WQ0002503_Monitoring - 11-2022_20230113

Monitoring Report Submittal
Permit Number #*
Name of Facility:*
Month: * November
Report Information
WQ0002503
FRIT CAR, INC.
Type *
NDMR, NDAR-1, NDAR-2, NDMLR
GW-59
Confirmation Email Address:*
Name of Submitter: *
Signature:
Date of submittal:
[e-mail]
Connie Pettis
Year:* 2022
Upload Document*
NDAR-NDMR NOVEMBER 8AMB
2022.pdf
PDF Only
2022-11 GW59.pdf 2AMB
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
-0 C15DWMV
1 /13/2023
This will be filled in automatically

Initial Review
Reviewer:
Gerald, Wanda
Is the project number correct?*
WQ0002503
Is the monitoring report accepted?*
Yes No
Regional Office*
Washington
Reviewer: _anonymous
Review Date: 2/6/2023

FORM: NDMR 07-13 NON -DISCHARGE MONITORING REPORT (NDMR) Page
Permit No.: WQ0002503
Facility Name: Frit Car, Inc.
County: Craven
Month: November
Year: 2022
PPI.
Flow Measuring Point: ❑ IMuent C EfFuent ❑ No flow generated
Parameter Monitoring Point: influent E] Effluent ❑ Groundwater Lowering ] Surface water
Parameter Code - ►
50050 ':
00400
0,0w46rap'. ,
00310
00940: '
C0665
t30G 8 0 ''
00680
00&60
00929
70300
C0530
003d
01445
32730
01092
y
U
Q
4..
�
L7
fl
Q i
-7,L cUa
QF
o
07 0
. -
0.:
n<
O2p.
U)
a
F
E
.
CJ
0
o
C
a=
iVUC
24-hr
hrs
1 GPD
su
:
mglL
mgJL
mg/L
mg/L
mg/L
mig1L
mg/L
mgJL
mg/L
mg/L
mg1L
rng/L
mg/L
1
07:00
8
140
6.72
-.4am
27.6
4720
544
153 `
28.1
0.05
12200
40200
604
0.289
3.19
<,04
0-791
2
07:00
8
ills,..., x
3
07:00
8
150
4
07:00
8
200
5
_
S
7
1 07:00
8
81
07:00
8
9
07:00
8
10
07:00
8
11
07:00
8
200
12
13
14
07:00
8
15
07:00
a
16
07:00
8
17
07:00
18
07:00
E
19
20
21
07:00
8
22
07:00
8
23
07:00
8
24
07:00
8
251
07:00
8
26
27
28
07:00
8
29
07:00
8
30
07:00
8
31
Average:
173
1,670.00
27.60
4,720.00:
544.00
163,00
28.10
.0,05
12,200.00
40,200,00
604.00
0129
3.19
0.00
0.79
Daily Maximum:
200
5,72
1,670-00
27.60
4,720.00
544.00
153.00
28.10
0.05
12,200.00
40,200,00
604.00
0.29
3.19
0.04
0.79
Daily Minimum:
140
6,72
11670.00
27.60
4,720.00
544.00
163,00
28 110
0.05
12,200.00
40.200.001
604,00
0,29
3.19
0.04
0.79
Sampling Type:
Monthly Avg. Limit:
Daily Limit:
Sample Frequency:

FORM: NDMR 07-13 NON -DISCHARGE MONITORING REPORT (NOIVIR) Page
Permit No.. WQ0002503E
Parameter Monitoring Point: Influent D� Effluent 0 GrDundwater I_Dwer�ng Surface Water
PararneterCode
s
•
Sampling Type -
Monthly Avg. Limit:

FORM: NDMR 07-13 NON -DISCHARGE MONITORING REPORT (NDMR) Page of
Sampling Person(s) Certified Laboratories
Name: Danny Hornbeck Name: Pace Analytical
Name: Name:
Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? M compliant ❑ Non -compliant
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective
action(s) taken. Attach additional sheets if necessary.
Operator in Responsible Charge (ORC) Certification Permittee Certification
ORC: Danny Hornbeck Permittee: Frit Car, Inc.
Certification No.: 26718 Signing Official: Michael Newby
Grade: Phone Number: 252-638-2675 Signing Official's Title, Senior Vice President
Has the ORC changed since the previous NDMR? ❑ Yes i❑ ND Phone Numbetj 251-867-7752 Permit Expiration: 2/2812029
Signature Date
By this signature. 1 certify that this report is accurrate and complete to the best Of my knowledge.
� yZ 3d Z 7i
Signature Date
I certify, under penalty of iaw. that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information
submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am
aware that there are significant penalties for submitting false informaton, including the possibility of fines and imprisonment for
knowing violations.
Mail Original and Two Copies to:
Division of Water Resources
Information Processing Unit
1517 Mail Service Center
Raleigh, North Carolina 27699-1617

FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page of
Permit No.: 0000#
, -
. I-�
#
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RAN
at this facility'?
F
Annual Raiefln),j
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FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page of
Did the application rates exceed the limits in Attachment B of your permit?
❑ Compliant
❑ Nor -compliant
Were adequate measures taken to prevent effluent ponding in or runoff from the sites?
E Compliant
❑ Norrccmpliant
Was a suitable vegetative cover maintained on all sites as specified in your permit?
0 Compliant
❑ Nor-Complianr
Were all setbacks listed in your permit maintained for every application to each permitted site?
❑ Compliant
❑ Nor-Complianr
Were all freeboards maintained in accordance with the specified freeboard heights in your permit?
0 Compliant
❑ Nor -Compliant
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective
action(s) taken. Attach additiona3 sheets if necessary.
Operator in Responsible Charge (QRC) Certification Permittee Certification
ORC: Danny Hornbeck Permittee:
Frit Car, Inc.
Certification No.: 26718 Signing Official: Michael Newby
Grade: Phone Number: 252-638-2675 Signing Official's Title: Senior Vice President
Has the ORC changed since the previous NDARA? ❑ yes , No Phone Number: 1-867-7762 Permit Exp.: 2/28/29
Signature Date
Date
By this signature. I certify that this report is accurrate and complete to the best of my knowledge. I certify, under penalty of law. that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my
inquiry of the person,or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, role. accurate, and complete. i am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
Mail Original and Two Copies to:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617

(� ace Analytical
11
ANALYTICAL REPORT
December 16, 2022
Frit Car Inc.
Sample Delivery Group
Samples Received:
Project Number:
Description:
L15634O9
12/02/2022
Bridgeton Facility Monthly
Report To: Connie Pettis
2012 US Hwy 17N
New Bern, NC 28560
Entire Report Reviewed By: q�"h
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1563409 12/16/22 12:02 1 of 23

TABLE OF CONTENTS
Cp: Cover Page
Tc: Table of Contents
Ss: Sample Summary
Cn: Case Narrative
GI: Glossary of Terms
Al: Accreditations & Locations
Sc: Sample Chain of Custody
2
3
4
5
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1563409 12/16/22 12:02 2 of 23

EFFLUENT L1563409-01 WW
Method
Subcontracted Analyses
SAMPLE SUMMARY
Collected by
DB
Batch Dilution Preparation
date/time
WG1968582 1 12/12/22 00:00
Collected date/time Received date/time
11/29/22 16:00 12/02/2216:33 C
P
Analysis
date/time
12/12/22 00:00
Analyst
Location
EWest Columbia, SC
29172 w
Fn
5G1
6AI
Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1563409 12/16/22 12:02 3 of 23

CASE NARRATIVE
FP
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
5G1
6AI
4�z
Sc
Heather J Wagner
Project Manager
Project Narrative
L1563409 -01 contains subout data that is included after the chain of custody.
ACCOUNT: PROJECT: SDG: DATE/TIME:
PAGE:
Frit Car Inc. L1563409 12/16/22 12:02
4 of 23

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not u
intended as a comprehensive explanation, and ifyou have additional questions please contactyour project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Fc
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions Fss]
SDG
Sample Delivery Group.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG.
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1563409 12/16/22 12:02 5 of 23

ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
Nebraska
N E-OS-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TNO02
California
2932
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolina 3
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky' 6
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee'"
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas5
LABO152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A2 LA
A2LA— ISO17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME:
Frit Car Inc. L1563409 12/16/22 12:02
PAGE:
6 of 23

L [5co314o4
Sample Receiving Summary Printed: 121212022445:24PMbyJS
Quote: 25738
Client: (2907) Pace Analytical LLC 1 Heather Wagner
Comments:
Project Name: Frit Car
Project Number:
Analysis Due: 12/12/2022
Report Due: 12/14/2022
Project Manager: JSH
Program Area: DoD QSM 5.3
PO Number:
Level 1 Review:
Level 2 Review:
Cooler # Cooler ID (if applicable) Temp P C) Comments
1 5,6
Shealy Ip: XK30021.001 Client ID: Effluent Collected: 11129/2022 at 1600 by CLIENT
Sample Receiving Matrix:Aqueous Received: 11/30/2022 1305 by KSC
Entered: 11130/2022 by KSC Receipt Method: Fed -Ex
Sample Containers: Qty Sample Containers
1 (053) Client provided G-NP
Tests: Method Test
365.1 Orthophosphate
Totals: Samples
1
(end or report)
Comments
Prep Method Protocol
Samples
Sample Containers Tests/items
1 1
Pace Analytical Services, LLC Page: 1 of 3
106 Vantage Point Drive West Columbia, SC 29172 803-791-9700 www.pacelabs.ccm - Frit Car, XK30021 Sample Receiving Summary v2 2

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SHEALY ENVIRONMENTAL SERVICES, INC.
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Pace Analytical Services, LLC Page: 2 of 3
106 Vantage Point Drive West Columbia, SC 29172 803-791-9700 www.pacelabs.com Frt Car, XK30021 Sample Receiving Summary v2.2

L-k5�4` 3LEaq
SHEALY ENVIRONMENTAL SERVICES, INC.
DC# Tltle_ Eta!-FRM-WCQL-0286 02_S2mples Receipt Checklist (SRC)
Effective Date: 912/2022
Sample Receipt Checklist (SRC;')
Chem 1", ('Dater 1nskrcted bplclate: Tl�2 ; t VM2(2'
.1" -#; XK30031
d
Ye-s
N i . Were cu seals pitsent on the coulee?
IVIYCSI
1
114011Tl:l I. IPtttstuci scats wce,e rGseul, were true intact, encl tutLeukrhl?
)H Strip II3_ "A Utiodne Strip II?, K, Tested by: N6
Diiolal terriwature ttpou receipt f Dcrived (C'an>er,1W) letupemire upon receipt SaSolid Snap-ntp ID NA
5.6 j5.6 oC NA /:1A cC NA INA qe P:A INA oC
Avilmd: 17Telnperarare Blauk�Af.,a its( BOIL1le, lit Our Ill: 3 IR onin c mectiouTacier. ° °c;
`,Ic hod of rat>lanT W Vet icc n Ice Pa,1- F-1 Ury Re n None
Yes
❑ No
a A
, tzele all c00 is rectxv at yr itrltnv 6.001M If no- was Project hlnua_er nolifi '?
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1114 w wx 'Notified by 1me f mind I face-10-race (C1rtic Ono.
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4 IS the coininizrleial Muria'S Picidug slip attached to di15 roan'
Ycs
YO
5 Were prnper cli,.tody )ntce41vcs (itlingitislwd,received) tbllow•cd?
✓
Yrx
Yes
No
No
6. Jv ere s nnplle tl]s 1 is ecI ult IILr Ct�C nhd all S72idplt c�tfainers?
?. Was collection (Late & tine listed cai the CO(' mid all soLgAe containers'}
Yes
No
8. Did all container I4)el in on iatiQit (ID. dale, litnc) agree R9ttk the COC?
Yes
No
9. Werc tests to be perfornicd listed on 1tr l'QC?
[DYes
E]No
10. Did all satnplcs Arrive in dht proper Coral hM for M11 test irtdler in good cowHilian
(iinbrokeu, lids on. etc)?
Ycs
Nu
11. Was adequate saWle vuhat_e availAble7
Ycs
NO
112 Wert all 5awplics ierelvrd %ijbin'f, the holdlq time Df 4813o1us. wj6cbevier Llni lit'st.?
EVI Ycs
Q NO
13. Were all samples coutl istrrs ticcatenrcd for? (No itiissfik7faccss)
Yes
Na
,fey+,
1 4' W'm WIi 8015C and RSX-175 samples free ai bubbles %"plea-ai7li (iAl"or Gltuu iel
dittnieter) in any of livi vials?
1 S. EVere all DMmClalsfuuLTicitL samples received at 0 H Of < 27
YcsTZo
Xc
16. Wci c ;dl c•,-iwde sal lts rrceivi-d az a pH - 12 aced .-al is slim pies received at a pFi > 9?
Ycs
17, Vbr:tc a alhp Cabe _ H3rTKNicylnt cip e3loLi6'5.1l60R.3 (c: 0.5inPL) S-M es Eii c
icsi(bini chlorine?
]Yes
I$. WITS EILC quore tltlttlber listed mi flit cnatahin labcll b yes, QROfeSamplepat
wtryatiou (Mas[
be coutpletcd fn: any suttltic{Sj utcanrrtl 1-t'cd ar with heart, ace ?
} r— 11
Sairipic(S) NA wav received incOttYctly preserved and were adjusted accordingly
nt sawple rccciving with ^ niL of circle one. TUS04, tlNti3- ILCL N.-LOB using SR # NA 1-1dime of prrstrva�on NA If MOT,'an [leunc prescrt'alive is Deeded pltue irate in rite COruiuic7its l,clow.
4aiupie(s) 14A ' e,c: received tsililt lnihltles>6 Font in diameter.
SantplcY(5) `Tx cvrze rerrivcd with TRC 7 0.5111 (lf ,?l9 is tip) amid tare
djinred nccordntt;ly iu smirpic ircciving with sodium r3tiosulfate (N'1i,910 witli Unit)Ltr 11}: NA
t:n1lUllPfliS'
Qualtrax It?; 563&0 Race' Analytical 5aruices, LLC Page 1 of 1
Pace Analytical Services, LLC Page: 3 of 3
106 Vantage Point Drive West Columbia, SC 29172 803-791-9700 www.pacelabs.com Fnt Car, XK30021 Sample Receiving Summary v2 2

0p
0
PaceAnalyfical
Report of Analysis
Pace Analytical LLC
12065 Lebanon Rd.
Mt. Juliet, TN 37122
Attention: Heather Wagner
Project Name: Bridgeton Facility Monthly
Project Number: WG1968582
Lot Number:XK30021
Date Completed:12/09/2022
12/10/2022 10:35 AM
Approved and released by:
Project Coordinator 1: Jenna S. Holliday
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page Iof14

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Pace Analytical LLC
Lot Number: XK30021
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Additionally, the
DoD QSM version 5.4 has been followed for these samples. Any exceptions to the TNI standards, the
Laboratory Quality Manual, SOPs, the DoD QSM, or policies are qualified on the results page or
discussed below.
Pace is a DoD/DOE accredited laboratory; however, the following analyses are currently not listed on our
DoD/DOE scope of accreditation: Drinking Water: pH EPA 150.1, Turbidity EPA 18.01, Metals EPA 200.7
& 200.8, Mercury EPA 245.1, Anions EPA 300.0, Cyanide EPA 335.4, Nitrates EPA 353.2,
Orthophosphate & Phosphorus EPA 365.1, EDB/DBCP EPA 504.1, HPC SIMPLATE, Color SM 2120 B-
2011, Alkalinity SM 2320 B-2011, Specific Conductance SM 2510 B-2011, Residue -filterable (TDS) SM
2540 C, Calcium Hardness (CaCO2) SM 3500-Ca B-2011, TRC SM 4500 Cl G-2011, pH SM 4500 H=B-
2011, E.Coli, Total Coliform; Non -Potable Water: Metals EPA 200.7, Strontium EPA 200.8, Chlorate EPA
300.0, Cyanide EPA 335.4, Phenolics EPA 420.4, 2-Methyl-4,6-Dinitrophenol EPA 625.1, Propane RSK-
175, Specific Conductance SM 2510 B-2011, Salinity SM250 B, Residue- total SM 2540 B, Sulfite SM
4500 SO32- B-2011, Amenable Cyanide SM 4500-CN- G-2011, BOD & CBOD SM 5210 B, MBAS SM
5540 C-2011; Solid and Chemical Materials: Boron & Titanium SW-846 601 OD, Boron, Molybdenum, &
Titanium SW-846 6020B, Alcohols & Glycols SW-846 8015C, Pentachlorophenol SW-846 8151A, Ethyl
Acetate, Hexane, & n-Hexane SW-846 8260D, SVOC 1,4-Dioxane, 3&4-Methylphenols, 4-Dimethyl
aminoazobenzene, 1,4-Naphthoquinone, 3,5-Dinitroaniline, PETN SW-846 8270E, Amenable Cyanide
SW-846 901213; Boron & Titanium SW-846 601 OD, Molybdenum SW-846 6020B, Ethylene Glycol SW-
846 8015B, Pentachlorophenol SW-846 8151A, Chloroprene SW-846 8260B, SVOC 1,3,5-
Trinitrobenzene, 1,4-Dioxane, 1,4-Naphthoquinone, 1,4-Phenylenediamine, 2,5-Dinitrotoluene, 2,6-
Dinitrotoluene, 3-Methylcholanthrene, 4- Aminobiphenyl, 4-Dimethyl aminoazo benzene, 4-Nitroquinoline-
1-oxide, 7,12- Dimethylbenzo(a)anth race ne, Chlorobenzilate, Diallate, Ethyl methanesulfonate, Isodrin,
Isosafrole, Methyl methanesulfonate, n-Nitrosomethylethylamine, n-Nitrosomorpholine, n-
Nitrosopiperidine, Piperonyl butoxide, Pronamide, Safrole, 3,5-Dinitroaniline, PETN SW-846 8270E, Oil &
Grease SW-846 9071 B.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 14

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
Orthophosphate Analysis
The matrix spike (MS) and matrix spike duplicate (MSD) for batch 61355 recovered outside of the
acceptance limits. The associated laboratory control sample (LCS) passed acceptance criteria. Therefore,
the data has been reported.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvww.pacelabs.com
Page 3of14

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Pace Analytical LLC
Lot Number: XK30021
Project Name: Bridgeton Facility Monthly
Project Number: WG1968582
Sample Number Sample ID Matrix Date Sampled Date Received
001 Effluent Aqueous 11/29/20221600 11/30/2022
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 14

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Pace Analytical LLC
Lot Number: XK30021
Project Name: Bridgeton Facility Monthly
Project Number: WG1968582
Sample Sample ID Matrix Parameter Method Result Q Units Page
(0 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 14

Inorganic non-metals
Client: Pace Analytical LLC Laboratory ID:XK30021-001
Description: Effluent Matrix: Aqueous
Date Sampled:11/29/2022 1600 Project Name: Bridgeton Facility Monthly
Date Received:11/30/2022 Project Number: WG1968582
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Orthophospha) 365.1 1 11/30/2022 1828 DMA 61355
CAS Analytical
Parameter Number Method Result Q LOQ LOD DL Units Run
Orthophosphate
365.1 0.050 US 0.050 0.050 0.050 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
U = Not detected at or above the LOD N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis LOD = Limit of Detection S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 14

QC Summary
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: XK30021
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 14

Inorganic non-metals - MB
Sample ID: XQ61355-001 Matrix: Aqueous
Batch:61355
Analytical Method: 365.1
Parameter Result Q Dil LOQ LOD DL Units Analysis Date
Orthophosphate 0.050 U 1 0.050 0.050 0.050 mg/L 11/30/20221828
LOQ = Limit of Quantitation U = Not detected at or above the LOD N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
LOD = Limit of Detection = RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: XK30021
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 14

Inorganic non-metals - LCS
Sample ID: XQ61355-002 Matrix: Aqueous
Batch:61355
Analytical Method: 365.1
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Orthophosphate 0.25 0.24 1 95 90-110 11/30/20221828
LOQ = Limit of Quantitation U = Not detected at or above the LOD N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
LOD = Limit of Detection = RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: XK30021
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 14

Inorganic non-metals - MS
Sample ID: XK30021-001 MS Matrix: Aqueous
Batch: 61355
Analytical Method: 365.1
Sample Spike
Amount Amount Result %Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Orthophosphate ND 0.25 0.022 N 1 8.7 90-110 11/30/20221828
LOQ = Limit of Quantitation U = Not detected at or above the LOD N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
LOD = Limit of Detection = RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: XK30021
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 14

Inorganic non-metals - MSD
Sample ID: XK30021-001MD Matrix: Aqueous
Batch: 61355
Analytical Method: 365.1
Sample Spike
Amount Amount Result %Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Orthophosphate ND 0.25 0.022 N 1 8.7 0.18 90-110 20 11/30/20221828
LOQ = Limit of Quantitation U = Not detected at or above the LOD N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
LOD = Limit of Detection = RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: XK30021
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 14

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 14

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of 14

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 14 of 14

(� ace Analytical
13
ANALYTICAL REPORT
December 30, 2022
Frit Car Inc.
Sample Delivery Group:-1562118
Samples Received: 11/30/2022
Project Number:
Description: Bridgeton Facility Monthly
Report To: Connie Pettis
2012 US Hwy 17N
New Bern, NC 28560
Entire Report Reviewed By: q�"h
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy ofthe information provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1562113 12/30/22 10:36 1 of 37

TABLE OF CONTENTS
Cp: Cover Page
u
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
FSSI
EFFLUENT L1562118-01
5
Fn
Qc: Quality Control Summary
7
Gravimetric Analysis by Method 2540 C-2011
7
Fr
Gravimetric Analysis by Method 2540 D-2015
8
Wet Chemistry by Method 300.0
9
Rc
Wet Chemistry by Method 350.1
11
F
Wet Chemistry by Method 351.2
12
Wet Chemistry by Method 365.4
13
[Al
Wet Chemistry by Method 420.4
14
Wet Chemistry by Method 4500H+ B-2011
16
RC
Wet Chemistry by Method 5210 B-2016
17
Wet Chemistry by Method 5310 B-2014
18
Metals (ICP) by Method 200.7
19
GI: Glossary of Terms
21
Al: Accreditations & Locations
22
Sc: Sample Chain of Custody
23
ACCOUNT: PROJECT: SDG:
DATE/TIME:
PAGE:
Frit Car Inc. L1562113
12/30/22 10:36
2 of 37

SAMPLE SUMMARY
Collected by Collected date/time Received date/time
EFFLUENT L1562118-01 WW Danny Hornbeck 11/29/2216:00 11/30/22 09:00 , C
P
Method
Calculated Results
Gravimetric Analysis by Method 2540 C-2011
Gravimetric Analysis by Method 2540 D-2015
Wet Chemistry by Method 300.0
Wet Chemistry by Method 300.0
Wet Chemistry by Method 350.1
Wet Chemistry by Method 351.2
Wet Chemistry by Method 365.4
Wet Chemistry by Method 420.4
Wet Chemistry by Method 4500H+ B-2011
Wet Chemistry by Method 5210 B-2016
Wet Chemistry by Method 5310 B-2014
Metals (ICP) by Method 200.7
Metals (ICP) by Method 200.7
Batch
Dilution
Preparation
Analysis
Analyst
date/time
date/time
WG1967977
1
12/03/2214:37
12/03/2214:37
LBR
WG1969036
1
12/04/2215:29
12/05/2212:14
DTM
WG1968020
1
12/01/2219:39
12/01/22 22:11
AS
WG1966879
10
11/30/2215:24
11/30/2215:24
LBR
WG1966879
100
11/30/2215:38
11/30/2215:38
LBR
WG1968999
20
12/04/2214:38
12/04/2214:38
BMD
WG1967977
25
12/02/2218:21
12/03/2214:37
LDT
WG1968838
200
12/02/2218:21
12/03/2215:04
LDT
WG1966901
1
12/02/22 08:00
12/02/2217:16
LDT
WG1968391
1
12/05/2214:40
12/05/2214:40
ARID
WG1966961
1
11/30/221157
12/05/22 09:41
ABA
WG1967456
2
12/01/22 14:02
12/01/22 14:02
SJF
WG1973597
1
12/15/22 08:28
12/15/22 18:09
ZSA
WG1973597
20
12/15/22 08:28
12/16/22 04:28
ABL
Location
FC
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fn
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fr
Mt. Juliet, TN
Mt. Juliet, TN
Rc
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
F,
Mt. Juliet, TN
F
RC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1562113 12/30/22 10:36 3 of 37

CASE NARRATIVE
FP
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
0
Fr
Rc
4�z
F,
Heather J Wagner
Project Manager
[Al
RC
Sample Delivery Group (SDG) Narrative
The following analysis were performed from an unpreserved, insufficiently or inadequately preserved sample.
Lab Sample ID Project Sample ID Method
L1562113-01 EFFLUENT 5310 B-2014, 350.1, 200.7
ACCOUNT: PROJECT: SDG: DATE/TIME:
PAGE:
Frit Car Inc. L1562113 12/30/22 10:36
4 of 37

SAMPLE RESULTS - 01
L1562118
EFFLUENT
Collected date/time: 11/29/22 16:00
Calculated Results
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date / time
Total Nitrogen 173000 1000
1 12/03/202214:37 WG1967977
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier RDL
Dilution Analysis Batch
Analyte ug/I ug/I
date / time
Dissolved Solids 40200000 400000
1 12/05/202212:14 WG1969036
Gravimetric Analysis by Method 2540 D-2015
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date / time
Suspended Solids 604000
Wet Chemistry by Method 300.0
100000 1 12/01/2022 22:11 WG1968020
Result
Qualifier RDL
Dilution
Analysis
Batch
Analyte ug/I
ug/I
date / time
Chloride 4720000
100000
100
11/30/202215:38
WG1966879
Nitrate as (N) 17000
1000
10
11/30/202215:24
WG1966879
Nitrite as (N) ND
1000
10
11/30/202215:24
WG1966879
Sulfate 1670000
50000
10
11/30/202215:24
WG1966879
Wet Chemistry by Method 350.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date / time
Ammonia Nitrogen 153000 5000 20 12/04/2022 14:38 WG1968999
Wet Chemistry by Method 351.2
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date / time
Kjeldahl Nitrogen, TKN 156000 6250 25 12/03/202214:37 WG1967977
Sample Narrative:
L1562118-01 WG1967977: Dilution due to matrix.
Wet Chemistry by Method 365.4
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date / time
Phosphorus, Total 544000 20000 200 12/03/202215:04 WG1968838
Wet Chemistry by Method 420.4
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date / time
Total Phenol by4AAP ND 40.0 1 12/02/202217:16 WG1966901
Wet Chemistry by Method 4500H+ B-2011
Result Qualifier Dilution Analysis Batch
Analyte su date / time
pH 6.72 T8 1 12/05/202214:40 WG1968391
Sample Narrative:
L1562118-01 WG1968391: 6.72 at20.3C
— FP
— Fc
FS
—
Fn—
—
Rc
�GI
[Al
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1562113 12/30/22 10:36 5 of 37

EFFLUENT SAMPLE RESULTS - 01
Collected date/time: 11/29/22 16:00 L1562118
Wet Chemistry by Method 5210 B-2016
Result Qualifier RDL Dilution Analysis
Analyte ug/I ug/I date / time
BOD 27600 K5 K8 K9 2000 1 12/05/2022 09:41 WG1966961
Wet Chemistry by Method 5310 B-2014
Result Qualifier RDL
Analyte ug/I ug/I
TOC (Total Organic Carbon) 28100 2000
Metals (ICP) by Method 200.7
Analyte
Cadmium
Chromium
Copper
Iron
Lead
Nickel
Sodium
Zinc
Batch
Dilution Analysis Batch
date / time
2 12/01/202214:02 WG1967456
Result
Qualifier RDL
Dilution
Analysis
Batch
ug/I
ug/I
date / time
28.2
2.00
1
12/15/202218:09
WG1973597
289
10.0
1
12/15/202218:09
WG1973597
83.0
10.0
1
12/15/202218:09
WG1973597
3190
100
1
12/15/202218:09
WG1973597
ND
100
20
12/16/2022 04:28
WG1973597
1180
200
20
12/16/2022 04:28
WG1973597
12200000
20000
20
12/16/2022 04:28
WG1973597
791
50.0
1
12/15/202218:09
WG1973597
— FP
FC
FS—
Fn
—
—
Rc
�GI
SAI
RC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1562113 12/30/22 10:36 6 of 37

WG1969036
Gravimetric Analysis by Method 2540 C-2011
Method Blank (MB)
(MB) R3369429-1 12/05/22 12:14
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/I ug/I ug/I
Dissolved Solids U 10000 10000
L1562166-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1562118-01
(OS) L1562166-01 12/05/22 12:14 • (DUP) R3369429-3 12/05/22 12:14
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I %_
Dissolved Solids 537000 569000 1 5.79 J3 5
L1562168-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1562163-01 12/05/22 12:14 • (DUP) R3369429-4 12/05/22 12:14
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
Dissolved Solids 390000 418000 1 6.93 J3 5
Laboratory Control Sample (LCS)
(LCS) R3369429-2 12/05/22 12:14
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I
Dissolved Solids 8800000 8320000 94.5 77.3-123
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1562113 12/30/22 10:36 7 of 37

WG1968020
Gravimetric Analysis by Method 2540 D-2015
Method Blank (MB)
(MB) R3867367-1 12/01/22 2211
MB Result
Analyte ug/I
Suspended Solids U
MB Qualifier MB MDL MB RDL
ug/I ug/I
2500 2500
L1562203-02 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1562118-01
(OS) L1562203-02 12/01/22 22:11 • (DUP) R3367367-3 12/01/22 22:11
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
Suspended Solids 204000 252000 1 20.9 J3 5
L1562362-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1562362-01 12/01/22 22:11 • (DUP) R3367367-4 12/01/22 22:11
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
Suspended Solids 20400 25600 1 22.6 P1 5
Laboratory Control Sample (LCS)
(LCS) R3367367-2 12/01/22 22:11
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I
Suspended Solids 773000 784000 101 85.7-114
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1562113 12/30/22 10:36 3 of 37

WG1966879
Wet Chemistry by Method 300.0
Method Blank (MB)
(MB) R3367374-1 11/30/22 1159
MB Result
Analyte
ug/I
Chloride
U
Nitrate
U
Nitrite
U
Sulfate
U
MB Qualifier MB MDL
MB RDL
ug/I
ug/I
379
1000
48.0
100
42.0
100
594
5000
L1561841-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1561341-01 11/30/22 13:21 • (DUP) R3867874-3 11/30/22 13:34
Original Result
DUP Result
Dilution DUP RPD
Analyte
ug/I
ug/I
Chloride
3770
3620
1 4.10
Nitrate
114
112
1 1.59
Nitrite
ND
ND
1 0.000
Sulfate
31700
31700
1 0.0375
L1562168-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1562163-01 11/30/22 2101 • (DUP) R3867874-6 11/30/22 2114
Original Result
DUP Result
Dilution DUP RPD
Analyte
ug/I
ug/I
Chloride
26700
26900
1 1.02
Nitrate
4950
4990
1 0.838
Nitrite
ND
ND
1 0.000
Sulfate
77500
77600
1 0.151
Laboratory Control Sample (LCS)
(LCS) R3867874-2 11/30/22 12:13
Spike Amount
LCS Result
LCS Rec.
Analyte ug/I
ug/I
Chloride 40000
38900
97.2
Nitrate 8000
7540
94.2
Nitrite 8000
7880
98.5
Sulfate 40000
38200
95.4
QUALITY CONTROL SUMMARY
L1562118-01
DUP Qualifier DUP RPD
Limits
20
20
20
20
DUP Qualifier DUP RPD
Limits
20
20
20
20
Rec. Limits LCS Qualifier
90.0-110
90.0-110
90.0-110
90.0-110
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1562113 12/30/22 10:36 9 of 37

WG1966879 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 300.0 L1562118-01
L1561841-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1561341-01 11/30/22 13:21 • (MS) R3367374-4 11/30/22 13:43 • (MSD) R3367374-5 11/30/22 14:02
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte
ug/I
ug/I
ug/I
ug/I
Chloride
50000
3770
52100
51900
96.7
96.2
1 80.0-120
0.470
20
Nitrate
5000
114
4580
4620
89.3
90.1
1 80.0-120
0.861
20
Nitrite
5000
ND
4960
4970
99.2
99.4
1 80.0-120
0.119
20
Sulfate
50000
31700
76400
76300
89.3
89.2
1 80.0-120
0.0906
20
L1562168-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1562163-01 11/30/22 2101 • (MS) R3367374-7 11/30/22 2123 • (MSD) R3367374-8 11/30/22 2142
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
ug/I
ug/I
ug/I
ug/I
Chloride
50000
26700
74000
74500
94.6
95.7
Nitrate
5000
4950
9280
9460
86.6
90.4
Nitrite
5000
ND
4940
5010
98.8
100
Sulfate
50000
77500
120000
121000
85.3
88.0
ACCOUNT:
Frit Car Inc.
PROJECT:
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
1 80.0-120 0.743 20
1 80.0-120 2.02 20
1 80.0-120 1.43 20
1 80.0-120 1.11 20
SDG: DATE/TIME: PAGE:
L1562113 12/30/22 10:36 10 of 37

WG1968999 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 350.1 L1562118-01
Method Blank (MB)
(MB) R3367974-1 12/04/22 13.55
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/I ug/I ug/I
Ammonia Nitrogen U 117 250
L1561910-04 Original Sample (OS) • Duplicate (DUP)
(OS) L1561910-04 12/04/22 14:02 • (DUP) R3867974-5 12/04/22 14:04
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I %_
Ammonia Nitrogen ND ND 1 0.000 10
L1562006-03 Original Sample (OS) • Duplicate (DUP)
(OS) L1562006-03 12/04/22 14:19 • (DUP) R3867974-7 12/04/22 14:20
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
Ammonia Nitrogen 4480 4430 1 1.17 10
Laboratory Control Sample (LCS)
(LCS) R3867974-2 12/04/22 13:56
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I
Ammonia Nitrogen 7500 7970 106 90.0-110
L1561910-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1561910-03 12/04/22 13:58 • (MS) R3867974-3 12/04/22 13:59 • (MSD) R3867974-4 12/04/22 14:01
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/I ug/I ug/I ug/I
Ammonia Nitrogen 5000 ND 4890 4990 97.9 99.7 1 90.0-110 1.84 10
L1562005-04 Original Sample (OS) • Matrix Spike (MS)
(OS) L1562005-04 12/04/22 14:16 • (MS) R3867974-6 12/04/22 1417
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte ug/I ug/I ug/I
Ammonia Nitrogen 5000 ND 5150 103 1 90.0-110
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1562113 12/30/22 10:36 11 of 37

WG1967977
Wet Chemistry by Method 351.2
Method Blank (MB)
(MB) R3367335-1 12/03/22 14:02
MB Result
Analyte ug/I
Kjeldahl Nitrogen, TKN U
MB Qualifier MB MDL MB RDL
ug/I ug/I
140 250
Laboratory Control Sample (LCS)
(LCS) R3867835-2 12/03/22 14:04
Spike Amount LCS Result
Analyte ug/I ug/I
Kjeldahl Nitrogen, TKN 12700 12500
QUALITY CONTROL SUMMARY
L1562118-01
LCS Rec. Rec. Limits LCS Qualifier
98.4 75.2-120
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1562113 12/30/22 10:36 12 of 37

WG1968838
Wet Chemistry by Method 365.4
Method Blank (MB)
(MB) R3367349-1 12/03/22 14:02
MB Result
Analyte ug/I
Phosphorus, Total U
MB Qualifier MB MDL MB RDL
ug/I ug/I
35.0 100
L1562162-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1562118-01
(OS) L1562162-01 12/03/22 15:07 • (DUP) R3867849-6 12/03/22 15:09
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
Phosphorus, Total 3680 3780 1 2.68 20
Laboratory Control Sample (LCS)
(LCS) R3867849-2 12/03/22 14:03
Spike Amount LCS Result
Analyte ug/I ug/I
Phosphorus, Total 3780 3640
LCS Rec. Rec. Limits LCS Qualifier
96.3 83.2-116
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1562113 12/30/22 10:36 13 of 37

WG1966901 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 420.4 L1562118-01
Method Blank (MB)
(MB) R3367672-1 12/02/22 17:07
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/I ug/I ug/I
Total Phenol by4AAP U 8.30 40.0
L1561702-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1561702-01 12/02/22 17:08 • (DUP) R3867672-3 12/02/22 17:09
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I %_
Total Phenol by4AAP ND ND 1 0.000 20
L1561820-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1561320-01 12/02/22 17:12 • (DUP) R3867672-6 12/02/22 1713
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
Total Phenol by4AAP ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3867672-2 12/02/22 17:08
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I
Total Phenol by4AAP 500 534 107 90.0-110
L1561702-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1561702-01 12/02/22 17:08 • (MS) R3867672-4 12/02/22 17:10 • (MSD) R3867672-5 12/02/22 1711
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/I ug/I ug/I ug/I
Total Phenol by4AAP 1000 ND 756 840 75.6 84.0
1 90.0-110
J6 J6 10.4 20
Sample Narrative:
MS: Matrix spike failure due to matrix.
MSD: Matrix spike failure due to matrix.
ACCOUNT: PROJECT:
SDG:
DATE/TIME: PAGE:
Frit Car Inc.
L1562118
12/30/22 10:36 14 of 37

WG1966901
Wet Chemistry by Method 420.4
QUALITY CONTROL SUMMARY
L1562118-01
L1561820-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1561320-01 12/02/22 1712 • (MS) R3367672-7 12/02/22 1714
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte ug/I ug/I ug/I
Total Phenol by4AAP 1000 ND 910 91.0 1 90.0-110
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1562113 12/30/22 10:36 15 of 37

WG1968391 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 4500H+ B-2011 L1562118-01
L1562649-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1562649-01 12/05/22 14:40 • (DUP) R3363446-2 12/05/22 14:40
Original Result DUP Result Dilution DUP RPD
Analyte su su
pH 6.95 6.95 1 0.000
Sample Narrative:
OS: 6.95 at20.2C
DUP 6.95 at20.1C
L1563179-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1563179-01 12/05/22 14:40 • (DUP) R3868446-3 12/05/22 14:40
Original Result DUP Result Dilution DUP RPD
Analyte su su
pH 8.29 8.31 1 0.241
Sample Narrative:
OS: 8.29 at19.9C
DUP: 8.31 at19.9C
Laboratory Control Sample (LCS)
(LCS) R3868446-1 12/05/22 14:40
Spike Amount LCS Result LCS Rec. Rec. Limits
Analyte su su
pH 10.0 9.91 99.1 99.0-101
Sample Narrative:
LCS: 9.91 at19.8C
DUP Qualifier DUP RPD
Limits
DUP Qualifier DUP RPD
Limits
1
LCS Qualifier
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1562113 12/30/22 10:36 16 of 37

WG1966961
QUALITY CONTROL SUMMARY
Wet Chemistry by Method 5210 B-2016
L1562118-01
Method Blank (MB)
C p
(MB) R3363232-1 12/05/22 1142
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/I ug/I ug/I
ITC]
BOD 1380 131 200 200
FS
L1561589-01 Original Sample (OS) • Duplicate (DUP)
[�n]
(OS) L1561539-01 12/05/22 09:16 • (DUP) R3868232-3 12/05/22 09:18
Original Result DUP Result Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
F
Analyte ug/I ug/I
BOD 5220 4480 1 15.3
30
L1562205-01 Original Sample (OS) • Duplicate (DUP)
GI
(OS) L1562205-01 12/05/22 10:14 • (DUP) R3868232-4 12/05/22 1016
Original Result DUP Result Dilution DUP RPD
DUP Qualifier DUP RPD
1711
Limits
Analyte ug/I ug/I
BOD 153000 152000 1 0.656
30
FSc
Laboratory Control Sample (LCS)
(LCS) R3868232-2 12/05/22 09:14
Spike Amount
LCS Result LCS Rec.
Analyte ug/I
ug/I
BOD 198000
234000 118
Laboratory Control Sample (LCS)
(LCS) R3868232-5 12/05/22 10:27
Spike Amount
LCS Result LCS Rec.
Analyte ug/I
ug/I
BOD 198000
273000 138
Rec. Limits LCS Qualifier
84.6-115 J+
Rec. Limits LCS Qualifier
84.6-115 J+
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1562113 12/30/22 10:36 17 of 37

WG1967456
Wet Chemistry by Method 5310 B-2014
Method Blank (MB)
(MB) R3367339-2 12/01/22 07:27
MB Result
Analyte ug/I
TOC (Total Organic Carbon) 277
MB Qualifier MB MDL MB RDL
ug/I ug/I
J 102 1000
L1562152-05 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1562118-01
(OS) L1562152-05 12/01/22 15:59 • (DUP) R3367339-7 12/01/22 16:14
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
TOC (Total Organic Carbon) ND ND 1 9.13 20
L1562195-05 Original Sample (OS) • Duplicate (DUP)
(OS) L1562195-05 12/01/22 16:31 • (DUP) R3367339-8 12/01/22 16:53
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
TOC (Total Organic Carbon) 1620 1560 1 3.97 20
Laboratory Control Sample (LCS)
(LCS) R3367339-1 12/01/22 0711
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I
TOC (Total Organic Carbon) 75000 74900 99.9 85.0-115
L1561910-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1561910-05 12/01/22 09:14 • (MS) R3367339-3 12/01/22 09:35 • (MSD) R3367339-4 12/01/22 09:55
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec.
Analyte ug/I
ug/I
ug/I
ug/I
TOC (Total Organic Carbon) 50000
ND
59200
59300 117 117
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
1 80.0-120 0.203 20
L1562005-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1562005-01 12/01/22 10:12 • (MS) R3367339-5 12/01/22 10:34 • (MSD) R3367339-6 12/01/22 10:56
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/I
ug/I
ug/I
ug/I
TOC (Total Organic Carbon) 50000
2020
61900
62300 120 120 1 80.0-120 0.628 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1562113 12/30/22 10:36 13 of 37

WG1973597
Metals (ICP) by Method 200.7
Method Blank (MB)
(MB) R3872427-1 12/15/22 1744
MB Result
MB Qualifier MB MDL
MB RDL
Analyte ug/I
ug/I
ug/I
Cadmium U
0.552
2.00
Chromium U
1.63
10.0
Copper U
2.26
10.0
Iron U
20.5
100
Lead U
2.27
5.00
Nickel U
1.82
10.0
Sodium U
444
1000
Zinc U
5.78
50.0
Laboratory Control Sample (LCS)
QUALITY CONTROL SUMMARY
L1562118-01
(LCS) R3872427-2 12/15/22 17:47
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte ug/I
ug/I
Cadmium 1000
970
97.0
85.0-115
Chromium 1000
943
94.3
85.0-115
Copper 1000
955
95.5
85.0-115
Iron 10000
9370
93.7
85.0-115
Lead 1000
970
97.0
85.0-115
Nickel 1000
962
96.2
85.0-115
Sodium 10000
10100
101
85.0-115
Zinc 1000
957
95.7
85.0-115
L1564050-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1564050-01 12/15/22 17:50 • (MS) R3872427-4 12/15/22 17:55 • (MSD) R3872427-5 12/15/22 17:58
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
ug/I
ug/I
ug/I
ug/I
Cadmium
1000
ND
942
1020
94.2
102
1 70.0-130
Chromium
1000
ND
898
972
89.8
97.2
1 70.0-130
Copper
1000
ND
924
1000
92.4
100
1 70.0-130
Iron
10000
ND
9010
9800
90.1
98.0
1 70.0-130
Lead
1000
ND
937
1010
93.7
101
1 70.0-130
Nickel
1000
ND
921
997
92.1
99.7
1 70.0-130
Sodium
10000
27400
36100
38900
87.3
116
1 70.0-130
Zinc
1000
ND
916
993
89.9
97.5
1 70.0-130
MS Qualifier MSD Qualifier RPD RPD Limits
8.28 20
7.84 20
8.12 20
8.42 20
7.61 20
7.91 20
7.53 20
7.99 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1562113 12/30/22 10:36 19 of 37

WG1973597 QUALITY CONTROL SUMMARY
Metals (ICP) by Method 200.7 L1562118-01
L1564051-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1564051-01 12/15/22 13 01 • (MS) R3372427-6 12/15/22 13 03 • (MSD) R3372427-7 12/15/22 13 06
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
ug/I
ug/I
ug/I
ug/I
Cadmium
1000
ND
906
992
90.6
99.2
Chromium
1000
ND
861
947
86.1
94.7
Copper
1000
ND
886
979
88.6
97.9
Iron
10000
ND
8690
9600
86.9
96.0
Lead
1000
ND
892
983
89.2
98.3
Nickel
1000
ND
879
968
87.9
96.8
Sodium
10000
26000
36000
36700
99.8
107
Zinc
1000
ND
877
962
87.7
96.2
ACCOUNT:
Frit Car Inc.
PROJECT:
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 70.0-130
9.04
20
1 70.0-130
9.47
20
1 70.0-130
10.0
20
1 70.0-130
9.88
20
1 70.0-130
9.66
20
1 70.0-130
9.61
20
1 70.0-130
1.90
20
1 70.0-130
9.33
20
SDG:
DATE/TIME:
PAGE:
L1562113
12/30/22 10:36
20 of 37

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contactyour project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
u
Fc
Fss]
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
Fn
RDL
Reported Detection Limit.
Rec.
Recovery.
Fr
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
U
Not detected at the Reporting Limit (or MDL where applicable).
Fc
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
F
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
LEI
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
31
The blank depletion was greater than the recommended maximum depletion of 0.2mg/L.
J
The identification ofthe analyte is acceptable, the reported value is an estimate.
J3
The associated batch QC was outside the established quality control range for precision.
J6
The sample matrix interfered with the ability to make any accurate determination, spike value is low.
J+
The associated batch QC was outside the upper control limits, associated data has a potential positive bias.
K5
The Dilution water D.O. depletion was > 0.2 mg/L.
K8
Glucose/glutamic acid BOD/CBOD was above method acceptance levels.
K9
Test replicates show more than 30% difference between high and low values.
P1
RPD value not applicable for sample concentrations less than 5 times the reporting limit.
T8
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc.
L1562113 12/30/22 10:36 21 of 37

ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
Nebraska
N E-OS-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TNO02
California
2932
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704 _
Georgia
NELAP
North Carolina 3
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky' 6
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee'"
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas5
LABO152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A2 LA
A2LA— ISO17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
FP
Fc
FS-S
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME:
Frit Car Inc. L1562113 12/30/22 10:36
PAGE:
22 of 37

Company Name/Address:
Billing Information.
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Frlt Car Inc.
Accounts Payable LPChk'
Box 1344
2412 U5 Hwy 17N
Brewton, AL 36427
ace,
New Bern, NC 28564
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PaceAnalyfical
Report of Analysis
Pace Analytical LLC
12065 Lebanon Rd.
Mt. Juliet, TN 37122
Attention: Heather Wagner
Project Name: Bridgeton Facility Monthly
Project Number: WG1968582
Lot Number:XK30021
Date Completed:12/09/2022
12/10/2022 10:35 AM
Approved and released by:
Project Coordinator 1: Jenna S. Holliday
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page Iof14

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Pace Analytical LLC
Lot Number: XK30021
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Additionally, the
DoD QSM version 5.4 has been followed for these samples. Any exceptions to the TNI standards, the
Laboratory Quality Manual, SOPs, the DoD QSM, or policies are qualified on the results page or
discussed below.
Pace is a DoD/DOE accredited laboratory; however, the following analyses are currently not listed on our
DoD/DOE scope of accreditation: Drinking Water: pH EPA 150.1, Turbidity EPA 18.01, Metals EPA 200.7
& 200.8, Mercury EPA 245.1, Anions EPA 300.0, Cyanide EPA 335.4, Nitrates EPA 353.2,
Orthophosphate & Phosphorus EPA 365.1, EDB/DBCP EPA 504.1, HPC SIMPLATE, Color SM 2120 B-
2011, Alkalinity SM 2320 B-2011, Specific Conductance SM 2510 B-2011, Residue -filterable (TDS) SM
2540 C, Calcium Hardness (CaCO2) SM 3500-Ca B-2011, TRC SM 4500 Cl G-2011, pH SM 4500 H=B-
2011, E.Coli, Total Coliform; Non -Potable Water: Metals EPA 200.7, Strontium EPA 200.8, Chlorate EPA
300.0, Cyanide EPA 335.4, Phenolics EPA 420.4, 2-Methyl-4,6-Dinitrophenol EPA 625.1, Propane RSK-
175, Specific Conductance SM 2510 B-2011, Salinity SM250 B, Residue- total SM 2540 B, Sulfite SM
4500 SO32- B-2011, Amenable Cyanide SM 4500-CN- G-2011, BOD & CBOD SM 5210 B, MBAS SM
5540 C-2011; Solid and Chemical Materials: Boron & Titanium SW-846 601 OD, Boron, Molybdenum, &
Titanium SW-846 6020B, Alcohols & Glycols SW-846 8015C, Pentachlorophenol SW-846 8151A, Ethyl
Acetate, Hexane, & n-Hexane SW-846 8260D, SVOC 1,4-Dioxane, 3&4-Methylphenols, 4-Dimethyl
aminoazobenzene, 1,4-Naphthoquinone, 3,5-Dinitroaniline, PETN SW-846 8270E, Amenable Cyanide
SW-846 901213; Boron & Titanium SW-846 601 OD, Molybdenum SW-846 6020B, Ethylene Glycol SW-
846 8015B, Pentachlorophenol SW-846 8151A, Chloroprene SW-846 8260B, SVOC 1,3,5-
Trinitrobenzene, 1,4-Dioxane, 1,4-Naphthoquinone, 1,4-Phenylenediamine, 2,5-Dinitrotoluene, 2,6-
Dinitrotoluene, 3-Methylcholanthrene, 4- Aminobiphenyl, 4-Dimethyl aminoazo benzene, 4-Nitroquinoline-
1-oxide, 7,12- Dimethylbenzo(a)anth race ne, Chlorobenzilate, Diallate, Ethyl methanesulfonate, Isodrin,
Isosafrole, Methyl methanesulfonate, n-Nitrosomethylethylamine, n-Nitrosomorpholine, n-
Nitrosopiperidine, Piperonyl butoxide, Pronamide, Safrole, 3,5-Dinitroaniline, PETN SW-846 8270E, Oil &
Grease SW-846 9071 B.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 14

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
Orthophosphate Analysis
The matrix spike (MS) and matrix spike duplicate (MSD) for batch 61355 recovered outside of the
acceptance limits. The associated laboratory control sample (LCS) passed acceptance criteria. Therefore,
the data has been reported.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvww.pacelabs.com
Page 3of14

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Pace Analytical LLC
Lot Number: XK30021
Project Name: Bridgeton Facility Monthly
Project Number: WG1968582
Sample Number Sample ID Matrix Date Sampled Date Received
001 Effluent Aqueous 11/29/20221600 11/30/2022
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 14

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Pace Analytical LLC
Lot Number: XK30021
Project Name: Bridgeton Facility Monthly
Project Number: WG1968582
Sample Sample ID Matrix Parameter Method Result Q Units Page
(0 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 14

Inorganic non-metals
Client: Pace Analytical LLC Laboratory ID:XK30021-001
Description: Effluent Matrix: Aqueous
Date Sampled:11/29/2022 1600 Project Name: Bridgeton Facility Monthly
Date Received:11/30/2022 Project Number: WG1968582
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Orthophospha) 365.1 1 11/30/2022 1828 DMA 61355
CAS Analytical
Parameter Number Method Result Q LOQ LOD DL Units Run
Orthophosphate
365.1 0.050 US 0.050 0.050 0.050 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
U = Not detected at or above the LOD N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis LOD = Limit of Detection S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 14

QC Summary
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: XK30021
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 14

Inorganic non-metals - MB
Sample ID: XQ61355-001 Matrix: Aqueous
Batch:61355
Analytical Method: 365.1
Parameter Result Q Dil LOQ LOD DL Units Analysis Date
Orthophosphate 0.050 U 1 0.050 0.050 0.050 mg/L 11/30/20221828
LOQ = Limit of Quantitation U = Not detected at or above the LOD N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
LOD = Limit of Detection = RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: XK30021
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 14

Inorganic non-metals - LCS
Sample ID: XQ61355-002 Matrix: Aqueous
Batch:61355
Analytical Method: 365.1
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Orthophosphate 0.25 0.24 1 95 90-110 11/30/20221828
LOQ = Limit of Quantitation U = Not detected at or above the LOD N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
LOD = Limit of Detection = RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: XK30021
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 14

Inorganic non-metals - MS
Sample ID: XK30021-001 MS Matrix: Aqueous
Batch: 61355
Analytical Method: 365.1
Sample Spike
Amount Amount Result %Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Orthophosphate ND 0.25 0.022 N 1 8.7 90-110 11/30/20221828
LOQ = Limit of Quantitation U = Not detected at or above the LOD N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
LOD = Limit of Detection = RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: XK30021
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 14

Inorganic non-metals - MSD
Sample ID: XK30021-001MD Matrix: Aqueous
Batch: 61355
Analytical Method: 365.1
Sample Spike
Amount Amount Result %Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Orthophosphate ND 0.25 0.022 N 1 8.7 0.18 90-110 20 11/30/20221828
LOQ = Limit of Quantitation U = Not detected at or above the LOD N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
LOD = Limit of Detection = RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: XK30021
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 14

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 14

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of 14

PACE ANALYTICAL SERVICES, LLC
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Elyl
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rexichmi cbkri e?
Yes
R] NO
❑N,
18- Was Flit quote rRijuber lis4ed ou flx cautairiff iabel7 If yes, Qaote it
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coaJUtients:
Qua rax ID; 56380 paces Ana ytical Services, LLC Page 1 &I
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
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