WQ0010689_2022 Residual Annual Report_20230224 (2)

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * WQ0010689
Applicant/Permittee Baxter Healthcare Corporation
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Asheville
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* DEREK BOUCHARD
Email Address*
Derek—[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
8287566644
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0010689
Has Current Existing permit number
Applicant/Permittee Address*
65 Pitts Station Road, Marion, NC 28752
Facility Name*
Baxter Healthcare Corporation Class A Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2022 Annual Ash Report - Signed Reduced.pdf 3MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/24/2023

Baer
2/9/2023
Division of Water Resources
Water Quality Permitting Section
Non -Discharge Permitting Unit
1636 Mail Service Center
Raleigh, NC 27699-1636
RE: 2022 Annual Ash Report
Permit No. WQ0010689
Wood Boiler North Cove, NC
Enclosed is the 2022 Annual Ash Distribution Report using the forms provided by NCDEQ-
DWQ. Included in this report is the following information:
- Class A Annual DMSDF and Supplemental Information
- Annual Residual Sampling Summary Form and Form-B
- Ash Distribution Landowner Utilization Agreements
- Lab Sheets
There were no permit deviations during the 2022 Reporting Year.
If you have any questions or require additional information, please contact me at 828-756-6644
or at derek—[e-mail].
Sincerely,
Derek Bouchard
Environmental Manager
Attachments: Annual Ash Report (3 copies)
Baxter Healthcare Corporation
PO Box 1390, Marion, NC 28752
T 828, 756.4151

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0010689 FACILITY NAME: Baxter Healthcare Corporation North Cove Steam Generation Plant Ash
PHONE: [phone] COUNTY: McDowell OPERATOR: Baxter Healthcare
FACILITY TYPE (please check one): C1 Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
i] Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes © No -aiw If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources() (s include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment)
Bulkrno Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
February
WQ0010689
2.
364.77
38477
See DMSDF Supp. Form
36477
Land Application
March
April
May
WQ0010689
120
300.15
420 15
See DMSDF Supp. Form
30015
Land Application
June
WQ0010689
80
202.28
See DMSDF Supp. Form
20228
Land Application
July
August
September
October
WQ0010689
40
315 15
355 15
See DMSDF Supp Form
315 15
Land Application
November
December
Total from FORM DMSDF (sup)l
260
1182.35
1442.35
118235
Totals: Annual (dry ns).-I
260
1182.35
1 1442.35
1182.35
Amendment(s) used: I None
Bulking Agent(s) used: Dry Wood Chips
* If more space is required, attach additional information sheets (FORM DMSDF (supp))• Total Number of Form DMSDF rSupp)j
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit © Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: ❑ No ------- I- If No, Explain In Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
3 No contravention of Ground Water Quality Standards occurred at a monitoring well
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. l am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Si Permitlee Date Signature of Preparer** Date
(if different from Permittee)
*"Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26)
DEN FORM DMSDF (Supp) (1212006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: WQ0010689 FACILITY NAME: Baxter Healthcare Corporation North Cove Steam Generation Plant Ash
PHONE: [phone] COUNTY: McDowell OPERATOR: — Baxter
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
0 Distribution and Marketing (complete Parts A, and B)
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
February
WQ0010689
20.00
364.77
384.77
Bill Phillips, Will Penland, Paul
Baker, Max Holland, Paul Baker,
Jeff Banks
364.77
Land Application
May
WQ0010689
120.00
300.15
420.15
Bill Phillips, Jim Pate
300.15
Land Application
June
WQ0010689
80.00
202.28
292.28
Jim Brewer, Darryl Ledbetter, Jeff
Banks
202.28
Land Application
October
WQ0010689
4000
315.15
355.15
Keneth Hughes, Brad Smith, Jeff
Banks
315.15
Land Application
Totals:
Annual (dry tons):
260
1182.35
1442.35
1182.35
Amendment(s) used:1
Bulking
Agent(s) used: Dry Wood Chips
* If more space is required, attach additional information sheets (FORM DMSDF (supp)):
Total Number of Form DMSDF (Supp)l I
DENR FORM DMSDF (Supp) (1212006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0010689 Laboratory:
Baxter Healthcare Corporation North Cove
Facility Name: Steam Generation Plant Ash
Residual Source WQ # or WQ0010689
NPDES #:
WWTP Name: NA
Residual Analvsis Data
1) Pace Analytical Services
2)
3)
4)
5)
Parameter
(mg(kg)
Cone.
Limit
m
Sam le
NP12121A
NP12121B
SP3232022A
SP3232022B
NP7192022A
NP719202213
Percent Moisture {"/o)
NA
51.5
52.1
56.4
56.6
51.2
53.3
Aluminum
NA
8,730
7,320
11200
10300
10300
8570
Arsenic
75
3.4
ND
ND
ND
5.1
5.1
Cadmium
85
2.8
2.5
304
3.6
4.6
3.9
Copper
4,300
66.9
54.9
63.9
60.8
81
73.1
Lead
840
25
21.2
39
37
65.9
46.5
Mercury
57
ND
ND
ND
ND
ND
ND
Molybdenum
75
ND
ND
ND
ND
ND
ND
Nickel
420
17.5
15.1
17.1
17.1
17.5
16.1
Selenium
100
2.8
2.6
4.9
5.3
3.9
4
Zinc
7,500
249
220
250
247
356
332
Phosphorus
NA
1500
2750
3000
2710
389
2140
Calcium
NA
104,000
90300
139000
133000
133000
125000
Magnesium
NA
14,600
12600
15700
17900
14300
13500
Potassium
NA
16,800
15800 1
10800
10I00
18900
16300
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false infqMation, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM DMSDF (Supp) (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0010689 Laboratory: 1) Pace Analytical Services
Baxter Healthcare Corporation North Cove
Facility Name: Steam Generation Plant Ash 2)
Residual Source
NPDES # or WQ#:
WWTP Name:
Residual Analysis Data
WQ0010689
NA
3)
4)
5)
Parameter
(mg/kg)
Sample or Com osite Date
NP12121A
NP12121B
SP3232022A
SP3232022B
NP7192022A
NP7192022B
Ammonia
ND
ND
ND
ND
ND
Nitrate Nitrogen
ND
ND
ND
ND
ND
Nitrite Nitrogen
ND
ND
ND
ND
ND
ND
PAN (by calc)
1330
729
951
882
13600
1050
SAR ft calc)
7.59
7.7
3.3
3.03
6.94
6.65
TICK
4430
2430
3170
2940
45400
3510
Sodium
14200
13500
7390
6750
14300
13600
H
9.1
9
9.2
9.2
10.1
10
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant enalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
.I �N
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM DMSDF (Supp) (12/2006)

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/2025), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to _i I (Recipient). Application of
the aforementioned ash is prohibited except in accordance with the instructions on this sheet.
Transport: Adequate provisions shall he taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must he available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, harriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application: When using ash, the Billowing shall apply:
+ The ash application rates shall he limited to those that can be agronomically -justified (i.e., limited to that needed to meet the
liming requirements of the crops being grown on the land).
• Residual ash cake shall not be stockpiled for more than 60 days prior to land application
• Application of ash cake residuals shall not occur within 100 feet of a public or private water supply
• Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
perennial waterbodies, and wetlands
• Copies of this Utilization Agreement, Ash Permit No.WQ0010689, and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not he placed within one foot of the seasonal high water table or bedrock.
• Ash shall not he applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs Billowing a 0.5" rainfall
o If the land application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be held liable by Recipient or any third party for any spill. misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority. whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling
or other use of the ash.
Signed (Ash Recipient): Date: oCQU
Ash Recipient's Address: r S V� ��,
Intended Use of Ash:
Expected Qty/Yr: Q ft]
cres f nd: 12 _
Baxter Representative Signature:
Page 2 of' 3
Updated: January 2020

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/2025), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to fir4 . J6 (R9 pient). Application of
the aforementioned ash is prohibited except in accordance with the ins ructions on [hi heet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically -justified (i.e., limited to that needed to meet the
liming requirements of the crops being grown on the land).
• Residual ash cake shall not be stockpiled for more than 60 days prior to land application
• Application of ash cake residuals shall not occur within 100 feet of a public or private water supply
• Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
perennial waterbodies, and wetlands.
• Copies of this Utilization Agreement, Ash Permit No.WQ0010689, and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not be placed within one foot of the seasonal high water table or bedrock.
• Ash shall not be applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs following a 0.5" rainfall
o If the land application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling
or other use of the ash.
Signed (Ash Recipient): , Date: %,z
Ash Recipient's Mailing Address: [j'/DS �%F- /Yl�✓ NG
Intended Use of Ash and Crop Type: vJ 11 C.c. YVl jyy
Expected Qty/Yr: 60
Baxter Representative Signature:
Acres of Land: /i J %'ae h/
Page 2 of 3

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/2025), Baxter Copy
11"RBaxter Healthcare, Corp., is the generator of the ash provided toJ k (Recipient). Application of
the aforementioned ash is prohibited except in accordance with th instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed to meet the
liming requirements of the crops being grown on the land).
• Residual ash cake shall not be stockpiled for more than 60 days prior to land application
• Application of ash cake residuals shall not occur within 100 feet of a public or private water supply
• Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
perennial waterbodies, and wetlands.
• Copies of this Utilization Agreement, Ash Permit No.WQ0010689, and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not be placed within one foot of the seasonal high water table or bedrock.
• Ash shall not be applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs following a 0.5" rainfall
o If the land application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling
or other use of the ash.
i
Signed (Ash Recipient): / : J_ /, ^� �D/ate: —�
Ash Recipient's Mailing Address: f L?,2& A S � v� � /Y ooftiaw /VC
i r
Intended Use of Ash and Crop Type: J O / /
Expected QtyNr: 6 / .M it
Baxter Representative Signature:
Acres of Land: 4 4g
Page 2 of 3

A'r �j.
Baxter Healthcare, Corp.
2859 Old Linville Road
Marron, North Carolina 28752
Ash Distribution Utilization Agreement (Val' thru 3/30/2025), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to (Recipient). Application of
the aforementioned ash is prohibited except in accordance with the instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically -justified (i.e., limited to that needed to meet the
liming requirements of the crops being grown on the land).
• Residual ash cake shall not be stockpiled for more than GO days prior to land application
• Application or ash cake residuals shall not occur within 100 feet of a public or private water supply
• Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
perennial waterbodies, and wetlands.
• Copies of this Utilization Agreement, Ash Permit No.WQ00I0689, and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not be placed within one foot of the seasonal high water table or bedrock.
• Ash shall not be applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs following a 0.5" rainfall
o If the land application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling
or other use of the ash.
Signed (Ash Recipient): Date:' T '/
Ash Recipient's Address: l
Intended Use of Ash:
Expected Qty/Yr: ___,_3( /\/SS Acres ofLand:
Baxter Representative Signature:
Page 2 of 3
Updated: January 2020

lwn! R,-d�
Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/2025(), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to 14i'C �� be7 ef-(Rccipient). Application of
the aforementioned ash is prohibited except in accordance with the instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed to meet the
liming requirements of the crops being grown on the land).
• Residual ash cake shall not be stockpiled for more than 60 days prior to land application
• Application of ash cake residuals shall not occur within 100 feet of a public or private water supply
• Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
perennial waterbodies, and wetlands.
• Copies of this Utilization Agreement, Ash Permit No.WQ0010689, and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not be placed within one foot of the seasonal high water table or bedrock.
• Ash shall not be applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs following a 0.5" rainfaIl
o If the land application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling
or other use of the ash.
Signed (Ash Recipient): I. 6 fT- Date: l
Ash Recipient's Address: 1 T Iran � �} } t° _ M W 1 t) (\ 1AC o2 4 160
Intended Use of Ash; :S0t� QrD C.�Y1,Q�
Expected Qty/Yr:
Baxter Representative Signature:
Acres of Land: .w
Page 2 of 3
Updated: January 2020

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/202_ , Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to Ara sz:_�?'r r . Application of
the aforementioned ash is prohibited except in accordance with the instructions on this sheet.
Taansport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application: Wien using ash, the following shall apply:
• The mh application rztes shall be limited to those that can be agronomically justified (i.e., limited to that needed to meet the
liming requinmients of the crops being grown on the land).
• Residual ash cake shall not be stockpiled for more than 60 days prior to land application
• Application of ash cake residuals shall not occur within 100 feet of a public or private water supply
• Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
perennial watrrbodies, and wetlands.
• Copies of tbis Utilization Agreement, Ash Permit No.WQ0010689, and the Operation and Maintenance Plan shall be maintained
at the iand application site when bulk residuals are being applied.
• Ash shall not be placed within one foot of the seasonal high water table or bedrock.
• As1. shall not be applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff
0 During precipitation events or within 24-hrs following a 0.5" rainfall
e If the land application site does not have established vegetative cover crop
o if the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
vill have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,
judgment or recovery asserted against Baxter Healthcare, Cote by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling
or other use of the ash. 2141
Signed (Ash Recipient): Date:
Ash Recipient's Mailing Address: \' \
Intended Use of Ash and Crop Type:
'Expected Qtv/Yr: 3 v ] p wS Acres of Land:
Baxter Representative Signature:
Page 2 of 3

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/2025), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to ? Y< "A k� (Recipient). Application of
the aforementioned ash is prohibited except in accordance with the instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed to meet the
liming requirements of the crops being grown on the land).
• Residual ash cake shall not be stockpiled for more than 60 days prior to land application
• Application of ash cake residuals shall not occur within 100 feet of a public or private water supply
• Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
perennial waterbodies, and wetlands.
• Copies of this Utilization Agreement, Ash Permit No.WQ0010689, and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not be placed within one foot of the seasonal high water table or bedrock.
• Ash shall not be applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs following a 0.5" rainfall
o If the land application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling
or other use of the ash.
Signed (Ash Recipient): i'C Date: / il Z
Ash Recipient's Address: %lo �f 5� �!/R Y;/,g 1p
Intended Use of Ash:ll-�Y��
Expected QtyNr: T'r_— 1) / v �� f ocry,<of
Baxter Representative
Page 2 of 3
Updated: January 2020

axter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/2025), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to k--e 1) '1L )4 Lt C # l'4 (Recipient). Application of
the aforementioned ash is prohibited except in accordance with the instructions o this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed to meet the
liming requirements of the crops being grown on the land).
• ResiduaI ash cake shall not be stockpiled for more than 60 days prior to land application
• Application of ash cake residuals shall not occur within 100 feet of a public or private water supply
• Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
perennial waterbodies, and wetlands.
• Copies of this Utilization Agreement, Ash Permit No.WQ0010689, and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not be placed within one foot of the seasonal high water table or bedrock.
• Ash shall not be applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs following a 0.5" rainfall
o If the land application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling
or other use of the ash.
Signed (Ash Recipient): Date:
Ash Recipient's Address: MGjs //u b��Uc e 72'7
Intended Use of Ash:
Expected Qty/Yr: 3 ate rrS A o and -
Baxter Representative Signature: '
Page 2 of 3
Updated: January 2020

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreementt (Valid thru 3/30/2025), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to �`' �[ ll �' p (Recipient). Application of
the aforementioned ash is prohibited except in accordance with the instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed to meet the
liming requirements of the crops being grown on the land).
• Residual ash cake shall not be stockpiled for more than 60 days prior to land application
• Application of ash cake residuals shall not occur within 100 feet of a public or private water supply
• Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
perennial waterbodies, and wetlands.
• Copies of this Utilization Agreement, Ash Permit No.WQ0010689, and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not be placed within one foot of the seasonal high water table or bedrock.
• Ash shall not be applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs following a 0.5" rainfall
o If the land application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling
or other use of the ash.
Signed (Ash Recipient): 0141
4[WPS
Date:
jr�,—
Ash Recipients Address:
P o 3 a
s� I l 1�� t:c
�n r
,s" r�
Intended Use of Ash:©� n- l21 �� r/► '�
Expected Qty/Yr: es f Land: So
Baxter Representative Signature:
Page 2 of 3
Updated: January 2020
7

Wlu
axter Healthcare, Cor •
2859 Old Linville Road
Marion, North Carolina 28752
Ash )Distribution Utilization Agreement (Valid thru 3/3Q/2Q25)9 Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to e Lr �4d,�S
the aforementioned ash is prohibited except in accordance with the instructions oil thissheet. (Recipient), Application of
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from ca
rryinashuse of wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy condi onsor ifIeros on ornto anyrruanoffwaters. The
cannot be
controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed to meet the
liming requirements of the crops being grown on the land).
• Residual ash cake shall not be stockpiled for more than SO days prior to land application
• Application of ash cake residuals shall not occur within 100 feet of a public or private water supply
• Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
perennial waterbodies, and wetlands.
• Copies of this Utilization Agreement, Ash Permit No.WQ0010689, and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not be placed within one foot of the seasonal high water table or bedrock.
• Ash shall not be applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff o During precipitation events or within 24-hrs following a 0.5" rainfall
o If the land application site does not have established vegetative cover crop
n If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet, Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify,
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys'and fee ),clla m, demand, hld Baxter suit,ea Con
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including an
y governmenal authority,bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportationl�hether for
andling
or other use of the ash.
Signed (Ash Recipient): 3e����,kS
Date: 17 - ZZ
Ash Recipient's Mailing Address: g 7 i/ C o fj r,
/yc 12 &7sZ
Intended Use of Ash and Crop Type: L M r_
Expected Qty/Yr: — —�
Acres of Land: Q �j
Baxter Representative Signature —
Page 2 of 3

axter Healthcare, Corp.
2859 Old Linville, Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/2025), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to `7
the aforementioned ash is prohibited except in accordance with the instructions on this beet? (Recipient). Application of
Transport. Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (c.g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
Provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically -justified (i.e., limited to that needed to meet the
liming requirements of the crops being grown on the land).
• Residual ash cake shall not be stockpiled for more than 60 days prior to land application
• Application of ash cake residuals shall not occur within 100 feet of a public or private water supply
• Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
perennial waterbodies, and wetlands.
• Copies of this Utilization Agreement, Ash Permit No.WQ0010689, and the Operation. and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not be placed within one foot of the seasonal high water table or bedrock.
• Ash shall not be applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs following a 0.5" rainfall
o If the land application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify,
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys'and f es), claim,hold B�ter demand, suit, actiorn,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling
or other use of the ash.
Signed (Ash Recipient): Z�c C Date:
U� z2
Ash Recipient's Mailing Address: MgV 1A < Z Z
Intended Use of Ash and Crop Type: 5 . 2e f, J P n Sy�� /
Expected Qty/Yr: 02 2 �S0
Acres of band;
Baxter Representative Signature:
age 2 of 3

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
December 10, 2021
Mr. Ricky Styles
Baxter Healthcare
2859 Old Linville Road
Marion, NC 28752
RE: Project: North Pond Ash 12/1
Pace Project No.: 92575413
Dear Mr. Styles:
Enclosed are the analytical results for sample(s) received by the laboratory on December 02, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
1(828)254-7176
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 20

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: North Pond Ash 12/1
Pace Project No.: 92575413
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water#: LA029
Virginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
North Carolina Certification #: 381
South Carolina Certification #: 98011001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 20

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: North Pond Ash 12/1
Pace Project No.: 92575413
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92575413001 NP12121A
EPA 9045D
TBM
1
PASI-GA
EPA 601 OD
IDS, JOR
13
PASI-A
EPA 7471 B
RDT
1
PASI-A
SM 254OG-2011
KDF
1
PASI-C
SW-846
KDF
1
PASI-C
None
DMN
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
NGP
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
3
PASI-A
EPA 365.1 Rev 2.0 1993
MDW
1
PASI-A
92575413002 NP12121B
EPA9045D
TBM
1
PASI-GA
EPA 601OD
IDS, JOR
13
PASI-A
EPA 7471 B
RDT
1
PASI-A
SM 254OG-2011
KDF
1
PASI-C
SW-846
KDF
1
PASI-C
None
DMN
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
NGP
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
3
PASI-A
EPA 365.1 Rev 2.0 1993
MDW
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-GA = Pace Analytical Services - Peachtree Corners, GA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 20

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: North Pond Ash 12/1
Pace Project No.: 92575413
Sample: NP12121A
Lab ID: 92575413001 Collected:
12/01/21 09:00
Received: 12/02/21 11:46 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services - Peachtree Corners, GA
pH at 25 Degrees C
9.1 Std. Units
0.10
1
12/07/21 16:50
H3
6010 MET ICP
Analytical Method: EPA6010D Preparation
Method:
EPA 3050B
Pace Analytical Services - Asheville
Aluminum
8730 mg/kg
13.6
1
12/03/21 15:34
12/08/21 03:25
7429-90-5
Arsenic
3.4 mg/kg
3.4
1
12/03/21 15:34
12/08/21 03:25
7440-38-2
Cadmium
2.8 mg/kg
0.14
1
12/03/21 15:34
12/08/21 03:25
7440-43-9
Calcium
104000 mg/kg
339
10
12/03/21 15:34
12/08/21 17:25
7440-70-2
Copper
66.9 mg/kg
6.8
1
12/03/21 15:34
12/08/21 03:25
7440-50-8
Lead
25.0 mg/kg
1.4
1
12/03/21 15:34
12/08/21 03:25
7439-92-1
Magnesium
14600 mg/kg
136
10
12/03/21 15:34
12/08/21 17:25
7439-95-4
Molybdenum
ND mg/kg
6.8
1
12/03/21 15:34
12/08/21 03:25
7439-98-7
Nickel
17.5 mg/kg
0.68
1
12/03/21 15:34
12/08/21 03:25
7440-02-0
Potassium
16800 mg/kg
6780
10
12/03/21 15:34
12/08/21 17:25
7440-09-7
Selenium
2.8 mg/kg
1.4
1
12/03/21 15:34
12/08/21 03:25
7782-49-2
Sodium
14200 mg/kg
6780
10
12/03/21 15:34
12/08/21 17:25
7440-23-5
Zinc
249 mg/kg
1.4
1
12/03/21 15:34
12/08/21 03:25
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation
Method:
EPA 7471 B
Pace Analytical Services - Asheville
Mercury
ND mg/kg
0.0067
1
12/08/2114:45
12/08/2117:11
7439-97-6
2540G Total Percent Solids
Analytical Method: SM 2540G-2011
Pace Analytical Services - Charlotte
Total Solids
48.5 %
0.10
1
12/03/21 18:19
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
51.5 %
0.10
1
12/03/21 18:12
N2
Plant Available Nitrogen
Analytical Method: None
Pace Analytical Services - Asheville
Plant Available Nitrogen
1330 mg/kg
1
12/09/21 17:27
N2
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0
1993 Mod.
Preparation
Method:
EPA 350.1 Rev 2.0
1993 Mod.
Pace Analytical Services - Asheville
Nitrogen, Ammonia
ND mg/kg
20.6
1
12/09/21 09:13
12/09/21 12:18
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0
1993 Preparation
Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Kjeldahl, Total
4430 mg/kg
491
5
12/06/21 21:36
12/07/21 05:45
7727-37-9
M1
REPORT OF LABORATORY ANALYSIS
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9800 Kincey Ave. Suite 100
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ANALYTICAL RESULTS
Project: North Pond Ash 12/1
Pace Project No.: 92575413
Sample: NP12121A Lab ID: 92575413001 Collected: 12/01/21 09:00 Received: 12/02/21 11:46 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
353.2 Nitrogen, NO2/NO3 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, NO2 plus NO3 ND mg/kg 8.2 1 12/02/21 22:16 12/02/21 23:45
Nitrogen, Nitrate ND mg/kg 8.2 1 12/02/21 22:16 12/02/21 23:45 14797-55-8
Nitrogen, Nitrite ND mg/kg 8.2 1 12/02/21 22:16 12/02/21 23:45 14797-65-0
365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Phosphorus 1500 mg/kg 18.1 10 12/06/2122:17 12/07/2117:14 7723-14-0 M1
Date: 12/10/2021 03:47 PM
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: North Pond Ash 12/1
Pace Project No.: 92575413
Sample: NP12121B
Lab ID: 92575413002 Collected:
12/01/21 09:00
Received: 12/02/21 11:46 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services - Peachtree Corners, GA
pH at 25 Degrees C
9.0 Std. Units
0.10
1
12/07/21 16:50
H3
6010 MET ICP
Analytical Method: EPA6010D Preparation Method:
EPA 3050B
Pace Analytical Services - Asheville
Aluminum
7320 mg/kg
14.1
1
12/03/21 15:34
12/08/21 03:28
7429-90-5
Arsenic
ND mg/kg
3.5
1
12/03/21 15:34
12/08/21 03:28
7440-38-2
Cadmium
2.5 mg/kg
0.14
1
12/03/21 15:34
12/08/21 03:28
7440-43-9
Calcium
90300 mg/kg
353
10
12/03/21 15:34
12/08/21 17:29
7440-70-2
Copper
54.9 mg/kg
7.1
1
12/03/21 15:34
12/08/21 03:28
7440-50-8
Lead
21.2 mg/kg
1.4
1
12/03/21 15:34
12/08/21 03:28
7439-92-1
Magnesium
12600 mg/kg
14.1
1
12/03/21 15:34
12/08/21 03:28
7439-95-4
Molybdenum
ND mg/kg
7.1
1
12/03/21 15:34
12/08/21 03:28
7439-98-7
Nickel
15.1 mg/kg
0.71
1
12/03/21 15:34
12/08/21 03:28
7440-02-0
Potassium
15800 mg/kg
7060
10
12/03/21 15:34
12/08/21 17:29
7440-09-7
Selenium
2.6 mg/kg
1.4
1
12/03/21 15:34
12/08/21 03:28
7782-49-2
Sodium
13500 mg/kg
7060
10
12/03/21 15:34
12/08/21 17:29
7440-23-5
Zinc
220 mg/kg
1.4
1
12/03/21 15:34
12/08/21 03:28
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation Method:
EPA 7471 B
Pace Analytical Services - Asheville
Mercury
ND mg/kg
0.011
1
12/08/2114:45
12/08/2117:13
7439-97-6
2540G Total Percent Solids
Analytical Method: SM 2540G-2011
Pace Analytical Services - Charlotte
Total Solids
47.8 %
0.10
1
12/03/21 18:19
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
52.1 %
0.10
1
12/03/21 18:12
N2
Plant Available Nitrogen
Plant Available Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
Date: 12/10/2021 03:47 PM
Analytical Method: None
Pace Analytical Services - Asheville
729 mg/kg 1 12/09/2117:27 N2
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services - Asheville
ND mg/kg 20.5 1 12/09/2109:13 12/09/2112:20 7664-41-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
2430 mg/kg 104 1 12/06/2121:36 12/07/21 05:23 7727-37-9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: North Pond Ash 12/1
Pace Project No.: 92575413
Sample: NP12121B Lab ID: 92575413002 Collected: 12/01/21 09:00 Received: 12/02/21 11:46 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
353.2 Nitrogen, NO2/NO3 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, NO2 plus NO3 ND mg/kg 8.2 1 12/02/21 22:16 12/02/21 23:48
Nitrogen, Nitrate ND mg/kg 8.2 1 12/02/21 22:16 12/02/21 23:48 14797-55-8
Nitrogen, Nitrite ND mg/kg 8.2 1 12/02/21 22:16 12/02/21 23:48 14797-65-0
365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Phosphorus 2750 mg/kg 41.0 20 12/06/2122:17 12/07/2118:52 7723-14-0
Date: 12/10/2021 03:47 PM
REPORT OF LABORATORY ANALYSIS
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Page 7 of 20

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: North Pond Ash 12/1
Pace Project No.: 92575413
QC Batch: 664365 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Laboratory: Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92575413001, 92575413002
SAMPLE DUPLICATE: 3479851
92574046001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 7.6 7.8 4 H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: North Pond Ash 12/1
Pace Project No.: 92575413
QC Batch: 664418 Analysis Method: EPA 7471 B
QC Batch Method: EPA 7471 B Analysis Description: 7471 Mercury
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92575413001, 92575413002
METHOD BLANK: 3480194
Matrix:
Solid
Associated Lab Samples: 92575413001, 92575413002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Mercury
mg/kg
ND
0.0060
12/08/2116:57
LABORATORY CONTROL SAMPLE:
3480195
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Mercury
mg/kg
0.083
0.091
109 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3480196 3480197
MS MSD
92575657006 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 0.013 0.05 0.061 0.064 0.072 99 96 75-125 13
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 03:47 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 20

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: North Pond Ash 12/1
Pace Project No.: 92575413
QC Batch: 663797
QC Batch Method: EPA 3050B
Associated Lab Samples: 92575413001, 92575413002
METHOD BLANK: 3477116
Associated Lab Samples: 92575413001, 92575413002
Parameter Units
Aluminum
mg/kg
Arsenic
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Copper
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Sodium
mg/kg
Zinc
mg/kg
LABORATORY CONTROL SAMPLE:
3477117
Parameter
Units
Aluminum
mg/kg
Arsenic
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Copper
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Sodium
mg/kg
Zinc
mg/kg
QUALITY CONTROL DATA
Analysis Method: EPA6010D
Analysis Description: 6010 MET
Laboratory: Pace Analytical Services - Asheville
Matrix: Solid
Blank
Result
Spike
Cone.
500
50
50
500
50
50
500
50
50
500
50
500
50
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Reporting
Limit Analyzed
LCS
Result
498
45.1
46.2
493
45.6
45.4
486
51.8
45.8
ND
44.0
506
45.3
Qualifiers
10.0 12/08/21 02:43
2.5 12/08/21 02:43
0.10 12/08/21 02:43
25.0 12/08/21 02:43
5.0 12/08/21 02:43
1.0 12/08/21 02:43
10.0 12/08/21 02:43
5.0 12/08/21 02:43
0.50 12/08/21 02:43
500 12/08/21 02:43
1.0 12/08/21 02:43
500 12/08/21 02:43
1.0 12/08/21 02:43
LCS
% Rec
100
90
92
99
91
91
97
104
92
100
88
101
91
% Rec
Limits
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3477118
3477119
MS
MSD
92575146001 Spike
Spike
MS
MSD
MS MSD % Rec
Parameter Units Result Cone.
Cone.
Result
Result
% Rec % Rec Limits RPD Qual
Aluminum mg/kg 16800 967
1060
17900
19700
119 273 75-125 9 M1
Arsenic mg/kg ND 96.7
106
83.9
91.2
83 83 75-125 8
Results presented on this page are in the units indicated by the
"Units" column except where
an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 03:47 PM without the written consent of Pace Analytical Services, LLC.
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aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: North Pond Ash 12/1
Pace Project No.: 92575413
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3477118
3477119
MS
MSD
92575146001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
mg/kg
27.4
96.7
106
102
121
77
89
75-125
18
Calcium
mg/kg
23600
967
1060
23500
23700
-13
9
75-125
1 E,M1
Copper
mg/kg
4840
96.7
106
4500
4900
-346
54
75-125
8 M1
Lead
mg/kg
525
96.7
106
646
730
125
193
75-125
12 M1
Magnesium
mg/kg
1760
967
1060
2680
2840
95
102
75-125
6
Molybdenum
mg/kg
36.9
96.7
106
130
141
96
98
75-125
8
Nickel
mg/kg
257
96.7
106
327
334
72
72
75-125
2 M1
Potassium
mg/kg
ND
967
1060
1890
2000
113
113
75-125
6
Selenium
mg/kg
ND
96.7
106
77.9
85.7
79
79
75-125
9
Sodium
mg/kg
ND
967
1060
2080
2200
112
113
75-125
5
Zinc
mg/kg
19100
96.7
106
17800
18100
-1390
-984
75-125
2 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 03:47 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 20

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: North Pond Ash 12/1
Pace Project No.: 92575413
QC Batch: 663903 Analysis Method: SW-846
QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92575413001, 92575413002
SAMPLE DUPLICATE: 3477888
92575343001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 79.0 78.8 0 N2
SAMPLE DUPLICATE: 3477889
92575616001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 14.1 13.3 6 N2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: North Pond Ash 12/1
Pace Project No.: 92575413
QC Batch: 664788 Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod. Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92575413001, 92575413002
METHOD BLANK: 3482268
Matrix:
Solid
Associated Lab Samples: 92575413001, 92575413002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Ammonia
mg/kg
ND
9.8
12/09/21 12:10
LABORATORY CONTROL SAMPLE:
3482269
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Nitrogen, Ammonia
mg/kg
481
490
102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3482270 3482271
MS MSD
92574959001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/kg ND 2810 2860 2850 2860 101 99 90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/10/2021 03:47 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 20

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: North Pond Ash 12/1
Pace Project No.: 92575413
QC Batch: 664139 Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92575413001, 92575413002
METHOD BLANK: 3478851
Matrix:
Solid
Associated Lab Samples: 92575413001, 92575413002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg
ND
50.0
12/07/21 05:17
LABORATORY CONTROL SAMPLE:
3478852
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg
1000
995
99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3478853 3478854
MS MSD
92575413001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 4430 1790 1960 5750 5340 73 46 90-110 7 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/10/2021 03:47 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 20

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: North Pond Ash 12/1
Pace Project No.: 92575413
QC Batch: 663585 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92575413001, 92575413002
METHOD BLANK: 3476144
Associated Lab Samples: 92575413001, 92575413002
Parameter Units
Nitrogen, Nitrate mg/kg
Nitrogen, Nitrite mg/kg
Nitrogen, NO2 plus NO3 mg/kg
Matrix: Solid
Blank Reporting
Result Limit Analyzed
ND 4.0 12/02/2123:42
ND 4.0 12/02/2123:42
ND 4.0 12/02/2123:42
Qualifiers
LABORATORY CONTROL SAMPLE: 3476145
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/kg 15 14.7 98 90-110
Nitrogen, Nitrite mg/kg 10 10.3 103 90-110
Nitrogen, NO2 plus NO3 mg/kg 25 25.0 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3476146
3476147
MS
MSD
92575413001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits RPD Qual
Nitrogen, Nitrate
mg/kg
ND
29.9
30.5
34.3
34.1
115
112
90-110 1
Nitrogen, Nitrite
mg/kg
ND
20
20.4
21.3
20.9
107
103
90-110 2
Nitrogen, NO2 plus NO3
mg/kg
ND
49.9
50.9
55.6
55.0
105
102
90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: North Pond Ash 12/1
Pace Project No.: 92575413
QC Batch: 664233 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92575413001, 92575413002
METHOD BLANK: 3479396
Matrix:
Solid
Associated Lab Samples: 92575413001, 92575413002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Phosphorus
mg/kg
ND
0.76
12/07/2117:13
LABORATORY CONTROL SAMPLE:
3479397
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Phosphorus
mg/kg
36.2
38.1
105 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3479398 3479399
MS MSD
92575413001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/kg 1500 95.4 93.8 1700 1790 211 309 90-110 5 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/10/2021 03:47 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 20

Pace Analytical Services, LLC
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Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: North Pond Ash 12/1
Pace Project No.: 92575413
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
E Analyte concentration exceeded the calibration range. The reported result is estimated.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 03:47 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 20

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
North Pond Ash 12/1
92575413
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92575413001
NP12121A
EPA 9045D
664365
92575413002
NP12121B
EPA 9045D
664365
92575413001
NP12121A
EPA3050B
663797
EPA 6010D
663920
92575413002
NP12121B
EPA3050B
663797
EPA 6010D
663920
92575413001
NP12121A
EPA 7471B
664418
EPA 7471B
664805
92575413002
NP12121B
EPA 7471B
664418
EPA 7471B
664805
92575413001
NP12121A
SM 2540G-2011
664082
92575413002
NP12121B
SM 2540G-2011
664082
92575413001
NP12121A
SW-846
663903
92575413002
NP12121B
SW-846
663903
92575413001
NP12121A
None
665118
92575413002
NP12121B
None
665118
92575413001
NP12121A
EPA 350.1 Rev 2.0
1993
664788
EPA 350.1 Rev 2.0
1993
664949
Mod.
Mod.
92575413002
NP12121B
EPA 350.1 Rev 2.0
1993
664788
EPA 350.1 Rev 2.0
1993
664949
Mod.
Mod.
92575413001
NP12121A
EPA 351.2 Rev 2.0
1993
664139
EPA 351.2 Rev 2.0
1993
664267
92575413002
NP12121B
EPA 351.2 Rev 2.0
1993
664139
EPA 351.2 Rev 2.0
1993
664267
92575413001
NP12121A
EPA 353.2 Rev 2.0
1993
663585
EPA 353.2 Rev 2.0
1993
663586
92575413002
NP12121B
EPA 353.2 Rev 2.0
1993
663585
EPA 353.2 Rev 2.0
1993
663586
92575413001
NP12121A
EPA 365.1 Rev 2.0
1993
664233
EPA 365.1 Rev 2.0
1993
664255
92575413002
NP12121B
EPA 365.1 Rev 2.0
1993
664233
EPA 365.1 Rev 2.0
1993
664255
Date: 12/10/2021 03:47 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 18 of 20

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P ge 19 of 20

Document Name:
Document Revised: November 15, 2021
Sample Condition Upon Receipt ($CUR)
Page 2 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.08
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottles
Project # Wa# : 575413
PM: CDl Due Date: 12/09/21
CLIENT: 92-Baxter
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pH Adjustment Log for Preserved Samples
Sample lu
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
Amount of Preservative
Lat ff
adjusted
added
Note- Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certificatinn Office (i.e.
Out of hold, incorrect preservative, put of temp, incorrect cnnta#Hers.
Page 20 of 20

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
April 24, 2022
Mr. Ricky Styles
Baxter Healthcare
2859 Old Linville Road
Marion, NC 28752
RE: Project: Baxter Biomass 4/6
Pace Project No.: 92597406
Dear Mr. Styles:
Enclosed are the analytical results for sample(s) received by the laboratory on April 06, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
��
Lorri Patton
[e-mail]
1(828)254-7176
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Baxter Biomass 4/6
Pace Project No.: 92597406
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water#: LA029
Virginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 23

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Baxter Biomass 4/6
Pace Project No.: 92597406
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92597406001 SP3232022A EPA 601 OD
CBV
13
PASI-A
EPA 601 OD
CBV
7
PASI-A
EPA 7470A
RDT
1
PASI-A
EPA 7471 B
DBB1
1
PASI-A
SW-846
KDF
1
PASI-C
EPA 9045D
YEG
1
PASI-A
None
DMN
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
NDS
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
SMT
3
PASI-A
EPA 365.1 Rev 2.0 1993
KDF1
1
PASI-A
92597406002 SP3232022B EPA 601 OD
CBV
13
PASI-A
EPA 601OD
CBV
7
PASI-A
EPA 7470A
RDT
1
PASI-A
EPA 7471 B
DBB1
1
PASI-A
SW-846
KDF
1
PASI-C
EPA 9045D
YEG
1
PASI-A
None
DMN
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
NDS
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
SMT
3
PASI-A
EPA 365.1 Rev 2.0 1993
KDF1
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Baxter Biomass 4/6
Pace Project No.: 92597406
Sample: SP3232022A
Lab ID: 92597406001 Collected: 04/06/22 09:30 Received: 04/06/22 11:03 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
Aluminum
11200 mg/kg 23.0 1 04/07/2210:30
04/11/2216:04
7429-90-5
Arsenic
ND mg/kg 5.7 1 04/07/2210:30
04/11/2216:04
7440-38-2
Cadmium
3.4 mg/kg 0.23 1 04/07/2210:30
04/11/2216:04
7440-43-9
Calcium
139000 mg/kg 574 10 04/07/2210:30
04/12/2213:03
7440-70-2
Copper
63.9 mg/kg 11.5 1 04/07/2210:30
04/11/2216:04
7440-50-8
Lead
39.0 mg/kg 2.3 1 04/07/2210:30
04/11/2216:04
7439-92-1
Magnesium
15700 mg/kg 23.0 1 04/07/2210:30
04/11/2216:04
7439-95-4
Molybdenum
ND mg/kg 11.5 1 04/07/2210:30
04/11/2216:04
7439-98-7
Nickel
17.1 mg/kg 1.1 1 04/07/2210:30
04/11/2216:04
7440-02-0
Potassium
10800 mg/kg 1150 1 04/07/2210:30
04/11/2216:04
7440-09-7
Selenium
4.9 mg/kg 2.3 1 04/07/2210:30
04/11/2216:04
7782-49-2
Sodium
7390 mg/kg 1150 1 04/07/2210:30
04/11/2216:04
7440-23-5
Zinc
250 mg/kg 2.3 1 04/07/2210:30
04/11/2216:04
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 04/07/22 14:59 Initial pH: 9.32; Final
pH: 2
Pace Analytical Services - Asheville
Arsenic
ND mg/L 0.050 1 04/09/22 03:47
04/11/22 11:09
7440-38-2
Barium
2.0 mg/L 0.25 1 04/09/22 03:47
04/11/22 11:09
7440-39-3
Cadmium
ND mg/L 0.0050 1 04/09/22 03:47
04/11/22 11:09
7440-43-9
Chromium
ND mg/L 0.050 1 04/09/22 03:47
04/11/22 11:09
7440-47-3
Lead
ND mg/L 0.025 1 04/09/22 03:47
04/11/22 11:09
7439-92-1
Selenium
ND mg/L 0.10 1 04/09/22 03:47
04/11/22 11:09
7782-49-2
Silver
ND mg/L 0.025 1 04/09/22 03:47
04/11/22 11:09
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311; 04/07/22 14:59 Initial pH: 9.32; Final
pH: 2
Pace Analytical Services - Asheville
Mercury
ND mg/L 0.00020 1 04/21/2211:08
04/21/2215:11
7439-97-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B
Pace Analytical Services - Asheville
Mercury
ND mg/kg 0.013 1 04/07/2213:36
04/12/2211:41
7439-97-6
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
56.4 % 0.10 1
04/07/22 16:04
N2
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
9.2 Std. Units 0.10 1
04/13/22 09:48
H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/24/2022 06:01 PM
without the written consent of Pace Analytical Services, LLC.
Page 4 of 23

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Baxter Biomass 4/6
Pace Project No.: 92597406
Sample: SP3232022A Lab ID: 92597406001 Collected: 04/06/22 09:30 Received: 04/06/22 11:03 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Plant Available Nitrogen
Plant Available Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
365.1 Phosphorus, Total
Phosphorus
Date: 04/24/2022 06:01 PM
Analytical Method: None
Pace Analytical Services - Asheville
951 mg/kg
1 04/19/2214:57 N2
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod.
Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services - Asheville
ND mg/kg 9.5
1 04/08/22 09:36 04/08/22 14:22 7664-41-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
3170 mg/kg 109
1 04/09/22 05:53 04/12/22 04:27 7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
ND mg/kg 9.0
1 04/06/22 22:42 04/07/22 00:43
ND mg/kg 9.0
1 04/06/22 22:42 04/07/22 00:43 14797-55-8
ND mg/kg 9.0
1 04/06/22 22:42 04/07/22 00:43 14797-65-0
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
3000 mg/kg 54.2
25 04/07/22 20:44 04/08/22 08:57 7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Baxter Biomass 4/6
Pace Project No.: 92597406
Sample: SP3232022B Lab ID: 92597406002 Collected: 04/06/22 09:30 Received: 04/06/22 11:03 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
Aluminum
10300 mg/kg
20.2
1
04/07/2210:30
04/11/2216:07
7429-90-5
Arsenic
ND mg/kg
5.1
1
04/07/2210:30
04/11/2216:07
7440-38-2
Cadmium
3.6 mg/kg
0.20
1
04/07/2210:30
04/11/2216:07
7440-43-9
Calcium
133000 mg/kg
505
10
04/07/2210:30
04/12/2213:06
7440-70-2
Copper
60.8 mg/kg
10.1
1
04/07/2210:30
04/11/2216:07
7440-50-8
Lead
37.0 mg/kg
2.0
1
04/07/2210:30
04/11/2216:07
7439-92-1
Magnesium
17900 mg/kg
20.2
1
04/07/2210:30
04/11/2216:07
7439-95-4
Molybdenum
ND mg/kg
10.1
1
04/07/2210:30
04/11/2216:07
7439-98-7
Nickel
17.1 mg/kg
1.0
1
04/07/2210:30
04/11/2216:07
7440-02-0
Potassium
10100 mg/kg
1010
1
04/07/2210:30
04/11/2216:07
7440-09-7
Selenium
5.3 mg/kg
2.0
1
04/07/2210:30
04/11/2216:07
7782-49-2
Sodium
6750 mg/kg
1010
1
04/07/2210:30
04/11/2216:07
7440-23-5
Zinc
247 mg/kg
2.0
1
04/07/2210:30
04/11/2216:07
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010D Preparation Method:
EPA 3010A
Leachate Method/Date: EPA 1311; 04/07/22 14:59
Initial
pH: 8.96; Final
pH: 2
Pace Analytical Services - Asheville
Arsenic
ND mg/L
0.050
1
04/09/22 03:47
04/11/22 11:13
7440-38-2
Barium
1.8 mg/L
0.25
1
04/09/22 03:47
04/11/22 11:13
7440-39-3
Cadmium
ND mg/L
0.0050
1
04/09/22 03:47
04/11/22 11:13
7440-43-9
Chromium
ND mg/L
0.050
1
04/09/22 03:47
04/11/22 11:13
7440-47-3
Lead
ND mg/L
0.025
1
04/09/22 03:47
04/11/22 11:13
7439-92-1
Selenium
ND mg/L
0.10
1
04/09/22 03:47
04/11/22 11:13
7782-49-2
Silver
ND mg/L
0.025
1
04/09/22 03:47
04/11/22 11:13
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470A Preparation
Method: EPA 7470A
Leachate Method/Date: EPA 1311; 04/07/22
14:59
Initial
pH: 8.96; Final
pH: 2
Pace Analytical Services - Asheville
Mercury
ND mg/L
0.00020
1
04/21/2211:08
04/21/2215:18
7439-97-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B
Pace Analytical Services - Asheville
Mercury
ND mg/kg
0.010
1
04/07/2213:36
04/12/2211:43
7439-97-6
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
56.6 %
0.10
1
04/07/22 16:04
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
9.2 Std. Units
0.10
1
04/13/22 09:50
REPORT OF LABORATORY ANALYSIS
N2
H3
This report shall not be reproduced, except in full,
Date: 04/24/2022 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 23

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Baxter Biomass 4/6
Pace Project No.: 92597406
Sample: SP3232022B Lab ID: 92597406002 Collected: 04/06/22 09:30 Received: 04/06/22 11:03 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Plant Available Nitrogen
Plant Available Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
365.1 Phosphorus, Total
Phosphorus
Date: 04/24/2022 06:01 PM
Analytical Method: None
Pace Analytical Services - Asheville
882 mg/kg
1 04/19/2214:57 N2
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod.
Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services - Asheville
ND mg/kg 11.1
1 04/08/22 09:36 04/08/22 14:23 7664-41-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
2940 mg/kg 110
1 04/09/22 05:53 04/12/22 04:29 7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
ND mg/kg 9.1
1 04/06/22 22:42 04/07/22 00:44
ND mg/kg 9.1
1 04/06/22 22:42 04/07/22 00:44 14797-55-8
ND mg/kg 9.1
1 04/06/22 22:42 04/07/22 00:44 14797-65-0
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
2710 mg/kg 53.3
25 04/07/22 20:44 04/08/22 08:57 7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Baxter Biomass 4/6
Pace Project No.: 92597406
QC Batch: 693209 Analysis Method: EPA 7470A
QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury TCLP
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92597406001, 92597406002
METHOD BLANK: 3543708
Matrix:
Water
Associated Lab Samples: 92597406001, 92597406002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Mercury
mg/L
ND
0.00020
04/21/2215:07
LABORATORY CONTROL SAMPLE:
3621209
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Mercury
mg/L
0.0025
0.0028
110 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3621210 3621211
MS MSD
92597406001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/L ND 0.0025 0.0025 0.0027 0.0026 109 104 75-125 4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/24/2022 06:01 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Baxter Biomass 4/6
Pace Project No.: 92597406
QC Batch: 690064 Analysis Method: EPA 7471 B
QC Batch Method: EPA 7471 B Analysis Description: 7471 Mercury
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92597406001, 92597406002
METHOD BLANK: 3605881
Matrix:
Solid
Associated Lab Samples: 92597406001, 92597406002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Mercury
mg/kg
ND
0.0036
04/12/2210:54
LABORATORY CONTROL SAMPLE:
3605882
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Mercury
mg/kg
0.05
0.051
102 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3605883 3605884
MS MSD
92596819001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg ND 0.077 0.077 0.079 0.083 98 103 75-125 5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/24/2022 06:01 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Baxter Biomass 4/6
Pace Project No.: 92597406
QC Batch: 689996
QC Batch Method: EPA 3050B
Associated Lab Samples: 92597406001, 92597406002
METHOD BLANK: 3605409
Associated Lab Samples: 92597406001, 92597406002
Parameter Units
Aluminum
mg/kg
Arsenic
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Copper
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Sodium
mg/kg
Zinc
mg/kg
LABORATORY CONTROL SAMPLE:
3605410
Parameter
Units
Aluminum
mg/kg
Arsenic
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Copper
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Sodium
mg/kg
Zinc
mg/kg
QUALITY CONTROL DATA
Analysis Method: EPA6010D
Analysis Description: 6010 MET
Laboratory: Pace Analytical Services - Asheville
Matrix: Solid
Blank
Result
Spike
Cone.
500
50
50
500
50
50
500
50
50
500
50
500
50
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Reporting
Limit Analyzed
Qualifiers
10.0
04/11/2215:22
2.5
04/11/2215:22
0.10
04/11/2215:22
25.0
04/11/2215:22
5.0
04/11/2215:22
1.0
04/11/2215:22
10.0
04/11/2215:22
5.0
04/11/2215:22
0.50
04/11/2215:22
500
04/11/2215:22
1.0
04/11/2215:22
500
04/11/2215:22
1.0
04/11/2215:22
LCS
Result
511
44.9
46.3
502
48.5
47.2
481
50.2
47.8
507
41.4
499J
46.2
LCS
% Rec
102
90
93
100
97
94
96
100
96
101
83
100
92
% Rec
Limits
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3605411
3605412
MS
MSD
92597456001
Spike
Spike
MS
MSD
MS MSD % Rec
Parameter Units Result
Cone.
Cone.
Result
Result
% Rec % Rec Limits RPD Qual
Aluminum mg/kg 730
719
719
2030
2260
181 213 75-125 11 M1
Arsenic mg/kg ND
71.9
71.9
64.9
66.6
89 92 75-125 2
Results presented on this page are in the units indicated by the
"Units" column except where
an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/24/2022 06:01 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Baxter Biomass 4/6
Pace Project No.: 92597406
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3605411
3605412
MS
MSD
92597456001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
mg/kg
ND
71.9
71.9
65.6
66.6
91
93
75-125
2
Calcium
mg/kg
728
719
719
1460
1380
102
90
75-125
6
Copper
mg/kg
ND
71.9
71.9
70.3
70.9
97
98
75-125
1
Lead
mg/kg
ND
71.9
71.9
67.5
68.0
93
93
75-125
1
Magnesium
mg/kg
457
719
719
1230
1220
107
106
75-125
0
Molybdenum
mg/kg
ND
71.9
71.9
69.4
70.5
96
98
75-125
2
Nickel
mg/kg
ND
71.9
71.9
67.2
68.4
93
95
75-125
2
Potassium
mg/kg
ND
719
719
830
870
102
108
75-125
5
Selenium
mg/kg
ND
71.9
71.9
58.7
59.7
80
82
75-125
2
Sodium
mg/kg
1300
719
719
2190
2110
124
113
75-125
4
Zinc
mg/kg
ND
71.9
71.9
65.8
66.3
91
92
75-125
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/24/2022 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Baxter Biomass 4/6
Pace Project No.: 92597406
QC Batch: 690519 Analysis Method: EPA 601 OD
QC Batch Method: EPA 3010A Analysis Description: 6010 MET TCLP
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92597406001, 92597406002
METHOD BLANK: 3605494
Matrix:
Water
Associated Lab Samples:
92597406001, 92597406002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
mg/L
ND
0.050
04/11/2210:06
Barium
mg/L
ND
0.25
04/11/2210:06
Cadmium
mg/L
ND
0.0050
04/11/2210:06
Chromium
mg/L
ND
0.050
04/11/2210:06
Lead
mg/L
ND
0.025
04/11/2210:06
Selenium
mg/L
ND
0.10
04/11/2210:06
Silver
mg/L
ND
0.025
04/11/2210:06
LABORATORY CONTROL SAMPLE:
3608634
Parameter
Units
Arsenic
mg/L
Barium
mg/L
Cadmium
mg/L
Chromium
mg/L
Lead
mg/L
Selenium
mg/L
Silver
mg/L
Spike
1-CS
LCS
% Rec
Cone.
Result
% Rec
Limits Qualifiers
2.5
2.5
101
80-120
2.5
2.3
94
80-120
2.5
2.4
97
80-120
2.5
2.5
99
80-120
2.5
2.4
96
80-120
2.5
2.6
104
80-120
1.2
1.2
98
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3608635
3608636
MS
MSD
92594869001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/L
ND
2.5
2.5
2.5
2.5
101
100
75-125
1
Barium
mg/L
0.35
2.5
2.5
2.8
2.7
96
94
75-125
2
Cadmium
mg/L
ND
2.5
2.5
2.4
2.4
97
95
75-125
2
Chromium
mg/L
ND
2.5
2.5
2.5
2.4
99
98
75-125
2
Lead
mg/L
ND
2.5
2.5
2.4
2.3
96
94
75-125
2
Selenium
mg/L
ND
2.5
2.5
2.6
2.6
104
103
75-125
1
Silver
mg/L
ND
1.2
1.2
1.2
1.2
99
97
75-125
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/24/2022 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Baxter Biomass 4/6
Pace Project No.: 92597406
QC Batch: 690166 Analysis Method: SW-846
QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92597406001, 92597406002
SAMPLE DUPLICATE: 3606722
92597287001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 15.6 14.8 5 N2
SAMPLE DUPLICATE: 3606723
92597472001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 3.3 3.1 6 N2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/24/2022 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Baxter Biomass 4/6
Pace Project No.: 92597406
QC Batch: 691081 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92597406001, 92597406002
SAMPLE DUPLICATE: 3611234
92597406001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 9.2 9.2 0 H3
SAMPLE DUPLICATE: 3611235
92598352003 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 4.5 4.5 0 H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/24/2022 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Baxter Biomass 4/6
Pace Project No.: 92597406
QC Batch: 690300 Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod. Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92597406001, 92597406002
METHOD BLANK: 3607259
Matrix:
Solid
Associated Lab Samples: 92597406001, 92597406002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Ammonia
mg/kg
ND
8.1
04/08/22 14:09
LABORATORY CONTROL SAMPLE:
3607260
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Nitrogen, Ammonia
mg/kg
325
334
103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3607261 3607262
MS MSD
92596872001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/kg 183 511 412 632 522 88 82 90-110 19 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/24/2022 06:01 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Baxter Biomass 4/6
Pace Project No.: 92597406
QC Batch: 690263 Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92597406001, 92597406002
METHOD BLANK: 3607212
Matrix:
Solid
Associated Lab Samples: 92597406001, 92597406002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg
ND
50.0
04/12/22 04:16
LABORATORY CONTROL SAMPLE:
3607213
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg
1000
960
96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3607214 3607215
MS MSD
92596735002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 43800 3920 3050 46300 48400 62 151 90-110 5 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/24/2022 06:01 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Baxter Biomass 4/6
Pace Project No.: 92597406
QC Batch: 689936 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92597406001, 92597406002
METHOD BLANK: 3605268
Associated Lab Samples: 92597406001, 92597406002
Parameter Units
Nitrogen, Nitrate mg/kg
Nitrogen, Nitrite mg/kg
Nitrogen, NO2 plus NO3 mg/kg
Matrix: Solid
Blank Reporting
Result Limit Analyzed
ND 4.0 04/07/22 00:35
ND 4.0 04/07/22 00:35
ND 4.0 04/07/22 00:35
Qualifiers
LABORATORY CONTROL SAMPLE:
3605269
Spike
LCS LCS % Rec
Parameter
Units
Cone.
Result % Rec Limits Qualifiers
Nitrogen, Nitrate
mg/kg
14.9
14.9 100 90-110
Nitrogen, Nitrite
mg/kg
9.9
9.9 100 90-110
Nitrogen, NO2 plus NO3
mg/kg
24.8
24.8 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3605270
3605271
MS
MSD
92597562001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits RPD Qual
Nitrogen, Nitrate
mg/kg
ND
64.4
64.8
72.9
71.8
113
111
90-110 2
Nitrogen, Nitrite
mg/kg
ND
42.8
43.2
66.2
67.3
134
136
90-110 2 M1
Nitrogen, NO2 plus NO3
mg/kg
ND
107
108
139
139
124
123
90-110 0 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/24/2022 06:01 PM without the written consent of Pace Analytical Services, LLC.
Page 17 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Baxter Biomass 4/6
Pace Project No.: 92597406
QC Batch: 690144 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92597406001, 92597406002
METHOD BLANK: 3606514
Matrix:
Solid
Associated Lab Samples: 92597406001, 92597406002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Phosphorus
mg/kg
ND
0.96
04/08/22 08:37
LABORATORY CONTROL SAMPLE:
3606515
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Phosphorus
mg/kg
42.4
43.2
102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3606516 3606517
MS MSD
92596422001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/kg 11200 159 171 6470 6510 -2990 -2750 90-110 1 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/24/2022 06:01 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 23

Pace Analytical Services, LLC
aceAnalytical 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: Baxter Biomass 4/6
Pace Project No.: 92597406
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/24/2022 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Baxter Biomass 4/6
92597406
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92597406001
SP3232022A
EPA 3050B
689996
EPA 6010D
690050
92597406002
SP3232022B
EPA 3050B
689996
EPA 6010D
690050
92597406001
SP3232022A
EPA 3010A
690519
EPA 6010D
690540
92597406002
SP3232022B
EPA 3010A
690519
EPA 6010D
690540
92597406001
SP3232022A
EPA 7470A
693209
EPA 7470A
693302
92597406002
SP3232022B
EPA 7470A
693209
EPA 7470A
693302
92597406001
SP3232022A
EPA 7471B
690064
EPA 7471B
690295
92597406002
SP3232022B
EPA 7471B
690064
EPA 7471B
690295
92597406001
SP3232022A
SW-846
690166
92597406002
SP3232022B
SW-846
690166
92597406001
SP3232022A
EPA 9045D
691081
92597406002
SP3232022B
EPA 9045D
691081
92597406001
SP3232022A
None
692630
92597406002
SP3232022B
None
692630
92597406001
SP3232022A
EPA 350.1 Rev 2.0
1993
690300
EPA 350.1 Rev 2.0
1993
690353
Mod.
Mod.
92597406002
SP3232022B
EPA 350.1 Rev 2.0
1993
690300
EPA 350.1 Rev 2.0
1993
690353
Mod.
Mod.
92597406001
SP3232022A
EPA 351.2 Rev 2.0
1993
690263
EPA 351.2 Rev 2.0
1993
690873
92597406002
SP3232022B
EPA 351.2 Rev 2.0
1993
690263
EPA 351.2 Rev 2.0
1993
690873
92597406001
SP3232022A
EPA 353.2 Rev 2.0
1993
689936
EPA 353.2 Rev 2.0
1993
689944
92597406002
SP3232022B
EPA 353.2 Rev 2.0
1993
689936
EPA 353.2 Rev 2.0
1993
689944
92597406001
SP3232022A
EPA 365.1 Rev 2.0
1993
690144
EPA 365.1 Rev 2.0
1993
690232
92597406002
SP3232022B
EPA 365.1 Rev 2.0
1993
690144
EPA 365.1 Rev 2.0
1993
690232
Date: 04/24/2022 06:01 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 20 of 23

Document Name: Document Revised: November 15, 2021
Sample Condition Upon Receipt (SOUR) Page 1 of 2
aCPAmlytical Document Na.: Issuing Authority:
F-CAR-05-033-Rev.08 Pace Carolinas Quality Office
LaboratoryeEdenn
ng samples:
Asheville Greenwood ❑ Hunterwille ❑ Raleigh[] Mechanicsville❑ Atlanta[:] Kernersville❑
SampleConclition Client Name: Project WO# • 925974Q6
L U ion Receipt#: I V
IIIIII III Illll II II III
Courier: []Fed Ex UPS ❑LISPS [Client
❑ commercial ❑Pace ❑Other: 92597406
Custody Seal Present? ❑Yes X----s-eais Intact? [-]Yes Na
DateJlnitials Person Examining Contents:_.,,/�
Packing Material: ❑Bubble wrap ❑Bubble Bags one ❑ Other Biological Tissue Fin?
Thermometer: ❑Yes [-]No❑ /A
IRGunID: 43r- I Owe ❑Blue None
Type of Ice:
p Correction Factor:
Cooler Temp: I" k Add/Subtract ('C) 9 Temps ould be above freezing to VC
Samples out of temp criteria. 5amples on ice, cooling process
Cooler Temp Corrected ("C); IIJ A� has begun
USDA Regulated Soil (❑ N/A, water sample)
Did samples origi a in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate From a foreign source (internati lly,
I~lvaa Nn including Hawaii and Puerto Ricol? nYes YTNa
Cum ments/Discrepancy:
Chain of Custody Present?
s
[]No
❑NIA
1.
samples Arrived within Hold Time?
es
[]NO
[]N/A
2.
Short Hold Time Analysis (472 hr.)?
Yes
[]No
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
o
❑NIA
4.
Sufficient Volume?
2<5
❑No
[]N/A
5.
Correct Containers Used?
Pa ce Containers U sed ?
es
j3yes
No
❑N/A
❑N/A
6.
Containers Intact?
16Yes
ONO
❑N%
7.
Dissolved analysis: Samples Field Filtered? []Yes
[-]NO
N/A
3.
Sample Labels Match CDC?
-lncludesDate/Time/ID/Analysis
``Yes
Matrix: V
❑Na
❑N/A
� 9.
Heads pace in VOA Vials (>5-6mm)?
❑Yes
❑No
❑NI
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
❑No
❑Nn
LJ<JA
Zq,A
11.
COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes []NO
Lot 0 of split containers:
CLIENT NOTIFICATION/FESOLIFTION
Person contacted: Date/Time:
Project Manager SCURF Review: Date:
Project Manager SRF Review: _ _ Date: Page 21 of 23

Document Name:
Sample Condition Upon Receipt (SOUR)
ceAnalytical' Document No.:
1: -CAR- CS -0 3 3- R e v.0 8
*Check mark top half of box if pH and/or dechlorination is Project ft
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottles
Document Revised: November 15, 2021
Page 2 of 2
Issuing Authority:
r•: nrr•
5I-974
WO#...92C
PM: CDl Due Date: 04/20/22
CLIENT: 92—Baxter
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Sample 10
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
Amount of Preservative
Lot H
adjusted
added
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNH Certification Office Rv.
Out of hoid, incorrect preservative, out of temp, incorrect containers.
Page 22 of 23

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Page 23 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
August 09, 2022
Mr. Ricky Styles
Baxter Healthcare
2859 Old Linville Road
Marion, NC 28752
RE: Project: Baxter Biomass 7/19
Pace Project No.: 92615930
Dear Mr. Styles:
Enclosed are the analytical results for sample(s) received by the laboratory on July 20, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
��
Lorri Patton
[e-mail]
1(828)254-7176
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Baxter Biomass 7/19
Pace Project No.: 92615930
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water#: LA029
Virginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Baxter Biomass 7/19
Pace Project No.: 92615930
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92615930001 NP7192022A EPA 601OD
RDT
18
PASI-A
EPA 601 OD
DEC
7
PASI-A
EPA7470A
NMP
1
PASI-A
EPA 7471B
NMP
1
PASI-A
SW-846
KDF
1
PASI-C
EPA 9045D
YEG
1
PASI-A
None
MDW
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
KDF1
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
3
PASI-A
EPA 365.1 Rev 2.0 1993
SMT
1
PASI-A
92615930002 NP7192022B EPA 601OD
RDT
18
PASI-A
EPA 601OD
DEC
7
PASI-A
EPA7470A
NMP
1
PASI-A
EPA 7471B
NMP
1
PASI-A
SW-846
KDF
1
PASI-C
EPA 9045D
YEG
1
PASI-A
None
MDW
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
KDF1
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
3
PASI-A
EPA 365.1 Rev 2.0 1993
SMT
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 23

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Baxter Biomass 7/19
Pace Project No.: 92615930
Sample: NP7192022A Lab ID: 92615930001 Collected: 07/19/22 09:30 Received: 07/20/22 12:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
Aluminum
10300 mg/kg
17.1
1
07/29/22 11:46
08/03/22 20:05
7429-90-5
Arsenic
5.1 mg/kg
4.3
1
07/29/22 11:46
08/03/22 20:05
7440-38-2
Barium
1380 mg/kg
1.7
1
07/29/22 11:46
08/03/22 20:05
7440-39-3
Cadmium
4.6 mg/kg
0.17
1
07/29/22 11:46
08/03/22 20:05
7440-43-9
Calcium
133000 mg/kg
427
10
07/29/22 11:46
08/04/2216:18
7440-70-2
Chromium
15.6 mg/kg
0.85
1
07/29/22 11:46
08/03/22 20:05
7440-47-3
Copper
81.0 mg/kg
8.5
1
07/29/22 11:46
08/03/22 20:05
7440-50-8
Iron
7260 mg/kg
85.3
1
07/29/22 11:46
08/03/22 20:05
7439-89-6
Lead
65.9 mg/kg
1.7
1
07/29/22 11:46
08/03/22 20:05
7439-92-1
Magnesium
14300 mg/kg
17.1
1
07/29/22 11:46
08/03/22 20:05
7439-95-4
Manganese
4200 mg/kg
8.5
10
07/29/22 11:46
08/04/2216:18
7439-96-5
Molybdenum
ND mg/kg
8.5
1
07/29/22 11:46
08/03/22 20:05
7439-98-7
Nickel
17.5 mg/kg
0.85
1
07/29/22 11:46
08/03/22 20:05
7440-02-0
Potassium
18900 mg/kg
8530
10
07/29/22 11:46
08/04/2216:18
7440-09-7
Selenium
3.9 mg/kg
1.7
1
07/29/22 11:46
08/03/22 20:05
7782-49-2
Silver
ND mg/kg
0.85
1
07/29/22 11:46
08/03/22 20:05
7440-22-4
Sodium
14300 mg/kg
853
1
07/29/22 11:46
08/03/22 20:05
7440-23-5
Zinc
356 mg/kg
1.7
1
07/29/22 11:46
08/03/22 20:05
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010D Preparation Method:
EPA 3010A
Leachate Method/Date: EPA 1311; 07/21/22
15:05
Initial
pH: 10.07; Final pH: 2
Pace Analytical Services - Asheville
Arsenic
ND mg/L
0.050
1
07/24/2211:02
07/26/2218:35
7440-38-2
Barium
1.2 mg/L
0.25
1
07/24/2211:02
07/25/2219:49
7440-39-3
Cadmium
ND mg/L
0.0050
1
07/24/2211:02
07/25/2219:49
7440-43-9
Chromium
ND mg/L
0.050
1
07/24/2211:02
07/25/2219:49
7440-47-3
Lead
ND mg/L
0.025
1
07/24/2211:02
07/25/2219:49
7439-92-1
Selenium
ND mg/L
0.10
1
07/24/2211:02
07/26/2218:35
7782-49-2
Silver
ND mg/L
0.025
1
07/24/2211:02
07/26/2218:35
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470A Preparation
Method: EPA 7470A
Leachate Method/Date: EPA 1311; 07/21/22
15:05
Initial
pH: 10.07; Final pH: 2
Pace Analytical Services - Asheville
Mercury
ND mg/L
0.00020
1
08/08/2214:35
08/09/2211:25
7439-97-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation
Method: EPA 7471 B
Pace Analytical Services - Asheville
Mercury
ND mg/kg
0.0092
1
08/01/2213:34
08/02/2213:28
7439-97-6
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
51.2 %
0.10
1
07/26/22 16:15
REPORT OF LABORATORY ANALYSIS
N2
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Date: 08/09/2022 04:07 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 23

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Baxter Biomass 7/19
Pace Project No.: 92615930
Sample: NP7192022A
Lab ID: 92615930001 Collected: 07/19/22 09:30 Received: 07/20/22 12:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
10.1 Std. Units 0.10 1 07/29/22 12:09 H3
Plant Available Nitrogen
Analytical Method: None
Pace Analytical Services - Asheville
Plant Available Nitrogen
13600 mg/kg 1 07/29/22 17:24 N2
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services - Asheville
Nitrogen, Ammonia
ND mg/kg 18.3 1 07/25/22 11:25 07/25/22 14:13 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Kjeldahl, Total
45400 mg/kg 4650 50 07/22/22 15:23 07/26/22 05:00 7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, NO2 plus NO3
ND mg/kg 8.1 1 07/21/22 00:34 07/21/22 02:08
Nitrogen, Nitrate
ND mg/kg 8.1 1 07/21/22 00:34 07/21/22 02:08 14797-55-8
Nitrogen, Nitrite
ND mg/kg 8.1 1 07/21/22 00:34 07/21/22 02:08 14797-65-0
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Phosphorus
389 mg/kg 46.5 25 07/26/2217:38 07/27/2217:57 7723-14-0
REPORT OF LABORATORY ANALYSIS
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Date: 08/09/2022 04:07 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Baxter Biomass 7/19
Pace Project No.: 92615930
Sample: NP7192022B Lab ID: 92615930002 Collected: 07/19/22 09:30 Received: 07/20/22 12:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
Aluminum
8570 mg/kg
20.2
1
07/29/22 11:46
08/03/22 20:08
7429-90-5
Arsenic
5.1 mg/kg
5.1
1
07/29/22 11:46
08/03/22 20:08
7440-38-2
Barium
1320 mg/kg
2.0
1
07/29/22 11:46
08/03/22 20:08
7440-39-3
Cadmium
3.9 mg/kg
0.20
1
07/29/22 11:46
08/03/22 20:08
7440-43-9
Calcium
125000 mg/kg
505
10
07/29/22 11:46
08/04/2216:21
7440-70-2
Chromium
14.0 mg/kg
1.0
1
07/29/22 11:46
08/03/22 20:08
7440-47-3
Copper
73.1 mg/kg
10.1
1
07/29/22 11:46
08/03/22 20:08
7440-50-8
Iron
6450 mg/kg
101
1
07/29/22 11:46
08/03/22 20:08
7439-89-6
Lead
46.5 mg/kg
2.0
1
07/29/22 11:46
08/03/22 20:08
7439-92-1
Magnesium
13500 mg/kg
20.2
1
07/29/22 11:46
08/03/22 20:08
7439-95-4
Manganese
3910 mg/kg
10.1
10
07/29/22 11:46
08/04/2216:21
7439-96-5
Molybdenum
ND mg/kg
10.1
1
07/29/22 11:46
08/03/22 20:08
7439-98-7
Nickel
16.1 mg/kg
1.0
1
07/29/22 11:46
08/03/22 20:08
7440-02-0
Potassium
16300 mg/kg
1010
1
07/29/22 11:46
08/03/22 20:08
7440-09-7
Selenium
4.0 mg/kg
2.0
1
07/29/22 11:46
08/03/22 20:08
7782-49-2
Silver
ND mg/kg
1.0
1
07/29/22 11:46
08/03/22 20:08
7440-22-4
Sodium
13600 mg/kg
1010
1
07/29/22 11:46
08/03/22 20:08
7440-23-5
Zinc
332 mg/kg
2.0
1
07/29/22 11:46
08/03/22 20:08
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010D Preparation Method:
EPA 3010A
Leachate Method/Date: EPA 1311; 07/21/22
15:05
Initial
pH: 9.94; Final
pH: 2
Pace Analytical Services - Asheville
Arsenic
ND mg/L
0.050
1
07/24/2211:02
07/26/2218:38
7440-38-2
Barium
1.3 mg/L
0.25
1
07/24/2211:02
07/25/2219:52
7440-39-3
Cadmium
ND mg/L
0.0050
1
07/24/2211:02
07/25/2219:52
7440-43-9
Chromium
ND mg/L
0.050
1
07/24/2211:02
07/25/2219:52
7440-47-3
Lead
ND mg/L
0.025
1
07/24/2211:02
07/25/2219:52
7439-92-1
Selenium
ND mg/L
0.10
1
07/24/2211:02
07/26/2218:38
7782-49-2
Silver
ND mg/L
0.025
1
07/24/2211:02
07/26/2218:38
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470A Preparation
Method: EPA 7470A
Leachate Method/Date: EPA 1311; 07/21/22
15:05
Initial
pH: 9.94; Final
pH: 2
Pace Analytical Services - Asheville
Mercury
ND mg/L
0.00020
1
08/08/2214:35
08/09/2211:28
7439-97-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation
Method: EPA 7471 B
Pace Analytical Services - Asheville
Mercury
ND mg/kg
0.0092
1
08/01/2213:34
08/02/2213:30
7439-97-6
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
53.3 %
0.10
1
07/26/22 16:15
REPORT OF LABORATORY ANALYSIS
N2
This report shall not be reproduced, except in full,
Date: 08/09/2022 04:07 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Baxter Biomass 7/19
Pace Project No.: 92615930
Sample: NP7192022B
Lab ID: 92615930002 Collected: 07/19/22 09:30 Received: 07/20/22 12:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
10 Std. Units 0.10 1 07/29/22 12:11 H3
Plant Available Nitrogen
Analytical Method: None
Pace Analytical Services - Asheville
Plant Available Nitrogen
1050 mg/kg 1 07/29/22 17:24 N2
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services - Asheville
Nitrogen, Ammonia
ND mg/kg 12.9 1 07/25/22 11:25 07/25/22 14:14 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Kjeldahl, Total
3510 mg/kg 93.1 1 07/22/22 15:23 07/26/22 02:57 7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, NO2 plus NO3
ND mg/kg 8.5 1 07/21/22 00:34 07/21/22 02:12
Nitrogen, Nitrate
ND mg/kg 8.5 1 07/21/22 00:34 07/21/22 02:12 14797-55-8
Nitrogen, Nitrite
ND mg/kg 8.5 1 07/21/22 00:34 07/21/22 02:12 14797-65-0
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Phosphorus
2140 mg/kg 50.5 25 07/26/2217:38 07/27/2217:57 7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/09/2022 04:07 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Baxter Biomass 7/19
Pace Project No.: 92615930
QC Batch: 715575 Analysis Method: EPA 7470A
QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury TCLP
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92615930001, 92615930002
METHOD BLANK: 3712720
Matrix:
Water
Associated Lab Samples: 92615930001, 92615930002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Mercury
mg/L
ND
0.00020
08/09/2211:13
LABORATORY CONTROL SAMPLE:
3730484
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Mercury
mg/L
0.0025
0.0025
99 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3730485 3730486
MS MSD
50321272001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/L ND 0.0025 0.0025 0.0026 0.0025 103 98 75-125 5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/09/2022 04:07 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Baxter Biomass 7/19
Pace Project No.: 92615930
QC Batch: 713816 Analysis Method: EPA 7471 B
QC Batch Method: EPA 7471 B Analysis Description: 7471 Mercury
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92615930001, 92615930002
METHOD BLANK: 3721615
Matrix:
Solid
Associated Lab Samples: 92615930001, 92615930002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Mercury
mg/kg
ND
0.0060
08/02/2213:18
LABORATORY CONTROL SAMPLE:
3721616
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Mercury
mg/kg
0.083
0.080
96 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3721617 3721618
MS MSD
92615359001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 1.1 0.32 0.32 0.54 0.69 -166 -119 75-125 24 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/09/2022 04:07 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Baxter Biomass 7/19
Pace Project No.: 92615930
QC Batch: 713717 Analysis Method: EPA6010D
QC Batch Method: EPA 3050B Analysis Description: 6010 MET
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92615930001, 92615930002
METHOD BLANK: 3721148
Associated Lab Samples: 92615930001, 92615930002
Parameter Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed Qualifiers
Aluminum
mg/kg
ND
10.0
08/03/2218:34
Arsenic
mg/kg
ND
2.5
08/03/2218:34
Barium
mg/kg
ND
1.0
08/03/2218:34
Cadmium
mg/kg
ND
0.10
08/03/2218:34
Calcium
mg/kg
ND
25.0
08/03/2218:34
Chromium
mg/kg
ND
0.50
08/03/2218:34
Copper
mg/kg
ND
5.0
08/03/2218:34
Iron
mg/kg
ND
50.0
08/03/2218:34
Lead
mg/kg
ND
1.0
08/03/2218:34
Magnesium
mg/kg
ND
10.0
08/04/2215:50
Manganese
mg/kg
ND
0.50
08/03/2218:34
Molybdenum
mg/kg
ND
5.0
08/03/2218:34
Nickel
mg/kg
ND
0.50
08/03/2218:34
Potassium
mg/kg
ND
500
08/04/2215:50
Selenium
mg/kg
ND
1.0
08/03/2218:34
Silver
mg/kg
ND
0.50
08/03/2218:34
Sodium
mg/kg
ND
500
08/04/2215:50
Zinc
mg/kg
ND
1.0
08/03/2218:34
LABORATORY CONTROL SAMPLE:
Parameter
3721149
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Aluminum
mg/kg
500
503
101
80-120
Arsenic
mg/kg
50
47.6
95
80-120
Barium
mg/kg
50
49.5
99
80-120
Cadmium
mg/kg
50
49.9
100
80-120
Calcium
mg/kg
500
498
100
80-120
Chromium
mg/kg
50
51.0
102
80-120
Copper
mg/kg
50
48.3
97
80-120
Iron
mg/kg
500
511
102
80-120
Lead
mg/kg
50
49.8
100
80-120
Magnesium
mg/kg
500
514
103
80-120
Manganese
mg/kg
50
51.2
102
80-120
Molybdenum
mg/kg
50
53.2
106
80-120
Nickel
mg/kg
50
49.9
100
80-120
Potassium
mg/kg
500
ND
98
80-120
Selenium
mg/kg
50
46.9
94
80-120
Silver
mg/kg
25
23.6
95
80-120
Sodium
mg/kg
500
527
105
80-120
Results presented on this page are in the units indicated
by the "Units" column except
where an alternate unit
is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/09/2022 04:07 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Baxter Biomass 7/19
Pace Project No.: 92615930
LABORATORY CONTROL SAMPLE:
3721149
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
% Rec
Limits
Qualifiers
Zinc
mg/kg
50
49.6
99
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3721150
3721151
MS
MSD
92616081001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Aluminum
mg/kg
7050
530
520
11700
11400
869
840
75-125
2 M1
Arsenic
mg/kg
ND
53
52
47.5
44.0
87
82
75-125
8
Barium
mg/kg
33.6
53
52
78.1
74.2
84
78
75-125
5
Cadmium
mg/kg
ND
53
52
49.9
46.3
94
89
75-125
7
Calcium
mg/kg
43.4
530
520
535
497
93
87
75-125
7
Chromium
mg/kg
10.5
53
52
56.9
53.2
88
82
75-125
7
Copper
mg/kg
ND
53
52
55.4
52.2
99
95
75-125
6
Iron
mg/kg
6520
530
520
5640
5300
-166
-234
75-125
6 M1
Lead
mg/kg
8.9
53
52
56.9
53.9
91
87
75-125
5
Magnesium
mg/kg
155
530
520
673
619
98
89
75-125
8
Manganese
mg/kg
196
53
52
219
205
45
18
75-125
7 M1
Molybdenum
mg/kg
ND
53
52
49.9
46.3
94
89
75-125
7
Nickel
mg/kg
2.3
53
52
53.0
49.4
96
91
75-125
7
Potassium
mg/kg
ND
530
520
704
652
104
96
75-125
8
Selenium
mg/kg
ND
53
52
46.6
43.7
87
83
75-125
6
Silver
mg/kg
ND
26.4
26
24.2
22.4
91
86
75-125
8
Sodium
mg/kg
ND
530
520
511J
475J
95
90
75-125
Zinc
mg/kg
9.0
53
52
61.8
58.5
100
95
75-125
5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/09/2022 04:07 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Baxter Biomass 7/19
Pace Project No.: 92615930
QC Batch: 712520 Analysis Method: EPA 601 OD
QC Batch Method: EPA 3010A Analysis Description: 6010 MET TCLP
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92615930001, 92615930002
METHOD BLANK: 3712720
Matrix:
Water
Associated Lab Samples:
92615930001, 92615930002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
mg/L
ND
0.050
07/25/22 09:38
Barium
mg/L
ND
0.25
07/25/22 09:38
Cadmium
mg/L
ND
0.0050
07/25/22 09:38
Chromium
mg/L
ND
0.050
07/25/22 09:38
Lead
mg/L
ND
0.025
07/25/22 09:38
Selenium
mg/L
ND
0.10
07/25/22 09:38
Silver
mg/L
ND
0.025
07/25/22 09:38
LABORATORY CONTROL SAMPLE:
3715124
Parameter
Units
Arsenic
mg/L
Barium
mg/L
Cadmium
mg/L
Chromium
mg/L
Lead
mg/L
Selenium
mg/L
Silver
mg/L
Spike
1-CS
LCS
% Rec
Cone.
Result
% Rec
Limits Qualifiers
2.5
2.5
99
80-120
2.5
2.3
94
80-120
2.5
2.5
98
80-120
2.5
2.5
98
80-120
2.5
2.4
96
80-120
2.5
2.7
106
80-120
1.2
1.2
96
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3715125
3715126
MS
MSD
92615519001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/L
ND
2.5
2.5
2.4
2.4
98
98
75-125
0
Barium
mg/L
ND
2.5
2.5
2.4
2.3
94
93
75-125
1
Cadmium
mg/L
ND
2.5
2.5
2.4
2.4
97
97
75-125
1
Chromium
mg/L
ND
2.5
2.5
2.4
2.4
97
97
75-125
0
Lead
mg/L
ND
2.5
2.5
2.4
2.4
96
95
75-125
1
Selenium
mg/L
ND
2.5
2.5
2.6
2.6
105
105
75-125
0
Silver
mg/L
ND
1.2
1.2
1.2
1.2
95
95
75-125
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/09/2022 04:07 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 23

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Baxter Biomass 7/19
Pace Project No.: 92615930
QC Batch: 712948 Analysis Method: SW-846
QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92615930001, 92615930002
SAMPLE DUPLICATE: 3717461
92615420001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 13.2 12.8 3 N2
SAMPLE DUPLICATE: 3717462
92616438014 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 19.2 19.3 0 N2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Baxter Biomass 7/19
Pace Project No.: 92615930
QC Batch: 713737 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92615930001, 92615930002
SAMPLE DUPLICATE: 3721203
92615930001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 10.1 10.2 0 H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/09/2022 04:07 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Baxter Biomass 7/19
Pace Project No.: 92615930
QC Batch: 712559
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod
Associated Lab Samples: 92615930001, 92615930002
METHOD BLANK: 3715233
Associated Lab Samples: 92615930001, 92615930002
Parameter Units
Nitrogen, Ammonia mg/kg
LABORATORY CONTROL SAMPLE: 3715234
Parameter Units
Nitrogen, Ammonia mg/kg
QUALITY CONTROL DATA
Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services - Asheville
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 8.9 07/25/2213:47
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
431 440 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3715235 3715236
MS MSD
92615359001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/kg 8800 2330 1990 10300 11700 64 147 90-110 13 M1,R1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3715237 3715238
MS MSD
92615702001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/kg 2290 2760 3490 5180 5970 105 106 90-110 14 R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/09/2022 04:07 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Baxter Biomass 7/19
Pace Project No.: 92615930
QC Batch: 712342 Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92615930001, 92615930002
METHOD BLANK: 3714236
Matrix:
Solid
Associated Lab Samples: 92615930001, 92615930002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg
ND
50.0
07/26/22 02:50
LABORATORY CONTROL SAMPLE:
3714237
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg
1000
925
93 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3714238 3714239
MS MSD
92615702001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 46200 7230 7950 52800 53800 92 96 90-110 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/09/2022 04:07 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Baxter Biomass 7/19
Pace Project No.: 92615930
QC Batch: 711923 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92615930001, 92615930002
METHOD BLANK: 3712342
Associated Lab Samples: 92615930001, 92615930002
Parameter Units
Nitrogen, Nitrate mg/kg
Nitrogen, Nitrite mg/kg
Nitrogen, NO2 plus NO3 mg/kg
Matrix: Solid
Blank Reporting
Result Limit Analyzed
ND 4.0 07/21/22 02:06
ND 4.0 07/21/22 02:06
ND 4.0 07/21/22 02:06
Qualifiers
LABORATORY CONTROL SAMPLE:
3712343
Spike
LCS LCS % Rec
Parameter
Units
Cone.
Result % Rec Limits Qualifiers
Nitrogen, Nitrate
mg/kg
14.9
15.1 101 90-110
Nitrogen, Nitrite
mg/kg
10
10.4 104 90-110
Nitrogen, NO2 plus NO3
mg/kg
24.9
25.5 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3712344
3712345
MS
MSD
92615930001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits RPD Qual
Nitrogen, Nitrate
mg/kg
ND
30.5
30.5
32.7
30.6
107
101
90-110 7
Nitrogen, Nitrite
mg/kg
ND
20.5
20.3
21.8
20.9
102
99
90-110 4
Nitrogen, NO2 plus NO3
mg/kg
ND
51
50.8
54.5
51.5
105
100
90-110 6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/09/2022 04:07 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Baxter Biomass 7/19
Pace Project No.: 92615930
QC Batch: 712755 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92615930001, 92615930002
METHOD BLANK: 3716592
Matrix:
Solid
Associated Lab Samples: 92615930001, 92615930002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Phosphorus
mg/kg
ND
0.93
07/27/2217:47
LABORATORY CONTROL SAMPLE:
3716593
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Phosphorus
mg/kg
49
49.9
102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3716594 3716595
MS MSD
92614156001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/kg 203 76.2 77.8 242 200 51 -4 90-110 19 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/09/2022 04:07 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 23

Pace Analytical Services, LLC
aceAnalytical 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: Baxter Biomass 7/19
Pace Project No.: 92615930
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
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Date: 08/09/2022 04:07 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Baxter Biomass 7/19
92615930
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92615930001
NP7192022A
EPA3050B
713717
EPA 6010D
713837
92615930002
NP7192022B
EPA3050B
713717
EPA 6010D
713837
92615930001
NP7192022A
EPA 3010A
712520
EPA 6010D
712534
92615930002
NP7192022B
EPA 3010A
712520
EPA 6010D
712534
92615930001
NP7192022A
EPA 7470A
715575
EPA 7470A
715903
92615930002
NP7192022B
EPA 7470A
715575
EPA 7470A
715903
92615930001
NP7192022A
EPA 7471B
713816
EPA 7471B
714190
92615930002
NP7192022B
EPA 7471B
713816
EPA 7471B
714190
92615930001
NP7192022A
SW-846
712948
92615930002
NP7192022B
SW-846
712948
92615930001
NP7192022A
EPA 9045D
713737
92615930002
NP7192022B
EPA 9045D
713737
92615930001
NP7192022A
None
713914
92615930002
NP7192022B
None
713914
92615930001
NP7192022A
EPA 350.1 Rev 2.0
1993
712559
EPA 350.1 Rev 2.0
1993
712640
Mod.
Mod.
92615930002
NP7192022B
EPA 350.1 Rev 2.0
1993
712559
EPA 350.1 Rev 2.0
1993
712640
Mod.
Mod.
92615930001
NP7192022A
EPA 351.2 Rev 2.0
1993
712342
EPA 351.2 Rev 2.0
1993
712773
92615930002
NP7192022B
EPA 351.2 Rev 2.0
1993
712342
EPA 351.2 Rev 2.0
1993
712773
92615930001
NP7192022A
EPA 353.2 Rev 2.0
1993
711923
EPA 353.2 Rev 2.0
1993
711925
92615930002
NP7192022B
EPA 353.2 Rev 2.0
1993
711923
EPA 353.2 Rev 2.0
1993
711925
92615930001
NP7192022A
EPA 365.1 Rev 2.0
1993
712755
EPA 365.1 Rev 2.0
1993
713028
92615930002
NP7192022B
EPA 365.1 Rev 2.0
1993
712755
EPA 365.1 Rev 2.0
1993
713028
Date: 08/09/2022 04:07 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 20 of 23

DC#- Title: ENV-FRM-HUNT-0083 v0'!_Sample Condition Upon Receipt
Effective Date: 06/1212022
Laboratory receiving samples:
Asheville % Eden❑ Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑ Atlanta❑ Kernersville❑
Sample Condition Client Name: Project #: W0# : 92615930
Upon Receipt �
�'JC: �C � S, � C'• Mir � > `+ I+
Courier: []Fed Ex ❑LIPS ❑USPS I-I�Client II I III I II IIIII lll� III
❑ Commercial ❑Pace ❑Other: `�J' 92615830 I 1
Custody Seal Present? ❑Yes ❑No Seals Intact? Dyes No I r I�
Dale/Initials Person Examining Contents: S �'� f
Packing Material: ❑Bubble Wrap ❑Bubble Bags [None ❑ Other Biological Tissue Frozen?
Thermometer: n ❑Yes ❑No ❑N/A
❑ /A� I R Gun ID: t Vt / 1
Type of Ice: ❑Wet []Blue ❑None
A lI / Correction Factor-,
Cooler Temp: �Add/Subtract (°C))
Cooler Temp Corrected (°C): A/ 4
USDA Regulated Soil (❑ N/A, water sample)
Did samples originate in a quarantine zone within the United 5tates: CA, NY, or SC
lrh.A, m ..0 nYcc NNn
Temp should be above freezing to VC
❑Samples out of temp criteria. Samples on ice, cooling process
has begun
Did samples originate from a foreign source (internationally,
including Hawaii and Puerto Ricol? MYes r%o
Comments/Discrepancy:
Chain of Custody Present?
Yes
❑ND
❑N/A
1.
Samples Arrived within Hold Time?
Yes
[]No
❑NIA
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes
®No
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
DNo
❑N/A
4.
Sufficient Volume?
(MYes
[:]No
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
Yes
Eyes
[:]No
[:]No
❑N/A
❑N/A
6.
Containers Intact?
Yes
❑No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
❑No
N/A
8.
Sample Labels Match COO
-includes Date/Time/ID/Analysis Matrix:
Oyes
J�
❑No
[I N/A
9.
Headspace in VOA Vials (>5.6mm)?
[]Yes
[]No
ftN/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
[:]No
[]No
ON/A
N/A
11.
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Lot ID of split containers:
Date/Time:
Date:
Date:
Flela data xequfreae VYes UNo
Page 21 of 23
QLlaltrax ID: 69614 Page 1 of 2

DC#_Title: ENV-FRM-HUN1-0084 v01 rTech Spec Sample Condition
Upon Receipt
wtrr"-nw a
Effective Date: 05/12/2022
*Check mark top half of box if pH and/or dechlorination
is verified and within the acceptance range for
preservation samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottles
***Check all unpreserved Nitrates for chlorine
Project # I WO# : 92615930
PM: LJP Due Date: 08/03/22
CLIENT: 92—Baxter
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot k
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le.
out of hold, Incorrect preservative, out of temp, incorrect containers)
Qualtrax Document ID: 70677
Page 2 of 2
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