WQ0002503_Monitoring - 11-2022_20230113 (2)

Monitoring Report Submittal
Permit Number #*
Name of Facility:*
Month: * November
Report Information
WQ0002503
FRIT CAR, INC.
Type *
NDMR, NDAR-1, NDAR-2, NDMLR
GW-59
Confirmation Email Address:*
Name of Submitter: *
Signature:
Date of submittal:
[e-mail]
Connie Pettis
Year:* 2022
Upload Document*
NDAR-NDMR NOVEMBER 8AMB
2022.pdf
PDF Only
2022-11 GW59.pdf 2AMB
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
-0 C15DWMV
1 /13/2023
This will be filled in automatically

Initial Review
Reviewer:
Gerald, Wanda
Is the project number correct?*
WQ0002503
Is the monitoring report accepted?*
Yes No
Regional Office*
Washington
Reviewer: _anonymous
Review Date: 2/6/2023

GW-59A COMPLIANCE. REPORT FORM Permit 9 vX=o 503
(Submit one each monitoring period with GI -S9 forms.)
1
Enter date monitoring results were due. ( 12-31 22 ) Will this monitoring report (GW-59 and GW-59A)
YES
NO
be submitted after the established due date?
X
2
Was any required information missing on the GW-59 report forms?
YES
O
IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc.)? lithe answer is 'Tes", contact the Regional Office for guidance.
y
4
Are any monitored constituents equal to or above the established standards?
S
NO
If the answer to question 4 is "NO'; skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below:
Mw-1, IRON 004S
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
YES
NO
same constituent(s) in the same well(s) in the last two years?
X
If the answer to question 5 is "NO", skip to section 8.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
Are the monitoring wells listed in section 5 located at or. beyond the review boundary?
S
NO
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly
located; contact the Regional Office.
7
Is the permittee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem?
v
/�
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation
fines, and/or penalties.
NO EFFLMENT }IRS REEN APPLIED TO T4E 5PRAlf1 LD SINGE FEB. 20M
8
The person completing this portion (GW-59A) of the monitoring report should sign below and submit this
form with G W-59 forms for required wells to the address provided at the top of the current GW-59 form.
1 hereby ackn Iedge that thta above information was evaluated and the information submitted in this
repo (om »ce Report OW49A) is true and complete to the best of my knowledge.
VA ( /Se
/L�2 q
Signatur4 of Permittee (or Authorized Agent) Date
CNN-59A 12/8/2003

SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
• • •
•
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 2/28/2029
Facility Name: FRIT CAR, INC.
Non -Discharge UIC
Permit Name (if different): SAME AS ABOVE
NPDES WQ0002503 Other
Facility Address: 2012 HIGHWAY 17 NORTH
TYPE OF PERMITTED OPERATION BEING MONITORED
BRIDGETON NC 28519 County CRAVEN
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑■ Spray Field ❑ Remediation:
Contact Person: MICHAEL NEWBY
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: FRIT CAR SPRAYFIELD
No. of wells to be sampled: 4
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-1
Date sample collected: 11/9/2022
FIELD ANALYSES:
WAS
Well Depth: 15.65 ft.
Well Diameter: 2 in.
pH 00400: 5.83 units Temp. 00010: 20.5 °C
DRY at
Depth to Water Level 82546: 8.23 ft. below measuring point Screened Interval: ft. to
ft.
Spec. Cond. 00094: µMhos
time ofsampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: NONE
check
Volume of water pumped/bailed before sampling: 3.56
gallons
Appearance CLEAR
here:❑
Samples for metals were collected unfiltered: ❑■ YES
❑ NO and field acidified: ❑■ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 11/18/2022
Laboratory Name: PACE ANALYTICAL
Certification No. EnV375
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L
Pb - Lead 01051 <2.0 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620 .156
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665 <• 10
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 131 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 0068o 57.3 mg/L
Ca - Calcium 00916
mg/L
Chloride 0094o 2.38 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034 <2.0
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042 <.005
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 <100
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 18.8 mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑■ Yes (1) ❑ No (0)
Specific Conductance 00095 µMhos
K - Potassium 00937
mg/L
VOC 7873 method #
Total Ammonia 00610 <.25 mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen, NH, as N, Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
, method #
TKN as N 00625 mg/L
Ni - Nickel 01067 <2.0
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Michael Newby, Senior Vice President
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.06-07-2018

SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
• • •
•
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 2/28/2029
Facility Name: FRIT CAR, INC.
Non -Discharge UIC
Permit Name (if different): SAME AS ABOVE
NPDES WQ0002503 Other
Facility Address: 2012 HIGHWAY 17 NORTH
TYPE OF PERMITTED OPERATION BEING MONITORED
BRIDGETON NC 28519 County CRAVEN
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑■ Spray Field ❑ Remediation:
Contact Person: MICHAEL NEWBY
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: FRIT CAR SPRAYFIELD
No. of wells to be sampled: 4
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-5
Date sample collected: 11/9/2022
FIELD ANALYSES:
WAS
Well Depth: 15.25 ft.
Well Diameter: 2 in.
pH 00400: 5.01 units Temp. 00010: 19.3 °C
DRY at
Depth to Water Level 82546: 8.05 ft. below measuring point Screened Interval: ft. to
ft.
Spec. Cond. 00094: µMhos
time ofsampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: NONE
check
Volume of water pumped/bailed before sampling: 3•45
gallons
Appearance CLEAR
here:❑
Samples for metals were collected unfiltered: ❑■ YES
❑ NO and field acidified: ❑■ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 11/18/2022
Laboratory Name: PACE ANALYTICAL
Certification No. EnV375
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L
Pb - Lead 01051 3.45 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620 <• 10
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665 <0.1
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 703oo 72 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 0068o 2.75 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 16.3 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034 <2.0
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042 <.005
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 176
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 19.2 mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑■ Yes (1) ❑ No (0)
Specific Conductance 00095 µMhos
K - Potassium 00937
mg/L
VOC 7873 method #
Total Ammonia 00610 <.25 mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen, NH, as N, Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
, method #
TKN as N 00625 mg/L
Ni - Nickel 01067 <2.0
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Michael Newby, Senior Vice President fin,,// �� Iz�2g /22—
Permittee (or Authorized Agent) Name and Title - Please print or type Signatut of Perm ed Agent) (Date)
GW-59 Rev.06-07-2018

SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
• • •
•
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 2/28/2029
Facility Name: FRIT CAR, INC.
Non -Discharge UIC
Permit Name (if different): SAME AS ABOVE
NPDES WQ0002503 Other
Facility Address: 2012 HIGHWAY 17 NORTH
TYPE OF PERMITTED OPERATION BEING MONITORED
BRIDGETON NC 28519 County CRAVEN
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑■ Spray Field ❑ Remediation:
Contact Person: MICHAEL NEWBY
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: FRIT CAR SPRAYFIELD
No. of wells to be sampled: 4
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-6
Date sample collected: 11/9/2022
FIELD ANALYSES:
WAS
Well Depth: 19.68 ft.
Well Diameter: 2 in.
pH 00400: 4.89 units Temp. 00010: 19.2 °C
DRY at
Depth to Water Level 82546: 12.13 ft. below measuring point Screened Interval: ft. to
ft.
Spec. Cond. 00094: µMhos
time ofsampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: NONE
check
Volume of water pumped/bailed before sampling: 3.63
gallons
Appearance CLEAR
here:❑
Samples for metals were collected unfiltered: ❑■ YES
❑ NO and field acidified: ❑■ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 11/18/2022
Laboratory Name: PACE ANALYTICAL
Certification No. EnV375
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L
Pb - Lead 01051 <2.0 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620 <• 10
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665 <• 10
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 703oo 56 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 00680 1.29 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 14.1 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034 <2.0
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042 <.005
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 177
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 10.9 mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑■ Yes (1) ❑ No (0)
Specific Conductance 00095 µMhos
K - Potassium 00937
mg/L
VOC 7873 method #
Total Ammonia 00610 <.25 mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen, NH, as N, Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
, method #
TKN as N 00625 mg/L
Ni - Nickel 01067 <2.0
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Michael Newby, Senior Vice President
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.06-07-2018

SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
• • •
•
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 2/28/2029
Facility Name: FRIT CAR, INC.
Non -Discharge UIC
Permit Name (if different): SAME AS ABOVE
NPDES WQ0002503 Other
Facility Address: 2012 HIGHWAY 17 NORTH
TYPE OF PERMITTED OPERATION BEING MONITORED
BRIDGETON NC 28519 County CRAVEN
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑■ Spray Field ❑ Remediation:
Contact Person: MICHAEL NEWBY
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: FRIT CAR SPRAYFIELD
No. of wells to be sampled: 4
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-7
Date sample collected: 11/9/2022
FIELD ANALYSES:
WAS
Well Depth: 16.18 ft.
Well Diameter: 2 in.
pH 00400: 4.82 units Temp. 00010: 19.5 °C
DRY at
Depth to Water Level 82546: 9.02 ft. below measuring point Screened Interval: ft. to
ft.
Spec. Cond. 00094: µMhos
time ofsampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: NONE
check
Volume of water pumped/bailed before sampling: 3.44
gallons
Appearance CLEAR
here:❑
Samples for metals were collected unfiltered: ❑■ YES
❑ NO and field acidified: ❑■ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 11/18/2022
Laboratory Name: PACE ANALYTICAL
Certification No. EnV375
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L
Pb - Lead 01051 <2.0 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620 .127
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665 <0.1
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 703oo 480 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 00680 12.3 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 131 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034 <2.0
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042 <.005
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 5530
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 162 mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑■ Yes (1) ❑ No (0)
Specific Conductance 00095 µMhos
K - Potassium 00937
mg/L
VOC 7873 method #
Total Ammonia 00610 <.25 mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen, NH, as N, Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
, method #
TKN as N 00625 mg/L
Ni - Nickel 01067 <2.0
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Michael Newby, Senior Vice President IL4j( rZ/29/I-
Permittee (or Authorized Agent) Name and Title - Please print or type Signat re of Permitte r Authorized A nt) (Date)
GW-59 Rev.06-07-2018

(� ace Analytical
11
ANALYTICAL REPORT
November 28, 2022
Frit Car Inc.
Sample Delivery Group: L1556126
Samples Received: 11/10/2022
Project Number: 8522112
Description: Groundwater Monitoring
Report To: Connie Pettis
2012 US Hwy 17N
New Bern, NC 28560
Entire Report Reviewed By: q�"h
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 3522112 L1556126 11/23/22 11:12 1 of 37

TABLE OF CONTENTS
Cp: Cover Page
u
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
Fss]
MW-1 L1556126-01
5
Fn
MW-5 L1556126-02
8
MW-6 L1556126-03
11
Fr
MW-7 L1556126-04
14
Qc: Quality Control Summary
17
Rc
Gravimetric Analysis by Method 2540 C-2011
17
F
Wet Chemistry by Method 350.1
19
Wet Chemistry by Method 365.4
20
[Al
Wet Chemistry by Method 9056A
21
Wet Chemistry by Method 9060A
23
RC
Metals (ICPMS) by Method 6020B
25
Volatile Organic Compounds (GC/MS) by Method 8260D
27
GI: Glossary of Terms
35
al: Accreditations & Locations
36
Sc: Sample Chain of Custody
37
ACCOUNT: PROJECT: SDG:
DATE/TIME:
PAGE:
Frit Car Inc. 3522112 L1556126
11/23/22 11:12
2 of 37

SAMPLE SUMMARY
Collected by
Collected date/time
Received date/time
MW-1 L1556126-01 GW
Brent Heard
11/09/2210:10
11/10/22 09:00
FP
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
F
Gravimetric Analysis by Method 2540 C-2011
WG1960409
1
11/16/2210:44
11/16/2214:05
SGB
Mt. Juliet, TN
Wet Chemistry by Method 350.1
WG1958220
1
11/15/221112
11/15/221112
JAR
Mt. Juliet, TN
Wet Chemistry by Method 365.4
WG1959629
1
11/14/22 07:54
11/14/2219:32
CAT
Mt. Juliet, TN
Wet Chemistry by Method 9056A
WG1957691
1
11/11/22 03:09
11/11/22 03:09
LBR
Mt. Juliet, TN
Wet Chemistry by Method 9060A
WG1964116
10
11/24/22 04:45
11/24/22 04:45
LOH
Mt. Juliet, TN
Fn
Metals (ICPMS) by Method 6020B
WG1959108
1
11/18/22 10:54
11/18/2218:40
JPD
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG1959267
1
11/18/22 09:05
11/18/2215:12
JPD
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1959639
25
11/15/22 07:49
11/15/22 07:49
ACG
Mt. Juliet, TN
Fr
Collected by
Collected date/time
Received date/time
Rc
MW-5 L1556126-02 GW
Brent Heard
11/09/221138
11/10/22 09:00
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
7
G�
date/time
date/time
Gravimetric Analysis by Method 2540 C-2011
WG1960409
1
11/16/2210:44
11/16/2214:05
SGB
Mt. Juliet, TN
,
Wet Chemistry by Method 350.1
WG1958220
1
11/15/221113
11/15/221113
JAR
Mt. Juliet, TN
Wet Chemistry by Method 365.4
WG1959629
1
11/14/22 07:54
11/14/2219:34
CAT
Mt. Juliet, TN
Wet Chemistry by Method 9056A
WG1957691
1
11/11/22 04:36
11/11/22 04:36
LBR
Mt. Juliet, TN
RC
Wet Chemistry by Method 9060A
WG1964116
1
11/24/22 05:01
11/24/22 05:01
LOH
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG1959108
1
11/18/22 10:54
11/18/2218:43
JPD
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG1959267
1
11/18/22 09:05
11/18/2215:15
JPD
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1958902
1
11/13/2216:36
11/13/22 16:36
MGF
Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
MW-6 L1556126-03 GW
Brent Heard
11/09/2213:44
11/10/22 09:00
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
Gravimetric Analysis by Method 2540 C-2011
WG1960409
1
11/16/2210:44
11/16/2214:05
SGB
Mt. Juliet, TN
Wet Chemistry by Method 350.1
WG1958220
1
11/15/221115
11/15/221115
JAR
Mt. Juliet, TN
Wet Chemistry by Method 365.4
WG1959629
1
11/14/22 07:54
11/14/2219:39
CAT
Mt. Juliet, TN
Wet Chemistry by Method 9056A
WG1957691
1
11/11/22 05:01
11/11/22 05:01
LBR
Mt. Juliet, TN
Wet Chemistry by Method 9060A
WG1964117
1
11/23/22 2119
11/23/22 2119
LOH
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG1959108
1
11/18/22 10:54
11/18/2219:04
JPD
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG1959267
1
11/18/22 09:05
11/18/2215:19
JPD
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1958902
1
11/13/2216:58
11/13/22 16:58
MGF
Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
MW-7 L1556126-04 GW
Brent Heard
11/09/2214:50
11/10/22 09:00
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
Gravimetric Analysis by Method 2540 C-2011
WG1960402
1
11/16/2210:16
11/16/2212:25
DTM
Mt. Juliet, TN
Wet Chemistry by Method 350.1
WG1958220
1
11/15/221118
11/15/221118
JAR
Mt. Juliet, TN
Wet Chemistry by Method 365.4
WG1959629
1
11/14/22 07:54
11/14/2219:40
CAT
Mt. Juliet, TN
Wet Chemistry by Method 9056A
WG1957691
1
11/11/22 06:16
11/11/22 06:16
LBR
Mt. Juliet, TN
Wet Chemistry by Method 9060A
WG1964117
1
11/23/22 2142
11/23/22 2142
LOH
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG1959108
1
11/18/22 10:54
11/18/2219:08
JPD
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG1959267
1
11/18/22 09:05
11/18/2215:22
JPD
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1958902
1
11/13/2217:20
11/13/22 17:20
MGF
Mt. Juliet, TN
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Frit Car Inc.
3522112
L1556126
11/23/22 11:12
3 of 37

CASE NARRATIVE
FP
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
0
Fr
Rc
4�z
F,
Heather J Wagner
F
Project Manager
RC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 3522112 L1556126 11/23/22 11:12 4 of 37

MW-1 SAMPLE RESULTS - 01
Collected date/time: 11/09/22 10:10 L1556126
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date / time
Dissolved Solids 131000
10000
1 11/16/202214:05 WG1960409
Wet Chemistry by Method 350.1
Result
Qualifier RDL
Dilution Analysis Batch
Analyte ug/I
ug/I
date / time
Ammonia Nitrogen ND
250
1 11/15/20221112 WG1958220
Wet Chemistry by Method 365.4
Result Qualifier RDL
Analyte ug/I ug/I
Phosphorus, Total ND 100
Wet Chemistry by Method 9056A
Result Qualifier
RDL
Analyte ug/I
ug/I
Chloride 2380
1000
Nitrate as (N) 156
100
Sulfate 18800
5000
Wet Chemistry by Method 9060A
Dilution Analysis Batch
date / time
1 11/14/202219:32 WG1959629
Dilution Analysis
Batch
date / time
1 11/11/2022 03:09
WG1957691
1 11/11/2022 03:09
WG1957691
1 11/11/2022 03:09
WG1957691
Result Qualifier
RDL Dilution
Analysis
Batch
Analyte ug/I
ug/I
date / time
TOC (Total Organic Carbon) 57300 B
10000 10
11/24/2022 04:45
WG1964116
Metals (ICPMS) by Method 6020B
Result Qualifier
RDL Dilution
Analysis
Batch
Analyte ug/I
ug/I
date / time
Chromium ND
2.00 1
11/18/202215:12
WG1959267
Chromium, Dissolved ND
2.00 1
11/18/202218:40
WG1959108
Copper ND
5.00 1
11/18/202215:12
WG1959267
Copper, Dissolved ND
5.00 1
11/18/202218:40
WG1959108
Iron ND
100 1
11/18/202215:12
WG1959267
Iron,Dissolved ND
100 1
11/18/202218:40
WG1959108
Lead ND
2.00 1
11/18/202215:12
WG1959267
Lead,Dissolved ND
2.00 1
11/18/202218:40
WG1959108
Nickel ND
2.00 1
11/18/202215:12
WG1959267
Nickel, Dissolved ND
2.00 1
11/18/202218:40
WG1959108
Volatile Organic Compounds (GC/MS) by Method
8260D
— Fp
— Fc
FS
—
Fn—
—
Rc
�GI
— SAI
Rc
Result
Qualifier RDL
Dilution
Analysis
Batch
Analyte
ug/I
ug/I
date / time
Acetone
ND
1250
25
11/15/2022 0749
WG1959639
Acrolein
ND
1250
25
11/15/2022 0749
WG1959639
Acrylonitrile
ND
250
25
11/15/2022 0749
WG1959639
Benzene
ND
25.0
25
11/15/2022 0749
WG1959639
Bromobenzene
ND
25.0
25
11/15/2022 0749
WG1959639
Bromodichloromethane
ND
25.0
25
11/15/2022 0749
WG1959639
Bromoform
ND
25.0
25
11/15/2022 0749
WG1959639
Bromomethane
ND
125
25
11/15/2022 0749
WG1959639
n-Butylbenzene
ND
25.0
25
11/15/2022 0749
WG1959639
sec-Butylbenzene
ND
25.0
25
11/15/2022 0749
WG1959639
tert-Butyl benzene
ND
25.0
25
11/15/2022 0749
WG1959639
Carbon tetrachloride
ND
25.0
25
11/15/2022 0749
WG1959639
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Frit Car Inc.
3522112
L1556126
11/23/22 11:12 5 of 37

MW-1 SAMPLE RESULTS - 01
Collected date/time: 11/09/22 10:10 L1556126
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier RDL
Dilution
Analysis
Batch
FPAnalyte
ug/I
ug/I
date / time
Chlorobenzene
ND
25.0
25
11/15/2022 0749
WG1959639
F
Chlorodibromomethane
ND
25.0
25
11/15/2022 0749
WG1959639
Chloroethane
ND
125
25
11/15/2022 0749
WG1959639
Chloroform
ND
125
25
11/15/2022 0749
WG1959639
SS
F
Chloromethane
ND
62.5
25
11/15/2022 0749
WG1959639
2-Chlorotoluene
ND
25.0
25
11/15/2022 07:49
WG1959639
Fn
4-Chlorotoluene
ND
25.0
25
11/15/2022 0749
WG1959639
1,2-Dibromo-3-Chloropropane
ND
125
25
11/15/2022 0749
WG1959639
1,2-Dibromoethane
ND
25.0
25
11/15/2022 07:49
WG1959639
Dibromomethane
ND
25.0
25
11/15/2022 0749
WG1959639
1,2-Dichlorobenzene
ND
25.0
25
11/15/2022 0749
WG1959639
6
QC
1,3-Dichlorobenzene
ND
25.0
25
11/15/2022 07:49
WG1959639
1,4-Dichlorobenzene
ND
25.0
25
11/15/2022 0749
WG1959639
Dichlorodifuoromethane
ND
125
25
11/15/2022 07:49
WG1959639
,
1,1-Dichloroethane
ND
25.0
25
11/15/2022 0749
WG1959639
1,2-Dichloroethane
ND
25.0
25
11/15/2022 0749
WG1959639
F
1,1-Dichloroethene
ND
25.0
25
11/15/2022 0749
WG1959639
cis-1,2-Dichloroethene
ND
25.0
25
11/15/2022 0749
WG1959639
trans-1,2-Dichloroethene
ND
25.0
25
11/15/2022 07:49
WG1959639
F
1,2-Dichloropropane
ND
25.0
25
11/15/2022 0749
WG1959639
1,1-Dichloropropene
ND
25.0
25
11/15/2022 0749
WG1959639
1,3-Dichloropropane
ND
25.0
25
11/15/2022 0749
WG1959639
cis-1,3-Dichloropropene
ND
25.0
25
11/15/2022 0749
WG1959639
trans-1,3-Dichloropropene
ND
25.0
25
11/15/2022 0749
WG1959639
2,2-Dichloropropane
ND
25.0
25
11/15/2022 0749
WG1959639
Di -isopropyl ether
ND
25.0
25
11/15/2022 0749
WG1959639
Ethylbenzene
ND
25.0
25
11/15/2022 0749
WG1959639
Hexachloro-1,3-butadiene
ND
25.0
25
11/15/2022 0749
WG1959639
Isopropylbenzene
ND
25.0
25
11/15/2022 0749
WG1959639
p-Isopropyltoluene
ND
25.0
25
11/15/2022 0749
WG1959639
2-Butanone (MEK)
ND
250
25
11/15/2022 0749
WG1959639
Methylene Chloride
ND
125
25
11/15/2022 0749
WG1959639
4-Methyl-2-pentanone (MIBK)
ND
250
25
11/15/2022 0749
WG1959639
Methyl tert-butyl ether
ND
25.0
25
11/15/2022 0749
WG1959639
Naphthalene
ND
125
25
11/15/2022 0749
WG1959639
n-Propylbenzene
ND
25.0
25
11/15/2022 0749
WG1959639
Styrene
ND
25.0
25
11/15/2022 0749
WG1959639
1,1,1,2-Tetrachloroethane
ND
25.0
25
11/15/2022 0749
WG1959639
1,1,2,2-Tetrachloroethane
ND
25.0
25
11/15/2022 0749
WG1959639
1,1,2-Trichlorotrifluoroethane
ND
25.0
25
11/15/2022 0749
WG1959639
Tetrachloroethene
ND
25.0
25
11/15/2022 0749
WG1959639
Toluene
ND
25.0
25
11/15/2022 0749
WG1959639
1,2,3-Trichlorobenzene
ND
25.0
25
11/15/2022 0749
WG1959639
1,2,4-Trichlorobenzene
ND
25.0
25
11/15/2022 0749
WG1959639
1,1,1-Trichloroethane
ND
25.0
25
11/15/2022 0749
WG1959639
1,1,2-Trichloroethane
ND
25.0
25
11/15/2022 0749
WG1959639
Trichloroethene
ND
25.0
25
11/15/2022 0749
WG1959639
Trichlorofluoromethane
ND
125
25
11/15/2022 0749
WG1959639
1,2,3-Trichloropropane
ND
62.5
25
11/15/2022 0749
WG1959639
1,2,4-Trimethylbenzene
ND
25.0
25
11/15/2022 0749
WG1959639
1,2,3-Trimethylbenzene
ND
25.0
25
11/15/2022 0749
WG1959639
1,3,5-Trimethylbenzene
ND
25.0
25
11/15/2022 0749
WG1959639
Vinyl chloride
ND
25.0
25
11/15/2022 0749
WG1959639
Xylenes, Total
ND
75.0
25
11/15/2022 0749
WG1959639
(S Toluene-dH
101
80.0-120
1111512022 07.49
WG1959639
(S 4-Bromofluorobenzene
96.8
77.0-126
1111512022 07.49
WG1959639
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Frit Car Inc.
3522112
L1556126
11/23/22 11:12
6 of 37

MW-1 SAMPLE RESULTS - 01
Collected date/time: 11/09/22 10:10 L1556126
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier RDL Dilution Analysis
Analyte ug/I ug/I date / time
(S) 1,2-Dichloroethone-d4 100 70.0-130 11115120220749
Sample Narrative:
L1556126-01 WG1959639: Dilution due to foam.
Batch
WG1959639
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 3522112 L1556126 11/23/22 11:12 7 of 37

MW-5 SAMPLE RESULTS - 02
Collected date/time: 11/09/22 11:38 L1556126
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date / time
Dissolved Solids 72000
10000
1 11/16/202214:05 WG1960409
Wet Chemistry by Method 350.1
Result
Qualifier RDL
Dilution Analysis Batch
Analyte ug/I
ug/I
date / time
Ammonia Nitrogen ND
250
1 11/15/20221113 WG1958220
Wet Chemistry by Method 365.4
Result Qualifier RDL
Analyte ug/I ug/I
Phosphorus, Total ND 100
Wet Chemistry by Method 9056A
Result Qualifier
RDL
Analyte ug/I
ug/I
Chloride 16300
1000
Nitrate as (N) ND
100
Sulfate 19200
5000
Wet Chemistry by Method 9060A
Dilution Analysis Batch
date / time
1 11/14/202219:34 WG1959629
Dilution Analysis
Batch
date / time
1 11/11/2022 04:36
WG1957691
1 11/11/2022 04:36
WG1957691
1 11/11/2022 04:36
WG1957691
Result Qualifier
RDL Dilution
Analysis
Batch
Analyte ug/I
ug/I
date / time
TOC (Total Organic Carbon) 2750 B
1000 1
11/24/2022 05:01
WG1964116
Metals (ICPMS) by Method 6020B
Result Qualifier
RDL Dilution
Analysis
Batch
Analyte ug/I
ug/I
date / time
Chromium ND
2.00 1
11/18/202215:15
WG1959267
Chromium, Dissolved ND
2.00 1
11/18/202218:43
WG1959108
Copper ND
5.00 1
11/18/202215:15
WG1959267
Copper, Dissolved ND
5.00 1
11/18/202218:43
WG1959108
Iron 176
100 1
11/18/202215:15
WG1959267
Iron,Dissolved ND
100 1
11/18/202218:43
WG1959108
Lead ND
2.00 1
11/18/202215:15
WG1959267
Lead,Dissolved ND
2.00 1
11/18/202218:43
WG1959108
Nickel ND
2.00 1
11/18/202215:15
WG1959267
Nickel, Dissolved ND
2.00 1
11/18/202218:43
WG1959108
Volatile Organic Compounds (GC/MS) by Method
8260D
— Fp
— Fc
FS
—
Fn—
—
Rc
�GI
— SAI
Rc
Result
Qualifier RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
date / time
Acetone
ND
50.0
1 11/13/202216:36
WG1958902
Acrolein
ND
J4 50.0
1 11/13/202216:36
WG1958902
Acrylonitrile
ND
10.0
1 11/13/202216:36
WG1958902
Benzene
ND
1.00
1 11/13/202216:36
WG1958902
Bromobenzene
ND
1.00
1 11/13/202216:36
WG1958902
Bromodichloromethane
ND
1.00
1 11/13/202216:36
WG1958902
Bromoform
ND
1.00
1 11/13/202216:36
WG1958902
Bromomethane
ND
5.00
1 11/13/202216:36
WG1958902
n-Butylbenzene
ND
1.00
1 11/13/202216:36
WG1958902
sec-Butylbenzene
ND
1.00
1 11/13/202216:36
WG1958902
tert-Butyl benzene
ND
1.00
1 11/13/202216:36
WG1958902
Carbon tetrachloride
ND
1.00
1 11/13/202216:36
WG1958902
ACCOUNT:
PROJECT: SDG:
DATE/TIME: PAGE:
Frit Car Inc.
3522112 L1556126
11/23/22 11:12 3 of 37

MW-5 SAMPLE
Collected date/time: 11/09/22 11:38
Volatile Organic Compounds (GC/MS) by Method 8260D
RESULTS - 02
L1556126
Result
Qualifier RDL Dilution Analysis
Batch
FPAnalyte
ug/I
ug/I
date / time
Chlorobenzene
ND
1.00 1
11/13/202216:36
WG1958902
F
Chlorodibromomethane
ND
1.00 1
11/13/202216:36
WG1958902
Chloroethane
ND
5.00 1
11/13/202216:36
WG1958902
Chloroform
ND
5.00 1
11/13/202216:36
WG1958902
Fss]
Chloromethane
ND
2.50 1
11/13/202216:36
WG1958902
2-Chlorotoluene
ND
1.00 1
11/13/202216:36
WG1958902
Fn
4-Chlorotoluene
ND
1.00 1
11/13/202216:36
WG1958902
1,2-Dibromo-3-Chloropropane
ND
5.00 1
11/13/202216:36
WG1958902
1,2-Dibromoethane
ND
1.00 1
11/13/202216:36
WG1958902
Dibromomethane
ND
1.00 1
11/13/202216:36
WG1958902
1,2-Dichlorobenzene
ND
1.00 1
11/13/202216:36
WG1958902
6
QC
1,3-Dichlorobenzene
ND
1.00 1
11/13/202216:36
WG1958902
1,4-Dichlorobenzene
ND
1.00 1
11/13/202216:36
WG1958902
Dichlorodifuoromethane
ND
5.00 1
11/13/202216:36
WG1958902
F
1,1-Dichloroethane
ND
1.00 1
11/13/202216:36
WG1958902
1,2-Dichloroethane
ND
1.00 1
11/13/202216:36
WG1958902
F
1,1-Dichloroethene
ND
1.00 1
11/13/202216:36
WG1958902
cis-1,2-Dichloroethene
ND
1.00 1
11/13/202216:36
WG1958902
trans-1,2-Dichloroethene
ND
1.00 1
11/13/202216:36
WG1958902
Rc
1,2-Dichloropropane
ND
1.00 1
11/13/202216:36
WG1958902
1,1-Dichloropropene
ND
1.00 1
11/13/202216:36
WG1958902
1,3-Dichloropropane
ND
1.00 1
11/13/202216:36
WG1958902
cis-1,3-Dichloropropene
ND
1.00 1
11/13/202216:36
WG1958902
trans-1,3-Dichloropropene
ND
1.00 1
11/13/202216:36
WG1958902
2,2-Dichloropropane
ND
1.00 1
11/13/202216:36
WG1958902
Di -isopropyl ether
ND
1.00 1
11/13/202216:36
WG1958902
Ethylbenzene
ND
1.00 1
11/13/202216:36
WG1958902
Hexachloro-1,3-butadiene
ND
1.00 1
11/13/202216:36
WG1958902
Isopropylbenzene
ND
1.00 1
11/13/202216:36
WG1958902
p-Isopropyltoluene
ND
1.00 1
11/13/202216:36
WG1958902
2-Butanone (MEK)
ND
10.0 1
11/13/202216:36
WG1958902
Methylene Chloride
ND
5.00 1
11/13/202216:36
WG1958902
4-Methyl-2-pentanone (MIBK)
ND
10.0 1
11/13/202216:36
WG1958902
Methyl tert-butyl ether
ND
1.00 1
11/13/202216:36
WG1958902
Naphthalene
ND
5.00 1
11/13/202216:36
WG1958902
n-Propylbenzene
ND
1.00 1
11/13/202216:36
WG1958902
Styrene
ND
1.00 1
11/13/202216:36
WG1958902
1,1,1,2-Tetrachloroethane
ND
1.00 1
11/13/202216:36
WG1958902
1,1,2,2-Tetrachloroethane
ND
1.00 1
11/13/202216:36
WG1958902
1,1,2-Trichlorotrifluoroethane
ND
1.00 1
11/13/202216:36
WG1958902
Tetrachloroethene
ND
1.00 1
11/13/202216:36
WG1958902
Toluene
ND
1.00 1
11/13/202216:36
WG1958902
1,2,3-Trichlorobenzene
ND
1.00 1
11/13/202216:36
WG1958902
1,2,4-Trichlorobenzene
ND
1.00 1
11/13/202216:36
WG1958902
1,1,1-Trichloroethane
ND
1.00 1
11/13/202216:36
WG1958902
1,1,2-Trichloroethane
ND
1.00 1
11/13/202216:36
WG1958902
Trichloroethene
ND
1.00 1
11/13/202216:36
WG1958902
Trichlorofluoromethane
ND
5.00 1
11/13/202216:36
WG1958902
1,2,3-Trichloropropane
ND
2.50 1
11/13/202216:36
WG1958902
1,2,4-Trimethylbenzene
ND
1.00 1
11/13/202216:36
WG1958902
1,2,3-Trimethylbenzene
ND
1.00 1
11/13/202216:36
WG1958902
1,3,5-Trimethylbenzene
ND
1.00 1
11/13/202216:36
WG1958902
Vinyl chloride
ND
1.00 1
11/13/202216:36
WG1958902
Xylenes, Total
ND
3.00 1
11/13/202216:36
WG1958902
(S Toluene-dH
100
80.0-120
111131202216.36
WG1958902
(S 4-Bromofluorobenzene
101
77.0-126
111131202216.36
WG1958902
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Frit Car Inc.
3522112
L1556126
11/23/22 11:12
9 of 37

MW-5 SAMPLE RESULTS - 02
Collected date/time: 11/09/22 11:38 L1556126
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier RDL Dilution Analysis
Analyte ug/I ug/I date / time
(S) 1,2-Dichloroethone-d4 108 70.0-130 111131202216.36
Batch
WG1958902
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 3522112 L1556126 11/23/22 11:12 10 of 37

MW-6 SAMPLE RESULTS - 03
Collected date/time: 11/09/22 13:44 L1556126
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date / time
Dissolved Solids 56000
10000
1 11/16/202214:05 WG1960409
Wet Chemistry by Method 350.1
Result
Qualifier RDL
Dilution Analysis Batch
Analyte ug/I
ug/I
date / time
Ammonia Nitrogen ND
250
1 11/15/20221115 WG1958220
Wet Chemistry by Method 365.4
Result Qualifier RDL
Analyte ug/I ug/I
Phosphorus, Total ND 100
Wet Chemistry by Method 9056A
Result Qualifier
RDL
Analyte ug/I _
ug/I
Chloride 14100
1000
Nitrate as (N) ND
100
Sulfate 10900
5000
Wet Chemistry by Method 9060A
Dilution Analysis Batch
date / time
1 11/14/202219:39 WG1959629
Dilution Analysis
Batch
date / time
1 11/11/2022 05:01
WG1957691
1 11/11/2022 05:01
WG1957691
1 11/11/2022 05:01
WG1957691
Result Qualifier
RDL Dilution
Analysis
Batch
Analyte ug/I
ug/I
date / time
TOC (Total Organic Carbon) 1290 B
1000 1
11/23/2022 21:19
WG1964117
Metals (ICPMS) by Method 6020B
Result Qualifier
RDL Dilution
Analysis
Batch
Analyte ug/I
ug/I
date / time
Chromium ND
2.00 1
11/18/202215:19
WG1959267
Chromium, Dissolved ND
2.00 1
11/18/202219:04
WG1959108
Copper ND
5.00 1
11/18/202215:19
WG1959267
Copper, Dissolved ND
5.00 1
11/18/202219:04
WG1959108
Iron 177
100 1
11/18/202215:19
WG1959267
Iron,Dissolved 119
100 1
11/18/202219:04
WG1959108
Lead ND
2.00 1
11/18/202215:19
WG1959267
Lead,Dissolved ND
2.00 1
11/18/202219:04
WG1959108
Nickel ND
2.00 1
11/18/202215:19
WG1959267
Nickel, Dissolved ND
2.00 1
11/18/202219:04
WG1959108
Volatile Organic Compounds (GC/MS) by Method
8260D
— Fp
— Fc
FS
—
Fn—
—
Rc
�GI
— SAI
Rc
Result
Qualifier RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
date / time
Acetone
ND
50.0
1 11/13/202216:58
WG1958902
Acrolein
ND
J4 50.0
1 11/13/202216:58
WG1958902
Acrylonitrile
ND
10.0
1 11/13/202216:58
WG1958902
Benzene
ND
1.00
1 11/13/202216:58
WG1958902
Bromobenzene
ND
1.00
1 11/13/202216:58
WG1958902
Bromodichloromethane
ND
1.00
1 11/13/202216:58
WG1958902
Bromoform
ND
1.00
1 11/13/202216:58
WG1958902
Bromomethane
ND
5.00
1 11/13/202216:58
WG1958902
n-Butylbenzene
ND
1.00
1 11/13/202216:58
WG1958902
sec-Butylbenzene
ND
1.00
1 11/13/202216:58
WG1958902
tert-Butyl benzene
ND
1.00
1 11/13/202216:58
WG1958902
Carbon tetrachloride
ND
1.00
1 11/13/202216:58
WG1958902
ACCOUNT:
PROJECT: SDG:
DATE/TIME: PAGE:
Frit Car Inc.
3522112 L1556126
11/23/22 11:12 11 of 37

MW-6 SAMPLE
Collected date/time: 11/09/22 13:44
Volatile Organic Compounds (GC/MS) by Method 8260D
RESULTS - 03
L1556126
Result
Qualifier RDL Dilution Analysis
Batch
FPAnalyte
ug/I
ug/I
date / time
Chlorobenzene
ND
1.00 1
11/13/202216:58
WG1958902
F
Chlorodibromomethane
ND
1.00 1
11/13/202216:58
WG1958902
Chloroethane
ND
5.00 1
11/13/202216:58
WG1958902
Chloroform
ND
5.00 1
11/13/202216:58
WG1958902
Fss]
Chloromethane
ND
2.50 1
11/13/202216:58
WG1958902
2-Chlorotoluene
ND
1.00 1
11/13/202216:58
WG1958902
Fn
4-Chlorotoluene
ND
1.00 1
11/13/202216:58
WG1958902
1,2-Dibromo-3-Chloropropane
ND
5.00 1
11/13/202216:58
WG1958902
1,2-Dibromoethane
ND
1.00 1
11/13/202216:58
WG1958902
Dibromomethane
ND
1.00 1
11/13/202216:58
WG1958902
1,2-Dichlorobenzene
ND
1.00 1
11/13/202216:58
WG1958902
6
QC
1,3-Dichlorobenzene
ND
1.00 1
11/13/202216:58
WG1958902
1,4-Dichlorobenzene
ND
1.00 1
11/13/202216:58
WG1958902
Dichlorodifuoromethane
ND
5.00 1
11/13/202216:58
WG1958902
F
1,1-Dichloroethane
ND
1.00 1
11/13/202216:58
WG1958902
1,2-Dichloroethane
ND
1.00 1
11/13/202216:58
WG1958902
F
1,1-Dichloroethene
ND
1.00 1
11/13/202216:58
WG1958902
cis-1,2-Dichloroethene
ND
1.00 1
11/13/202216:58
WG1958902
trans-1,2-Dichloroethene
ND
1.00 1
11/13/202216:58
WG1958902
Rc
1,2-Dichloropropane
ND
1.00 1
11/13/202216:58
WG1958902
1,1-Dichloropropene
ND
1.00 1
11/13/202216:58
WG1958902
1,3-Dichloropropane
ND
1.00 1
11/13/202216:58
WG1958902
cis-1,3-Dichloropropene
ND
1.00 1
11/13/202216:58
WG1958902
trans-1,3-Dichloropropene
ND
1.00 1
11/13/202216:58
WG1958902
2,2-Dichloropropane
ND
1.00 1
11/13/202216:58
WG1958902
Di -isopropyl ether
ND
1.00 1
11/13/202216:58
WG1958902
Ethylbenzene
ND
1.00 1
11/13/202216:58
WG1958902
Hexachloro-1,3-butadiene
ND
1.00 1
11/13/202216:58
WG1958902
Isopropylbenzene
ND
1.00 1
11/13/202216:58
WG1958902
p-Isopropyltoluene
ND
1.00 1
11/13/202216:58
WG1958902
2-Butanone (MEK)
ND
10.0 1
11/13/202216:58
WG1958902
Methylene Chloride
ND
5.00 1
11/13/202216:58
WG1958902
4-Methyl-2-pentanone (MIBK)
ND
10.0 1
11/13/202216:58
WG1958902
Methyl tert-butyl ether
ND
1.00 1
11/13/202216:58
WG1958902
Naphthalene
ND
5.00 1
11/13/202216:58
WG1958902
n-Propylbenzene
ND
1.00 1
11/13/202216:58
WG1958902
Styrene
ND
1.00 1
11/13/202216:58
WG1958902
1,1,1,2-Tetrachloroethane
ND
1.00 1
11/13/202216:58
WG1958902
1,1,2,2-Tetrachloroethane
ND
1.00 1
11/13/202216:58
WG1958902
1,1,2-Trichlorotrifluoroethane
ND
1.00 1
11/13/202216:58
WG1958902
Tetrachloroethene
ND
1.00 1
11/13/202216:58
WG1958902
Toluene
ND
1.00 1
11/13/202216:58
WG1958902
1,2,3-Trichlorobenzene
ND
1.00 1
11/13/202216:58
WG1958902
1,2,4-Trichlorobenzene
ND
1.00 1
11/13/202216:58
WG1958902
1,1,1-Trichloroethane
ND
1.00 1
11/13/202216:58
WG1958902
1,1,2-Trichloroethane
ND
1.00 1
11/13/202216:58
WG1958902
Trichloroethene
ND
1.00 1
11/13/202216:58
WG1958902
Trichlorofluoromethane
ND
5.00 1
11/13/202216:58
WG1958902
1,2,3-Trichloropropane
ND
2.50 1
11/13/202216:58
WG1958902
1,2,4-Trimethylbenzene
ND
1.00 1
11/13/202216:58
WG1958902
1,2,3-Trimethylbenzene
ND
1.00 1
11/13/202216:58
WG1958902
1,3,5-Trimethylbenzene
ND
1.00 1
11/13/202216:58
WG1958902
Vinyl chloride
ND
1.00 1
11/13/202216:58
WG1958902
Xylenes, Total
ND
3.00 1
11/13/202216:58
WG1958902
(S Toluene-dH
102
80.0-120
111131202216.58
WG1958902
(S 4-Bromofluorobenzene
98.9
77.0-126
111131202216.58
WG1958902
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Frit Car Inc.
3522112
L1556126
11/23/22 11:12
12 of 37

MW-6 SAMPLE RESULTS - 03
Collected date/time: 11/09/22 13:44 L1556126
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier RDL Dilution Analysis
Analyte ug/I ug/I date / time
(S) 1,2-Dichloroethone-d4 109 70.0-130 111131202216.58
Batch
WG1958902
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 3522112 L1556126 11/23/22 11:12 13 of 37

MW-7 SAMPLE RESULTS - 04
Collected date/time: 11/09/22 14:50 L1556126
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date / time
Dissolved Solids 480000
10000
1 11/16/202212:25 WG1960402
Wet Chemistry by Method 350.1
Result
Qualifier RDL
Dilution Analysis Batch
Analyte ug/I
ug/I
date / time
Ammonia Nitrogen ND
250
1 11/15/20221118 WG1958220
Wet Chemistry by Method 365.4
Result Qualifier RDL
Analyte ug/I ug/I
Phosphorus, Total ND 100
Wet Chemistry by Method 9056A
Result Qualifier
RDL
Analyte ug/I
ug/I
Chloride 131000
1000
Nitrate as (N) 127
100
Sulfate 162000
5000
Wet Chemistry by Method 9060A
Dilution Analysis Batch
date / time
1 11/14/202219:40 WG1959629
Dilution Analysis
Batch
date / time
1 11/11/2022 06:16
WG1957691
1 11/11/2022 06:16
WG1957691
1 11/11/2022 06:16
WG1957691
Result Qualifier
RDL Dilution
Analysis
Batch
Analyte ug/I
ug/I
date / time
TOC (Total Organic Carbon) 12300
1000 1
11/23/2022 2142
WG1964117
Metals (ICPMS) by Method 6020B
Result Qualifier
RDL Dilution
Analysis
Batch
Analyte ug/I
ug/I
date / time
Chromium ND
2.00 1
11/18/202215:22
WG1959267
Chromium, Dissolved ND
2.00 1
11/18/202219:08
WG1959108
Copper ND
5.00 1
11/18/202215:22
WG1959267
Copper, Dissolved ND
5.00 1
11/18/202219:08
WG1959108
Iron 5530
100 1
11/18/202215:22
WG1959267
Iron,Dissolved 711
100 1
11/18/202219:08
WG1959108
Lead ND
2.00 1
11/18/202215:22
WG1959267
Lead,Dissolved ND
2.00 1
11/18/202219:08
WG1959108
Nickel ND
2.00 1
11/18/202215:22
WG1959267
Nickel, Dissolved ND
2.00 1
11/18/202219:08
WG1959108
Volatile Organic Compounds (GC/MS) by Method
8260D
— Fp
— Fc
FS
—
Fn—
—
Rc
�GI
— SAI
Rc
Result
Qualifier RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
date / time
Acetone
ND
50.0
1 11/13/202217:20
WG1958902
Acrolein
ND
J4 50.0
1 11/13/202217:20
WG1958902
Acrylonitrile
ND
10.0
1 11/13/202217:20
WG1958902
Benzene
ND
1.00
1 11/13/202217:20
WG1958902
Bromobenzene
ND
1.00
1 11/13/202217:20
WG1958902
Bromodichloromethane
ND
1.00
1 11/13/202217:20
WG1958902
Bromoform
ND
1.00
1 11/13/202217:20
WG1958902
Bromomethane
ND
5.00
1 11/13/202217:20
WG1958902
n-Butylbenzene
ND
1.00
1 11/13/202217:20
WG1958902
sec-Butylbenzene
ND
1.00
1 11/13/202217:20
WG1958902
tert-Butyl benzene
ND
1.00
1 11/13/202217:20
WG1958902
Carbon tetrachloride
ND
1.00
1 11/13/202217:20
WG1958902
ACCOUNT:
PROJECT: SDG:
DATE/TIME: PAGE:
Frit Car Inc.
3522112 L1556126
11/23/22 11:12 14 of 37

MW-7 SAMPLE
Collected date/time: 11/09/22 14:50
Volatile Organic Compounds (GC/MS) by Method 8260D
RESULTS - 04
L1556126
Result
Qualifier RDL Dilution Analysis
Batch
FPAnalyte
ug/I
ug/I
date / time
Chlorobenzene
ND
1.00 1
11/13/202217:20
WG1958902
F
Chlorodibromomethane
ND
1.00 1
11/13/202217:20
WG1958902
Chloroethane
ND
5.00 1
11/13/202217:20
WG1958902
Chloroform
ND
5.00 1
11/13/202217:20
WG1958902
Fss]
Chloromethane
ND
2.50 1
11/13/202217:20
WG1958902
2-Chlorotoluene
ND
1.00 1
11/13/202217:20
WG1958902
Fn
4-Chlorotoluene
ND
1.00 1
11/13/202217:20
WG1958902
1,2-Dibromo-3-Chloropropane
ND
5.00 1
11/13/202217:20
WG1958902
1,2-Dibromoethane
ND
1.00 1
11/13/202217:20
WG1958902
Dibromomethane
ND
1.00 1
11/13/202217:20
WG1958902
1,2-Dichlorobenzene
ND
1.00 1
11/13/202217:20
WG1958902
6
QC
1,3-Dichlorobenzene
ND
1.00 1
11/13/202217:20
WG1958902
1,4-Dichlorobenzene
ND
1.00 1
11/13/202217:20
WG1958902
Dichlorodifuoromethane
ND
5.00 1
11/13/202217:20
WG1958902
F
1,1-Dichloroethane
ND
1.00 1
11/13/202217:20
WG1958902
1,2-Dichloroethane
ND
1.00 1
11/13/202217:20
WG1958902
F
1,1-Dichloroethene
ND
1.00 1
11/13/202217:20
WG1958902
cis-1,2-Dichloroethene
ND
1.00 1
11/13/202217:20
WG1958902
trans-1,2-Dichloroethene
ND
1.00 1
11/13/202217:20
WG1958902
Rc
1,2-Dichloropropane
ND
1.00 1
11/13/202217:20
WG1958902
1,1-Dichloropropene
ND
1.00 1
11/13/202217:20
WG1958902
1,3-Dichloropropane
ND
1.00 1
11/13/202217:20
WG1958902
cis-1,3-Dichloropropene
ND
1.00 1
11/13/202217:20
WG1958902
trans-1,3-Dichloropropene
ND
1.00 1
11/13/202217:20
WG1958902
2,2-Dichloropropane
ND
1.00 1
11/13/202217:20
WG1958902
Di -isopropyl ether
ND
1.00 1
11/13/202217:20
WG1958902
Ethylbenzene
ND
1.00 1
11/13/202217:20
WG1958902
Hexachloro-1,3-butadiene
ND
1.00 1
11/13/202217:20
WG1958902
Isopropylbenzene
ND
1.00 1
11/13/202217:20
WG1958902
p-Isopropyltoluene
ND
1.00 1
11/13/202217:20
WG1958902
2-Butanone (MEK)
ND
10.0 1
11/13/202217:20
WG1958902
Methylene Chloride
ND
5.00 1
11/13/202217:20
WG1958902
4-Methyl-2-pentanone (MIBK)
ND
10.0 1
11/13/202217:20
WG1958902
Methyl tert-butyl ether
ND
1.00 1
11/13/202217:20
WG1958902
Naphthalene
ND
5.00 1
11/13/202217:20
WG1958902
n-Propylbenzene
ND
1.00 1
11/13/202217:20
WG1958902
Styrene
ND
1.00 1
11/13/202217:20
WG1958902
1,1,1,2-Tetrachloroethane
ND
1.00 1
11/13/202217:20
WG1958902
1,1,2,2-Tetrachloroethane
ND
1.00 1
11/13/202217:20
WG1958902
1,1,2-Trichlorotrifluoroethane
ND
1.00 1
11/13/202217:20
WG1958902
Tetrachloroethene
ND
1.00 1
11/13/202217:20
WG1958902
Toluene
ND
1.00 1
11/13/202217:20
WG1958902
1,2,3-Trichlorobenzene
ND
1.00 1
11/13/202217:20
WG1958902
1,2,4-Trichlorobenzene
ND
1.00 1
11/13/202217:20
WG1958902
1,1,1-Trichloroethane
ND
1.00 1
11/13/202217:20
WG1958902
1,1,2-Trichloroethane
ND
1.00 1
11/13/202217:20
WG1958902
Trichloroethene
ND
1.00 1
11/13/202217:20
WG1958902
Trichlorofluoromethane
ND
5.00 1
11/13/202217:20
WG1958902
1,2,3-Trichloropropane
ND
2.50 1
11/13/202217:20
WG1958902
1,2,4-Trimethylbenzene
ND
1.00 1
11/13/202217:20
WG1958902
1,2,3-Trimethylbenzene
ND
1.00 1
11/13/202217:20
WG1958902
1,3,5-Trimethylbenzene
ND
1.00 1
11/13/202217:20
WG1958902
Vinyl chloride
ND
1.00 1
11/13/202217:20
WG1958902
Xylenes, Total
ND
3.00 1
11/13/202217:20
WG1958902
(S Toluene-dH
102
80.0-120
111131202217.20
WG1958902
(S 4-Bromofluorobenzene
98.8
77.0-126
111131202217.20
WG1958902
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Frit Car Inc.
3522112
L1556126
11/23/22 11:12
15 of 37

MW-7 SAMPLE RESULTS - 04
Collected date/time: 11/09/22 14:50 L1556126
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier RDL Dilution Analysis
Analyte ug/I ug/I date / time
(S) 1,2-Dichloroethone-d4 106 70.0-130 111131202217.20
Batch
WG1958902
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 3522112 L1556126 11/23/22 11:12 16 of 37

WG1960402
Gravimetric Analysis by Method 2540 C-2011
Method Blank (MB)
(MB) R3363236-1 11/16/22 12:25
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/I ug/I ug/I
Dissolved Solids U 10000 10000
L1555591-09 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1556126-04
(OS) L1555591-09 11/16/22 12:25 • (DUP) R3363236-3 11/16/22 12:25
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
Dissolved Solids 26000 28000 1 7.41 P1 5
L1556017-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1556017-01 11/16/22 12:25 • (DUP) R3363236-4 11/16/22 12:25
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
Dissolved Solids 1090000 1140000 1 4.47 5
Laboratory Control Sample (LCS)
(LCS) R3363236-2 11/16/22 12:25
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I
Dissolved Solids 8800000 8540000 97.0 77.3-123
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG1960409
Gravimetric Analysis by Method 2540 C-2011
Method Blank (MB)
(MB) R3363629-1 11/16/22 14:05
MB Result
Analyte ug/I
Dissolved Solids U
MB Qualifier MB MDL MB RDL
ug/I ug/I
10000 10000
L1556859-02 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
11556126-01,02,03
(OS) L1556359-02 11/16/22 14:05 • (DUP) R3363629-3 11/16/22 14:05
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I %_
Dissolved Solids 593000 602000 1 1.51 5
L1556859-03 Original Sample (OS) • Duplicate (DUP)
(OS) L1556359-03 11/16/22 14:05 • (DUP) R3363629-4 11/16/22 14:05
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
Dissolved Solids 242000 247000 1 2.04 5
Laboratory Control Sample (LCS)
(LCS) R3363629-2 11/16/22 14:05
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I
Dissolved Solids 8800000 9080000 103 77.3-123
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 3522112 L1556126 11/23/22 11:12 13 of 37

WG1958220 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 350.1 11556126-01,02,03,04
Method Blank (MB)
(MB) R3361090-1 11/15/22 10:45
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/I ug/I ug/I
Ammonia Nitrogen U 117 250
L1556091-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1556091-01 11/15/22 10:58 • (DUP) R3361090-5 11/15/22 1104
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I %_
Ammonia Nitrogen ND ND 1 0.000 10
L1556126-04 Original Sample (OS) • Duplicate (DUP)
(OS) L1556126-04 11/15/22 1118 • (DUP) R3361090-7 11/15/22 1124
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
Ammonia Nitrogen ND ND 1 3.86 10
Laboratory Control Sample (LCS)
(LCS) R3861090-2 11/15/22 10:46
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I
Ammonia Nitrogen 7500 7640 102 90.0-110
L1556079-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1556079-02 11/15/22 10:54 • (MS) R3361090-3 11/15/22 10:55 • (MSD) R3361090-4 11/15/22 10:57
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/I ug/I ug/I ug/I
Ammonia Nitrogen 5000 ND 5020 5020 100 100 1 90.0-110 0.120 10
L1556126-03 Original Sample (OS) • Matrix Spike (MS)
(OS) L1556126-03 11/15/22 1115 • (MS) R3361090-6 11/15/22 1116
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte ug/I ug/I ug/I
Ammonia Nitrogen 5000 ND 5110 102 1 90.0-110
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG1959629
Wet Chemistry by Method 365.4
Method Blank (MB)
(MB) R3360376-1 11/14/22 19:07
MB Result
Analyte ug/I
Phosphorus, Total U
MB Qualifier MB MDL MB RDL
ug/I ug/I
35.0 100
L1555749-03 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1556126-01,02,03,04
(OS) L1555749-03 11/14/22 1917 • (DUP) R3360376-9 11/14/22 19:18
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
Phosphorus, Total 4370 4000 1 8.84 20
Laboratory Control Sample (LCS)
(LCS) R3860876-2 11/14/22 19:08
Spike Amount LCS Result
Analyte ug/I ug/I
Phosphorus, Total 3780 3870
LCS Rec. Rec. Limits LCS Qualifier
102 83.2-116
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 3522112 L1556126 11/23/22 11:12 20 of 37

WG1957691 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9056A 11556126-01,02,03,04
Method Blank (MB)
(MB) R3360376-1 11/11/22 00:39
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/I ug/I ug/I
Chloride U 379 1000
Nitrate U 48.0 100
Sulfate U 594 5000
L1556135-05 Original Sample (OS) • Duplicate (DUP)
(OS) L1556135-05 11/11/22 07:06 • (DUP) R3360376-5 11/11/22 07:18
Original Result DUP Result Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
Chloride 20300 20400 1 0.237
15
Nitrate ND ND 1 0.000
15
Sulfate 1770000 1780000 1 0.415
E 15
L1556126-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1556126-01 11/11/22 03:09 • (DUP) R3360376-3 11/11/22 03:22
Original Result
DUP Result
Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
Analyte
ug/I
ug/I
Chloride
2380
2300
1 3.63
15
Nitrate
156
160
1 3.04
15
Sulfate
18800
18800
1 0.169
15
Laboratory Control Sample (LCS)
(LCS) R3860376-2 11/11/22 00:52
Spike Amount
LCS Result
Analyte ug/I
ug/I
Chloride 40000
42100
Nitrate 8000
8300
Sulfate 40000
42600
LCS Rec.
105
104
107
Rec. Limits LCS Qualifier
80.0-120
80.0-120
80.0-120
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 3522112 L1556126 11/23/22 11:12 21 of 37

WG1957691 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9056A 11556126-01,02,03,04
L1556135-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1556135-05 11/11/22 07:06 • (MS) R3360376-6 11/11/22 07:31 • (MSD) R3360376-7 11/11/22 03 03
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte
ug/I
ug/I
ug/I
ug/I
Chloride
50000
20300
71500
71500
102
102
1 80.0-120
0.00854
15
Nitrate
5000
ND
5050
5940
101
119
1 80.0-120
J3 16.2
15
Sulfate
50000
1770000
1780000
1790000
2.91
37.9
1 80.0-120
E V E V 0.980
15
L1556126-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1556126-01 11/11/22 03:09 • (MS) R3360376-4 11/11/22 03:34
Spike Amount
Original Result
MS Result
MS Rec.
Dilution Rec. Limits MS Qualifier
Analyte
ug/I
ug/I
ug/I
Chloride
50000
2380
54900
105
1 80.0-120
Nitrate
5000
156
5390
105
1 80.0-120
Sulfate
50000
18800
70800
104
1 80.0-120
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG1964116
Wet Chemistry by Method 9060A
Method Blank (MB)
(MB) R3364757-2 11/23/22 2019
MB Result
Analyte ug/I
TOC (Total Organic Carbon) 665
MB Qualifier MB MDL MB RDL
ug/I ug/I
J 102 1000
L1555559-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
11556126-01,02
(OS) L1555559-01 11/23/22 20:36 • (DUP) R3364757-3 11/23/22 20:49
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I %_
TOC (Total Organic Carbon) 2420 2230 1 8.05 20
L1555720-05 Original Sample (OS) • Duplicate (DUP)
(OS) L1555720-05 11/23/22 21:45 • (DUP) R3364757-4 11/23/22 22:01
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
TOC (Total Organic Carbon) 1610 1400 1 14.0 20
Laboratory Control Sample (LCS)
(LCS) R3364757-1 11/23/22 20:03
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I
TOC (Total Organic Carbon) 75000 77000 103 85.0-115
L1555720-09 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1555720-09 11/23/22 23:43 • (MS) R3364757-5 11/24/22 00:10 • (MSD) R3364757-6 11/24/22 00:27
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec.
Analyte ug/I
ug/I
ug/I
ug/I
TOC (Total Organic Carbon) 50000
1590
63400
63400 124 124
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
1 80.0-120 J5 J5 0.0158 20
L1555720-10 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1555720-10 11/24/22 00:47 • (MS) R3364757-7 11/24/22 01:10 • (MSD) R3364757-8 11/24/22 0130
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/I
ug/I
ug/I
ug/I
TOC (Total Organic Carbon) 50000
1610
63000
63900 123 125
1 80.0-120
J5 J5 1.42 20
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Frit Car Inc.
3522112
L1556126
11/23/22 11:12 23 of 37

WG1964117
Wet Chemistry by Method 9060A
Method Blank (MB)
(MB) R3864780-2 11/23/22 2059
MB Result
Analyte ug/I
TOC (Total Organic Carbon) 276
MB Qualifier MB MDL MB RDL
ug/I ug/I
J 102 1000
L1556135-04 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
11556126-03,04
(OS) L1556135-04 11/24/22 01:01 • (DUP) R3364730-7 11/24/22 0118
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
TOC (Total Organic Carbon) 1010 ND 1 6.24 20
L1556135-05 Original Sample (OS) • Duplicate (DUP)
(OS) L1556135-05 11/24/22 01:36 • (DUP) R3364730-8 11/24/22 0153
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
TOC (Total Organic Carbon) 1110 1260 1 12.5 20
Laboratory Control Sample (LCS)
(LCS) R3864780-1 11/23/22 20:43
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I
TOC (Total Organic Carbon) 75000 74600 99.4 85.0-115
L1556135-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1556135-01 11/23/22 2158 • (MS) R3864780-3 11/23/22 22:21 • (MSD) R3864780-4 11/23/22 22:43
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution
Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte ug/I ug/I ug/I ug/I
TOC (Total Organic Carbon) 50000 ND 59100 59200 117 117 1
80.0-120
0.0169
20
L1556135-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1556135-02 11/23/22 23:01 • (MS) R3864780-5 11/23/22 23:24 • (MSD) R3864780-6 11/23/22 23:46
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution
Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte ug/I ug/I ug/I ug/I
TOC (Total Organic Carbon) 50000 2600 61700 62200 118 119 1
80.0-120
0.920
20
ACCOUNT: PROJECT:
SDG:
DATE/TIME:
PAGE:
Frit Car Inc. 8522112 L1556126
11/28/22 11:12
24 of 37

WG1959108
Metals (ICPMS) by Method 6020B
Method Blank (MB)
(MB) R3362940-2 11/13/22 17:33
MB Result
Analyte
ug/I
Chromium, Dissolved
U
Copper, Dissolved
U
Iron,Dissolved
U
Lead,Dissolved
U
Nickel, Dissolved
U
MB Qualifier MB MDL
ug/I
1.24
1.51
28.1
0.849
0.816
Laboratory Control Sample (LCS)
(LCS) R3362940-3 11/13/22 17:37
Spike Amount LCS Result
Analyte ug/I ug/I
Chromium, Dissolved
50.0
50.0
Copper, Dissolved
50.0
50.6
Iron,Dissolved
5000
5230
Lead,Dissolved
50.0
48.8
Nickel, Dissolved
50.0
49.3
LCS Rec.
100
101
105
97.6
98.7
QUALITY CONTROL SUMMARY
L1556126-01,02,03,04
MB RDL
ug/I
2.00
5.00
100
2.00
2.00
Rec. Limits
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
LCS Qualifier
L1554937-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1554937-03 11/13/22 17:40 • (MS) R3362940-5 11/13/22 17:47 • (MSD) R3362940-6 11/13/22 17:50
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
ug/I
ug/I
ug/I
ug/I
Chromium, Dissolved
50.0
ND
49.8
52.9
99.7
106
1 75.0-125
Copper, Dissolved
50.0
9.39
53.9
53.7
89.1
88.6
1 75.0-125
Iron,Dissolved
5000
ND
5000
5340
100
107
1 75.0-125
Lead,Dissolved
50.0
ND
48.6
49.6
97.3
99.2
1 75.0-125
Nickel, Dissolved
50.0
14.8
62.9
64.6
96.3
99.6
1 75.0-125
MS Qualifier MSD Qualifier RPD
5.89
0.414
6.54
1.97
2.56
RPD Limits
20
20
20
20
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG1959267
Metals (ICPMS) by Method 6020B
Method Blank (MB)
(MB) R3362314-1 11/13/22 14:22
MB Result
Analyte
ug/I
Chromium
U
Copper
U
Iron
U
Lead
U
Nickel
U
MB Qualifier MB MDL
MB RDL
ug/I
ug/I
1.24
2.00
1.51
5.00
28.1
100
0.849
2.00
0.816
2.00
Laboratory Control Sample (LCS)
(LCS) R3862814-2 11/18/22 14:26
Spike Amount
LCS Result
Analyte ug/I
ug/I
Chromium 50.0
48.7
Copper 50.0
48.4
Iron 5000
4880
Lead 50.0
46.8
Nickel 50.0
48.1
QUALITY CONTROL SUMMARY
L1556126-01,02,03,04
LCS Rec. Rec. Limits LCS Qualifier
97.4
80.0-120
96.8
80.0-120
97.7
80.0-120
93.6
80.0-120
96.2
80.0-120
L1556122-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1556122-01 11/13/22 14:29 • (MS) R3362314-4 11/13/22 14:36 • (MSD) R3362314-5 11/13/22 14:39
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
ug/I
ug/I
ug/I
ug/I
Chromium
50.0
ND
49.7
51.0
99.4
102
1 75.0-125
Copper
50.0
ND
51.4
53.2
103
106
1 75.0-125
Iron
5000
269
5190
5380
98.4
102
1 75.0-125
Lead
50.0
ND
48.0
47.6
96.1
95.2
1 75.0-125
Nickel
50.0
ND
48.5
49.5
97.0
99.0
1 75.0-125
MS Qualifier MSD Qualifier RPD RPD Limits
2.54 20
3.43 20
3.72 20
0.922 20
1.98 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 3522112 L1556126 11/23/22 11:12 26 of 37

WG1958902
Volatile Organic Compounds (GC/MS) by Method 8260D
Method Blank (MB)
(MB) R3362343-2 11/13/22 09:36
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
ug/I
ug/I
ug/I
Acetone
U
11.3
50.0
Acrolein
U
2.54
50.0
Acrylonitrile
U
0.671
10.0
Benzene
U
0.0941
1.00
Bromobenzene
U
0.118
1.00
Bromodichloromethane
U
0.136
1.00
Bromoform
U
0.129
1.00
Bromomethane
U
0.605
5.00
n-Butylbenzene
U
0.157
1.00
sec-Butylbenzene
U
0.125
1.00
tert-Butyl benzene
U
0.127
1.00
Carbon tetrachloride
U
0.128
1.00
Chlorobenzene
U
0.116
1.00
Chlorodibromamethane
U
0.140
1.00
Chloroethane
U
0.192
5.00
Chloroform
U
0.111
5.00
Chloromethane
U
0.960
2.50
2-Chlorotoluene
U
0.106
1.00
4-Chlorotoluene
U
0.114
1.00
1,2-Dibromo-3-Chloropropane
U
0.276
5.00
1,2-Dibromoethane
U
0.126
1.00
Dibromomethane
U
0.122
1.00
1,2-Dichlorobenzene
U
0.107
1.00
1,3-Dichlorobenzene
U
0.110
1.00
1,4-Dichlorobenzene
U
0.120
1.00
Dichlorodifuoromethane
U
0.374
5.00
1,1-Dichloroethane
U
0.100
1.00
1,2-Dichloroethane
U
0.0819
1.00
1,1-Dichloroethene
U
0.188
1.00
cis-1,2-Dichloroethene
U
0.126
1.00
trans-1,2-Dichloroethene
U
0.149
1.00
1,2-Dichloropropane
U
0.149
1.00
1,1-Dichloropropene
U
0.142
1.00
1,3-Dichloropropane
U
0.110
1.00
cis-1,3-Dichloropropene
U
0.111
1.00
trans-1,3-Dichloropropene
U
0.118
1.00
2,2-Dichloropropane
U
0.161
1.00
Di -isopropyl ether
U
0.105
1.00
Ethylbenzene
U
0.137
1.00
Hexachloro-1,3-butadiene
U
0.337
1.00
QUALITY CONTROL SUMMARY
-1556126-02,03,04
ACCOUNT:
Frit Car Inc.
PROJECT: SDG: DATE/TIME: PAGE:
3522112 L1556126 11/23/22 11:12 27 of 37

WG1958902
QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS)
by Method 8260D
11556126-02,03,04
Method Blank (MB)
C p
(MB) R3362343-2 11/13/22 09:36
MB Result
MB Qualifier MB MDL
MB RDL
Analyte ug/I
ug/I
ug/I
ITC]
Isopropylbenzene U
0.105
1.00
p-Isopropyltoluene U
0.120
1.00
FSS
2-Butanone (MEK) U
1.19
10.0
Methylene Chloride U
0.430
5.00
4-Methyl-2-pentanone (MIBK) U
0.478
10.0
[Cn]
Methyl tert-butyl ether U
0.101
1.00
Naphthalene U
1.00
5.00
5
Sr
n-Propylbenzene U
0.0993
1.00
Styrene U
0.118
1.00
1,1,1,2-Tetrachloroethane U
0.147
1.00
�
1,1,2,2-Tetrachloroethane U
0.133
1.00
1,1,2-Trichlorotrifluoroethane U
0.180
1.00
7GI
Tetrachloroethene U
0.300
1.00
Toluene U
0.278
1.00
1,2,3-Trichlorobenzene U
0.230
1.00
FAI
1,2,4-Trichlorobenzene U
0.481
1.00
1,1,1-Trichloroethane U
0.149
1.00
FS
1,1,2-Trichloroethane U
0.158
1.00
Trichloroethene U
0.190
1.00
Trichlorofluoromethane U
0.160
5.00
1,2,3-Trichloropropane U
0.237
2.50
1,2,4-Trimethylbenzene U
0.322
1.00
1,2,3-Trimethylbenzene U
0.104
1.00
1,3,5-Trimethylbenzene U
0.104
1.00
Vinyl chloride U
0.234
1.00
Xylenes, Total U
0.174
3.00
(S) Toluene-dH 105
80.0-120
(S) 4-Bromofluorobenzene 98.8
77.0-126
(S) 1,2-Dichloroethone-d4 109
70.0-130
Laboratory Control Sample (LCS)
(LCS) R3862848-1 11/13/22 08:52
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
ug/I
ug/I
Acetone
25.0
25.8
103
19.0-160
Acrolein
25.0
58.3
233
10.0-160 J4
Acrylonitrile
25.0
28.6
114
55.0-149
Benzene
5.00
5.15
103
70.0-123
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc.
3522112 L1556126 11/23/22 11:12 23 of 37

WG1958902 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D 11556126-02,03,04
Laboratory Control Sample (LCS)
C p
(LCS) R3362343-1 11/13/22 03 52
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte ug/I
ug/I
%
%
ITC]
Bromobenzene 5.00
4.43
88.6
73.0-121
Bromodichloromethane 5.00
5.59
112
75.0-120
FS
Bromoform 5.00
5.40
108
68.0-132
Bromomethane 5.00
5.28
106
10.0-160
n-Butylbenzene 5.00
4.26
85.2
73.0-125
[Cn]
sec-Butylbenzene 5.00
4.49
89.8
75.0-125
tert-Butyl benzene 5.00
4.56
91.2
76.0-124
5
Sr
Carbon tetrachloride 5.00
5.44
109
68.0-126
Chlorobenzene 5.00
5.47
109
80.0-121
Chlorodibromamethane 5.00
5.68
114
77.0-125
Chloroethane 5.00
6.18
124
47.0-150
Chloroform 5.00
5.48
110
73.0-120
7GI
Chloromethane 5.00
6.44
129
41.0-142
2-Chlorotoluene 5.00
4.79
95.8
76.0-123
4-Chlorotoluene 5.00
4.53
90.6
75.0-122
FAI
1,2-Dibromo-3-Chloropropane 5.00
5.49
110
58.0-134
1,2-Dibromoethane 5.00
5.30
106
80.0-122
FS
Dibromomethane 5.00
5.89
118
80.0-120
1,2-Dichlorobenzene 5.00
5.33
107
79.0-121
1,3-Dichlorobenzene 5.00
5.24
105
79.0-120
1,4-Dichlorobenzene 5.00
5.13
103
79.0-120
Dichlorodifuoromethane 5.00
4.64
92.8
51.0-149
1,1-Dichloroethane 5.00
5.55
111
70.0-126
1,2-Dichloroethane 5.00
5.32
106
70.0-128
1,1-Dichloroethene 5.00
5.90
118
71.0-124
cis-1,2-Dichloroethene 5.00
5.43
109
73.0-120
trans-1,2-Dichloroethene 5.00
5.36
107
73.0-120
1,2-Dichloropropane 5.00
5.40
108
77.0-125
1,1-Dichloropropene 5.00
5.05
101
74.0-126
1,3-Dichloropropane 5.00
5.24
105
80.0-120
cis-1,3-Dichloropropene 5.00
5.19
104
80.0-123
trans-1,3-Dichloropropene 5.00
4.57
91.4
78.0-124
2,2-Dichloropropane 5.00
4.63
92.6
58.0-130
Di -isopropyl ether 5.00
5.09
102
58.0-138
Ethylbenzene 5.00
4.94
98.8
79.0-123
Hexachloro-1,3-butadiene 5.00
5.24
105
54.0-138
Isopropylbenzene 5.00
5.30
106
76.0-127
p-Isopropyltoluene 5.00
4.23
84.6
76.0-125
2-Butanone (MEK) 25.0
25.2
101
44.0-160
Methylene Chloride 5.00
5.66
113
67.0-120
ACCOUNT:
PROJECT: SDG: DATE/TIME:
PAGE:
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29 of 37

WG1958902 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D 11556126-02,03,04
Laboratory Control Sample (LCS)
(LCS) R3862848-1 11/13/22 08:52
Spike Amount
LCS Result
LCS Rec.
Rec. Limits
Analyte
ug/I
ug/I
4-Methyl-2-pentanone (MIBK)
25.0
26.4
106
68.0-142
Methyl tert-butyl ether
5.00
5.36
107
68.0-125
Naphthalene
5.00
4.98
99.6
54.0-135
n-Propylbenzene
5.00
4.39
87.8
77.0-124
Styrene
5.00
5.04
101
73.0-130
1,1,1,2-Tetrachloroethane
5.00
5.65
113
75.0-125
1,1,2,2-Tetrachloroethane
5.00
4.70
94.0
65.0-130
1,1,2-Trichlorotrifluoroethane
5.00
5.57
ill
69.0-132
Tetrachloroethene
5.00
5.48
110
72.0-132
Toluene
5.00
4.92
98.4
79.0-120
1,2,3-Trichlorobenzene
5.00
5.38
108
50.0-138
1,2,4-Trichlorobenzene
5.00
4.92
98.4
57.0-137
1,1,1-Trichloroethane
5.00
5.46
109
73.0-124
1,1,2-Trichloroethane
5.00
5.26
105
80.0-120
Trichloroethene
5.00
5.99
120
78.0-124
Trichlorofluoromethane
5.00
5.72
114
59.0-147
1,2,3-Trichloropropane
5.00
5.24
105
73.0-130
1,2,4-Trimethylbenzene
5.00
4.53
90.6
76.0-121
1,2,3-Trimethylbenzene
5.00
4.94
98.8
77.0-120
1,3,5-Trimethylbenzene
5.00
4.35
87.0
76.0-122
Vinyl chloride
5.00
6.53
131
67.0-131
Xylenes, Total
15.0
15.1
101
79.0-123
(S) Toluene-dH
100
80.0-120
(S) 4-Bromofluorobenzene
102
77.0-126
(S) 1,2-Dichloroethone-d4
101
70.0-130
LCS Qualifier
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG1959639
Volatile Organic Compounds (GC/MS) by Method 8260D
Method Blank (MB)
(MB) R3362910-2 11/15/22 0144
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
ug/I
ug/I
ug/I
Acetone
U
11.3
50.0
Acrolein
U
2.54
50.0
Acrylonitrile
U
0.671
10.0
Benzene
U
0.0941
1.00
Bromobenzene
U
0.118
1.00
Bromodichloromethane
U
0.136
1.00
Bromoform
U
0.129
1.00
Bromomethane
U
0.605
5.00
n-Butylbenzene
U
0.157
1.00
sec-Butylbenzene
U
0.125
1.00
tert-Butyl benzene
U
0.127
1.00
Carbon tetrachloride
U
0.128
1.00
Chlorobenzene
U
0.116
1.00
Chlorodibromamethane
U
0.140
1.00
Chloroethane
U
0.192
5.00
Chloroform
U
0.111
5.00
Chloromethane
U
0.960
2.50
2-Chlorotoluene
U
0.106
1.00
4-Chlorotoluene
U
0.114
1.00
1,2-Dibromo-3-Chloropropane
U
0.276
5.00
1,2-Dibromoethane
U
0.126
1.00
Dibromomethane
U
0.122
1.00
1,2-Dichlorobenzene
U
0.107
1.00
1,3-Dichlorobenzene
U
0.110
1.00
1,4-Dichlorobenzene
U
0.120
1.00
Dichlorodifuoromethane
U
0.374
5.00
1,1-Dichloroethane
U
0.100
1.00
1,2-Dichloroethane
U
0.0819
1.00
1,1-Dichloroethene
U
0.188
1.00
cis-1,2-Dichloroethene
U
0.126
1.00
trans-1,2-Dichloroethene
U
0.149
1.00
1,2-Dichloropropane
U
0.149
1.00
1,1-Dichloropropene
U
0.142
1.00
1,3-Dichloropropane
U
0.110
1.00
cis-1,3-Dichloropropene
U
0.111
1.00
trans-1,3-Dichloropropene
U
0.118
1.00
2,2-Dichloropropane
U
0.161
1.00
Di -isopropyl ether
U
0.105
1.00
Ethylbenzene
U
0.137
1.00
Hexachloro-1,3-butadiene
U
0.337
1.00
QUALITY CONTROL SUMMARY
-1556126-01
ACCOUNT:
Frit Car Inc.
PROJECT: SDG: DATE/TIME: PAGE:
3522112 L1556126 11/23/22 11:12 31 of 37

WG1959639
QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS)
by Method 8260D
L1556126-01
Method Blank (MB)
C p
(MB) R3362910-2 11/15/22 0144
MB Result
MB Qualifier MB MDL
MB RDL
Analyte ug/I
ug/I
ug/I
ITC]
Isopropylbenzene U
0.105
1.00
p-Isopropyltoluene U
0.120
1.00
FSS
2-Butanone (MEK) U
1.19
10.0
Methylene Chloride U
0.430
5.00
4-Methyl-2-pentanone (MIBK) U
0.478
10.0
[Cn]
Methyl tert-butyl ether U
0.101
1.00
Naphthalene U
1.00
5.00
5
Sr
n-Propylbenzene U
0.0993
1.00
Styrene U
0.118
1.00
1,1,1,2-Tetrachloroethane U
0.147
1.00
�
1,1,2,2-Tetrachloroethane U
0.133
1.00
1,1,2-Trichlorotrifluoroethane U
0.180
1.00
7GI
Tetrachloroethene U
0.300
1.00
Toluene U
0.278
1.00
1,2,3-Trichlorobenzene U
0.230
1.00
FAI
1,2,4-Trichlorobenzene U
0.481
1.00
1,1,1-Trichloroethane U
0.149
1.00
FS
1,1,2-Trichloroethane U
0.158
1.00
Trichloroethene U
0.190
1.00
Trichlorofluoromethane U
0.160
5.00
1,2,3-Trichloropropane U
0.237
2.50
1,2,4-Trimethylbenzene U
0.322
1.00
1,2,3-Trimethylbenzene U
0.104
1.00
1,3,5-Trimethylbenzene U
0.104
1.00
Vinyl chloride U
0.234
1.00
Xylenes, Total U
0.174
3.00
(S) Toluene-dH 104
80.0-120
(S) 4-Bromofluorobenzene 99.0
77.0-126
(S) 1,2-Dichloroethone-d4 101
70.0-130
Laboratory Control Sample (LCS)
(LCS) R3862910-1 11/15/22 0105
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
ug/I
ug/I
Acetone
25.0
23.4
93.6
19.0-160
Acrolein
25.0
24.4
97.6
10.0-160
Acrylonitrile
25.0
23.8
95.2
55.0-149
Benzene
5.00
4.96
99.2
70.0-123
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
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3522112 L1556126 11/23/22 11:12 32 of 37

WG1959639 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1556126-01
Laboratory Control Sample (LCS)
C p
(LCS) R3362910-1 11/15/22 0105
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte ug/I
ug/I
%
%
ITC]
Bromobenzene 5.00
5.03
101
73.0-121
Bromodichloromethane 5.00
4.33
86.6
75.0-120
FS
Bromoform 5.00
4.47
89.4
68.0-132
Bromomethane 5.00
6.05
121
10.0-160
n-Butylbenzene 5.00
4.84
96.8
73.0-125
[Cn]
sec-Butylbenzene 5.00
4.96
99.2
75.0-125
tert-Butyl benzene 5.00
5.03
101
76.0-124
5
Sr
Carbon tetrachloride 5.00
5.03
101
68.0-126
Chlorobenzene 5.00
4.79
95.8
80.0-121
Chlorodibromamethane 5.00
4.72
94.4
77.0-125
Chloroethane 5.00
4.91
98.2
47.0-150
Chloroform 5.00
4.48
89.6
73.0-120
7GI
Chloromethane 5.00
5.31
106
41.0-142
2-Chlorotoluene 5.00
5.10
102
76.0-123
4-Chlorotoluene 5.00
4.86
97.2
75.0-122
FAI
1,2-Dibromo-3-Chloropropane 5.00
4.72
94.4
58.0-134
1,2-Dibromoethane 5.00
4.80
96.0
80.0-122
FS
Dibromomethane 5.00
4.70
94.0
80.0-120
1,2-Dichlorobenzene 5.00
4.98
99.6
79.0-121
1,3-Dichlorobenzene 5.00
5.10
102
79.0-120
1,4-Dichlorobenzene 5.00
5.08
102
79.0-120
Dichlorodifuoromethane 5.00
5.64
113
51.0-149
1,1-Dichloroethane 5.00
4.80
96.0
70.0-126
1,2-Dichloroethane 5.00
4.64
92.8
70.0-128
1,1-Dichloroethene 5.00
4.83
96.6
71.0-124
cis-1,2-Dichloroethene 5.00
4.61
92.2
73.0-120
trans-1,2-Dichloroethene 5.00
4.68
93.6
73.0-120
1,2-Dichloropropane 5.00
5.03
101
77.0-125
1,1-Dichloropropene 5.00
4.87
97.4
74.0-126
1,3-Dichloropropane 5.00
5.02
100
80.0-120
cis-1,3-Dichloropropene 5.00
4.50
90.0
80.0-123
trans-1,3-Dichloropropene 5.00
4.95
99.0
78.0-124
2,2-Dichloropropane 5.00
4.61
92.2
58.0-130
Di -isopropyl ether 5.00
5.03
101
58.0-138
Ethylbenzene 5.00
5.10
102
79.0-123
Hexachloro-1,3-butadiene 5.00
4.78
95.6
54.0-138
Isopropylbenzene 5.00
4.87
97.4
76.0-127
p-Isopropyltoluene 5.00
4.92
98.4
76.0-125
2-Butanone (MEK) 25.0
23.9
95.6
44.0-160
Methylene Chloride 5.00
4.87
97.4
67.0-120
ACCOUNT:
PROJECT: SDG: DATE/TIME:
PAGE:
Frit Car Inc.
3522112 L1556126 11/23/22 11:12
33 of 37

WG1959639 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1556126-01
Laboratory Control Sample (LCS)
(LCS) R3862910-1 11/15/22 0105
Spike Amount
LCS Result
LCS Rec.
Rec. Limits
Analyte
ug/I
ug/I
4-Methyl-2-pentanone (MIBK)
25.0
25.2
101
68.0-142
Methyl tert-butyl ether
5.00
4.83
96.6
68.0-125
Naphthalene
5.00
4.56
91.2
54.0-135
n-Propylbenzene
5.00
4.81
96.2
77.0-124
Styrene
5.00
4.90
98.0
73.0-130
1,1,1,2-Tetrachloroethane
5.00
4.50
90.0
75.0-125
1,1,2,2-Tetrachloroethane
5.00
5.18
104
65.0-130
1,1,2-Trichlorotrifluoroethane
5.00
5.07
101
69.0-132
Tetrachloroethene
5.00
5.22
104
72.0-132
Toluene
5.00
4.95
99.0
79.0-120
1,2,3-Trichlorobenzene
5.00
4.69
93.8
50.0-138
1,2,4-Trichlorobenzene
5.00
4.76
95.2
57.0-137
1,1,1-Trichloroethane
5.00
4.75
95.0
73.0-124
1,1,2-Trichloroethane
5.00
5.23
105
80.0-120
Trichloroethene
5.00
4.63
92.6
78.0-124
Trichlorofluoromethane
5.00
4.89
97.8
59.0-147
1,2,3-Trichloropropane
5.00
4.94
98.8
73.0-130
1,2,4-Trimethylbenzene
5.00
5.09
102
76.0-121
1,2,3-Trimethylbenzene
5.00
4.97
99.4
77.0-120
1,3,5-Trimethylbenzene
5.00
5.01
100
76.0-122
Vinyl chloride
5.00
5.33
107
67.0-131
Xylenes, Total
15.0
14.8
98.7
79.0-123
(S) Toluene-dH
101
80.0-120
(S) 4-Bromofluorobenzene
101
77.0-126
(S) 1,2-Dichloroethone-d4
98.1
70.0-130
LCS Qualifier
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contactyour project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
u
Fc
Fss]
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
Fn
RDL
Reported Detection Limit.
Rec.
Recovery.
Fr
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
F
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
F
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Rc
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
B
The same analyte is found in the associated blank.
E
The analyte concentration exceeds the upper limit ofthe calibration range ofthe instrument established by the initial
calibration (ICAL).
J
The identification ofthe analyte is acceptable, the reported value is an estimate.
J3
The associated batch QC was outside the established quality control range for precision.
J4
The associated batch QC was outside the established quality control range for accuracy.
J5
The sample matrix interfered with the ability to make any accurate determination, spike value is high.
P1
RPD value not applicable for sample concentrations less than 5 times the reporting limit.
v
The sample concentration is too high to evaluate accurate spike recoveries.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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ACCREDITATIONS & LOCATIONS
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122
F
Alabama
40660
Nebraska
N E-OS-15-05
Alaska
17-026
Nevada
TN000032021-1
Fc
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TNO02
California
2932
New Mexico
TN00003
Fss]
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704
3
Fn
Georgia
NELAP
North Carolina
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Fr
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
6
QC
Kansas
E-10277
Rhode Island
LA000356
Kentucky' 6
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
7
C71
Louisiana
A130792
Tennessee'"
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas5
LABO152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
110033
F
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A2 LA
A2LA— ISO17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks
3 Aquatic Toxicity "Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are
applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods
specified on each scope of accreditation held by Pace
Analytical.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 3522112 L1556126 11/23/22 11:12 36 of 37

Company Name/Address:
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New ern, NC 29560
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ADVANCING SCIENCE
MT 1ULIET, TN
Report to:
Email To: [e-mail]
Connie Pettis
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*Matrix:Remarks:
sample Receipt checklist
SS - Soil AIR •Air F- Filter pH Temp
COC Seal present/Intact: NP Y _N
GW- Groundwater 6-Bioassay
COC Signed/Accurate: Y N
WW -Wastewater Flow Other
ROttles arrive intact: Y _N
Correct bottles used: Y N
DW - Drinking Water
Samples re urned via:
Sufficient volume sent: y —N
—
OT - Other Track ing#
1JF5 FedEx Courier
If Applicable
VOA Zero Fleadspace: N
preservation Correct:/Chec3:ed: �N
RAD Screen <0.5 mR/hr: N
Relinquished by: (Signature) Date:
Time:
Received by: (Signature)
Trip Blank Received: Yes /
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Relinquished by : (Signature) Date:
Time:
Received by: (Signatur)
TempMlk m Bottles Received:
If preservation required by Login: Date/Time
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Time:
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Date Time:
Hold:
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