WQ0003281_2022 Residual Annual Report_20230224 (2)

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * WQ0003281
Applicant/Permittee City of Belmont
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Mooresville
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Tanya S. Carter
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
7048253791
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0003281
Has Current Existing permit number
Applicant/Permittee Address*
PO Box 431 Belmont, NC 28012
Facility Name*
City of Belmont Class B Residuals Program
Please provide comments/notes on your current submittal below.
Attached is the 2022 Land Application Report
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Signed Land App Report 2022.pdf 1.38MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
S &&wlt
Submission Date 2/24/2023

CITY OF
BELMONT
2022
City of Belmont
Wastewater Treatment Plant
2022 Annual Report
Land Application Program
Permit # WQ0003281

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0003281 County: Gaston Year: 2022
Facility Name (as shown on permit):
Land Application Operator:
City of Belmont
Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
0 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
U.S. Biosolids, Inc,
Total number of application fields in thepermit:
3
Total number of fields utilized for land application during the year:
1
Total amount of dry tons applied during the year for all application sites:
152.53
Total number of acres utilizes for land application during the year:
42.4
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2022 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. 0 Yes ® No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and time was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Permittee Name and Title (type or print)
Sfgna ure ermittee Date
Al
2-8-2023
Signature olf Preparer* i Dbte Signature of Land 9pptier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Belmont Total Dry Tons Applied (Annual):
WQ0003281 Cation Exchange Capacity (non 503 only):
Thomas Warren Owner: Thomas Warren Predominant Soil Series:
152.51
GaB2
42.4 Acres Permitted: 42.4 Site #: BT 9-1 Field #: BT 9-1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
W-Mr
Com-
posite
Date
©
©
0
©
l0
m
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
I
2
3
4 v
jj
B
7
_8j
9j
i s
IIJ
12
H
DT/Ac./
App.
Event
3.60
Arsenic
0.106
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.106
Cadmium
0.021
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.021
Copper
2.410
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0A00
0.000
0.000
0.060
2.410
Chromium
0.470
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.470
Lead
0.160
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000..
0.000
0.160
Mercury
0.008
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
1 0.000
0.000
0000.
0.008
Molyb-
0.053
0.000
06000
0.000
0.000
0.000
0.000
0.000
0.000
.0.000
0.000
0.000
0.053
denum
Nickel
0.156
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000.
0.000
0.156
Selenium
0.106
0.000
0.000
0.000
0.000
0.000
0.000...0.000
0.000
0.000
0..000
0.000
0.106.
Zinc
14J00
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
14.100
Total
Phos-
197.116
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
. 0.000
0.000
197.116
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Sigpature of Land 4plier
2-8-2023
Date
bFNR FORM MFLSF (12/2006)

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Belmont
WWTP Name: City of Belmont WWTP
WQ Permit Number:
NPDES Number:
WQ0003281
NCO21181
Monitoring Period: From l/1/2022 To 12/31/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A: Alt. A (time/temp) ❑
Alt B (Alk Treatment) E3
Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs 0
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost E
Heat Drying 0
Heat Treatment E3
Thermophilic ❑
Beta Ray E3
Gamma Ray 0
Pasteurization E3
Class B:
jAlt. (1) Fecal Density p
Alt. (2) Process to Significantly Reduce Pathogens E3
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization E3
Air Drying Cl
Composting ©
Aerobic Digestion 0
Anaerobic Digestion ❑
If applicable to alternative performed Class A or Class B complete the following monitoring data:
Parameter
Allowable Level
Sludge
g
Pathogen Density
NUMDor Of
Excee-
Frequency
of Analncesysis
Sample
Type
Analytical
Tech-
ni aue
Minimum
Geo. Meant254781
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
WN
3406
8270
MPN/g
0
7
grab
sm9221 c
CFU
1000 mpn per gram
of total solid (dry
wei ht
Sahnonella bacteria
(in lieu of fecal
coliform)
3 NTN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.l (VS reduction) ©
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) 0
jAlt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization []
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable)13
Alt. 9 (Injection) 0
Alt. 10 (incorporation) 0
No vector attraction reduction alternatives were performed 0
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Dennis Key US Biosolids, Inc.
Prebarer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
,Iui 2-8-2023
Signatur of Preparer* D Signature of Land Ap er (if applicable) Date
*Preparer is defined in 40 C)aR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (1212006)

;TATESVI LLE
kNALY TICAL
Analytical Results
US Biosolids
958 Hoots Rd
Roaring River, NC 28669
Entered: 3/10/22
Reported: 4/19/22
Sample ID: 220310-21-01
PARAMETER: Vector Attraction Reduction Aerobicall Digested Sludge 30da
Total Solids Volatile Solids % Volatile Solids
Week 1 1.67 0.91 0.5449
Week 2 1.61 0.87 0.5404
Week 3 1.60 0.86 0.5375
Week 4 1.58 0.86 0.5443
Week 5 1.53 0.81 0.5294
Week 6 1.52 0.81 0.5329
Volatile Solids Reduction: 0.5449 - 0.5329 X 100 = 4.6 %
0.5499 (0.5449 X 0.5329)
Respectfully submitted,
Melissa Myers
Statesville Analytical, Inc.
NC WW Cert.# 440NC

30 Day Bench Worksheet
Sample ID ## 220310-21-01
WF,FK 1
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
1.66
0,91
2
1.66
0.90
3
1.67
0.92
Avera g e:
1.67
1 0.91
0.5449
WEEK 2
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
1.61
0.87
2
1.61
0.87
3
1.61
0.87
Avera e:
1.61
0.87
0.5404
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
1.59
0.86
2
1.61
0.85
3
1.61
1 0.88
Average:
1.60
0.86
0.5375
WF.F.K 4
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
1.59
0.86
2
1.58
0.85
3
1.56
1 0.86
Average:
1.58
1 0.86
0.5443
WEEK 5
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
1.54
0.81
2
1.52
0.81
3
1.53
0.81
Average;
1.53
0.81
1 0.5294
WEEK 6
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
1.52
0.81
2
1.53
0.81
3
1.51
1 0.81
Average:
1.52
1 0.81
0.5329
Van Kleeck Reduction: 0.5449 -- 0.5329 X 100 - 4.6 %
0.5449 -- ( 0.5449 X 0.5329)
Final Result: 4.6%

Analytical Results STATESVILLE
ANALYTICAL
U.S. Biosolids Inc`
958 Hoots Road
Roaring River, NC 28669
Receive Date: 03/10/2022
Reported: 04/19/2022
For:
Comments:
Sample Number Parameter Sample ID Result
220310-21-01 30 Day Benchscale Belmont 4.6
220310-21-01 TCLP Belmont See Attached
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
Unit Method Analyzed Analyst
EPA62F�R-92I0 03/10/2022 MD
as Noted 03/11/2022 PACE
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 37

Condition of Receipt
Sample Number 220310-21-01 Temp on Arrival: 5.1
Parameter Schedule:
Received on Ice
Parameter Schedule: iCLP
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 37

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Page 3 of 37

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PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 4 of 37

aceAnalytical®
WW.¢ecelaba.cam
March 31, 2022
Crystal Little
Statesville Analytical, Inc.
122 Court Street
PO Sox 228
Statesville, NC 28687
RE: Project: BELMONT FULL TCLP
Pace Project No.: 92593154
Dear Crystal Little:
Pace Analytical Services, LLC
9800 i9ncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on March 11, 2022. The results relate only to
the samples Included In thls report. 'Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this final report were generated: by each of the follovAng laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Sarvtces - Peachtree Corners, GA
• Pace Analytical Services - New Orleans
• Pace Analytical Services - Greensburg
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyrlek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced, except in full,
without the written consent of Pace Analyticei Services, LLc.
Page 1 or 33
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 5 of 37

aceAnaIXicaie
urww.paeele5ssom
Project: BELMONT FULL TCLP
Pace Project No.: 92593154.
Pace Analytical Services Now Orleans
Florida Department of Health (NELAC): E=87595
Illinois Environmental Protection Agency: 0025721
Kansas Department of Health and Environment (NELAC):
E-10266
Louisiana Dept of Environmental Quality (NELAClLELAP):
02006
Pace Analytical Services Pennsylvania
1638 Roseytown Rd Suites 2,38,4, Greensburg, PA 15601
ANAB DOD-ELAP Red Accreditation #. L2417
Alabama Certification #: 41590
Arizona Certification M. AZO734
Arkansas Certification
California Certification fk 04222CA
Colorado Certification #: PA01547
Connecticut Certification #: PH-0694
Delaware Certification
EPA Region 4 DW Rad
FlorldarrN1 Certification M E87683
Georgia Cartlficatan M C040
Guam Certification
Florida: Cart E871149 SEKS WET
Hawaii Certification
Idaho Certification
Illinois Certification
Indiana Certification
Iowa Coffication #: 391
Kensas[TNI Certificallon #: E40358
Kentucky Certification #: KY90133
KY W W Permit #. KY0098221
KY WW Permit #. KY0000221
Louisiana DHHITNI Certificatton #: LA180012
Louisiana DEQITNI Certification #: 4086
Maine Certification #: 2017020
Maryland Certification #: 308
Massachusetts Certification #: M-PA1457
MichigardPADEP Certification #: 9991
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntenville, NO 26078
(704)87&9092
CERTIFICATIONS
Texas Commission on Env. Quality (NELAC):
T104704406.09-TX
U.S. Dept ofAgriculture Foreign Soil Import: P330-10-
00119
Missouri Certification #: 235
Montana Certification #: Certo082
Nebraska Certification # NE-OS-29-14
Nevada Certification #: PA014572018-1
New HampshlrelTNI Certification #: 297617
New derseylTNI Certification #: PA051
New Mexico Certification #: PA01457
New York/TNI Certification #. 10888
North Carolina Certification #: 42706
North Dakota Certification #: R-190
Ohio EPA Red Approval: #41249
OregonfTNl Certification #: PA200002-010
PennsylvaniafrNI Certification #:.65-00282
Puerto Rico Certification #. PA01457
Rhode Island Certification #: 65-00282
South Dakota Certification
Tennessee CerUficatton #: 02867
TexaslTNI Certification #: T1047041MI7-3
UtehlrNI Certification #: PA014572017-9
USDA Soil Permit#: P330-17-00091
Vermont Dept. of Health: ID# VT 0282
Virgin ISlandlPADEP Certification
VlrginlalVELAP Certification #: 460198
Washington Certification #: C868
West Vlrginla DEP Certification #:143
West Virginia DHHR Certification M.9964C
Wisconsin Approve List for Red
Wyoming Cortificaton #: 8TM3-L
PaceAnalydcal Services Charlotte
South Carolina Laboratory ID: 99006
South Carolina CertBcation #: 99006001
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Drinking Water Cert. #: 99006003
North Carolina Drinking Water Certification #: 37706
FloridalNELAP Certification #: E87627.
North Carolina Field Services Certification #: 5342
KenWokyUST Certification #: 84
North Carolina Wastewater Certification #: 12
Louisiana DoH Drinking Water #: LA029
South Carolina Laboratory ID: 99006
V€rglnialVELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverslde Ddve, Asheville, NC 28804 South Carolina Laboratory ID: 99030
FloridalNELAP Certification #: E87648 South Carolina Certification #: 99030001
North Carolina Drinking Water Certification #: 37712 VlrglnialVELAP Certification # 460222
North Carolina WastewataT Certification #: 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pars Analytical Servicas,'LLC.
Page 2 of 33
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 6 of 37

Pace Analytical Services, LLC
(��A'cmnaljftale 9800lanaeyAve. suite 100
Huntersville, NC 28078
www.paeelakmm (704)8759692
CERTIFICATIONS
Project. BELMONTFULLTCLP
Pace Project No.: 92593154
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Comers, GA 30092 North Carolina Cerificatlon M 381
Florida DOH Certification M E87315 South Carolina Certification M 98011001
Georgia DW Inorganics Certification M 812
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In NO.
without the written consent of Pace Ano"cal Services, LLC.
Page 3 of 33
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 7 of 37

IMAnalydcal"
MrwPacdtE►sam
SAMPLE ANALYTE COUNT
Project: BELMONT FULL TCLP
Pace Project No.: 92593154
Pace Analytical Services, LLC
91100 Klncey Ave. Sulle 10D
Huntersville, NC 2BD78
p04j875-9n92
Analyles
Lab ID Sample ID Method
Analysts
Reported
Laboratory
92593154001 220310-21-01 EPA80818
SEM
9
PASI-C
EPA8082A
GEM
8
PASI-C
EPA6010D
DRB
7
PASI-GA
EPA7470A
VB
1
PASI-GA
EPA 8270E
PKS
is
PASI-C
EPA 8260D
SAS
14
PASI-O
SW-846
KDF
1
PASI-C
EPA 1010B
MJP
1
PASI-A
EPA9045D
YEG
1
PASI-A
EPA 9095E
YEG
1
PASI-A
Moisture
GGG1
1
PASI-N
SW-8467.3.3.2
DWR
1
PASI-N
SM 4500S2-F-2011
NAH
1
PASI-PA
923931M002 220310.21.01 EPA8082A
GEM
8
PASI-C
PASI-A = Pace Analytical Services -Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-GA = Pace Analytical Services - Peachtree Comers, GA
PASI-N w Pace Analytical Services - New Orleans
PASI-PA= Pace Analytical Services - Greensburg
REPORT OF LABORATORY ANALYSIS
This report shall riot be reproduced, except In full,
wilhoutthe written consent of Pace Analytical Servlces,LLC.
Page 4 of 33
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 8 of 37

aceAnaljftal
www,pacoltbs.com
ANALYTICAL RESULTS .
Project: BELMONTFULLTCLP
Pace Project No.: 92593154
Pace Analytical Services, LLC
9800 t(€nceyAve. Suite 100
Huntersvilla, NC 28078
[phone]
Sample: 220310.21.01 Lab 10: 92593154001 Collected: 03110122 10.30 Received; 03/11/22 10:27 Matrix: Solid
Results reported on a dry weight" basis and are acyusted forpercent moisture, sample size and any dilutions.
Parameters Results units Report Limit OF Prepared Analyzed CAS No. Qual
8081 TCLP Pesticides RVE
Analytical Method: EPA80818 Preparation Method: EPA3510C
Leachate MethodlDate: EPA 1311; 0311612215:08 Initial pH: 5.28: Final pH: 5
Pace Analytical Services - Charlotte
gamma-BHC (Lindane)
ND ug1L 0.50 1
03/16122 17:21 0311712212:04 58-89-9
Chlordane (Technical)
ND. ugiL 3.0 1
03/1612217:21 0311712212:04 57-74-9
Endrin
ND ug1L 0.50 1
03/1612217:21 0311712212:04 72-20-8
Heptachlor
ND ugiL 0,50 1
0311612217:21 0311712212:04 76-44-8
Hoptachlorepoxide
ND ug1L 0.50 1
03116/2217:21 03117/2212:04 1024-57-3
Methoxyshlor
ND ug1L 1000 1
031161221721 03/1712212:04 7243-5
Toxaphane
ND ug1L 3.0 1
0311612217:2t 0311712212:04 8001-35-2
Surrogates
Decachlorobiphenyl (S)
85 % 10-154 1
03/16/22 17:21 03/17/22 12:04 2051-24.3
Teirachloro-m-xylene (S)
104 % 10-184 1
03/16/22 17:21 03/17i22 12:04 877-09-e
8082 TCLP PCBs RVE
Analytical Method: EPA 8082A Preparation Method; EPA 3510C
Leachate MethodlDate; EPA 1311; 03116/22 15:08 Initial pH: 5.28; Final pH: 5
Pace Analytical Services - Charlotte
PCB-1016 (Aroclor 1016)
N❑ ugiL 1000 1
03/16/2217:21 03117/2219:52 12674-11 2
PCB-1221 (Aroclor 1221)
ND ugiL 1000 1
0311612217:21 03/1712219:52 11104-28-2
PCB-1232 (Aroclor 1232)
ND ugiL 1000 1
0311612217:21 03117/2219.52 11141-16-5
PCB-1242 (Aroclor 1242)
ND u911. 1000 1
0311612217:21 03117122 19:52 63469-21-9
PC13-1248 (Arodor 1248)
ND ugiL 1000 1
0311612217:21 03117122 19:52 12672-29-6
PCB-1254 (Aroclor 1254)
ND ug1L 1000 1
03/16122 17:21 03117122 19:52 11097-69.1
PCB-1260 (Aroclor 1260)
ND ug1L 1000 1
03/16/22 1721 03117122 19:52 11096-82-6
Surrogates
Decachlorobiphenyl (S)
80 °% 10-181 1
0311612217:21 03117122 19:52 2051-24-3
60100 ATL ICP, TCLP
Analytical Method: EPA 601OD Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 03/21/2214:20 Initial
pH: 7.53; Final pH: 7,54
Pace Analytical Services - Peachtree Comers, GA
Arsenic
ND mg1L 0.30 1
0312212214:34 03123/2212:33 7440-38-2
Barium
ND mg1L 0.50 1
03/22/2214:34 0312312212:33 7440+39-3
Cadmium
ND mg1L 0.10 1
03122/2214:34 0312312212:33 7440-43-9
Chromium
ND , mg1L 0.10 1
03122/2214:34 03/23/2212:33 7440-47-3
Lead
ND mgiL 0,26 1
0312212214:34 0312312212:33 7439-92-1
Selenium
ND mg1L 0.40 1
03)2212214:34 0312312212.33 T78249-2
Silver
ND mg1L 0.10 1
0312212214:34 0312312212:33 7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470A Preparation Method: EPA7470A
Leachate Method/Date: EPA 1311; 0312i12214:20 Initial pH: 7,53; Final pit: 7.54
Pace Analytical Services - Peachtree Comers, GA
Mercury
ND mgiL 0.0050 1
0312212215:00 0312312211:00 7439-97-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/31/2022 05:28 PM without the written consent of Pace Analytical Serv€ces,iLC.
Page 5 of 33
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 9 of 37

aceAnaIXical
www,pardebeom
ANALYTICAL RESULTS
Project: BELMONTFULLTCLP
Pace Project Nc.:: 92593154
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntetsvlile, Nc 26078
[phone]
Sample: 220310.21-01 Lab 10: 92593164001 Collected: 0311012210:30 Received: OW112210:27 Matrix: Solid
Results reported an a dry weight' basis and are adjusted rorpercent moisture, sample size and any dilutions.
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
8270E TCLP RVE
Analytical Method: EPA 8270E Preparation Method: F-PA 3510C
Leachate MethodlOate: EPA 1311; 03115/2215:08 Initial pH: 5.28; Final pH: 5
Pace Analytical
Services - Charlotte
1,4-Dichiorobenzene
NO
ugtL
50.0
1
03116122.17!28 03117f2213:03 106-46-7
2,4-Dinitmtoluene
NO
uglL
50.0
1
(LV1612217:28 03117/2213:03 121A4-2
Hexachloro-1,3•butadione
NO
ug1L
50.0
1
0311612217:28 0311712213:03 87-68-3
Hexachlorobenzene
NO
ug1L
50.0
1
0311612217:28 0311712213:03 118-741
Hexachloroethane
NO
ug1L
50.0
1
031M217:28 0311712213:03 67 72-1
2-Methylphenol(o-Cresol)
NO
uglL
50.0
1
03116/2217:28 0311712213:03 95.48-7
3&4-Methylphenol(m&p Cresol)
NO
uglL
50.0
1
0311612217:28 03117122 13:03 15831-10A
Nitrobenzene
NO
ug1L
50.0
1
0311612217:26 0311712213:03 98-95-3
Pentachlerophenol
NO
uglL
100
1
03/16/2217:28 0311712213:03 87-86-6
Pyridine
NO
ug1L
50.0
1
03/1612217:28 03/1712213:03 110-86-1
2,4,5-Trichloraphenol
NO
ug1L
50.0
1
0311612217:28 0311712213:03 96-95-4
2,4,6-Trichloraphenol
ND
ug1L
.60.0
1
0311812217:28 03/1712213:03 88.06-2
Surrogates
Nltrobenzene-d5 (3)
38
%
10-144
1
0311612217:28 0311712213:03 4165-60-0
2 Fluoroblphenyt (S)
39
%
10-130
1
0311612217:28 0311712213:03 321-60-B
Terphanyt-dl4 (S)
96
%
34-163
1
03116/22 17:28 0311712213.03 171851-0
Phenol -de (S)
27
%
10.130
1
031t6/2217.28 03117/221103 13127-80-3
2-Fluorophenal (S)
33
%
10-130
1
03/16/22 17:28 03/17/221103 367-12-4
2,4.6-Tdbromophenol (S)
84
%
10-144
1
03116122 17:28 0311712213:03 118-79-6
8260D MSV TCLP
Analytical Method: EPA 8260D Leachate MethodlDale: EPA 1311: 03116122 13:08
Pace Analytical
Services - Charlotte
Benzene
NO
ug1L
100
20
0311712212:50 7tA3-2
2-Butanone (MEK)
NO
ug1L
200
20
03/17/22 112:50 78-93-3
Carbon tetrachloride
NO
ug1L
100
20
0311712212:50 56-235
Chiambenzene
NO
ug1L
100
20
0311712212:50 108-90-7
Chloroform
ND
ug1L
100
20
0311712212:50 67-66-3
1,4-Dichlorobenzene
NO
uglL
i00
20
031171221Z50 10B-46-7
1,2-Dichloroethane
NO
uglL
100
20
0311712212:50 107-06-2
1.1-Dichloroethene
NO
uglL
100
20
03/1712212:50 75.35-4
Tetrachtoroelhene
ND
uglL
100
20
03A712212:50 127-184
Tdchloroethene
NO
ug1L
100
20
03MV2212:50 79.01-8
vinyl chlorlde
NO
uglL
100
20
03I1712212:50 75-01-4
Surrogates
1.2-Dichloroethane-d4 (S)
89
%
70-130
20
0311712212:50 17060-07-0
Toluene-d8 (S)
110
%
67-135
20
0311712212:50 2037-26-5
4-Bromolluorobenzene (S)
95
%
70430
20
03/17122 12:50 460.00-4
Percent Moisture
Analytical Method: SW-846
Pace Analytical
Services - Charlotte
Percent Moisture
97.3
%
0.10
1
03114/2216:25 N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
bate: 0313112.022 05:28 PM without the written consent of Pace AnaWral Services, LLC. Page 6 of 33
PO Box 228 a Statesville, NC 28687 • 704/872/4697
Page 10 of 37

Pace Analytical Services, LLC
aceArralytical m 9800 KinceyAve. Sulte 100
Huntersville, NC28078
wwwplcollbracm (704)M-9092
ANALYTICAL RESULTS
Project: BELMONTFULLTCLP
Pace Project No.: 92593154
Sample: 220310.21.01 Lab ID: 92593154001 Collected: 03/10122 10:30 Received: 0311112210:27 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted rorpercent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1010 Flashpaint,Closed Cup
Analytical Method: EPA 1010E
Pace Analytical Services -Asheville
Flashpoint
s200 deg F 70.0
1
03123/2214:00
9045 pH $oil
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
6.7 Std. Units 0.10
1
0311812213:07 H3
9095 Paint Filter Liquid Test
Analytical Method: EPA 9095B
Pace Analytical Services -Asheville
Free Liquids
FAIL 1.0
1
03118/2215:66
Percent Moisture
Analytical Method: Moisture
Pace Analytical Services - New Orleans
Percent Moisture
99.8 % 0.50
1
03/2412212:05
733C S Reactive Cyanide
Analytical Method: SW-846 7.3.3.2 Preparation Method: SW 846 7.3.3.2
Pace Analytical Services - New Orleans
Cyanide, Reactive
ND mg/kg 25.0
1
03/26122 07.45 03125122 13:14
734E Reactive Sulfide
Analytical Method: SM 4500S2-F-2011 Preparation. Method: SW-846 7,3.4.2
Pace Analytical Services - Greensburg
Sulfide, Reactive
ND mgfkg 367
1
03116122 20:45 03116122 20:48
Sample: 220310.21-01
Lab ID: 92593154002 Collected: 03110t2210:30
Received: 03/11/22 10:27 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No. Dual
8082 GCS PCB RVE
Analytical Method: EPA 8082A Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
PCB-1016 (Aroclnr 1016)
ND ug1L 5.0
1
03I2412217:06 03125122 07:43 12674-11-2
PCB-1221 (Arocior1221)
ND uglL 5.0
1
0312412217:06 03125/2207:43 11104-28.2
PCB-1232 (Aroclnr 1232)
ND ug1L 5.0
1
03/2412217:06 03/25122 07:43 11141-16-5
PCB-1242 (Aroclnr 1242)
ND ugtL 6.0
1
03124/2217:06 03195M 07:43 53469-21-9
PCB-1248 (Aroclnr 1248)
ND ugfL 5.0
1
03/24/2217:06 03/25/22 07:43 12672-29-6
PCB-1254 (Amclor 1254)
ND uglL 5.0
1
0312412217:06 03/25/22 07.43 11097.694
PCBA260 (Aroclnr 1260)
ND uglL 5.0
1
0312412217:06 03/25/22 07:43 11095.82-5
Surrogates
Decachlorobiphenyl (S)
50 % 10-181
1
03/24/22 17:06 03/25122 07:43 2051-24-3
REPORT OF LABORATORY ANALYSIS
This report shall not be ropmduced, except in full,
Date: 03131/2022 05:28 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 33
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 11 of 37

aceAnalXical
www,paaelehs;am
Project:
BELMONTFULLTCLP
Pace Project No.:
92593154
QC Batch:
6863N
QC Batch Method:
EPA3010A
Associated Lab Samples: 92593154001
METHOD BLANK: 3587256
Associated Lab Samples: 92693154001
Pace Analytical Services, LLC
9800 Kineey Ave. Suite 100
Huntersvilla, NC 2807a
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 6010D
Analysis Destripl€on: 6010D ATL TCLP
Laboratory: Pace Analytical Services - Peachtree Comers, GA
Matrix: Water
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
mg1L
ND
0.30
0312312212:23 BC
Barium
mg1L
NO
0.60
03123M212:23
Cadmium
mg1L
NO
0.10
0312312212:23
Chromium
mg1L
ND
0.10
03123/2212:23
Lead
mg1L
ND
0.25
0312312212:23
Selenium
mg1L
NO
0.40
03123/2212:23
Silver
mg1L
NO
0.10
031252212:23
LABORATORY CONTROL SAMPLE: 3688514
Spike
LCS
LCS
% Roo
Parameter
Units
Cone.
Result
e% Rec
Limits Quallners
Arsenic
mg1L
10
10.1
101
80-120
Barium
mg1L
10
9.6
96
80-120
Cadmium
mg1L
10
10.0
100
80-120
Chromium
mg1L
10
9.8
9B
80-120
Lead
mg1L
10
10.2
102
80-120
Selenium
mg1L
10
9.9
99
80-120
Silver
mg1L
10
9.7
97
80-120
MATRIX SPIKE 6 MATRIX SPIKE DUPLICATE:
3588515
3588516
MS
MSD
92593154001
Spike
Spike
MS
MSD
MS
MSD
% Rao
Parameter
Units
Result
Cone.
Cone.
Result
Result
e% Rao
e% Rao
Limits
RPD Qual
Arsenic
mg1L
ND
10
10
10.6
10.2
104
101
75-125
3
Barium
mgiL
ND
10
10
10.3
10
102
100
75-125
3
Cadmium
mg1L
NO
10
10
10,3
10.2
103
102
75-125
2
Chromium
mg1L
NO
t0
10
10.2
10.1
102
100
75.125
1
Lead
mgiL
NO
10
10
10.5
10.2
105
102
75-125
2
Selenium
mgiL
ND
10
10
10.2
10
101
99
75-125
2
Silver
mg1L
NO
10
10
1012
10.0
101
100
75-125
1
Reauitspresented on this page are in the units indicated by the •units'cutumn except where an ellemala.unit Is presented to the right at the resulL
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduoed, except in full,
Date. 03/3112,022 05:28 PM without the written consent of PaceAnslygcal Services. U.C.
Page 8 of 33
PO Box 228 a Statesville, NC 28687 • 704/872/4697
Page 12 of 37

(�IacleAnalj4ical
www.paceleba.wm
QUALITY CONTROL DATA
Project: BELMONT FULL TCLP
Pace Project No.: 92593154
Pace Analytical Services, LLC
9800 KInceyAve. Suite 100
Huntersvllle, NC 28078
(704)B7&9092-
QC Batch: 686416
Analysis Method:
EPA7470A
QC Batch Method: EPA 7470A
Analysis Description;
7470 Mercury TCLP, ATL
Laboratory:
Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92593154001
METHOD BLANK: 35B7256
Matrix: Water
Associated Lab Samples: 925931540D1
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Mercury mgfL
ND 0,0050 0312312210:36
LABORATORY CONTROL SAMPLE: 35BB642
Spike LCS
LCS % Rae
Parameter Units
Cone. Result
% Rec Limits Qualifiers
Mercury mgfL
0.017 0,019
113 W120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3588643 3588644
MS MSD
92594047001
Spike Spike MS
MSD MS MSD e% Rae
Parameter Units Result
Cone. Cone, Result
Result %Rec %Rec Limits RPD Qual
Mercury mg1L 0.00025
0.017 0.017 0.14 0.28 832 1680 75-125 6B
J
Results presented on this pagaare En the unita Endicated bythe "Units" column exmptwharaan alternate unAis presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/3112022 05:28 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 33
PO Box 228 • Statesville, NC 28687 • 704/872/4697
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aceAnalj4dal
www,pacelabtls m
QUALITY CONTROL DATA
Project: BELMQNTFULLTCLP
Pace Project No.: 92593154
QC Batch: 685391 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysts Descript€on: 826OD MSV TCLP
Laboratory: pace Analytical Services - Charlotte
Associated Lab Samples: 92593154001
METHOD BLANK: 3583022
Matrix: Water
Associated Lab Samples: 92593154001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,1-01chloroethene
ug1L
ND
5.0
0311712211:01
1,2-Dichtarosthene
uglL
NO
5.0
o311712211:01
IA-Dichtorobenzene
ug1L
ND
5.0
0311712211:01
2-Bulanone (MEK)
ug1L
ND
10.0
0311712211:01
Benzene
uglL
NO
5.0
03/17/2211:01
Carbon tetrachloride
ug1L
ND
5.0
03/17/22 11:01
Chlarobenzene
ug1L
NO
5.0
0311712211:01
Chloroform
tI91L
ND
5.0
03/17/22 41:01
Tatfactiloroethene
uglL
NO
5.0
0311712211:01
Trichloroathens
uglL
ND
5.0
0311712211:01
Vinyl chloride
ug1L
ND
5.0
0311712211:01
1,2-Dfchloroethene-d4 (S)
%
94
70-130
03/17/2211:01
4-Bromofiuorobenzene (S)
%
103
70-130
0311712211:01
Toluene-da (S)
%
109
67-135
03/17/22 11:01
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 1100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
3583821
Spike
LCS
LCS
% Rec
Parameter
Units
Cont.
Result
% Rec
Limits Qualifiers
1,1-Dichforeethene
uglL
5o
44.7
89
70-132
1,2-01chlaroethane
ug1L
50
50.0
10D
70-130
1,4-Dichlorobenzene
ug1L
50
50.7
101
70-130
2-Bulanone (MEK)
ug1L
100
BBA
86
70-133
Benzene
uglL
50
48A
97
70-130
Carbon tetrachloride
uglL
50
45.7
91
70-130
Chlarobenzene
ug1L
50
47.3
95
70-130
Chloroform
uglL
50
49.9
100
70-130
Tatrachloroethene
uglL
50
46.5
93
70-130
Trichloroethane
ug1L
50
49.8
100
70-130
Vinyl chloride
ug1L
50
43.6
87
59-142
1,2-Dichlaroelhane-d4 (S)
%
106
70-130
4-Bromoffuorobenzene (S)
%
98
70-130
Toluene-dS (8)
%
98
67-135
Results presented on this page are In the units Indicated by the'aolts" column esceptwhem an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not 4e reproduced, except in full,
Date: 03/3112022 05:28 PM without the written consent cf Pace Analytical Services, I.I.C.
Page 10 of 33
PO Box 228 a Statesville, NC 28687 • 704/872/4697
Page 14 of 37

Pace Analytical Services, LLC
aica!® 880010nceyAve. BuitelOD
ceftyHuntersvllle, NC 28078
tllww.paeelahs.eom [phone]
QUALITY CONTROL DATA
Project: BELMONTRILLTCLP
Pace Project No-: 92593154
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3583823
MS
92593329001 Spike
Parameter Units Result Conc-
MSD
Spike
Cone.
3583824
MS
Result
MSD
Result
MS
% Rea
MSD
e% Rec
e% Rea
Limits
RPD Qual
1,1-Dichtoroethene
ug1L
NO
400
400
367
386
92
97
70-158
5
1,2-Dichloroethene
ug1L
NO
400
400
415
424
104
106
67-138
2
1,4-Dichlorobenzene
ug1L
NO
400
400
447
470
112
118
70-133
5
2-Butanone(MEK)
uglL
509
800
Soo
1160
1220
82
88
61-147
4
Benzene
ug1L
ND
400
400
413
436
103
109
67-150
6
Carbon tetrachloride
uglL
ND
400
40D
402
419
101
105
70=147
4
Chlorobenzene
uglL
ND
400
400
407
420
102
105
70.137
3
Chloroform
ug1L
NO
400
400
425
438
106
109
70-144
3
Teirachloreeihene
uglL
ND
400
400
396
412
99
103
70-139
4
Trlchloroethene
uglL
ND
400
400
431
458
108
114
70.149
6
Vinyl chloride
uglL
ND
400
400
350
348
88
87
55.172
1
12-Dichloroethane-0 (S)
e%
102
103
70-130
4-Bromofluorobenzene (S)
%
94
97
70-130
Toluene -dB (S)
%
97
98
67-135
Results presented on this page are In the units Indleated by the'Unile Womn wept Where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Oete: 03/31/2022 05:28 PM without the written consent of PaceAneWcal Services, LLC.
Page 11 of 33
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 15 Of 37

(�1I Analoicale
-3ce wwtrprcelrha.ctsb
QUALITY CONTROL DATA
Project: BELMONT FULL TCLP
Pace Project No.: 92593154
QC Hatch: 685197 Analysis Method: EPA 8081E
QC Batch Method: EPA3510C Analysis Description: 8081 TOLP Pesticides RV
Laboratory: Pace Analytical Services - Chadotte
Associated Lab Samples: 92693154001
METHOD BLANK: 3580719
Associated Lab Samples: 92593154001
Parameter
Chlardane (Technlcal)
Endrin
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
Decachloroblphenyl(S)
Tetrachloro-m-xylene (5)
MaWK: Water
Units
Blank
Result
Reporting
Limit
Analyzed Qualifiers
u911-
NO
3.0
03117/22 08:28
uglL
NO
0.60
0311712208:28
ugIL
NO
0.50
03117122OB:28
uglL
NO
0.50
0311712208:2B
uglL
NO
0.60
0311712208:28
ug1L
NO
1000
0311712208:28
uglL
NO
3.0
03/1712208:28
%
116
10-154
03/17/2208:28
%
102
10-184
03117/22 08:28
Pace Analytical Services, LLC
980010nceyAve. Sulte100
Huntersvilla, NC 20078
[phone]
LABORATORY CONTROL SAMPLE:
3582988
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Endrin
ug1L
1.2
1.1
91
41-155
gamma-BHC (Lindane)
ug1L
1.2
0.99
79
42-146
Heplachlor
ug1L
1.2
1.0
84
23-135
Heptachlor epoxide
uglL
1.2
1.0
84
39-142
Methoxychlor
uglL
3.8
3.2.1
87
55-173
Decachloroblphenyl (S)
%
100
10-154
Tetrachloro,m-xylene (S)
%
80
10-184
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3582989
MS
92593152001
Spike
Parameter
Units
Result
Conc.
Endrin
uglL
NO
C2
gamma-BHC (Lindane)
uglL
NO
1.2
Heplachlor
uglL
NO
1.2
Heptachlor epoxide
uglL.
ND
1.2
Methoxychlor
ug1L
ND
3.8
Decachlorahiphenyt (S)
%
Tetrachloro-m-xylene (S)
%
3582990
MSD
Spike
MS
MSD
MS
MSD
% Roo
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1.2
1.1
0,79
86
63
23-171
31 R1
1.2
1.0
0.76
83
61
29.157
31 R1
1.2
1.1
0A0
88
64
11-149
31 R1
1.2
1.0
0.79
82
64
21-157
26
3.8
3.3J
2AJ
88
65
33-193
98
77
10-154
88
68
10-184
Results presented an this page are In the unite Indicated by the 'Units" column ncept.whom an skemate.unit Is presented to ghe right of the mull.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03131=22 05:28 PM without the written consent of Pace Analytical Services, LLC,
Page 12 of 33
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 16 of 37

aceAnali6cal
Inrw.puehda.cam
QUALITY CONTROL DATA
Project: BELMONT FULL TCLP
Pace Project No.: 92593154
QC Batch: 686918 Analysis Method: EPA 8082A
QC Batch Method: EPA3510C Analysts Description: 8082 GCS PCB
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92593164002
METHOD BLANK: 3590933
Associated Lab Samples: 92593154002
Parameter
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1200 (Aroclor 1260)
Decachlorobiphenyl (S)
Matrix: water
Blank
Reporting
Units
Result
Limit
Analyzed Qualifiers
ug/L
NO
0.50
03125/22 08:21
ug/L
ND
0.50
03125122 08:21
ug1L
ND
0.50
03125/22 08:21
ug1L
ND
0.50
0312aW 08:21
ug/L
NO
0.50
03/25/22 08:21
ug/L
ND
0.50
0312512208:21
ug1L
ND
0.50
0312512208:21
%
102
10-181
03/25122 08:21
Pace Analytical Services, LLG
980D KinceyAve. Suite 100
Huntersville, NC 28D78
(704)87M092
LABORATORY CONTROL SAMPLE: 3590934
Spike LCS LCS % Rao
Parameter Units Conc. Result % Rec Limits Qualifiers
PCB-1016 (Arocor 1016) ugll_ 5 4.6 92 41-137
PCB-1260 (Aroclor 1260) ug1L 5 4.4 88 42-156
Decachlorobiphenyl (S) % 103 10-181
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE:
3590935
3590936
MS
MSD
92594786014 Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
PCB-1016 {Aroclor'1016)
ug1L
ND 8.3
8.3
29.1
24.7
349
298
22-145 16 M1
PCB-1260 (Aroclor 1260)
ug1L
ND 8.3
8.3
4.3
4.6
52
54
10A67 3
Decachlorobiphonyl(S)
%
52
57
10-1B1
Results presented on this pals ara In the units Indicated by the "Unite column except where an alternate unit is presented to the rFght ofthe result
REPORT OF LABORATORY ANALYSIS
This report Shall not be reproduced, except in full,
Date: 03/31/2022 05:28 PM without Hie written consent of Pace Analytical Senrsce% LLC.
Page 13 of 33
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 17 of 37

aceftlXical
www.yuellblimm
QUALITY CONTROL DATA
Project: BELMONT FULL TCLP
Pace Project No.: 92593154
Pace Analytical Services, LLG
9800 KlnceyAve. Suite 100
Huntsrsville, NO 28078
[phone]
QC Batch: 685198
Analysis Method: EPA 8082A
QC Satch Method: EPA 3510C
Analysis Description: 8082 TCLP PCB RV
Laboratory. Pace Analytical Services - Charlotte
Associated Lab Samples: 92593154001
METHOD BLANK: 3580719
Matrix: Water
Associated Lab Samples: 92593154001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
PCB-1016 (Aroolor 1016)
ug1L
NO 1000
03/1712220:66
PCB-1221 (Arocior1221)
ug1L
ND 1000
0311712220:56
PCEI-1232 (Aroclor 1232)
ugn-
NO 1000
0311712220:56
PCB-1242 (Aroclor 1242)
ug/L
ND 1000
03/17122 20:56
PCB-124B (Aroclar 1248)
ug1L
ND 1000
03M7122 20:56
PCB-1254 (Aroclor 1254)
uglL
ND 1000
03/17/22 20:56
PCB-126D(Aroclor 1260)
ug1L
ND loco
0311712220:56
Decachlorobiphenyl (S)
%
98 10-181
03117/22 20:56
LABORATORY CONTROL SAMPLE: 3582995
Spike LCS
LCS % Rec
Parameter
Units
Cone. Result
% Rea Limits Qualifiers
PCII-1016 (Aroclor 1018)
ug1L
25 NO
75 41-137
PCB-1250 (Aroclor 1260)
ug1L
25 ND
75 42-156
Decachloroblphenyl (S)
%
90 10-181
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3582996 3582997
MSMSD
92593154001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units
Result
Cone. Cone. Result
Result % Rec % Rec
Limits RPD Qual
PCB-1016 (Arocior1016) ug1L
ND
25 25 ND
ND 64 80
22-145
PCB-1260 (Aroclor 1260) ugR
ND
25 25 ND
NO 54 66
10-167
Decachlorobiphenyl (S) %
58 79
10-181
Results preeemsd an thls page am In the units Indicated by the "Unite" column exceptwhem an allernato unit Is presented to the right orthe msulL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In Ng,
Date: 03/31/2022 05:28 PM without the wdttan consent. of Pace Analytical Sertdces, LLC.
Page 14 of 33
PO Box 228 a, Statesville, NC 28687 • 704/872/4697
Page 15 of 37

,�acmnafjftal'
wwwpacalabs.tam
QUALITY CONTROL DATA
Project: BELMONTFULLTCLP
Pace Project No.: 92593154
QC Batch: 685196 Analysis Method: EPA 8270E
QC Batch Method: EPA 3510C Analysis Description: 8270E TCLP MSSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92693154001
METHOD BLANK: 3580719
Matrix: Water
Associated Lab Samples: 92593154001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dlchlorobenzene
ug1L
ND
50.0
D311712211:47
2,4,5-Trichlorophenol
ug1L
ND
50.0
0311712211:47
2,4,6-Trichlorophenol
uglL
ND
50.0
0311712211:47
2A-Din[trotoluene
ug11-
ND
50.0
0311712211:47
2-Methylphenol(o-Cresol)
uglL
ND
50.0
03/17/2211.47
3&4-Methylphenal(m&p Cresol)
uglL
ND
50.0
03117/2211.47
Hexachloro-1,3-butadiene
uglL
ND
50.0
03117/2211,47
Hexachlorabenzene
ug1L
ND
5D:0
03117/22 11:47
Hexachloroethans
ug1L
ND
50.0
0311712211:47
Nitrobenzene
ug1L
ND
50.0
0311712211:47
Pentachlorophanot
ug1L
ND
100
0311712211:47
Pyridine
ug1L
ND
50.0
03)1712211:47
2,4,6 Tdbrornophenol (S)
%
78
10-144
0311712211:47
2-Fluorobiphenyt (S)
era
70
10-130
03/1712211:47
2-Fluorophenol (S)
%
65
10-130
0311712211:47
Nitrobenzene-d5 (S)
%
75
10-144
03/1712211:47
Phenol-d6 (8)
%
50
10-130
0311712211:47
Terphenyt=d14 (S)
%
90
34.163
03/1712211.47
LABORATORY CONTROL SAMPLE: 3582984
Pace Analytical Services, LLC
980010nceyAve. Sdite.100
HuntersvTile, NC 28D78
[phone]
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rao
Limits Qualifiers
1,4-Dichlorobenzene
uglL
500
213
43
18-130
2,4,5-Tdchlorophenol
uglL
500
373
75
35-130
2,4,6-Tdchlorophenol
uglL
500
361
72
31-130
24-01nitrotoluene
ugll-
500
362
72
37-136
2-Methylphenol(o-Cresol)
ug1L
Soo
342
68
35-130
3&4-Methyiphenol(m&p Cresol)
ug1L
Soo
329
fib
34-130
Hexachloro-1,3-butadiene
ug1L
600
182
36
11-130
Hexachlorabenzene
uglL
500
324
65
311-130
Hexnchloroethane
ug1L
500
200
40
14-130
Nitrabenzene
ug1L
Soo
329
66
36-130
Pentachlorophenal
ug1L
1000
735
73
23-149
Pyddlne
ug1L
500
269
54
10-130
2,4,6-Tribromophenol (S)
%
81
10-144
2-Ftuorobiphenyl (S)
%
61
10-130
2-Fluorophenol (S)
%
60
10-130
Nitrobenzene-0(S)
%
73
10-144
Phenol-d6 (S)
%
47
10-130
Results presented an this page are In the unite Indicated by the `UnlW column 69ceptwhom an alternate unit Is presented to the right ofthe result.
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced,-exnepi In full,
Dale: 03131/2022 05:28 PM without the writtan consent of Pace Analytical Servlcss, U-0,
Page 15 of 33
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 19 of 37

aceAnalytical®
(�urureapatalahs.tais
Project: BELMONTFULLTCLP
Pace Project No.., 92593154
LABORATORY CONTROL SAMPLE: 3502984
Parameter Units
Terphenyl-d14 (S) %
Pace Analytical Servlees, LLC
9800 KlnceyAve. Suite 100
Huntersville, NC 20078
(704)B75.9092
QUALITY CONTROL DATA
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
76 34-163
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3582985
M$
92593168001
Spike
Parameter
Units
Result
Conc.
1,4-Dichlorobenzene
ug1L
ND
500
2,4,5-Tdchlorophenol
ug1L
ND
500
2,4,6 Tdchlorophenol
ug1L
ND
500
2,4-Dinitrotoiuene
ug/L
ND
Sao
2-Methylphenol(o-Cresol)
ug1L
ND
500
W-Methylphengl(m&p
ug1L
ND
500
Cresol)
Hexachloro-1,3-butadlene
ug1L
ND
500
Hexachtorobenzene
ug1L
ND
500
Hexachloroethane
ug1L
ND
500
Nitrobenzene
ug1L
ND
500
Pentachlorophenol
ug1L
ND
1000
Pyridine
ug1L
ND
500
2A6-Tribrom0phenol (8)
%
2-Fluorob€phenyl (S)
%
2-Rucrophonot (S)
%
Nilrobenzene-0 (S)
%
phenol-d6 (8)
%
Terphenyl-d14 (S)
%
3582986
MSD
Spike
MS
MSD
MS
MSO
% Rec
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
Qual
500
266
325
47
69
10-130
20
500
436
23.2J
87
5
10-143
Mi
50o
433
N❑
87
0
10-147
M1
600
424
532
85
106
29-148
23
500
413
309
83
62
20-130
29
600
403
246
81
49
16-130
48
R1
600
233
269
40
47
10.130
14
500
372
493
74
99
29.130
28
500
265
323
49
60
10-130
20
500
401
465
a0
93
25-130
15
1000
642
ND
84
0
10-175
Mi
500
27.5J
394
6
79
10.130
M1
96
4
10-144
s0
69
85
10-130
69
2
10-130
50
84
99
10-144
53
12
10-130
81
105
34-163
Results presented on this page are In the units Indicated by the "Units" column except where an Memos unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fug,
Date: 0313112022 05:28 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 33
PO Box 228 • Statesville, NC 28687 e 704/872/4697
Page 20 of 37

aceARalytica!®
srrra!pacefadaxam
Project: BELMONT FULL TCLP
Pace Project No.: 92593154
QC Batch: 684609
QC Batch Method: SW-846
Associated Lab Samples: 92593154001
SAMPLE DUPLICATE: 3580360
Parameter Units
Percent Moisture e/
SAMPLE DUPLICATE: 3580361
Parameter
Percent Moisture
QUALITY CONTROL DATA
Analysis Method: SW-846
Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
92593219001 Dup
Result Result RPD Qualifiers
17.4 16.5 5 N2
92593154001 Dup
Units Result Result
y 97.3 97.3
RPD Qualifiers
0 N2
Pace Analytical Services, LLC
980010nceyAve. Suite 100
Huntenivilie, NC 28078
[phone]
Results proseatod on this page are In the units Indicated by the "Unite" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shalt not be reproduced, except in TO.
Date: 03/31/2022 05:28 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 33
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 21 of 37

aceAnaiXical
www.pacstahsaarn
QUALITY CONTROL DATA
Project: BELMONTFULLTCLP
Pace Project No.: 92593154
QC Batch: 686715 Analysis Method: EPA 1010B
QC Batch Method. EPA 1010B Analysis Description: 1010, Flash Point, Closed Cup
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92593154001
SAMPLE DUPLICATE: 3590016
92594112001 Dup
Parameter Units Result Result RFO Qualifiers
Flashpoint deg F <75 <75
Pace Analytical Services, LLC
980010nceyAve. Suite 100
Huntersyllle. NC 28078
[phone]
Results presented an this page ate In the unite indicated by the "Units" column except where an alternate unit Is presented to the dghtafttw result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,.
Date: 03131/2022 05:28 PM without the written oonsentot Pate Analytical Services, LLC.
Page 18 of 33
PO Box 228 is Statesville, NC 28687 • 704/872/4697
Page 22 of 37

alceAnalytical
wwwpeeele4etore
QUALITY CONTROL DATA
Project: BELMONT FULLTCLP
Pace Project No.: 92593154
QC Batch: 685576 Analysis Method: EPA 90450
QC Batch Method: EPA 9045D Analysis DescripFion: 9045 pH
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92593154001
SAMPLE DUPLICATE: 3585153
92593060001 Dap
Parameter Units Result Resuft RPD Qualifiers
pH at 25 Degrees C Std. Units 5.9 5.8 1 H3
SAMPLE DUPLICATE: 3585154
92593136001 D0p
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 4.8 4.8 1 H3
Pace Analytical services, LLC
9800 Mncey Ave. Suite 100
Huntersvllle. NC 28078
[phone]
Results presented onthla page are In the unEta Indicated by the "ILIAW caluren aaeept where an alternate unit is presented to the rlghtorthe result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In fall,.
Date: 03131=22 05:28 PM without the written consent of Pace Analocal Servlces,tLC• Page 19 of 33
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 23 of 37

(�IaceAnall6cal
www,pacstalid com
QUALITY CONTROL DATA
Project: BELMONT FULL TCLP
Pace Project No.: 92593154
Pace Analytical Services, LLC
9800 Klncey Ave. Sulle 100
Huntersvlle, NO 26078
[phone]
QC Batch: 250865 Analysis Method: Moisture
QC Batch Method: Moisture Analysis Description: Dry WeightFercent Moisture
Laboratory: Pace Analytical Services - New Orleans
Associated Lab Samples: 92593154001
SAMPLE DUPLICATE: 9192074
40242008001 Dup
Parameter Units Result Result
Percent Moisture % 23.9 22.3
RPD Qualifiers
7
Results presented an this page are In the units Indicated by the 'Unite column except when an altomato unit is presented to the rlghtofthe mault
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 03131/2022 05:28 PM without Ow wdttan consent of Pace Analytical Semites, LLD.
Page 20 of 33
PO Box 228 • Statesville, NC 28687 e 704/872/4697
Page 24 of 37

aceAnalXicai®
www.pacalabaxam
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Klncey Ave. Stille 100
Hunteraville, NC 28078
[phone]
Project: BELMONT FULL TCLP
Pace Project No.: 92593154
QC Batch: 251006
Analysis Method:
SVV-846 7.3.3.2
QC Batch Method: SW-846 7.3.3.2
Anaiys€s Description:
733C Reactive Cyanide
Laboratory:
Paoe Analytical Services - New Orleans
Associated Lab Samples: 92593154001
METHOD BLANK: 1192710
Matrix: Solid
Associated Lab Samples: 92593154001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Cyanide, Reactive
mglkg
ND 25,0 03I25122 13:38
LABORATORY CONTROL SAMPLE: 1192711
Spike LCS
LCS e% Rea
Parameter
Units
Conc. Result
°% Rea Unilts Oualiflers
Cyanide, Reactive
mglkg
iD0 ND
12 1-110
MATRIX SPIKE SAMPLE: 1192713
92593152001 Spike
MS MS e% Rea
Parameter
Units
Result Conn.
Result e% Rea Limits Qualifiers
Cyanide, Reactive
inglkg
ND 100
ND 15 1-110
SAMPLE DUPLICATE: 1192712
92593162001 pup
Parameter
Units
Result Result
RPD Quatiflers
Cyanide, Reactive
mglkg
ND ND
Results presented on this page are In the units Indicated by the 'Unite coluronexcspl whet* an alternate unit Ia presented to the right ortlra result.
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except in full,
Date: 03/31/2022 05:28 PM without the written consent of Pace An"cal Services, LLC. Page 21 of 33
PO Box 228 • Statesville, IBC 28687 • 704/872/4697
Page 25 of 37

(�IacI Analytical
e wrlmpaaetati cars
QUALITY CONTROL DATA
Project: BELMONT FULL TCLP
Pace Project No.: 92693164
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersville, NC 28078
j704i878-9092
QC Balch: 490850 Analysis Method: SM 4500S2-F-2011
QC Batch Method: SW-846 7.3A.2 Analysis Description: 734S Reactive Sulfide
Laboratory: Pace Analytical Services - Greensburg
Associated: Lab Samples: 92593154001
METHOD BLANK: 2374523
Assoclated:Lab Samples: 92593154001
Parameter Units
Sulfide, Reactive mg"
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 10.0 03116122.20:48
LABORATORY CONTROL SAMPLE: 2374524
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Sulfide, Reactive mg/kg 114 ND 7 0-52
SAMPLE DUPLICATE: 2374525
30471067001 Dup
Parameter Units Result Result RPD Qualifiers
Sulfide, Reactive mglkg ND ND H1
Results presented on this page are lathe units indicated by the Units" column except whore an sitemate n{tli rs presented to the right of the vault
REPORT OF LABORATORY ANALYSIS
This repots shall not be reproduced, except In full,
Date; 03131/2022 05:28 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 33
PO Box 228 h Statesville, NC 28687 • 704/872/4697
Page 26 of 37

Pace Analytical Services, LLC
lac
eArralytical 9e0DIOnceyAve. Suite
Huntersvllle, NC 2SD78
wtwxpacela6scam
(704]675A092
QUALIFIERS
Project: BELMONTFULLTCLP
Pace Project No.: 92593154
DEFINITIONS
❑F - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution at the sample aliquot
NO - Not Detected at or above adjusted reporting limit.
TNTC -Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit,
PQL- Practical Quantilation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenythydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The resultfor each analyte is
a combined concentration.
Consistent with EPA guidelines, unroundeddata are displayed and have been used to calculate °% recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D)- Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC. Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended In SW846 Chapter 4 for the analysis of Acrole€n and Acrylonitdle by EPA
Method 6260.
N-Nitrosodlphenylamine decomposes and cannot be separated from Dlpherrylamine using Method 8270. The result reported for
each analyte, Is a combined concentration.
Reported:results are not rounded until the final step prior to reporting, Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters,
PaceAnalytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
BC The.same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the
laboratory reporting limit.
H1 Analysis conducted outside the EPA method holding time.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The tab does not hold NEIACJTN€ accreditation for this parameter but other aeereditationslcertifications may apply. A
complete list of acereditationsfcertifications Is available upon request.
R1 RPD value was outside control limits.
SO Surrogate recovery outside laboratory control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 03131/2022 05:28 PM without the written consent of Face Analytical Services, U.C. Page 23 of 33
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 27 of 37

5ac
(
eAna1j&ca1
www.pacalab.I=
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: BELMONT FULL TCLP
Pace Project NO.: 92593154
Pace Analptleal Services, LLC
9800WnceyAve. Sulle100
Huntersville, NO 2078
(704)87&9092
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92593154001
22031041-01
EPA3510C
685197
EPA8081B
685387
92593164002
220310-21.01
EPA 3510C
686916
EPA 80M
687223
92693154001
220310-21-01
EPA3510C
685198
EPA 8082A
605388
92593154001
220310-21.01
EPA3010A
680388
EPA6010D
686504
92593154001
220310.21.01
EPA7470A
686416
EPA7470A
686632
92693154001
220310.21.01
EPA3510C
685196
EPA8270E
685411
92593154001
220310-21.01
EPA MOD
685391
92593154001
220310.21.01
SW-846
684609
92693154001
220310.21.01
E:PA1010B
686715
92593164001
220310.21.01
EPA 9045D
685576
92693154001
220310-21.01
EPA 9095E
685833
92593154001
220310-21.01
Moisture
250865
92593154001
220310.21.01
SW-8467.3.3.2
251006
SWa467.3.3.2
25.1049
92593154001
220310-21.01
SW-846 7.3A.2
490850
SM 45O0-S2-F-2011
490951
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 03131/2022 05:28 PM without the written oonsenl of Pace Analytical Services, LLC, Page 24 of 33
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 28 of 37

aeeAnalylica! n
Document Name:
Sample Condition U on Receipt SCUR
Dacurnent Revised: November 15, 2021
Page 1 of 2
Document No.:
F-CAR•CS-033-Rev.08
Issuing Authority:
Pace Carolinas Qualit oHlce
Laboratory recelving samples:
Asheville ❑ Eden[] Greenwood ❑ HuntersvIlle v� Ralelgh❑
Mechanicsville❑ Atlanta[] Kernersville❑
Client Name:
17-
� GIB PraJe�t W® ; 921593154
Courier: F� Elc ❑UPS LISPS ❑Client
❑ Commercial Pace ❑Other.'
i 1
Custody Seal Present? ❑Yes VN. Seals Intact?' ❑Yes '194.
92593A5'4
Date/6-10 lsParsonEKnminingcontents: 7,I,m
Packing Material: ' - []Bubble Wrap ❑Rubble Bags ❑None ❑. Other
TheTmemete . ,� /t
Biological Tissue Fr ran?
Des ❑No A
IRGunIP: � �„ e❑glue
�f1`- Type Ice:
❑Non¢
of
j� Correction Factor: f�
Cooler Temp: L� Add/Subtract ('C) V
Temp should be above freezing to 6'C
C-Temp-Temp-Corrected•{'C •
❑Samples our of comp criteria. Samples on Ire, cooling process
USDA Regulated Soil ( /A, -ter sample)
Old samples originate In a quarantine zone within the United States; CA, NY, at SC (check maps:?
old samples odglnate from a foreign source linlernationpty,
CaIns mentE Dlscre an :
Chain of Custody Present?
es
No
OWA
1.
Samples Arrived within Hold ThFie2
qlyts
ONo
ONJA
2.
Short Hold Time Ane1 sts 42 hr.)?
Yes
No
N!A
3.
Rush Turn Around Time Re uested?
OVes
12ho
N A
4.
SuBiclentvolume?
at
ONO
N/A
S.
Correct Containers Used?
-Pace Containers Used?
Y
ONO
❑No
©N/A
N/A
6,
Contalnerslntact?
" es
ON.
ONM
7,
Dissolved analysis! Sam des Field Filtered?
❑Yes
ONO
04111
S,
Sample Labels Match COC?
-Includes0ateifdme/ID/Anal sis Matrla;
oes
ONO
EIN/A
9,
Heads ace In VbA Vials aS•61nm17
Qyes
ONO
t 4/A
10,
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
Del
ONO
QNo
-©fV/A
Ulll /A
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split ccoainers:
CLIENT NDTIFICATION/RESOLUTION
Project Manager SCURF Review:
Project Manager SRF Reulaw:
note:
Date:
FICUDetaRoqulred? ❑Yes QNo
Page 25 of 33
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 29 of 37

Document Name:
Document Revised: November 15, 2021
aceAnatrcaf�
Sample condition Upon Recelpt (SCURI
Page 2 of 2
Document Nb.;
EdAR-0-033•Rev.09
Issuing Authority:
Pace Carolinas Quality Office
*Check mark top half of bats If pH and/or dechlorinatlan Is
verified end within the acceptance range for preservation
Samples.
Exceptions: VOA, Conform, TOC, Oil and Grease, ORO/8015 {water) DOC, LLR9
**Bottom half of box Is to list number of battles
Projec.Wo# 92593154.
PM: TIH Due Date: 03/25/22
CLIENT: 82-Statesvil.
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pH Adjustment
Log for Preserved Samples
Samplala
Type ofYressivaliva
pH upon receipt
Date preservation adjusted I
Timepraaarvulon
Amount ofpresarvallve
Loth
adjusted
added
Note: Whanevaf thole is a dircrepanq affectln$Nonh Car011ea[OMP11011ce sampiec, dcupY U. fP,awm, ww, vc wn wum nm u, rorynu
out of hold, rnconect preservative,out of temp, Incorrect containers.
Page 26 of 33
PO Box 228 * Statesville, NC 28687 * 704/872/4697
Page 30 of 37

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PO Box 228 • Statesville, NC 28687 ■ 704/872/4697
Page 31 of 37

ANALYTICAL ENVIRONMENTAL SERVICES, INC.
AES
March 22, 2022
Tyriek Hooks
Pace Analytical
9800 Kincey Ave Suite 100
Huntersville NC 28078-8400
RE: 92593154
Dear 'IyriekHooks- Order No: 2203173
Analytical Environmental Services, Inc. received I samples on 3/l G/2022 8,03:00 AM
for the analyses presented in following report.
"No problems were encountered during the analyses except as noted in the Case Narrative or by qualifiers in
the report or QC Summary. Additionally, all results for the associated Quality Control samples were within
EPA and/or AES established limits.
AES's accreditation are as follows:
-NELAP/State of Florida Laboratory ID E87582 for analysis of Nou-Potable Water, Solid & Chemical
Materials, Air & Emissions Volatile Organics, and Drinking Water Microbiology & Metals, effective
07/01 /21-06130/22.
State of Georgia, Department of Natural Resources ID #800 for analysis of Drinking Water Metals, effective
through 06/30/22 and Total Coliforms/ E. coli, effective 04/20/20-04/24/23.
-AIHA-LAP, LLC Laboratory ID: 100671 for Industrial Hygiene samples (Metals and PCM Asbestos),
Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal) Direct
Examination, effective until I1101123.
These results relate only to the items tested as received. This report may only be reproduced in full.
If you have any questions regarding these test results, please feel free to call.
Sincerely,
(Pta/ln6 !1(kOOLt Bf (.
Paris Masoudi
Project Manager
3030 F.•• «l • ti..l I�rivc • e\lla«lx, G •margin 3()341I • Tcl: 17t).457.3177 • Fax: [phone] • Toll rtm; 800.972.4889
u w.a�,atlanla.eom Page 28 of 33
Page I of 6
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 32 of 37

Chain of Custody
PAS] Charlotte Laboratory
Workorder: 92593154 Workorder Name: BELMONT FULLTCLP Results Requested By:
_ aceAlnapical'
wwupacrl�b}ee�r-
1
3l2512022 2n I 4-21
Roped l Invoice To
7ubconVacl To
Re uasled Analysis
Tyriek Hooks
Pace Analytical Charlotte
AES
P.D. TIH 92593154
9800KInceyAve. Suite100
3080 Presidential Drive
Huntersvilte, NC 28078
Atlanta. GA 30340
Phone (704)SM-9092
Email [e-mail]
`a
iE
State of Sample Origin: NC
Preserved Contalners
n
d
Collect
s
Item
Sampla 10
t}alafTlme
Lab IO -
ntalrix
LAB 0aE OFFLY
2203WV-01
3114120221020
92503154001
Safid
I
X
2
3
4
5
-
-
Comments
Trensfors
Releasad By
natemme
Received Sy
0ataftime
1i5
.)t.D.^t �w
SA.4 f1Fe3
3
Cooler Temperature on Receipt
°C Cusmd Seat Y or
N Received an Ice Y or N Samples Intact Y or, N
Tuesday. March is. 2022 WAS:51 Al
FMT-ALL-0-002rev_0024M MKOD9 RW 2916633
Page 2 0f 6
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 33 of 37

Analytical Environmental Services, Inc
Date: 22-Mar-22
Client: Pace Analytical Client Semple ID: 220310-21-01
Project Name: 92593154 Collection Date: 3/10/2022 10:30:00 AM
Lab ID: 2203173-001 Matrix: Solid
Analyses
Result
Reporting Qua[
Units BatchI❑
Ublu([nn DatcAnaiyzed Analyst
Limit
Factor
HERBICIDES,TCLP SW1311/8151A
(SW3510C)
2,4,5-TP (Silvex)
BRL
0.20
nig)L 332828
1 03/1812022 17:28 'KH
2,9--D
BRL
0.20
WW.L 332828
1 03/18/202217:28 KH
Surr: DCAA
53.3
50.1-120
%REC 332828
1 0311B/i02217:28 rKH
Quaaacm Value exceeds maximum con am vnnt Icvcl
BRL Below repotting limit
hl Hnfding7imca forpmpacerion v[mvlysis cxcaded
N Analyto no[NELAC certified
e Analyta Actccledinilro asanciateJ meliood filaok
> Qravler MLitt acault:value
E Eaitn¢ted (vslpc above gnwtimtion —go)
5 Spike Recovery ouuide limits due io:ma[rix
Norr Scc case nnuutive
F Annl}—d inihe 161e ich la¢d-Wi.n tlnmtlta me[lred
< Lesa than Rosvh value
3 Esthnatedvalnedrteetcdheln Reponinsl:lark Page 30of33
Page 3 of 6
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 34 of 37

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PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 35 of 37

Analytical Environmental Services, Inc Dale: 22-Mar-i2
Client; Pam Analylical ANALYTICAL QC SUMMARY RE,
Project Name; 92593154
Warkorder: 2203173 ButchlD: 332828
Sample ID: MD-332828 Client 11): Units: mg1L Prep Date: 0311712022 Run No: 490708
SampWTTyp : MDLK Tm[Cede: RERDICIDFS,T61-P IM1311m151A B.feh[D: 332828 Analysis Date: 0.411012022 Seq No: 11123561
Analyte Result RPT Limit SPKvalue SPKReFVaI %RGC Low Limit High Limit RPD ReMat %RPD RPDLimil Qunl
2,4,5-TP(Silvex) 19RL 0.20
2.4-1) 13RL 0.20
Sum DCAA 0.3087 0 0.5000 - 61.7 50, I 120
Sample [D: LCS-332828 Client ID: Units: mg1L - Prep Date: 03117/2022 Run No: 480709
sampleTgpe: LCS Tes[Cede: IIeRIICIDPS,TCLP 51VI311MISIA BatCWD: 332826 Analysis Date: 0311192022 Seq No: 11123562
Analyte Result RPT Liotit SPKvalue SPKRcfVal %REC Low Limit High Limit RPD Ref Vol %RPD RPDLimil Quul
2,4,5-TP (Silvex) 0.3439 0.20 0.5000 68.9 50.5 120
2,4-D 0,3315 0.20 0.5000 66.3 48.8 120
Surr: DCAA 0:4001 0 0.5000 80.0 50.1 120
Sample EDT 2203HII-002AMS Client ID: Unils: mg1L Prep Dale: 0311712022 Run No: 48.0708
Samplaljvpa: MS TwXodeu IIERMCIDPS,TCLP 5W13HIS151A BaldtiD: 332828 Analysis Date: 0311812022 Seq No: 11123564
Analyte Result RPT Limit SPK value SPK WWI %REC Law Limit High Limit RPD Ref Vet %RPD RPD Limit Qual
2,4,5-TP(Silvex)
0:3496
0.20
0.5000
69.9
50.5 120
2,4-D
03391
0.20
0.5000
67.8
47.1 120
Surr: DCAA
0.3906
0
0.5000
78.1
50.1 120
pueuP.m a om,n Jmn 9-1.'lee a Rrmll,vlue 0 -n mdc-k6...-iAdmedwd bl,,
an ui4 ­A-1 a Fae�J te.-b-q'.1,nlivn'"4 11 11ddJ lima Fm lm=Um -IpI4 n=dW
r W-W wlwde d'd W., lupna.y Lima, N Am711n nut NllAC.n OW R Wm uol.idelimli. Jue lu n.ulrix
Vp ilm Rcpn,dng Lb,ft s sane lte.n,W.Wd. lim;,. Juntiu,nauu Page 32 of 33
Page 5 of 6
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 36 of 37

End of Report
Pegs 33 of 33
Page 6 of 6
PO Box 228 * Statesville, NC 28687 * 704/872/4697
Page 37 of 37

Waypoint(D
ANALYTICAL
3/24/2022
US Biosolids Inc
Dennis Key
958 Hoots Road
Roaring River, NC, 28669
Ref: Analytical Testing
Report Number: 22-074-0005
Project Description: Belmont
7621 Whitepine Road, Richmond, VA 23237
Main 904-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Dennis Key:
Waypoint Analytical Virginia, Inc. received sample(s) on 3/15/2022 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
T"r'c Mt G/v"r
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

0 (D
Waypoint
ANALYTICAL
7621. White pine Roan, Richmond, VA 23237
Main 804-743-9401 ° Fax SO4-271-6446
www.waypointanalytical.com
Sample Summary Table
Report Number. 22-074-0005
Client Project Description: Belmont
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
57148
Belmont
Solids
03/14/2022 11:30
03/15/2022
57148
Belmont
Solids
03/14/2022 11:30
03/15/2022
SM-4500-NH3C
WP MTN
57148
Belmont
Solids
03/14/2022 11:30
03/15/2022
9045D
WP MTN
57148
Belmont
Solids
03/14/2022 11:30
03/15/2022
4500NO3F-2011
WP MTN
57148
Belmont
Solids
03/14/2022 11:30
03/15/2022
6010D
WP MTN
57148
Belmont
Solids
03/14/2022 11:30
03/15/2022
SW-7471B
WP MTN
57148
Belmont
Solids
03/14/2022 11:30
03/15/2022
SM-4500-NH3C-TKN
WP MTN
57148
Belmont
Solids
03/14/2022 11:30
03/15/2022
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 7

Waypoint
ANALYTICAL
46381
US Biosolids Inc Project Belmont
Dennis Key
958 Hoots Road Information
Roaring River , NC 28669
Report Number: 22-074-0005
Lab No : 57148
Sample ID : Belmont
7521 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalyUcal.com
REPORT OFANAL YSTS
Report Date : 03/24/2022
Received : 03/15/2022
TWIT Mt (rrowr
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 3/ 14/2022 11:30
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
96.6
%
0.010
Sulfur
9470
mg/Kg - dry
294
Calcium
16000
mg/Kg - dry
1470
Aluminum
51200
mg/Kg - dry
147
Manganese
1160
mg/Kg - dry
14.7
Organic N
32060
mg/Kg - dry
7353
Nickel
21.7
mg/Kg - dry
7.35
Lead
22.3
mg/Kg - dry
8.82
Arsenic
<14.7
mg/Kg - dry
14.7
Selenium
<14.7
mg/Kg - dry
14.7
Test
Results
Units
MQL
1
03/16/2216:04
FMM
SM-254OG
1
03/22/22 23:49
JTR
6010D
1
03/22/22 2149
JTR
6010D
1
03/22/22 23:49
JTR
6010D
1
03/22/22 23:49
JTR
6010D
1
03/21/22 11:30
CALCULATION
1
03/22/22 23:49
JTR
6010D
1
03/22/22 23:49
JTR
6010D
1
03/22/22 23:49
JTR
6610D
1
03/22/22 23:49
JTR
6010D
DF
Date 1 Time
By
Analytical
Analyzed
Method
Total Solids
3.39
%
0.010
1 03/16/22 16:04
FMM
SM-2540G
Phosphorus
27400
mg/Kg - dry
147
1 03/22/22 23:49
JTR
6010D
Copper
335
mg/Kg - dry
14.7
1 03/22/22 23:49
JTR
6010D
Total Kjeldahl Nitrogen 32100 mg/Kg - dry 7350 1 03/21/22 11:30 JPJ ;M-4500-NH3C-TK1`
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 3 of 7

0
Waypoint 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www-waypaintanalytical.com
46381
US Biosolids Inc Project Belmont
Dennis Key Report Date ; 03/24/2022
958 Hoots Road Information : Received ; 03/15/2022
Roaring River, NC 28669
Twuict �rraw
Report Number: 22-074-0005 RFPORTOFANALY9IS
Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No : 57148 Matrix: Solids
Sample ID : Belmont Sampled: 3/14/2022 11:30
Potassium
3240
mg/Kg - dry
294
1
03/22/22 23:49
JTR
6010D
Magnesium
3470
mg/Kg - dry
147
1
03/22/22 23:49
JTR
6010D
Sodium
7820
mg/Kg - dry
735
1
03/23/22 23:24
JTR
60101)
Iron
28300
mg/Kg - dry
294
1
03/22/22 23:49
JTR
6010D
Zinc
1960
mg/Kg - dry
36.8
1
03/22/22 23:49
JTR
6010D
Ammonia Nitrogen
<2940
mg/Kg - dry
2940
1
03/22/22 09:30
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
721
mg/Kg - dry
147
1
03/22/22 14:30
ZBD
4500NO3F-2011
Cadmium
<2.94
mg/Kg - dry
2.94
1
03/22/22 23:49
JTR
6010D
Chromium
65.3
mg/Kg - dry
7.35
1
03/22/22 23:49
JTR
6010D
Mercury
1.08
mg/Kg - dry
0.465
1
03/21/22 14:48
ZMT
SW-7471B
PH
5.9
s.u,
1
03/22/2215:55
DRS
9045D
Molybdenum
<7.35
mg/Kg - dry
7.35
1
03/22/22 23:49
JTR
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 7

Waypoint.(b
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalydcal.com
Client: US Biosolids Inc CASE NARRATIVE
Project: Belmont
Lab Report Number: 22-074-0005
Date: 3/24/2022
Metals Analysis Method 6010D
Sample 91067 (EA-3-2)
Analyte: Aluminum
QC Batch No: L606891/1-605686
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 91067 (EA-3-2)
Analyte: Calcium
QC Batch No: L606489/L605686
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 91067 (EA-3-2)
Analyte: Potassium
QC Batch No: 1-606891/1-605686
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 91067 (EA-3-2)
Analyte: Magnesium
QC Batch No: L606489/1-605686
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 91067 (EA-3-2)
Analyte: Manganese
QC Batch No: 1-6068911605686
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 91067 (EA-3-2)
Analyte: Phosphorus
QC Batch No: L606489/L605686
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 5 of 7

0 (D
Waypoint.
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-4401 ° Fax [phone]
www.wayWntanalytical.com
Shipment Receipt Form
Customer Number: 46381
Customer Name: US Biosolids Inc
Report Number: 22-074-0005
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
Yes
0 No
Number of coolers/boxes received
F 1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
# Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
# Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
Yes
0 No
Samples in proper containers?
Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
# N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
[_ Low concentration EnCore samplers (48 hr)
[_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: jBrandi Watson Date & Time: 03/15/2022 13:49:43
Page 6 of 7

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Page 7 of 7

Analytical Results
U.S. Biosolids Inc
958 Hoots Road
Roaring River, NC 28669
Receive Date: 03/10/2022
Reported: 03/11/2022
For: Belmont
Comments: GEOMETRIC MEAN: 8,270 MPN/g
STATESVILLE
ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
220310-41-01
Fecal Coliforms
B-1
16026
MPNIg
sM9221cE-2006
03/10/2022
MD
220310-41-01
Percent Solids
B-1
3.12
%
SM25408-2011
03/10/2022
MD
220310-41-02
Fecal Coliforms
B-2
9375
MPN/g
SM92210E-2006
03/10/2022
MD
220310-41-02
Percent Solids
B-2
3.20
%
SM254082011
03/10/2022
MD
220310-41-03
Fecal Coliforms
B-3
7279
MPNtg
SM92210E.2006
03/10/2022
MD
220310-41-03
Percent Solids
B-3
3.16
%
SM25408.2011
03/10/2022
MD
220310-41-04
Fecal Coliforms
B-4
3406
MPN/g
W922ME-2006
03/10/2022
MD
220310-41-04
Percent Solids
B-4
3.23
%
SM25408.2011
03/1012022
MD
220310-41-05
Fecal Coliforms
B-5
25478
MPN/g
SM92210E-2006
03/10/2022
MD
220310-41-05
Percent Solids
8-5
3.14
%
SM254682011
03/10/2022
MD
220310-41-06
Fecal Coliforms
B-6
3963
MPN/g
SM92210E-2006
03/10/2022
MD
220310-41-06
Percent Solids
B-6
3,28
%
SN12540R-2011
03/10/2022
MD
220310-41-07
Fecal Coliforms
8-7
7034
MPN/g
SN192210E-2006
03/10/2022
MD
220310-41-07
Percent Solids
B-7
3.27
%
SM2540B-2011
03/10/2022
MD
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 - Statesville, NC 28687 - 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 220310-41-01 Tem on Arrival: 5.1
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 220310-41-02 Temp on Arrival: 5.1
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 220310-41-03 Temp on Arrival: 5.1
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 220310-41-04 Ternon Arrival: 5.1
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule, Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 220310-41-05 Temp on Arrival: 5.1
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 - Statesville, NC 28687 - 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 22031041-06 Temp on Arrival: 5.1
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
.Sale Number 220310-41-07 Tem p on Arrival: 5.1
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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