WQ0023306_2022 Residual Annual Report_20230105 (2)

Initial Review
Reviewer
Thornburg, Nathaniel D
Is this submittal an application? (Excluding additional information.)*
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * WQ0023306
ApplicantlPermittee City of New Bern
Email Notifications
Does this need review by the hydrogeologist?* Yes No
Regional Office
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Name* Tony Hawkins
Email Address*
[e-mail]
Project Information
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
2526397555
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
hftps://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Perm it Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number: *
WQ0023306
Has Current Existing permit number
Applicant/Permittee Address*
PO Box 1129 New Bern, NC 28563
Facility Name*
City of New Bern Class A Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
sludge report 2022.pdf 6.9MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality (NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
94rWaRAW
Submission Date 1/5/2023

Everything comes together here
Department of Public Utilities
Wastewater Treatment Plant
307 Glenburnie ]give
New Berri, NC 28560-2816
January 4, 2023
NCDr,NR-D Q
Information Processing Unit
161.7 Mail Service Center
Raleigh, NC 27699-1617
Reference: 2022 Land Application annual Report
City of New Benz
CLASS A RESIDUALS Permit Number WQ0023306
The City of New Bern is submitting all monitoring and reporting requirements as specified in the above
referenced permit for its land application program for Sewage Sludge. The city has managed and compiled the
submitted data.
The city produced approximately 4866 dried tons Of sludge during 2022. 1.118 tons went to the Craven County
Solid Waste Management Authority to be used for ground cover and 3747 tons went to farmland. which met the
Class A Sewage Sludge criteria. The report includes forin ACF, form I)MSDF, form RSSF, form MFLSF, I-ab
Sheets, and form. PVRF 2T.
If any further information is required, please contact Tony Hawkins at [phone].
Sincerely,
Tony :Hawkins
Treatment Plants Manager
Enclosures
Cc: File

ANNUAL LAND APPLICATION CERTIFICATION FORM.
WQ :lPermit#: WQ0023306 County: Craven year:
2022
Facility Name (as shown on permit):
Land. Application Operator:
City of Now Bern
Tony Hawkins Phone:
Land application of residuals as allowed by the permit occurred during the past calendar year:
21 Yes [J No - 1f No, skip Part A, and Part 13 and proceed to Part C. Also, 1f residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
[phone]
Total number of application fields in the ermit: I 1.
Total number of fields utilized for land application during the year:1
27
Total amount of dry tons applied during the year for all application sites:
4,866
Total number of acres utilizes for land application during the year:
440
Part B - Annual Coml2iance Statement:
Facility was compliant during calendar year 2022 with all conditions of the land application permit
(including but not limited to items 1- 3 below) issued by the Division of Water Resources. RJ Yes 0 No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pll was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual `ITLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T. 1 105,(a) or the Pollutant
Loading Rates in 15A NCAC 02T. I 105(b) (applicable to 40 C,FR Part 503 regulated facilities),
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part.
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .111.1 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations .and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
1 1) Vegetative cower was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
°l certify, under penalty of lase, that the above information is, to the best of any knowledge and belief, true, accurate,
and complete. 1 am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Tony Hawkins Plant Manager
Permittee Name and Title#ype or print)
Signature of Pennittee
Date
ignature of Preparer' Date
Signature of Land Applier
.Date
(if different from. Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM AGF (12/2006)

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702

ANWAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be s"bnnitted in Aunnzual. Report
Facility Name:
Permit
4-
perator:
Acres Used:
City of New Bern
WQ0023306
Tony Ilawvkins Owner:
n/a Acres Permitted.
Total. Ivry Tarts Applied (Annual). 4866.00
Cation Exchange Capacity (groat 503 only).
City of New Bern. Predominant Soil Series:
3122 Site #: land field Field #4
K
farms
Sample or
_
_._
5
6
7
8
9
10
11
1
Com-
posite
Date
1/12/22
2/3/22
3/2/22
4/6/22
5/4122
6/l/22
7/19/22
8/3/21
9/15/22
10/6122
11/3/22
12/1f22
%, Solids
28.63
46.02
32.17
31.99
27.45
26.9
Arsenic
<2.5
1 <2.5
<2.5
<2.5
<2.5
3.1.
<2.5
2.5
<2.5
<2.5
<2.5
<2.5
Cadmium
<0.05
<0.5
<0.5
<2.5
<0.5
<0.5
<0.5
<0.5
0.66
0.59
0.52
<0.5
Copper
152
1.09
94
84
98
128
1 129
98
202
180
151
99
hromium
10
7
8
6
7
8
8
5
14
13
9.4
4
Lead
6.8
4.9
4.1
3.9
4.5
5.5
6.4
5 A
9.3
10
7.3
4.6
[Mercury
0.16
0.1.2
0,21
0.12
0.23
0,19
0.19
0.24
0,34
0,33
0.24
0.12
Molyb-
5
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
denum
Nickel
7
<5.0
<5.0
<5.0
® 6
6
6
<5.0
9.1
8.5
7
<5.O
Selenium
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
Zinc 348
262
179
201
241
326
330
1 241
470
495
344
232
Total
Phos- 0.7620
c24280
c13390
c16560
e13430
c2609
c16270
c1.1680
09900
c18610
c20680
c21090
horus
Annual Heavy
Metal field
Loadings
(Calculated
in lbslacr°e):
Total 1
2
3
4
5
76
7
8
9
1 o
11
12 7
DT/Ac./
-
__.
App
a ,
Event
Arsenic
144#49#19440
######
######
######
0.000
######
O,000
######
######
######
# ####
######
Cadmium
######
######
######
######
######
######
######
#######
0.000
0.000
0,000
#######
######
Copper
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Chromiurn
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0X0
0,000
0.000
0.000
0.000
Mercury
0.000
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.0010
######
######
######
######
####!###
######
######
######
######
######
# #####
######
denurn
Nickel 1
0.000
######
######
94#444
0.000
0.000
0.000
#44#44
0.000 1
0.000
0.000 14#4#4#
######
Selenium
#999#4
######
#######
######
######
9#44#4
######
######
#######
######
#######
######
########
Zinc
0.000
0.000
0,000 1
0,000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
Total
Plies- ######
###### ###### ###### ###### ######
###### ######
####### ###### ###### ###### ## ###
ltorus
"I certify, under
penalty of law, that this document was prepared
under my direction
or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier Date:
DENR FORM MFLSF (12/2006)

I J-11313(2' RJ t IL'
Drinking Water ID:. 37715
Wastewater ID: 10
64 (')A[0/10C,,� I DRNE
'EJ\JV1LE, r,4 C',, 27858
CITY OF NEW BERN (BIOSOLIDS)
ATTN: TONY HAWKINS
P.O. Box 1129
NEW BERM, NC 28563
REVIEWED BY:
Holding
Holding
Holding
Holding
Holding
Analysis
Metbod
PARAMETERS Basin-FC#1
Basin-FC#2
Bashi-1+C#3
Basin-FC#4
Basin-FC#5
Date Analyst
Code
Total Solids, % 28.63
40.21
26,00
31.45
28.27
01/13/22 DNS
254OG-15
Fecal Coliform (MPN), /gram Solids < 1.8
< 1.8
< 1.8
< 1.8
< 1.8
01/12/22 JMS
9221E-14

1'I`i J11 1 [11
Drinking water ID; 37715
114
CITY OF NEW BERN (BIOSOLIDS;
ATTN: TONY HAWKINS
�P.O. BOX 1129
NEW BERN, NC 28563
(252)
( ), ��252)
DATE COLLECTED: 01/12/22
DATE REPORTED ; 01/19/22
ffaffivzzffll*r
Holding
Holding
Analysis
Method
PARAMETERS Basin-FC#6
Basin-FC#7
Date Analyst
Code
Total Solids, % 20.94
22.59
01/13/22 DNS
2540G-15
Fecal Coliform (MPN), /grarn Solids < 1.8
<1.8
01/12/22 JMS
9221E-14

CITY OF NEW BERN (BIOSOLIDS)
ATTN- TONY HAWKINS
P.O. BOX 1129
NEW BERN, NC 28563
Holding
Analysis
Method
PARAMETERS Basin (RA)
Date
Analyst
Code
Aluminum, (dry wt. basis), mg/kg
3276
01/18/22
LFJ
EPA200.7
Arsenic (dry wt, basis), mg/kg
< 2.5
01/21/22
MTM
311313-04
Calcium (dry wt. basis), mg/kg
194602
01/18/22
LFJ
EPA200.7
Cadmium (dry wt. basis), iing/kg
<0.5
01/19/22
MTM
31130-04
Copper (dry wt. basis), mg/kg
152
01/18/22
LFJ
EPA200.7
Chromitim, T.(dry wt. basis),mg/kg
10
01/18/22
LFJ
EPA200.7
Lead (dry weight basis), mg/kg
6.8
01/19/22
MTM
3113B-04
Magnesium (dry wt, basis), mg/kg
5430
01/18/22
LFJ
EPA200.7
Mercury (dry wt. basis), mg/kg
0.16
01/1.9/22
MTM
EPA7471 B
Nickel (dry wt. basis), mg/kg
7
01118/22
LFJ
EPA200.7
Potassium (dry wt. basis), mg/kg
6084
01/18/22
LFJ
EPA200.7
Selenium (dry wt, basis), mg/kg
<5.0
01/18/22
MTM
3113B-04
Silver (dry wt. basis), mg/kg
3
01/18/22
LFJ
EPA200.7
Sodium (dry wt. basis), mg/kg
1350
01/18/22
LFJ
EPA2W7
Zinc (dry wt. basis), mg/kg
348
01/18/22
LFJ
EPA200.7
Total Cyanide (dry weight), ing/kg
67,24
01/18/22
HMM
450OCNE-16
TKN (dry wt.), ing/lig
c 45730
01/19/22
TRJ
351.2 112-93
Ammonia Nitrogen (dry wt.),mg/kg
c 342,8
.01/24/22
BM D
350.11 112�93
Phosphorus, T. (dry wt.), ing/kg
c 17620
01/19/22
BIM D
365.4-74
Nitrate+Nitrite (dry wt.), mg/kg
c 62.78
01/24/22
TRJ
353.2 122-93
Plant Available Nitrogen, nag/kg
18389
02/03/22
MAO
Molybdenum (dry wt. basis), mg/kg
5
01/26/22
LFJ
EPA200.7
ptewater ID1 10
F1 N1 E 4 2 5,1) 5 r3 - 6,") 0 8
6 ,333,
DATE COLLECTED: 01/12/22
DATE REPORTED : 02/04/22
REVIEWED BY:
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure,

114 K %A r,,), I ED F10 V E
E, N
CITY OF NEW BERN
ATTN: TONY HAWKINS
WASTEWATER TREATMENT PLANT
307 GLENBURNIE DRIVE
NEW BERN, NC 28560
Fftial Analysis Method
Effluent Date Analyst Code
Total lqeldahl Nitrogen as N,mg/l U4 02/03/22 KES 351.2 R2-93
OrInking Water IVr 37715
Wastewater lv10
('j
X '�27'`&06`1`
DATE COLLECTED: 01/27/22
DATE REPORTED : 02/04/22
REVIEWED BY:

laoeAnalj4ical"
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Mark Oliveira
Environment 1
114 Oakmont Dr
Greenville, NC 27858
Project: Environment 1
Pace Project No.: 92582476
Page 1 of 1
Report Date: 01/27/2022
Date Received: 01/13/2022
Sample: RAW I Lab ID: 92582476001 Collected: 01/06/22 10:59 Matrix: Water
Method Parameters Results Units Report Limit Analyzed Qualifiers
EPA420A Rev 1.0 1993 Phenolics, Total Recoverable 0.040 mg1L 0.020 01126/2214:17 M1
Sample: Fl EF Lab ID: 92582476002 Collected: 01/06/22 10:50 Matrix: Water
Method Parameters Results Units Report Limit Analyzed Qualifiers
EPA420.4 Rev 1.0 1993 Phenolics, Total Recoverable ND mg/L 0.020 01/26/22 14:22 M1,R1
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was
/outside control limits.
Reviewed by: ,
Stephanie Knott
704-977-0981
stephanie.kno€[e-mail]
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804 South Carolina Laboratory ID: 99030
Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001
North Carolina Drinking Water Certification #: 37712 Virginia/VELAP Certification #: 460222
North Carolina Wastewater Certification #: 40
Page 1 of 5

Drinking Water ID: 37715
CITY OF NEW BERN (BIOSOLIDS)
ATTN: TONY HAWKINS
P.O. BOX 1129
NEW BERN, NC 28563
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt, basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), q-ng/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt, basis), mug/kg
Silver (dry wt, basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Cyanide (dry weight), mg/kg
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),ing/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mg/kg
Holding Analysis Method
Basin (RA) Date Analyst Code
2616
02/08/22
LFJ
EPA200.7
< 2.5
02/10/22
MTM
3113B-04
267816
02/08/22
LFJ
EPA200.7
< 0.5
02/08/22
MTM
3113B-04
109
02/08/22
LFJ
EPA2W7
7
02/08/22
LFJ
EPA200.7
4.9
02/09/22
MTM
3113B-04
4773
02/08/22
LFJ
EPA200.7
0J2
02/10/22
MTM
EPA7471B
< 5,0
02/08/22
LFJ
EPA200.7
5100
02/09/22
LFJ
EPA200.7
<�5.0
02/11/22
M"t VI
31 i'3B-04
< 2.5
02/08/22
LFJ
EPA200.7
< 1250
02/08/22
LEY
EPA200.7
262
02/08/22
LFJ
EPA200.7
26.3
02/03/22
HMM
450OCNE-16
c 30450
02/11/22
TRJ
351.2 112-93
c 55.89
02/08/22
KES
350.1 112-93
c 24290
02/11/22
KEA S
365.4-74
c 41.92
02109/22
TRJ
353.2 1i2-93
12228
02/15/22
MAO
< 5.0
02/08/22
LFJ
EPA200.7
P —RD 1,
FAX
DATE COLLECTED: 02/03/22
DATE REPORTED : 02/25/22
REVIEWED B'Y
c Uncertified data. DWR does not offer non-aqueOus Certification for this analytical procedure.

(j"Ji "j)
_7 71 (p
7,
1 f 4 (,)A K f",,1 0 �',J "V C r F",, 1',,/E
(",J`EEC kWLLE 1 -0,,1178!::�9,
CITY OF NEW BERN (BIOSOLIDS)
ATTN: TONY HAWXINS
P.O. BOX 1129
NEW BERN, NC 28563
lrinkinj, Water 1037715
Wastewater IDro 10
756-6208
DATE COLLECTED: 03/02/22
DATE REPORTED : 03/08/22i
REVIEWED BY:
Holdhig
Holding
Holding
Holding
Holding
Analysis
Method
PARAMETERS Basin-FUl
Basin-FC#2
1lasin-FC#3
1lasin-FC#4
Basin-FC#5
Date Analyst
Code
Total Solids, % 46,02
41,85
46.69
39.03
48,77
03/02/22 JMS
2540G-15
Fecal Coliform (NVN)�, /grain Solids < 0.4
< 0.4
<0.4
< 0.5
<0.4
03/02/22 CAW
9221E-14

01. '0111]
17 00 U""'
CITY OF NEW BERN (BIOSOLID,S)
ATTN: TONY HAWKINS
P.O. BOX 1129
NEW BERN, NC 28563
Z)r4Akio,q Wotear toi 57715
Wastewater ID� 10
DATE COLLECTED: 03/02/22
DATE REPORTED - 03/08/22
REVIEWED BY:
Holding
Holding
Analysis
Method
PARAMETERS Basin-FC#6
Basin-FC#7
Date Analyst
Code
Total Solids, % 38.79
48.22
03/02/22 JMS
2544G-15
Fecal Coliform (MPN), /gram Solids <0.5
<0A
03/02/22 CAW
9221E-14

uwl
11,1- K N,/1 0 1 F1 1) R Vv'E
CITY OF NEW BERN (BIOSOLIDS)
ATTN: TONY HAWKINS
P.O. BOX 1129
NEW BERN, NC 28563
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt, basis), ing/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), ing/lig
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt, basis), mg/kg
Silver (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Cyanide (dry weight), mg/lig
TK,N (dry wt.), mg/kg
Ammonia Nitrogen (dry w(.),uig/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt, basis), mg/kg
Holding Analysis Method
Basin (RA) Date Analyst Code
2268
03107/22
LFJ
EPA200.7
< 2.5
03108/22
mTM
3113B-04
334618
03/07/22
LFJ
EPA200.7
< 0.5
03/08/22
MTM
3113B-04
94
03/07/22
LFJ
EPA200.7
8
03/07/22
LFJ
EPA200.7
4.1
03/09/22
MTM
311313-04
3621
03/07/22
LFJ
EPA200.7
0.21
03/14/22
MTM
EPA7471B
< 5,0
03/07/22
U1
EP, 200.7
2141
03/07/22
LFJ
EPA200.7
<5.0
03/08/22
MTM
3113B-04
< 2.5
03/07/22
LFJ
EPA200.7
< 1250
03/07/22
LFJ
EPA200,7
179
03/07/22
LFJ
EPA200.7
51.77
03/15/22
HMM
450OCNE-16
c 16880
03/08/22
TRJ
351.2 112-93
c 31.96
0"' /09/22
TRJ
350.1 R2-93
c 13390
03/08/22
BMD
365A-74
c 88.88
03109/22
ICES
353,2 112-93
6844
03/18/22
KES
< 5.0
03/07/22
LFJ
EPA200.7
REVIEWHD BY:
wastewater vD�
F�'� hCTIF (25r 75f3 61"1"08
F14"Ix
c Uncertified data. DWR does not offer non-aqueoua certification for this analytical procedure.

[' , " '`(­­'["'­� - 'I ­'­ "" 1J� ( (;�7 0)
�IJ [J"LR � (2::) �_� � � �"' '�"' III] ff [11`
_5,
CITY OF NEW BERN (BIOSOLIDS)
ATTN: TONY HAWKINS
P.O. BOX 1129
NEW BERN, NC 28563
Holding
Analysis
Method
PARAMETERS Basin (RA)
Date Analyst
Code
Aluminum, (dry wt. basis), mg/kg
2140
04/18/22
LFJ
EPA200.7
Arsenic (dry wt. basis), mg/kg
<15
04/13/22
MTM
311313-04
Calcium (dry wt. basis), mg/kg
320265
04/18/22
LFJ
EPA200.7
Cadmium (dry wt, basis), mg/kg
<0.5
04/14122
MTM
3113B-04
Copper (dry wt, basis), mg/kg
84
04/18/22
LFJ
EPA200.7
Chromium, T,(dry wt. basis),ing/kg
6
04/18/22
LFJ
EPA200.7
Lead (dry weight basis), mg/kg
3.9
04112/22
MTM
311313-04
Magnesium (dry wt. basis), mg/lig
4874
04/18/22
LFJ
EPA200.7
Mercury (dry wt. basis), mg/kg
0.12
04/27/22
MTM
E P ' A7471B
Nickel (dry wt. basis), mg/kg
< 5.0
04/18/22
LFJ
EPA200.7
Potassium (dry wt. basis), mg/kg
3783
04/18/22
LFJ
EPA200.7
Selenium (dry wt. basis), mg/kg
< 5.0
04/20/22
MTM
3113B-04
Silver (dry wt, basis), mg/kg
< 2.5
04/18/22
LFJ
EPA200.7
Sodium (dry wt. basis), mg/kg
< 1250
04/18/22
LFJ
EPA200.7
Zinc (dry wt. basis), mg/kg
201
04118/22
LFJ
EPA200.7
Total Cyanide (dry weight), mg/kg
55.02
04/19/22
HMM
450OCNE-16
TKN (dry wt.), mg/kg
c 20600
04/13/22
BMD
351.2 112-93
Ammonia Nitrogen (dry wt,),mg/kg
c 141.2
04114/22
BMID
350.1 RZ-93
Phosphorus, T. (dry wt.), mg/kg
c 16560
04/13/22
TRJ
365.4-74
Nitrate+Nitrite (dry wt.), mg/kg
c, 49.73
04/12/22
ICES
353.2 R2-93
Plant Available Nitrogen, mg/kg
8304
04/22/22
ICES
Molybdenum (dry wt. basis), mg/kg
< 5.0
04/18122
LFJ
EPA200.7
Wastewater ID; 10
F:AX 756 J 51
ID#; 214
I-, I'll ­­, UTERENUFA
REVIEWED BY:
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure,

I'D
"'I ["'J " F, V k
LE, 27858
CITY OF NEW BERN (BIOSOL;IDS:
ATTN: TONY HI ICI AWKINS
P.O. BOX 1129
NEW BERN, NC 28563
ID#: 214 A
REVIEWED BY:
Wastewater TD:; 10
(,�`52) 756
Holding
Holding
Holding
Holding
Holding
Analysis
Method
PARAMETERS l3ashi-FC#1
Basin-FC#2
Basin-FC#3
Basin-FC#4
Basin-FC#5
Date Analyst
Code
Total Solids, % 32.17
33.83
31.34
32.26
35.36
05/05122 JMS
25411G-15
Fecal Coliform (MPN), /grain, Solids < 1.8
<1.8
< 1.8
<1.8
< 1.8
05/09/22 HCE
9221E-14

WaateWater TD: TO
(0t
CITY OF NEW BERN (BIOSOLIDS)
ATTN: TONY HAWKINS
P.O. BOX 11298NEW BERN, NC 28563
REVIEWED BY:
Holding
Holding
Analysis
Method
PARAMETERS Basin-FC#6
Basin-FC#7
Date Analyst
Code
Total Solids, % 30.65
32,35
05/05/22 JMS
2540G-15
Fecal Coliform (MPN), /gram Solids <L8
< 1.8
05/09/22 HCE
9221E-14

"I f
H
U "'9 If f)k[dj! j , 1-
Drinking Water ID: 37715
Wastewater ID: 10
G
CITY OF NEW BERN (BIOSOLIDS)
ATTN; TONY HAWKINS
P.O. BOX 1129
NEW BERN, NC 28563
REVIEWED BY:
Holding
Analysis
Method
PARAMETERS Basin (RA)
Date Analyst
Code
Aluminum, (dry wt. basis), mg/kg
2721
05/17/22
LFJ
EPA200.7
Arsenic (dry wt. basis), mg/kg
< 2.5
05/19/22
MTM
311313-04
Calcium (dry wt. basis), ing/kg
381499
05/17/22
LFJ
EPA200.7
Cadmium (dry wt. basis), mg/kg
<0.5
05/18/22
MTM
3113B-04
Copper (dry wt. basis), mg/kg
98
05/17/22
LFJ
EPA200.7
Chromium, T.(dry wt, basis),ing/kg
7
05/17/22
LFJ
EPA200.7
Lead (dry weight basis), mg/kg
4.5
05117/22
MTM
3113B-04
Magnesium (dry wt. basis), mg/kg
5486
05/17/22
LFJ
EPA200.7
Mercury (dry wt. basis), rng/kg
0.23
05/25/22
MTM
EPA7471B
Nickel (dry wt. basis), mg/kg
6
05/17122
LFJ
EPA200.7
Potassium (dry wt. basis), mglkg
4067
05/17/22
LFJ
EPA200.7
Selenium (dry wt. basis), mg/kg
< 5X
05/17/22
MTM
3f1311-04
Silver (dry wt. basis), mg/kg
< 2.5
05119/22
LFJ
EPA200.7
Sodium (dry wt. basis), mg/kg
< 1250
05/17/22
LFJ
EPA200.7
Zinc (dry wt. basis), mg/kg
241
05/17/22
LFJ
EPA200.7
Total Cyanide (dry weight), mg/kg
35.74
05/16/22
JMS
450OCNE-16
TKN (dry wt.), mg/kg
c 29810
05/10/22
TRJ
351.2 R.2-93
Ammonia Nitrogen (dry wt.),mg/kg
c 46.95
05/12122
BMD
350A R2-93
Phosphorus, T. (dry wt.), mg/kg
C 13430
05,11w122
BMD
365.4-74
Nitrate+Nitrite (dry wt.), mg/kg
c 102.9
05/10/22
KES
353.2 R2-93
Plant Available Nitrogen, r"gilig
9055
05/23/22
KES
Molybdenum (dry wt. basis), mg/kg
< 5.O
05i17/22
LFJ
EPA200.7
["J[� 7�� ... . .. . ; '2 �u 3
FAX'
c Uncertified data. DWR doers not offer non -aqueous certification for this analytical procedure.

1'Rll W
CITY OF NEW BERN (BIOSOLIDS)
ATTN: TONY HAWRINS
P.O. BOX 1125
NEW BERN, NC 28563
REVIEWED BY:
Holding
Analysis
Method
PARAMETERS Basin (RA)
Date Analyst
Code
Aluminum, (dry wt. basis), mg/kg
2869
06/07/22
LFJ
EPA200.7
Arsenic (dry wt. basis), mg/kg
3.1
06/07/22
MTM
3113B-04
Calcium (dry wt, basis), mg/kg
287436
06/07/22
LFJ
EPA200.7
Cadmium (dry wt. basis), mg/kg
<0.5
06/08/22
MTM
311313-04
Copper (dry wt. basis), i-ng/kg
128
06/07/22
LFJ
EPA200.7
Chromium, T.(dry wt. basis),mglkg
8
06/07/22
LFJ
EPA200.7
Lead (dry weight basis), mg/kg
5.5
06/07/22
MTM
3113B-04
Magnesium (dry wt. basis), mg/kg
5180
06/07/22
LFJ
EPA200.7
Mercury (dry wt. basis), mg/kg
0.19
06/23/22
MTM
EPA7471B
Nickel (dry wt, basis), mg/kg
6
06/07/22
LFJ
Ek200.7
Potassium (dry wt. basis), mg/hg
4119
06/07/22
LFJ
EPA200.7
Selenium (dry wt. basis), mg/kg
< 5.0
06/07/22
MTM
311313-04
Silver (dry wt. basis), mg/kg
< 2.5
06/07/22
LFJ
EPA200.7
Sodium (dry wt. basis), mg/kg
< 1250
06/07122
LFJ
EPA200.7
Zinc (dry wt. basis), mg/kg
326
06/07/22
LFJ
EPA200.7
Total Cyanide (dry weight),, mg/kg
79.69
06/14/22
HNIM
450OCNE-16
TKN (dry wt.), mg/kg
c 17390
06/07/22
TRJ
351.2 R2-93
Ammonia Nitrogen (dry
c 245.6
06/16/22
HNIM
350.1 R-1-93
Phosphorus, T. (dry wt.), mg/kg
c 2609
06/07/22
BMD
365A-74
Nitrate+Nitrite (dry wt.), mg/kg
c 116.9
06/09/22
KES
353.2 R2-93
Plant Available Nitrogen, mg/kg
709,8
06/21/22
ICES
Molybdenum (dry wt. basis), mg/kg
<5.0
06/07/22
LFJ
EPA200.7
orinking Water TD; 377�5
Wastewater ID; 10
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

,1
Driaking Water ID: 37'J15
was�pwater ID� I'D
CITY OF NEW BERN (BIOSOLIDS)
ATTN; TONY HAWKINS
P.O. BOX 1129
NEW BERN, NC 28563
REVIEWED BY:
Holding
Holding
Holding
Holding
Holding
Analysis
Method
PARAMETERS Basin-FC#1
13asin-FC#2
Basin-FC#3
1lasin.-FC#4
1lasin-FC#5
Date Analyst
Code
Total Solids, % 31.99
29.65
31.86
31.88
31.45
07/19/22 JMS
254OG-15
Fecal Coliform (MWN), /gram Solids <L8
< 1.8
< 1.8
< 1.8
< 1.8
07/19/22 JMS
9221 E-1 4

TDrinking Water ID' 37715
)
XD; 10
f I ",,/ E
"2
CITY OF NEW BERN (BIOSOLIDS)
ATTN: TONY HAWKINS
P.O. BOX 1129
NEW BERN, NC 28563
DATE COLLECTS ; 07/19/22
DATE REPORTED . 07/26/22
REVIEWED BY:
Holding
Holding
Analysis
Method
PARAMETE RS Basin-FC#6
Basin-FC#7
Date Analyst
Code
Total Solids, % 32.54
31.60
07/19/22 JMS
2540G-15
Fecal Coliform (MPN), /gram Solids < 1.8
< 1.8
07/19/22 JMS
9221E-14

..... ......
Q
J B
F),Rl'vE
i_�� V, L S
CITY OF NEW BERN (BIOSOLIDS,
ATTN: TONY RAWKINS
P40. BOX 1129
NEW BERN, NC 2�8563
REVIEWED BY:
Holding
Analysis
Method
PARAMETERS Basin (RA)
Date Analyst
Code
Aluminum, (dry wt. basis), mg/kg
3208
07/25/22
LFJ
EPA200.7
Arsenic (dry wt. basis,), mg/kg,
< 2.5
07/26/22
MTM
3113B-04
Calcium (dry wt. basis), mg/kg
301912
07/25/22
LFJ
EPA200.7
Cadmium (dry wt. basis), mg/kg
< 0.5
07/25/22
M[TM
3113B-04
Copper (dry wt, basis), mg/kg
129
07/25/22
LFJ
EPA200.7
Chromium, T.(dry wt. basis),mg/kg
8
07/25/22
LFJ
EPA200.7
Lead (dry weight basis), mg/kg
6.4
07/26122
MTM
311311-04
Magnesium (dry wC basis), mg/kg
5382
07/25/22
LFJ
EPA200.7
Mercury (dry wt. basis), mg/kg
0.19
08/02/22
MTM
EPA747111
Nickel (dry wt. basis), mg/kg
6
07/25/22
LFJ
EP�200.7
Potassium (dry wt. basis), mg/kg
3663
07/25/22
LFJ
EPA200.7
Selenium (dry wt. basis), mg/kg
<5.0
07/27/22
MTM
311311-04
Silver (dry wt. basis), mg/kg
< 2.5
07125/22
LFJ
EPA200.7
Sodium (dry wt. basis), mg/kg
< 1250
07/25/22
LFJ
EPA200.7
Zinc (dry wt. basis), mg/kg
330
07/25/22
LFJ
EPA200.7
Total Cyanide (dry weight), mg/kg
31.96
07/28/22
HMM
450OCNE-16
TKN (dry wt.), mg/kg
c 15120
07/26/22
KIES
351.2 R2-93
Ammonia Nitrogen, (dry wt.),mg/kg
c 59.86
08/02/22
RES
350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg
c 16270
07/26/22
TRJ
365.4-74
Nitrate+Nitrite (dry wt.), mg/kg
c 46.89
08/09/22
KES
353,2 112-93
Plant Available Nitrogen, mg/kg
6101
08/12/22
KES
Molybdenum, (dry wt. basis), mg/kg
< 5.0
07125/22
LFJ
EPA200.7
Drinking Water ID37715
Wastewater ID; 10
c Uncertified data, DWR does not offer non -aqueous certification for this analytical procedure.

J
Driakiag Water 1p3,1715
Wastewater 1Dz 10
„CAI F f-11 kl L E, N,
CITY OF NEW BERN (BIOSOLIDS)
ATTN: TONY HAWKINS
P.O. BOX 1129
NEW BERN, NC 28563
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt, basis), mg/kg
Cadmium (dry wt. basis), ingilig
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg1kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt, basis), mg/kg
Silver (dry wt. basis), mg/kg
Sodium (dry wt, basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Cyanide (dry weight), mg/kg
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry ivt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mg/kg
Holding Analysis Method
Basin (RA) Date Analyst Code
2549
08/11/22
LFJ
EPA200.7
2.5
08/11/22
MTM
3113B-04
365356
08111/22
LFJ
EPA200.7
<0.5
08112/22
MTM
3113B-04
98
08/10/22
LFJ
EPA200.7
5
08/10/22
LFJ
EPA200.7
5.4
08/12/22
MTM
3113B-04
3477
08/25/22
LFJ
EPA200.7
0.24
08/17/22
MTM
EPA7471B
< 5.0
08/10/22
LFJ
EiU00.7
1605
08/25/22
LFJ
EPA200.7
<5.0
08/11/22
MTM
3113B-04
< 2.5
08/10/22
LFJ
EPA200.7
< 1250
08/11/22
LFJ
EPA200.7
241
08/10/22
LFJ
EPA200.7
23.81
08/09/22
HMM
450OCNE-16
c 16150
08/11/22
BMD
351.2 112-93
c 225.5
08,112/22
BMD
359.1 R2-93
c 11680
08/11/22
TRJ
365.4-74
c 47.60
08/09/22
LEES
353.2 112-93
6530
08/29/22
TEES
< 5.0
08/10/22
LFJ
EPA200.7
REVIEWED BY:
F" F ',I �' 11 C 1 1. 4 L 1 ( : - I '. "
c Uncertified data. DWR does not offer non -aqueous Certification for this analytical procedure.

17",
U J[;1d;Ll
i'
CITY OF NEW BERN (BIOSOLIDS)
ATTN- TONY HAWKINS
P.O. BOX 1129
NEW BERN, NC 28563
Analysis
Method
PARAMETERS
Basin (RA)
Date
Analyst
Code
Aluminum, (dry wt. basis), mg/kg
4125
09/27122
MTM
EPA200.7
Arsenic (dry wt. basis), mg/kg
< 2.5
09127/22
MTM
3113B-04
Calcium (dry wt. basis), mg/kg
188291
09/30/22
MTM
EPA200.7
Cadmium (dry wt. basis), mg/kg
0.66
09/27/22
MTM
311311-04
Copper (dry wt. basis), mg/kg
202
09/27/22
MTM
EPA200.7
Chromium, T.(dry wt. basis),mg/kg
14
09/27/22
MTM
EPA200.7
Lead (dry weight basis), mg/kg
9.3
09/27/22
MTM
311311-04
Magnesium (dry wt. basis), mg/kg
6321
09/27/22
MTM
EPA200.7
Mercury (dry wt. basis), mg/kg
0.34
09/27/22
MTM
INN
EPA7471B
Nickel (dry wt. basis), mg/kg
9.1
09/27/22
EPA200,7
Potassium (dry wt. basis), mglkg
3833
09/30/22
MTM
EPA200.7
Selenium (dry wt. basis),. mg/kg
< 5.0
09/28/22
MTM
3113B-04
Silver (dry wt. basis), mg/kg
< 2.5
09/27/22
MTM
EPA200.7
Sodium (dry wt. basis), mg/lig
1552
09/27/22
MTM
EPA200.7
Zinc (dry wt. basis), mg/kg
470
09/27/22
MTM
EPA200.7
Total Cyanide (dry weight), mg/kg
116.4
09/20/22
HMM
450OCNE-16
TKN (dry wt.), mg/kg
c 30250
09/20/22
KES
351.2 182-93
Ammonia Nitrogen (dry wt.),mg/kg
c 63.63
09/21/22
KES
350.1 112-93
Phosphorus, T. (dry wt.), mglkg
c 19900
09/20/22
TRJ
365.4-74
Nitrate+Nitrite (dry wt,), mg/kg
c 82.52
09120/22
BMD
353.2 R2-93
Plant Available Nitrogen, mg/kg
12189
09/27/22
KES
Molybdenum (dry wt. basis), mg/kg
<5.0
09/27/22
MTM
EPA200.7
Drinking Water 10,; a7715
Wastewater IDg 10
DATE COLLECTED: 09/15/22
DATE REPORTED 09/30/22
REVIEWED BY.
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

CITY OF NEW BERN (BIOSOLIDS)
ATTIT: TONY HAWKINS
P.O. BOX 1129
NEW BERN, NC 28563
9 '�
REVIEWED BY:
Drinking Water ID37715
Wastewater TV; 10
7 E-,l
Holding
Holding
Holding
Holding
Holding
AnalysLs
Method
PARAMETERS Basin-FC#1
Basi71-FC#2
Basin-FC#3
Basin-FC#4
Basin-FC#5
Date Analyst
Code
Total Solids, % 27.45
27.40
25.34
29,16
26,66
09/15/22 JMS
2544G-15
Fecal Coliform (MPN), /gram Solids < 1.8
< 1.8
< 1.8
< 1,8
< 1.8
09/15/22 DNS
9221E-14

fIf f
Iq
2735
CITY OF NEW BERN (BIOSOLIDS)
ATTN: TONY HAWXINS
P.O. BOX 1129
NEW BERNI NC 28563
REVIEWED BY:
Holding
Holding
Analysis
Method
PARAMETERS Basin-FC#6
Basin-FC#7
Date Analyst
Code
Total Solids, % 2531
31.31
09/15/22 JMS
2540G-15
Fecal Coliform (MPN), /gram Solids < 1.8
< 1.8
0945/22 DNS
9221E-14
DrinkiZg W&ter rD: 37715
WasLewater ID; 10

CITY OF NEW FERN (BIOSOLIDS)
ATTN: TONY HAWKINS
P.0, BOX 1129
NEW BERN, NC 28563
Holding
Analysis
Method
PARAMETERS Basin
(RA)
Date Analyst
Code
Aluminum, (dry mi. basis), ing/kg
4240
10/18/22
TWIT M
EPA200.7
Arsenic (dry wt. basis), mg/kg
<15
10121/22
MTM
3113B-04
Calcium (dry wt. basis), mg/kg
230300
10/17/22
MTM
EPA200.7
Cadmium (dry wt. basis), nig/kg
0.59
10/19/22
MTM
311313-04
Copper (dry wt. basis), mg/kg
180
10/17/22
MTM
EPA200.7
Chromium, T.(dry wt. basis),mg/kg
13
10/17/22
MTM
EPA200.7
Lead (dry weight basis), ing/kg
10
10/18/22
MTM
311313-04
Magnesium (dry wt. basis), mg/kg
5427
10/17122
MTM
EPA200.7
Mercury (dry wt. basis), mglkg
0.33
10/13/22
MTM
EPA7471B
Nickel (dry wt. basis), ing/kg
8.5
10117/22
Wf M
0A200.7
Potassium (dry wt. basis), mg/kg
3597
10/18/22
NTTM
EPA200.7
Selenjum (dry wt. basis), rng/kg
< 5,0
10/24/22
MTM
311313-04
Silver (dry wt. basis), mglkg
2.9
10/17/22
MTM
EPA200,7
Sodium (dry wt. basis), ntgikg
1404
10/17/22
MTM
EPA200.7
Zinc (dry wt, basis), inglkg
495
10i17/22
MTM
EPA200.7
Total Cyanide (dry weight), mg/kg
41.65
10/17/22
HMM
450OCNE-16
TKN (dry wt.),, mg/kg
c 31120
10/11/22
TIZJ
351.2 1t2-93
Ammonia Nitrogen (dry wt,),mgtkg
c 538.9
10/11/22
KES
350A R2-93
Phosphorus, T. (dry wt.), mg/kg
c 18610
10/11/22
BMD
365.4-74
Nitrate+Nitrite (dry wt.), mg/kg
C 50,89
10/11122
KE S
353.2 112-93
Plant Available Nitrogen, Eng/kg
12553
10/18/22
KES
Molybdenum (dry wt. basis), mg/kg
< 5.0
10/17/22
MTM
EPA200.7
ID#: 214
DATE COLLECTED: 10/06/22
DATE REPORTED : 10/25/22
,
REVIEWED BY.
c Uncertified data. DWR does not offer ncn-aqueous certification for this analytical procedure.

�p,��,����1������.�li�l!�.�����1�°���:����u r���A� ��Ii.����G�,k��,,���'�cN��o��p�` �������uo��..x��f�
Drinking Water TD: 37715
114 0/kWOP4 I- ID`WVF-E
GREENIVU I IE, NtC, 27858
CITY OF NEW BERN (BIOSOLIDS)
ATTN: TONY HAWKINS
P.O. BOX 1129
NEW BERN, NC 28563
REVIEWED BY:
Holding
Analysis
Method
PARAMETERS Basin (RA)
Date
Analyst
Code
Aluminum, (dry wt. basis), mg/kg
3247
11/16/22
MTM
EPA200.7
Arsenic (dry wt. basis), rng/kg
< 2.5
11/17/22
DRC
3113B-04
Calcitan (dry wt. basis), mg/kg
205604
11/16/22
MTM
EPA200.7
Cadmium (dry wt. basis), mg/kg
0.52
11/17/22
DRC
311311-04
Copper (dry wt. basis), mg/kg
151
11121/22
MTM
EPA200.7
Chromium, T.(dry wt. basis),mg/kg
9.4
11/16/22
MTM
EPA200.7
Lead (dry weight basis), mg/kg
7.3
11/17/22
DRC
311311-04
Magnesium (dry wt. basis), mg/kg
5940
11/21/22
MTM
EPA200.7
Mercury (dry wt. basis), mg/kg
0.24
11/22/22
DRC
EPA7471B
Nickel (dry wt. basis), mg/kg
7.0
11/21/22
MTM.
EPA200.7
Potassium (dry wt. basis), mg/kg
4561
11116/22
MTM
EPA200.7
Selenium (dry wt. basis), mg/kg
<5X
11/16/22
DRC
3113B-04
Silver (dry wt. basis), mg/kg
3A
11/16/22
MTM
EPA200.7
Sodium (dry wt. basis), mgikg
1411
11116/22
MTM
EPA200.7
Zinc (dry wt. basis), mg/kg
344
11/16/22
MTM
EPA200.7
Total Cyanide (dry weight), mg/kg
13.79
11/09/22
HMM
4500CNE-16
TKN (dry wt.), mg/kg
c 28330
11/15122
TRJ
351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/kg
c 80.85
11/15/22
KES
350.1 R2-93
Phosphorus, T. (dry wt.), mg/leg
c 20680
II/W22
BMD
365.4-74
Nitrate+Nitrite (dry wt.), mg/kg
c 43.92
11/15/22
KES
353.2 R2-93
Plant Available Nitrogen, mg/kg
11384
11/16/22
KES
Molybdenum (dry wt. basis), mg/kg
< 5.0
11121/22
MTM
EPA200.7
G:152� 7 5(5- j2M3
FAX �252) 756 063'3
c Tincertified data. DWR does not offer non -aqueous certification for this analytical procedure.

,iF",EF.,'NV1H F, N 27858
CITY OF NEW BERN (BIOSOLIDS)
ATTN: TONY HAWKINS
P.O. BOX 1129
NEW BERN, NC 28563
FAY (",252) 1
DATE COLLECTED: 11/03/22
DATE REPORTED : 11/09/22
REVIEWED BY:
Holding
Holding
Holding
Holding
Holdhig
Analysis
Method
PARAMETERS Basin-FC#1
Basin-FC#2
Basin-FC#3
Basin-FC#4
Basin-FC#5
Date Analyst
Code
Total Solids, % 26.90
26.42
25.13
25.40
24.48
11/03/22 JMS
2540G-15
Fecal Coliform (MPN), /gram Solids 2.9
< 1.8
< 1.8
< 1.8
<1.8
11/03/22 JDJ
9221E-14

2 7858
CITY OF NEW BERN (BIOSOLIDS)
ATTN: TONY HAWKINS
P.O. BOX 1129
NEW BERN, NC 28563
Wattewatex ID� 10
71' r32(7)8
DATE COLLECTED: 11/03/22
DATE REPORTED . 11/09/22
Holding
Holding
Analysis
Method
PARAMETERS Basin-FC#6
Basin-FC#7
Date Analyst
Code
Total Solids, % 25.21
26.57
11/03/22 JMS
2540G-15
Fecal Coliforru (MPN), /gram Solids <1.8
< 1.8
11/03,/22 JDJ
9221E-14

j 'E" � "[1] DU '11raa
"I I t 0AKM1(')J14]' DRIVE
GFiEEP,,Mll ] IE, N,C 27858
wl2
CITY OF NEW BERN (BIOSOLIDS)
ATTN: TONY HAWKINS
P.O. BOX 1129
NEW BERN, NC 28563
REVIEWED BY:
Holding
Analysis
Method
PARAMIETERS Basin
(RA)
Date Analyst
Code
Aluminum, (dry wt. basis), mg/kg
2224
12/08/22
MTM
EPA200.7
Arsenic (dry wt. basis), mg/kg
< 2.5
12/08/22
DRC
311313-04
Calcium (dry wt. basis), mg/kg
287670
12/08/22
NIT
EPA200.7
Cadmium (dry wt. basis), mg/kg
<0.5
12/12/22
DRC
311313-04
Copper (dry wt. basis), mg/kg
99
12/08/22
MTM
E1"A200.7
Chromium, T.(dry wt. basis),rng/kg
4.0
12/08/22
MTM
EPA200.7
Lead (dry weight basis), mg/kg
4.6
12/12/22
DRC
3113B-04
Magnesium (dry wt. basis), mg/kg
5637
12/08/22
MTM
EPA200.7
Mercury (dry wt. basis), mg/kg
0.12
12/13/22
DRC
EPA7471B
Nickel (dry wt. basis), mg/kg
<5.0
12108/22
I%ffM
EPA200.7
Potassium (dry wt. basis), mg/kg
3887
12/09/22
?vff M
EPA200.7
Selenium (dry wt. basis), mg/kg
< 5.0
12/09/22,
DRC
3113B-04
Silver (dry wt. basis), mg/kg
2.7
12/08/22
MTM
EPA200.7
Sodium (dry wt. basis), mg/kg
1659
12/08/22
MTM
L, PA200 . 7
Zinc (dry wt. basis), mg/kg
232
12/08/22
MTM
EPA200.7
Total Cyanide (dry weight), mg/kg
37.74
12/14/22
HMM
450OCNE-16
TKN (dry wt.), mg/kg
c 25620
12/08/22
BMD
35L2 R2-93
Ammonia Nitrogen (dry wt.),mg/kg
c 211.7
12/12/22
T PUT
350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg
c 21090
12/08122
KES
365.4-74
Nitrate+Nitrite (dry wt.), mg/kg
c 49.93
12/07/22
KES
353.2 122-93
Plant Available Nitrogen, mg/kg
10320
12/27/22
ICES
Molybdenum (dry wt. basis), mg/kg
< 5.0
12/09/22
MTM
EPA200.7
FIF,10114E (252) 756-4,3208
��:�:,AX (252) 756­101("333
c Uncertified data, DWR does not offer non -aqueous certification for this analytical procedure.

V
1,he result: Sit forth IIQI•en' l "IrQ rcovitle d by SGS w-th Arnerica Inc.
Technical Report for'
Environment 1, Inc
City of New Bern (Biosoilds); New Bern, NC
214A
SGS Job Number: FA97918
Sampling Date: 08/03/22
Report to:
Environment 1, Inc
PO Box 7085
Greenville, NC 27835
abrown@envlronTl7 e-nt l lnc . com
TTN: Ann Brown
Antoumted Report
Test results contained within this data package meet the requirements Norm Farmer
of the National Environmental Laboratory Accreditation Program Technical Director
and/or state specific certification programs as applicable.
Client Service contact: Ariel Hartney 407-425-6700
Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, IL, UT, VT, WA, Wl, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
SGS mtit a sole uta to ,v 4 i LA �3L motl ttc ito 3� it, tlxis ou cix.aeto' 1' easo sbarc voqa ideas akxwt
r <:t3t1_ortr�� tt��rE1:.�c�titio -t t} is report i5 e:i Lt3 ntlE��,i;:cl, how %� L' Can sake v0u l at_
G
1 of 26
FA D7918

SGS North America Inc.
Sample Summary
Environment 1, Inc
Job No: FA97918
City of New Bern (Biosoilds); New Bern, NC
Project No: 214A
,ample
Collected
Matrix
Client
dumber
Date Time By
Received Code 'Type
Sample ID
......
Thrs rprrt corits results rrted a� Nll Tot detected Tl�ec�llgoapples
Organics ND = Not detected above the MDL
FA97918-1 08/03/22 13:25 AH 08/06/22 SO Soil
FA979i8-11';.. 08/03/22 I3:25 AH 08/06/22 SO Soil
HOLDING BASIN (RA)
............................................................ .
HOLDING BASIN (RA)
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
L:7
FA97918

Summary of Hits
Job Number:
FA97918
Account:
Environment 1, Inc
Project:
City of New Bern (Biosoilds); New Bern, NC
Collected:
08/03/22
Lab Sample ID Client Sample ID Result/
Analyte Qual RI, MDL Units Method
FA97918-1 HOLDING BASIN (RA)
Corrosivity as pH 12.1'
FA97918-1I, HOLDING BASIN (RA)
2-Butanone (MEK) 0,0352J..0.050
su
0.020 mg/I
SW846 CHAP?
SW846 8260D
Page 1 of 1
4 of 26
FAVM

SGS North America Inc.
Report of Analysis
Client Sample ID: HOLDING BASIN (RA)
Lab Sample ID: FA97918-1 Date Sampled: 08/03/22
Matrix: SO - Soil Date Received: 08/06/22
Percent Solids: 35.2
Project: City of New Bern (Biosoilds); New Bern, NC
General Chemistry
Analyte
Corrosivity as pH
Solids, Percent
RL = Reporting Limit
Page 1 of 1
Result
RL Units
DF
Analyzed
By
Method
12.1 _
su
1
08/16/22 15:35
ST
SW846 CHAP?
35.2
%
1
08/10/2215:20
ST
SM1925400
F1
6 of 26
FAV91 a

SGS North America Inc.
Report of .Analysis
ent Sample ID: HOLDING BASIN (RA)s
ab Sample ID: FA97918-1L Date Sampled: 08/03/22
Matrix: SO - Soil Date Received: 08/06/22
Method: SW846 9260D SW846 1311 Percent Solids: 35.2
Project: City of New Sera (Biosoilds); New Bern, NC
Page 1 of 1
L
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
:un #1 2P92205.D
10
08/22/22 17:29
JL
08/15/22 14:00
OP92563
V2P3559
1,un #2 5E33639.D
10
08/24/22 13:16
JL
08/15/22 14:00
OP92563
V5E1537
Purge Volume
:un 41 5.0 ml
:un #2 5.0 ml
VOA TCLP List
CAS No. Compound
71-43-2
Benzene
78-93-3
2-Butanone (MEK)
56-23-5
Carbon Tetrachloride b
108-90-7
Cblorobenzene
67-66-3
Chloroform
106-46-7
1,4-Dichlorobenzene
107-06-2
1,2-Dichloroethane
75-35-4
1, 1 -Dichloroethylene
127-18-4
Tetrachloroethylene
79-01-6
Trichloroethylene
75-01-4
Vinyl Chloride
CAS No. Surrogate Recoveries
1868-53-7 Di.bromofluoromethane
17060-07-0 1,2-Dichloroethane-D4
2037-26-5 Toluene-D8
460-00-4 4-Bromofluorobenzene
Result HW# MCL RL
ND
D018
0.50
0.010
00352''
D035
200
0.050
ND
D019
0.50
0.010
ND
D021
100
0.010
ND
D022
6.0
0.010
ND
D027
7.5
0.010
ND
D028
0.50
0.010
ND
D029
0.70
0.010
0.70
0.010
.ND...D039
'ND
D040
0.50
0.010
ND :
D043
0.20
0.010
Run# I Run# 2 Limits
98%
100%
83-118%
109%
10:0%
79-125%
95%
103%
85-112%
101%
.109%
83-118%
(a) Result is from Run# 2
(b) Associated CCV outside control limits high, sample is ND,
TCLP Leachate method SW846 1311
MDL Units Q
0.0031
mg/1
0.020
mg/1 J
0.0036
mg/1
0.0020
mg/1
0.0030
mgh
0.0026
mg/1
0.0031
mg/l
0.0032
mgh
0.0022
mg/1
0.0035
mg/I
0.0041
mg/I
ND — Not detected MDL = Method Detection Limit J — Indicates an estimated value
MCL = Maximum Contamination Level (40 CFR 261 7/1/I 1) B — Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 26
FA97918

SGS North America Inc.
Deport of .Analysis
Client Sample ID: HOLDING BASIN (RA)
Lab Sample ID: FA97918-IL Date Sampled: 08/03/22
Matrix: SO - Soil Date Received: 08/06/22
Method: SW846 8270E SW846 3510C Percent Solids: 35.2
Project: City of New Bern (Biosoilds); New Bern, NC
Page 1 of 1
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
,un #1 6FI5308.D 1 08/16/22 16:19 WH 08/16/22 08:02 OP92584 S617572
,un #2
Initial Volume Final Volume
.un #1 100 znl 1.0 ml
,un #2
ABN TCLP List
CAS No. Compound
95-48-7 2-Methylphenol
3&4-Methylphenol
87-86-5
Pentachlorophenol
95-95-4
2,4,5-Trichlorophenol d
88-06-2
2,4,6-Trichlorophenol
106-46-7
1,4-Dichlorobenzene
121-14-2
2,4-Dinitrotoluene
118-74-1
Hexachlorobenzene
87-69-3
Hexachlorobutadiene
67-72-1
Hexachloroethane
98-95-3
Nitrobenzene
110-96-1
Pyridine
CAS No. Surrogate Recoveries
367-12-4
2-Fluorophenot
4165-62-2
Phenol-d5
118-79-6
2,4,6-Tribromophenol
4165-60-0
Nitrobenzene-d5
321-60-8
2-)~luorobiphenyl
1718-51-0
TeTphenyl-d14
Result RW# MCL RL
ND
D023
200
0.050
ND
D024
200
0.050
ND
D037
100
0.25
ND
D041
400
0.050
ND
D042
2,0
0,050
ND
D027
7.5
0.050
NIX
D030
0.13
0A50
ND
D032
0.13
0.050
ND
D033
0.50
0.050
ND
D034
3.0
0.050
ND
D036
2.0
0.050
ND
D038
5.0
0.10
Run# 1 Run# 2 Limits
3'6%d' .
14-67%
27°Jo
10-50%
::: :
33-118%
76%%:. ':
42-108%
.
40-106%
83%
39-121%
(a) Associated CCV outside of control limits high, sample was ND.
TCLP Leachate method SW846 1311
MDL Units Q
0.0056 mg/l
0.0098 mg/l
0.050 mg/1
0.0074 mgll
0.0075 mg/l
0.0050 mgll
0.0081 mgll
0.0069 mgll
0.0050 mg/I
0.016 mg/I
0.0093 mg/I
0.020 mg/1
ND mm Not detected MDL — Method Detection limit J = Indicates an estimated value
MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N Indicates presumptive evidence of a compound
N�
8of26
FA97913

SGS North America Inc.
Report of analysis
Client Sample Ill. HOLDING BASIN (RA)
Lab Sample ID: FA97918-IL Date Sampled: 08/03/22
Matrix: SO - Soil Date Received: 08/06/22
Method: SW846 8151A SW846 351OC Percent Solids: 35.2
Project: City of New Bern (Biosoilds); New Bern, NC
Page I of I E
M I
File ID DF ,Analyzed By Prep Date Prep Batch Analytical Rauh
Run #1 CC084314.1) 1 08/17/22 17:09 AF 08/16/22 08:12 OP92586 GCC2164
Run #2
Initial Volume Final Volume
Run #1 10.0 ml 5.0 ml
Run #2
Herbicide TCLP List
CAS No.
Compound
94-75-7
2,4-D
93-72-1
2,4,5-TP (Silvex)
CAS No.
Surrogate Recoveries
19719-28-9
2,4-DCAA
TCLP Leachate method SW846 1311
Result
IIW#
MCL RL
MDL Units Q
ND
D016
10 0.050
0.017 mg/I
ND
D01.7
1.0 0.0050
0.0013 mg/1
Run# 1
Run# 2
Limits
700N ''
39-135%
ND = Not detected MDL — Method Detection Limit J = Indicates an estimated value
MCL — Maximum Contamination Level (40 CPR 261 7/1/11) B = Indicates analyte found in associated method blank
L — Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound

SGS North America Inc.
Report of Analysis
;lient Sample ID: HOLDING BASIN (RA)
gab Sample ID: FA97918-IL Date Sampled: 08/03/22
latrix: SO - Soil Date Received: 08/06/22
Zehod: SW846 8081E SW846 3510C Percent Solids: 35.2
'roject: City of New Bern (Biosoilds); New Bern, NC
Page 1 of 1
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ST163253.1) 1 08/16/22 18:22 EM 08/16/22 08:06 OP92585 GST3978
Run #2
Initial Volume Final Volume
un #1 100 ml 5.0 ml
un #2
Pesticide TCLP List
TCLP Leachate method SW846 1311
CAS No.
Compound
Result
HW#
MCL RL
MDL
Units Q
58-89-9
gamma-BHC (Lindane) a
ND
D013
0.40 0.00010
0.000022
mg/1
12789-03-6
Chlordane
ND
D020
0.030 0.0010
0.00038
mg/1
72-20-8
Endrin
ND
D012
0.020 0,00020
0,000021
mg/1
76-44-8
Heptachlor
ND
D031
0.0080 0,00010
0.000026
mg/1
1024-57-3
Heptachlor epoxide
ND
D031
0.0080 0.00010
0.000020
mg/1
72-43-5
Methoxychlor a
ND
D014
10 0.00020
0.000050
mg/1
8001-35-2
Toxaphene
ND
D015
0.50 0.0050
0.0021
mg/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
877-09-8
Tetrachloro-m-xylene
.85%
42-127%
2051-24-3
Decachlorobiphenyl
109%
27-127%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit 1 — Indicates an estimated value
MCI. — Maximum Contamination Level (40 CFR 261 7/l/11) B = Indicates analyte found in associated method blank
E — Indicates value exceeds calibration range N — Indicates presumptive evidence of a compound
11
10 of 26
FAO'T918

SGS North America Inc.
Report of Analysis
:lient Sample ID: HOLDING BASH (RA)
,ab Sample ID: FA97918-1L Date Sampled: 08/03/22
4atrix: SO - Soil Date .Received: 08/06/22
Percent Solids: 35.2
'roject: City of New Bern (Biosoilds); New Bern, NC
Page 1 of 1
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DIa .Prep Analyzed By Method Prep Method
Arsenic
< GAO
D004
5.0
0.10
mg/1
1
08/19/22
08/22/22
LM
SW846 601OD 2
SW846 3010A 4
Barium
<2.0
D005
100
2.0
mg/1
1
08/19/22
08/22/22
LM
SW846 601OD 2
SW946 3010A 4
Cadmium
< 0.05 0.
D006
1.0
0.050
mg/1
1
08/19/22
08/22/22
LM
SW846 601OD 2
SW846 3010A 4
Chromium
<0.10
D007
5.0
0.10
mg/1
1
08/19/22
08/22/22
LM
SW846 6010D 2
SW846 3010A 4
Lead
<0.050
D008
5,0
0.050
mg/1
1
08/19/22
08/22/22
LM
SW846 601OD 2
SW846 301OA 4
Mercury
<0.0050':
D009
0.20
0.0050
mg/1
1
08/18/22
08/18/22
.1c
SW846 7470A 1
SW846 7470A 3
Selenium
<0110
D0W
1.0
0.10
mg/1
1
08/19/22
09/22/22
LM
SW846601OD2
SW8463010A4
Silver
< 0:10
D011
5.0
0.10
mg/1
1
08/19/22
08/22/22
LM
SW846 601OD 2
SW846 3010A 4
(1) Instrument QC Batch: MA18853
(2) Instrument QC Batch: MA18858
(3) Prep QC Batch: MP41096
(4) Prep QC Batch: MP41100
RL = Reporting .Limit
MCL = Maximum Contamination Level (40 CFR 261 7/1/11)
SGS Ii Ot26
FA97M

SAMPLE SUMMARY
Ca!!ccled by Collected dat- lAirne Received datel':ime
'HOLDING BASIL (RA) L1524201-01 Solld
68;C3r22 `3 25 OS111J22 OSA5
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
dateltime
dateltime
i
Wet Chemistry by Method 9012 3
WG1906868
1 08/12/22 1518
0811312211:50
LDT
Mt. Juliet, TN
Wet Chemistry by Method 9034-9030B
WG1910308
1 C811312210:00
08/1412217:00
RMR
Mt. Juliet, TN
Wet Chemistry by Method D93/1010A
WG1911295
1 C8116J22 02:00
08/16/22 02:00
JAR
Mt. Juliet, TN
c
e�t
i
BSc

HQLDING.BASIN (RA) SAMPLE RESULTS - 01
1
Collected dateltime: 08/O 1M 13:25 _ _ _ L1524201 - _ -
Wet� Chemistry by Method 9012 B
Result Qualifier LQQ Dilution Analysis
Analyte mglkg inglkg date ! time
Reactive Cyanide C 392 0.300 1 OS1131202211.50
Wet Chemistry by McIl-iod 9034-9030B
Result Qualifier 1-O0 Dilution Analysis
Analyte mg/kg rng/kg date ! time
.. ... ... ......... ....._... ..
Reactive Sulfide ND 7'8 75.0 1. 08114I202217700
Wet Chemistry by Metod D93/1010A
Result Oualifier Dilution Analysis Batch
Analyte Deg. F date I time
Ignitabd€ty DNI at 170 1 08/1612022 02:00 WG1911295

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=AS7918

ANNUAL PATI-1C1bCgEN AND VECTOR ATTRACTION REDUCTION FORM (02'r Rules)
Facility Name: City of New Bern WQ Permit Number. WQ0023306
WWTP Flame: City of New fern WWTP
NPl)ES Number:
Monitoring Period; From 1i1/2022 To 12/31/202.2
Pathogen Deduction (1.5A NCAC 02T.1106) - Please indicate level achieved and alternative perfor ed-
Class A4
Alt, A (time/temp) N�
Alt B (Alk Treatment) N" ,„
Alt. (Prier "l"estln) ,
Alt.l (1Jri Priem Test)
Pieces to Fui-ther Reduce Pathogengs F I
If applicable to alternative
performed (Class A only) indicate "Process to Further Deduce Pathogens":
Compost
fleat. Drying D
Feat Treatment [J
`I"herniophilic
Beta Ray
y (
Garni-na Ray ND
Pasteurization , w �
Class
Alt. (1) Fecal Density N
Alt. (G) Process to ST 1 icantly Reduce Pathogens
If applicable to alternative performed (Class II only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization �„ Air Drying Non Composting; [J Aerobic Digestion NW, i
Anaerobic Digestior. E)'
If applicable to alternative performed (Class A or Class Il) complete the following monitoring data;
Allowable Level Pathogen Density um er o Analytical
� y Frequency Sample
"fech-
Parameter in Sludge Excee- of Analysis Type
M.inimu Geo. Mean Units
dences ni ua e
2 x 10 to the
MPN
<1.8
1.8
<1.8
MPN
7
bi month])
grab
n/a
6tb power
per grain of
l"ecal Coliforrn
total solids
CFU
1000 mpn per gram
of.'total solid (dry
weight)
Salmonella bacteria
3 MPN per 4 grams
(in lieu of fecal
total solid (dry
colifomi
Wei lrt
Ve�6r Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative a
Alt.l (VS reduction) N of
Alt. 2 (40-day bend) [I
"Alt. 3 (30 day bench) El
I Alt. 4 (Spec. 02 uptake) N
Alt. 5 (1.4-Day Aerobic) (III
Alt. 6 (Alk. Stabilization l l
Alt 7 (Drying - Stable) o
Alt. 8 (Drying - Unstable)
Alt. 9 (Injection) (j
Alt. 10 (incorporation) 0
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT ENT (please cheek the appropriate statement)
NM "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .11.07 have been met."
"I certify, render penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T.1107 have not been meet," (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been meta I am aware that there are
significant penalties for false certification including fine and imprisonment."
Tony Hawkins / Manager
Preparer Name and Tit (type t or print) Land. Applier Name and Title (if applicable)(type or print)
ri.
(,Signature i
(,, g of Preparcr* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26)
DENR FORM PVRF 02T (12/2006)