WQ0002503_Monitoring - 07-2022_20230113

Monitoring Report Submittal
Permit Number #*
Name of Facility:*
Month: * July
Report Information
WQ0002503
FRIT CAR, INC.
Type *
NDMR, NDAR-1, NDAR-2, NDMLR
G W-59
Confirmation Email Address:*
Name of Submitter: *
Signature:
Date of submittal:
Initial Review
[e-mail]
Connie Pettis
O
Year:* 2022
Upload Document*
NDAR-NDMR JULY 2022.pdf 4.09MB
PDF Only
2022-07 GW59.pdf 4.88MB
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-7, NDAR-2, NDMLR, GW-59).
1 /13/2023
This will be filled in automatically

Reviewer: Gerald, Wanda
Is the project number correct?* WQ0002503
Is the monitoring report accepted?* Yes No
Regional Office* Washington
Reviewer: _anonymous
Review Date: 2/6/2023

FORM: NEAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-'I) Page
Permit • 111/01
County: Craven
,
irrigation occur
at this facility?
■-
Crop:Did
Cover
�•
Crop-
YESCover
NO
r-M
Hourlyr
Hourly
Annual Rate (in)::
Annual &ate (in):
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1 11
1

FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page of
Did the application rates exceed the limits in Attachment B of your permit?
0 Compliant
❑ Non -Compliant
Were adequate measures taken to prevent effluent ponding in or runoff from the sites?
0 Compliant
❑ Non -Compliant
Was a suitable vegetative cover maintained on a[] sites as specified in your permit?
[Z Compliant
❑ Non -Compliant
Were all setbacks listed in your permit maintained for every application to each permitted site?
Q Compliant
❑ Non -Compliant
Were all freeboards maintained in accordance with the specified freeboard heights in your permit?
Q Compliant
❑ Non -Compliant
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective
action(s) taken. Attach additional sheets if necessarv.
Operator in Responsible Charge (ORC) Certification Permittee Certification
ORC: Danny Hornbeck Permittee:
Frit Car, Inc.
Certification No.: 26718 Signing Official: Michael Newby
Grade: Phone Number: 252-638-2675 Signing Official's Title: Senior Vice President
Has the ORG changed since the previous NDAR-1? ❑ Yes 0 No Phone Numb . 251-867-7752 Permit Exp.: 6/30/22
Signature i ✓ date 11 Ignature Date
By this signature, I certify that this report is accurrate and complete to the best of my knowledge. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
Mail Original and Two Copies to:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617

FORM: NDMR 07-13 NON -DISCHARGE MONITORING REPORT (NDMR) Page
Permit No.: WQ0002503
Facility Name: Frit Car, Inc.
County: Craved
Month: July
Year: 2022
PPI:
Flow Measuring Point: ❑ influent ❑� Effluent ❑ No flow generated
Parameter Monitoring Point: ❑ Influent ❑✓ Effluent ❑ Groundwater Lowering E Surface Water
Parameter Code -►
50050
00400
00945
00310
00940
C0665
00610
00680
00660
00929
70300
C0530
01034
01045
32730
01092
T
f3
-
Qv
d+
0
O
E �
F-
V
0
u
:
N
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m
r
V
= r
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to V
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Q
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(0 V
o
F
[
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a
t9
~ N to
n
O
N
y
l
E
U
C
o
-
N
O
a
U
N
24-hr
hrs
GPD
I su
mg/L
mg1L
mg/L
mg/L
mg1L
mg1L
mglL
mg1L
mglL
mg1L
mg/L
mg/L
mglL
mg[L
1
07:00
8
6.26
1310
<2.00
6400
453
172
17.5
0.22
8670
23000
896
0,243
19
<.04
1.74
2
3
4
5
07:00
07:00
8
8
&
07:00
8
70
7
1 07:00
8
8
1 07:00
8
70
9
10
11
07:00
8
12
07:00
8
140
13
07:00
8
14
07:00
8
15
07:00
8
16
17
181
19
07:00
07:00
8
8
20
07:00
8
21
22
07:00
07:00
8
8
23
24
25
07:00
8
26
07:00
8
27
07:00
8
28
07:00
8
29
07:00
8
30
31
Average:
93
1,310.00
0.00
6,400.00
453.00
172.00
17.50
0.22
8,670.00
23,000.00
896.00
0.24
19.00
0.00
1.74
Daily Maximum:
140
6.26
1,310.00
2.00
6,400.00
453.00
172.00
17.50
0.22
8,670.00
23,000.00
896.00
0.24
19.00
0.04
1.74
Daily Minimum:
Sampling Type:
70
6.26
1,310.00
2.00
6,400.00
453.00
172.00
17.50
0.22
8,670.00
23,000.00
896.00
0.24
19.00
0.04
1.74
Monthly Avg. Limit:
Daily Limit:
Sample Frequency:

FORM: NDMR 07-13 NON -DISCHARGE MONITORING REPORT (NDMR) Page __ of
Permit No.: VV00002503
Facility Name: Frit Car, Inc.
County: Craven
Month: July
Year: 2022
PPI: Flow Measuring
Point: ❑ Influent ❑✓ Effluent ❑ No flaw generated Parameter
Monitoring Point: ❑ influent
0 Effluent ❑ Groundwater Lowering
❑ Surface Water
Parameter Code — 10 50050
01027 00625 01042 01051 01067 00620 00600
c
a
y
a c
co
a
0
RoU
�
F
W
0
O
}-
24-hr
hrs
GPD
mg/L
mg/L
mg1L
mg/L
mglL
mg/L
mg/L
1
0.054
171
0.181
<.05
1.88
18.4
168
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
Average:
#DIV10?
0.05
171.00
0.18
0.00
1.88
18.40
168.00
Daily Maximum:
0
0.05
171.00
0.18
0.05
1.88
18.40
168.00
Daily Minimum:
0
0.05
171,00
0.18
6.05
1.88
18.40
168.00
Sampling Type:
Monthly Avg. Limit:
Daily Limit:
Sample Frequency:

FORM: NDMR 07-13 NON -DISCHARGE MONITORING REPORT (NDMR) Page of
Sampling Person(s) Certified Laboratories
Name: Danny Hornbeck Name: Pace Analytical
Name: Name:
Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? 0 compliant ❑ Non -compliant
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective
action(s) taken. Aftach addltlnn Al shppic if narpcc
Operator in Responsible Charge (ORC) Certification Permittee Certification
ORC: Danny Hornbeck Permittee: Frit Car, Inc.
Certification No.: 26718 Signing Official: Michael Newby
Grade: Phone Number: 252-638-2675 Signing Official's Title: Senior Vice President
Has the ORC changed since the previous NDMR? ❑ Yes 0 No Phone Num 251-867-7752 Permit Expiration: 2/28/2029
r
Signature Date Signature Date
By this signature, I certify that this report is accurrate and complete to the best of my knowledge. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on
my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
Mail Original and Two Copies to:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center

(� ace Analytical
11
ANALYTICAL REPORT
October 31, 2022
Frit Car Inc.
Sample Delivery Group: L1543726
Samples Received: 10/06/2022
Project Number:
Description: Bridgeton Facility Monthly (PARTIAL)
Report To: Connie Pettis
2012 US Hwy 17N
New Bern, NC 28560
Entire Report Reviewed By: q�"h
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1543726 10/31/22 13:47 1 of 13

TABLE OF CONTENTS
Cp: Cover Page
u
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
,i
FSSI
EFFLUENT L1543726-01
5
Fn
Qc: Quality Control Summary
Wet Chemistry by Method 350.1
Fr
Wet Chemistry by Method 351.2
8
Wet Chemistry by Method 353.2
9
Rc
Metals (ICP) by Method 200.7
F
GI: Glossary of Terms
11
.d: Accreditations & Locations
12
[Al
Sc: Sample Chain of Custody
13
RC
ACCOUNT: PROJECT:
SDG: DATE/TIME:
PAGE:
Frit Car Inc.
L1543726 10/31/22 13:47
2 of 13

SAMPLE SUMMARY
Collected by Collected date/time Received date/time
EFFLUENT L1543726-01 WW Danny Hornbeck 10/05/2215:40 10/06/22 09:00 , C
P
Method
Calculated Results
Wet Chemistry by Method 350.1
Wet Chemistry by Method 351.2
Wet Chemistry by Method 353.2
Metals (ICP) by Method 200.7
Batch
Dilution
Preparation
Analysis
Analyst
date/time
date/time
WG1940735
1
10/28/2215:45
10/28/2215:45
JD
WG1940472
20
10/11/2213:09
10/11/2213:09
BMD
WG1950337
20
10/28/22 09:45
10/28/2215:45
LDT
WG1940735
10
10/12/2214:18
10/12/2214:18
JCS
WG1944096
10
10/21/2216:38
10/25/22 05:47
CCE
Location
FC
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fn
Fr
Rc
F,
F
RC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1543726 10/31/22 13:47 3 of 13

CASE NARRATIVE
FP
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
0
Fr
Rc
4�z
F,
Heather J Wagner
Project Manager
[Al
RC
Sample Delivery Group (SDG) Narrative
The following analysis were performed from an unpreserved, insufficiently or inadequately preserved sample.
Lab Sample ID Project Sample ID Method
L1543726-01 EFFLUENT 353.2, 351.2
ACCOUNT: PROJECT: SDG: DATE/TIME:
PAGE:
Frit Car Inc. L1543726 10/31/22 13:47
4 of 13

SAMPLE RESULTS - 01
L1543726
EFFLUENT
Collected date/time: 10/05/22 15:40
Calculated Results
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date / time
Total Nitrogen 190000
1000
1 10/28/2022 15:45 WG1940735
Wet Chemistry by Method 350.1
Result
Qualifier RDL
Dilution Analysis Batch
Analyte ug/I
ug/I
date / time
Ammonia Nitrogen 168000
5000
20 10/11/202213:09 WG1940472
Wet Chemistry by Method 351.2
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date / time
Kjeldahl Nitrogen, TKN 171000 J5 5000 20 10/28/2022 15:45 WG1950337
Wet Chemistry by Method 353.2
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date / time
Nitrate -Nitrite 18400 1000 10 10/12/202214:18 WG1940735
Metals (ICP) by Method 200.7
Result
Qualifier RDL
Analyte
ug/I
ug/I
Cadmium
54.0
20.0
Copper
181
100
Lead
ND
50.0
Nickel
1880
100
Zinc
1740
500
Dilution
Analysis
Batch
date / time
10
10/25/2022 05:47
WG1944096
10
10/25/2022 05:47
WG1944096
10
10/25/2022 05:47
WG1944096
10
10/25/2022 05:47
WG1944096
10
10/25/2022 05:47
WG1944096
— FP
— Fc
FS
—
Fn—
—
Rc
�GI
[Al
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1543726 10/31/22 13:47 5 of 13

WG1940472 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 350.1 L1543726-01
Method Blank (MB)
(MB) R3347306-1 10/11/22 12:49
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/I ug/I ug/I
Ammonia Nitrogen U 117 250
L1543670-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1543670-01 10/11/22 12:57 • (DUP) R3347306-5 10/11/22 12:58
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I %_
Ammonia Nitrogen ND ND 1 0.000 10
L1543746-07 Original Sample (OS) • Duplicate (DUP)
(OS) L1543746-07 10/11/22 13:21 • (DUP) R3347306-9 10/11/22 13:22
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
Ammonia Nitrogen 35500 35300 10 0.619 10
Laboratory Control Sample (LCS)
(LCS) R3847306-2 10/11/22 12:51
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I
Ammonia Nitrogen 7500 7300 97.3 90.0-110
L1543661-12 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1543661-12 10/11/22 12:52 • (MS) R3347306-3 10/11/22 12:54 • (MSD) R3347306-4 10/11/22 12:55
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/I ug/I ug/I ug/I
Ammonia Nitrogen 5000 3180 7770 7890 91.8 94.2 1 90.0-110 1.56 10
L1543746-06 Original Sample (OS) • Matrix Spike (MS)
(OS) L1543746-06 10/11/22 13:50 • (MS) R3347306-10 10/11/22 13:51
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte ug/I ug/I ug/I
Ammonia Nitrogen 100000 118000 208000 89.2 20 90.0-110 E J6
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1543726 10/31/22 13:47 6 of 13

W G1940472
Wet Chemistry by Method 350.1
QUALITY CONTROL SUMMARY
L1543726-01
L1543746-06 Original Sample (OS) • Matrix Spike (MS)
(OS) L1543746-06 10/11/22 13:50 • (MS) R3347306-10 10/11/22 13:51
Spike Amount Original Result MS Result MS Rec.
Analyte ug/I _ ug/I ug/I
Sample Narrative:
MS: Matrix spike failure due to matrix interference.
Dilution Rec. Limits MS Qualifier
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1543726 10/31/22 13:47 7 of 13

WG1950337
Wet Chemistry by Method 351.2
Method Blank (MB)
(MB) R3354367-1 10/23/22 15:43
MB Result
Analyte ug/I
Kjeldahl Nitrogen, TKN U
MB Qualifier MB MDL MB RDL
ug/I ug/I
140 250
L1543726-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1543726-01
(OS) L1543726-01 10/23/22 15:45 • (DUP) R3854367-3 10/23/22 15:47
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
Kjeldahl Nitrogen, TKN 171000 180000 20 4.89 20
Laboratory Control Sample (LCS)
(LCS) R3854367-2 10/28/22 15:44
Spike Amount LCS Result LCS Rec.
Analyte ug/I ug/I
Kjeldahl Nitrogen, TKN 12700 13900 109
Rec. Limits LCS Qualifier
75.2-120
L1543726-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1543726-01 10/23/22 15:45 • (MS) R3854367-4 10/23/22 15:48 • (MSD) R3854367-5 10/23/22 15:50
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec.
Analyte ug/I
ug/I
ug/I
ug/I
Kjeldahl Nitrogen, TKN 100000
171000
268000
294000 96.6 123
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
20 90.0-110 J5 9.25
RPD Limits
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1543726 10/31/22 13:47 3 of 13

WG1940735
Wet Chemistry by Method 353.2
Method Blank (MB)
(MB) R3347634-1 10/12/22 1415
MB Result
Analyte ug/I
Nitrate -Nitrite U
MB Qualifier MB MDL MB RDL
ug/I ug/I
50.0 100
L1543733-03 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1543726-01
(OS) L1543733-03 10/12/22 14:21 • (DUP) R3847684-3 10/12/22 14:23
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
Nitrate -Nitrite 2570 2550 1 0.781 20
L1543866-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1543366-01 10/12/22 14:37 • (DUP) R3847684-6 10/12/22 14:38
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
Nitrate -Nitrite 647 643 1 0.620 20
Laboratory Control Sample (LCS)
(LCS) R3847684-2 10/12/22 1416
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I
Nitrate -Nitrite 2500 2600 104 90.0-110
L1543733-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1543733-03 10/12/22 14:21 • (MS) R3847684-4 10/12/22 14:24 • (MSD) R3847684-5 10/12/22 14:25
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/I ug/I ug/I ug/I
Nitrate -Nitrite 2500 2570 4910 4960 93.6 95.6 1 90.0-110 1.01 20
L1543866-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1543366-01 10/12/22 14:37 • (MS) R3847684-7 10/12/22 14:39
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte ug/I ug/I ug/I
Nitrate -Nitrite 2500 647 3140 99.7 1 90.0-110
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1543726 10/31/22 13:47 9 of 13

WG1944096
Metals (ICP) by Method 200.7
Method Blank (MB)
(MB) R3352423-1 10/24/22 20:07
MB Result
Analyte
ug/I
Cadmium
U
Copper
U
Lead
U
Nickel
U
Zinc
U
MB Qualifier MB MDL
ug/I
0.552
2.26
2.27
1.82
5.78
Laboratory Control Sample (LCS)
(LCS) R3852423-2 10/24/22 20:09
Spike Amount
LCS Result
Analyte
ug/I
ug/I
Cadmium
1000
1020
Copper
1000
1050
Lead
1000
1030
Nickel
1000
1020
Zinc
1000
1020
LCS Rec.
102
105
103
102
102
QUALITY CONTROL SUMMARY
L1543726-01
MB RDL
ug/I
2.00
10.0
5.00
10.0
50.0
Rec. Limits LCS Qualifier
85.0-115
85.0-115
85.0-115
85.0-115
L1542837-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1542337-01 10/24/22 20:12 • (MS) R3852423-4 10/24/22 20:18 • (MSD) R3852423-5 10/24/22 20 20
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
ug/I
ug/I
ug/I
ug/I
Cadmium
1000
ND
1020
1020
102
102
Copper
1000
ND
1030
1030
103
102
Lead
1000
ND
1030
1020
103
102
Nickel
1000
ND
1020
1020
102
102
Zinc
1000
ND
1000
1010
100
101
L1543871-13 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
Dilution Rec. Limits
70.0-130
70.0-130
70.0-130
70.0-130
70.0-130
MS Qualifier MSD Qualifier RPD
0.350
0.431
0.234
0.163
0.324
RPD Limits
20
20
20
20
20
(OS) L1543371-13 10/24/22 20:23 • (MS) R3852423-6 10/24/22 20:26 • (MSD) R3852423-7 10/24/22 20:29
Spike Amount
Original Result
MS Result
MSD Result MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte
ug/I
ug/I
ug/I
ug/I
Cadmium
1000
ND
1040
1050 104
105
1 70.0-130
0.437
20
Copper
1000
ND
1000
1020 99.8
102
1 70.0-130
2.14
20
Lead
1000
ND
997
1010 99.7
101
1 70.0-130
1.48
20
Nickel
1000
ND
1000
1020 99.3
101
1 70.0-130
1.87
20
Zinc
1000
ND
974
984 97.4
98.4
1 70.0-130
1.09
20
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Frit Car Inc.
L1543726
10/31/22 13:47
10 of 13

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contactyour project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
u
Fc
Fss]
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
Fn
RDL
Reported Detection Limit.
Rec.
Recovery.
Fr
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
U
Not detected at the Reporting Limit (or MDL where applicable).
Fc
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
F
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
LEI
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
E
The analyte concentration exceeds the upper limit ofthe calibration range ofthe instrument established by the initial
calibration (ICAL).
J5
The sample matrix interfered with the abilityto make any accurate determination, spike value is high.
J6
The sample matrix interfered with the abilityto make any accurate determination, spike value is low.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc.
L1543726 10/31/22 13:47 11 of 13

ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
Nebraska
N E-OS-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TNO02
California
2932
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704 _
Georgia
NELAP
North Carolina 3
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky' 6
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee'"
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas5
LABO152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A2 LA
A2LA— ISO17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
FP
Fc
FS-S
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME:
Frit Car Inc. L1543726 10/31/22 13:47
PAGE:
12 of 13

Frit Car Inc-
Billing lnfarmatlor-
Pres
Accounts Payable
Analysis /
Container/ Preservative
Chain of Custody Page _of
*ESC
2012 US Hwy 17N
Chk
PO Box 1340
New Bern, NC 28560
Brewton, AL36427
L.A.e $.C.,..N.C.e.$
Report to:
U065 Lebanon Rd
Email To:
Connie Pettis
[e-mail]
Mount Juliet, TN 31222Phone:
615-7nR-59$a -
i Phone: 80o-767-5859
Project
Project —
City/State
Bridgeton Facility Monthly (PARTIAL)
Collected:
—
/
/
Phone: 2$2-638-67$2
Client Project #
Lab Project #
Fax:
FRITINCNBNC-MONTHLY
o
C124
(a,7'8-5859Descf
Collected by 1prnt)
Site/facility ID N
P.O. #
.+
N 0
:FRITINCNBNC
e:T131137
jj
Collected by (signature):
RUShI (Lab MUST Be Notified) Quote #
Same Day _ Five Day
�
i
? ' Prelogin:
Next Day _ 5 Day (Rad Only) Date Results Needed
=
Y
TSR:Heather Wagner
Immediately /
_ Two Day 10 Day {Rad Onlyl No
Packed on Ice INY (�
_ Tbree Day of
f —
I I
i PB:
Via. Shipped ,
RP
Sample ID
Comp/Gras
MatrixDepth
Date
Time
ntrs
1
I
LiE
I i
I i
i
.0
]
l
* Matrix:Remarks:
a ni R nT x mm
` 3c_ "' 17,z r n=
SS - SOR AIR - Air F - Filter
pH Temp
GW - Groundwater B - Bioassay�.-
WW - WasteWater
—., _ :lc.v Other .. _
Co Yec L b L ins us�c : ✓_
DW - Drinking Water
Samples returned via:
OT - Other
—UPS _ FedEx —Courier Tracking Y f982- J✓ "y �$ 79
uu`
/
-- -
Pre Pr,a i7Pfdspaia
Relinquished by: (Signature)
Date:
Time:
Received by: (Signature) 1Yrip
Biank Received: YHC
FBA! �
eoH
TSR
- - -
Relinquished by : (Signature)
Date:
Time:
Received by: (Signature)
;p. oC Banies Receired:
If preservation required by Login: Date/Time
iT
Relinquished by: (Signature)
Date:
Time:
fiec ed for lab by: ISignaturel
Dat : Time:
{�
Hold: Condit:
NCF j CIK

(� ace Analytical
13
ANALYTICAL REPORT
August 26, 2022
Frit Car Inc.
Sample Delivery Group: L152O266
Samples Received: 07/30/2022
Project Number:
Description: Bridgeton Facility Monthly
Report To: Danny Hornbeck
2012 US Hwy 17N
New Bern, NC 28560
Entire Report Reviewed By: q�"h
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy ofthe information provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1520266 03/26/22 11:37 1 of 20

TABLE OF CONTENTS
Cp: Cover Page
u
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
FSSI
EFFLUENT L1520266-01
5
Fn
Qc: Quality Control Summary
7
Gravimetric Analysis by Method 2540 C-2011
7
Fr
Gravimetric Analysis by Method 2540 D-2015
8
Wet Chemistry by Method 300.0
9
Rc
Wet Chemistry by Method 350.1
10
F
Wet Chemistry by Method 365.4
11
Wet Chemistry by Method 420.4
12
[Al
Wet Chemistry by Method 4500H+ B-2011
13
Wet Chemistry by Method 4500P E-2011
14
RC
Wet Chemistry by Method 5210 B-2016
15
Wet Chemistry by Method 5310 B-2014
16
Metals (ICP) by Method 200.7
17
GI: Glossary of Terms
18
Al: Accreditations & Locations
19
Sc: Sample Chain of Custody
20
ACCOUNT: PROJECT: SDG:
DATE/TIME:
PAGE:
Frit Car Inc. L1520266
03/26/22 11:37
2 of 20

SAMPLE SUMMARY
EFFLUENT L1520266-01 WW
Collected by
Danny Hornbeck
Collected date/time
07/29/2214:30
Received date/time
07/30/22 08:45
FP
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
F
Gravimetric Analysis by Method 2540 C-2011
WG1905588
1
08/04/2216:39
08/04/2217:37
SLP
Mt. Juliet, TN
Gravimetric Analysis by Method 2540 D-2015
WG1905544
1
08/04/221121
08/04/2214:25
AEC
Mt. Juliet, TN
Wet Chemistry by Method 300.0
WG1903229
100
07/30/22 22:03
07/30/22 22:03
ELN
Mt. Juliet, TN
Wet Chemistry by Method 350.1
WG1905192
20
08/04/2213:35
08/04/2213:35
SL
Mt. Juliet, TN
Wet Chemistry by Method 365.4
WG1910113
250
08/04/22 08:28
08/12/2215:51
LDT
Mt. Juliet, TN
Fn
Wet Chemistry by Method 420.4
WG1907905
1
08/10/22 09:31
08/10/2217:43
CAT
Mt. Juliet, TN
Wet Chemistry by Method 4500H+ B-2011
WG1905171
1
08/04/2212:00
08/04/2212:00
SIDE
Mt. Juliet, TN
Wet Chemistry by Method 4500P E-2011
WG1903699
1
08/01/22 09:23
08/01/22 09:23
EPW
Mt. Juliet, TN
Fr
Wet Chemistry by Method 5210 B-2016
WG1903258
10
07/30/2215:08
08/04/221102
KFO
Mt. Juliet, TN
Wet Chemistry by Method 5310 B-2014
WG1909551
1
08/22/22 20:52
08/22/22 20:52
BGM
Mt. Juliet, TN
Rc
Metals (ICP) by Method 200.7
WG1907171
1
08/11/22 08:36
08/11/2218:34
ZSA
Mt. Juliet, TN
Metals (ICP) by Method 200.7
WG1907171
10
08/11/22 08:36
08/12/22 03:00
CCE
Mt. Juliet, TN
GI
SAI
RC
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Frit Car Inc.
L1520266
03/26/22 11:37
3 of 20

CASE NARRATIVE
FP
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
0
Fr
Rc
4�z
F,
Heather J Wagner
[Al
Project Manager
RC
Project Narrative
Method 4500P E-2011: The ortho phosphate analysis was performed out of hold due to laboratory error.
Sample Delivery Group (SDG) Narrative
The following analysis were performed from an unpreserved, insufficiently or inadequately preserved sample.
Lab Sample ID Project Sample ID Method
L1520266-01 EFFLUENT 5310 B-2014
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1520266 03/26/22 11:37 4 of 20

EFFLUENT SAMPLE RESULTS - 01
Collected date/time: 07/29/22 14:30 L1520266
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date / time
Dissolved Solids 23000000 400000
1 08/04/2022 17:37 WG1905588
Gravimetric Analysis by Method 2540 D-2015
Result Qualifier RDL
Dilution Analysis Batch
Analyte ug/I ug/I
date / time
Suspended Solids 896000 25000
1 08/04/2022 14:25 WG1905544
Wet Chemistry by Method 300.0
Result
Qualifier RDL
Dilution
Analysis
Batch
Analyte ug/I
ug/I
date / time
Chloride 6400000
100000
100
07/30/2022 22:03
WG1903229
Sulfate 1310000
500000
100
07/30/2022 22:03
WG1903229
Wet Chemistry by Method 350.1
Result
Qualifier RDL
Dilution
Analysis
Batch
Analyte ug/I
ug/I
date / time
Ammonia Nitrogen 172000
5000
20
08/04/2022 13:35
WG1905192
Wet Chemistry by Method 365.4
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date / time
Phosphorus, Total 453000
Wet Chemistry by Method 420.4
25000 250 08/12/202215:51 WG1910113
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date / time
Total Phenol by4AAP ND 40.0 1 08/10/202217:43 WG1907905
Wet Chemistry by Method 4500H+ B-2011
Result Qualifier Dilution Analysis Batch
Analyte su date / time
pH 6.26 T8 1 08/04/202212:00 WG1905171
Sample Narrative:
L1520266-01 WG1905171: 6.26 at 23.2C
Wet Chemistry by Method 4500P E-2011
Result Qualifier RDL
Analyte ug/I ug/I
Phosphate,Ortho 220 J6 Q 30.0
Wet Chemistry by Method 5210 B-2016
Result Qualifier
RDL
Analyte
ug/I
ug/I
BOD
ND K1
2000
Wet Chemistry by Method 5310 B-2014
Result Qualifier
RDL
Analyte
ug/I
ug/I
TOC (Total Organic Carbon)
17500
1000
Dilution Analysis Batch
date / time
1 08/01/2022 09:23 WG1903699
Dilution Analysis Batch
date / time
10 08/04/20221102 WG1903258
Dilution Analysis Batch
date / time
1 08/22/2022 20:52 WG1909551
— FP
- FC
FS
-
Fn-
-
Rc
R,
— [Al
- RC
ACCOUNT:
Frit Car Inc.
PROJECT: SDG: DATE/TIME: PAGE:
L1520266 03/26/22 11:37 5 of 20

EFFLUENT
Collected date/time: 07/29/22 14:30
Metals (ICP) by Method 200.7
SAMPLE
RESULTS - 01
L1520266
Result
Qualifier RDL Dilution Analysis
Batch
F
Analyte ug/I
ug/I
date / time
Chromium 243
10.0 1
08/11/202218:34
WG1907171
F
Iron 19000
100 1
08/11/202218:34
WG1907171
Sodium 8670000
10000 10
08/12/2022 03:00
WG1907171
Fss]
Fn
Rc
F,
F
RC
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Frit Car Inc.
L1520266
03/26/22 11:37
6 of 20

WG1905588
Gravimetric Analysis by Method 2540 C-2011
Method Blank (MB)
(MB) R3324141-1 03/04/22 17:37
MB Result
Analyte ug/I
Dissolved Solids U
MB Qualifier MB MDL MB RDL
ug/I ug/I
10000 10000
L1519965-02 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1520266-01
(OS) L1519965-02 03/04/22 17:37 • (DUP) R3324141-3 03/04/22 17:37
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
Dissolved Solids 860000 892000 1 3.65 5
L1519965-03 Original Sample (OS) • Duplicate (DUP)
(OS) L1519965-03 03/04/22 17:37 • (DUP) R3324141-4 03/04/22 17:37
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
Dissolved Solids 892000 900000 1 0.893 5
Laboratory Control Sample (LCS)
(LCS) R3824141-2 03/04/22 1737
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I
Dissolved Solids 8800000 8240000 93.6 77.3-123
ACCOUNT: PROJECT:
Frit Car Inc.
SDG: DATE/TIME: PAGE:
L1520266 03/26/22 11:37 7 of 20

WG1905544
Gravimetric Analysis by Method 2540 D-2015
Method Blank (MB)
(MB) R3823964-1 03/04/22 1425
MB Result
Analyte ug/I
Suspended Solids U
MB Qualifier MB MDL MB RDL
ug/I ug/I
2500 2500
L1520234-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1520266-01
(OS) L1520234-01 03/04/22 14:25 • (DUP) R3823964-3 03/04/22 14:25
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
Suspended Solids 10300 10500 1 2.41 5
Laboratory Control Sample (LCS)
(LCS) R3823964-2 08/04/22 1425
Spike Amount LCS Result
Analyte ug/I ug/I
Suspended Solids 773000 772000
LCS Rec. Rec. Limits LCS Qualifier
99.9 85.7-114
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1520266 03/26/22 11:37 3 of 20

WG1903229
Wet Chemistry by Method 300.0
Method Blank (MB)
(MB) R3322466-1 07/30/22 09:55
MB Result
Analyte
ug/I
Chloride
U
Sulfate
U
MB Qualifier MB MDL
MB RDL
ug/I
ug/I
379
1000
594
5000
L1519902-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1519902-01 07/30/22 16:51 • (DUP) R3822466-3 07/30/22 17:04
Original Result
DUP Result
Dilution DUP RPD
Analyte
ug/I
ug/I
Chloride
2890
2850
1 1.40
Sulfate
ND
ND
1 0.000
Laboratory Control Sample (LCS)
(LCS) R3822466-2 07/30/22 10:07
Spike Amount
LCS Result
LCS Rec.
Analyte ug/I
ug/I
Chloride 40000
40600
101
Sulfate 40000
40900
102
QUALITY CONTROL SUMMARY
L1520266-01
DUP Qualifier DUP RPD
Limits
20
20
Rec. Limits LCS Qualifier
90.0-110
90.0-110
L1519902-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1519902-01 07/30/22 16:51 • (MS) R3822466-4 07/30/22 1716
Spike Amount
Original Result
MS Result
MS Rec.
Analyte
ug/I
ug/I
ug/I
Chloride
50000
2890
53900
102
Sulfate
50000
ND
53100
102
Dilution Rec. Limits MS Qualifier
1 80.0-120
1 80.0-120
ACCOUNT: PROJECT:
Frit Car Inc.
SDG: DATE/TIME: PAGE:
L1520266 03/26/22 11:37 9 of 20

WG1905192 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 350.1 L1520266-01
Method Blank (MB)
(MB) R3322707-1 03/04/22 12:37
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/I ug/I ug/I
Ammonia Nitrogen U 117 250
L1520652-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1520652-01 03/04/22 12:58 • (DUP) R3322707-5 03/04/22 12:59
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I %_
Ammonia Nitrogen ND ND 1 0.000 10
L1520924-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1520924-01 03/04/22 13:23 • (DUP) R3322707-7 03/04/22 13:25
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
Ammonia Nitrogen 3170 3180 1 0.284 10
Laboratory Control Sample (LCS)
(LCS) R3822707-2 08/04/22 12:38
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I
Ammonia Nitrogen 7500 7550 101 90.0-110
L1520649-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1520649-01 03/04/22 12:49 • (MS) R3322707-3 03/04/22 12:50 • (MSD) R3322707-4 03/04/22 12:56
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/I ug/I ug/I ug/I
Ammonia Nitrogen 5000 282 5380 5390 102 102 1 90.0-110 0.111 10
L1520863-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1520363-01 03/04/22 13:20 • (MS) R3322707-6 03/04/22 13:22
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte ug/I ug/I ug/I
Ammonia Nitrogen 5000 3790 8640 97.0 1 90.0-110
ACCOUNT: PROJECT:
Frit Car Inc.
SDG: DATE/TIME: PAGE:
L1520266 03/26/22 11:37 10 of 20

WG1910113
Wet Chemistry by Method 365.4
Method Blank (MB)
(MB) R3325741-1 03/12/22 15:07
MB Result
Analyte ug/I
Phosphorus, Total U
MB Qualifier MB MDL MB RDL
ug/I ug/I
35.0 100
L1519763-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1520266-01
(OS) L1519763-01 03/12/22 15:10 • (DUP) R3325741-3 03/12/22 15:11
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I %_
Phosphorus, Total 1450 1480 1 2.05 20
Laboratory Control Sample (LCS)
(LCS) R3825741-2 08/12/22 15:09
Spike Amount LCS Result LCS Rec.
Analyte ug/I ug/I
Phosphorus, Total 3780 3640 96.3
Rec. Limits LCS Qualifier
83.2-116
L1519763-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1519763-01 03/12/22 15:10 • (MS) R3325741-4 03/12/22 15:12 • (MSD) R3325741-5 03/12/22 15:14
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec.
Analyte ug/I ug/I ug/I ug/I
Phosphorus, Total 2500 1450 3740 3740 91.6 91.6
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
1 90.0-110 0.000
RPD Limits
20
ACCOUNT: PROJECT:
Frit Car Inc.
SDG: DATE/TIME: PAGE:
L1520266 03/26/22 11:37 11 of 20

WG1907905
Wet Chemistry by Method 420.4
Method Blank (MB)
(MB) R3824891-1 03/10/22 1729
MB Result
Analyte ug/I
Total Phenol by4AAP U
MB Qualifier MB MDL MB RDL
ug/I ug/I
8.30 40.0
L1519342-02 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1520266-01
(OS) L1519342-02 03/10/22 17:33 • (DUP) R3324391-3 03/10/22 17:33
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I %_
Total Phenol by4AAP ND ND 1 0.000 20
L1521068-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1521063-01 03/10/22 17:44 • (DUP) R3324391-5 03/10/22 17:45
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
Total Phenol by4AAP ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3824891-2 03/10/22 1730
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I
Total Phenol by4AAP 500 520 104 90.0-110
L1519342-02 Original Sample (OS) • Matrix Spike (MS)
(OS) L1519342-02 03/10/22 17:33 • (MS) R3324391-4 03/10/22 17:34
Spike Amount Original Result MS Result MS Rec.
Analyte ug/I ug/I ug/I
Total Phenol by4AAP 1000 ND 965 96.5
Dilution Rec. Limits MS Qualifier
1 90.0-110
L1521068-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1521063-01 03/10/22 17:44 • (MS) R3324391-6 03/10/22 17:43 • (MSD) R3324391-7 03/10/22 17:43
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/I
ug/I
ug/I
ug/I
Total Phenol by4AAP 1000
ND
918
905 91.8 90.5 1 90.0-110 1.49 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1520266 03/26/22 11:37 12 of 20

WG1905171 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 4500H+ B-2011 L1520266-01
L1519873-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1519373-02 03/04/22 12:00 • (DUP) R3322641-2 03/04/22 12:00
Original Result DUP Result Dilution DUP RPD
Analyte su su
pH 7.84 7.88 1 0.509
Sample Narrative:
OS: 7.84 at 23.5C
DUP: 7.88 at 23.8C
L1520266-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1520266-01 03/04/22 12:00 • (DUP) R3322641-3 03/04/22 12:00
Original Result DUP Result Dilution DUP RPD
Analyte su su
pH 6.26 6.26 1 0.000
Sample Narrative:
OS: 6.26 at23.2C
DUP 6.26 at23.6C
Laboratory Control Sample (LCS)
(LCS) R3822641-1 08/04/22 12:00
Spike Amount LCS Result LCS Rec. Rec. Limits
Analyte su su
pH 10.0 9.94 99.4 99.0-101
Sample Narrative:
LCS: 9.94 at 24C
DUP Qualifier DUP RPD
Limits
DUP Qualifier DUP RPD
Limits
1
LCS Qualifier
ACCOUNT: PROJECT:
Frit Car Inc.
SDG: DATE/TIME: PAGE:
L1520266 03/26/22 11:37 13 of 20

WG1903699
Wet Chemistry by Method 4500P E-2011
Method Blank (MB)
(MB) R3321140-1 03/01/22 09:18
MB Result
Analyte ug/I
Phosphate,Ortho U
MB Qualifier MB MDL MB RDL
ug/I ug/I
14.0 30.0
L1520266-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1520266-01
(OS) L1520266-01 03/01/22 09:23 • (DUP) R3321140-3 03/01/22 09:23
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
Phosphate,Ortho 220 251 1 13.2 20
Laboratory Control Sample (LCS)
(LCS) R3821140-2 08/01/22 09:18
Spike Amount LCS Result LCS Rec.
Analyte ug/I ug/I
Phosphate,Ortho 245 212 86.7
Rec. Limits LCS Qualifier
85.0-115
L1520266-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1520266-01 03/01/22 09:23 • (MS) R3321140-4 03/01/22 09:24 • (MSD) R3321140-5 03/01/22 09:25
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec.
Analyte ug/I ug/I ug/I ug/I
Phosphate,Ortho 500 220 295 317 15.0 19.4
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
1 80.0-120 J6 J6 7.19
RPD Limits
20
ACCOUNT: PROJECT:
Frit Car Inc.
SDG: DATE/TIME: PAGE:
L1520266 03/26/22 11:37 14 of 20

WG1903258 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 5210 B-2016 L1520266-01
Method Blank (MB)
(MB) R3322632-1 03/04/22 1122
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/I ug/I ug/I
BOD U 200 200
L1520241-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1520241-01 03/04/22 10:55 • (DUP) R3822632-3 03/04/22 10:57
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I %_
BOD ND ND 1 0 K1 30
Laboratory Control Sample (LCS)
(LCS) R3822632-2 08/04/22 10:48
Spike Amount
LCS Result LCS Rec.
Analyte ug/I
ug/I
BOD 198000
184000 92.8
Laboratory Control Sample (LCS)
Rec. Limits LCS Qualifier
84.6-115
(LCS) R3822632-4 08/04/22 1105
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I
BOD 198000 188000 94.8 84.6-115
ACCOUNT: PROJECT:
Frit Car Inc.
SDG: DATE/TIME: PAGE:
L1520266 03/26/22 11:37 15 of 20

WG1909551
Wet Chemistry by Method 5310 B-2014
Method Blank (MB)
(MB) R3329144-2 03/22/22 18:52
MB Result
Analyte ug/I
TOC (Total Organic Carbon) U
MB Qualifier MB MDL MB RDL
ug/I ug/I
102 1000
L1519785-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1520266-01
(OS) L1519735-01 03/22/22 19:16 • (DUP) R3329144-3 03/22/22 19:40
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
TOC (Total Organic Carbon) 2040 2020 1 0.885 20
L1520655-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1520655-02 03/23/22 01:52 • (DUP) R3329144-6 03/23/22 02:11
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
TOC (Total Organic Carbon) ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3829144-1 08/22/22 18:31
Spike Amount
LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I
ug/I
TOC (Total Organic Carbon) 75000
77000 103 85.0-115
L1520361-08 Original Sample
(OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1520361-08 03/22/22 21:45 • (MS) R3329144-4 03/22/22 22:19 • (MSD) R3329144-5 03/22/22 22:42
Spike Amount
Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/I
ug/I ug/I ug/I
TOC (Total Organic Carbon) 50000
6700 52900 54200 92.3 95.0 1 80.0-120 2.52 20
L1520789-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1520739-03 03/23/22 05:24 • (MS) R3329144-7 03/23/22 05:47 • (MSD) R3329144-8 03/23/22 06:31
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/I
ug/I
ug/I
ug/I
TOC (Total Organic Carbon) 50000
25400
46400
55000 42.0 59.0 1 80.0-120 J6 J6 16.8 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1520266 03/26/22 11:37 16 of 20

WG1907171
Metals (ICP) by Method 200.7
Method Blank (MB)
(MB) R3825425-1 03/11/22 1750
MB Result
Analyte
ug/I
Chromium
U
Iron
U
Sodium
U
MB Qualifier MB MDL
MB RDL
ug/I
ug/I
1.63
10.0
20.5
100
444
1000
Laboratory Control Sample (LCS)
(LCS) R3825425-2 08/11/22 17:53
Spike Amount
LCS Result
LCS Rec.
Analyte ug/I
ug/I
Chromium 1000
1010
101
Iron 10000
10200
102
Sodium 10000
9820
98.2
QUALITY CONTROL SUMMARY
L1520266-01
Rec. Limits LCS Qualifier
85.0-115
85.0-115
85.0-115
L1518910-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1513910-01 03/11/22 17:56 • (MS) R3825425-4 03/11/22 18:01 • (MSD) R3825425-5 03/11/22 18:03
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
ug/I
ug/I
ug/I
ug/I
Chromium
1000
ND
1020
978
102
97.8
Iron
10000
556
11000
10500
105
99.4
Sodium
10000
43200
53100
49900
99.4
67.2
L1520111-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
1 70.0-130 4.54
1 70.0-130 4.79
1 70.0-130 V 6.25
RPD Limits
20
20
20
(OS) L1520111-01 03/11/22 18:06 • (MS) R3825425-6 03/11/22 18:09 • (MSD) R3825425-7 03/11/22 18:11
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte
ug/I
ug/I
ug/I
ug/I
Chromium
1000
541
1580
1570
104
103
1 70.0-130
0.628
20
Iron
10000
1180
11200
11300
100
101
1 70.0-130
0.939
20
Sodium
10000
649000
708000
698000
593
487
1 70.0-130
V V 1.51
20
ACCOUNT: PROJECT:
Frit Car Inc.
SDG: DATE/TIME: PAGE:
L1520266 03/26/22 11:37 17 of 20

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contactyour project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
u
Fc
Fss]
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
Fn
RDL
Reported Detection Limit.
Rec.
Recovery.
Fr
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
U
Not detected at the Reporting Limit (or MDL where applicable).
Fc
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
F
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
LEI
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J6
The sample matrix interfered with the ability to make any accurate determination, spike value is low.
K1
The sample dilutions set-up for the BOD/CBOD analysis did not meet the oxygen depletion criteria of at least 2 mg/L.
Reported result is an estimated value.
Q
Sample was prepared and/or analyzed past holding time as defined in the method. Concentrations should be
considered minimum values.
T8
Sample(s) received past/too close to holding time expiration.
v
The sample concentration is too high to evaluate accurate spike recoveries.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc.
L1520266 03/26/22 11:37 13 of 20

ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
Nebraska
N E-OS-15-05
Alaska
17-026
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TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TNO02
California
2932
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704 _
Georgia
NELAP
North Carolina 3
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky' 6
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee'"
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas5
LABO152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A2 LA
A2LA— ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
FP
Fc
FS-S
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME:
Frit Car Inc. L1520266 03/26/22 11:37
PAGE:
19 of 20

cow,Pany "Jame/Address.
Billing Information:
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Chain of Custody Page of
Frit Car Inc.
Accounts Payable ees
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2012 US Hwy 17N
Brewton, AL 36427
c
New Bern, NC 28560
PEOPLE ADVANCING SCIENCE
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MT JULIET, TN
Report to:
Email To: [e-mail]
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Matrix:Remarks: Sample Receipt Checklist
pH Temp CDC Seal Present/Intact:
SS -Sail AIR •Air IF - Filter —NP _,'r N
GW - Groundwater B- Bioassay COC Signed/Accurate: N
Ww- WasteWater Flow Other Bottles arrive intact: _N
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DW - Drinking Water Sufficienttvolumetles —N
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Samples returned vi — —
OT - Other Tracking # Q� / If able
CFO
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Relinquished by: (Sig natur Date: Time: Received by: (Signature) Trip Blank Received: Yes / o Preservation Correct/Checked: _
HCL MeoH
7/21� �IO RFD Screen <Q.5 mA/hr: —Y —N
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TBR
Relinquished by: (Signature)
Date:
Time,
Received by: (Signature)
Temi 07C Bottles Received:
If preservation required by Login: Date/Time
3-qio: 34 tO
Relinquished by: (Signature)
Date:
Time:
Received for lab by: (Signature)
Date: Time: q�
Hold:
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