarter 1 0.063664 / MGD /
2022 Quarter 2 0.061165 / MGD /
2022 1 st 6 Months(Avg) 0.062414 / MGD /
2022 lst6...(Max) 0.066742 / MGD /
2022 lst6...(Min) 0.054848 / MGD /
2022 lst6...(Count) 6 / /
Sample Date SampleID Result/Limit Mass/Limit
Barium
Tuesday,February 21,2023 10:46:OOPM *Indicates Violation **Indicates TRC Violation Page 2 of 11

Wolfspeed RTP
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Barium
03/16/2022 S CreeRTPP12031622 0.033 / mg/L /
Self
Mar 2022 Week 3 0.033 / mg/L /
Mar 2022 Average 0.033 / mg/L /
2022 Quarter 1 0.033 / mg/L /
2022 1 st 6 Months(Avg) 0.033 / mg/L /
2022 1st 6...(Max) 0.033 / mg/L /
2022 1st 6...(Min) 0.033 / mg/L /
2022 lst6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
03/16/2022 S CreeRTPP12031622 < 0.0005 / mg/L < /
Self
Mar 2022 Week 3 < 0.0005 / mg/L < /
Mar 2022 Average < 0.0005 / mg/L < /
2022 Quarter 1 < 0.0005 / mg/L < /
2022 1 st 6 Months(Avg) < 0.0005 / mg/L < /
2022 lst6...(Max) < 0.0005 / mg/L < /
2022 lst6...(Min) < 0.0005 / mg/L < /
2022 lst6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
02/22/2022 P CreeRTPP12022222 128 / mg/L /
POTW
03/16/2022 S CreeRTPP12031622 261 / mg/L /
Self
04/25/2022 S CreeRTPP12042522 136 / mg/L /
Self
06/12/2022 S CreeRTPP12062122 286 / mg/L /
Self
Feb 2022 Week 4 128 / mg/L /
Mar 2022 Week 3 261 / mg/L /
Apr 2022 Week 4 136 / mg/L /
Jun 2022 Week 2 286 / mg/L /
Feb 2022 Average 128 / mg/L /
Mar 2022 Average 261 / mg/L /
Apr 2022 Average 136 / mg/L /
Jun 2022 Average 286 / mg/L /
Tuesday,February 21,2023 10:46:OOPM *Indicates Violation **Indicates TRC Violation Page 3 of 11

Wolfspeed RTP
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
2022 Quarter 1 194.5 / mg/L /
2022 Quarter 2 211 / mg/L /
2022 1 st 6 Months(Avg) 202.75 / mg/L /
2022 lst6...(Max) 286 / mg/L /
2022 lst6...(Min) 128 / mg/L /
2022 lst6...(Count) 4 / /
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
03/16/2022 S CreeRTPP12031622 < 0.003 / mg/L < /
Self
Mar 2022 Week 3 < 0.003 / mg/L < /
Mar 2022 Average < 0.003 / mg/L < /
2022 Quarter 1 < 0.003 / mg/L < /
2022 1 st 6 Months(Avg) < 0.003 / mg/L < /
2022 lst6...(Max) < 0.003 / mg/L < /
2022 lst6...(Min) < 0.003 / mg/L < /
2022 lst6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
Copper
03/16/2022 S CreeRTPP12031622 0.023 / mg/L /
Self
04/25/2022 S CreeRTPP12042522 0.021 / mg/L /
Self
Mar 2022 Week 3 0.023 / mg/L /
Apr 2022 Week 4 0.021 / mg/L /
Mar 2022 Average 0.023 / mg/L /
Apr 2022 Average 0.021 / mg/L /
2022 Quarter 1 0.023 / mg/L /
2022 Quarter 2 0.021 / mg/L /
2022 1 st 6 Months(Avg) 0.022 / mg/L /
2022 lst6...(Max) 0.023 / mg/L /
2022 lst6...(Min) 0.021 / mg/L /
2022 lst6...(Count) 2 / /
Sample Date SampleID Result/Limit Mass/Limit
Cyanide
Tuesday,February 21,2023 10:46:OOPM *Indicates Violation **Indicates TRC Violation Page 4 of 11

Wolfspeed RTP
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
02/22/2022 P CreeRTPP12022222 < 0.003 / mg/L < /
POTW
03/16/2022 S CreeRTPP12031622 < 0.004 / mg/L < /
Self
Feb 2022 Week 4 < 0.003 / mg/L < /
Mar 2022 Week 3 < 0.004 / mg/L < /
Feb 2022 Average < 0.003 / mg/L < /
Mar 2022 Average < 0.004 / mg/L < /
2022 Quarter 1 < 0.003 / mg/L < /
2022 1 st 6 Months(Avg) < 0.003 / mg/L < /
2022 lst6...(Max) < 0.004 / mg/L < /
2022 lst6...(Min) < 0.003 / mg/L < /
2022 lst6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
02/22/2022 P CreeRTPP12022222 3.9 / 8.0 mg/L /
POTW
03/16/2022 S CreeRTPP12031622 3.4 / 8.0 mg/L /
Self
Feb 2022 Week 4 3.9 / mg/L /
Mar 2022 Week 3 3.4 / mg/L /
Feb 2022 Average 3.9 / 7.0 mg/L /
Mar 2022 Average 3.4 / 7.0 mg/L /
2022 Quarter 1 3.65 / mg/L /
2022 1 st 6 Months(Avg) 3.65 / mg/L /
2022 lst6...(Max) 3.9 / mg/L /
2022 lst6...(Min) 3.4 / mg/L /
2022 lst6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Lead
03/16/2022 S CreeRTPP12031622 < 0.0025 / mg/L < /
Self
Mar 2022 Week 3 < 0.0025 / mg/L < /
Mar 2022 Average < 0.0025 / mg/L < /
2022 Quarter 1 < 0.0025 / mg/L < /
2022 1 st 6 Months(Avg) < 0.0025 / mg/L < /
2022 lst6...(Max) < 0.0025 / mg/L < /
Tuesday,February 21,2023 10:46:OOPM *Indicates Violation **Indicates TRC Violation Page 5 of 11

Wolfspeed RTP
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Lead
2022 1st 6...(Min) < 0.0025 / mg/L < /
2022 lst6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
03/16/2022 S CreeRTPP12031622 0.000004 / mg/L /
Self
06/13/2022 S CreeRTPP12061322 0.000005 / mg/L /
POTWHg
Mar 2022 Week 3 0.000004 / mg/L /
Jun 2022 Week 2 0.000005 / mg/L /
Mar 2022 Average 0.000004 / 0.000142 mg/L /
Jun 2022 Average 0.000005 / 0.000142 mg/L /
2022 Quarter 1 0.000004 / mg/L /
2022 Quarter 2 0.000005 / mg/L /
2022 1st 6 Months(Avg) 0.000005 / mg/L /
2022 lst6...(Max) 0.000005 / mg/L /
2022 lst6...(Min) 0.000004 / mg/L /
2022 lst6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
02/22/2022 P CreeRTPP12022222 0.004 / mg/L /
POTW
03/16/2022 S CreeRTPP12031622 < 0.003 / mg/L < /
Self
Feb 2022 Week 4 0.004 / mg/L /
Mar 2022 Week 3 < 0.003 / mg/L < /
Feb 2022 Average 0.004 / mg/L /
Mar 2022 Average < 0.003 / mg/L < /
2022 Quarter 1 < 0.003 / mg/L < /
2022 1 st 6 Months(Avg) < 0.003 / mg/L < /
2022 1st 6...(Max) 0.004 / mg/L /
2022 1st 6...(Min) < 0.003 / mg/L < /
2022 lst6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
Tuesday,February 21,2023 10:46:OOPM *Indicates Violation **Indicates TRC Violation Page 6 of 11

Wolfspeed RTP
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
03/16/2022 S CreeRTPP12031622 < 0.0025 / mg/L < /
Self
Mar 2022 Week 3 < 0.0025 / mg/L < /
Mar 2022 Average < 0.0025 / mg/L < /
2022 Quarter 1 < 0.0025 / mg/L < /
2022 1 st 6 Months(Avg) < 0.0025 / mg/L < /
2022 1st 6...(Max) < 0.0025 / mg/L < /
2022 lst6...(Min) < 0.0025 / mg/L < /
2022 lst6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
02/22/2022 P CreeRTPP12022222 3.9 / mg/L /
POTW
Feb 2022 Week 4 3.9 / mg/L /
Feb 2022 Average 3.9 / mg/L /
2022 Quarter 1 3.9 / mg/L /
2022 1 st 6 Months(Avg) 3.9 / mg/L /
2022 lst6...(Max) 3.9 / mg/L /
2022 lst6...(Min) 3.9 / mg/L /
2022 lst6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
02/22/2022 P CreeRTPP12022222 13 / mg/L /
POTW
03/16/2022 S CreeRTPP12031622 14.2 / mg/L /
Self
Feb 2022 Week 4 13 / mg/L /
Mar 2022 Week 3 14.2 / mg/L /
Feb 2022 Average 13 / mg/L /
Mar 2022 Average 14.2 / mg/L /
2022 Quarter 1 13.6 / mg/L /
2022 1 st 6 Months(Avg) 13.6 / mg/L /
2022 lst6...(Max) 14.2 / mg/L /
2022 lst6...(Min) 13 / mg/L /
2022 lst6...(Count) 2
Tuesday,February 21,2023 10:46:OOPM *Indicates Violation **Indicates TRC Violation Page 7 of 11

Wolfspeed RTP
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
02/22/2022 P CreeRTPP12022222 < 2.5 / 200 mg/L < /
POTW
03/16/2022 S CreeRTPP12031622 < 2.5 / 200 mg/L < /
Self
Feb 2022 Week 4 < 2.5 / mg/L < /
Mar 2022 Week 3 < 2.5 / mg/L < /
Feb 2022 Average < 2.5 / mg/L < /
Mar 2022 Average < 2.5 / mg/L < /
2022 Quarter 1 < 2.5 / mg/L < /
2022 1 st 6 Months(Avg) < 2.5 / mg/L < /
2022 lst6...(Max) < 2.5 / mg/L < /
2022 lst6...(Min) < 2.5 / mg/L < /
2022 lst6...(Count) 2
Sample Date SamplelD Result l Limit Mass/Limit
pH
02/22/2022 P CreeRTPP12022222 7.1 / 5.0-10.5 su /
POTW
03/16/2022 S CreeRTPP12031622 7.6 / 5.0-10.5 su /
Self
Feb 2022 Week 4 7.1 / Su /
Mar 2022 Week 3 7.6 / Su /
Feb 2022 Average 7.1 / su /
Mar 2022 Average 7.6 / su /
2022 Quarter 1 7.35 / su /
2022 1 st 6 Months(Avg) 7.35 / Su /
2022 lst6...(Max) 7.6 / Su /
2022 lst6...(Min) 7.1 / su /
2022 lst6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Selenium
03/16/2022 S CreeRTPP12031622 < 0.005 / mg/L < /
Self
Mar 2022 Week 3 < 0.005 / mg/L < /
Mar 2022 Average < 0.005 / mg/L < /
2022 Quarter 1 < 0.005 / mg/L < /
2022 1 st 6 Months(Avg) < 0.005 / mg/L < /
2022 lst6...(Max) < 0.005 / mg/L < /
Tuesday,February 21,2023 10:46:OOPM *Indicates Violation **Indicates TRC Violation Page 8 of 11

Wolfspeed RTP
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Selenium
2022 1st 6...(Min) < 0.005 / mg/L < /
2022 lst6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
Silver
03/16/2022 S CreeRTPP12031622 < 0.0025 / mg/L < /
Self
Mar 2022 Week 3 < 0.0025 / mg/L < /
Mar 2022 Average < 0.0025 / mg/L < /
2022 Quarter 1 < 0.0025 / mg/L < /
2022 1 st 6 Months(Avg) < 0.0025 / mg/L < /
2022 lst6...(Max) < 0.0025 / mg/L < /
2022 lst6...(Min) < 0.0025 / mg/L < /
2022 lst6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
02/22/2022 P CreeRTPP12022222 17 / 66 °C /
POTW
03/16/2022 S CreeRTPP12031622 20.1 / 66 °C /
Self
Feb 2022 Week 4 17 / °C /
Mar 2022 Week 3 20.1 / °C /
Feb 2022 Average 17 / °C /
Mar 2022 Average 20.1 / °C /
2022 Quarter 1 18.6 / °C /
2022 1 st 6 Months(Avg) 18.6 / °C /
2022 lst6...(Max) 20.1 / °C /
2022 lst6...(Min) 17 / °C /
2022 lst6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
TKN
02/22/2022 P CreeRTPP12022222 9.15 / mg/L /
POTW
Feb 2022 Week 4 9.15 / mg/L /
Feb 2022 Average 9.15 / mg/L /
2022 Quarter 1 9.15 / mg/L /
Tuesday,February 21,2023 10:46:OOPM *Indicates Violation **Indicates TRC Violation Page 9 of 11

Wolfspeed RTP
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
TKN
2022 1 st 6 Months(Avg) 9.15 / mg/L /
2022 lst6...(Max) 9.15 / mg/L /
2022 lst6...(Min) 9.15 / mg/L /
2022 lst6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
02/22/2022 P CreeRTPP12022222 2.02 / mg/L /
POTW
03/16/2022 S CreeRTPP12031622 1.9 / mg/L /
Self
Feb 2022 Week 4 2.02 / mg/L /
Mar 2022 Week 3 1.9 / mg/L /
Feb 2022 Average 2.02 / mg/L /
Mar 2022 Average 1.9 / mg/L /
2022 Quarter 1 1.96 / mg/L /
2022 1 st 6 Months(Avg) 1.96 / mg/L /
2022 lst6...(Max) 2.02 / mg/L /
2022 lst6...(Min) 1.9 / mg/L /
2022 lst6...(Count) 2 / /
Sample Date SampleID Result/Limit Mass/Limit
VOC
03/16/2022 S CreeRTPP12031622 0.59 / mg/L /
Self
04/25/2022 S CreeRTPP12042522 0.042 / mg/L /
Self
06/12/2022 S CreeRTPP12062122 0.046 / mg/L /
Self
Mar 2022 Week 3 0.59 / mg/L /
Apr 2022 Week 4 0.042 / mg/L /
Jun 2022 Week 2 0.046 / mg/L /
Mar 2022 Average 0.59 / mg/L /
Apr 2022 Average 0.042 / mg/L /
Jun 2022 Average 0.046 / mg/L /
2022 Quarter 1 0.59 / mg/L /
2022 Quarter 2 0.044 / mg/L /
2022 1 st 6 Months(Avg) 0.226 / mg/L /
2022 lst6...(Max) 0.59 / mg/L /
Tuesday,February 21,2023 10:46:OOPM *Indicates Violation **Indicates TRC Violation Page 10 of 11

Wolfspeed RTP
SAMPLE OVERVIEW
11112022 To 613012022 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
VOC
2022 1st 6...(Min) 0.042 / mg/L /
2022 lst6...(Count) 3
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
03/16/2022 S CreeRTPP12031622 0.48 / mg/L /
Self
Mar 2022 Week 3 0.48 / mg/L /
Mar 2022 Average 0.48 / mg/L /
2022 Quarter 1 0.48 / mg/L /
2022 1 st 6 Months(Avg) 0.48 / mg/L /
2022 lst6...(Max) 0.48 / mg/L /
2022 lst6...(Min) 0.48 / mg/L /
2022 lst6...(Count) 1
Tuesday,February 21,2023 10:46:OOPM *Indicates Violation **Indicates TRC Violation Page 11 of 11

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Acetone
07/11/2022 P AstraZeneca071122PO 0.451 /20.7 mg/L /
TW
08/29/2022 S AstraZeneca082922Sel < 0.025 /20.7 mg/L < /
f
Jul 2022 Week 2 0.451 / mg/L /
Aug 2022 Week 4 < 0.025 / mg/L < /
Jul 2022 Average 0.451 /8.2 mg/L /
Aug 2022 Average < 0.025 /8.2 mg/L < /
2022 Quarter 3 < 0.238 / mg/L < /
2022 2nd 6 Months(Avg) < 0.238 / mg/L < /
2022 2nd 6...(Max) 0.451 / mg/L /
2022 2nd 6...(Min) < 0.025 / mg/L < /
2022 2nd 6...(Count) 2
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2022 S AstraZeneca0722F1ow 0.000091 / MGD /
08/31/2022 S AstraZeneca0822F1ow 0.000506 / MGD /
09/30/2022 S AstraZeneca0922F1ow 0.002412 / MGD /
10/31/2022 S AstraZeneca1022Flow 0.000097 / MGD /
11/30/2022 S AstraZeneca1122FIow 0.000091 / MGD /
12/31/2022 S AstraZenecal222FIow 0.000026 / MGD /
Jul 2022 Week 4 0.000091 / MGD /
Aug 2022 Week 4 0.000506 / MGD /
Sep 2022 Week 4 0.002412 / MGD /
Oct 2022 Week 4 0.000097 / MGD /
Nov 2022 Week 4 0.000091 / MGD /
Dec 2022 Week 4 0.000026 / MGD /
Jul 2022 Average 0.000091 /0.002 MGD /
Aug 2022 Average 0.000506 /0.002 MGD /
Sep 2022 Average 0.002412 /0.002 MGD * /
Oct 2022 Average 0.000097 /0.002 MGD /
Nov 2022 Average 0.000091 /0.002 MGD /
Dec 2022 Average 0.000026 /0.002 MGD /
2022 Quarter 3 0.001003 / MGD /
Friday,February 17,2023 5:54:27PM *Indicates Violation **Indicates TRC Violation Page 1 of 5

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Average Flow for Month
2022 Quarter 4 0.000071 / MGD /
2022 2nd 6 Months(Avg) 0.000537 / MGD /
2022 2nd 6...(Max) 0.002412 / MGD /
2022 2nd 6...(Min) 0.000026 / MGD /
2022 2nd 6...(Count) 6
■
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 1 16.67 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
COD
07/11/2022 P AstraZeneca071122PO < 7.5 / mg/L < /
TW
08/29/2022 S AstraZeneca082922Se1 < 7.5 / mg/L < /
f
Jul 2022 Week 2 < 7.5 / mg/L < /
Aug 2022 Week 4 < 7.5 / mg/L < /
Jul 2022 Average < 7.5 / mg/L < /
Aug 2022 Average < 7.5 / mg/L < /
2022 Quarter 3 < 7.5 / mg/L < /
2022 2nd 6 Months(Avg) < 7.5 / mg/L < /
2022 2nd 6...(Max) < 7.5 / mg/L < /
2022 2nd 6...(Min) < 7.5 / mg/L < /
2022 2nd 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
07/11/2022 P AstraZeneca071122P0 < 0.005 /20.7 mg/L < /
TW
08/29/2022 S AstraZeneca082922Sel < 0.005 /20.7 mg/L < /
f
Jul 2022 Week 2 < 0.005 / mg/L < /
Aug 2022 Week 4 < 0.005 / mg/L < /
Jul 2022 Average < 0.005 /8.2 mg/L < /
Aug 2022 Average < 0.005 /8.2 mg/L < /
2022 Quarter 3 < 0.005 / mg/L < /
2022 2nd 6 Months(Avg) < 0.005 / mg/L < /
2022 2nd 6...(Max) < 0.005 / mg/L < /
Friday,February 17,2023 5:54:27PM *Indicates Violation **Indicates TRC Violation Page 2 of 5

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Ethyl acetate
2022 2nd 6...(Min) < 0.005 / mg/L < /
2022 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Isopropyl acetate
07/11/2022 P AstraZeneca071122PO < 0.005 /20.7 mg/L < /
TW
08/29/2022 S AstraZeneca082922Sel < 0.005 /20.7 mg/L < /
f
Jul 2022 Week 2 < 0.005 / mg/L < /
Aug 2022 Week 4 < 0.005 / mg/L < /
Jul 2022 Average < 0.005 /8.2 mg/L < /
Aug 2022 Average < 0.005 /8.2 mg/L < /
2022 Quarter 3 < 0.005 / mg/L < /
2022 2nd 6 Months(Avg) < 0.005 / mg/L < /
2022 2nd 6...(Max) < 0.005 / mg/L < /
2022 2nd 6...(Min) < 0.005 / mg/L < /
2022 2nd 6...(Count) 2
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Mercury-LL
10/03/2022 P AstraZenecal00322PO 0.000002 /0.000142 mg/L /
TWHg
Oct 2022 Week 1 0.000002 / mg/L /
Oct 2022 Average 0.000002 / mg/L /
2022 Quarter 4 0.000002 / mg/L /
2022 2nd 6 Months(Avg) 0.000002 / mg/L /
Friday,February 17,2023 5:54:27PM *Indicates Violation **Indicates TRC Violation Page 3 of 5

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Mercury-LL
2022 2nd 6...(Max) 0.000002 / mg/L /
2022 2nd 6...(Min) 0.000002 / mg/L /
2022 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
07/11/2022 P AstraZeneca071122PO < 0.005 /3.0 mg/L < /
TW
08/29/2022 S AstraZeneca082922Sel < 0.005 /3.0 mg/L < /
f
Jul 2022 Week 2 < 0.005 / mg/L < /
Aug 2022 Week 4 < 0.005 / mg/L < /
Jul 2022 Average < 0.005 /0.7 mg/L < /
Aug 2022 Average < 0.005 /0.7 mg/L < /
2022 Quarter 3 < 0.005 / mg/L < /
2022 2nd 6 Months(Avg) < 0.005 / mg/L < /
2022 2nd 6...(Max) < 0.005 / mg/L < /
2022 2nd 6...(Min) < 0.005 / mg/L < /
2022 2nd 6...(Count) 2
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
07/11/2022 P AstraZeneca071122PO < 0.005 /20.7 mg/L < /
TW
08/29/2022 S AstraZeneca082922Se1 < 0.005 /20.7 mg/L < /
IF
Jul 2022 Week 2 < 0.005 /8.2 mg/L < /
Friday,February 17,2023 5:54:27PM *Indicates Violation **Indicates TRC Violation Page 4 of 5

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
n-Amyl acetate
Aug 2022 Week 4 < 0.005 /8.2 mg/L < /
Jul 2022 Average < 0.005 / mg/L < /
Aug 2022 Average < 0.005 / mg/L < /
2022 Quarter 3 < 0.005 / mg/L < /
2022 2nd 6 Months(Avg) < 0.005 / mg/L < /
2022 2nd 6...(Max) < 0.005 / mg/L < /
2022 2nd 6...(Min) < 0.005 / mg/L < /
2022 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
pH
07/11/2022 P AstraZeneca071122PO 6.9 /6.0-10.0 SU /
TW
08/29/2022 S AstraZeneca082922Sel 7.6 /6.0-10.0 SU /
f
Jul 2022 Week 2 6.9 / SU /
Aug 2022 Week 4 7.6 / SU /
Jul 2022 Average 6.9 / SU /
Aug 2022 Average 7.6 / SU /
2022 Quarter 3 7.25 / SU /
2022 2nd 6 Months(Avg) 7.25 / SU /
2022 2nd 6...(Max) 7.6 / SU /
2022 2nd 6...(Min) 6.9 / SU /
2022 2nd 6...(Count) 2
■
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Friday,February 17,2023 5:54:27PM *Indicates Violation **Indicates TRC Violation Page 5 of 5

Aurobindo USA
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Acetone
12/16/2022 S Aurobindol21622Self 0.109 /5.59 mg/L /
Dec 2022 Week 3 0.109 / mg/L /
Dec 2022 Average 0.109 /2.21 mg/L /
2022 Quarter 4 0.109 / mg/L /
2022 2nd 6 Months(Avg) 0.109 / mg/L /
2022 2nd 6...(Max) 0.109 / mg/L /
2022 2nd 6...(Min) 0.109 / mg/L /
2022 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Ammonia
10/27/2022 P Aurobindol02722POT 20.1 / mg/L /
W
12/16/2022 S Aurobindo121622Self 13 / mg/L /
Oct 2022 Week 4 20.1 / mg/L /
Dec 2022 Week 3 13 / mg/L /
Oct 2022 Average 20.1 / mg/L /
Dec 2022 Average 13 / mg/L /
2022 Quarter 4 16.55 / mg/L /
2022 2nd 6 Months(Avg) 16.55 / mg/L /
2022 2nd 6...(Max) 20.1 / mg/L /
2022 2nd 6...(Min) 13 / mg/L /
2022 2nd 6...(Count) 2 / /
Sample Date SampleID Result/Limit Mass/Limit
Average Flow for Month
07/20/2022 S Aurobindo0722F1ow 0.004612 / MGD /
08/17/2022 S Aurobindo0822F1ow 0.00353 / MGD /
09/22/2022 S Aurobindo0922F1ow 0.003175 / MGD /
10/20/2022 S Aurobindol022F1ow 0.002805 / MGD /
11/17/2022 S AurobindoI122F1ow 0.002427 / MGD /
12/21/2022 S Aurobindol222F1ow 0.005404 / MGD /
Jul 2022 Week 3 0.004612 / MGD /
Aug 2022 Week 3 0.00353 / MGD /
Friday,February 17,2023 5:55:24PM *Indicates Violation **Indicates TRC Violation Page 1 of 11

Aurobindo USA
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
Average Flow for Month
Sep 2022 Week 4 0.003175 / MGD /
Oct 2022 Week 3 0.002805 / MGD /
Nov 2022 Week 3 0.002427 / MGD /
Dec 2022 Week 3 0.005404 / MGD /
Jul 2022 Average 0.004612 /0.039 MGD /
Aug 2022 Average 0.00353 /0.039 MGD /
Sep 2022 Average 0.003175 /0.039 MGD /
Oct 2022 Average 0.002805 /0.039 MGD /
Nov 2022 Average 0.002427 /0.039 MGD /
Dec 2022 Average 0.005404 /0.039 MGD /
2022 Quarter 3 0.003772 / MGD /
2022 Quarter 4 0.003545 / MGD /
2022 2nd 6 Months(Avg) 0.003659 / MGD /
2022 2nd 6...(Max) 0.005404 / MGD /
2022 2nd 6...(Min) 0.002427 / MGD /
2022 2nd 6...(Count) 6
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
BOD
10/27/2022 P Aurobindol02722POT 218 / mg/L /
W
12/16/2022 S Aurobindo121622Self 40 / mg/L /
Oct 2022 Week 4 218 / mg/L /
Dec 2022 Week 3 40 / mg/L /
Oct 2022 Average 218 / mg/L /
Dec 2022 Average 40 / mg/L /
2022 Quarter 4 129 / mg/L /
2022 2nd 6 Months(Avg) 129 / mg/L /
2022 2nd 6...(Max) 218 / mg/L /
2022 2nd 6...(Min) 40 / mg/L /
2022 2nd 6...(Count) 2
Sample Date SampleID Result/Limit Mass/Limit
Cadmium
Friday,February 17,2023 5:55:24PM *Indicates Violation **Indicates TRC Violation Page 2 of 11

Aurobindo USA
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Cadmium
10/27/2022 P Aurobindol02722POT < 0.00008 / mg/L < /
W
12/16/2022 S Aurobindol21622Self < 0.00008 / mg/L < /
Oct 2022 Week 4 < 0.00008 / mg/L < /
Dec 2022 Week 3 < 0.00008 / mg/L < /
Oct 2022 Average < 0.00008 / mg/L < /
Dec 2022 Average < 0.00008 / mg/L < /
2022 Quarter 4 < 0.00008 / mg/L < /
2022 2nd 6 Months(Avg) < 0.00008 / mg/L < /
2022 2nd 6...(Max) < 0.00008 / mg/L < /
2022 2nd 6...(Min) < 0.00008 / mg/L < /
2022 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
10/27/2022 P Aurobindo102722POT 40.5 / mg/L /
W
12/16/2022 S Aurobindol21622Self 204 / mg/L /
Oct 2022 Week 4 40.5 / mg/L /
Dec 2022 Week 3 204 / mg/L /
Oct 2022 Average 40.5 / mg/L /
Dec 2022 Average 204 / mg/L /
2022 Quarter 4 122.25 / mg/L /
2022 2nd 6 Months(Avg) 122.25 / mg/L /
2022 2nd 6...(Max) 204 / mg/L /
2022 2nd 6...(Min) 40.5 / mg/L /
2022 2nd 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
COD
10/27/2022 P Aurobindol02722POT 303 / mg/L /
W
12/16/2022 S Aurobindol21622Self 157 / mg/L /
Oct 2022 Week 4 303 / mg/L /
Dec 2022 Week 3 157 / mg/L /
Oct 2022 Average 303 / mg/L /
Dec 2022 Average 157 / mg/L /
2022 Quarter 4 230 / mg/L /
2022 2nd 6 Months(Avg) 230 / mg/L /
2022 2nd 6...(Max) 303 / mg/L /
2022 2nd 6...(Min) 157 / mg/L /
2022 2nd 6...(Count) 2
Friday,February 17,2023 5:55:24PM *Indicates Violation **Indicates TRC Violation Page 3 of 11

Aurobindo USA
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Copper
10/27/2022 P Aurobindol02722POT 0.048 / mg/L /
W
12/16/2022 S Aurobindol21622Self 0.12 / mg/L /
Oct 2022 Week 4 0.048 / mg/L /
Dec 2022 Week 3 0.12 / mg/L /
Oct 2022 Average 0.048 / mg/L /
Dec 2022 Average 0.12 / mg/L /
2022 Quarter 4 0.084 / mg/L /
2022 2nd 6 Months(Avg) 0.084 / mg/L /
2022 2nd 6...(Max) 0.12 / mg/L /
2022 2nd 6...(Min) 0.048 / mg/L /
2022 2nd 6...(Count) 2 / /
Sample Date SampleID Result/Limit Mass/Limit
Cyanide
10/27/2022 P Aurobindo102722POT < 0.003 / mg/L < /
W
12/16/2022 S Aurobindo121622Self < 0.003 / mg/L < /
Oct 2022 Week 4 < 0.003 / mg/L < /
Dec 2022 Week 3 < 0.003 / mg/L < /
Oct 2022 Average < 0.003 / mg/L < /
Dec 2022 Average < 0.003 / mg/L < /
2022 Quarter 4 < 0.003 / mg/L < /
2022 2nd 6 Months(Avg) < 0.003 / mg/L < /
2022 2nd 6...(Max) < 0.003 / mg/L < /
2022 2nd 6...(Min) < 0.003 / mg/L < /
2022 2nd 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
12/16/2022 S Aurobindol21622Self < 0.005 /5.59 mg/L < /
Dec 2022 Week 3 < 0.005 / mg/L < /
Dec 2022 Average < 0.005 /2.21 mg/L < /
2022 Quarter 4 < 0.005 / mg/L < /
2022 2nd 6 Months(Avg) < 0.005 / mg/L < /
2022 2nd 6...(Max) < 0.005 / mg/L < /
2022 2nd 6...(Min) < 0.005 / mg/L < /
2022 2nd 6...(Count) 1 / /
Friday,February 17,2023 5:55:24PM *Indicates Violation **Indicates TRC Violation Page 4 of 11

Aurobindo USA
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
10/27/2022 P Aurobindo102722POT 0.64 / mg/L /
W
12/16/2022 S Aurobindol21622Self 0.57 / mg/L /
Oct 2022 Week 4 0.64 / mg/L /
Dec 2022 Week 3 0.57 / mg/L /
Oct 2022 Average 0.64 / mg/L /
Dec 2022 Average 0.57 / mg/L /
2022 Quarter 4 0.61 / mg/L /
2022 2nd 6 Months(Avg) 0.61 / mg/L /
2022 2nd 6...(Max) 0.64 / mg/L /
2022 2nd 6...(Min) 0.57 / mg/L /
2022 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
12/16/2022 S Aurobindol21622Self < 0.005 /5.59 mg/L < /
Dec 2022 Week 3 < 0.005 / mg/L < /
Dec 2022 Average < 0.005 /2.21 mg/L < /
2022 Quarter 4 < 0.005 / mg/L < /
2022 2nd 6 Months(Avg) < 0.005 / mg/L < /
2022 2nd 6...(Max) < 0.005 / mg/L < /
2022 2nd 6...(Min) < 0.005 / mg/L < /
2022 2nd 6...(Count) 1
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
Friday,February 17,2023 5:55:24PM *Indicates Violation **Indicates TRC Violation Page 5 of 11

Aurobindo USA
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Mercury-LL
10/27/2022 P Aurobindol02722POT 0.00004 /0.000142 mg/L /
W
12/16/2022 S Aurobindol21622Self 0.000028 /0.000142 mg/L /
Oct 2022 Week 4 0.00004 / mg/L /
Dec 2022 Week 3 0.000028 / mg/L /
Oct 2022 Average 0.00004 / mg/L /
Dec 2022 Average 0.000028 / mg/L /
2022 Quarter 4 0.000034 / mg/L /
2022 2nd 6 Months(Avg) 0.000034 / mg/L /
2022 2nd 6...(Max) 0.00004 / mg/L /
2022 2nd 6...(Min) 0.000028 / mg/L /
2022 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
12/16/2022 S Aurobindo121622Self < 0.005 /0.81 mg/L < /
Dec 2022 Week 3 < 0.005 / mg/L < /
Dec 2022 Average < 0.005 /0.18 mg/L < /
2022 Quarter 4 < 0.005 / mg/L < /
2022 2nd 6 Months(Avg) < 0.005 / mg/L < /
2022 2nd 6...(Max) < 0.005 / mg/L < /
2022 2nd 6...(Min) < 0.005 / mg/L < /
2022 2nd 6...(Count) 1
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
Friday,February 17,2023 5:55:24PM *Indicates Violation **Indicates TRC Violation Page 6 of 11

Aurobindo USA
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Molybdenum
10/27/2022 P Aurobindol02722POT < 0.001 / mg/L < /
W
12/16/2022 S Aurobindol21622Self < 0.001 / mg/L < /
Oct 2022 Week 4 < 0.001 / mg/L < /
Dec 2022 Week 3 < 0.001 / mg/L < /
Oct 2022 Average < 0.001 / mg/L < /
Dec 2022 Average < 0.001 / mg/L < /
2022 Quarter 4 < 0.001 / mg/L < /
2022 2nd 6 Months(Avg) < 0.001 / mg/L < /
2022 2nd 6...(Max) < 0.001 / mg/L < /
2022 2nd 6...(Min) < 0.001 / mg/L < /
2022 2nd 6...(Count) 2 / /
Sample Date SampleID Result/Limit Mass/Limit
n-Amyl acetate
12/16/2022 S Aurobindo121622Self < 0.005 /5.59 mg/L < /
Dec 2022 Week 3 < 0.005 / mg/L < /
Dec 2022 Average < 0.005 /2.21 mg/L < /
2022 Quarter 4 < 0.005 / mg/L < /
2022 2nd 6 Months(Avg) < 0.005 / mg/L < /
2022 2nd 6...(Max) < 0.005 / mg/L < /
2022 2nd 6...(Min) < 0.005 / mg/L < /
2022 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
10/27/2022 P Aurobindol02722POT 0.5 / mg/L /
W
12/16/2022 S Aurobindol21622Self 1.5 / mg/L /
Oct 2022 Week 4 0.5 / mg/L /
Dec 2022 Week 3 1.5 / mg/L /
Oct 2022 Average 0.5 / mg/L /
Dec 2022 Average 1.5 / mg/L /
2022 Quarter 4 1 / mg/L /
Friday,February 17,2023 5:55:24PM *Indicates Violation **Indicates TRC Violation Page 7 of 11

Aurobindo USA
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
Nitrate-Nitrite
2022 2nd 6 Months(Avg) 1.0 / mg/L /
2022 2nd 6...(Max) 1.5 / mg/L /
2022 2nd 6...(Min) 0.5 / mg/L /
2022 2nd 6...(Count) 2 / /
Sample Date SampleID Result/Limit Mass/Limit
Nitrogen,Total
10/27/2022 P Aurobindol02722POT 45.5 / mg/L /
W
12/16/2022 S Aurobindo121622Self 27.3 / mg/L /
Oct 2022 Week 4 45.5 / mg/L /
Dec 2022 Week 3 27.3 / mg/L /
Oct 2022 Average 45.5 / mg/L /
Dec 2022 Average 27.3 / mg/L /
2022 Quarter 4 36.4 / mg/L /
2022 2nd 6 Months(Avg) 36.4 / mg/L /
2022 2nd 6...(Max) 45.5 / mg/L /
2022 2nd 6...(Min) 27.3 / mg/L /
2022 2nd 6...(Count) 2 / /
Sample Date SampleID Result/Limit Mass/Limit
Oil&Grease,Total
10/27/2022 P Aurobindo102722POT < 2.5 /200 mg/L < /
W
12/16/2022 S Aurobindol21622Self < 2.5 /200 mg/L < /
Oct 2022 Week 4 < 2.5 / mg/L < /
Dec 2022 Week 3 < 2.5 / mg/L < /
Oct 2022 Average < 2.5 / mg/L < /
Dec 2022 Average < 2.5 / mg/L < /
2022 Quarter 4 < 2.5 / mg/L < /
2022 2nd 6 Months(Avg) < 2.5 / mg/L < /
2022 2nd 6...(Max) < 2.5 / mg/L < /
2022 2nd 6...(Min) < 2.5 / mg/L < /
2022 2nd 6...(Count) 2
■
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Friday,February 17,2023 5:55:24PM *Indicates Violation **Indicates TRC Violation Page 8 of 11

Aurobindo USA
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
pH
10/27/2022 P Aurobindo102722POT 8.5 /6.0-10.0 SU /
W
12/16/2022 S Aurobindol21622Self 7.3 /6.0-10.0 SU /
Oct 2022 Week 4 8.5 / SU /
Dec 2022 Week 3 7.3 / SU /
Oct 2022 Average 8.5 / SU /
Dec 2022 Average 7.3 / SU /
2022 Quarter 4 7.9 / SU /
2022 2nd 6 Months(Avg) 7.9 / SU /
2022 2nd 6...(Max) 8.5 / SU /
2022 2nd 6...(Min) 7.3 / SU /
2022 2nd 6...(Count) 2
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
10/27/2022 P Aurobindo102722POT 19 /66 °C /
W
12/16/2022 S Aurobindol21622Self 13 /66 °C /
Oct 2022 Week 4 19 / °C /
Dec 2022 Week 3 13 / °C /
Oct 2022 Average 19 / °C /
Dec 2022 Average 13 / °C /
2022 Quarter 4 16 / °C /
2022 2nd 6 Months(Avg) 16 / °C /
2022 2nd 6...(Max) 19 / °C /
2022 2nd 6...(Min) 13 / °C /
2022 2nd 6...(Count) 2
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Friday,February 17,2023 5:55:24PM *Indicates Violation **Indicates TRC Violation Page 9 of 11

Aurobindo USA
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
TKN
10/27/2022 P Aurobindol02722POT 45 / mg/L /
W
12/16/2022 S Aurobindol21622Self 25.8 / mg/L /
Oct 2022 Week 4 45 / mg/L /
Dec 2022 Week 3 25.8 / mg/L /
Oct 2022 Average 45 / mg/L /
Dec 2022 Average 25.8 / mg/L /
2022 Quarter 4 35.4 / mg/L /
2022 2nd 6 Months(Avg) 35.4 / mg/L /
2022 2nd 6...(Max) 45 / mg/L /
2022 2nd 6...(Min) 25.8 / mg/L /
2022 2nd 6...(Count) 2 / /
Sample Date SampleID Result/Limit Mass/Limit
Total Phosphorus
10/27/2022 P Aurobindo102722POT 5.12 / mg/L /
W
12/16/2022 S Aurobindo121622Self 4.39 / mg/L /
Oct 2022 Week 4 5.12 / mg/L /
Dec 2022 Week 3 4.39 / mg/L /
Oct 2022 Average 5.12 / mg/L /
Dec 2022 Average 4.39 / mg/L /
2022 Quarter 4 4.755 / mg/L /
2022 2nd 6 Months(Avg) 4.755 / mg/L /
2022 2nd 6...(Max) 5.12 / mg/L /
2022 2nd 6...(Min) 4.39 / mg/L /
2022 2nd 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
TSS
10/27/2022 P Aurobindol02722POT 121 / mg/L /
W
12/16/2022 S Aurobindol21622Self 102 / mg/L /
Oct 2022 Week 4 121 / mg/L /
Dec 2022 Week 3 102 / mg/L /
Oct 2022 Average 121 / mg/L /
Dec 2022 Average 102 / mg/L /
2022 Quarter 4 111.5 / mg/L /
2022 2nd 6 Months(Avg) 111.5 / mg/L /
2022 2nd 6...(Max) 121 / mg/L /
2022 2nd 6...(Min) 102 / mg/L /
2022 2nd 6...(Count) 2
Friday,February 17,2023 5:55:24PM *Indicates Violation **Indicates TRC Violation Page 10 of 11

Aurobindo USA
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
VOC
12/16/2022 S Aurobindo121622Self 0.109 / mg/L /
Dec 2022 Week 3 0.109 / mg/L /
Dec 2022 Average 0.109 / mg/L /
2022 Quarter 4 0.109 / mg/L /
2022 2nd 6 Months(Avg) 0.109 / mg/L /
2022 2nd 6...(Max) 0.109 / mg/L /
2022 2nd 6...(Min) 0.109 / mg/L /
2022 2nd 6...(Count) 1 / /
Sample Date SampleID Result/Limit Mass/Limit
Zinc
10/27/2022 P Aurobindol02722POT 0.132 / mg/L /
W
12/16/2022 S Aurobindo121622Self 0.482 / mg/L /
Oct 2022 Week 4 0.132 / mg/L /
Dec 2022 Week 3 0.482 / mg/L /
Oct 2022 Average 0.132 / mg/L /
Dec 2022 Average 0.482 / mg/L /
2022 Quarter 4 0.307 / mg/L /
2022 2nd 6 Months(Avg) 0.307 / mg/L /
2022 2nd 6...(Max) 0.482 / mg/L /
2022 2nd 6...(Min) 0.132 / mg/L /
2022 2nd 6...(Count) 2
Friday,February 17,2023 5:55:24PM *Indicates Violation **Indicates TRC Violation Page 11 of 11

Biogen
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Acetone
07/22/2022 P Biogen072222POTW < 0.025 / 12.19 mg/L < 0.0259 / lbs/day
Jul 2022 Week 4 < 0.025 / mg/L < 0.0259 / lbs/day
Jul 2022 Average < 0.025 /4.83 mg/L < 0.0259 / lbs/day
2022 Quarter 3 < 0.025 / mg/L < 0.0259 / lbs/day
2022 2nd 6 Months(Avg) < 0.025 / mg/L < 0.0259 / lbs/day
2022 2nd 6...(Max) < 0.025 / mg/L < 0.0259 / lbs/day
2022 2nd 6...(Min) < 0.025 / mg/L < 0.0259 / lbs/day
2022 2nd 6...(Count) 1 / 1 /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Ammonia
07/22/2022 P Biogen072222POTW 2.3 / mg/L 2.3809 / lbs/day
08/23/2022 S Biogen082322Self 2.08 / mg/L 1.6757 / lbs/day
Jul 2022 Week 4 2.3 / mg/L 2.3809 / lbs/day
Aug 2022 Week 4 2.08 / mg/L 1.6757 / lbs/day
Jul 2022 Average 2.3 / mg/L 2.3809 / lbs/day
Aug 2022 Average 2.08 / mg/L 1.6757 / lbs/day
2022 Quarter 3 2.19 / mg/L 2.0283 / lbs/day
2022 2nd 6 Months(Avg) 2.19 / mg/L 2.0283 / lbs/day
2022 2nd 6...(Max) 2.3 / mg/L 2.3809 / lbs/day
2022 2nd 6...(Min) 2.08 / mg/L 1.6757 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2022 S Biogen0722F1ow 0.138686 / MGD /
08/31/2022 S Biogen0822F1ow 0.101592 / MGD /
09/30/2022 S Biogen0922F1ow 0.088561 / MGD /
10/31/2022 S Biogen1022171ow 0.052482 / MGD /
11/30/2022 S Biogen1122171ow 0.052086 / MGD /
12/31/2022 S Biogen1222171ow 0.074441 / MGD /
Jul 2022 Week 4 0.138686 / MGD /
Aug 2022 Week 4 0.101592 / MGD /
Wednesday,February 22,2023 12:09:54PM *Indicates Violation **Indicates TRC Violation Page 1 of 11

Biogen
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Average Flow for Month
Sep 2022 Week 4 0.088561 / MGD /
Oct 2022 Week 4 0.052482 / MGD /
Nov 2022 Week 4 0.052086 / MGD /
Dec 2022 Week 4 0.074441 / MGD /
Jul 2022 Average 0.138686 / MGD /
Aug 2022 Average 0.101592 /0.125 MGD /
Sep 2022 Average 0.088561 /0.125 MGD /
Oct 2022 Average 0.052482 /0.125 MGD /
Nov 2022 Average 0.052086 /0.125 MGD /
Dec 2022 Average 0.074441 /0.125 MGD /
2022 Quarter 3 0.138686 / MGD /
2022 Quarter 3 0.095077 / MGD /
2022 Quarter 3 0.138686 / MGD /
2022 Quarter 3 0.095077 / MGD /
2022 Quarter 4 0.05967 / MGD /
2022 2nd 6 Months(Avg) 0.084641 / MGD /
2022 2nd 6...(Max) 0.138686 / MGD /
2022 2nd 6...(Min) 0.052086 / MGD /
2022 2nd 6...(Count) 6
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 5
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
BOD
07/22/2022 P Biogen072222POTW 81.5 / mg/L 84.366 / lbs/day
08/23/2022 S Biogen082322Self 92.8 / mg/L 74.764 / lbs/day
Jul 2022 Week 4 81.5 / mg/L 84.366 / lbs/day
Aug 2022 Week 4 92.8 / mg/L 74.764 / lbs/day
Jul 2022 Average 81.5 / mg/L 84.366 / lbs/day
Aug 2022 Average 92.8 / mg/L 74.764 / lbs/day
2022 Quarter 3 87.2 / mg/L 79.565 / lbs/day
2022 2nd 6 Months(Avg) 87.2 / mg/L 79.565 / lbs/day
2022 2nd 6...(Max) 92.8 / mg/L 84.366 / lbs/day
2022 2nd 6...(Min) 81.5 / mg/L 74.764 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Wednesday,February 22,2023 12:09:54PM *Indicates Violation **Indicates TRC Violation Page 2 of 11

Biogen
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Cadmium
07/22/2022 P Biogen072222POTW < 0.00008 / mg/L < 0.000078 / lbs/day
Jul 2022 Week 4 < 0.00008 / mg/L < 0.000078 / lbs/day
Jul 2022 Average < 0.00008 / mg/L < 0.000078 / lbs/day
2022 Quarter 3 < 0.00008 / mg/L < 0.000078 / lbs/day
2022 2nd 6 Months(Avg) < 0.00008 / mg/L < 0.000078 / lbs/day
2022 2nd 6...(Max) < 0.00008 / mg/L < 0.000078 / lbs/day
2022 2nd 6...(Min) < 0.00008 / mg/L < 0.000078 / lbs/day
2022 2nd 6...(Count) 1 / 1 /
Sample Date SampleID Result/Limit Mass/Limit
Chloride
07/22/2022 P Biogen072222POTW 91.1 / mg/L 94.3031 / lbs/day
08/23/2022 S Biogen082322Self 47.4 / mg/L 38.1875 / lbs/day
Jul 2022 Week 4 91.1 / mg/L 94.3031 / lbs/day
Aug 2022 Week 4 47.4 / mg/L 38.1875 / lbs/day
Jul 2022 Average 91.1 / mg/L 94.3031 / lbs/day
Aug 2022 Average 47.4 / mg/L 38.1875 / lbs/day
2022 Quarter 3 69.25 / mg/L 66.2453 / lbs/day
2022 2nd 6 Months(Avg) 69.25 / mg/L 66.2453 / lbs/day
2022 2nd 6...(Max) 91.1 / mg/L 94.3031 / lbs/day
2022 2nd 6...(Min) 47.4 / mg/L 38.1875 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
COD
07/22/2022 P Biogen072222POTW 120 / mg/L 124.22 / lbs/day
08/23/2022 S Biogen082322Self 175 / mg/L 140.99 / lbs/day
Jul 2022 Week 4 120 / mg/L 124.22 / lbs/day
Aug 2022 Week 4 175 / mg/L 140.99 / lbs/day
Jul 2022 Average 120 / mg/L 124.22 / lbs/day
Aug 2022 Average 175 / mg/L 140.99 / lbs/day
2022 Quarter 3 147.5 / mg/L 132.6 / lbs/day
2022 2nd 6 Months(Avg) 147.5 / mg/L 132.60 / lbs/day
2022 2nd 6...(Max) 175 / mg/L 140.99 / lbs/day
2022 2nd 6...(Min) 120 / mg/L 124.22 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
07/22/2022 P Biogen072222POTW < 0.003 /0.05 mg/L < 0.002588 / lbs/day
08/23/2022 S Biogen082322Self 0.033 /0.05 mg/L 0.026586 / lbs/day
Wednesday,February 22,2023 12:09:54PM *Indicates Violation **Indicates TRC Violation Page 3 of 11

Biogen
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Cyanide
Jul 2022 Week 4 < 0.003 / mg/L < 0.002588 / lbs/day
Aug 2022 Week 4 0.033 / mg/L 0.026586 / lbs/day
Jul 2022 Average < 0.003 /0.04 mg/L < 0.002588 / lbs/day
Aug 2022 Average 0.033 /0.04 mg/L 0.026586 / lbs/day
2022 Quarter 3 < 0.018 / mg/L < 0.014587 / lbs/day
2022 2nd 6 Months(Avg) < 0.018 / mg/L < 0.014587 / lbs/day
2022 2nd 6...(Max) 0.033 / mg/L 0.026586 / lbs/day
2022 2nd 6...(Min) < 0.003 / mg/L < 0.002588 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Diroximel fumarate
07/29/2022 S Biogen072922SelfDRF 0.049 / mg/L /
11/17/2022 S Biogen111722SelfDRF < 0.004 / mg/L < /
Jul 2022 Week 4 0.049 / mg/L /
Nov 2022 Week 3 < 0.004 / mg/L < /
Jul 2022 Average 0.049 / mg/L /
Nov 2022 Average < 0.004 / mg/L < /
2022 Quarter 3 0.049 / mg/L /
2022 Quarter 4 < 0.004 / mg/L < /
2022 2nd 6 Months(Avg) < 0.026 / mg/L < /
2022 2nd 6...(Max) 0.049 / mg/L /
2022 2nd 6...(Min) < 0.004 / mg/L < /
2022 2nd 6...(Count) 2
Sample Date SampleID Result/Limit Mass/Limit
Ethyl acetate
07/22/2022 P Biogen072222POTW < 0.005 / 12.19 mg/L < 0.0052 / lbs/day
Jul 2022 Week 4 < 0.005 / mg/L < 0.0052 / lbs/day
Jul 2022 Average < 0.005 /4.83 mg/L < 0.0052 / lbs/day
2022 Quarter 3 < 0.005 / mg/L < 0.0052 / lbs/day
2022 2nd 6 Months(Avg) < 0.005 / mg/L < 0.0052 / lbs/day
2022 2nd 6...(Max) < 0.005 / mg/L < 0.0052 / lbs/day
Wednesday,February 22,2023 12:09:54PM *Indicates Violation **Indicates TRC Violation Page 4 of 11

Biogen
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Ethyl acetate
2022 2nd 6...(Min) < 0.005 / mg/L < 0.0052 / lbs/day
2022 2nd 6...(Count) 1 / 1 /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Fluoride
07/22/2022 P Biogen072222POTW 0.96 / mg/L 0.9938 / lbs/day
08/23/2022 S Biogen082322Self 0.92 / mg/L 0.7388 / lbs/day
Jul 2022 Week 4 0.96 / mg/L 0.9938 / lbs/day
Aug 2022 Week 4 0.92 / mg/L 0.7388 / lbs/day
Jul 2022 Average 0.96 / mg/L 0.9938 / lbs/day
Aug 2022 Average 0.92 / mg/L 0.7388 / lbs/day
2022 Quarter 3 0.94 / mg/L 0.8663 / lbs/day
2022 2nd 6 Months(Avg) 0.94 / mg/L 0.8663 / lbs/day
2022 2nd 6...(Max) 0.96 / mg/L 0.9938 / lbs/day
2022 2nd 6...(Min) 0.92 / mg/L 0.7388 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
07/22/2022 P Biogen072222POTW < 0.005 / 12.19 mg/L < 0.0052 / lbs/day
Jul 2022 Week 4 < 0.005 / mg/L < 0.0052 / lbs/day
Jul 2022 Average < 0.005 /4.83 mg/L < 0.0052 / lbs/day
2022 Quarter 3 < 0.005 / mg/L < 0.0052 / lbs/day
2022 2nd 6 Months(Avg) < 0.005 / mg/L < 0.0052 / lbs/day
2022 2nd 6...(Max) < 0.005 / mg/L < 0.0052 / lbs/day
2022 2nd 6...(Min) < 0.005 / mg/L < 0.0052 / lbs/day
2022 2nd 6...(Count) 1 / 1 /
Wednesday,February 22,2023 12:09:54PM *Indicates Violation **Indicates TRC Violation Page 5 of 11

Biogen
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Mercury-LL
07/21/2022 P Biogen072122POTWH 0.000008 /0.000142 mg/L /
g
08/23/2022 S Biogen082322Self 0.000004 /0.000142 mg/L /
Jul 2022 Week 3 0.000008 / mg/L /
Aug 2022 Week 4 0.000004 / mg/L /
Jul 2022 Average 0.000008 / mg/L /
Aug 2022 Average 0.000004 / mg/L /
2022 Quarter 3 0.000006 / mg/L /
2022 2nd 6 Months(Avg) 0.000006 / mg/L /
2022 2nd 6...(Max) 0.000008 / mg/L /
2022 2nd 6...(Min) 0.000004 / mg/L /
2022 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Methylene Chloride
07/22/2022 P Biogen072222POTW < 0.005 / 1.77 mg/L < 0.005176 / lbs/day
Jul 2022 Week 4 < 0.005 / mg/L < 0.005176 / lbs/day
Jul 2022 Average < 0.005 /0.41 mg/L < 0.005176 / lbs/day
2022 Quarter 3 < 0.005 / mg/L < 0.005176 / lbs/day
2022 2nd 6 Months(Avg) < 0.005 / mg/L < 0.005176 / lbs/day
2022 2nd 6...(Max) < 0.005 / mg/L < 0.005176 / lbs/day
2022 2nd 6...(Min) < 0.005 / mg/L < 0.005176 / lbs/day
2022 2nd 6...(Count) 1 / 1 /
Wednesday,February 22,2023 12:09:54PM *Indicates Violation **Indicates TRC Violation Page 6 of 11

Biogen
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Molybdenum
07/22/2022 P Biogen072222POTW < 0.001 / mg/L < 0.001 / lbs/day
Jul 2022 Week 4 < 0.001 / mg/L < 0.001 / lbs/day
Jul 2022 Average < 0.001 / mg/L < 0.001 / lbs/day
2022 Quarter 3 < 0.001 / mg/L < 0.001 / lbs/day
2022 2nd 6 Months(Avg) < 0.001 / mg/L < 0.0010 / lbs/day
2022 2nd 6...(Max) < 0.001 / mg/L < 0.0010 / lbs/day
2022 2nd 6...(Min) < 0.001 / mg/L < 0.0010 / lbs/day
2022 2nd 6...(Count) 1 / 1 /
Sample Date SampleID Result/Limit Mass/Limit
n-Amyl acetate
07/22/2022 P Biogen072222POTW < 0.005 / 12.19 mg/L < 0.0052 / lbs/day
Jul 2022 Week 4 < 0.005 / mg/L < 0.0052 / lbs/day
Jul 2022 Average < 0.005 /4.83 mg/L < 0.0052 / lbs/day
2022 Quarter 3 < 0.005 / mg/L < 0.0052 / lbs/day
2022 2nd 6 Months(Avg) < 0.005 / mg/L < 0.0052 / lbs/day
2022 2nd 6...(Max) < 0.005 / mg/L < 0.0052 / lbs/day
2022 2nd 6...(Min) < 0.005 / mg/L < 0.0052 / lbs/day
2022 2nd 6...(Count) 1 / 1 /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Nitrate-Nitrite
07/22/2022 P Biogen072222POTW 0.2 / mg/L 0.238 / lbs/day
08/23/2022 S Biogen082322Self 0.4 / mg/L 0.322 / lbs/day
Jul 2022 Week 4 0.2 / mg/L 0.238 / lbs/day
Wednesday,February 22,2023 12:09:54PM *Indicates Violation **Indicates TRC Violation Page 7 of 11

Biogen
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
Nitrate-Nitrite
Aug 2022 Week 4 0.4 / mg/L 0.322 / lbs/day
Jul 2022 Average 0.2 / mg/L 0.238 / lbs/day
Aug 2022 Average 0.4 / mg/L 0.322 / lbs/day
2022 Quarter 3 0.3 / mg/L 0.28 / lbs/day
2022 2nd 6 Months(Avg) 0.3 / mg/L 0.280 / lbs/day
2022 2nd 6...(Max) 0.4 / mg/L 0.322 / lbs/day
2022 2nd 6...(Min) 0.2 / mg/L 0.238 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SampleID Result/Limit Mass/Limit
Nitrogen,Total
07/22/2022 P Biogen072222POTW 7.03 / mg/L 7.277 / lbs/day
08/23/2022 S Biogen082322Self 8.97 / mg/L 7.227 / lbs/day
Jul 2022 Week 4 7.03 / mg/L 7.277 / lbs/day
Aug 2022 Week 4 8.97 / mg/L 7.227 / lbs/day
Jul 2022 Average 7.03 / mg/L 7.277 / lbs/day
Aug 2022 Average 8.97 / mg/L 7.227 / lbs/day
2022 Quarter 3 8 / mg/L 7.252 / lbs/day
2022 2nd 6 Months(Avg) 8 / mg/L 7.252 / lbs/day
2022 2nd 6...(Max) 8.97 / mg/L 7.277 / lbs/day
2022 2nd 6...(Min) 7.03 / mg/L 7.227 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SampleID Result/Limit Mass/Limit
Oil&Grease,Total
07/22/2022 P Biogen072222POTW < 2.5 /200 mg/L < /
Jul 2022 Week 4 < 2.5 / mg/L < /
Jul 2022 Average < 2.5 / mg/L < /
2022 Quarter 3 < 2.5 / mg/L < /
2022 2nd 6 Months(Avg) < 2.5 / mg/L < /
2022 2nd 6...(Max) < 2.5 / mg/L < /
2022 2nd 6...(Min) < 2.5 / mg/L < /
2022 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Wednesday,February 22,2023 12:09:54PM *Indicates Violation **Indicates TRC Violation Page 8 of 11

Biogen
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
pH
07/22/2022 P Biogen072222POTW 7.4 /5.5-10.5 SU /
08/23/2022 S Biogen082322Self 8.13 /5.5-10.5 SU /
Jul 2022 Week 4 7.4 / SU /
Aug 2022 Week 4 8.13 / SU /
Jul 2022 Average 7.4 / SU /
Aug 2022 Average 8.13 / SU /
2022 Quarter 3 7.77 / SU /
2022 2nd 6 Months(Avg) 7.77 / SU /
2022 2nd 6...(Max) 8.13 / SU /
2022 2nd 6...(Min) 7.4 / SU /
2022 2nd 6...(Count) 2
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
07/22/2022 P Biogen072222POTW 30 /66 °C /
08/23/2022 S Biogen082322Self 27.8 /66 °C /
Jul 2022 Week 4 30 / °C /
Aug 2022 Week 4 27.8 / °C /
Jul 2022 Average 30 / °C /
Aug 2022 Average 27.8 / °C /
2022 Quarter 3 28.9 / °C /
2022 2nd 6 Months(Avg) 28.9 / °C /
2022 2nd 6...(Max) 30 / °C /
2022 2nd 6...(Min) 27.8 / °C /
2022 2nd 6...(Count) 2
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Wednesday,February 22,2023 12:09:54PM *Indicates Violation **Indicates TRC Violation Page 9 of 11

Biogen
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
TKN
07/22/2022 P Biogen072222POTW 6.8 / mg/L 7.039 / lbs/day
08/23/2022 S Biogen082322Self 8.57 / mg/L 6.904 / lbs/day
Jul 2022 Week 4 6.8 / mg/L 7.039 / lbs/day
Aug 2022 Week 4 8.57 / mg/L 6.904 / lbs/day
Jul 2022 Average 6.8 / mg/L 7.039 / lbs/day
Aug 2022 Average 8.57 / mg/L 6.904 / lbs/day
2022 Quarter 3 7.69 / mg/L 6.972 / lbs/day
2022 2nd 6 Months(Avg) 7.69 / mg/L 6.972 / lbs/day
2022 2nd 6...(Max) 8.57 / mg/L 7.039 / lbs/day
2022 2nd 6...(Min) 6.8 / mg/L 6.904 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
07/22/2022 P Biogen072222POTW 1.48 / mg/L 1.532 / lbs/day
08/23/2022 S Biogen082322Self 0.516 / mg/L 0.4157 / lbs/day
Jul 2022 Week 4 1.48 / mg/L 1.532 / lbs/day
Aug 2022 Week 4 0.516 / mg/L 0.4157 / lbs/day
Jul 2022 Average 1.48 / mg/L 1.532 / lbs/day
Aug 2022 Average 0.516 / mg/L 0.4157 / lbs/day
2022 Quarter 3 0.998 / mg/L 0.9739 / lbs/day
2022 2nd 6 Months(Avg) 0.998 / mg/L 0.9739 / lbs/day
2022 2nd 6...(Max) 1.48 / mg/L 1.5320 / lbs/day
2022 2nd 6...(Min) 0.516 / mg/L 0.4157 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
TSS
07/22/2022 P Biogen072222POTW 74 / mg/L 76.601899 / lbs/day
08/23/2022 S Biogen082322Self 84 / mg/L 67.674096 / lbs/day
Jul 2022 Week 4 74 / mg/L 76.601899 / lbs/day
Aug 2022 Week 4 84 / mg/L 67.674096 / lbs/day
Jul 2022 Average 74 / mg/L 76.601899 / lbs/day
Aug 2022 Average 84 / mg/L 67.674096 / lbs/day
2022 Quarter 3 79 / mg/L 72.137998 / lbs/day
2022 2nd 6 Months(Avg) 79 / mg/L 72.138 / lbs/day
2022 2nd 6...(Max) 84 / mg/L 76.601899 / lbs/day
2022 2nd 6...(Min) 74 / mg/L 67.674096 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Wednesday,February 22,2023 12:09:54PM *Indicates Violation **Indicates TRC Violation Page 10 of 11

Biogen
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Zinc
07/22/2022 P Biogen072222POTW 0.354 / mg/L 0.366861 / lbs/day
08/23/2022 S Biogen082322Self 0.302 / mg/L 0.243304 / lbs/day
Jul 2022 Week 4 0.354 / mg/L 0.366861 / lbs/day
Aug 2022 Week 4 0.302 / mg/L 0.243304 / lbs/day
Jul 2022 Average 0.354 / mg/L 0.366861 / lbs/day
Aug 2022 Average 0.302 / mg/L 0.243304 / lbs/day
2022 Quarter 3 0.328 / mg/L 0.305083 / lbs/day
2022 2nd 6 Months(Avg) 0.328 / mg/L 0.305083 / lbs/day
2022 2nd 6...(Max) 0.354 / mg/L 0.366861 / lbs/day
2022 2nd 6...(Min) 0.302 / mg/L 0.243304 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Wednesday,February 22,2023 12:09:54PM *Indicates Violation **Indicates TRC Violation Page 11 of 11

Cintas Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
Aluminum
08/17/2022 S Cintas081722Self 1.64 / mg/L 0.906798 / lbs/day
Aug 2022 Week 3 1.64 / mg/L 0.906798 / lbs/day
Aug 2022 Average 1.64 / mg/L 0.906798 / lbs/day
2022 Quarter 3 1.64 / mg/L 0.906798 / lbs/day
2022 2nd 6 Months(Avg) 1.64 / mg/L 0.906798 / lbs/day
2022 2nd 6...(Max) 1.64 / mg/L 0.906798 / lbs/day
2022 2nd 6...(Min) 1.64 / mg/L 0.906798 / lbs/day
2022 2nd 6...(Count) 1 / 1 /
Sample Date SampleID Result/Limit Mass/Limit
Ammonia
07/26/2022 S Cintas072622Self 2.9 / mg/L 0.9634 / lbs/day
08/17/2022 S Cintas081722Self 7.1 / mg/L 3.9258 / lbs/day
10/11/2022 S Cintas101122Self 3.2 / mg/L 1.2881 / lbs/day
12/20/2022 S Cintasl22022Self 6.2 / mg/L 1.9281 / lbs/day
Jul 2022 Week 4 2.9 / mg/L 0.9634 / lbs/day
Aug 2022 Week 3 7.1 / mg/L 3.9258 / lbs/day
Oct 2022 Week 2 3.2 / mg/L 1.2881 / lbs/day
Dec 2022 Week 3 6.2 / mg/L 1.9281 / lbs/day
Jul 2022 Average 2.9 / mg/L 0.9634 / lbs/day
Aug 2022 Average 7.1 / mg/L 3.9258 / lbs/day
Oct 2022 Average 3.2 / mg/L 1.2881 / lbs/day
Dec 2022 Average 6.2 / mg/L 1.9281 / lbs/day
2022 Quarter 3 5 / mg/L 2.4446 / lbs/day
2022 Quarter 4 3.2 / mg/L 1.2881 / lbs/day
2022 Quarter 4 6.2 / mg/L 1.9281 / lbs/day
2022 Quarter 4 6.2 / mg/L 1.9281 / lbs/day
2022 Quarter 4 3.2 / mg/L 1.2881 / lbs/day
2022 2nd 6 Months(Avg) 4.85 / mg/L 2.0263 / lbs/day
2022 2nd 6...(Max) 7.1 / mg/L 3.9258 / lbs/day
2022 2nd 6...(Min) 2.9 / mg/L 0.9634 / lbs/day
2022 2nd 6...(Count) 4 / 4 /
Sample Date SampleID Result/Limit Mass/Limit
Average Flow for Month
07/31/2022 S Cintas0722F1ow 0.046067 /0.180 MGD /
08/31/2022 S Cintas0822F1ow 0.055934 /0.180 MGD /
09/30/2022 S Cintas0922F1ow 0.04572 /0.180 MGD /
10/31/2022 S Cintasl022F1ow 0.055371 /0.180 MGD /
11/30/2022 S CintasI122F1ow 0.052794 / MGD /
12/31/2022 S Cintas1222171ow 0.049431 / MGD /
Jul 2022 Week 4 0.046067 / MGD /
Monday,February 27,2023 4:23:55PM *Indicates Violation **Indicates TRC Violation Page 1 of 15

Cintas Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Average Flow for Month
Aug 2022 Week 4 0.055934 / MGD /
Sep 2022 Week 4 0.04572 / MGD /
Oct 2022 Week 4 0.055371 / MGD /
Nov 2022 Week 4 0.052794 / MGD /
Dec 2022 Week 4 0.049431 / MGD /
Jul 2022 Average 0.046067 /0.120 MGD /
Aug 2022 Average 0.055934 /0.120 MGD /
Sep 2022 Average 0.04572 /0.120 MGD /
Oct 2022 Average 0.055371 /0.120 MGD /
Nov 2022 Average 0.052794 /0.100 MGD /
Dec 2022 Average 0.049431 /0.100 MGD /
2022 Quarter 3 0.04924 / MGD /
2022 Quarter 4 0.055371 / MGD /
2022 Quarter 4 0.051113 / MGD /
2022 Quarter 4 0.051113 / MGD /
2022 Quarter 4 0.055371 / MGD /
2022 2nd 6 Months(Avg) 0.050886 / MGD /
2022 2nd 6...(Max) 0.055934 / MGD /
2022 2nd 6...(Min) 0.04572 / MGD /
2022 2nd 6...(Count) 6
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 5
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
BOD
07/26/2022 S Cintas072622Self 292 / mg/L 97.002 / lbs/day
07/28/2022 P Cintas072822POTW 437 / mg/L /
08/04/2022 P Cintas08O422POTW 623 / mg/L /
08/17/2022 S Cintas081722Self 386 / mg/L 213.429 / lbs/day
09/20/2022 P Cintas092022POTW 399 / mg/L /
09/20/2022 S Cintas092022Self 251 / mg/L 93.664 / lbs/day
10/11/2022 S Cintas101122Self 235 / mg/L 94.593 / lbs/day
10/19/2022 P Cintas101922POTW 296 / mg/L /
11/08/2022 S Cintasl10822Self 352 / mg/L 133.656 / lbs/day
11/15/2022 P Cintasl11522POTW 220 / mg/L /
12/13/2022 P Cintas121322POTW 404 / mg/L /
Monday,February 27,2023 4:23:55PM *Indicates Violation **Indicates TRC Violation Page 2 of 15

Cintas Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
BOD
12/13/2022 P Cintas021322POTW 404 / mg/L /
12/20/2022 S Cintasl22022Self 1090 / mg/L 338.97 / lbs/day
Jul 2022 Week 4 364.5 / mg/L 97.002 / lbs/day
Aug 2022 Week 1 623 / mg/L /
Aug 2022 Week 3 386 / mg/L 213.429 / lbs/day
Sep 2022 Week 3 325 / mg/L 93.664 / lbs/day
Oct 2022 Week 2 235 / mg/L 94.593 / lbs/day
Oct 2022 Week 3 296 / mg/L /
Nov 2022 Week 2 352 / mg/L 133.656 / lbs/day
Nov 2022 Week 3 220 / mg/L /
Dec 2022 Week 2 404 / mg/L /
Dec 2022 Week 3 1090 / mg/L 338.97 / lbs/day
Jul 2022 Average 364.5 / mg/L 97.002 / lbs/day
Aug 2022 Average 504.5 / mg/L 213.429 / lbs/day
Sep 2022 Average 325 / mg/L 93.664 / lbs/day
Oct 2022 Average 265.5 / mg/L 94.593 / lbs/day
Nov 2022 Average 286 / mg/L 133.656 / lbs/day
Dec 2022 Average 632.7 / mg/L 338.97 / lbs/day
2022 Quarter 3 398 / mg/L 134.699 / lbs/day
2022 Quarter 4 265.5 / mg/L 94.593 / lbs/day
2022 Quarter 4 494 / mg/L 236.313 / lbs/day
2022 Quarter 4 494 / mg/L 236.313 / lbs/day
2022 Quarter 4 265.5 / mg/L 94.593 / lbs/day
2022 2nd 6 Months(Avg) 414.5 / mg/L 161.886 / lbs/day
2022 2nd 6...(Max) 1090 / mg/L 338.970 / lbs/day
2022 2nd 6...(Min) 220 / mg/L /
2022 2nd 6...(Count) 13 / 6 /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
08/17/2022 S Cintas081722Self 0.001 / mg/L 0.000553 / lbs/day
Aug 2022 Week 3 0.001 / mg/L 0.000553 / lbs/day
Aug 2022 Average 0.001 / mg/L 0.000553 / lbs/day
2022 Quarter 3 0.001 / mg/L 0.000553 / lbs/day
2022 2nd 6 Months(Avg) 0.001 / mg/L 0.000553 / lbs/day
2022 2nd 6...(Max) 0.001 / mg/L 0.000553 / lbs/day
2022 2nd 6...(Min) 0.001 / mg/L 0.000553 / lbs/day
2022 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
07/28/2022 P Cintas072822POTW 131 / mg/L /
Monday,February 27,2023 4:23:55PM *Indicates Violation **Indicates TRC Violation Page 3 of 15

Cintas Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Chloride
Jul 2022 Week 4 131 / mg/L /
Jul 2022 Average 131 / mg/L /
2022 Quarter 3 131 / mg/L /
2022 2nd 6 Months(Avg) 131 / mg/L /
2022 2nd 6...(Max) 131 / mg/L /
2022 2nd 6...(Min) 131 / mg/L /
2022 2nd 6...(Count) 1 / /
Sample Date SampleID Result/Limit Mass Mmit
Chromium
08/17/2022 S Cintas081722Self 0.016 / mg/L 0.009013 / lbs/day
10/11/2022 S Cintas101122Self 0.005 / mg/L 0.002013 / lbs/day
Aug 2022 Week 3 0.016 / mg/L 0.009013 / lbs/day
Oct 2022 Week 2 0.005 / mg/L 0.002013 / lbs/day
Aug 2022 Average 0.016 / mg/L 0.009013 / lbs/day
Oct 2022 Average 0.005 / mg/L 0.002013 / lbs/day
2022 Quarter 3 0.016 / mg/L 0.009013 / lbs/day
2022 Quarter 4 0.005 / mg/L 0.002013 / lbs/day
2022 2nd 6 Months(Avg) 0.011 / mg/L 0.005513 / lbs/day
2022 2nd 6...(Max) 0.016 / mg/L 0.009013 / lbs/day
2022 2nd 6...(Min) 0.005 / mg/L 0.002013 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
08/17/2022 S Cintas081722Self 0.156 / mg/L 0.086256 / lbs/day
10/11/2022 S CintasIO1122Self 0.048 / mg/L 0.019321 / lbs/day
Aug 2022 Week 3 0.156 / mg/L 0.086256 / lbs/day
Oct 2022 Week 2 0.048 / mg/L 0.019321 / lbs/day
Aug 2022 Average 0.156 / mg/L 0.086256 / lbs/day
Oct 2022 Average 0.048 / mg/L 0.019321 / lbs/day
2022 Quarter 3 0.156 / mg/L 0.086256 / lbs/day
2022 Quarter 4 0.048 / mg/L 0.019321 / lbs/day
2022 2nd 6 Months(Avg) 0.102 / mg/L 0.052789 / lbs/day
2022 2nd 6...(Max) 0.156 / mg/L 0.086256 / lbs/day
2022 2nd 6...(Min) 0.048 / mg/L 0.019321 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
07/26/2022 S Cintas072622Self 6.3 / mg/L 2.0929 / lbs/day
Monday,February 27,2023 4:23:55PM *Indicates Violation **Indicates TRC Violation Page 4 of 15

Cintas Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Fluoride
07/28/2022 P Cintas072822POTW 0.88 / mg/L /
08/17/2022 S Cintas081722Self 0.27 / mg/L 0.1493 / lbs/day
09/20/2022 S Cintas092022Self < 0.05 / mg/L < 0.0187 / lbs/day
10/11/2022 S CintasIO1122Self 0.41 / mg/L 0.165 / lbs/day
Jul 2022 Week 4 3.59 / mg/L 2.0929 / lbs/day
Aug 2022 Week 3 0.27 / mg/L 0.1493 / lbs/day
Sep 2022 Week 3 < 0.05 / mg/L < 0.0187 / lbs/day
Oct 2022 Week 2 0.41 / mg/L 0.165 / lbs/day
Jul 2022 Average 3.59 / mg/L 2.0929 / lbs/day
Aug 2022 Average 0.27 / mg/L 0.1493 / lbs/day
Sep 2022 Average < 0.05 / mg/L < 0.0187 / lbs/day
Oct 2022 Average 0.41 / mg/L 0.165 / lbs/day
2022 Quarter 3 < 1.88 / mg/L < 0.7536 / lbs/day
2022 Quarter 4 0.41 / mg/L 0.165 / lbs/day
2022 2nd 6 Months(Avg) < 1.58 / mg/L < 0.6065 / lbs/day
2022 2nd 6...(Max) 6.3 / mg/L 2.0929 / lbs/day
2022 2nd 6...(Min) < 0.05 / mg/L < /
2022 2nd 6...(Count) 5 / 4 /
Sample Date SamplelD Result/Limit Mass/Limit
Lead
08/17/2022 S Cintas081722Self 0.0164 / mg/L 0.009068 / lbs/day
10/11/2022 S Cintas101122Self 0.0059 / mg/L 0.002375 / lbs/day
Aug 2022 Week 3 0.0164 / mg/L 0.009068 / lbs/day
Oct 2022 Week 2 0.0059 / mg/L 0.002375 / lbs/day
Aug 2022 Average 0.0164 / mg/L 0.009068 / lbs/day
Oct 2022 Average 0.0059 / mg/L 0.002375 / lbs/day
2022 Quarter 3 0.0164 / mg/L 0.009068 / lbs/day
2022 Quarter 4 0.0059 / mg/L 0.002375 / lbs/day
2022 2nd 6 Months(Avg) 0.0112 / mg/L 0.005721 / lbs/day
2022 2nd 6...(Max) 0.0164 / mg/L 0.009068 / lbs/day
2022 2nd 6...(Min) 0.0059 / mg/L 0.002375 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
08/24/2022 S Cintas08l722SeltHg 0.000013 /0.000142 mg/L /
10/19/2022 P CintasIO1922POTWH 0.000027 /0.000142 mg/L /
g
Aug 2022 Week 4 0.000013 / mg/L /
Oct 2022 Week 3 0.000027 / mg/L /
Aug 2022 Average 0.000013 / mg/L /
Monday,February 27,2023 4:23:55PM *Indicates Violation **Indicates TRC Violation Page 5 of 15

Cintas Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
Mercury-LL
Oct 2022 Average 0.000027 / mg/L /
2022 Quarter 3 0.000013 / mg/L /
2022 Quarter 4 0.000027 / mg/L /
2022 2nd 6 Months(Avg) 0.00002 / mg/L /
2022 2nd 6...(Max) 0.000027 / mg/L /
2022 2nd 6...(Min) 0.000013 / mg/L /
2022 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Molybdenum
08/17/2022 S Cintas081722Self 0 / mg/L 0.0137 / lbs/day
10/11/2022 S Cintasl01122Self 0 / mg/L 0.0028 / lbs/day
Aug 2022 Week 3 0 / mg/L 0.0137 / lbs/day
Oct 2022 Week 2 0 / mg/L 0.0028 / lbs/day
Aug 2022 Average 0 / mg/L 0.0137 / lbs/day
Oct 2022 Average 0 / mg/L 0.0028 / lbs/day
2022 Quarter 3 0 / mg/L 0.0137 / lbs/day
2022 Quarter 4 0 / mg/L 0.0028 / lbs/day
2022 2nd 6 Months(Avg) 0.0 / mg/L 0.0082 / lbs/day
2022 2nd 6...(Max) 0.0 / mg/L 0.0137 / lbs/day
2022 2nd 6...(Min) 0.0 / mg/L 0.0028 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SampleID Result/Limit Mass/Limit
Nickel
08/17/2022 S CintasO81722Self 0.0263 / mg/L 0.014542 / lbs/day
10/11/2022 S CintasIO1122Self 0.014 / mg/L 0.005635 / lbs/day
Aug 2022 Week 3 0.0263 / mg/L 0.014542 / lbs/day
Oct 2022 Week 2 0.014 / mg/L 0.005635 / lbs/day
Aug 2022 Average 0.0263 / mg/L 0.014542 / lbs/day
Oct 2022 Average 0.014 / mg/L 0.005635 / lbs/day
2022 Quarter 3 0.0263 / mg/L 0.014542 / lbs/day
2022 Quarter 4 0.014 / mg/L 0.005635 / lbs/day
Monday,February 27,2023 4:23:55PM *Indicates Violation **Indicates TRC Violation Page 6 of 15

Cintas Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Nickel
2022 2nd 6 Months(Avg) 0.0202 / mg/L 0.010089 / lbs/day
2022 2nd 6...(Max) 0.0263 / mg/L 0.014542 / lbs/day
2022 2nd 6...(Min) 0.014 / mg/L 0.005635 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
07/26/2022 S Cintas072622Self 0.1 / mg/L 0.023 / lbs/day
07/28/2022 P Cintas072822POTW 0.1 / mg/L /
08/17/2022 S Cintas081722Self < 0 / mg/L < 0.011 / lbs/day
09/20/2022 S Cintas092022Self 0.1 / mg/L 0.045 / lbs/day
10/11/2022 S Cintas101122Self 0 / mg/L 0.019 / lbs/day
11/08/2022 S Cintasl10822Self 0.2 / mg/L 0.087 / lbs/day
12/20/2022 S Cintasl22022Self 0.3 / mg/L 0.078 / lbs/day
Jul 2022 Week 4 0.1 / mg/L 0.023 / lbs/day
Aug 2022 Week 3 < 0 / mg/L < 0.011 / lbs/day
Sep 2022 Week 3 0.1 / mg/L 0.045 / lbs/day
Oct 2022 Week 2 0 / mg/L 0.019 / lbs/day
Nov 2022 Week 2 0.2 / mg/L 0.087 / lbs/day
Dec 2022 Week 3 0.3 / mg/L 0.078 / lbs/day
Jul 2022 Average 0.1 / mg/L 0.023 / lbs/day
Aug 2022 Average < 0 / mg/L < 0.011 / lbs/day
Sep 2022 Average 0.1 / mg/L 0.045 / lbs/day
Oct 2022 Average 0 / mg/L 0.019 / lbs/day
Nov 2022 Average 0.2 / mg/L 0.087 / lbs/day
Dec 2022 Average 0.3 / mg/L 0.078 / lbs/day
2022 Quarter 3 < 0.1 / mg/L < 0.026 / lbs/day
2022 Quarter 4 0.2 / mg/L 0.061 / lbs/day
2022 2nd 6 Months(Avg) < 0.1 / mg/L < 0.044 / lbs/day
2022 2nd 6...(Max) 0.3 / mg/L 0.087 / lbs/day
2022 2nd 6...(Min) < 0.0 / mg/L < /
2022 2nd 6...(Count) 7 / 6 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
07/26/2022 S Cintas072622Self 27.9 / mg/L 9.268 / lbs/day
07/28/2022 P Cintas072822POTW 35.5 / mg/L /
08/17/2022 S Cintas081722Self 26.2 / mg/L 14.487 / lbs/day
09/20/2022 S Cintas092022Self 43 / mg/L 16.046 / lbs/day
10/11/2022 S CintasIO1122Self 13.5 / mg/L 5.434 / lbs/day
11/08/2022 S Cintas110822Self 62 / mg/L 23.542 / lbs/day
12/20/2022 S Cintasl22022Self 36.9 / mg/L 11.475 / lbs/day
Monday,February 27,2023 4:23:55PM *Indicates Violation **Indicates TRC Violation Page 7 of 15

Cintas Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Nitrogen,Total
Jul 2022 Week 4 31.7 / mg/L 9.268 / lbs/day
Aug 2022 Week 3 26.2 / mg/L 14.487 / lbs/day
Sep 2022 Week 3 43 / mg/L 16.046 / lbs/day
Oct 2022 Week 2 13.5 / mg/L 5.434 / lbs/day
Nov 2022 Week 2 62 / mg/L 23.542 / lbs/day
Dec 2022 Week 3 36.9 / mg/L 11.475 / lbs/day
Jul 2022 Average 31.7 / mg/L 9.268 / lbs/day
Aug 2022 Average 26.2 / mg/L 14.487 / lbs/day
Sep 2022 Average 43 / mg/L 16.046 / lbs/day
Oct 2022 Average 13.5 / mg/L 5.434 / lbs/day
Nov 2022 Average 62 / mg/L 23.542 / lbs/day
Dec 2022 Average 36.9 / mg/L 11.475 / lbs/day
2022 Quarter 3 33.15 / mg/L 13.267 / lbs/day
2022 Quarter 4 13.5 / mg/L 5.434 / lbs/day
2022 Quarter 4 49.45 / mg/L 17.508 / lbs/day
2022 Quarter 4 49.45 / mg/L 17.508 / lbs/day
2022 Quarter 4 13.5 / mg/L 5.434 / lbs/day
2022 2nd 6 Months(Avg) 35 / mg/L 13.375 / lbs/day
2022 2nd 6...(Max) 62 / mg/L 23.542 / lbs/day
2022 2nd 6...(Min) 13.5 / mg/L /
2022 2nd 6...(Count) 7 / 6 /
Sample Date SampleID Result/Limit Mass/Limit
Oil&Grease,HEM(Polar)
07/26/2022 S Cintas072622Self 48.7 / 100 mg/L 16.178085 / lbs/day
07/28/2022 P Cintas072822POTW < 2.5 / 100 mg/L < /
08/17/2022 S Cintas081722Self < 2.5 / 100 mg/L < 1.382313 / lbs/day
09/20/2022 S Cintas092022Self < 2.5 / 100 mg/L < 0.932912 / lbs/day
10/11/2022 S Cintas101122Self 4.8 / 100 mg/L 1.932104 / lbs/day
11/08/2022 S Cintasl10822Self 5.5 / 100 mg/L 2.088369 / lbs/day
12/20/2022 S Cintasl22022Self 161 / 100 mg/L * * 50.068089 / lbs/day
Jul 2022 Week 4 < 25.6 / mg/L < 16.178085 / lbs/day
Aug 2022 Week 3 < 2.5 / mg/L < 1.382313 / lbs/day
Sep 2022 Week 3 < 2.5 / mg/L < 0.932912 / lbs/day
Oct 2022 Week 2 4.8 / mg/L 1.932104 / lbs/day
Nov 2022 Week 2 5.5 / mg/L 2.088369 / lbs/day
Dec 2022 Week 3 161 / mg/L 50.068089 / lbs/day
Jul 2022 Average < 25.6 / mg/L < 16.178085 / lbs/day
Aug 2022 Average < 2.5 / mg/L < 1.382313 / lbs/day
Sep 2022 Average < 2.5 / mg/L < 0.932912 / lbs/day
Oct 2022 Average 4.8 / mg/L 1.932104 / lbs/day
Nov 2022 Average 5.5 / mg/L 2.088369 / lbs/day
Monday,February 27,2023 4:23:55PM *Indicates Violation **Indicates TRC Violation Page 8 of 15

Cintas Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Oil&Grease,HEM(Polar)
Dec 2022 Average 161 / mg/L 50.068089 / lbs/day
2022 Quarter 3 < 14.1 / mg/L < 6.164437 / lbs/day
2022 Quarter 4 4.8 / mg/L 1.932104 / lbs/day
2022 Quarter 4 83.3 / mg/L 26.078229 / lbs/day
2022 Quarter 4 83.3 / mg/L 26.078229 / lbs/day
2022 Quarter 4 4.8 / mg/L 1.932104 / lbs/day
2022 2nd 6 Months(Avg) < 32.5 / mg/L < 12.097 / lbs/day
2022 2nd 6...(Max) 161 / mg/L 50.068089 / lbs/day
2022 2nd 6...(Min) < 2.5 / mg/L < /
2022 2nd 6...(Count) 7 / 6 /
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 5
#Over Daily C: 1 14.29 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 1 14.29 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,SGT-HEM(Non-Polar)
07/26/2022 S Cintas072622Self < 2.5 / 100 mg/L < 0.8305 / lbs/day
07/28/2022 P Cintas072822POTW < 2.5 / 100 mg/L < /
08/17/2022 S Cintas081722Self < 2.5 / 100 mg/L < 1.3823 / lbs/day
09/20/2022 S Cintas092022Self < 2.5 / 100 mg/L < 0.9329 / lbs/day
10/11/2022 S Cintas101122Self 4.8 / 100 mg/L 1.9321 / lbs/day
11/08/2022 S Cintasl10822Self < 2.5 / 100 mg/L < 0.9493 / lbs/day
12/20/2022 S Cintasl22022Self 23 / 100 mg/L 7.1526 / lbs/day
Jul 2022 Week 4 < 2.5 / mg/L < 0.8305 / lbs/day
Aug 2022 Week 3 < 2.5 / mg/L < 1.3823 / lbs/day
Sep 2022 Week 3 < 2.5 / mg/L < 0.9329 / lbs/day
Oct 2022 Week 2 4.8 / mg/L 1.9321 / lbs/day
Nov 2022 Week 2 < 2.5 / mg/L < 0.9493 / lbs/day
Dec 2022 Week 3 23 / mg/L 7.1526 / lbs/day
Jul 2022 Average < 2.5 / mg/L < 0.8305 / lbs/day
Aug 2022 Average < 2.5 / mg/L < 1.3823 / lbs/day
Sep 2022 Average < 2.5 / mg/L < 0.9329 / lbs/day
Oct 2022 Average 4.8 / mg/L 1.9321 / lbs/day
Nov 2022 Average < 2.5 / mg/L < 0.9493 / lbs/day
Dec 2022 Average 23 / mg/L 7.1526 / lbs/day
2022 Quarter 3 < 2.5 / mg/L < 1.0486 / lbs/day
2022 Quarter 4 4.8 / mg/L 1.9321 / lbs/day
Monday,February 27,2023 4:23:55PM *Indicates Violation **Indicates TRC Violation Page 9 of 15

Cintas Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,SGT-HEM(Non-Polar)
2022 Quarter 4 < 12.8 / mg/L < 4.0509 / lbs/day
2022 Quarter 4 < 12.8 / mg/L < 4.0509 / lbs/day
2022 Quarter 4 4.8 / mg/L 1.9321 / lbs/day
2022 2nd 6 Months(Avg) < 5.8 / mg/L < 2.1966 / lbs/day
2022 2nd 6...(Max) 23 / mg/L 7.1526 / lbs/day
2022 2nd 6...(Min) < 2.5 / mg/L < /
2022 2nd 6...(Count) 7 / 6 /
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 5
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass Mmit
pH
07/26/2022 S Cintas072622Self 7.3 /6.0-10.5 SU /
07/28/2022 P Cintas072822POTW 7.2 /6.0-10.5 SU /
08/17/2022 S Cintas081722Self 7.2 /6.0-10.5 SU /
09/20/2022 S Cintas092022Self 7.6 /6.0-10.5 SU /
10/11/2022 S Cintas101122Self 7.9 /6.0-10.5 SU /
11/08/2022 S Cintasl10822Self 7.3 /6.0-10.5 SU /
12/20/2022 S Cintasl22022Self 7.4 /6.0-10.5 SU /
Jul 2022 Week 4 7.25 / SU /
Aug 2022 Week 3 7.2 / SU /
Sep 2022 Week 3 7.6 / SU /
Oct 2022 Week 2 7.9 / SU /
Nov 2022 Week 2 7.3 / SU /
Dec 2022 Week 3 7.4 / SU /
Jul 2022 Average 7.25 / SU /
Aug 2022 Average 7.2 / SU /
Sep 2022 Average 7.6 / SU /
Oct 2022 Average 7.9 / SU /
Nov 2022 Average 7.3 / SU /
Dec 2022 Average 7.4 / SU /
2022 Quarter 3 7.33 / SU /
2022 Quarter 4 7.9 / SU /
2022 Quarter 4 7.35 / SU /
2022 Quarter 4 7.35 / SU /
2022 Quarter 4 7.9 / SU /
Monday,February 27,2023 4:23:55PM *Indicates Violation **Indicates TRC Violation Page 10 of 15

Cintas Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
pH
2022 2nd 6 Months(Avg) 7.41 / SU /
2022 2nd 6...(Max) 7.9 / SU /
2022 2nd 6...(Min) 7.2 / SU /
2022 2nd 6...(Count) 7 / /
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 5
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Silver
08/17/2022 S Cintas081722Self 0.0021 / mg/L 0.001161 / lbs/day
Aug 2022 Week 3 0.0021 / mg/L 0.001161 / lbs/day
Aug 2022 Average 0.0021 / mg/L 0.001161 / lbs/day
2022 Quarter 3 0.0021 / mg/L 0.001161 / lbs/day
2022 2nd 6 Months(Avg) 0.0021 / mg/L 0.001161 / lbs/day
2022 2nd 6...(Max) 0.0021 / mg/L 0.001161 / lbs/day
2022 2nd 6...(Min) 0.0021 / mg/L 0.001161 / lbs/day
2022 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
07/26/2022 S Cintas072622Self 24.7 /66 °C /
07/28/2022 P Cintas072822POTW 29.3 /66 °C /
08/17/2022 S Cintas081722Self 21.2 /66 °C /
09/20/2022 S Cintas092022Self 32.1 /66 °C /
10/11/2022 S CintasIO1122Self 34.4 /66 °C /
11/08/2022 S Cintas110822Self 31.4 /66 °C /
12/20/2022 S Cintasl22022Self 30.8 /66 °C /
Jul 2022 Week 4 27 / °C /
Aug 2022 Week 3 21.2 / °C /
Sep 2022 Week 3 32.1 / °C /
Oct 2022 Week 2 34.4 / °C /
Nov 2022 Week 2 31.4 / °C /
Dec 2022 Week 3 30.8 / °C /
Jul 2022 Average 27 / °C /
Aug 2022 Average 21.2 / °C /
Monday,February 27,2023 4:23:55PM *Indicates Violation **Indicates TRC Violation Page 11 of 15

Cintas Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Temperature
Sep 2022 Average 32.1 / °C /
Oct 2022 Average 34.4 / °C /
Nov 2022 Average 31.4 / °C /
Dec 2022 Average 30.8 / °C /
2022 Quarter 3 26.8 / °C /
2022 Quarter 4 34.4 / °C /
2022 Quarter 4 31.1 / °C /
2022 Quarter 4 31.1 / °C /
2022 Quarter 4 34.4 / °C /
2022 2nd 6 Months(Avg) 29.1 / °C /
2022 2nd 6...(Max) 34.4 / °C /
2022 2nd 6...(Min) 21.2 / °C /
2022 2nd 6...(Count) 7
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 5
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass Mmit
TKN
07/26/2022 S Cintas072622Self 27.9 / mg/L 9.268 / lbs/day
07/28/2022 P Cintas072822POTW 35.4 / mg/L /
08/04/2022 P Cintas08O422POTW 27.8 / mg/L /
08/17/2022 S Cintas081722Self 26.1 / mg/L 14.431 / lbs/day
09/20/2022 P Cintas092022POTW 36.9 / mg/L /
09/20/2022 S Cintas092022Self 42.9 / mg/L 16.009 / lbs/day
10/11/2022 S Cintas101122Self 13.5 / mg/L 5.434 / lbs/day
10/19/2022 P Cintasl01922POTW 21.1 / mg/L /
11/08/2022 S Cintasl10822Self 61.8 / mg/L 23.466 / lbs/day
11/15/2022 P Cintasl11522POTW 48.3 / mg/L /
12/13/2022 P Cintas121322POTW 37 / mg/L /
12/13/2022 P Cintas021322POTW 37 / mg/L /
12/20/2022 S Cintasl22022Self 36.7 / mg/L 11.413 / lbs/day
Jul 2022 Week 4 31.65 / mg/L 9.268 / lbs/day
Aug 2022 Week 1 27.8 / mg/L /
Aug 2022 Week 3 26.1 / mg/L 14.431 / lbs/day
Sep 2022 Week 3 39.9 / mg/L 16.009 / lbs/day
Oct 2022 Week 2 13.5 / mg/L 5.434 / lbs/day
Monday,February 27,2023 4:23:55PM *Indicates Violation **Indicates TRC Violation Page 12 of 15

Cintas Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
TKN
Oct 2022 Week 3 21.1 / mg/L /
Nov 2022 Week 2 61.8 / mg/L 23.466 / lbs/day
Nov 2022 Week 3 48.3 / mg/L /
Dec 2022 Week 2 37 / mg/L /
Dec 2022 Week 3 36.7 / mg/L 11.413 / lbs/day
Jul 2022 Average 31.65 / mg/L 9.268 / lbs/day
Aug 2022 Average 26.95 / mg/L 14.431 / lbs/day
Sep 2022 Average 39.9 / mg/L 16.009 / lbs/day
Oct 2022 Average 17.3 / mg/L 5.434 / lbs/day
Nov 2022 Average 55.05 / mg/L 23.466 / lbs/day
Dec 2022 Average 36.9 / mg/L 11.413 / lbs/day
2022 Quarter 3 32.83 / mg/L 13.236 / lbs/day
2022 Quarter 4 17.3 / mg/L 5.434 / lbs/day
2022 Quarter 4 44.16 / mg/L 17.439 / lbs/day
2022 Quarter 4 44.16 / mg/L 17.439 / lbs/day
2022 Quarter 4 17.3 / mg/L 5.434 / lbs/day
2022 2nd 6 Months(Avg) 34.8 / mg/L 13.337 / lbs/day
2022 2nd 6...(Max) 61.8 / mg/L 23.466 / lbs/day
2022 2nd 6...(Min) 13.5 / mg/L /
2022 2nd 6...(Count) 13 / 6 /
Sample Date SampleID Result/Limit Mass/Limit
Total Phosphorus
07/26/2022 S Cintas072622Self 1.8 / mg/L 0.598 / lbs/day
07/28/2022 P Cintas072822POTW 4.03 / mg/L /
08/04/2022 P Cintas08O422POTW 2.69 / mg/L /
08/17/2022 S Cintas081722Self 3.5 / mg/L 1.9352 / lbs/day
09/20/2022 P Cintas092022POTW 3.95 / mg/L /
09/20/2022 S Cintas092022Self 4.3 / mg/L 1.6046 / lbs/day
10/11/2022 S Cintas101122Self 1.7 / mg/L 0.6843 / lbs/day
10/19/2022 P Cintasl01922POTW 4.49 / mg/L /
11/08/2022 S Cintasl10822Self 6.5 / mg/L 2.4681 / lbs/day
11/15/2022 P Cintasll1522POTW 4.29 / mg/L /
12/13/2022 P Cintas121322POTW 3.32 / mg/L /
12/13/2022 P Cintas021322POTW 3.32 / mg/L /
12/20/2022 S Cintasl22022Self 3.5 / mg/L 1.0884 / lbs/day
Jul 2022 Week 4 2.915 / mg/L 0.598 / lbs/day
Aug 2022 Week 1 2.69 / mg/L /
Aug 2022 Week 3 3.5 / mg/L 1.9352 / lbs/day
Sep 2022 Week 3 4.125 / mg/L 1.6046 / lbs/day
Oct 2022 Week 2 1.7 / mg/L 0.6843 / lbs/day
Oct 2022 Week 3 4.49 / mg/L /
Monday,February 27,2023 4:23:55PM *Indicates Violation **Indicates TRC Violation Page 13 of 15

Cintas Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Total Phosphorus
Nov 2022 Week 2 6.5 / mg/L 2.4681 / lbs/day
Nov 2022 Week 3 4.29 / mg/L /
Dec 2022 Week 2 3.32 / mg/L /
Dec 2022 Week 3 3.5 / mg/L 1.0884 / lbs/day
Jul 2022 Average 2.915 / mg/L 0.598 / lbs/day
Aug 2022 Average 3.095 / mg/L 1.9352 / lbs/day
Sep 2022 Average 4.125 / mg/L 1.6046 / lbs/day
Oct 2022 Average 3.095 / mg/L 0.6843 / lbs/day
Nov 2022 Average 5.395 / mg/L 2.4681 / lbs/day
Dec 2022 Average 3.38 / mg/L 1.0884 / lbs/day
2022 Quarter 3 3.378 / mg/L 1.3793 / lbs/day
2022 Quarter 4 3.095 / mg/L 0.6843 / lbs/day
2022 Quarter 4 4.186 / mg/L 1.7783 / lbs/day
2022 Quarter 4 4.186 / mg/L 1.7783 / lbs/day
2022 Quarter 4 3.095 / mg/L 0.6843 / lbs/day
2022 2nd 6 Months(Avg) 3.645 / mg/L 1.3964 / lbs/day
2022 2nd 6...(Max) 6.5 / mg/L 2.4681 / lbs/day
2022 2nd 6...(Min) 1.7 / mg/L /
2022 2nd 6...(Count) 13 / 6 /
Sample Date SampleID Result/Limit Mass Mmit
TSS
07/26/2022 S Cintas072622Self 204 / mg/L 67.768572 / lbs/day
07/28/2022 P Cintas072822POTW 208 / mg/L /
08/04/2022 P Cintas08O422POTW 180 / mg/L /
08/17/2022 S Cintas081722Self 137 / mg/L 75.750769 / lbs/day
09/20/2022 P Cintas092022POTW 115 / mg/L /
09/20/2022 S Cintas092022Self 113 / mg/L 42.16764 / lbs/day
10/11/2022 S Cintas101122Self 66.3 / mg/L 26.687193 / lbs/day
10/19/2022 P Cintasl01922POTW 232 / mg/L /
11/08/2022 S Cintasl10822Self 145 / mg/L 55.05701 / lbs/day
11/15/2022 P Cintas111522POTW 130 / mg/L /
12/13/2022 P Cintas121322POTW 220 / mg/L /
12/13/2022 P Cintas021322POTW 220 / mg/L /
12/20/2022 S Cintasl22022Self 329 / mg/L 102.313052 / lbs/day
Jul 2022 Week 4 206 / mg/L 67.768572 / lbs/day
Aug 2022 Week 1 180 / mg/L /
Aug 2022 Week 3 137 / mg/L 75.750769 / lbs/day
Sep 2022 Week 3 114 / mg/L 42.16764 / lbs/day
Oct 2022 Week 2 66.3 / mg/L 26.687193 / lbs/day
Oct 2022 Week 3 232 / mg/L /
Nov 2022 Week 2 145 / mg/L 55.05701 / lbs/day
Monday,February 27,2023 4:23:55PM *Indicates Violation **Indicates TRC Violation Page 14 of 15

Cintas Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
TSS
Nov 2022 Week 3 130 / mg/L /
Dec 2022 Week 2 220 / mg/L /
Dec 2022 Week 3 329 / mg/L 102.313052 / lbs/day
Jul 2022 Average 206 / mg/L 67.768572 / lbs/day
Aug 2022 Average 158.5 / mg/L 75.750769 / lbs/day
Sep 2022 Average 114 / mg/L 42.16764 / lbs/day
Oct 2022 Average 149.2 / mg/L 26.687193 / lbs/day
Nov 2022 Average 137.5 / mg/L 55.05701 / lbs/day
Dec 2022 Average 256.3 / mg/L 102.313052 / lbs/day
2022 Quarter 3 159.5 / mg/L 61.89566 / lbs/day
2022 Quarter 4 149.2 / mg/L 26.687193 / lbs/day
2022 Quarter 4 208.8 / mg/L 78.685031 / lbs/day
2022 Quarter 4 208.8 / mg/L 78.685031 / lbs/day
2022 Quarter 4 149.2 / mg/L 26.687193 / lbs/day
2022 2nd 6 Months(Avg) 176.9 / mg/L 61.624 / lbs/day
2022 2nd 6...(Max) 329 / mg/L 102.313052 / lbs/day
2022 2nd 6...(Min) 66.3 / mg/L /
2022 2nd 6...(Count) 13 / 6 /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
07/26/2022 S Cintas072622Self 1 / mg/L 0.332199 / lbs/day
08/17/2022 S Cintas081722Self 0.917 / mg/L 0.507033 / lbs/day
09/20/2022 S Cintas092022Self 0.65 / mg/L 0.242557 / lbs/day
10/11/2022 S Cintas101122Self 0.93 / mg/L 0.374345 / lbs/day
Jul 2022 Week 4 1 / mg/L 0.332199 / lbs/day
Aug 2022 Week 3 0.917 / mg/L 0.507033 / lbs/day
Sep 2022 Week 3 0.65 / mg/L 0.242557 / lbs/day
Oct 2022 Week 2 0.93 / mg/L 0.374345 / lbs/day
Jul 2022 Average 1 / mg/L 0.332199 / lbs/day
Aug 2022 Average 0.917 / mg/L 0.507033 / lbs/day
Sep 2022 Average 0.65 / mg/L 0.242557 / lbs/day
Oct 2022 Average 0.93 / mg/L 0.374345 / lbs/day
2022 Quarter 3 0.856 / mg/L 0.360596 / lbs/day
2022 Quarter 4 0.93 / mg/L 0.374345 / lbs/day
2022 2nd 6 Months(Avg) 0.874 / mg/L 0.364033 / lbs/day
2022 2nd 6...(Max) 1 / mg/L 0.507033 / lbs/day
2022 2nd 6...(Min) 0.65 / mg/L 0.242557 / lbs/day
2022 2nd 6...(Count) 4 / 4 /
Monday,February 27,2023 4:23:55PM *Indicates Violation **Indicates TRC Violation Page 15 of 15

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Aluminum
07/19/2022 S Micross071922Self 0.03 / mg/L 0.012416 / lbs/day
09/15/2022 P Micross091522POTW 0.021 / mg/L 0.008235 / lbs/day
Jul 2022 Week 3 0.03 / mg/L 0.012416 / lbs/day
Sep 2022 Week 3 0.021 / mg/L 0.008235 / lbs/day
Jul 2022 Average 0.03 / mg/L 0.012416 / lbs/day
Sep 2022 Average 0.021 / mg/L 0.008235 / lbs/day
2022 Quarter 3 0.026 / mg/L 0.010326 / lbs/day
2022 2nd 6 Months(Avg) 0.026 / mg/L 0.010326 / lbs/day
2022 2nd 6...(Max) 0.03 / mg/L 0.012416 / lbs/day
2022 2nd 6...(Min) 0.021 / mg/L 0.008235 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
07/19/2022 S Micross071922Self 3.1 / mg/L 1.283 / lbs/day
09/15/2022 P Micross091522POTW 3.7 / mg/L 1.4238 / lbs/day
Jul 2022 Week 3 3.1 / mg/L 1.283 / lbs/day
Sep 2022 Week 3 3.7 / mg/L 1.4238 / lbs/day
Jul 2022 Average 3.1 / mg/L 1.283 / lbs/day
Sep 2022 Average 3.7 / mg/L 1.4238 / lbs/day
2022 Quarter 3 3.4 / mg/L 1.3534 / lbs/day
2022 2nd 6 Months(Avg) 3.4 / mg/L 1.3534 / lbs/day
2022 2nd 6...(Max) 3.7 / mg/L 1.4238 / lbs/day
2022 2nd 6...(Min) 3.1 / mg/L 1.2830 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2022 S Micross0722F1ow 0.053525 /0.100 MGD /
08/31/2022 S Micross0822F1ow 0.051315 /0.100 MGD /
09/30/2022 S Micross0922F1ow 0.045624 /0.100 MGD /
10/31/2022 S Microssl022F1ow 0.039206 /0.100 MGD /
11/30/2022 S Microssll22F1ow 0.030206 /0.100 MGD /
12/31/2022 S Micross1222171ow 0.023056 /0.100 MGD /
Jul 2022 Week 4 0.053525 / MGD /
Aug 2022 Week 4 0.051315 / MGD /
Sep 2022 Week 4 0.045624 / MGD /
Oct 2022 Week 4 0.039206 / MGD /
Nov 2022 Week 4 0.030206 / MGD /
Dec 2022 Week 4 0.023056 / MGD /
Jul 2022 Average 0.053525 /0.075 MGD /
Aug 2022 Average 0.051315 /0.075 MGD /
Tuesday,February 21,2023 2:34:50PM *Indicates Violation **Indicates TRC Violation Page 1 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Sep 2022 Average 0.045624 /0.075 MGD /
Oct 2022 Average 0.039206 /0.075 MGD /
Nov 2022 Average 0.030206 /0.075 MGD /
Dec 2022 Average 0.023056 /0.075 MGD /
2022 Quarter 3 0.050155 / MGD /
2022 Quarter 4 0.030823 / MGD /
2022 2nd 6 Months(Avg) 0.040489 / MGD /
2022 2nd 6...(Max) 0.053525 / MGD /
2022 2nd 6...(Min) 0.023056 / MGD /
2022 2nd 6...(Count) 6
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
09/15/2022 P Micross091522POTW < 0.00008 / mg/L < 0.000029 / lbs/day
Sep 2022 Week 3 < 0.00008 / mg/L < 0.000029 / lbs/day
Sep 2022 Average < 0.00008 / mg/L < 0.000029 / lbs/day
2022 Quarter 3 < 0.00008 / mg/L < 0.000029 / lbs/day
2022 2nd 6 Months(Avg) < 0.00008 / mg/L < 0.000029 / lbs/day
2022 2nd 6...(Max) < 0.00008 / mg/L < 0.000029 / lbs/day
2022 2nd 6...(Min) < 0.00008 / mg/L < 0.000029 / lbs/day
2022 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
07/19/2022 S Micross071922Self 19 / mg/L 7.8636 / lbs/day
09/15/2022 P Micross091522POTW 28.5 / mg/L 10.9675 / lbs/day
Jul 2022 Week 3 19 / mg/L 7.8636 / lbs/day
Sep 2022 Week 3 28.5 / mg/L 10.9675 / lbs/day
Jul 2022 Average 19 / mg/L 7.8636 / lbs/day
Sep 2022 Average 28.5 / mg/L 10.9675 / lbs/day
2022 Quarter 3 23.75 / mg/L 9.4155 / lbs/day
2022 2nd 6 Months(Avg) 23.75 / mg/L 9.4155 / lbs/day
2022 2nd 6...(Max) 28.5 / mg/L 10.9675 / lbs/day
Tuesday,February 21,2023 2:34:50PM *Indicates Violation **Indicates TRC Violation Page 2 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: '001
Sample Date Sample-ID Result/Limit Mass/Limit
Chloride
2022 2nd 6...(Min) 19 / mg/L 7.8636 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SampleID Result/Limit Mass/Limit
Chromium
07/19/2022 S Micross071922Self 0.001 / mg/L 0.000372 / lbs/day
09/15/2022 P Micross091522POTW < 0.001 / mg/L < 0.000385 / lbs/day
Jul 2022 Week 3 0.001 / mg/L 0.000372 / lbs/day
Sep 2022 Week 3 < 0.001 / mg/L < 0.000385 / lbs/day
Jul 2022 Average 0.001 / mg/L 0.000372 / lbs/day
Sep 2022 Average < 0.001 / mg/L < 0.000385 / lbs/day
2022 Quarter 3 < 0.001 / mg/L < 0.000379 / lbs/day
2022 2nd 6 Months(Avg) < 0.001 / mg/L < 0.000379 / lbs/day
2022 2nd 6...(Max) < 0.001 / mg/L < 0.000385 / lbs/day
2022 2nd 6...(Min) 0.001 / mg/L 0.000372 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SampleID Result/Limit Mass/Limit
Copper
07/19/2022 S Micross071922Self 0.034 / mg/L 0.013906 / lbs/day
09/15/2022 P Micross091522POTW 0.025 / mg/L 0.009775 / lbs/day
Jul 2022 Week 3 0.034 / mg/L 0.013906 / lbs/day
Sep 2022 Week 3 0.025 / mg/L 0.009775 / lbs/day
Jul 2022 Average 0.034 / mg/L 0.013906 / lbs/day
Sep 2022 Average 0.025 / mg/L 0.009775 / lbs/day
2022 Quarter 3 0.03 / mg/L 0.01184 / lbs/day
2022 2nd 6 Months(Avg) 0.030 / mg/L 0.011840 / lbs/day
2022 2nd 6...(Max) 0.034 / mg/L 0.013906 / lbs/day
2022 2nd 6...(Min) 0.025 / mg/L 0.009775 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
09/15/2022 P Micross091522POTW < 0.003 / mg/L < 0.000962 / lbs/day
Sep 2022 Week 3 < 0.003 / mg/L < 0.000962 / lbs/day
Sep 2022 Average < 0.003 / mg/L < 0.000962 / lbs/day
2022 Quarter 3 < 0.003 / mg/L < 0.000962 / lbs/day
2022 2nd 6 Months(Avg) < 0.003 / mg/L < 0.000962 / lbs/day
2022 2nd 6...(Max) < 0.003 / mg/L < 0.000962 / lbs/day
2022 2nd 6...(Min) < 0.003 / mg/L < 0.000962 / lbs/day
2022 2nd 6...(Count) 1 / 1 /
Tuesday,February 21,2023 2:34:50PM *Indicates Violation **Indicates TRC Violation Page 3 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
07/19/2022 S Micross071922Self 1.7 / mg/L 0.7036 / lbs/day
09/15/2022 P Micross091522POTW 3.1 / mg/L 1.193 / lbs/day
Jul 2022 Week 3 1.7 / mg/L 0.7036 / lbs/day
Sep 2022 Week 3 3.1 / mg/L 1.193 / lbs/day
Jul 2022 Average 1.7 / mg/L 0.7036 / lbs/day
Sep 2022 Average 3.1 / mg/L 1.193 / lbs/day
2022 Quarter 3 2.4 / mg/L 0.9483 / lbs/day
2022 2nd 6 Months(Avg) 2.4 / mg/L 0.9483 / lbs/day
2022 2nd 6...(Max) 3.1 / mg/L 1.1930 / lbs/day
2022 2nd 6...(Min) 1.7 / mg/L 0.7036 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Lead
09/15/2022 P Micross091522POTW 0.0018 / mg/L 0.0007 / lbs/day
Sep 2022 Week 3 0.0018 / mg/L 0.0007 / lbs/day
Sep 2022 Average 0.0018 / mg/L 0.0007 / lbs/day
2022 Quarter 3 0.0018 / mg/L 0.0007 / lbs/day
2022 2nd 6 Months(Avg) 0.0018 / mg/L 0.000700 / lbs/day
2022 2nd 6...(Max) 0.0018 / mg/L 0.000700 / lbs/day
2022 2nd 6...(Min) 0.0018 / mg/L 0.000700 / lbs/day
2022 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
08/12/2022 S Micross081222Self1-lg 0.000004 /0.000142 mg/L /
11/04/2022 P Microssl10422POTW 0.000012 /0.000142 mg/L /
Hg
Aug 2022 Week 2 0.000004 / mg/L /
Nov 2022 Week 1 0.000012 / mg/L /
Aug 2022 Average 0.000004 / mg/L /
Nov 2022 Average 0.000012 / mg/L /
2022 Quarter 3 0.000004 / mg/L /
2022 Quarter 4 0.000012 / mg/L /
2022 2nd 6 Months(Avg) 0.000008 / mg/L /
2022 2nd 6...(Max) 0.000012 / mg/L /
2022 2nd 6...(Min) 0.000004 / mg/L /
2022 2nd 6...(Count) 2 / /
Tuesday,February 21,2023 2:34:50PM *Indicates Violation **Indicates TRC Violation Page 4 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: '001
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
09/15/2022 P Micross091522POTW 0.007 / mg/L 0.0028 / lbs/day
Sep 2022 Week 3 0.007 / mg/L 0.0028 / lbs/day
Sep 2022 Average 0.007 / mg/L 0.0028 / lbs/day
2022 Quarter 3 0.007 / mg/L 0.0028 / lbs/day
2022 2nd 6 Months(Avg) 0.007 / mg/L 0.0028 / lbs/day
2022 2nd 6...(Max) 0.007 / mg/L 0.0028 / lbs/day
2022 2nd 6...(Min) 0.007 / mg/L 0.0028 / lbs/day
2022 2nd 6...(Count) 1 / 1 /
Sample Date SampleID Result/Limit Mass/Limit
Nickel
07/19/2022 S Micross071922Self 0.018 / mg/L 0.00745 / lbs/day
09/15/2022 P Micross091522POTW 0.0063 / mg/L 0.002405 / lbs/day
Jul 2022 Week 3 0.018 / mg/L 0.00745 / lbs/day
Sep 2022 Week 3 0.0063 / mg/L 0.002405 / lbs/day
Jul 2022 Average 0.018 / mg/L 0.00745 / lbs/day
Sep 2022 Average 0.0063 / mg/L 0.002405 / lbs/day
2022 Quarter 3 0.0121 / mg/L 0.004927 / lbs/day
2022 2nd 6 Months(Avg) 0.0121 / mg/L 0.004927 / lbs/day
2022 2nd 6...(Max) 0.018 / mg/L 0.007450 / lbs/day
2022 2nd 6...(Min) 0.0063 / mg/L 0.002405 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
07/19/2022 S Micross071922Self 1.2 / mg/L 0.497 / lbs/day
09/15/2022 P Micross091522POTW 0.9 / mg/L 0.346 / lbs/day
Jul 2022 Week 3 1.2 / mg/L 0.497 / lbs/day
Sep 2022 Week 3 0.9 / mg/L 0.346 / lbs/day
Jul 2022 Average 1.2 / mg/L 0.497 / lbs/day
Sep 2022 Average 0.9 / mg/L 0.346 / lbs/day
2022 Quarter 3 1.1 / mg/L 0.421 / lbs/day
2022 2nd 6 Months(Avg) 1.1 / mg/L 0.421 / lbs/day
Tuesday,February 21,2023 2:34:50PM *Indicates Violation **Indicates TRC Violation Page 5 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
2022 2nd 6...(Max) 1.2 / mg/L 0.497 / lbs/day
2022 2nd 6...(Min) 0.9 / mg/L 0.346 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SampleID Result/Limit Mass/Limit
Nitrogen,Total
09/15/2022 P Micross091522POTW 7.67 / mg/L 2.952 / lbs/day
Sep 2022 Week 3 7.67 / mg/L 2.952 / lbs/day
Sep 2022 Average 7.67 / mg/L 2.952 / lbs/day
2022 Quarter 3 7.67 / mg/L 2.952 / lbs/day
2022 2nd 6 Months(Avg) 7.67 / mg/L 2.952 / lbs/day
2022 2nd 6...(Max) 7.67 / mg/L 2.952 / lbs/day
2022 2nd 6...(Min) 7.67 / mg/L 2.952 / lbs/day
2022 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
09/15/2022 P Micross091522POTW < 2.5 /200 mg/L < /
Sep 2022 Week 3 < 2.5 / mg/L < /
Sep 2022 Average < 2.5 / mg/L < /
2022 Quarter 3 < 2.5 / mg/L < /
2022 2nd 6 Months(Avg) < 2.5 / mg/L < /
2022 2nd 6...(Max) < 2.5 / mg/L < /
2022 2nd 6...(Min) < 2.5 / mg/L < /
2022 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
07/19/2022 S Micross071922Self 6.3 /5.5-10.5 SU /
08/12/2022 S Micross08l222SelfHg 6.8 /5.5-10.5 SU /
09/15/2022 P Micross091522POTW 6.8 /5.5-10.5 SU /
Jul 2022 Week 3 6.3 / SU /
Aug 2022 Week 2 6.8 / SU /
Tuesday,February 21,2023 2:34:50PM *Indicates Violation **Indicates TRC Violation Page 6 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: '001
Sample Date Sample-ID Result/Limit Mass/Limit
pH
Sep 2022 Week 3 6.8 / SU /
Jul 2022 Average 6.3 / SU /
Aug 2022 Average 6.8 / SU /
Sep 2022 Average 6.8 / SU /
2022 Quarter 3 6.63 / SU /
2022 2nd 6 Months(Avg) 6.63 / SU /
2022 2nd 6...(Max) 6.8 / SU /
2022 2nd 6...(Min) 6.3 / SU /
2022 2nd 6...(Count) 3
Sample Count: 3 Months Sampled: 3 Weeks Sampled: 3 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Selenium
09/15/2022 P Micross091522POTW < 0.0005 / mg/L < 0.000192 / lbs/day
Sep 2022 Week 3 < 0.0005 / mg/L < 0.000192 / lbs/day
Sep 2022 Average < 0.0005 / mg/L < 0.000192 / lbs/day
2022 Quarter 3 < 0.0005 / mg/L < 0.000192 / lbs/day
2022 2nd 6 Months(Avg) < 0.0005 / mg/L < 0.000192 / lbs/day
2022 2nd 6...(Max) < 0.0005 / mg/L < 0.000192 / lbs/day
2022 2nd 6...(Min) < 0.0005 / mg/L < 0.000192 / lbs/day
2022 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Silver
09/15/2022 P Micross091522POTW < 0.0003 / mg/L < 0.000096 / lbs/day
Sep 2022 Week 3 < 0.0003 / mg/L < 0.000096 / lbs/day
Sep 2022 Average < 0.0003 / mg/L < 0.000096 / lbs/day
2022 Quarter 3 < 0.0003 / mg/L < 0.000096 / lbs/day
2022 2nd 6 Months(Avg) < 0.0003 / mg/L < 0.000096 / lbs/day
2022 2nd 6...(Max) < 0.0003 / mg/L < 0.000096 / lbs/day
2022 2nd 6...(Min) < 0.0003 / mg/L < 0.000096 / lbs/day
2022 2nd 6...(Count) 1 / 1 /
Tuesday,February 21,2023 2:34:50PM *Indicates Violation **Indicates TRC Violation Page 7 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SampleID Result/Limit Mass/Limit
Temperature
07/19/2022 S Micross071922Self 23.3 /66 °C /
08/12/2022 S Micross081222Self lg 21.7 /66 °C /
09/15/2022 P Micross091522POTW 26 /66 °C /
Jul 2022 Week 3 23.3 / °C /
Aug 2022 Week 2 21.7 / °C /
Sep 2022 Week 3 26 / °C /
Jul 2022 Average 23.3 / °C /
Aug 2022 Average 21.7 / °C /
Sep 2022 Average 26 / °C /
2022 Quarter 3 23.7 / °C /
2022 2nd 6 Months(Avg) 23.7 / °C /
2022 2nd 6...(Max) 26 / °C /
2022 2nd 6...(Min) 21.7 / °C /
2022 2nd 6...(Count) 3
T
Sample Count: 3 Months Sampled: 3 Weeks Sampled: 3 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Tin
07/19/2022 S Micross071922Self 0.007000000 / mg/L 0.002897108 / lbs/day
Jul 2022 Week 3 0 / mg/L 0 / lbs/day
Jul 2022 Average 0 / mg/L 0 / lbs/day
2022 Quarter 3 0 / mg/L 0 / lbs/day
2022 2nd 6 Months(Avg) 0 / mg/L 0 / lbs/day
2022 2nd 6...(Max) 0 / mg/L 0 / lbs/day
2022 2nd 6...(Min) 0 / mg/L 0 / lbs/day
2022 2nd 6...(Count) 1 / 1 /
Sample Date SampleID Result/Limit Mass/Limit
TKN
07/19/2022 S Micross071922Self 6.9 / mg/L 2.856 / lbs/day
09/15/2022 P Micross091522POTW 6.77 / mg/L 2.605 / lbs/day
Jul 2022 Week 3 6.9 / mg/L 2.856 / lbs/day
Sep 2022 Week 3 6.77 / mg/L 2.605 / lbs/day
Jul 2022 Average 6.9 / mg/L 2.856 / lbs/day
Tuesday,February 21,2023 2:34:50PM *Indicates Violation **Indicates TRC Violation Page 8 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: '001
Sample Date Sample-ID Result/Limit Mass/Limit
TKN
Sep 2022 Average 6.77 / mg/L 2.605 / lbs/day
2022 Quarter 3 6.84 / mg/L 2.73 / lbs/day
2022 2nd 6 Months(Avg) 6.84 / mg/L 2.730 / lbs/day
2022 2nd 6...(Max) 6.9 / mg/L 2.856 / lbs/day
2022 2nd 6...(Min) 6.77 / mg/L 2.605 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SampleID Result/Limit Mass/Limit
Total Phosphorus
09/15/2022 P Micross091522POTW 4.46 / mg/L 1.7163 / lbs/day
Sep 2022 Week 3 4.46 / mg/L 1.7163 / lbs/day
Sep 2022 Average 4.46 / mg/L 1.7163 / lbs/day
2022 Quarter 3 4.46 / mg/L 1.7163 / lbs/day
2022 2nd 6 Months(Avg) 4.46 / mg/L 1.7163 / lbs/day
2022 2nd 6...(Max) 4.46 / mg/L 1.7163 / lbs/day
2022 2nd 6...(Min) 4.46 / mg/L 1.7163 / lbs/day
2022 2nd 6...(Count) 1 / 1 /
Sample Date Sample-ID Result/Limit Mass/Limit
Zinc
07/19/2022 S Micross071922Self 0.559 / mg/L 0.231355 / lbs/day
09/15/2022 P Micross091522POTW 0.322 / mg/L 0.123913 / lbs/day
Jul 2022 Week 3 0.559 / mg/L 0.231355 / lbs/day
Sep 2022 Week 3 0.322 / mg/L 0.123913 / lbs/day
Jul 2022 Average 0.559 / mg/L 0.231355 / lbs/day
Sep 2022 Average 0.322 / mg/L 0.123913 / lbs/day
2022 Quarter 3 0.441 / mg/L 0.177634 / lbs/day
2022 2nd 6 Months(Avg) 0.441 / mg/L 0.177634 / lbs/day
2022 2nd 6...(Max) 0.559 / mg/L 0.231355 / lbs/day
2022 2nd 6...(Min) 0.322 / mg/L 0.123913 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Tuesday,February 21,2023 2:34:50PM *Indicates Violation **Indicates TRC Violation Page 9 of 9

MP Pharma Services, Inc.
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
09/16/2022 S MPPharma09l622Se 0.035 / 20.7 mg/L /
if
10/03/2022 P MPPharmal00322P < 0.025 / 20.7 mg/L < /
OTW
Sep 2022 Week 3 0.035 / mg/L /
Oct 2022 Week 1 < 0.025 / mg/L < /
Sep 2022 Average 0.035 / 8.2 mg/L /
Oct 2022 Average < 0.025 / 8.2 mg/L < /
2022 Quarter 3 0.035 / mg/L /
2022 Quarter 4 < 0.025 / mg/L < /
2022 2nd 6 Months(Avg) < 0.030 / mg/L < /
2022 2nd 6...(Max) 0.035 / mg/L /
2022 2nd 6...(Min) < 0.025 / mg/L < /
2022 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2022 S MPPharma0722F1ow 0.002061 / MGD /
08/31/2022 S MPPharma0822F1ow 0.001661 / MGD /
09/30/2022 S MPPhartna0922F1ow 0.001834 / MGD /
10/31/2022 S MPPharmal022F1ow 0.001937 / MGD /
11/30/2022 S MPPharmal122F1ow 0.001217 / MGD /
12/31/2022 S MPPharmal222F1ow 0.001213 / MGD /
Jul 2022 Week 4 0.002061 / MGD /
Aug 2022 Week 4 0.001661 / MGD /
Sep 2022 Week 4 0.001834 / MGD /
Oct 2022 Week 4 0.001937 / MGD /
Nov 2022 Week 4 0.001217 / MGD /
Dec 2022 Week 4 0.001213 / MGD /
Ju12022 Average 0.002061 / 0.002 MGD * /
Aug 2022 Average 0.001661 / 0.002 MGD /
Sep 2022 Average 0.001834 / 0.002 MGD /
Oct 2022 Average 0.001937 / 0.002 MGD /
Nov 2022 Average 0.001217 / 0.002 MGD /
Dec 2022 Average 0.001213 / 0.002 MGD /
2022 Quarter 3 0.001852 / MGD /
2022 Quarter 4 0.001456 / MGD /
2022 2nd 6 Months(Avg) 0.001654 / MGD /
Tuesday,February 21,2023 10:58:57PM *Indicates Violation **Indicates TRC Violation Page 1 of 5

MP Pharma Services, Inc.
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
2022 2nd 6...(Max) 0.002061 / MGD /
2022 2nd 6...(Min) 0.001213 / MGD /
2022 2nd 6...(Count) 6 / /
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
09/16/2022 S MPPharma091622Se < 0.05 / 20.7 mg/L < /
if
10/03/2022 P MPPharma100322P < 0.005 / 20.7 mg/L < /
OTW
Sep 2022 Week 3 < 0.05 / mg/L < /
Oct 2022 Week I < 0.005 / mg/L < /
Sep 2022 Average < 0.05 / 8.2 mg/L < /
Oct 2022 Average < 0.005 / 8.2 mg/L < /
2022 Quarter 3 < 0.05 / mg/L < /
2022 Quarter 4 < 0.005 / mg/L < /
2022 2nd 6 Months(Avg) < 0.028 / mg/L < /
2022 2nd 6...(Max) < 0.05 / mg/L < /
2022 2nd 6...(Min) < 0.005 / mg/L < /
2022 2nd 6...(Count) 2 / /
Sample Date SampleID Result/Limit Mass/Limit
Isopropyl acetate
09/16/2022 S MPPhartna09l622Se < 0.05 / 20.7 mg/L < /
if
10/03/2022 P MPPharma100322P < 0.005 / 20.7 mg/L < /
OTW
Sep 2022 Week 3 < 0.05 / mg/L < /
Oct 2022 Week 1 < 0.005 / mg/L < /
Sep 2022 Average < 0.05 / 8.2 mg/L < /
Oct 2022 Average < 0.005 / 8.2 mg/L < /
2022 Quarter 3 < 0.05 / mg/L < /
2022 Quarter 4 < 0.005 / mg/L < /
2022 2nd 6 Months(Avg) < 0.028 / mg/L < /
2022 2nd 6...(Max) < 0.05 / mg/L < /
2022 2nd 6...(Min) < 0.005 / mg/L < /
2022 2nd 6...(Count) 2 / /
Tuesday,February 21,2023 10:58:57PM *Indicates Violation **Indicates TRC Violation Page 2 of 5

MP Pharma Services, Inc.
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
09/16/2022 S MPPharma09l622Se 0.000002 / 0.000142 mg/L /
if
10/03/2022 P MPPharma100322P 0.000001 / 0.000142 mg/L /
OTWHg
Sep 2022 Week 3 0.000002 / mg/L /
Oct 2022 Week 1 0.000001 / mg/L /
Sep 2022 Average 0.000002 / mg/L /
Oct 2022 Average 0.000001 / mg/L /
2022 Quarter 3 0.000002 / mg/L /
2022 Quarter 4 0.000001 / mg/L /
2022 2nd 6 Months(Avg) 0.000002 / mg/L /
2022 2nd 6...(Max) 0.000002 / mg/L /
2022 2nd 6...(Min) 0.000001 / mg/L /
2022 2nd 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
09/16/2022 S MPPharma091622Se < 0.003 / 3.0 mg/L < /
if
10/03/2022 P MPPharma100322P < 0.005 / 3.0 mg/L < /
OTW
Sep 2022 Week 3 < 0.003 / mg/L < /
Oct 2022 Week 1 < 0.005 / mg/L < /
Sep 2022 Average < 0.003 / 0.7 mg/L < /
Oct 2022 Average < 0.005 / 0.7 mg/L < /
2022 Quarter 3 < 0.003 / mg/L < /
2022 Quarter 4 < 0.005 / mg/L < /
2022 2nd 6 Months(Avg) < 0.004 / mg/L < /
2022 2nd 6...(Max) < 0.005 / mg/L < /
2022 2nd 6...(Min) < 0.003 / mg/L < /
2022 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
09/16/2022 S MPPhanna09l622Se < 0.025 / 20.7 mg/L < /
if
10/03/2022 P MPPharma100322P < 0.005 / 20.7 mg/L < /
OTW
Sep 2022 Week 3 < 0.025 / mg/L < /
Oct 2022 Week 1 < 0.005 / mg/L < /
Tuesday,February 21,2023 10:58:57PM *Indicates Violation **Indicates TRC Violation Page 3 of 5

MP Pharma Services, Inc.
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
Sep 2022 Average < 0.025 / 8.2 mg/L < /
Oct 2022 Average < 0.005 / 8.2 mg/L < /
2022 Quarter 3 < 0.025 / mg/L < /
2022 Quarter 4 < 0.005 / mg/L < /
2022 2nd 6 Months(Avg) < 0.015 / mg/L < /
2022 2nd 6...(Max) < 0.025 / mg/L < /
2022 2nd 6...(Min) < 0.005 / mg/L < /
2022 2nd 6...(Count) 2 / /
Sample Date SampleID Result/Limit Mass/Limit
PH
09/16/2022 S MPPharma091622Se 7.4 / 6.0-10.0 su /
if
10/03/2022 P MPPharma100322P 7.2 / 6.0-10.0 su /
OTW
Sep 2022 Week 3 7.4 / su /
Oct 2022 Week 1 7.2 / su /
Sep 2022 Average 7.4 / Su /
Oct 2022 Average 7.2 / su /
2022 Quarter 3 7.4 / su /
2022 Quarter 4 7.2 / su /
2022 2nd 6 Months(Avg) 7.3 / su /
2022 2nd 6...(Max) 7.4 / su /
2022 2nd 6...(Min) 7.2 / su /
2022 2nd 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
09/16/2022 S MPPhanna09l622Se 24.7 / 66 °C /
if
10/03/2022 P MPPharma100322P 22 / 66 °C /
OTW
Sep 2022 Week 3 24.7 / °C /
Oct 2022 Week 1 22 / °C /
Sep 2022 Average 24.7 / °C /
Oct 2022 Average 22 / °C /
2022 Quarter 3 24.7 / °C /
2022 Quarter 4 22 / °C /
2022 2nd 6 Months(Avg) 23.4 / °C /
Tuesday,February 21,2023 10:58:57PM *Indicates Violation **Indicates TRC Violation Page 4 of 5

MP Pharma Services, Inc.
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
2022 2nd 6...(Max) 24.7 / °C /
2022 2nd 6...(Min) 22 / °C /
2022 2nd 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
VOC
09/16/2022 S MPPhartna09l622Se 0.0478 / mg/L /
if
Sep 2022 Week 3 0.0478 / mg/L /
Sep 2022 Average 0.0478 / mg/L /
2022 Quarter 3 0.0478 / mg/L /
2022 2nd 6 Months(Avg) 0.0478 / mg/L /
2022 2nd 6...(Max) 0.0478 / mg/L /
2022 2nd 6...(Min) 0.0478 / mg/L /
2022 2nd 6...(Count) 1
Tuesday,February 21,2023 10:58:57PM *Indicates Violation **Indicates TRC Violation Page 5 of 5

Phononic
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Average Flow for Month
07/31/2022 S Phononic0722F1ow 0.026 / MGD /
08/31/2022 S Phononic0822F1ow 0.026 / MGD /
09/30/2022 S Phononic0922F1ow 0.029934 / MGD /
10/31/2022 S Phononic1022F1ow 0.015867 / MGD /
11/30/2022 S PhononicI122F1ow 0.015549 / MGD /
12/31/2022 S Phononicl222F1ow 0.009309 / MGD /
Jul 2022 Week 4 0.026 / MGD /
Aug 2022 Week 4 0.026 / MGD /
Sep 2022 Week 4 0.029934 / MGD /
Oct 2022 Week 4 0.015867 / MGD /
Nov 2022 Week 4 0.015549 / MGD /
Dec 2022 Week 4 0.009309 / MGD /
Jul 2022 Average 0.026 /0.020 MGD * /
Aug 2022 Average 0.026 /0.020 MGD * /
Sep 2022 Average 0.029934 /0.020 MGD * /
Oct 2022 Average 0.015867 /0.020 MGD /
Nov 2022 Average 0.015549 /0.020 MGD /
Dec 2022 Average 0.009309 /0.020 MGD /
2022 Quarter 3 0.027311 / MGD /
2022 Quarter 4 0.013575 / MGD /
2022 2nd 6 Months(Avg) 0.020443 / MGD /
2022 2nd 6...(Max) 0.029934 / MGD /
2022 2nd 6...(Min) 0.009309 / MGD /
2022 2nd 6...(Count) 6
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 3 50.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Bismuth
07/07/2022 S Phononic07O722Self 0.161 / mg/L /
07/08/2022 S Phononic07O822Self 0.147 / mg/L /
07/28/2022 S Phononic072822Self 0.071 / mg/L /
08/01/2022 P Phononic080122POT 0.193 / mg/L /
W
09/01/2022 S Phononic090122Self 0.013 / mg/L /
10/07/2022 S Phononicl00722Self 0.046 / mg/L /
Monday,February 27,2023 4:55:14PM *Indicates Violation **Indicates TRC Violation Page 1 of 6

Phononic
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Bismuth
10/31/2022 S Phononic103122Self 0.01 / mg/L /
11/29/2022 S Phononic112922Self 0.008 / mg/L /
12/16/2022 S Phononic121622Self < 0.003 / mg/L < /
Jul 2022 Week 1 0.161 / mg/L /
Jul 2022 Week 2 0.147 / mg/L /
Jul 2022 Week 4 0.071 / mg/L /
Aug 2022 Week 1 0.193 / mg/L /
Sep 2022 Week 1 0.013 / mg/L /
Oct 2022 Week 1 0.046 / mg/L /
Oct 2022 Week 4 0.01 / mg/L /
Nov 2022 Week 4 0.008 / mg/L /
Dec 2022 Week 3 < 0.003 / mg/L < /
Jul 2022 Average 0.126 / mg/L /
Aug 2022 Average 0.193 / mg/L /
Sep 2022 Average 0.013 / mg/L /
Oct 2022 Average 0.028 / mg/L /
Nov 2022 Average 0.008 / mg/L /
Dec 2022 Average < 0.003 / mg/L < /
2022 Quarter 3 0.117 / mg/L /
2022 Quarter 4 < 0.017 / mg/L < /
2022 2nd 6 Months(Avg) < 0.072 / mg/L < /
2022 2nd 6...(Max) 0.193 / mg/L /
2022 2nd 6...(Min) < 0.003 / mg/L < /
2022 2nd 6...(Count) 9 / /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
08/01/2022 P Phononic080122POT 0.000002 /0.000142 mg/L /
WHg
10/26/2022 S Phononic102622SelfH < 0.000001 /0.000142 mg/L < /
g
Aug 2022 Week 1 0.000002 / mg/L /
Oct 2022 Week 4 < 0.000001 / mg/L < /
Aug 2022 Average 0.000002 / mg/L /
Oct 2022 Average < 0.000001 / mg/L < /
2022 Quarter 3 0.000002 / mg/L /
2022 Quarter 4 < 0.000001 / mg/L < /
2022 2nd 6 Months(Avg) < 0.000001 / mg/L < /
2022 2nd 6...(Max) 0.000002 / mg/L /
2022 2nd 6...(Min) < 0.000001 / mg/L < /
2022 2nd 6...(Count) 2
Monday,February 27,2023 4:55:14PM *Indicates Violation **Indicates TRC Violation Page 2 of 6

Phononic
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Molybdenum
08/01/2022 P Phononic080122POT < 0.001 / mg/L < 0.0002 / lbs/day
W
10/26/2022 S Phononic102622Self < 0.003 / mg/L < /
Aug 2022 Week 1 < 0.001 / mg/L < 0.0002 / lbs/day
Oct 2022 Week 4 < 0.003 / mg/L < /
Aug 2022 Average < 0.001 / mg/L < 0.0002 / lbs/day
Oct 2022 Average < 0.003 / mg/L < /
2022 Quarter 3 < 0.001 / mg/L < 0.0002 / lbs/day
2022 Quarter 4 < 0.003 / mg/L < /
2022 2nd 6 Months(Avg) < 0.002 / mg/L < 0.0002 / lbs/day
2022 2nd 6...(Max) < 0.003 / mg/L < 0.0002 / lbs/day
2022 2nd 6...(Min) < 0.001 / mg/L < /
2022 2nd 6...(Count) 2 / 1 /
Sample Date SampleID Result/Limit Mass/Limit
Nickel
07/07/2022 S Phononic070722Se1f 0.102 / mg/L 0.027222 / 0.02 lbs/day * *
07/08/2022 S Phononic070822Se1f 0.107 / mg/L 0.02231 / 0.02 lbs/day *
07/28/2022 S Phononic072822Self 0.282 / mg/L 0.061149 / 0.02 lbs/day * *
08/01/2022 P Phononic080122POT 0.858 / mg/L 0.186049 / 0.02 lbs/day * *
W
09/01/2022 S Phononic090122Self < 0.0003 / mg/L < 0.000054 / 0.02 lbs/day
10/07/2022 S Phononicl00722Self 0.143 / mg/L 0.018923 / 0.02 lbs/day
10/31/2022 S Phononic103122Self 0.098 / mg/L 0.012968 / 0.02 lbs/day
11/01/2022 S Phononictl0122Self 0.075 / mg/L 0.009726 / 0.02 lbs/day
11/29/2022 S Phononicll2922Self 0.033 / mg/L 0.004279 / 0.02 lbs/day
12/06/2022 S Phononic120622Self 0.022 / mg/L 0.003033 / 0.02 lbs/day
12/13/2022 S Phononic121322Self 0.024 / mg/L 0.003776 / 0.02 lbs/day
12/16/2022 S Phononic121622Self 0.037 / mg/L 0.002873 / 0.02 lbs/day
12/20/2022 S Phononicl22022Self 0.016 / mg/L 0.002724 / 0.02 lbs/day
Jul 2022 Week 1 0.102 / mg/L 0.027222 / lbs/day
Jul 2022 Week 2 0.107 / mg/L 0.02231 / lbs/day
Jul 2022 Week 4 0.282 / mg/L 0.061149 / lbs/day
Aug 2022 Week 1 0.858 / mg/L 0.186049 / lbs/day
Sep 2022 Week 1 < 0.0003 / mg/L < 0.000054 / lbs/day
Monday,February 27,2023 4:55:14PM *Indicates Violation **Indicates TRC Violation Page 3 of 6

Phononic
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Nickel
Oct 2022 Week 1 0.143 / mg/L 0.018923 / lbs/day
Nov 2022 Week 1 0.075 / mg/L 0.009726 / lbs/day
Oct 2022 Week 4 0.098 / mg/L 0.012968 / lbs/day
Nov 2022 Week 4 0.033 / mg/L 0.004279 / lbs/day
Dec 2022 Week 1 0.022 / mg/L 0.003033 / lbs/day
Dec 2022 Week 2 0.024 / mg/L 0.003776 / lbs/day
Dec 2022 Week 3 0.0265 / mg/L 0.002798 / lbs/day
Jul 2022 Average 0.1637 / mg/L 0.036893 / lbs/day
Aug 2022 Average 0.858 / mg/L 0.186049 / lbs/day
Sep 2022 Average < 0.0003 / mg/L < 0.000054 / lbs/day
Oct 2022 Average 0.1205 / mg/L 0.015946 / lbs/day
Nov 2022 Average 0.054 / mg/L 0.007003 / lbs/day
Dec 2022 Average 0.0248 / mg/L 0.003101 / lbs/day
2022 Quarter 3 < 0.2699 / mg/L < 0.059357 / lbs/day
2022 Quarter 4 0.056 / mg/L 0.007288 / lbs/day
2022 2nd 6 Months(Avg) < 0.1383 / mg/L < 0.027314 / lbs/day
2022 2nd 6...(Max) 0.858 / mg/L 0.186049 / lbs/day
2022 2nd 6...(Min) < 0.0003 / mg/L < 0.000054 / lbs/day
2022 2nd 6...(Count) 13 / 13 /
Sample Count: 13 Months Sampled: 6 Weeks Sampled: 12 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 4 30.77 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 3 23.08 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
08/01/2022 P Phononic080122POT 8.4 /5.5-10 SU /
W
10/24/2022 S Phononic 102422 Self 6.5 /5.5- 10 SU /
Aug 2022 Week 1 8.4 / SU /
Oct 2022 Week 4 6.5 / SU /
Aug 2022 Average 8.4 / SU /
Oct 2022 Average 6.5 / SU /
2022 Quarter 3 8.4 / SU /
2022 Quarter 4 6.5 / SU /
2022 2nd 6 Months(Avg) 7.45 / SU /
2022 2nd 6...(Max) 8.4 / SU /
2022 2nd 6...(Min) 6.5 / SU /
Monday,February 27,2023 4:55:14PM *Indicates Violation **Indicates TRC Violation Page 4 of 6

Phononic
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
pH
2022 2nd 6...(Count) 2
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Tellurium
07/07/2022 S Phononic07O722Self 0.194 / mg/L /
07/08/2022 S Phononic07O822Self 0.176 / mg/L /
07/28/2022 S Phononic072822Self 0.425 / mg/L /
08/01/2022 P Phononic080122POT 0.502 / mg/L /
W
09/01/2022 S Phononic090122Self 0.023 / mg/L /
10/07/2022 S Phononicl00722Self 0.183 / mg/L /
10/31/2022 S Phononic103122Self 0.172 / mg/L /
11/29/2022 S Phononicll2922Self 0.027 / mg/L /
12/16/2022 S Phononic121622Self 0.011 / mg/L /
Jul 2022 Week 1 0.194 / mg/L /
Jul 2022 Week 2 0.176 / mg/L /
Aug 2022 Week 1 0.502 / mg/L /
Jul 2022 Week 4 0.425 / mg/L /
Sep 2022 Week 1 0.023 / mg/L /
Oct 2022 Week 1 0.183 / mg/L /
Oct 2022 Week 4 0.172 / mg/L /
Nov 2022 Week 4 0.027 / mg/L /
Dec 2022 Week 3 0.011 / mg/L /
Jul 2022 Average 0.265 / mg/L /
Aug 2022 Average 0.502 / mg/L /
Sep 2022 Average 0.023 / mg/L /
Oct 2022 Average 0.178 / mg/L /
Nov 2022 Average 0.027 / mg/L /
Dec 2022 Average 0.011 / mg/L /
2022 Quarter 3 0.264 / mg/L /
2022 Quarter 4 0.098 / mg/L /
2022 2nd 6 Months(Avg) 0.190 / mg/L /
2022 2nd 6...(Max) 0.502 / mg/L /
2022 2nd 6...(Min) 0.011 / mg/L /
Monday,February 27,2023 4:55:14PM *Indicates Violation **Indicates TRC Violation Page 5 of 6

Phononic
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Tellurium
2022 2nd 6...(Count) 9
Sample Date SamplelD Result/Limit Mass/Limit
TTO
08/01/2022 P Phononic080122POT < 0.25 / 1.37 mg/L < 0.05421 / lbs/day
W
10/24/2022 S Phononic102422Self < 0.005 / 1.37 mg/L < /
Aug 2022 Week 1 < 0.25 / mg/L < 0.05421 / lbs/day
Oct 2022 Week 4 < 0.005 / mg/L < /
Aug 2022 Average < 0.25 / mg/L < 0.05421 / lbs/day
Oct 2022 Average < 0.005 / mg/L < /
2022 Quarter 3 < 0.25 / mg/L < 0.05421 / lbs/day
2022 Quarter 4 < 0.005 / mg/L < /
2022 2nd 6 Months(Avg) < 0.1275 / mg/L < 0.05421 / lbs/day
2022 2nd 6...(Max) < 0.25 / mg/L < 0.05421 / lbs/day
2022 2nd 6...(Min) < 0.005 / mg/L < /
2022 2nd 6...(Count) 2 / 1 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Monday,February 27,2023 4:55:14PM *Indicates Violation **Indicates TRC Violation Page 6 of 6

PowerSecure
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Aluminum
08/23/2022 S PowerSecure082322Se 2.4 / mg/L /
if
09/08/2022 P PowerSecure09O822P 4.01 / mg/L /
OTW
Aug 2022 Week 4 2.4 / mg/L /
Sep 2022 Week 2 4.01 / mg/L /
Aug 2022 Average 2.4 / mg/L /
Sep 2022 Average 4.01 / mg/L /
2022 Quarter 3 3.205 / mg/L /
2022 2nd 6 Months(Avg) 3.205 / mg/L /
2022 2nd 6...(Max) 4.01 / mg/L /
2022 2nd 6...(Min) 2.4 / mg/L /
2022 2nd 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2022 S PowerSecure0722F1ow 0.000031 / MGD /
08/31/2022 S PowerSecure0822F1ow 0.000077 / MGD /
09/30/2022 S PowerSecure0922F1ow 0.004304 / MGD /
10/20/2022 S PowerSecurel022F1ow 0.004396 / MGD /
11/17/2022 S PowerSecurell22FIow 0.004078 / MGD /
12/31/2022 S PowerSecurel222F1ow 0.001489 / MGD /
Jul 2022 Week 4 0.000031 / MGD /
Aug 2022 Week 4 0.000077 / MGD /
Sep 2022 Week 4 0.004304 / MGD /
Oct 2022 Week 3 0.004396 / MGD /
Nov 2022 Week 3 0.004078 / MGD /
Dec 2022 Week 4 0.001489 / MGD /
Jul 2022 Average 0.000031 /0.006 MGD /
Aug 2022 Average 0.000077 /0.006 MGD /
Sep 2022 Average 0.004304 /0.006 MGD /
Oct 2022 Average 0.004396 /0.006 MGD /
Nov 2022 Average 0.004078 /0.006 MGD /
Dec 2022 Average 0.001489 /0.006 MGD /
2022 Quarter 3 0.001471 / MGD /
2022 Quarter 4 0.003321 / MGD /
2022 2nd 6 Months(Avg) 0.002396 / MGD /
2022 2nd 6...(Max) 0.004396 / MGD /
2022 2nd 6...(Min) 0.000031 / MGD /
2022 2nd 6...(Count) 6
Tuesday,February 21,2023 2:41:35PM *Indicates Violation **Indicates TRC Violation Page 1 of 9

PowerSecure
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
08/23/2022 S PowerSecure082322Se 0.00025 /0.11 mg/L /
if
09/08/2022 P PowerSecure090822P < 0.00008 /0.11 mg/L < /
OTW
Aug 2022 Week 4 0.00025 / mg/L /
Sep 2022 Week 2 < 0.00008 / mg/L < /
Aug 2022 Average 0.00025 /0.07 mg/L /
Sep 2022 Average < 0.00008 /0.07 mg/L < /
2022 Quarter 3 < 0.00016 / mg/L < /
2022 2nd 6 Months(Avg) < 0.00016 / mg/L < /
2022 2nd 6...(Max) 0.00025 / mg/L /
2022 2nd 6...(Min) < 0.00008 / mg/L < /
2022 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
08/23/2022 S PowerSecure082322Se 1750 / mg/L /
if
09/08/2022 P PowerSecure09O822P 2780 / mg/L /
OTW
Aug 2022 Week 4 1750 / mg/L /
Sep 2022 Week 2 2780 / mg/L /
Aug 2022 Average 1750 / mg/L /
Sep 2022 Average 2780 / mg/L /
2022 Quarter 3 2265 / mg/L /
2022 2nd 6 Months(Avg) 2265 / mg/L /
2022 2nd 6...(Max) 2780 / mg/L /
Tuesday,February 21,2023 2:41:35PM *Indicates Violation **Indicates TRC Violation Page 2 of 9

PowerSecure
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Chloride
2022 2nd 6...(Min) 1750 / mg/L /
2022 2nd 6...(Count) 2 / /
Sample Date SampleID Result/Limit Mass/Limit
Chromium
08/23/2022 S PowerSecure082322Se < 0.001 /2.77 mg/L < /
if
09/08/2022 P PowerSecure09O822P < 0.001 /2.77 mg/L < /
OTW
Aug 2022 Week 4 < 0.001 / mg/L < /
Sep 2022 Week 2 < 0.001 / mg/L < /
Aug 2022 Average < 0.001 / 1.71 mg/L < /
Sep 2022 Average < 0.001 / 1.71 mg/L < /
2022 Quarter 3 < 0.001 / mg/L < /
2022 2nd 6 Months(Avg) < 0.001 / mg/L < /
2022 2nd 6...(Max) < 0.001 / mg/L < /
2022 2nd 6...(Min) < 0.001 / mg/L < /
2022 2nd 6...(Count) 2
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Copper
08/23/2022 S PowerSecure082322Se 0.32 /3.38 mg/L /
if
09/08/2022 P PowerSecure09O822P 0.174 /3.38 mg/L /
OTW
Aug 2022 Week 4 0.32 / mg/L /
Sep 2022 Week 2 0.174 / mg/L /
Aug 2022 Average 0.32 /2.07 mg/L /
Sep 2022 Average 0.174 /2.07 mg/L /
2022 Quarter 3 0.247 / mg/L /
2022 2nd 6 Months(Avg) 0.247 / mg/L /
2022 2nd 6...(Max) 0.32 / mg/L /
2022 2nd 6...(Min) 0.174 / mg/L /
2022 2nd 6...(Count) 2
Tuesday,February 21,2023 2:41:35PM *Indicates Violation **Indicates TRC Violation Page 3 of 9

PowerSecure
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
08/23/2022 S PowerSecure082322Se < 0.003 /0.60 mg/L < /
if
09/08/2022 P PowerSecure090822P < 0.003 /0.60 mg/L < /
OTW
Aug 2022 Week 4 < 0.003 / mg/L < /
Sep 2022 Week 2 < 0.003 / mg/L < /
Aug 2022 Average < 0.003 10.50 mg/L < /
Sep 2022 Average < 0.003 10.50 mg/L < /
2022 Quarter 3 < 0.003 / mg/L < /
2022 2nd 6 Months(Avg) < 0.003 / mg/L < /
2022 2nd 6...(Max) < 0.003 / mg/L < /
2022 2nd 6...(Min) < 0.003 / mg/L < /
2022 2nd 6...(Count) 2
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
09/08/2022 P PowerSecure09O822P 4.87 / mg/L /
OTW
Sep 2022 Week 2 4.87 / mg/L /
Sep 2022 Average 4.87 / mg/L /
2022 Quarter 3 4.87 / mg/L /
2022 2nd 6 Months(Avg) 4.87 / mg/L /
2022 2nd 6...(Max) 4.87 / mg/L /
2022 2nd 6...(Min) 4.87 / mg/L /
2022 2nd 6...(Count) 1
Tuesday,February 21,2023 2:41:35PM *Indicates Violation **Indicates TRC Violation Page 4 of 9

PowerSecure
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Lead
08/23/2022 S PowerSecure082322Se < 0.0005 /0.69 mg/L < /
if
09/08/2022 P PowerSecure090822P < 0.0003 /0.69 mg/L < /
OTW
Aug 2022 Week 4 < 0.0005 / mg/L < /
Sep 2022 Week 2 < 0.0003 / mg/L < /
Aug 2022 Average < 0.0005 /0.43 mg/L < /
Sep 2022 Average < 0.0003 /0.43 mg/L < /
2022 Quarter 3 < 0.0004 / mg/L < /
2022 2nd 6 Months(Avg) < 0.0004 / mg/L < /
2022 2nd 6...(Max) < 0.0005 / mg/L < /
2022 2nd 6...(Min) < 0.0003 / mg/L < /
2022 2nd 6...(Count) 2
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury
08/23/2022 S PowerSecure082322Se < 0 /0.000142 mg/L < /
if
Aug 2022 Week 4 < 0 / mg/L < /
Aug 2022 Average < 0 / mg/L < /
2022 Quarter 3 < 0 / mg/L < /
2022 2nd 6 Months(Avg) < 0.00000 / mg/L < /
2022 2nd 6...(Max) < 0.00000 / mg/L < /
2022 2nd 6...(Min) < 0.00000 / mg/L < /
2022 2nd 6...(Count) 1
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Tuesday,February 21,2023 2:41:35PM *Indicates Violation **Indicates TRC Violation Page 5 of 9

PowerSecure
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Mercury-LL
11/30/2022 P PowerSecure113022P 0.000004 / mg/L /
OTVMg
Nov 2022 Week 4 0.000004 / mg/L /
Nov 2022 Average 0.000004 / mg/L /
2022 Quarter 4 0.000004 / mg/L /
2022 2nd 6 Months(Avg) 0.000004 / mg/L /
2022 2nd 6...(Max) 0.000004 / mg/L /
2022 2nd 6...(Min) 0.000004 / mg/L /
2022 2nd 6...(Count) 1 / /
Sample Date SampleID Result/Limit Mass/Limit
Molybdenum
08/23/2022 S PowerSecure082322Se 0.003 / mg/L /
if
Aug 2022 Week 4 0.003 / mg/L /
Aug 2022 Average 0.003 / mg/L /
2022 Quarter 3 0.003 / mg/L /
2022 2nd 6 Months(Avg) 0.003 / mg/L /
2022 2nd 6...(Max) 0.003 / mg/L /
2022 2nd 6...(Min) 0.003 / mg/L /
2022 2nd 6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
08/23/2022 S PowerSecure082322Se 0.0086 / 1.30 mg/L /
if
09/08/2022 P PowerSecure09O822P 0.009 / 1.30 mg/L /
OTW
Sep 2022 Week 2 0.009 / mg/L /
Aug 2022 Week 4 0.0086 / mg/L /
Aug 2022 Average 0.0086 / 1.00 mg/L /
Sep 2022 Average 0.009 / 1.00 mg/L /
2022 Quarter 3 0.0088 / mg/L /
2022 2nd 6 Months(Avg) 0.0088 / mg/L /
2022 2nd 6...(Max) 0.009 / mg/L /
2022 2nd 6...(Min) 0.0086 / mg/L /
2022 2nd 6...(Count) 2
Tuesday,February 21,2023 2:41:35PM *Indicates Violation **Indicates TRC Violation Page 6 of 9

PowerSecure
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
08/23/2022 S PowerSecure082322Se 6.65 /6.0-10.0 SU /
if
09/08/2022 P PowerSecure090822P 7.9 /6.0-10.0 SU /
OTW
Aug 2022 Week 4 6.65 / SU /
Sep 2022 Week 2 7.9 / SU /
Aug 2022 Average 6.65 / SU /
Sep 2022 Average 7.9 / SU /
2022 Quarter 3 7.28 / SU /
2022 2nd 6 Months(Avg) 7.28 / SU /
2022 2nd 6...(Max) 7.9 / SU /
2022 2nd 6...(Min) 6.65 / SU /
2022 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Silver
08/23/2022 S PowerSecure082322Se 0.0009 /0.43 mg/L /
if
09/08/2022 P PowerSecure09O822P < 0.0003 /0.43 mg/L < /
OTW
Aug 2022 Week 4 0.0009 / mg/L /
Sep 2022 Week 2 < 0.0003 / mg/L < /
Aug 2022 Average 0.0009 /0.24 mg/L /
Sep 2022 Average < 0.0003 /0.24 mg/L < /
2022 Quarter 3 < 0.0006 / mg/L < /
2022 2nd 6 Months(Avg) < 0.0006 / mg/L < /
2022 2nd 6...(Max) 0.0009 / mg/L /
Tuesday,February 21,2023 2:41:35PM *Indicates Violation **Indicates TRC Violation Page 7 of 9

PowerSecure
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Silver
2022 2nd 6...(Min) < 0.0003 / mg/L < /
2022 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
TTO
08/23/2022 S PowerSecure082322Se < 0.025 /2.13 mg/L < /
if
Aug 2022 Week 4 < 0.025 / mg/L < /
Aug 2022 Average < 0.025 / mg/L < /
2022 Quarter 3 < 0.025 / mg/L < /
2022 2nd 6 Months(Avg) < 0.025 / mg/L < /
2022 2nd 6...(Max) < 0.025 / mg/L < /
2022 2nd 6...(Min) < 0.025 / mg/L < /
2022 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date Sample-ID Result/Limit Mass/Limit
Zinc
08/23/2022 S PowerSecure082322Se 0.078 /2.61 mg/L /
if
09/08/2022 P PowerSecure09O822P 0.031 /2.61 mg/L /
OTW
Aug 2022 Week 4 0.078 / mg/L /
Sep 2022 Week 2 0.031 / mg/L /
Aug 2022 Average 0.078 / 1.48 mg/L /
Sep 2022 Average 0.031 / 1.48 mg/L /
2022 Quarter 3 0.055 / mg/L /
2022 2nd 6 Months(Avg) 0.055 / mg/L /
Tuesday,February 21,2023 2:41:35PM *Indicates Violation **Indicates TRC Violation Page 8 of 9

PowerSecure
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Zinc
2022 2nd 6...(Max) 0.078 / mg/L /
2022 2nd 6...(Min) 0.031 / mg/L /
2022 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Tuesday,February 21,2023 2:41:35PM *Indicates Violation **Indicates TRC Violation Page 9 of 9

SCM Metal Products, Inc.
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
08/03/2022 S SCM080322Sself 2.6 / mg/L 0.3353 / lbs/day
08/11/2022 P SCM08 I 122POTW 6.8 / mg/L 0.818 / lbs/day
Aug 2022 Week 1 2.6 / mg/L 0.3353 / lbs/day
Aug 2022 Week 2 6.8 / mg/L 0.818 / lbs/day
Aug 2022 Average 4.7 / mg/L 0.5766 / lbs/day
2022 Quarter 3 4.7 / mg/L 0.5766 / lbs/day
2022 2nd 6 Months(Avg) 4.7 / mg/L 0.5766 / lbs/day
2022 2nd 6...(Max) 6.8 / mg/L 0.8180 / lbs/day
2022 2nd 6...(Min) 2.6 / mg/L 0.3353 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2022 S SCM0722171ow 0.013826 / 0.080 MGD /
08/31/2022 S SCM0822171ow 0.013283 / 0.080 MGD /
09/30/2022 S SCM0922171ow 0.013863 / 0.080 MGD /
10/31/2022 S SCM1022171ow 0.012825 / 0.080 MGD /
11/30/2022 S SCM1122171ow 0.013768 / 0.080 MGD /
12/31/2022 S SCM1222171ow 0.013242 / 0.080 MGD /
Jul 2022 Week 4 0.013826 / MGD /
Aug 2022 Week 4 0.013283 / MGD /
Sep 2022 Week 4 0.013863 / MGD /
Oct 2022 Week 4 0.012825 / MGD /
Nov 2022 Week 4 0.013768 / MGD /
Dec 2022 Week 4 0.013242 / MGD /
Jul 2022 Average 0.013826 / 0.050 MGD /
Aug 2022 Average 0.013283 / 0.050 MGD /
Sep 2022 Average 0.013863 / 0.050 MGD /
Oct 2022 Average 0.012825 / 0.050 MGD /
Nov 2022 Average 0.013768 / 0.050 MGD /
Dec 2022 Average 0.013242 / 0.050 MGD /
2022 Quarter 3 0.013657 / MGD /
2022 Quarter 4 0.013278 / MGD /
2022 2nd 6 Months(Avg) 0.013468 / MGD /
2022 2nd 6...(Max) 0.013863 / MGD /
2022 2nd 6...(Min) 0.012825 / MGD /
2022 2nd 6...(Count) 6
Tuesday,February 21,2023 7:40:17PM *Indicates Violation **Indicates TRC Violation Page 1 of 9

SCM Metal Products, Inc.
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
08/03/2022 S SCM080322Sself < 0.0005 / mg/L < 0.000064 / lbs/day
08/11/2022 P SCM08 I 122POTW < 0.00008 / mg/L < 0.000009 / lbs/day
Aug 2022 Week 1 < 0.0005 / mg/L < 0.000064 / lbs/day
Aug 2022 Week 2 < 0.00008 / mg/L < 0.000009 / lbs/day
Aug 2022 Average < 0.00029 / mg/L < 0.000037 / lbs/day
2022 Quarter 3 < 0.00029 / mg/L < 0.000037 / lbs/day
2022 2nd 6 Months(Avg) < 0.00029 / mg/L < 0.000037 / lbs/day
2022 2nd 6...(Max) < 0.0005 / mg/L < 0.000064 / lbs/day
2022 2nd 6...(Min) < 0.00008 / mg/L < 0.000009 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
08/03/2022 S SCM080322Sself 18 / mg/L 2.3213 / lbs/day
08/11/2022 P SCM081122POTW 21 / mg/L 2.526 / lbs/day
Aug 2022 Week 1 18 / mg/L 2.3213 / lbs/day
Aug 2022 Week 2 21 / mg/L 2.526 / lbs/day
Aug 2022 Average 19.5 / mg/L 2.4237 / lbs/day
2022 Quarter 3 19.5 / mg/L 2.4237 / lbs/day
2022 2nd 6 Months(Avg) 19.5 / mg/L 2.4237 / lbs/day
2022 2nd 6...(Max) 21 / mg/L 2.5260 / lbs/day
2022 2nd 6...(Min) 18 / mg/L 2.3213 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
08/03/2022 S SCM080322Sself 0.673 / 0.75 mg/L 0.086791 / lbs/day
08/11/2022 P SCM08 I 122POTW 0.121 / 0.75 mg/L 0.014555 / lbs/day
09/09/2022 S SCM090922Self 0.16 / 0.75 mg/L /
11/02/2022 S SCM110222Self 0.12 / 0.75 mg/L 0.012202 / lbs/day
Aug 2022 Week 1 0.673 / mg/L 0.086791 / lbs/day
Aug 2022 Week 2 0.121 / mg/L 0.014555 / lbs/day
Sep 2022 Week 2 0.16 / mg/L /
Nov 2022 Week 1 0.12 / mg/L 0.012202 / lbs/day
Aug 2022 Average 0.397 / 0.50 mg/L 0.050673 / lbs/day
Sep 2022 Average 0.16 / 0.50 mg/L /
Nov 2022 Average 0.12 / 0.50 mg/L 0.012202 / lbs/day
Tuesday,February 21,2023 7:40:17PM *Indicates Violation **Indicates TRC Violation Page 2 of 9

SCM Metal Products, Inc.
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Copper
2022 Quarter 3 0.318 / mg/L 0.050673 / lbs/day
2022 Quarter 4 0.12 / mg/L 0.012202 / lbs/day
2022 2nd 6 Months(Avg) 0.269 / mg/L 0.037849 / lbs/day
2022 2nd 6...(Max) 0.673 / mg/L 0.086791 / lbs/day
2022 2nd 6...(Min) 0.12 / mg/L /
2022 2nd 6...(Count) 4 / 3 /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
08/03/2022 S SCM080322Sself < 0.005 / 0.04 mg/L < 0.000645 / lbs/day
08/11/2022 P SCM081122POTW 0.01 / 0.04 mg/L 0.001203 / lbs/day
Aug 2022 Week 1 < 0.005 / mg/L < 0.000645 / lbs/day
Aug 2022 Week 2 0.01 / mg/L 0.001203 / lbs/day
Aug 2022 Average < 0.008 / 0.03 mg/L < 0.000924 / lbs/day
2022 Quarter 3 < 0.008 / mg/L < 0.000924 / lbs/day
2022 2nd 6 Months(Avg) < 0.008 / mg/L < 0.000924 / lbs/day
2022 2nd 6...(Max) 0.01 / mg/L 0.001203 / lbs/day
2022 2nd 6...(Min) < 0.005 / mg/L < 0.000645 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
08/03/2022 S SCM080322Sself 0.41 / mg/L 0.0529 / lbs/day
08/11/2022 P SCM081122POTW 0.67 / mg/L 0.0806 / lbs/day
Aug 2022 Week 1 0.41 / mg/L 0.0529 / lbs/day
Aug 2022 Week 2 0.67 / mg/L 0.0806 / lbs/day
Aug 2022 Average 0.54 / mg/L 0.0667 / lbs/day
2022 Quarter 3 0.54 / mg/L 0.0667 / lbs/day
2022 2nd 6 Months(Avg) 0.54 / mg/L 0.0667 / lbs/day
2022 2nd 6...(Max) 0.67 / mg/L 0.0806 / lbs/day
2022 2nd 6...(Min) 0.41 / mg/L 0.0529 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Lead
08/03/2022 S SCM080322Sself < 0.005 / 0.20 mg/L < 0.000645 / lbs/day
Tuesday,February 21,2023 7:40:17PM *Indicates Violation **Indicates TRC Violation Page 3 of 9

SCM Metal Products, Inc.
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Lead
08/11/2022 P SCM081122POTW 0.0016 / 0.20 mg/L 0.000186 / lbs/day
09/09/2022 S SCM090922Self < 0.005 / 0.20 mg/L < /
11/02/2022 S SCM110222Self < 0.0005 / 0.20 mg/L < 0.000051 / lbs/day
Aug 2022 Week 1 < 0.005 / mg/L < 0.000645 / lbs/day
Aug 2022 Week 2 0.0016 / mg/L 0.000186 / lbs/day
Sep 2022 Week 2 < 0.005 / mg/L < /
Nov 2022 Week 1 < 0.0005 / mg/L < 0.000051 / lbs/day
Aug 2022 Average < 0.0033 / 0.10 mg/L < 0.000416 / lbs/day
Sep 2022 Average < 0.005 / 0.10 mg/L < /
Nov 2022 Average < 0.0005 / 0.10 mg/L < 0.000051 / lbs/day
2022 Quarter 3 < 0.0039 / mg/L < 0.000416 / lbs/day
2022 Quarter 4 < 0.0005 / mg/L < 0.000051 / lbs/day
2022 2nd 6 Months(Avg) < 0.0030 / mg/L < 0.000294 / lbs/day
2022 2nd 6...(Max) < 0.005 / mg/L < 0.000645 / lbs/day
2022 2nd 6...(Min) < 0.0005 / mg/L < /
2022 2nd 6...(Count) 4 / 3 /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
08/03/2022 S SCM080322Sself 0.000002 / 0.000142 mg/L /
08/10/2022 P SCM081022POTW 0.000006 / 0.000142 ing/L /
Hg
Aug 2022 Week 1 0.000002 / mg/L /
Aug 2022 Week 2 0.000006 / mg/L /
Aug 2022 Average 0.000004 / mg/L /
2022 Quarter 3 0.000004 / mg/L /
2022 2nd 6 Months(Avg) 0.000004 / mg/L /
2022 2nd 6...(Max) 0.000006 / mg/L /
2022 2nd 6...(Min) 0.000002 / mg/L /
2022 2nd 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
08/03/2022 S SCM080322Sself < 0.005 / mg/L < 0.0006 / lbs/day
08/11/2022 P SCM081122POTW < 0.001 / mg/L < 0.0001 / lbs/day
Aug 2022 Week 1 < 0.005 / mg/L < 0.0006 / lbs/day
Aug 2022 Week 2 < 0.001 / mg/L < 0.0001 / lbs/day
Tuesday,February 21,2023 7:40:17PM *Indicates Violation **Indicates TRC Violation Page 4 of 9

SCM Metal Products, Inc.
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
Aug 2022 Average < 0.003 / mg/L < 0.0004 / lbs/day
2022 Quarter 3 < 0.003 / mg/L < 0.0004 / lbs/day
2022 2nd 6 Months(Avg) < 0.003 / mg/L < 0.0004 / lbs/day
2022 2nd 6...(Max) < 0.005 / mg/L < 0.0006 / lbs/day
2022 2nd 6...(Min) < 0.001 / mg/L < 0.0001 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
08/03/2022 S SCM080322Sself < 0.0025 / mg/L < 0.000322 / lbs/day
08/11/2022 P SCM081122POTW 0.0013 / mg/L 0.00016 / lbs/day
Aug 2022 Week 1 < 0.0025 / mg/L < 0.000322 / lbs/day
Aug 2022 Week 2 0.0013 / mg/L 0.00016 / lbs/day
Aug 2022 Average < 0.0019 / mg/L < 0.000241 / lbs/day
2022 Quarter 3 < 0.0019 / mg/L < 0.000241 / lbs/day
2022 2nd 6 Months(Avg) < 0.0019 / mg/L < 0.000241 / lbs/day
2022 2nd 6...(Max) < 0.0025 / mg/L < 0.000322 / lbs/day
2022 2nd 6...(Min) 0.0013 / mg/L 0.000160 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
08/03/2022 S SCM080322Sself 0.1 / mg/L 0.014 / lbs/day
08/11/2022 P SCM081122POTW 0.1 / mg/L 0.014 / lbs/day
Aug 2022 Week 1 0.1 / mg/L 0.014 / lbs/day
Aug 2022 Week 2 0.1 / mg/L 0.014 / lbs/day
Aug 2022 Average 0.1 / mg/L 0.014 / lbs/day
2022 Quarter 3 0.1 / mg/L 0.014 / lbs/day
2022 2nd 6 Months(Avg) 0.1 / mg/L 0.014 / lbs/day
2022 2nd 6...(Max) 0.1 / mg/L 0.014 / lbs/day
2022 2nd 6...(Min) 0.1 / mg/L 0.014 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
08/03/2022 S SCM080322Sself 7 / mg/L 0.903 / lbs/day
Tuesday,February 21,2023 7:40:17PM *Indicates Violation **Indicates TRC Violation Page 5 of 9

SCM Metal Products, Inc.
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
08/11/2022 P SCM081122POTW 13.1 / mg/L 1.576 / lbs/day
Aug 2022 Week 1 7 / mg/L 0.903 / lbs/day
Aug 2022 Week 2 13.1 / mg/L 1.576 / lbs/day
Aug 2022 Average 10.05 / mg/L 1.239 / lbs/day
2022 Quarter 3 10.05 / mg/L 1.239 / lbs/day
2022 2nd 6 Months(Avg) 10.05 / mg/L 1.239 / lbs/day
2022 2nd 6...(Max) 13.1 / mg/L 1.576 / lbs/day
2022 2nd 6...(Min) 7 / mg/L 0.903 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
08/03/2022 S SCM080322Sself < 2.5 / 200 mg/L < /
08/11/2022 P SCM081122POTW < 2.5 / 200 mg/L < /
Aug 2022 Week 1 < 2.5 / mg/L < /
Aug 2022 Week 2 < 2.5 / mg/L < /
Aug 2022 Average < 2.5 / mg/L < /
2022 Quarter 3 < 2.5 / mg/L < /
2022 2nd 6 Months(Avg) < 2.5 / mg/L < /
2022 2nd 6...(Max) < 2.5 / mg/L < /
2022 2nd 6...(Min) < 2.5 / mg/L < /
2022 2nd 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
pH
08/03/2022 S SCM080322Sself 7.4 / 6.0-10.5 su /
08/11/2022 P SCM081122POTW 7.5 / 6.0-10.5 su /
09/09/2022 S SCM090922Self 7.4 / 6.0-10.5 su /
11/02/2022 S SCM110222Self 8 / 6.0-10.5 su /
Aug 2022 Week 1 7.4 / su /
Aug 2022 Week 2 7.5 / su /
Sep 2022 Week 2 7.4 / su /
Nov 2022 Week 1 8 / su /
Aug 2022 Average 7.45 / su /
Sep 2022 Average 7.4 / su /
Nov 2022 Average 8 / su /
2022 Quarter 3 7.43 / su /
Tuesday,February 21,2023 7:40:17PM *Indicates Violation **Indicates TRC Violation Page 6 of 9

SCM Metal Products, Inc.
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
PH
2022 Quarter 4 8 / Su /
2022 2nd 6 Months(Avg) 7.58 / Su /
2022 2nd 6...(Max) 8 / su /
2022 2nd 6...(Min) 7.4 / su /
2022 2nd 6...(Count) 4 / /
Sample Date SamplelD Result/Limit Mass/Limit
Selenium
08/03/2022 S SCM080322Sself < 0.0075 / mg/L < 0.000967 / lbs/day
08/11/2022 P SCM081122POTW < 0.0005 / mg/L < 0.00006 / lbs/day
Aug 2022 Week 1 < 0.0075 / mg/L < 0.000967 / lbs/day
Aug 2022 Week 2 < 0.0005 / mg/L < 0.00006 / lbs/day
Aug 2022 Average < 0.004 / mg/L < 0.000514 / lbs/day
2022 Quarter 3 < 0.004 / mg/L < 0.000514 / lbs/day
2022 2nd 6 Months(Avg) < 0.004 / mg/L < 0.000514 / lbs/day
2022 2nd 6...(Max) < 0.0075 / mg/L < 0.000967 / lbs/day
2022 2nd 6...(Min) < 0.0005 / mg/L < 0.000060 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
08/03/2022 S SCM080322Sself 29.3 / 66 °C /
08/11/2022 P SCM081122POTW 27 / 66 °C /
09/09/2022 S SCM090922Self 25.9 / 66 °C /
11/02/2022 S SCM110222Self 20.7 / 66 °C /
Aug 2022 Week 1 29.3 / °C /
Aug 2022 Week 2 27 / °C /
Sep 2022 Week 2 25.9 / °C /
Nov 2022 Week 1 20.7 / °C /
Aug 2022 Average 28.2 / °C /
Sep 2022 Average 25.9 / °C /
Nov 2022 Average 20.7 / °C /
2022 Quarter 3 27.4 / °C /
2022 Quarter 4 20.7 / °C /
2022 2nd 6 Months(Avg) 25.7 / °C /
2022 2nd 6...(Max) 29.3 / °C /
2022 2nd 6...(Min) 20.7 / °C /
Tuesday,February 21,2023 7:40:17PM *Indicates Violation **Indicates TRC Violation Page 7 of 9

SCM Metal Products, Inc.
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
2022 2nd 6...(Count) 4
Sample Date SamplelD Result/Limit Mass/Limit
TKN
08/03/2022 S SCM080322Sself 6.9 / mg/L 0.89 / lbs/day
08/11/2022 P SCM081122POTW 13 / mg/L 1.564 / lbs/day
Aug 2022 Week 1 6.9 / mg/L 0.89 / lbs/day
Aug 2022 Week 2 13 / mg/L 1.564 / lbs/day
Aug 2022 Average 9.95 / mg/L 1.227 / lbs/day
2022 Quarter 3 9.95 / mg/L 1.227 / lbs/day
2022 2nd 6 Months(Avg) 9.95 / mg/L 1.227 / lbs/day
2022 2nd 6...(Max) 13 / mg/L 1.564 / lbs/day
2022 2nd 6...(Min) 6.9 / mg/L 0.890 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
08/03/2022 S SCM080322Sself 1.2 / mg/L 0.1548 / lbs/day
08/11/2022 P SCM081122POTW 1.49 / mg/L 0.1792 / lbs/day
Aug 2022 Week 1 1.2 / mg/L 0.1548 / lbs/day
Aug 2022 Week 2 1.49 / mg/L 0.1792 / lbs/day
Aug 2022 Average 1.345 / mg/L 0.167 / lbs/day
2022 Quarter 3 1.345 / mg/L 0.167 / lbs/day
2022 2nd 6 Months(Avg) 1.345 / mg/L 0.1670 / lbs/day
2022 2nd 6...(Max) 1.49 / mg/L 0.1792 / lbs/day
2022 2nd 6...(Min) 1.2 / mg/L 0.1548 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
08/03/2022 S SCM080322Sself 0.0228 / mg/L /
Aug 2022 Week 1 0.0228 / mg/L /
Aug 2022 Average 0.0228 / mg/L /
2022 Quarter 3 0.0228 / mg/L /
2022 2nd 6 Months(Avg) 0.0228 / mg/L /
2022 2nd 6...(Max) 0.0228 / mg/L /
Tuesday,February 21,2023 7:40:17PM *Indicates Violation **Indicates TRC Violation Page 8 of 9

SCM Metal Products, Inc.
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
VOC
2022 2nd 6...(Min) 0.0228 / mg/L /
2022 2nd 6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
08/03/2022 S SCM080322Sself 0.505 / mg/L 0.065126 / lbs/day
08/11/2022 P SCM081122POTW 0.296 / mg/L 0.035605 / lbs/day
Aug 2022 Week 1 0.505 / mg/L 0.065126 / lbs/day
Aug 2022 Week 2 0.296 / mg/L 0.035605 / lbs/day
Aug 2022 Average 0.401 / mg/L 0.050365 / lbs/day
2022 Quarter 3 0.401 / mg/L 0.050365 / lbs/day
2022 2nd 6 Months(Avg) 0.401 / mg/L 0.050365 / lbs/day
2022 2nd 6...(Max) 0.505 / mg/L 0.065126 / lbs/day
2022 2nd 6...(Min) 0.296 / mg/L 0.035605 / lbs/day
2022 2nd 6...(Count) 2 / 2 /
Tuesday,February 21,2023 7:40:17PM *Indicates Violation **Indicates TRC Violation Page 9 of 9

Tereus Pharma
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
08/24/2022 S Tergus082422Self 0.01 /20.7 mg/L /
09/09/2022 P Tergus09O922POTW < 0.025 /20.7 mg/L < /
Aug 2022 Week 4 0.01 / mg/L /
Sep 2022 Week 2 < 0.025 / mg/L < /
Aug 2022 Average 0.01 /8.2 mg/L /
Sep 2022 Average < 0.025 /8.2 mg/L < /
2022 Quarter 3 < 0.017 / mg/L < /
2022 2nd 6 Months(Avg) < 0.017 / mg/L < /
2022 2nd 6...(Max) < 0.025 / mg/L < /
2022 2nd 6...(Min) 0.010 / mg/L /
2022 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Arsenic
08/24/2022 S Tergus082422Self < 0.0005 / mg/L < /
09/09/2022 P Tergus09O922POTW < 0.001 / mg/L < /
Aug 2022 Week 4 < 0.0005 / mg/L < /
Sep 2022 Week 2 < 0.001 / mg/L < /
Aug 2022 Average < 0.0005 / mg/L < /
Sep 2022 Average < 0.001 / mg/L < /
2022 Quarter 3 < 0.0007 / mg/L < /
2022 2nd 6 Months(Avg) < 0.0007 / mg/L < /
2022 2nd 6...(Max) < 0.001 / mg/L < /
2022 2nd 6...(Min) < 0.0005 / mg/L < /
2022 2nd 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2022 S Tergus0722F1ow 0.000118 / MGD /
08/31/2022 S Tergus0822F1ow 0.000158 / MGD /
09/30/2022 S Tergus0922F1ow 0.000148 / MGD /
Jul 2022 Week 4 0.000118 / MGD /
Aug 2022 Week 4 0.000158 / MGD /
Tuesday,February 28,2023 9:51:21AM *Indicates Violation **Indicates TRC Violation Page 1 of 12

Tereus Pharma
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Sep 2022 Week 4 0.000148 / MGD /
Jul 2022 Average 0.000118 / MGD /
Aug 2022 Average 0.000158 / MGD /
Sep 2022 Average 0.000148 / MGD /
2022 Quarter 3 0.000141 / MGD /
2022 2nd 6 Months(Avg) 0.000141 / MGD /
2022 2nd 6...(Max) 0.000158 / MGD /
2022 2nd 6...(Min) 0.000118 / MGD /
2022 2nd 6...(Count) 3
Sample Date SampleID Result/Limit Mass/Limit
BOD
08/24/2022 S Tergus082422Self 274 / mg/L /
09/09/2022 P Tergus09O922POTW 33 / mg/L /
Aug 2022 Week 4 274 / mg/L /
Sep 2022 Week 2 33 / mg/L /
Aug 2022 Average 274 / mg/L /
Sep 2022 Average 33 / mg/L /
2022 Quarter 3 153.5 / mg/L /
2022 2nd 6 Months(Avg) 153.5 / mg/L /
2022 2nd 6...(Max) 274 / mg/L /
2022 2nd 6...(Min) 33 / mg/L /
2022 2nd 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
08/24/2022 S Tergus082422Self < 0.00004 / mg/L < /
09/09/2022 P Tergus09O922POTW < 0.00008 / mg/L < /
Aug 2022 Week 4 < 0.00004 / mg/L < /
Sep 2022 Week 2 < 0.00008 / mg/L < /
Aug 2022 Average < 0.00004 / mg/L < /
Sep 2022 Average < 0.00008 / mg/L < /
2022 Quarter 3 < 0.00006 / mg/L < /
2022 2nd 6 Months(Avg) < 0.00006 / mg/L < /
2022 2nd 6...(Max) < 0.00008 / mg/L < /
2022 2nd 6...(Min) < 0.00004 / mg/L < /
2022 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
08/24/2022 S Tergus082422Self 12 / mg/L /
Tuesday,February 28,2023 9:51:21AM *Indicates Violation **Indicates TRC Violation Page 2 of 12

Tereus Pharma
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Chloride
09/09/2022 P Tergus09O922POTW 12.7 / mg/L /
Aug 2022 Week 4 12 / mg/L /
Sep 2022 Week 2 12.7 / mg/L /
Aug 2022 Average 12 / mg/L /
Sep 2022 Average 12.7 / mg/L /
2022 Quarter 3 12.35 / mg/L /
2022 2nd 6 Months(Avg) 12.35 / mg/L /
2022 2nd 6...(Max) 12.7 / mg/L /
2022 2nd 6...(Min) 12 / mg/L /
2022 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
08/24/2022 S Tergus082422Self 0.003 / mg/L /
09/09/2022 P Tergus09O922POTW < 0.001 / mg/L < /
Aug 2022 Week 4 0.003 / mg/L /
Sep 2022 Week 2 < 0.001 / mg/L < /
Aug 2022 Average 0.003 / mg/L /
Sep 2022 Average < 0.001 / mg/L < /
2022 Quarter 3 < 0.002 / mg/L < /
2022 2nd 6 Months(Avg) < 0.002 / mg/L < /
2022 2nd 6...(Max) 0.003 / mg/L /
2022 2nd 6...(Min) < 0.001 / mg/L < /
2022 2nd 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Copper
08/24/2022 S Tergus082422Self 0.173 / mg/L /
09/09/2022 P Tergus09O922POTW 0.077 / mg/L /
Aug 2022 Week 4 0.173 / mg/L /
Sep 2022 Week 2 0.077 / mg/L /
Aug 2022 Average 0.173 / mg/L /
Sep 2022 Average 0.077 / mg/L /
2022 Quarter 3 0.125 / mg/L /
2022 2nd 6 Months(Avg) 0.125 / mg/L /
2022 2nd 6...(Max) 0.173 / mg/L /
2022 2nd 6...(Min) 0.077 / mg/L /
2022 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
Tuesday,February 28,2023 9:51:21AM *Indicates Violation **Indicates TRC Violation Page 3 of 12

Tereus Pharma
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
08/24/2022 S Tergus082422Self < 0.001 / mg/L < /
09/09/2022 P Tergus09O922POTW < 0.003 / mg/L < /
Aug 2022 Week 4 < 0.001 / mg/L < /
Sep 2022 Week 2 < 0.003 / mg/L < /
Aug 2022 Average < 0.001 / mg/L < /
Sep 2022 Average < 0.003 / mg/L < /
2022 Quarter 3 < 0.002 / mg/L < /
2022 2nd 6 Months(Avg) < 0.002 / mg/L < /
2022 2nd 6...(Max) < 0.003 / mg/L < /
2022 2nd 6...(Min) < 0.001 / mg/L < /
2022 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
08/24/2022 S Tergus082422Self < 0.003 /20.7 mg/L < /
09/09/2022 P Tergus09O922POTW < 0.005 /20.7 mg/L < /
Aug 2022 Week 4 < 0.003 / mg/L < /
Sep 2022 Week 2 < 0.005 / mg/L < /
Aug 2022 Average < 0.003 /8.2 mg/L < /
Sep 2022 Average < 0.005 /8.2 mg/L < /
2022 Quarter 3 < 0.004 / mg/L < /
2022 2nd 6 Months(Avg) < 0.004 / mg/L < /
2022 2nd 6...(Max) < 0.005 / mg/L < /
2022 2nd 6...(Min) < 0.003 / mg/L < /
2022 2nd 6...(Count) 2
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
08/24/2022 S Tergus082422Self < 0.05 / mg/L < /
09/09/2022 P Tergus09O922POTW 0.79 / mg/L /
Aug 2022 Week 4 < 0.05 / mg/L < /
Sep 2022 Week 2 0.79 / mg/L /
Aug 2022 Average < 0.05 / mg/L < /
Tuesday,February 28,2023 9:51:21AM *Indicates Violation **Indicates TRC Violation Page 4 of 12

Tereus Pharma
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Fluoride
Sep 2022 Average 0.79 / mg/L /
2022 Quarter 3 < 0.42 / mg/L < /
2022 2nd 6 Months(Avg) < 0.42 / mg/L < /
2022 2nd 6...(Max) 0.79 / mg/L /
2022 2nd 6...(Min) < 0.05 / mg/L < /
2022 2nd 6...(Count) 2 / /
Sample Date SampleID Result/Limit Mass/Limit
Isopropyl acetate
08/24/2022 S Tergus082422Self < 0.003 /20.7 mg/L < /
09/09/2022 P Tergus09O922POTW < 0.005 /20.7 mg/L < /
Aug 2022 Week 4 < 0.003 / mg/L < /
Sep 2022 Week 2 < 0.005 / mg/L < /
Aug 2022 Average < 0.003 /8.2 mg/L < /
Sep 2022 Average < 0.005 /8.2 mg/L < /
2022 Quarter 3 < 0.004 / mg/L < /
2022 2nd 6 Months(Avg) < 0.004 / mg/L < /
2022 2nd 6...(Max) < 0.005 / mg/L < /
2022 2nd 6...(Min) < 0.003 / mg/L < /
2022 2nd 6...(Count) 2
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Lead
08/24/2022 S Tergus082422Self 0.0008 / mg/L /
09/09/2022 P Tergus09O922POTW < 0.0003 / mg/L < /
Aug 2022 Week 4 0.0008 / mg/L /
Sep 2022 Week 2 < 0.0003 / mg/L < /
Aug 2022 Average 0.0008 / mg/L /
Sep 2022 Average < 0.0003 / mg/L < /
2022 Quarter 3 < 0.0005 / mg/L < /
2022 2nd 6 Months(Avg) < 0.0005 / mg/L < /
2022 2nd 6...(Max) 0.0008 / mg/L /
2022 2nd 6...(Min) < 0.0003 / mg/L < /
Tuesday,February 28,2023 9:51:21AM *Indicates Violation **Indicates TRC Violation Page 5 of 12

Tereus Pharma
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
Lead
2022 2nd 6...(Count) 2
Sample Date SampleID Result/Limit Mass/Limit
Mercury-LL
08/24/2022 S Tergus082422SelfHg < 0.000001 /0.000142 mg/L < /
09/08/2022 P Tergus09O822POTW-H 0.000001 /0.000142 mg/L /
9
Aug 2022 Week 4 < 0.000001 / mg/L < /
Sep 2022 Week 2 0.000001 / mg/L /
Aug 2022 Average < 0.000001 / mg/L < /
Sep 2022 Average 0.000001 / mg/L /
2022 Quarter 3 < 0.000001 / mg/L < /
2022 2nd 6 Months(Avg) < 0.000001 / mg/L < /
2022 2nd 6...(Max) 0.000001 / mg/L /
2022 2nd 6...(Min) < 0.000001 / mg/L < /
2022 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Methylene Chloride
08/24/2022 S Tergus082422Self < 0.002 /3.0 mg/L < /
09/09/2022 P Tergus09O922POTW < 0.003 /3.0 mg/L < /
Aug 2022 Week 4 < 0.002 / mg/L < /
Sep 2022 Week 2 < 0.003 / mg/L < /
Aug 2022 Average < 0.002 /0.7 mg/L < /
Sep 2022 Average < 0.003 /0.7 mg/L < /
2022 Quarter 3 < 0.002 / mg/L < /
2022 2nd 6 Months(Avg) < 0.002 / mg/L < /
2022 2nd 6...(Max) < 0.003 / mg/L < /
2022 2nd 6...(Min) < 0.002 / mg/L < /
2022 2nd 6...(Count) 2 / /
Tuesday,February 28,2023 9:51:21AM *Indicates Violation **Indicates TRC Violation Page 6 of 12

Tereus Pharma
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
08/24/2022 S Tergus082422Self < 0.003 / mg/L < /
09/09/2022 P Tergus09O922POTW < 0.001 / mg/L < /
Aug 2022 Week 4 < 0.003 / mg/L < /
Sep 2022 Week 2 < 0.001 / mg/L < /
Aug 2022 Average < 0.003 / mg/L < /
Sep 2022 Average < 0.001 / mg/L < /
2022 Quarter 3 < 0.002 / mg/L < /
2022 2nd 6 Months(Avg) < 0.002 / mg/L < /
2022 2nd 6...(Max) < 0.003 / mg/L < /
2022 2nd 6...(Min) < 0.001 / mg/L < /
2022 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
08/24/2022 S Tergus082422Self < 0.001 /20.7 mg/L < /
09/09/2022 P Tergus09O922POTW < 0.005 /20.7 mg/L < /
Aug 2022 Week 4 < 0.001 / mg/L < /
Sep 2022 Week 2 < 0.005 / mg/L < /
Aug 2022 Average < 0.001 /8.2 mg/L < /
Sep 2022 Average < 0.005 /8.2 mg/L < /
2022 Quarter 3 < 0.003 / mg/L < /
2022 2nd 6 Months(Avg) < 0.003 / mg/L < /
2022 2nd 6...(Max) < 0.005 / mg/L < /
2022 2nd 6...(Min) < 0.001 / mg/L < /
2022 2nd 6...(Count) 2
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Tuesday,February 28,2023 9:51:21AM *Indicates Violation **Indicates TRC Violation Page 7 of 12

Tereus Pharma
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
08/24/2022 S Tergus082422Self 0.005 / mg/L /
09/09/2022 P Tergus09O922POTW 0.001 / mg/L /
Sep 2022 Week 2 0.001 / mg/L /
Aug 2022 Week 4 0.005 / mg/L /
Aug 2022 Average 0.005 / mg/L /
Sep 2022 Average 0.001 / mg/L /
2022 Quarter 3 0.003 / mg/L /
2022 2nd 6 Months(Avg) 0.003 / mg/L /
2022 2nd 6...(Max) 0.005 / mg/L /
2022 2nd 6...(Min) 0.001 / mg/L /
2022 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
08/24/2022 S Tergus082422Self 0.1 / mg/L /
09/09/2022 P Tergus09O922POTW < 0.1 / mg/L < /
Aug 2022 Week 4 0.1 / mg/L /
Sep 2022 Week 2 < 0.1 / mg/L < /
Aug 2022 Average 0.1 / mg/L /
Sep 2022 Average < 0.1 / mg/L < /
2022 Quarter 3 < 0.1 / mg/L < /
2022 2nd 6 Months(Avg) < 0.1 / mg/L < /
2022 2nd 6...(Max) 0.1 / mg/L /
2022 2nd 6...(Min) < 0.1 / mg/L < /
2022 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
08/24/2022 S Tergus082422Self 5.85 / mg/L /
09/09/2022 P Tergus09O922POTW 0.73 / mg/L /
Aug 2022 Week 4 5.85 / mg/L /
Sep 2022 Week 2 0.73 / mg/L /
Aug 2022 Average 5.85 / mg/L /
Sep 2022 Average 0.73 / mg/L /
2022 Quarter 3 3.29 / mg/L /
2022 2nd 6 Months(Avg) 3.29 / mg/L /
2022 2nd 6...(Max) 5.85 / mg/L /
2022 2nd 6...(Min) 0.73 / mg/L /
2022 2nd 6...(Count) 2 / /
Tuesday,February 28,2023 9:51:21AM *Indicates Violation **Indicates TRC Violation Page 8 of 12

Tereus Pharma
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
08/24/2022 S Tergus082422Self < 2.5 /200 mg/L < /
09/09/2022 P Tergus09O922POTW < 2.5 /200 mg/L < /
Aug 2022 Week 4 < 2.5 / mg/L < /
Sep 2022 Week 2 < 2.5 / mg/L < /
Aug 2022 Average < 2.5 / mg/L < /
Sep 2022 Average < 2.5 / mg/L < /
2022 Quarter 3 < 2.5 / mg/L < /
2022 2nd 6 Months(Avg) < 2.5 / mg/L < /
2022 2nd 6...(Max) < 2.5 / mg/L < /
2022 2nd 6...(Min) < 2.5 / mg/L < /
2022 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
09/09/2022 P Tergus09O922POTW 9.5 /6.0-10.0 SU /
09/28/2022 S Tergus092822Self 8 /6.0-10.0 SU /
Sep 2022 Week 2 9.5 / SU /
Sep 2022 Week 4 8 / SU /
Sep 2022 Average 8.75 / SU /
2022 Quarter 3 8.75 / SU /
2022 2nd 6 Months(Avg) 8.75 / SU /
2022 2nd 6...(Max) 9.5 / SU /
2022 2nd 6...(Min) 8 / SU /
2022 2nd 6...(Count) 2
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Tuesday,February 28,2023 9:51:21AM *Indicates Violation **Indicates TRC Violation Page 9 of 12

Tereus Pharma
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Selenium
08/24/2022 S Tergus082422Self < 0.001 / mg/L < /
09/09/2022 P Tergus09O922POTW < 0.0005 / mg/L < /
Aug 2022 Week 4 < 0.001 / mg/L < /
Sep 2022 Week 2 < 0.0005 / mg/L < /
Aug 2022 Average < 0.001 / mg/L < /
Sep 2022 Average < 0.0005 / mg/L < /
2022 Quarter 3 < 0.0008 / mg/L < /
2022 2nd 6 Months(Avg) < 0.0008 / mg/L < /
2022 2nd 6...(Max) < 0.001 / mg/L < /
2022 2nd 6...(Min) < 0.0005 / mg/L < /
2022 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Silver
08/24/2022 S Tergus082422Self < 0.0005 / mg/L < /
09/09/2022 P Tergus09O922POTW < 0.0003 / mg/L < /
Aug 2022 Week 4 < 0.0005 / mg/L < /
Sep 2022 Week 2 < 0.0003 / mg/L < /
Aug 2022 Average < 0.0005 / mg/L < /
Sep 2022 Average < 0.0003 / mg/L < /
2022 Quarter 3 < 0.0004 / mg/L < /
2022 2nd 6 Months(Avg) < 0.0004 / mg/L < /
2022 2nd 6...(Max) < 0.0005 / mg/L < /
2022 2nd 6...(Min) < 0.0003 / mg/L < /
2022 2nd 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
09/09/2022 P Tergus09O922POTW 29 /66 °C /
09/28/2022 S Tergus092822Self 28.8 /66 °C /
Sep 2022 Week 2 29 / °C /
Sep 2022 Week 4 28.8 / °C /
Sep 2022 Average 28.9 / °C /
2022 Quarter 3 28.9 / °C /
2022 2nd 6 Months(Avg) 28.9 / °C /
2022 2nd 6...(Max) 29 / °C /
2022 2nd 6...(Min) 28.8 / °C /
2022 2nd 6...(Count) 2
Tuesday,February 28,2023 9:51:21AM *Indicates Violation **Indicates TRC Violation Page 10 of 12

Tereus Pharma
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
08/24/2022 S Tergus082422Self 5.78 / mg/L /
09/09/2022 P Tergus09O922POTW 0.73 / mg/L /
Aug 2022 Week 4 5.78 / mg/L /
Sep 2022 Week 2 0.73 / mg/L /
Aug 2022 Average 5.78 / mg/L /
Sep 2022 Average 0.73 / mg/L /
2022 Quarter 3 3.26 / mg/L /
2022 2nd 6 Months(Avg) 3.26 / mg/L /
2022 2nd 6...(Max) 5.78 / mg/L /
2022 2nd 6...(Min) 0.73 / mg/L /
2022 2nd 6...(Count) 2 / /
Sample Date SampleID Result/Limit Mass/Limit
Total Phosphorus
08/24/2022 S Tergus082422Self 5.98 / mg/L /
09/09/2022 P Tergus09O922POTW 0.716 / mg/L /
Aug 2022 Week 4 5.98 / mg/L /
Sep 2022 Week 2 0.716 / mg/L /
Aug 2022 Average 5.98 / mg/L /
Sep 2022 Average 0.716 / mg/L /
2022 Quarter 3 3.348 / mg/L /
2022 2nd 6 Months(Avg) 3.348 / mg/L /
2022 2nd 6...(Max) 5.98 / mg/L /
2022 2nd 6...(Min) 0.716 / mg/L /
2022 2nd 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
TSS
08/24/2022 S Tergus082422Self 5.6 / mg/L /
09/09/2022 P Tergus09O922POTW < 1.7 / mg/L < /
Aug 2022 Week 4 5.6 / mg/L /
Sep 2022 Week 2 < 1.7 / mg/L < /
Aug 2022 Average 5.6 / mg/L /
Tuesday,February 28,2023 9:51:21AM *Indicates Violation **Indicates TRC Violation Page 11 of 12

Tereus Pharma
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
TSS
Sep 2022 Average < 1.7 / mg/L < /
2022 Quarter 3 < 3.7 / mg/L < /
2022 2nd 6 Months(Avg) < 3.7 / mg/L < /
2022 2nd 6...(Max) 5.6 / mg/L /
2022 2nd 6...(Min) < 1.7 / mg/L < /
2022 2nd 6...(Count) 2 / /
Sample Date SampleID Result/Limit Mass/Limit
VOC
08/24/2022 S Tergus082422Self 0.028 / mg/L /
09/09/2022 P Tergus09O922POTW < 0.025 / mg/L < /
Aug 2022 Week 4 0.028 / mg/L /
Sep 2022 Week 2 < 0.025 / mg/L < /
Aug 2022 Average 0.028 / mg/L /
Sep 2022 Average < 0.025 / mg/L < /
2022 Quarter 3 < 0.0265 / mg/L < /
2022 2nd 6 Months(Avg) < 0.0265 / mg/L < /
2022 2nd 6...(Max) 0.028 / mg/L /
2022 2nd 6...(Min) < 0.025 / mg/L < /
2022 2nd 6...(Count) 2 / /
Sample Date SampleID Result/Limit Mass/Limit
Zinc
08/24/2022 S Tergus082422Self 0.495 / mg/L /
09/09/2022 P Tergus09O922POTW 0.365 / mg/L /
Aug 2022 Week 4 0.495 / mg/L /
Sep 2022 Week 2 0.365 / mg/L /
Aug 2022 Average 0.495 / mg/L /
Sep 2022 Average 0.365 / mg/L /
2022 Quarter 3 0.43 / mg/L /
2022 2nd 6 Months(Avg) 0.43 / mg/L /
2022 2nd 6...(Max) 0.495 / mg/L /
2022 2nd 6...(Min) 0.365 / mg/L /
2022 2nd 6...(Count) 2 / /
Tuesday,February 28,2023 9:51:21AM *Indicates Violation **Indicates TRC Violation Page 12 of 12

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Acetone
08/11/2022 P TriPharm081122POT < 0.025 /5.44 mg/L < 0.0009 / lbs/day
W
08/30/2022 S TriPharm083022Self < 0.025 /5.44 mg/L < /
Aug 2022 Week 2 < 0.025 / mg/L < 0.0009 / lbs/day
Aug 2022 Week 4 < 0.025 / mg/L < /
Aug 2022 Average < 0.025 /2.15 mg/L < 0.0009 / lbs/day
2022 Quarter 3 < 0.025 / mg/L < 0.0009 / lbs/day
2022 2nd 6 Months(Avg) < 0.025 / mg/L < 0.0009 / lbs/day
2022 2nd 6...(Max) < 0.025 / mg/L < 0.0009 / lbs/day
2022 2nd 6...(Min) < 0.025 / mg/L < /
2022 2nd 6...(Count) 2 / 1 /
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
08/11/2022 P TriPharm081122POT 0.2 / mg/L 0.0074 / lbs/day
W
08/30/2022 S TriPharm083022Self 0.3 / mg/L /
Aug 2022 Week 2 0.2 / mg/L 0.0074 / lbs/day
Aug 2022 Week 4 0.3 / mg/L /
Aug 2022 Average 0.25 / mg/L 0.0074 / lbs/day
2022 Quarter 3 0.25 / mg/L 0.0074 / lbs/day
2022 2nd 6 Months(Avg) 0.25 / mg/L 0.0074 / lbs/day
2022 2nd 6...(Max) 0.3 / mg/L 0.0074 / lbs/day
2022 2nd 6...(Min) 0.2 / mg/L /
2022 2nd 6...(Count) 2 / 1 /
Sample Date SampleID Result/Limit Mass/Limit
Average Flow for Month
07/31/2022 S TriPharm0722F1ow 0.003894 / MGD /
08/31/2022 S TriPharm0822F1ow 0.004329 / MGD /
09/30/2022 S TriPharm0922F1ow 0.006561 / MGD /
10/31/2022 S TriPharm1022171ow 0.00534 / MGD /
11/30/2022 S TriPharmll22F1ow 0.004877 / MGD /
12/31/2022 S TriPharml222F1ow 0.005555 / MGD /
Monday,February 27,2023 3:47:36PM *Indicates Violation **Indicates TRC Violation Page 1 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Average Flow for Month
Jul 2022 Week 4 0.003894 / MGD /
Aug 2022 Week 4 0.004329 / MGD /
Sep 2022 Week 4 0.006561 / MGD /
Oct 2022 Week 4 0.00534 / MGD /
Nov 2022 Week 4 0.004877 / MGD /
Dec 2022 Week 4 0.005555 / MGD /
Jul 2022 Average 0.003894 10.005 MGD /
Aug 2022 Average 0.004329 10.005 MGD /
Sep 2022 Average 0.006561 10.005 MGD * /
Oct 2022 Average 0.00534 10.005 MGD * /
Nov 2022 Average 0.004877 10.005 MGD /
Dec 2022 Average 0.005555 10.005 MGD * /
2022 Quarter 3 0.004928 / MGD /
2022 Quarter 4 0.005257 / MGD /
2022 2nd 6 Months(Avg) 0.005093 / MGD /
2022 2nd 6...(Max) 0.006561 / MGD /
2022 2nd 6...(Min) 0.003894 / MGD /
2022 2nd 6...(Count) 6
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 3 50.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
BOD
08/11/2022 P TriPharm081122POT 6.4 / mg/L 0.236 / lbs/day
W
08/30/2022 S TriPharm083022Self 3.2 / mg/L /
Aug 2022 Week 2 6.4 / mg/L 0.236 / lbs/day
Aug 2022 Week 4 3.2 / mg/L /
Aug 2022 Average 4.8 / mg/L 0.236 / lbs/day
2022 Quarter 3 4.8 / mg/L 0.236 / lbs/day
2022 2nd 6 Months(Avg) 4.8 / mg/L 0.236 / lbs/day
2022 2nd 6...(Max) 6.4 / mg/L 0.236 / lbs/day
2022 2nd 6...(Min) 3.2 / mg/L /
2022 2nd 6...(Count) 2 / 1 /
Monday,February 27,2023 3:47:36PM *Indicates Violation **Indicates TRC Violation Page 2 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Cadmium
08/11/2022 P TriPharm081122POT < 0.00008 / mg/L < 0.000003 / lbs/day
W
08/30/2022 S TriPharm083022Self < 0.00008 / mg/L < /
Aug 2022 Week 2 < 0.00008 / mg/L < 0.000003 / lbs/day
Aug 2022 Week 4 < 0.00008 / mg/L < /
Aug 2022 Average < 0.00008 / mg/L < 0.000003 / lbs/day
2022 Quarter 3 < 0.00008 / mg/L < 0.000003 / lbs/day
2022 2nd 6 Months(Avg) < 0.00008 / mg/L < 0.000003 / lbs/day
2022 2nd 6...(Max) < 0.00008 / mg/L < 0.000003 / lbs/day
2022 2nd 6...(Min) < 0.00008 / mg/L < /
2022 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
08/11/2022 P TriPharm081122POT 545 / mg/L 20.113 / lbs/day
W
08/30/2022 S TriPhann083022Self 12.7 / mg/L /
Aug 2022 Week 2 545 / mg/L 20.113 / lbs/day
Aug 2022 Week 4 12.7 / mg/L /
Aug 2022 Average 278.85 / mg/L 20.113 / lbs/day
2022 Quarter 3 278.85 / mg/L 20.113 / lbs/day
2022 2nd 6 Months(Avg) 278.85 / mg/L 20.113 / lbs/day
2022 2nd 6...(Max) 545 / mg/L 20.1130 / lbs/day
2022 2nd 6...(Min) 12.7 / mg/L /
2022 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass l Limit
COD
08/11/2022 P TriPharm081122POT < 7.5 / mg/L < 0.28 / lbs/day
W
08/30/2022 S TriPharm083022Self < 7.5 / mg/L < /
Aug 2022 Week 2 < 7.5 / mg/L < 0.28 / lbs/day
Aug 2022 Week 4 < 7.5 / mg/L < /
Aug 2022 Average < 7.5 / mg/L < 0.28 / lbs/day
2022 Quarter 3 < 7.5 / mg/L < 0.28 / lbs/day
2022 2nd 6 Months(Avg) < 7.5 / mg/L < 0.28 / lbs/day
2022 2nd 6...(Max) < 7.5 / mg/L < 0.28 / lbs/day
2022 2nd 6...(Min) < 7.5 / mg/L < /
2022 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
Monday,February 27,2023 3:47:36PM *Indicates Violation **Indicates TRC Violation Page 3 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Ethyl acetate
08/11/2022 P TriPharm081122POT < 0.005 /5.44 mg/L < 0.0002 / lbs/day
W
08/30/2022 S TriPharm083022Self < 0.005 /5.44 mg/L < /
Aug 2022 Week 2 < 0.005 / mg/L < 0.0002 / lbs/day
Aug 2022 Week 4 < 0.005 / mg/L < /
Aug 2022 Average < 0.005 /2.15 mg/L < 0.0002 / lbs/day
2022 Quarter 3 < 0.005 / mg/L < 0.0002 / lbs/day
2022 2nd 6 Months(Avg) < 0.005 / mg/L < 0.0002 / lbs/day
2022 2nd 6...(Max) < 0.005 / mg/L < 0.0002 / lbs/day
2022 2nd 6...(Min) < 0.005 / mg/L < /
2022 2nd 6...(Count) 2 / 1 /
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
08/11/2022 P TriPharm081122POT 0.85 / mg/L 0.0314 / lbs/day
W
08/30/2022 S TriPharm083022Self 0.66 / mg/L /
Aug 2022 Week 2 0.85 / mg/L 0.0314 / lbs/day
Aug 2022 Week 4 0.66 / mg/L /
Aug 2022 Average 0.76 / mg/L 0.0314 / lbs/day
2022 Quarter 3 0.76 / mg/L 0.0314 / lbs/day
2022 2nd 6 Months(Avg) 0.76 / mg/L 0.0314 / lbs/day
2022 2nd 6...(Max) 0.85 / mg/L 0.0314 / lbs/day
2022 2nd 6...(Min) 0.66 / mg/L /
2022 2nd 6...(Count) 2 / 1 /
Sample Date SampleID Result/Limit Mass/Limit
Isopropyl acetate
08/11/2022 P TriPharm081122POT < 0.005 /5.44 mg/L < 0.0002 / lbs/day
W
08/30/2022 S TriPharm083022Self < 0.005 /5.44 mg/L < /
Aug 2022 Week 2 < 0.005 / mg/L < 0.0002 / lbs/day
Aug 2022 Week 4 < 0.005 / mg/L < /
Aug 2022 Average < 0.005 /2.15 mg/L < 0.0002 / lbs/day
2022 Quarter 3 < 0.005 / mg/L < 0.0002 / lbs/day
Monday,February 27,2023 3:47:36PM *Indicates Violation **Indicates TRC Violation Page 4 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Isopropyl acetate
2022 2nd 6 Months(Avg) < 0.005 / mg/L < 0.0002 / lbs/day
2022 2nd 6...(Max) < 0.005 / mg/L < 0.0002 / lbs/day
2022 2nd 6...(Min) < 0.005 / mg/L < /
2022 2nd 6...(Count) 2 / 1 /
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
08/10/2022 P TriPharm081022POT 0.000002 /0.000142 mg/L /
WHg
08/30/2022 S TriPharm083022Self-I 0.000002 /0.000142 mg/L /
g
Aug 2022 Week 2 0.000002 / mg/L /
Aug 2022 Week 4 0.000002 / mg/L /
Aug 2022 Average 0.000002 / mg/L /
2022 Quarter 3 0.000002 / mg/L /
2022 2nd 6 Months(Avg) 0.000002 / mg/L /
2022 2nd 6...(Max) 0.000002 / mg/L /
2022 2nd 6...(Min) 0.000002 / mg/L /
2022 2nd 6...(Count) 2
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
08/11/2022 P TriPharm081122POT < 0.003 /0.78 mg/L < 0.000092 / lbs/day
W
08/30/2022 S TriPharm083022Self < 0.003 /0.78 mg/L < /
Aug 2022 Week 2 < 0.003 / mg/L < 0.000092 / lbs/day
Aug 2022 Week 4 < 0.003 / mg/L < /
Monday,February 27,2023 3:47:36PM *Indicates Violation **Indicates TRC Violation Page 5 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
Methylene Chloride
Aug 2022 Average < 0.003 /0.18 mg/L < 0.000092 / lbs/day
2022 Quarter 3 < 0.003 / mg/L < 0.000092 / lbs/day
2022 2nd 6 Months(Avg) < 0.003 / mg/L < 0.000092 / lbs/day
2022 2nd 6...(Max) < 0.003 / mg/L < 0.000092 / lbs/day
2022 2nd 6...(Min) < 0.003 / mg/L < /
2022 2nd 6...(Count) 2 / 1 /
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Molybdenum
08/11/2022 P TriPharm081122POT < 0.001 / mg/L < 0 / lbs/day
W
08/30/2022 S TriPharm083022Self < 0.001 / mg/L < /
Aug 2022 Week 2 < 0.001 / mg/L < 0 / lbs/day
Aug 2022 Week 4 < 0.001 / mg/L < /
Aug 2022 Average < 0.001 / mg/L < 0 / lbs/day
2022 Quarter 3 < 0.001 / mg/L < 0 / lbs/day
2022 2nd 6 Months(Avg) < 0.001 / mg/L < 0.0000 / lbs/day
2022 2nd 6...(Max) < 0.001 / mg/L < 0.0000 / lbs/day
2022 2nd 6...(Min) < 0.001 / mg/L < /
2022 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
08/11/2022 P TriPharm081122POT < 0.005 /5.44 mg/L < 0.0002 / lbs/day
W
08/30/2022 S TriPharm083022Self < 0.005 /5.44 mg/L < /
Aug 2022 Week 2 < 0.005 / mg/L < 0.0002 / lbs/day
Aug 2022 Week 4 < 0.005 / mg/L < /
Aug 2022 Average < 0.005 /2.15 mg/L < 0.0002 / lbs/day
2022 Quarter 3 < 0.005 / mg/L < 0.0002 / lbs/day
2022 2nd 6 Months(Avg) < 0.005 / mg/L < 0.0002 / lbs/day
2022 2nd 6...(Max) < 0.005 / mg/L < 0.0002 / lbs/day
2022 2nd 6...(Min) < 0.005 / mg/L < /
2022 2nd 6...(Count) 2 / 1 /
Monday,February 27,2023 3:47:36PM *Indicates Violation **Indicates TRC Violation Page 6 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Nitrate-Nitrite
08/11/2022 P TriPharm081122POT 0.6 / mg/L 0.023 / lbs/day
W
08/30/2022 S TriPharm083022Self 0.8 / mg/L /
Aug 2022 Week 2 0.6 / mg/L 0.023 / lbs/day
Aug 2022 Week 4 0.8 / mg/L /
Aug 2022 Average 0.7 / mg/L 0.023 / lbs/day
2022 Quarter 3 0.7 / mg/L 0.023 / lbs/day
2022 2nd 6 Months(Avg) 0.7 / mg/L 0.023 / lbs/day
2022 2nd 6...(Max) 0.8 / mg/L 0.023 / lbs/day
2022 2nd 6...(Min) 0.6 / mg/L /
2022 2nd 6...(Count) 2 / 1 /
Sample Date SampleID Result/Limit Mass/Limit
Nitrogen,Total
08/11/2022 P TriPharm081122POT 1.42 / mg/L 0.052 / lbs/day
W
08/30/2022 S TriPharm083022Self 1.17 / mg/L /
Aug 2022 Week 2 1.42 / mg/L 0.052 / lbs/day
Aug 2022 Week 4 1.17 / mg/L /
Aug 2022 Average 1.3 / mg/L 0.052 / lbs/day
2022 Quarter 3 1.3 / mg/L 0.052 / lbs/day
2022 2nd 6 Months(Avg) 1.30 / mg/L 0.052 / lbs/day
2022 2nd 6...(Max) 1.42 / mg/L 0.052 / lbs/day
2022 2nd 6...(Min) 1.17 / mg/L /
2022 2nd 6...(Count) 2 / 1 /
Sample Date SampleID Result/Limit Mass/Limit
pH
08/11/2022 P TriPharm081122POT 7.8 /5.5-10.5 SU /
W
08/30/2022 S TriPharm083022Self 7.3 /5.5-10.5 SU /
Aug 2022 Week 2 7.8 / SU /
Aug 2022 Week 4 7.3 / SU /
Aug 2022 Average 7.55 / SU /
2022 Quarter 3 7.55 / SU /
Monday,February 27,2023 3:47:36PM *Indicates Violation **Indicates TRC Violation Page 7 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
pH
2022 2nd 6 Months(Avg) 7.55 / SU /
2022 2nd 6...(Max) 7.8 / SU /
2022 2nd 6...(Min) 7.3 / SU /
2022 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
08/11/2022 P TriPharm081122POT 32 /66 °C /
W
08/30/2022 S TriPharm083022Self 32 /66 °C /
Aug 2022 Week 2 32 / °C /
Aug 2022 Week 4 32 / °C /
Aug 2022 Average 32 / °C /
2022 Quarter 3 32 / °C /
2022 2nd 6 Months(Avg) 32 / °C /
2022 2nd 6...(Max) 32 / °C /
2022 2nd 6...(Min) 32 / °C /
2022 2nd 6...(Count) 2
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
08/11/2022 P TriPharm081122POT 0.8 / mg/L 0.03 / lbs/day
W
08/30/2022 S TriPharm083022Self 0.39 / mg/L /
Aug 2022 Week 2 0.8 / mg/L 0.03 / lbs/day
Aug 2022 Week 4 0.39 / mg/L /
Monday,February 27,2023 3:47:36PM *Indicates Violation **Indicates TRC Violation Page 8 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
TKN
Aug 2022 Average 0.6 / mg/L 0.03 / lbs/day
2022 Quarter 3 0.6 / mg/L 0.03 / lbs/day
2022 2nd 6 Months(Avg) 0.60 / mg/L 0.030 / lbs/day
2022 2nd 6...(Max) 0.8 / mg/L 0.030 / lbs/day
2022 2nd 6...(Min) 0.39 / mg/L /
2022 2nd 6...(Count) 2 / 1 /
Sample Date SampleID Result/Limit Mass/Limit
Total Phosphorus
08/11/2022 P TriPharm081122POT 0.585 / mg/L 0.0216 / lbs/day
W
08/30/2022 S TriPharm083022Self 0.921 / mg/L /
Aug 2022 Week 2 0.585 / mg/L 0.0216 / lbs/day
Aug 2022 Week 4 0.921 / mg/L /
Aug 2022 Average 0.753 / mg/L 0.0216 / lbs/day
2022 Quarter 3 0.753 / mg/L 0.0216 / lbs/day
2022 2nd 6 Months(Avg) 0.753 / mg/L 0.0216 / lbs/day
2022 2nd 6...(Max) 0.921 / mg/L 0.0216 / lbs/day
2022 2nd 6...(Min) 0.585 / mg/L /
2022 2nd 6...(Count) 2 / 1 /
Sample Date Sample-ID Result/Limit Mass/Limit
TSS
08/11/2022 P TriPharm081122POT < 1.5 / mg/L < 0.055357 / lbs/day
W
08/30/2022 S TriPharm083022Self < 1.6 / mg/L < /
Aug 2022 Week 2 < 1.5 / mg/L < 0.055357 / lbs/day
Aug 2022 Week 4 < 1.6 / mg/L < /
Aug 2022 Average < 1.5 / mg/L < 0.055357 / lbs/day
2022 Quarter 3 < 1.5 / mg/L < 0.055357 / lbs/day
2022 2nd 6 Months(Avg) < 1.5 / mg/L < 0.055357 / lbs/day
2022 2nd 6...(Max) < 1.6 / mg/L < 0.055357 / lbs/day
2022 2nd 6...(Min) < 1.5 / mg/L < /
2022 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
08/11/2022 P TriPharm081122POT 0.0087 / mg/L /
W
08/30/2022 S TriPharm083022Self < 0.005 / mg/L < /
Aug 2022 Week 2 0.0087 / mg/L /
Aug 2022 Week 4 < 0.005 / mg/L < /
Monday,February 27,2023 3:47:36PM *Indicates Violation **Indicates TRC Violation Page 9 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample-ID Result/Limit Mass/Limit
VOC
Aug 2022 Average < 0.0069 / mg/L < /
2022 Quarter 3 < 0.0069 / mg/L < /
2022 2nd 6 Months(Avg) < 0.0069 / mg/L < /
2022 2nd 6...(Max) 0.0087 / mg/L /
2022 2nd 6...(Min) < 0.005 / mg/L < /
2022 2nd 6...(Count) 2 / /
Sample Date SampleID Result/Limit Mass/Limit
Zinc
08/11/2022 P TriPharm081122POT 0.284 / mg/L 0.010481 / lbs/day
W
08/30/2022 S TriPharm083022Self 0.189 / mg/L /
Aug 2022 Week 2 0.284 / mg/L 0.010481 / lbs/day
Aug 2022 Week 4 0.189 / mg/L /
Aug 2022 Average 0.237 / mg/L 0.010481 / lbs/day
2022 Quarter 3 0.237 / mg/L 0.010481 / lbs/day
2022 2nd 6 Months(Avg) 0.237 / mg/L 0.010481 / lbs/day
2022 2nd 6...(Max) 0.284 / mg/L 0.010481 / lbs/day
2022 2nd 6...(Min) 0.189 / mg/L /
2022 2nd 6...(Count) 2 / 1 /
Monday,February 27,2023 3:47:36PM *Indicates Violation **Indicates TRC Violation Page 10 of 10

United Therapeutics Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
07/14/2022 S UTP1071422Self 3.7 / mg/L 1.3226 / lbs/day
08/10/2022 P UTP1081022POTW 2.1 / mg/L /
Jul 2022 Week 2 3.7 / mg/L 1.3226 / lbs/day
Aug 2022 Week 2 2.1 / mg/L /
Jul 2022 Average 3.7 / mg/L 1.3226 / lbs/day
Aug 2022 Average 2.1 / mg/L /
2022 Quarter 3 2.9 / mg/L 1.3226 / lbs/day
2022 2nd 6 Months(Avg) 2.9 / mg/L 1.3226 / lbs/day
2022 2nd 6...(Max) 3.7 / mg/L 1.3226 / lbs/day
2022 2nd 6...(Min) 2.1 / mg/L /
2022 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2022 S UTP10722171ow 0.036 / MGD /
08/31/2022 S UTP10822F1ow 0.035 / MGD /
09/30/2022 S UTP10922F1ow 0.03 / MGD /
10/31/2022 S UTPI1022F1ow 0.027 / MGD /
11/30/2022 S UTP11122171ow 0.031 / MGD /
12/31/2022 S UTP11222171ow 0.026 / MGD /
Jul 2022 Week 4 0.036 / MGD /
Aug 2022 Week 4 0.035 / MGD /
Sep 2022 Week 4 0.03 / MGD /
Oct 2022 Week 4 0.027 / MGD /
Nov 2022 Week 4 0.031 / MGD /
Dec 2022 Week 4 0.026 / MGD /
Jul 2022 Average 0.036 / MGD /
Aug 2022 Average 0.035 / MGD /
Sep 2022 Average 0.03 / MGD /
Oct 2022 Average 0.027 / MGD /
Nov 2022 Average 0.031 / MGD /
Dec 2022 Average 0.026 / MGD /
2022 Quarter 3 0.033667 / MGD /
2022 Quarter 4 0.028 / MGD /
2022 2nd 6 Months(Avg) 0.030833 / MGD /
2022 2nd 6...(Max) 0.036 / MGD /
2022 2nd 6...(Min) 0.026 / MGD /
Tuesday,February 21,2023 10:23:40PM *Indicates Violation **Indicates TRC Violation Pagel of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
2022 2nd 6...(Count) 6
Sample Date SamplelD Result/Limit Mass/Limit
BOD
07/14/2022 S UTP1071422Self 32.9 / mg/L 11.76 / lbs/day
08/10/2022 P UTP1081022POTW 40.6 / mg/L /
Jul 2022 Week 2 32.9 / mg/L 11.76 / lbs/day
Aug 2022 Week 2 40.6 / mg/L /
Jul 2022 Average 32.9 / mg/L 11.76 / lbs/day
Aug 2022 Average 40.6 / mg/L /
2022 Quarter 3 36.8 / mg/L 11.76 / lbs/day
2022 2nd 6 Months(Avg) 36.8 / mg/L 11.760 / lbs/day
2022 2nd 6...(Max) 40.6 / mg/L 11.760 / lbs/day
2022 2nd 6...(Min) 32.9 / mg/L /
2022 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
07/14/2022 S UTP1071422Self < 0.0005 / mg/L < 0.000179 / lbs/day
Jul 2022 Week 2 < 0.0005 / mg/L < 0.000179 / lbs/day
Jul 2022 Average < 0.0005 / mg/L < 0.000179 / lbs/day
2022 Quarter 3 < 0.0005 / mg/L < 0.000179 / lbs/day
2022 2nd 6 Months(Avg) < 0.0005 / mg/L < 0.000179 / lbs/day
2022 2nd 6...(Max) < 0.0005 / mg/L < 0.000179 / lbs/day
2022 2nd 6...(Min) < 0.0005 / mg/L < 0.000179 / lbs/day
2022 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
07/14/2022 S UTP1071422Self 60.5 / mg/L 21.6259 / lbs/day
08/10/2022 P UTP1081022POTW 29.5 / mg/L /
Jul 2022 Week 2 60.5 / mg/L 21.6259 / lbs/day
Aug 2022 Week 2 29.5 / mg/L /
Jul 2022 Average 60.5 / mg/L 21.6259 / lbs/day
Aug 2022 Average 29.5 / mg/L /
2022 Quarter 3 45 / mg/L 21.6259 / lbs/day
Tuesday,February 21,2023 10:23:40PM *Indicates Violation **Indicates TRC Violation Page 2 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
2022 2nd 6 Months(Avg) 45 / mg/L 21.6259 / lbs/day
2022 2nd 6...(Max) 60.5 / mg/L 21.6259 / lbs/day
2022 2nd 6...(Min) 29.5 / mg/L /
2022 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
COD
07/14/2022 S UTP1071422Self 138 / mg/L 49.33 / lbs/day
08/10/2022 P UTP1081022POTW 92 / mg/L /
Jul 2022 Week 2 138 / mg/L 49.33 / lbs/day
Aug 2022 Week 2 92 / mg/L /
Jul 2022 Average 138 / mg/L 49.33 / lbs/day
Aug 2022 Average 92 / mg/L /
2022 Quarter 3 115 / mg/L 49.33 / lbs/day
2022 2nd 6 Months(Avg) 115 / mg/L 49.33 / lbs/day
2022 2nd 6...(Max) 138 / mg/L 49.33 / lbs/day
2022 2nd 6...(Min) 92 / mg/L /
2022 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
07/14/2022 S UTP1071422Self 1.4 / mg/L 0.5004 / lbs/day
Jul 2022 Week 2 1.4 / mg/L 0.5004 / lbs/day
Jul 2022 Average 1.4 / mg/L 0.5004 / lbs/day
2022 Quarter 3 1.4 / mg/L 0.5004 / lbs/day
2022 2nd 6 Months(Avg) 1.4 / mg/L 0.5004 / lbs/day
2022 2nd 6...(Max) 1.4 / mg/L 0.5004 / lbs/day
2022 2nd 6...(Min) 1.4 / mg/L 0.5004 / lbs/day
2022 2nd 6...(Count) 1 / I /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
07/14/2022 S UTP1071422SelfHg 0.000002 / 0.000142 mg/L /
08/10/2022 P UTP1081022POTW 0.000002 / 0.000142 mg/L /
Hg
Jul 2022 Week 2 0.000002 / mg/L /
Aug 2022 Week 2 0.000002 / mg/L /
Tuesday,February 21,2023 10:23:40PM *Indicates Violation **Indicates TRC Violation Page 3 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
Jul 2022 Average 0.000002 / mg/L /
Aug 2022 Average 0.000002 / mg/L /
2022 Quarter 3 0.000002 / mg/L /
2022 2nd 6 Months(Avg) 0.000002 / mg/L /
2022 2nd 6...(Max) 0.000002 / mg/L /
2022 2nd 6...(Min) 0.000002 / mg/L /
2022 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
07/14/2022 S UTP1071422Self < 0.003 / mg/L < 0.0009 / lbs/day
Jul 2022 Week 2 < 0.003 / mg/L < 0.0009 / lbs/day
Jul 2022 Average < 0.003 / mg/L < 0.0009 / lbs/day
2022 Quarter 3 < 0.003 / mg/L < 0.0009 / lbs/day
2022 2nd 6 Months(Avg) < 0.003 / mg/L < 0.0009 / lbs/day
2022 2nd 6...(Max) < 0.003 / mg/L < 0.0009 / lbs/day
2022 2nd 6...(Min) < 0.003 / mg/L < 0.0009 / lbs/day
2022 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
07/14/2022 S UTP1071422Self 0.6 / mg/L 0.2 / lbs/day
08/10/2022 P UTP1081022POTW 0.3 / mg/L /
Jul 2022 Week 2 0.6 / mg/L 0.2 / lbs/day
Aug 2022 Week 2 0.3 / mg/L /
Jul 2022 Average 0.6 / mg/L 0.2 / lbs/day
Aug 2022 Average 0.3 / mg/L /
2022 Quarter 3 0.4 / mg/L 0.2 / lbs/day
2022 2nd 6 Months(Avg) 0.4 / mg/L 0.200 / lbs/day
2022 2nd 6...(Max) 0.6 / mg/L 0.200 / lbs/day
2022 2nd 6...(Min) 0.3 / mg/L /
2022 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
07/14/2022 S UTP1071422Self 13.5 / mg/L 4.826 / lbs/day
Tuesday,February 21,2023 10:23:40PM *Indicates Violation **Indicates TRC Violation Page 4 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
08/10/2022 P UTP1081022POTW 7.12 / mg/L /
Jul 2022 Week 2 13.5 / mg/L 4.826 / lbs/day
Aug 2022 Week 2 7.12 / mg/L /
Jul 2022 Average 13.5 / mg/L 4.826 / lbs/day
Aug 2022 Average 7.12 / mg/L /
2022 Quarter 3 10.31 / mg/L 4.826 / lbs/day
2022 2nd 6 Months(Avg) 10.31 / mg/L 4.826 / lbs/day
2022 2nd 6...(Max) 13.5 / mg/L 4.826 / lbs/day
2022 2nd 6...(Min) 7.12 / mg/L /
2022 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
07/14/2022 S UTP1071422Self < 2.5 / 200 mg/L < /
08/10/2022 P UTP1081022POTW < 2.5 / 200 mg/L < /
Jul 2022 Week 2 < 2.5 / mg/L < /
Aug 2022 Week 2 < 2.5 / mg/L < /
Jul 2022 Average < 2.5 / mg/L < /
Aug 2022 Average < 2.5 / mg/L < /
2022 Quarter 3 < 2.5 / mg/L < /
2022 2nd 6 Months(Avg) < 2.5 / mg/L < /
2022 2nd 6...(Max) < 2.5 / mg/L < /
2022 2nd 6...(Min) < 2.5 / mg/L < /
2022 2nd 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
pH
07/14/2022 S UTP1071422Self 7.3 / 5.5-10.0 Su /
08/10/2022 P UTP1081022POTW 7 / 5.5-10.0 su /
Jul 2022 Week 2 7.3 / su /
Aug 2022 Week 2 7 / su /
Jul 2022 Average 7.3 / su /
Aug 2022 Average 7 / Su /
2022 Quarter 3 7.15 / su /
2022 2nd 6 Months(Avg) 7.15 / su /
2022 2nd 6...(Max) 7.3 / su /
2022 2nd 6...(Min) 7 / Su /
Tuesday,February 21,2023 10:23:40PM *Indicates Violation **Indicates TRC Violation Page 5 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
pH
2022 2nd 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
07/14/2022 S UTP1071422Self 27 / 66 °C /
08/10/2022 P UTP1081022POTW 26 / 66 °C /
Jul 2022 Week 2 27 / °C /
Aug 2022 Week 2 26 / °C /
Jul 2022 Average 27 / °C /
Aug 2022 Average 26 / °C /
2022 Quarter 3 26.5 / °C /
2022 2nd 6 Months(Avg) 26.5 / °C /
2022 2nd 6...(Max) 27 / °C /
2022 2nd 6...(Min) 26 / °C /
2022 2nd 6...(Count) 2
Sample Date SamplelD Result/Limit Mass/Limit
TKN
07/14/2022 S UTP1071422Self 12.9 / mg/L 4.611 / lbs/day
08/10/2022 P UTP1081022POTW 6.87 / mg/L /
Jul 2022 Week 2 12.9 / mg/L 4.611 / lbs/day
Aug 2022 Week 2 6.87 / mg/L /
Jul 2022 Average 12.9 / mg/L 4.611 / lbs/day
Aug 2022 Average 6.87 / mg/L /
2022 Quarter 3 9.89 / mg/L 4.611 / lbs/day
2022 2nd 6 Months(Avg) 9.89 / mg/L 4.611 / lbs/day
2022 2nd 6...(Max) 12.9 / mg/L 4.611 / lbs/day
2022 2nd 6...(Min) 6.87 / mg/L /
2022 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
07/14/2022 S UTP1071422Self 2.1 / mg/L 0.7507 / lbs/day
08/10/2022 P UTP1081022POTW 1.5 / mg/L /
Jul 2022 Week 2 2.1 / mg/L 0.7507 / lbs/day
Aug 2022 Week 2 1.5 / mg/L /
Tuesday,February 21,2023 10:23:40PM *Indicates Violation **Indicates TRC Violation Page 6 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
Jul 2022 Average 2.1 / mg/L 0.7507 / lbs/day
Aug 2022 Average 1.5 / mg/L /
2022 Quarter 3 1.8 / mg/L 0.7507 / lbs/day
2022 2nd 6 Months(Avg) 1.8 / mg/L 0.7507 / lbs/day
2022 2nd 6...(Max) 2.1 / mg/L 0.7507 / lbs/day
2022 2nd 6...(Min) 1.5 / mg/L /
2022 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
TSS
07/14/2022 S UTP1071422Self 19.3 / mg/L 6.898831 / lbs/day
08/10/2022 P UTP1081022POTW 20 / mg/L /
Jul 2022 Week 2 19.3 / mg/L 6.898831 / lbs/day
Aug 2022 Week 2 20 / mg/L /
Jul 2022 Average 19.3 / mg/L 6.898831 / lbs/day
Aug 2022 Average 20 / mg/L /
2022 Quarter 3 19.7 / mg/L 6.898831 / lbs/day
2022 2nd 6 Months(Avg) 19.7 / mg/L 6.89883 / lbs/day
2022 2nd 6...(Max) 20 / mg/L 6.898831 / lbs/day
2022 2nd 6...(Min) 19.3 / mg/L /
2022 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
07/14/2022 S UTP1071422Self 0.0229 / mg/L /
Jul 2022 Week 2 0.0229 / mg/L /
Jul 2022 Average 0.0229 / mg/L /
2022 Quarter 3 0.0229 / mg/L /
2022 2nd 6 Months(Avg) 0.0229 / mg/L /
2022 2nd 6...(Max) 0.0229 / mg/L /
2022 2nd 6...(Min) 0.0229 / mg/L /
2022 2nd 6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
07/14/2022 S UTP1071422Self 0.87 / mg/L 0.310984 / lbs/day
Tuesday,February 21,2023 10:23:40PM *Indicates Violation **Indicates TRC Violation Page 7 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
Jul 2022 Week 2 0.87 / mg/L 0.310984 / lbs/day
Jul 2022 Average 0.87 / mg/L 0.310984 / lbs/day
2022 Quarter 3 0.87 / mg/L 0.310984 / lbs/day
2022 2nd 6 Months(Avg) 0.87 / mg/L 0.310984 / lbs/day
2022 2nd 6...(Max) 0.87 / mg/L 0.310984 / lbs/day
2022 2nd 6...(Min) 0.87 / mg/L 0.310984 / lbs/day
2022 2nd 6...(Count) 1 / 1 /
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 002
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
07/14/2022 S UTP2071422Self 0.002 / 20.7 mg/L /
Jul 2022 Week 2 0.002 / mg/L /
Jul 2022 Average 0.002 / 8.2 mg/L /
2022 Quarter 3 0.002 / mg/L /
2022 2nd 6 Months(Avg) 0.002 / mg/L /
2022 2nd 6...(Max) 0.002 / mg/L /
2022 2nd 6...(Min) 0.002 / mg/L /
2022 2nd 6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
07/14/2022 S UTP2071422Self < 0.001 / 20.7 mg/L < /
Jul 2022 Week 2 < 0.001 / mg/L < /
Jul 2022 Average < 0.001 / 8.2 mg/L < /
2022 Quarter 3 < 0.001 / mg/L < /
2022 2nd 6 Months(Avg) < 0.001 / mg/L < /
2022 2nd 6...(Max) < 0.001 / mg/L < /
2022 2nd 6...(Min) < 0.001 / mg/L < /
2022 2nd 6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
07/14/2022 S UTP2071422Self < 0.001 / 20.7 mg/L < /
Tuesday,February 21,2023 10:23:40PM *Indicates Violation **Indicates TRC Violation Page 8 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 002
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
Jul 2022 Week 2 < 0.001 / mg/L < /
Jul 2022 Average < 0.001 / 8.2 mg/L < /
2022 Quarter 3 < 0.001 / mg/L < /
2022 2nd 6 Months(Avg) < 0.001 / mg/L < /
2022 2nd 6...(Max) < 0.001 / mg/L < /
2022 2nd 6...(Min) < 0.001 / mg/L < /
2022 2nd 6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
07/14/2022 S UTP2071422Self 0.047 / 3.0 mg/L /
Jul 2022 Week 2 0.047 / mg/L /
Jul 2022 Average 0.047 / 0.7 mg/L /
2022 Quarter 3 0.047 / mg/L /
2022 2nd 6 Months(Avg) 0.047 / mg/L /
2022 2nd 6...(Max) 0.047 / mg/L /
2022 2nd 6...(Min) 0.047 / mg/L /
2022 2nd 6...(Count) 1
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
07/14/2022 S UTP2071422Self < 0.003 / 20.7 mg/L < /
Jul 2022 Week 2 < 0.003 / mg/L < /
Jul 2022 Average < 0.003 / 8.2 mg/L < /
2022 Quarter 3 < 0.003 / mg/L < /
2022 2nd 6 Months(Avg) < 0.003 / mg/L < /
2022 2nd 6...(Max) < 0.003 / mg/L < /
2022 2nd 6...(Min) < 0.003 / mg/L < /
2022 2nd 6...(Count) 1
Tuesday,February 21,2023 10:23:40PM *Indicates Violation **Indicates TRC Violation Page 1 of 1

Wolfspeed Durham
SAMPLE OVERVIEW
71812022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
08/23/2022 S WolfspeedP8082322 18.32 / mg/L /
Self
10/26/2022 P WolfspeedP8102622 21.1 / mg/L 78.3084 / lbs/day
POTW
Aug 2022 Week 4 18.32 / mg/L /
Oct 2022 Week 4 21.1 / mg/L 78.3084 / lbs/day
Aug 2022 Average 18.32 / mg/L /
Oct 2022 Average 21.1 / mg/L 78.3084 / lbs/day
2022 Quarter 3 18.32 / mg/L /
2022 Quarter 4 21.1 / mg/L 78.3084 / lbs/day
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2022 S CreeP80722F1ow 0.396031 / MGD /
08/31/2022 S CreeP80822Flow 0.42658 / MGD /
09/30/2022 S CreeP80922F1ow 0.430034 / MGD /
10/31/2022 S WolfspeedP81022F1 0.446132 / MGD /
ow
11/30/2022 S WolfspeedP81122F10 0.483766 / MGD /
w
12/31/2022 S WolfspeedP81222F1 0.453032 / MGD /
ow
Ju12022 Week 4 0.396031 / MGD /
Aug 2022 Week 4 0.42658 / MGD /
Sep 2022 Week 4 0.430034 / MGD /
Oct 2022 Week 4 0.446132 / MGD /
Nov 2022 Week 4 0.483766 / MGD /
Dec 2022 Week 4 0.453032 / MGD /
Ju12022 Average 0.396031 / MGD /
Aug 2022 Average 0.42658 / MGD /
Sep 2022 Average 0.430034 / MGD /
Oct 2022 Average 0.446132 / MGD /
Nov 2022 Average 0.483766 / MGD /
Dec 2022 Average 0.453032 / MGD /
2022 Quarter 3 0.417548 / MGD /
2022 Quarter 4 0.460977 / MGD /
Sample Date SamplelD Result/Limit Mass/Limit
Barium
Tuesday,February 28,2023 10:31:03AM *Indicates Violation **Indicates TRC Violation Page 1 of 5

Wolfspeed Durham
SAMPLE OVERVIEW
71812022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Barium
08/23/2022 S WolfspeedP8082322 0.028 / mg/L /
Self
Aug 2022 Week 4 0.028 / mg/L /
Aug 2022 Average 0.028 / mg/L /
2022 Quarter 3 0.028 / mg/L /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
08/23/2022 S WolfspeedP8082322 126 / mg/L /
Self
10/26/2022 P WolfspeedP8102622 80 / mg/L 296.904 / lbs/day
POTW
Aug 2022 Week 4 126 / mg/L /
Oct 2022 Week 4 80 / mg/L 296.904 / lbs/day
Aug 2022 Average 126 / mg/L /
Oct 2022 Average 80 / mg/L 296.904 / lbs/day
2022 Quarter 3 126 / mg/L /
2022 Quarter 4 80 / mg/L 296.904 / lbs/day
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
08/23/2022 S WolfspeedP8082322 < 0.003 / mg/L < /
Self
10/26/2022 P WolfspeedP8102622 0.006 / mg/L 0.022268 / lbs/day
POTW
Aug 2022 Week 4 < 0.003 / mg/L < /
Oct 2022 Week 4 0.006 / mg/L 0.022268 / lbs/day
Aug 2022 Average < 0.003 / mg/L < /
Oct 2022 Average 0.006 / mg/L 0.022268 / lbs/day
2022 Quarter 3 < 0.003 / mg/L < /
2022 Quarter 4 0.006 / mg/L 0.022268 / lbs/day
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
08/23/2022 S WolfspeedP8082322 1.7 / mg/L /
Self
10/26/2022 P WolfspeedP8102622 1.98 / mg/L 7.3484 / lbs/day
POTW
Aug 2022 Week 4 1.7 / mg/L /
Oct 2022 Week 4 1.98 / mg/L 7.3484 / lbs/day
Tuesday,February 28,2023 10:31:03AM *Indicates Violation **Indicates TRC Violation Page 2 of 5

Wolfspeed Durham
SAMPLE OVERVIEW
71812022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
Aug 2022 Average 1.7 / mg/L /
Oct 2022 Average 1.98 / mg/L 7.3484 / lbs/day
2022 Quarter 3 1.7 / mg/L /
2022 Quarter 4 1.98 / mg/L 7.3484 / lbs/day
Sample Date SamplelD Result/Limit Mass/Limit
Iodine
08/23/2022 S WolfspeedP8082322 0.014 / mg/L /
Self
Aug 2022 Week 4 0.014 / /
Aug 2022 Average 0.014
2022 Quarter 3 0.014
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
08/23/2022 S WolfspeedP8082322 0.000006 / mg/L /
Self
10/25/2022 P WolfspeedP8102522 0.000007 / mg/L /
POTWHg
Aug 2022 Week 4 0.000006 / mg/L /
Oct 2022 Week 4 0.000007 / mg/L /
Aug 2022 Average 0.000006 / mg/L /
Oct 2022 Average 0.000007 / mg/L /
2022 Quarter 3 0.000006 / mg/L /
2022 Quarter 4 0.000007 / mg/L /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
08/23/2022 S WolfspeedP8082322 6 / mg/L /
Self
10/26/2022 P WolfspeedP8102622 5.6 / mg/L 20.932 / lbs/day
POTW
Aug 2022 Week 4 6 / mg/L /
Oct 2022 Week 4 5.6 / mg/L 20.932 / lbs/day
Aug 2022 Average 6 / mg/L /
Oct 2022 Average 5.6 / mg/L 20.932 / lbs/day
2022 Quarter 3 6 / mg/L /
2022 Quarter 4 5.6 / mg/L 20.932 / lbs/day
Tuesday,February 28,2023 10:31:03AM *Indicates Violation **Indicates TRC Violation Page 3 of 5

Wolfspeed Durham
SAMPLE OVERVIEW
71812022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
08/23/2022 S WolfspeedP8082322 30.81 / mg/L /
Self
10/26/2022 P WolfspeedP8102622 31.9 / mg/L 118.39 / lbs/day
POTW
Aug 2022 Week 4 30.81 / mg/L /
Oct 2022 Week 4 31.9 / mg/L 118.39 / lbs/day
Aug 2022 Average 30.81 / mg/L /
Oct 2022 Average 31.9 / mg/L 118.39 / lbs/day
2022 Quarter 3 30.81 / mg/L /
2022 Quarter 4 31.9 / mg/L 118.39 / lbs/day
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
10/26/2022 P WolfspeedP8102622 < 2.5 / mg/L < /
POTW
Oct 2022 Week 4 < 2.5 / mg/L < /
Oct 2022 Average < 2.5 / mg/L < /
2022 Quarter 4 < 2.5 / mg/L < /
Sample Date SamplelD Result/Limit Mass/Limit
pH
08/23/2022 S WolfspeedP8082322 8.6 / 5.0-10.5 Su /
Self
10/26/2022 P WolfspeedP8102622 8.9 / 5.0-10.5 Su /
POTW
Aug 2022 Week 4 8.6 / Su /
Oct 2022 Week 4 8.9 / Su /
Aug 2022 Average 8.6 / Su /
Oct 2022 Average 8.9 / Su /
2022 Quarter 3 8.6 / Su /
2022 Quarter 4 8.9 / Su /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
08/23/2022 S WolfspeedP8082322 23.5 / 66 °C /
Self
10/26/2022 P WolfspeedP8102622 20 / 66 °C /
POTW
Aug 2022 Week 4 23.5 / °C /
Oct 2022 Week 4 20 / °C /
Tuesday,February 28,2023 10:31:03AM *Indicates Violation **Indicates TRC Violation Page 4 of 5

Wolfspeed Durham
SAMPLE OVERVIEW
71812022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
Aug 2022 Average 23.5 / °C /
Oct 2022 Average 20 / °C /
2022 Quarter 3 23.5 / °C /
2022 Quarter 20 / °C /
Sample Date SamplelD Result/Limit Mass/Limit
TKN
08/23/2022 S WolfspeedP8082322 24.84 / mg/L /
Self
10/26/2022 P WolfspeedP8102622 26.2 / mg/L 97.236 / lbs/day
POTW
Aug 2022 Week 4 24.84 / mg/L /
Oct 2022 Week 4 26.2 / mg/L 97.236 / lbs/day
Aug 2022 Average 24.84 / mg/L /
Oct 2022 Average 26.2 / mg/L 97.236 / lbs/day
2022 Quarter 3 24.84 / mg/L /
2022 Quarter 4 26.2 / mg/L 97.236 / lbs/day
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
08/23/2022 S WolfspeedP8082322 0.305 / mWL /
Self
Aug 2022 Week 4 0.305 / mg/L /
Aug 2022 Average 0.305 / mg/L /
2022 Quarter 3 0.305 / mg/L /
Sample Date SamplelD Result/Limit Mass/Limit
Zirconium
08/23/2022 S WolfspeedP8082322 < 0.0005 / mg/L < /
Self
Aug 2022 Week 4 < 0.0005 / < /
Aug 2022 Average < 0.0005 / < /
2022 Quarter 3 < 0.0005 / < /
71812022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 009
Tuesday,February 28,2023 10:31:03AM *Indicates Violation **Indicates TRC Violation Page 5 of 5

Wolfspeed Durham
SAMPLE OVERVIEW
71812022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2022 S CreeP90722F1ow 0.04986 / MGD /
08/31/2022 S CreeP90822F1ow 0.053088 / MGD /
09/30/2022 S CreeP90922Flow 0.090582 / MGD /
10/31/2022 S WolfspeedP91022F1 0.046633 / MGD /
ow
11/30/2022 S WolfspeedP91122F10 0.048043 / MGD /
w
12/31/2022 S WolfspeedP91222F1 0.043529 / MGD /
ow
Jul 2022 Week 4 0.04986 / MGD /
Aug 2022 Week 4 0.053088 / MGD /
Sep 2022 Week 4 0.090582 / MGD /
Oct 2022 Week 4 0.046633 / MGD /
Nov 2022 Week 4 0.048043 / MGD /
Dec 2022 Week 4 0.043529 / MGD /
Jul 2022 Average 0.04986 / MGD /
Aug 2022 Average 0.053088 / MGD /
Sep 2022 Average 0.090582 / MGD /
Oct 2022 Average 0.046633 / MGD /
Nov 2022 Average 0.048043 / MGD /
Dec 2022 Average 0.043529 / MGD /
2022 Quarter 3 0.06451 / MGD /
2022 Quarter 4 0.046068 / MGD /
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
08/23/2022 S WolfspeedP9082322 2.2 / mg/L /
Self
10/25/2022 P WolfspeedP9102522 0.64 / mg/L /
POTW
Aug 2022 Week 4 2.2 / mg/L /
Oct 2022 Week 4 0.64 / mg/L /
Aug 2022 Average 2.2 / mg/L /
Oct 2022 Average 0.64 / mg/L /
2022 Quarter 3 2.2 / mg/L /
2022 Quarter 4 0.64 / mg/L /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
Tuesday,February 28,2023 10:31:03AM *Indicates Violation **Indicates TRC Violation Page 1 of 2

Wolfspeed Durham
SAMPLE OVERVIEW
71812022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
08/23/2022 S WolfspeedP9082322 0.000004 / mg/L /
Self
10/25/2022 P WolfspeedP9102522 0.000007 / mg/L /
POTWhg
Aug 2022 Week 4 0.000004 / mg/L /
Oct 2022 Week 4 0.000007 / mg/L /
Aug 2022 Average 0.000004 / mg/L /
Oct 2022 Average 0.000007 / mg/L /
2022 Quarter 3 0.000004 / mg/L /
2022 Quarter 4 0.000007 / mg/L /
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
10/25/2022 P WolfspeedP9102522 0.002 / mg/L /
POTW
Oct 2022 Week 4 0.002 / mg/L /
Oct 2022 Average 0.002 / mg/L /
2022 Quarter 4 0.002 / mg/L /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
10/25/2022 P WolfspeedP9102522 < 2.5 / mg/L < /
POTW
Oct 2022 Week 4 < 2.5 / mg/L < /
Oct 2022 Average < 2.5 / mg/L < /
2022 Quarter 4 < 2.5 / mg/L < /
Sample Date SampleLD Result/Limit Mass I Limit
pH
08/23/2022 S WolfspeedP9082322 7.5 / 5.0-10.5 Su /
Self
10/25/2022 P WolfspeedP9102522 7 / 5.0-10.5 Su /
POTW
Aug 2022 Week 4 7.5 / Su /
Oct 2022 Week 4 7 / Su /
Aug 2022 Average 7.5 / Su /
Oct 2022 Average 7 / Su /
2022 Quarter 3 7.5 / Su /
2022 Quarter 4 7 / Su /
Tuesday,February 28,2023 10:31:03AM *Indicates Violation **Indicates TRC Violation Page 2 of 2

Wolfspeed Durham
SAMPLE OVERVIEW
71812022 To 1213112022 Sample Type: Effluent Wastewater Outfall: All
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2022 S Cree0722171ow 0.445891 / 0.600 MGD /
08/31/2022 S Cree0822171ow 0.479667 / 0.600 MGD /
09/30/2022 S Cree0922F1ow 0.520615 / 0.600 MGD /
10/31/2022 S Wolfspeed1022171ow 0.492765 / 0.600 MGD /
11/30/2022 S Wolfspeed1122171ow 0.530208 / 0.600 MGD /
12/31/2022 S Wolfspeed1222171ow 0.496561 / 0.600 MGD /
Jul 2022 Week 4 0.445891 / MGD /
Aug 2022 Week 4 0.479667 / MGD /
Sep 2022 Week 4 0.520615 / MGD /
Oct 2022 Week 4 0.492765 / MGD /
Nov 2022 Week 4 0.530208 / MGD /
Dec 2022 Week 4 0.496561 / MGD /
Jul 2022 Average 0.445891 / 0.451 MGD /
Aug 2022 Average 0.479667 / 0.451 MGD * /
Sep 2022 Average 0.520615 / 0.451 MGD * /
Oct 2022 Average 0.492765 / 0.451 MGD * /
Nov 2022 Average 0.530208 / 0.451 MGD * /
Dec 2022 Average 0.496561 / 0.451 MGD * /
2022 Quarter 3 0.482058 / MGD /
2022 Quarter 4 0.506511 / MGD /
71812022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 013
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2022 S CreeP130722F1ow 0.000223 / MGD /
08/31/2022 S CreePl30822F1ow 0.000458 / MGD /
09/30/2022 S CreeP130922F1ow 0.000564 / MGD /
10/31/2022 S WolfspeedP131022F 0.000688 / MGD /
low
11/30/2022 S WolfspeedP131122171 0.000646 / MGD /
ow
12/31/2022 S WolfspeedP131222F 0.000439 / MGD /
low
Jul 2022 Week 4 0.000223 / MGD /
Aug 2022 Week 4 0.000458 / MGD /
Sep 2022 Week 4 0.000564 / MGD /
Oct 2022 Week 4 0.000688 / MGD /
Tuesday,February 28,2023 10:31:03AM *Indicates Violation **Indicates TRC Violation Page 1 of 1

Wolfspeed Durham
SAMPLE OVERVIEW
71812022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 013
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Nov 2022 Week 4 0.000646 / MGD /
Dec 2022 Week 4 0.000439 / MGD /
Jul 2022 Average 0.000223 / 0.030 MGD /
Aug 2022 Average 0.000458 / 0.030 MGD /
Sep 2022 Average 0.000564 / 0.030 MGD /
Oct 2022 Average 0.000688 / 0.030 MGD /
Nov 2022 Average 0.000646 / 0.030 MGD /
Dec 2022 Average 0.000439 / 0.030 MGD /
2022 Quarter 3 0.000415 / MGD /
2022 Quarter 4 0.000591 / MGD /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
08/18/2022 S WolfspeedP1308182 < 0.00005 / 0.11 mg/L < /
2Self
08/23/2022 S WolfspeedP1308232 < 0.0005 / 0.11 mg/L < /
2Self
08/25/2022 S WolfspeedP1308252 < 0.00005 / 0.11 mg/L < /
2Self
10/24/2022 P WolfspeedP1310242 < 0.00008 / 0.11 mg/L < /
2POTW
Aug 2022 Week 3 < 0.00005 / mg/L < /
Aug 2022 Week 4 < 0.00028 / mg/L < /
Oct 2022 Week 4 < 0.00008 / mg/L < /
Aug 2022 Average < 0.0002 / 0.07 mg/L < /
Oct 2022 Average < 0.00008 / 0.07 mg/L < /
2022 Quarter 3 < 0.0002 / mg/L < /
2022 Quarter 4 < 0.00008 / mg/L < /
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
08/18/2022 S WolfspeedP1308182 < 0.003 / 2.77 mg/L < /
2Self
08/23/2022 S WolfspeedP1308232 < 0.003 / 2.77 mg/L < /
2Self
08/25/2022 S WolfspeedP1308252 < 0.003 / 2.77 mg/L < /
2Self
10/24/2022 P WolfspeedP1310242 < 0.001 / 2.77 mg/L < /
2POTW
Aug 2022 Week 3 < 0.003 / mg/L < /
Aug 2022 Week 4 < 0.003 / mg/L < /
Tuesday,February 28,2023 10:31:03AM *Indicates Violation **Indicates TRC Violation Page 1 of 5

Wolfspeed Durham
SAMPLE OVERVIEW
71812022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 013
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
Oct 2022 Week 4 < 0.001 / mg/L < /
Aug 2022 Average < 0.003 / 1.71 mg/L < /
Oct 2022 Average < 0.001 / 1.71 mg/L < /
2022 Quarter 3 < 0.003 / mg/L < /
2022 Quarter 4 < 0.001 / mg/L < /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
08/18/2022 S WolfspeedP1308182 < 0.001 / 3.38 mg/L < /
2Self
08/23/2022 S WolfspeedP1308232 < 0.001 / 3.38 mg/L < /
2Self
08/25/2022 S WolfspeedP1308252 < 0.001 / 3.38 mg/L < /
2Self
10/24/2022 P WolfspeedP1310242 < 0.001 / 3.38 mg/L < /
2POTW
Aug 2022 Week 3 < 0.001 / mg/L < /
Aug 2022 Week 4 < 0.001 / mg/L < /
Oct 2022 Week 4 < 0.001 / mg/L < /
Aug 2022 Average < 0.001 / 2.07 mg/L < /
Oct 2022 Average < 0.001 / 2.07 mg/L < /
2022 Quarter 3 < 0.001 / mg/L < /
2022 Quarter 4 < 0.001 / mg/L < /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
08/18/2022 S WolfspeedP1308182 < 0.001 / 1.20 mg/L < /
2Self
08/23/2022 S WolfspeedP1308232 < 0.001 / 1.20 mg/L < /
2Self
10/24/2022 P WolfspeedP1310242 < 0.003 / 1.20 mg/L < /
2POTW
Aug 2022 Week 3 < 0.001 / mg/L < /
Aug 2022 Week 4 < 0.001 / mg/L < /
Oct 2022 Week 4 < 0.003 / mg/L < /
Aug 2022 Average < 0.001 / 0.65 mg/L < /
Oct 2022 Average < 0.003 / 0.65 mg/L < /
2022 Quarter 3 < 0.001 / mg/L < /
2022 Quarter 4 < 0.003 / mg/L < /
Tuesday,February 28,2023 10:31:03AM *Indicates Violation **Indicates TRC Violation Page 2 of 5

Wolfspeed Durham
SAMPLE OVERVIEW
71812022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 013
Sample Date SamplelD Result/Limit Mass/Limit
Lead
08/18/2022 S WolfspeedP1308182 < 0.005 / 0.69 mg/L < /
2Self
08/23/2022 S WolfspeedP1308232 < 0.0025 / 0.69 mg/L < /
2Self
08/25/2022 S WolfspeedP1308252 < 0.005 / 0.69 mg/L < /
2Self
10/24/2022 P WolfspeedP1310242 < 0.0003 / 0.69 mg/L < /
2POTW
Aug 2022 Week 3 < 0.005 / mg/L < /
Aug 2022 Week 4 < 0.0038 / mg/L < /
Oct 2022 Week 4 < 0.0003 / mg/L < /
Aug 2022 Average < 0.0042 / 0.43 mg/L < /
Oct 2022 Average < 0.0003 / 0.43 mg/L < /
2022 Quarter 3 < 0.0042 / mg/L < /
2022 Quarter 4 < 0.0003 / mg/L < /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
08/18/2022 S WolfspeedP1308182 < 0.0025 / 3.98 mg/L < /
2Self
08/23/2022 S WolfspeedP1308232 < 0.005 / 3.98 mg/L < /
2Self
08/25/2022 S WolfspeedP1308252 < 0.0025 / 3.98 mg/L < /
2Self
10/24/2022 P WolfspeedP1310242 0.001 / 3.98 mg/L /
2POTW
Aug 2022 Week 3 < 0.0025 / mg/L < /
Aug 2022 Week 4 < 0.0038 / mg/L < /
Oct 2022 Week 4 0.001 / mg/L /
Aug 2022 Average < 0.0033 / 2.38 mg/L < /
Oct 2022 Average 0.001 / 2.38 mg/L /
2022 Quarter 3 < 0.0033 / mg/L < /
2022 Quarter 4 0.001 / mg/L /
Sample Date SamplelD Result/Limit Mass/Limit
pH
08/18/2022 S WolfspeedP1308182 6.6 / Su /
2Self
08/25/2022 S WolfspeedP1308252 3.1 / Su /
2Self
Aug 2022 Week 3 6.6 / Su /
Aug 2022 Week 4 3.1 / su /
Tuesday,February 28,2023 10:31:03AM *Indicates Violation **Indicates TRC Violation Page 3 of 5

Wolfspeed Durham
SAMPLE OVERVIEW
71812022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 013
Sample Date SamplelD Result/Limit Mass/Limit
PH
Aug 2022 Average 4.85 / Su /
2022 Quarter 3 4.85 / Su /
Sample Date SamplelD Result/Limit Mass/Limit
Silver
08/18/2022 S WolfspeedP1308182 < 0.0025 / 0.43 mg/L < /
2Self
08/23/2022 S WolfspeedP1308232 < 0.0025 / 0.43 mg/L < /
2Self
08/25/2022 S WolfspeedP1308252 < 0.0025 / 0.43 mg/L < /
2Self
10/24/2022 P WolfspeedP1310242 < 0.0003 / 0.43 mg/L < /
2POTW
Aug 2022 Week 3 < 0.0025 / mg/L < /
Aug 2022 Week 4 < 0.0025 / mg/L < /
Oct 2022 Week 4 < 0.0003 / mg/L < /
Aug 2022 Average < 0.0025 / 0.24 mg/L < /
Oct 2022 Average < 0.0003 / 0.24 mg/L < /
2022 Quarter 3 < 0.0025 / mg/L < /
2022 Quarter 4 < 0.0003 / mg/L < /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
08/18/2022 S WolfspeedP1308182 21.9 / °C /
2Self
08/25/2022 S WolfspeedP1308252 21.9 / °C /
2Self
Aug 2022 Week 3 21.9 / °C /
Aug 2022 Week 4 21.9 / °C /
Aug 2022 Average 21.9 / °C /
2022 Quarter 3 21.9 / °C /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
08/18/2022 S WolfspeedP1308182 0.025 / 2.61 mg/L /
2Self
08/23/2022 S WolfspeedP1308232 < 0.005 / 2.61 mg/L < /
2Self
08/25/2022 S WolfspeedP1308252 0.025 / 2.61 mg/L /
2Self
10/24/2022 P WolfspeedP1310242 < 0.003 / 2.61 mg/L < /
2POTW
Tuesday,February 28,2023 10:31:03AM *Indicates Violation **Indicates TRC Violation Page 4 of 5

Wolfspeed Durham
SAMPLE OVERVIEW
71812022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 013
Sample Date SampleID Result/Limit Mass/Limit
Zinc
Aug 2022 Week 3 0.025 / mg/L /
Aug 2022 Week 4 < 0.015 / mg/L < /
Oct 2022 Week 4 < 0.003 / mg/L < /
Aug 2022 Average < 0.019 / 1.48 mg/L < /
Oct 2022 Average < 0.003 / 1.48 mg/L < /
2022 Quarter 3 < 0.019 / mg/L < /
2022 Quarter 4 < 0.003 / mg/L < /
Tuesday,February 28,2023 10:31:03AM *Indicates Violation **Indicates TRC Violation Page 5 of 5

Wolfspeed RTP
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 012
Sample Date Sample-ID Result/Limit Mass/Limit
Ammonia
08/23/2022 S CreeRTPP12082322Se 2.81 / mg/L /
if
11/30/2022 P WolfspeedRTPP12113 2.6 / mg/L /
022POTW
Aug 2022 Week 4 2.81 / mg/L /
Nov 2022 Week 4 2.6 / mg/L /
Aug 2022 Average 2.81 / mg/L /
Nov 2022 Average 2.6 / mg/L /
2022 Quarter 3 2.81 / mg/L /
2022 Quarter 4 2.6 / mg/L /
2022 2nd 6 Months(Avg) 2.71 / mg/L /
2022 2nd 6...(Max) 2.81 / mg/L /
2022 2nd 6...(Min) 2.6 / mg/L /
2022 2nd 6...(Count) 2
Sample Date SampleLD Result/Limit Mass/Limit
Average Flow for Month
07/31/2022 S CreeRTPP120722F1ow 0.068034 /0.469 MGD /
08/31/2022 S CreeRTPP120822F1ow 0.066045 /0.469 MGD /
09/30/2022 S CreeRTPP120922F1ow 0.070573 /0.469 MGD /
09/30/2022 S WolfspeedRTPP12092 0.070573 /0.469 MGD /
2Flow
10/31/2022 S WolfspeedRTPP12102 0.069115 /0.469 MGD /
2Flow
11/30/2022 S WolfspeedRTPP12112 0.050661 /0.469 MGD /
2Flow
12/31/2022 S WolfspeedRTPP12122 0.058776 /0.469 MGD /
2Flow
Jul 2022 Week 4 0.068034 / MGD /
Aug 2022 Week 4 0.066045 / MGD /
Sep 2022 Week 4 0.070573 / MGD /
Oct 2022 Week 4 0.069115 / MGD /
Nov 2022 Week 4 0.050661 / MGD /
Dec 2022 Week 4 0.058776 / MGD /
Jul 2022 Average 0.068034 /0.329 MGD /
Aug 2022 Average 0.066045 /0.329 MGD /
Sep 2022 Average 0.070573 /0.329 MGD /
Oct 2022 Average 0.069115 /0.329 MGD /
Nov 2022 Average 0.050661 /0.329 MGD /
Dec 2022 Average 0.058776 /0.329 MGD /
2022 Quarter 3 0.068806 / MGD /
2022 Quarter 4 0.054719 / MGD /
2022 Quarter 4 0.069115 / MGD /
2022 Quarter 4 0.054719 / MGD /
2022 Quarter 4 0.069115 / MGD /
Tuesday,February 28,2023 10:04:06AM *Indicates Violation **Indicates TRC Violation Page 1 of 7

Wolfspeed RTP
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SampleID Result/Limit Mass/Limit
Average Flow for Month
2022 2nd 6 Months(Avg) 0.064825 / MGD /
2022 2nd 6...(Max) 0.070573 / MGD /
2022 2nd 6...(Min) 0.050661 / MGD /
2022 2nd 6...(Count) 7 / /
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 5
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Chloride
08/23/2022 S CreeRTPP12082322Se 123 / mg/L /
if
11/30/2022 P WolfspeedRTPP12113 III / mg/L /
022POTW
Aug 2022 Week 4 123 / mg/L /
Nov 2022 Week 4 111 / mg/L /
Aug 2022 Average 123 / mg/L /
Nov 2022 Average III / mg/L /
2022 Quarter 3 123 / mg/L /
2022 Quarter 4 111 / mg/L /
2022 2nd 6 Months(Avg) 117 / mg/L /
2022 2nd 6...(Max) 123 / mg/L /
2022 2nd 6...(Min) III / mg/L /
2022 2nd 6...(Count) 2
Sample Date SampleID Result/Limit Mass/Limit
Cyanide
08/23/2022 S CreeRTPP12082322Se < 0.003 / mg/L < /
if
11/30/2022 P WolfspeedRTPP12113 0.006 / mg/L /
022POTW
Aug 2022 Week 4 < 0.003 / mg/L < /
Nov 2022 Week 4 0.006 / mg/L /
Aug 2022 Average < 0.003 / mg/L < /
Nov 2022 Average 0.006 / mg/L /
2022 Quarter 3 < 0.003 / mg/L < /
2022 Quarter 4 0.006 / mg/L /
2022 2nd 6 Months(Avg) < 0.004 / mg/L < /
Tuesday,February 28,2023 10:04:06AM *Indicates Violation **Indicates TRC Violation Page 2 of 7

Wolfspeed RTP
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 012
Sample Date Sample-ID Result/Limit Mass/Limit
Cyanide
2022 2nd 6...(Max) 0.006 / mg/L /
2022 2nd 6...(Min) < 0.003 / mg/L < /
2022 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
08/23/2022 S CreeRTPP12082322Se 2.6 /8.0 mg/L /
if
11/30/2022 P WolfspeedRTPP12113 2.14 /8.0 mg/L /
022POTW
Aug 2022 Week 4 2.6 / mg/L /
Nov 2022 Week 4 2.14 / mg/L /
Aug 2022 Average 2.6 /7.0 mg/L /
Nov 2022 Average 2.14 /7.0 mg/L /
2022 Quarter 3 2.6 / mg/L /
2022 Quarter 4 2.14 / mg/L /
2022 2nd 6 Months(Avg) 2.37 / mg/L /
2022 2nd 6...(Max) 2.6 / mg/L /
2022 2nd 6...(Min) 2.14 / mg/L /
2022 2nd 6...(Count) 2
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
08/23/2022 S CreeRTPP12082322Se 0.000002 / mg/L /
if
11/30/2022 P WolfspeedRTPP12113 0.000009 / mg/L /
022POTWHg
Aug 2022 Week 4 0.000002 / mg/L /
Nov 2022 Week 4 0.000009 / mg/L /
Aug 2022 Average 0.000002 /0.000142 mg/L /
Nov 2022 Average 0.000009 /0.000142 mg/L /
2022 Quarter 3 0.000002 / mg/L /
2022 Quarter 4 0.000009 / mg/L /
2022 2nd 6 Months(Avg) 0.000006 / mg/L /
2022 2nd 6...(Max) 0.000009 / mg/L /
Tuesday,February 28,2023 10:04:06AM *Indicates Violation **Indicates TRC Violation Page 3 of 7

Wolfspeed RTP
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SampleID Result/Limit Mass/Limit
Mercury-LL
2022 2nd 6...(Min) 0.000002 / mg/L /
2022 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Molybdenum
08/23/2022 S CreeRTPP12082322Se < 0.005 / mg/L < /
if
11/30/2022 P WolfspeedRTPP12113 0.014 / mg/L /
022POTW
Aug 2022 Week 4 < 0.005 / mg/L < /
Nov 2022 Week 4 0.014 / mg/L /
Aug 2022 Average < 0.005 / mg/L < /
Nov 2022 Average 0.014 / mg/L /
2022 Quarter 3 < 0.005 / mg/L < /
2022 Quarter 4 0.014 / mg/L /
2022 2nd 6 Months(Avg) < 0.009 / mg/L < /
2022 2nd 6...(Max) 0.014 / mg/L /
2022 2nd 6...(Min) < 0.005 / mg/L < /
2022 2nd 6...(Count) 2
Sample Date SampleID Result/Limit Mass/Limit
Nitrate-Nitrite
11/30/2022 P WolfspeedRTPP12113 5.3 / mg/L /
022POTW
Nov 2022 Week 4 5.3 / mg/L /
Nov 2022 Average 5.3 / mg/L /
2022 Quarter 4 5.3 / mg/L /
2022 2nd 6 Months(Avg) 5.3 / mg/L /
2022 2nd 6...(Max) 5.3 / mg/L /
2022 2nd 6...(Min) 5.3 / mg/L /
2022 2nd 6...(Count) 1
Sample Date SampleID Result/Limit Mass/Limit
Nitrogen,Total
Tuesday,February 28,2023 10:04:06AM *Indicates Violation **Indicates TRC Violation Page 4 of 7

Wolfspeed RTP
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 012
Sample Date Sample- Result/Limit Mass/Limit
Nitrogen,Total
08/23/2022 S CreeRTPP12082322Se 14.28 / mg/L /
if
11/30/2022 P WolfspeedRTPP12113 15.6 / mg/L /
022POTW
Aug 2022 Week 4 14.28 / mg/L /
Nov 2022 Week 4 15.6 / mg/L /
Aug 2022 Average 14.28 / mg/L /
Nov 2022 Average 15.6 / mg/L /
2022 Quarter 3 14.28 / mg/L /
2022 Quarter 4 15.6 / mg/L /
2022 2nd 6 Months(Avg) 14.94 / mg/L /
2022 2nd 6...(Max) 15.6 / mg/L /
2022 2nd 6...(Min) 14.28 / mg/L /
2022 2nd 6...(Count) 2
Sample Date SampleLD Result/Limit Mass/Limit
Oil&Grease,Total
11/30/2022 P WolfspeedRTPP12113 < 2.5 /200 mg/L < /
022POTW
Nov 2022 Week 4 < 2.5 / mg/L < /
Nov 2022 Average < 2.5 / mg/L < /
2022 Quarter 4 < 2.5 / mg/L < /
2022 2nd 6 Months(Avg) < 2.5 / mg/L < /
2022 2nd 6...(Max) < 2.5 / mg/L < /
2022 2nd 6...(Min) < 2.5 / mg/L < /
2022 2nd 6...(Count) 1
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleLD Result/Limit Mass/Limit
pH
08/23/2022 S CreeRTPP12082322Se 7.3 /5.0-10.5 SU /
if
11/30/2022 P WolfspeedRTPP12113 7 /5.0-10.5 SU /
022POTW
Aug 2022 Week 4 7.3 / SU /
Nov 2022 Week 4 7 / SU /
Tuesday,February 28,2023 10:04:06AM *Indicates Violation **Indicates TRC Violation Page 5 of 7

Wolfspeed RTP
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
pH
Aug 2022 Average 7.3 / SU /
Nov 2022 Average 7 / SU /
2022 Quarter 3 7.3 / SU /
2022 Quarter 4 7 / SU /
2022 2nd 6 Months(Avg) 7.15 / SU /
2022 2nd 6...(Max) 7.3 / SU /
2022 2nd 6...(Min) 7 / SU /
2022 2nd 6...(Count) 2
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
Temperature
08/23/2022 S CreeRTPP12082322Se 26.8 /66 °C /
if
11/30/2022 P WolfspeedRTPP12113 16 /66 °C /
022POTW
Aug 2022 Week 4 26.8 / °C /
Nov 2022 Week 4 16 / °C /
Aug 2022 Average 26.8 / °C /
Nov 2022 Average 16 / °C /
2022 Quarter 3 26.8 / °C /
2022 Quarter 4 16 / °C /
2022 2nd 6 Months(Avg) 21.4 / °C /
2022 2nd 6...(Max) 26.8 / °C /
2022 2nd 6...(Min) 16 / °C /
2022 2nd 6...(Count) 2
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Tuesday,February 28,2023 10:04:06AM *Indicates Violation **Indicates TRC Violation Page 6 of 7

Wolfspeed RTP
SAMPLE OVERVIEW
71112022 To 1213112022 Sample Type: Effluent Wastewater Outfall: 012
Sample Date Sample-ID Result/Limit Mass/Limit
TKN
11/30/2022 P WolfspeedUPP12113 10.3 / mg/L /
022POTW
Nov 2022 Week 4 10.3 / mg/L /
Nov 2022 Average 10.3 / mg/L /
2022 Quarter 4 10.3 / mg/L /
2022 2nd 6 Months(Avg) 10.3 / mg/L /
2022 2nd 6...(Max) 10.3 / mg/L /
2022 2nd 6...(Min) 10.3 / mg/L /
2022 2nd 6...(Count) 1 / /
Sample Date SampleID Result/Limit Mass/Limit
Total Phosphorus
11/30/2022 P WolfspeedRTPP12113 1.61 / mg/L /
022POTW
Nov 2022 Week 4 1.61 / mg/L /
Nov 2022 Average 1.61 / mg/L /
2022 Quarter 4 1.61 / mg/L /
2022 2nd 6 Months(Avg) 1.61 / mg/L /
2022 2nd 6...(Max) 1.61 / mg/L /
2022 2nd 6...(Min) 1.61 / mg/L /
2022 2nd 6...(Count) 1
Tuesday,February 28,2023 10:04:06AM *Indicates Violation **Indicates TRC Violation Page 7 of 7