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HomeMy WebLinkAboutNC0023906_Application_20181203ROY COOPER NORTH CAROLINA Cotmnr Ertv&wwwnW Quality NUCHAEL S_ REGAN secrsOmy LINDA CULPEPPER Iiw r Diracmr December 03, 2018 Harry Tyson, Deputy City Manager City of Wilson 112 Goldsboro St E PO Box 10 Subject: Permit Renewal Application No. NCO023906 Wilson WWTP Wilson County Dear Applicant: The Water Quality Permitting Section acknowledges the December 3, 2018 receipt of your permit renewal application and supporting documentation. Your application will be assigned to a permit writer within the Section's NPDES WW permitting branch. Per G.S. 150E-3 your current permit does not expire until permit decision on the application is made. Continuation of the current permit is contingent on timely and sufficient application for renewal of the current permit. The permit writer will contact you if additional information is required to complete your permit renewal. Please respond in a timely manner to requests for additional information necessary to allow a complete review of the application and renewal of the permit. Information regarding the status of your renewal application can be found online using the Department of Environmental Quality's Environmental Application Tracker at: https•lldeg nc gov/permits-regulations/permit-guidance/environmental-application-tracker If you have any additional questions about the permit, please contact the primary reviewer of the application using the links available within the Application Tracker. ec: WQPS Laserfiche File w/application Sincerely, (� Wren Thedford Administrative Assistant Water Quality Permitting Section Q�� North Carolina Department of Environmental Quality I Division of Water Resources 1617 Mail service Center I Raleigh, North Carolina 27699-1617 919-807-6300 NORTH CAROLINA Justification for Reduction of Monitoring for City of Wilson Hominy Creek Water Reclamation Facility NPDES Permit No. NCO023906 As per NCDENR's document "DWQ Guidance Regarding the Reduction of Monitoring Frequencies in NPDES Permits for Exceptionally Performing Facilities" dated October 22, 2012, we respectfully request that the monitoring frequencies for BOD5, TSS, NH3-N, and Fecal Coliform be continued at the recommended twice per week minimum. The City of Wilson Hominy Creek Water Reclamation Facility is an Exceptionally Performing Facility and has demonstrated consistent, long-term treatment performance at levels far below effluent limitations (<50%) and should be considered for a reduction in monitoring from existing permit frequencies to a 2/week minimum frequency for BOD5, TSS, NH3-N, and Fecal Conform. Our facility meets all of the approval criteria for this request as outlined in the document: • The facility has not experienced a civil penalty assessment for permit limit violations for each target parameter during the previous three years. • Neither the permittee, nor any of its employees, have been convicted of criminal violations of the Clean Water Act within the previous five years. • The facility is not currently under a SOC for target parameter effluent limit noncompliance. • The facility is not on EPA's Quarterly Noncompliance Report for target parameter limit violations. • For BOD5, TSS, NH3-N, and Fecal Coliform, the three year arithmetic mean of effluent data is less than 50% of the monthly average limit. Parameter 3 year arithmetic mean Monthly Avp, Limit % of Monthly Avii. Limit BODs 1.1 m 5.0 m 22% <50% TSS 0.14 mg1L 30.0 m 0.5% <50% NH3-N 0.06 m 1.0 m 6% <50% Parameter 3 ar geometric man Monthly An, Limit % of Monthly Avg. Limit Fecal 1 3 cfu/100 mL 200 cft/100 mL 1.5% <50%) • No more than 15 daily sampling results over the 3 year review period exceeded 200% of the monthly average limit for BOD5, TSS, and NH3-N. o BOD: 200% of Summer monthly average limit of 5.0 mg/L equals 10.0 mg/L. BOD: 2000/ of Winter monthly average limit of 10.0 mg/L equals 20.0 mg/L. During the 3 year review period, no data exceeded 10.0 mg/L during the Summer and no data exceeded 20.0 mg/L during the Winter. Page 1 of 2 CITY OF WILSON INCORPORATED 1849 WATER RECLAMATION DIVISION I PO. BOX 10 1 WILSON, NORTH CAROLINA 27894-0010 I I252I 399-2491 I (252) 399-2209 EQUAL OPPORTUNITY EMPLOYER I AFFIRMATIVE ACTION EMPLOYER FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: City of Wilson - Hominy Creek WRF, NCO023906 Renewal FORM 2A NPDES FORM 2A APPLICATION OVERVIEW NPDES APPLICATION OVERVIEW RIVER BASIN: Neuse Form 2A has been developed in a modular format and consists of a "Basic Application Information" packet and a "Supplemental Application Information" packet. The Basic Application Information packet is divided into two parts. All applicants must complete Parts A and C. Applicants with a design flow greater than or equal to 0.1 mgd must also complete Part B. Some applicants must also complete the Supplemental Application Information packet. The following items explain which parts of Form 2A you must complete. BASIC APPLICATION INFORMATION: A. Basic Application Information for all Applicants. All applicants must complete questions A.1 through A.B. A treatment works that discharges effluent to surface waters of the United States must also answer questions A.9 through A.12. B. Additional Application Information for Applicants with a Design Flow 2 0.1 mgd. All treatment works that have design flows greater than or equal to 0.1 million gallons per day must complete questions B.1 through B.6. C. Certification. All applicants must complete Part C (Certification). SUPPLEMENTAL APPLICATION INFORMATION: D. Expanded Effluent Testing Data. A treatment works that discharges effluent to surface waters of the United States and meets one or more of the following criteria must complete Part D (Expanded Effluent Testing Data): 1. Has a design flow rate greater than or equal to 1 mgd, 2. Is required to have a pretreatment program (or has one in place), or 3. Is otherwise required by the permitting authority to provide the information- E. Toxicity Testing Data. A treatment works that meets one or more of the following criteria must complete Part E (Toxicity Testing Data): Has a design flow rate greater than or equal to 1 mgd, 2. Is required to have a pretreatment program (or has one in place), or 3. Is otherwise required by the permitting authority to submit results of toxicity testing. F. Industrial User Discharges and RCRAICERCLA Wastes. A treatment works that accepts process wastewater from any significant industrial users (SIUs) or receives RCRA or CERCLA wastes must complete Part F (Industrial User Discharges and RCRA/CERCLA Wastes). SIUs are defined as: 1. All industrial users subject to Categorical Pretreatment Standards under 40 Code of Federal Regulations (CFR) 403.6 and 40 CFR Chapter I, Subchapter N (see instructions); and 2. Any other industrial user that: a. Discharges an average of 25,000 gallons per day or more of process wastewater to the treatment works (with certain exclusions); or b. Contributes a process wastestream that makes up 5 percent or more of the average dry weather hydraulic or organic capacity of the treatment plant; or C. Is designated as an SIU by the control authority. G. Combined Sewer Systems. A treatment works that has a combined sewer system must complete Part G (Combined Sewer Systems). ALL APPLICANTS MUST COMPLETE PART C (CERTIFICATION) EPA Form 3510-2A (Rev. 1-99). Replaces EPA fortes 7550-6 6 7550-22. Page 1. of 4 s2 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: City of Wilson - Hominy Creek WRF, NC002— Renewal Neuse BASIC APPLICATION INFORMATION PART A. BASIC APPLICATION INFORMATION FOR ALL APPLICANTS: All treatment works must complete questions A.1 through A.8 of this Basic Application Information Packet A.I. Facility Information. Facility Name City of Wilson — Hominy Creek Water Reclamation Facility Mailing Address P.O. Box 10 Wilson NC 27894-0010 Contact Person Jimmy Pridoen Tide Water Reclamation Manager Telephone Number (252) 399-2491 - office / (252) 205-2519 - cell Facility Address 3100 Stantonsburg Road (not P.O. Box) Wilson NC 27893 A.2. Applicant Information. if the applicant is different from the above, provide the following: Applicant Name Same as above Mailing Address Same as above Same as above Contact Person came as above Title Same as above Telephone Number (Same as above) Same as above Is the applicant the owner or operator (or both) of the treatment works? ® owner ® operator Indicate whether correspondence regarding this permit should be directed to the facility or the applicant ® facility ❑ applicant A.3. Existing Environmental Permits. Provide the permit number of any existing environmental permits that have been issued to the treatment works (include state -issued permits). NPDES NCO023906 PSD NA UIC NA Other W00001896 & W00023177 RCRA NA Other W00018709 & NCG110000/NCG110081 A.4. Collection System Information. Provide information on municipalities and areas served by the facility. Provide the name and population of each entity and, if known, provide information on the type of collection system (combined vs. separate) and its ownership (municipal, private, etc.). Name Population Served Type of Collection System Ownership Wilson 49.620 Separate Municipal Lucema 1128 Separate Municipal Black Creek & Sims 763 & 283 Separate & Separate Municipal & Municipal Total population served 51,794 EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 2 of 42 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RNER BASIN: City of Wilson - Hominy Creek WRF, NCO023906 Renewal Neuse If yes, describe the mean(s) by which the wastewater from the treatment works is discharged or transported to the other treatment works (e.g., tank truck, pipe). Not Applicable If transport is by a party other then the applicant, provide. Transporter Name NA Mailing Address NA NA Contact Person NA Title NA Telephone Number (NAI NA For each treatment works that receives this discharge, provide the following Name NA Mailing Address NA NA Contact Person NA Title NA Telephone Number (NA) NA If known, provide the NPDES permit number of the treatment works that receives this discharge NA Provide the average daily flow rate from the treatment works into the receiving facility. NA mgd e. Does the treatment works discharge or dispose of its wastewater in a manner not included in A8. through A8.d above (e.g., underground percolation, well injection) ❑ Yes ® No If yes, provide the following for each disposal method: Description of method (including location and size of site(s) if applicable): NA Annual daily volume disposed by this methodNA Is disposal through this method E] continuous or ❑ intermittent? NA EPA Form 3510-2A (Rev. 1-99). Replaces EPA fortes 7550-8 8 7550-22. Page 4 of 42 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: City of Wilson - Hominy Creek WRF, NCO023906 I Renewal I Neuse WASTEWATER DISCHARGES: If you answered "Yes" to question A.8.a, complete questions A.9 through A.12 once for each outlet) (including bypass points) through which effluent is discharged. Do not include information on combined sewer overflows in this section. If you answered "No" to question A.8.a. go to Part B. "Additional Application Information for Applicants with a Design Flow Greater than or Equal to 0.1 mgd." A.9. Description of Outfall. a. Outfall number b. Location (City or tam, if applicable) (Zip Code) (County) (State) 35° 40' 37" 77° 54' 51" (Latitude) (Longitude) C. Distance from shore (if applicable) NA fL d. Depth below surface (if applicable) NA R. e. Average daily flow rate 9.22 mgd f. Does this outfall have either an intermittent or a periodic discharge? ❑ Yes ® No (go to A.9.g.) If yes, provide the following information: Number f times per year discharge occurs: NA Average duration of each discharge: NA Average flow per discharge: NA mgd Months in which discharge occurs: NA g. is outfall equipped with a diffuser? ❑ Yes ® No A.10. Description of Receiving waters. a. Name of receiving water Contentnea Creek b. Name of watershed (if known) Contentnea United States Soil Conservation Service 14-digit watershed code (if known): 03020203020030 C. Name of State ManagementfRiver Basin (if known): Neuse River Basin United States Geological Survey 8-digit hydrologic cataloging unit code (if known): 03020203 d. Critical low flow of receiving stream (if applicable) acute NA cis chronic NA cs a. Total hardness of receiving stream at critical low flow (if applicable): NA mg4 of CaCO3 EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 8 7550-22. Page 5 of 42 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: City of Wilson - Hominy Creek WRF, NCO023906 Renewal Neuse A.11. Description of Treatment a. what level of treatment are provided? Check all that apply. ® Primary ® Secondary ® Advanced ® Other. Describe: Biological Nutrient Removal b. Indicate the following removal rates (as applicable): Design BOD5 removal gr Design CBOD5 removal 98 % Design SS removal 98 % Design P removal 80 % Design N removal 88 % Other NH,-N 93 % C. What type of disinfection is used for the effluent from this orltfall? If disinfection varies by season, please describe: Chlorination using liawd sodium hvoochlor to If disinfection is by chlorination is dechlonnation used for this oulfall? ® Yes ❑ No Does the treatment plant have post aeration? ® Yes ❑ No A.12. Effluent Testing Information. All Applicants that discharge to waters of the US must provide effluent testing data for the following parameters. Provide the indicated effluent testing required by the permitting authority for each outfall through which effluent is discharged. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. At a minimum, effluent testing data must be based on at least three samples and must be no more than four and one-half years apart Outfall number: 001 (3-Year Data Set Used: October 2015 - September 2018) MAXIMUM DAILY VALUE AVERAGE DAILY VALUE PARAMETER Value Units Value Units Number of Samples pH (Minimum) 6.08 &u. pH (Maximum) 7.86 &u. Flow Rate 29.98 MGD 9.22 MGD 1,096 Temperature(writer) (Nov -Mar) 22.1 °C 15.3 °C 310 Temperature (Summer) (Apr -Oct) 28.5 °C 23.0 °C 439 ' For pH please report a minimum and a maximum dail value MAXIMUM DAILY AVERAGE DAILY DISCHARGE POLLUTANT DISCHARGE ANALYTICAL ML/MDL Cone. Units Cone. Units Number of METHOD Samples CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS BIOCHEMICAL OXYGEN OD5 8.3 m IL 1.1 m /L 740 SM5210 B 2.0 DEMAND (Report one) �CB0D5 NA NA NA NA NA NA NA FECAL COLIFORM '(Geometric Mean) 1,200 almlos mL 3' r: IW mL 315 SM9222 (D) I 1 Colilert 18 TOTAL SUSPENDED SOLIDS (TSS) 9.44 m IL 0.14 m IL 326 SM2540 D 2.50 END OF PART A. RFPFR TO THE APPI ICATION OVFRVIFW !PAGE 11 TO nFTFRMINF WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE - - EPA Form 3516-2A (Rev. 1-99). Replaces EPA forms 75506 & 7550.22. Page 6 of 42 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RNER BASIN: City of Wilson - Hominy Creek WRF, NCO023906 Renewal Neuse BASIC APPLICATION INFORMATION PART B. ADDITIONAL APPLICATION INFORMATION FOR APPLICANTS WITH A DESIGN FLOW GREATER THAN OR EQUAL TO 0.1 MGD (100,000 gallons per day). All applicants with a design flow rate 2 0.1 mgd must answer questions B.1 through B.6. All other: go to Part C (Certification). BA. Inflow and Infiltration. Estimate the average number of gallons per day that flow into the treatment works from inflow and/or infiltration. 2,400,000 gpd Briefly explain any steps underway or planned to minimize inflow and infiltration. City-wide sewer system rehabilitation plan includes 5 yr. 10 yr, and 20 yr plan for sewer line reolacemenVreoair, and manhole reolacemenVreoair. A crew is dedicated to monitoring and inspecting system 8.2. Topographic Map. Attach to this application a topographic map of the area extending at least one mile beyond facility property boundaries. This map must show the outline of the facility and the following information. (You may submit more than one map if one map does not show the entire area.) a. The area surrounding the treatment plant, including all unit processes. See attached b. The major pipes or other structures through which wastewater enters the treatment works and the pipes or other structures through which treated wastewater is discharged from the treatment plant. Include outfalls from bypass piping, ifapplicable. See attached c. Each well where wastewater from the treatment plant is injected underground. Not Applicable d. Wells, springs, other surface water bodies, and drinking water wells that are: 1) within %mile of the property boundaries of the treatment works, and 2) listed in public record or otherwise known to the applicant Not,Applicable e. Any areas where the sewage sludge produced by the treatment works is stored, treated, or disposed. See attached f. If the treatment works receives waste that is classified as hazardous under the Resource Conservation and Recovery Act (RCRA) by truck, rail, or special pipe, show on the map where the hazardous waste enters the treatment works and where it is treated, stored, and/or disposed. NA B.3. Process Flow Diagram or Schematic. Provide a diagram showing the processes of the treatment plant, including all bypass piping and all backup power sources or redundancy in the system. Also provide a water balance showing all treatment units, including disinfection (e.g., chlorination and dechlorination). The water balance must show daily average flow rates at influent and discharge points and approximate daily flow rates between treatment units. Include a brief narrative description of the diagram. See attached B.4. OperationlMalntenance Performed by Contractor(s). Are any operational or maintenance aspects (related to wastewater treatment and effluent quality) of the treatment works the responsibility of a contractor? ® Yes ❑ No If yes, list the name, address, telephone number, and status of each contractor and describe the contractors responsibilities (attach additional pages if necessary). Name: Granville Farms Inc Mailing Address: P.O. Box 1396 Oxford NC 27565 Telephone Number. (919) 690-8000 Responsibilities of Contractor Manage land application of residuals program B.5. Scheduled improvements and Schedules of Implementation. Provide information on any uncompleted implementation schedule or uncompleted plans for improvements that will affect the wastewater treatment, effluent quality, or design capacity of the treatment works. If the treatment works has several different implementation schedules or is planning several improvements, submit separate responses to question B.5 for each. (If none, go to question B.6.) a. List the outfall number (assigned in question A.9) for each outfall that is covered by this implementation schedule. None b. Indicate whether the planned improvements or implementation schedule are required by local, State. or Federal agencies. ❑ Yes ❑ No Not Applicable EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550.22. Page 7 of 42 3100 Old Stantonsburg Road, Wilson, NC - Google Maps Page 1 of 25 Gougl@ A} t https://maps.google.com/maps?hl=en&tab=wl 11/27/2012 Page 1 of 1 Print - Maps bfr)g Maps Old Stantonsburg Rd, Wilson, NC 27893 My Notes �] On the go? Use m.".com to rma maps. s direcwns. businesses, and more http://www.bing.comlmapslprint.aspx?mkt--en-us&z15&s=h&cp=35.687537, 77.8954O... 11/27/2012 Page 1 of 1 PnrT 43- Tre+� �.z a+d Print - Maps biftg Maps Old Stantonsburg Rd, Wilson, NC 27893 My Notes [a _ m.bing.com http://www.bing.com/mapslp int.aspx?mkt—en-us&z=16&s=h&cp=35.687537,-77.89540... 11/27/2012 Sr'-Q4A z. d a- SsL Jl �'' _ . • CAutRry Club `� •"III = O`p .F,' est Hmm %: g l .•PS \ U U r G E LO ul u d • �� 1 J-.� ' � .l i - c �+ p70 `o (SR c u •aoU SR n180I' k e 0 In �. n 23 g i ; — — 3o m ' 3 3 0, SR 1692 love _ - _v -, j I Club I f c it, 0 ,m ww O J ` GREEN ENGANEERINQ _o A,ER WASTEWATER SLRVEyM "ar'aH"`'T HOMINY CREEK '•r 3W !1 OOLDeMnO Br. Pa BON SW w&BM NG 27M O � 78 (2lQ, 897�6 PM(Pffi, 9t�7MY dAaOpMrlyaam WASTEWATER MANAGEMENT FACILITY JaWMY a, zoos 3 o r - 2OW crrY OF WLBON NORTH CAROUNA ry �'^ v t SI rf4 �6 Southside Ouffall l y Sri. F Y •� y, D F � -Aoi Export Outfail 1 i%n � t Lane.StreetOutfall Tois�n s rr 9y . Y r _ �r - ' a = T �oN Hominy Swamp.0utfa1l Toisno :JT R ✓ rn_ �_ �'� mom' Wi � e i. Toisnot Export Outfall VA ♦ i t-` k1 ' jxr i n r r tnea i -' Dischar a Point h' -f US.�x4 rGG I • 'l Part B- Item B.2.a&b&d X 9 HAzEN AND SAWYER i 8-L4;�FIC RE 1-1 CITY OF WILSON, NC HOMINY CREEK WWMF SITE LAYOUT Part B - Item B.3. Plant Description The Hominy Creek Water Reclamation Facility (WRF) is located south of the City of Wilson on SR 1602. Plant effluent from the facility is piped through approximately 7,700 feet of 48-inch outfall to Contentnea Creek. The discharge point is approximately 2.5 miles downstream of the Wiggins Mill Reservoir dam. Wastewater is conveyed to the Hominy Creek WRF by the Hominy Swamp, Contentnea and Toisnot Swamp interceptors. Flow enters the plant through the 36-inch Hominy Swamp Interceptor, the 30-inch Contentnea Interceptor and the 20-inch force main from the Toisnot Pump Station. A separate influent pump station at the treatment plant site conveys wastewater from the Hominy Swamp and Contentnea Interceptors to the preliminary treatment facilities. As shown in Figure 1-2, the Hominy Creek WRF provides tertiary treatment, including nitrogen and phosphorus removal, for a design capacity of 14 mgd. Raw wastewater from the off -site and on -site pump stations receives preliminary treatment by screening and grit removal before being conveyed to the primary clarifiers. From the primary clarifiers, flow is distributed to the biological nutrient removal (BNR) activated sludge stage. Major process units of the BNR activated sludge stage consist of a biological phosphorus removal (BPR) tank, seven (7) aeration tanks, five (5) secondary clarifiers and three (3) return activated sludge (RAS) pumping stations. Secondary clarifier effluent receives tertiary treatment in five (5) effluent filters and is then aerated and disinfected in two (2) post aeration/chlorine contact tanks to meet DO and fecal coliform effluent limits. The effluent is then dechlorinated at the end of the post aeration/chlorine contact tanks to meet a total residual chlorine effluent limit, and is discharged to Contentnea Creek through the 48-inch outfall. The two (2) preaeration basins shown on the schematic (Figure 1-2) are no longer in service. Part B - Item B.3. The solids handling facilities for the primary and waste activated sludge consist of two (2) gravity belt thickeners for waste activated sludge thickening, four (4) anaerobic digesters for solids stabilization, two (2) belt filter presses for dewatering, three (3) liquid sludge holding tanks, an alkaline sludge stabilization facility capable of producing a Class A stabilized sludge product and a covered sludge storage pad. The Class A dewatered sludge is disposed of by land application on privately -owned farm land. The anaerobically digested Class B sludge is land applied on privately -owned farm land or taken to a privately -owned composting facility. Existing sand drying beds are available for standby dewatering or for use when draining a digester for cleaning. FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: City of Wilson - Hominy Creek WRF, NCO023906 Renewal Neuse C. If the answer to 0.5.b is'1'es,' briefly describe, including new maximum daily inflow rate (H applicable). NA d. Provide dates imposed by any compliance schedule or any actual dates of completion for the implementation steps listed below, as applicable. For improvements planned independently of local, State, or Federal agencies, indicate planned or actual completion dates, as applicable. Indicate dates as accurately as possible. Schedule Actual Completion Implementation Stage MM/DD/YYYY MM/DD/YYYY - Begin Construction NA / NA / NA NA / NA / NA - End Construction NA / NA / NA NA / NA / NA - Begin Discharge NA / NA / NA NA / NA / NA - Attain Operational Level NA / NA / NA NA / NA / NA e. Haw appropriate permits/clearanms concerning other Federal/State requirements been obtained? NA ❑ Yes ❑ No Describe briefly: NA NA B.6. EFFLUENT TESTING DATA (GREATER THAN 0.1 MGD ONLY). Applicants that discharge to waters of the US must provide effluent testing data for the following parameters. Provide the indicated effluent testing required by the permitting authority for each outfall through which effluent is discharged. Do not include information On combine sewer overflows in this section. All information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. At a minimum effluent testing data must be based on at least three pollutant scans and must be no more than four and one-half years old. Outfall Number. 001 (3-Year Data Set Used: October 2015 - September 2018) MAXIMUM DAILY AVERAGE DAILY DISCHARGE DISCHARGE ANALYTICAL POLLUTANT METHOD MLIMDL Conc. Units Conc. Units Number of Samples CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS AMMONIA (as N) 1.53 mg/L 0.06 mg/L 324 SM4500-NH3 (E) 0.200 CHLORINE (TOTAL 14 pg/L 0 pg/L 749 SM4500-CI (G) 10.0 RESIDUAL, TRC) DISSOLVED OXYGEN 11.37 mg/L 9.17 mg/L 749 HACH 10360 0.01 TOTAL KJELDAHL 3.07 mg/L 0.723 mg/L 189 SM4500-NH3 (E) 0.200 NITROGEN (TKN) NITRATE PLUS NITRITE 4.03 mg/L 1.48 mg/L 189 SM4500-NO3 (E) 0.050 NITROGEN OIL and GREASE 30.5 mg/L 2.5 mg/L 12 EPA-1664A 5.0 PHOSPHORUS (Total) 1.36 mg/L 0.250 mg/L 158 SM4500-P (E) 0.050 TOTAL DISSOLVED SOLIDS 356 mg/L 305 mg/L 4 SM2540 (C) 10.0 (TDS) OTHER: Conductivity "15 pmhoslcm 502 pmhos/Crn 748 SM2510 (8) 10.0 END OF PART B. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE EPA Form 3510.2A (Rev. 1-99). Replaces EPA forms 7650-e & 7550-22, P,,ve a of 42 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: City of Wilson - Hominy Creek WRF, NCO023906 Renewal Neuse BASIC APPLICATION INFORMATION PART C. CERTIFICATION lit All applicants must complete the Certification Section. Refer to instructions to determine who is an officer for the purposes of this certification. All applicants must complete all applicable sections of Form 2P., as explained in the Application Overview. Indicate below which parts of Form 2A you have completed and are submitting. By signing this certification statement, applicants confirm that they have reviewed Form 2A and have completed all sections that apply to the facility for which this application is submitted. Indicate which parts of Form 2A you have completed and are submitting: ® Basic Application Information packet Supplemental Application Information packet: ® Part D (Expanded Effluent Testing Data) ® Part E (Toxicity Testing: Biomonitorirg Data) ® Part F (industrial User Discharges and RCRAIGERCLA Wastes) ❑ Part G (Combined Sewer Systems) ALL APPLICANTS MUST COMPLETE THE FOLLOWING CERTIFICATION. I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the intonmation submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief, true. accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Name and official We Harry Tvson Debut yvC\City Manager Signature . lam^ Telephone number (252) 399-2461 Date signed November 26, 2018 Upon request of the permitting authority, you must submit any other information necessary to assure wastewater treatment practices at the treatment works or identify appropriate permitting requirements. SEND COMPLETED FORMS TO: NCDENR/ DWQ Attn: NPDES Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 EPA Forth 3510-2A (Rev, 1-99), Replaces EPA fors 755M & 7550-22. Page 9 of.. _ FACILITY NAME AND PERMIT NUMBER: City of Wilson -Hominy Creek WRF, NC0023906 [PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Neuse SUPPLEMENTAL APPLICATION INFORMATION "Refer to attached Effluent Priority Pollutant Analyses' PART D. EXPANDED EFFLUENT TESTING DATA 'Refer to attached Effluent Priority Pollutant Analyses* Refer to the directions on the cover page to determine whether this section applies to the treatment works. Effluent Testing: 1.0 mgd and Pretreatment Works. If the treatment works has a design flow greater than or equal to 1.0 mgd or it has (or is required to have) a pretreatment program, or is otherwise required by the pemnitfing authority to provide the data, then provide effluent testing data for the following pollutants. Provide the indicated effluent testing information and any other information required by the permitting authority for each outfall through which effluent is discharged. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analyses conducted using 40 CFR Part 136 methods. In addition, these data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. Indicate in the blank rows provided below any data you may have on pollutants not specifically listed in this form. At a minimum, effluent testing data must be based on at least three pollutant scans and must be no more than four and one-half years old. Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.) POLLUTANT MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE ANALYTICAL METHOD MLIMDL Cone. Units Mass Units Conc. Units Mass Units Number of Samples METALS (TOTAL RECOVERABLE), CYANIDE, PHENOLS, AND HARDNESS. ANTIMONY <1.0 pg/L NA NA 0 pg/L NA NA 4 EPA 200.8 1.0 ARSENIC <10 pglL NA NA 0 pg/L NA NA 12 SM 3113 (B) 10 BERYLLIUM <0.10 pg/L NA NA 0 pg/L NA NA 4 EPA 200.8 0.10 CADMIUM <0,2 pg/L NA NA 0 Pg/L NA NA 12 SM 3113 (B) 0.2 CHROMIUM <5 pg/L NA NA 0 pg/L NA NA 12 SM 3113 (8) 5 COPPER 50.0 pg/L NA NA 5.00 pg/L NA NA 12 SM 3113 (B) 2 LEAD <10 pg/L NA NA 0 pg/L NA NA 12 SM 3113 (B) 10 MERCURY 0.52 ng/L NA NA 0.04 ng/L NA NA 12 EPA 1631 (E) 0.5 NICKEL <10 pg/L NA NA 0 pg/L NA NA 12 SM 3113 (B) 10 SELENIUM <5 pg/L NA NA 0 pg/L NA NA 12 SM 3113 (B) 5 SILVER <10 pg/L NA NA 0 pg/L NA NA 12 SM 3113 (B) 5 THALLIUM 0.0 pg/L NA NA 0 P91L NA NA 4 EPA 200.8 1.0 ZINC 25.2 pg/L NA NA 15.6 pg/L NA NA 12 SM 3113 (B) 10 CYANIDE <10 Pg/L NA NA 0 pg/L NA NA 12 EPA 335.4 10 TOTAL PHENOLIC COMPOUNDS 0.028 mg/L NA NA 0.013 mg/L NA NA 4 EPA 420.4 0.010 HARDNESS (as CaCO3) 56 mg/L NA NA 42.9 mg/L NA NA 12 SM 2340 (C) 0.662 Use this space (or a separate sheet) to provide information on other metals requested by the permit writer MOLYBDENUM 6 pg/L NA NA 2 pg/L NA NA 12 SM 3113 (B) 1 EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 10 of 42 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: City of Wilson - Hominy Creek WRF, NCO02390 Renewal Neuse Ouffall number: 001 (Complete once for each oulfall discharging effluent to waters of the United Stales.) MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE POLLUTANT ANALYTICAL METHOD MLIMDL Number Conc. Units Mass Units Cone. Units Mass Units of Samples VOLATILE ORGANIC COMPOUNDS ACROLEIN <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 624 5.0 ACRYLONITRILE <50.0 pg/L NA NA 0 pg/L NA NA 4 EPA 624 60.0 BENZENE <2.0 pg/L NA NA 0 pg/L NA NA 4 EPA 624 2.0 BROMOFORM <2.0 pg/L NA NA 0 pg/L NA NA 4 EPA 624 2.0 CARBON <2.0 pg/L NA NA 0 pg/L NA NA 4 EPA 624 2.0 TETRACHLORIDE CHLOROBENZENE <2.0 pg/L NA NA 0 pg/L NA NA 4 EPA 624 2.0 CHLORODIBROMO- <2.0 pg/L NA NA 0 pg/L NA NA 4 EPA 624 2.0 METHANE CHLOROETHANE <2.0 pg/L NA NA 0 pg/L NA NA 4 EPA 624 2.0 2-CHLOROETHYLVINYL <2.0 pg/L NA NA 0 pg/L NA NA 4 EPA 624 2.0 ETHER CHLOROFORM 8.3 pg/L NA NA 5.3 pg/L NA NA 4 EPA 624 2.0 DICHLOROBROMO- 3 7 pgA. NA NA 1.7 pg/L NA NA 12 EPA 624 2.0 METHANE 1,1-DICHLOROETHANE <2.0 pg/L NA NA 0 pg/L NA NA 4 EPA 624 2.0 1,2-DICHLOROETHANE <2.0 pg/L NA NA 0 pg/L NA NA 4 EPA 624 2.0 TRANS-I,2-DICHLORO- <20 pg/L NA NA 0 pg/L NA NA 4 EPA624 2.0 ETHYLENE 1,1-DICHLORO- <2.0 pg/L NA NA 0 pg/L NA NA 4 EPA 624 2.0 ETHYLENE 1,2-DICHLOROPROPANE <2.0 pg/L NA NA 0 pg/L NA NA 4 EPA 624 2.0 1,3-DICHLORO- <2.0 pg/L NA NA 0 pg/L NA NA 4 EPA 624 2.0 PROPYLENE ETHYLBENZENE <2.0 pg/L NA NA 0 pg/L NA NA 4 EPA 624 2.0 METHYL BROMIDE <2.0 pg/L NA NA 0 pg/L NA NA 4 EPA 624 2.0 METHYL CHLORIDE <2.0 pg/L NA NA 0 pg/L NA NA 4 EPA 624 2.0 METHYLENE CHLORIDE <2.0 pg/L NA NA 0 pg/L NA NA 4 EPA 624 2.0 1,1,2,2-TETRA- <2.0 pg/L NA NA 0 pg/L NA NA 4 EPA 624 2.0 CHLOROETHANE TETRACHLORO- <2.0 pg/L NA NA 0 pg/L NA NA 4 EPA 624 2.0 ETHYLENE TOLUENE <2.0 pg/L NA NA 0 pg/L NA NA 4 EPA 624 2.0 EPA Form 3510-2A (Rev. 1-99). Replaces EPA fortes 7550-6 & 755022. Page 11 of 42 FACILITY NAME AND PERMIT NUMBER: City of Wilson - Hominy Creek WRF, NCO023906 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Neuse Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.) POLLUTANT MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE ANALYTICAL METHOD ML/MDL Conc. Units Mass Units Conc. Units Mass Units Number of Samples TRICHLOROETHANE <2.0 pg/L NA NA 0 pg/L NA NA 4 EPA 624 2.0 1,1,2- TRICHLOROETHANE <2.0 pg/L NA NA 0 pg/L NA NA 4 EPA 624 2.0 TRICHLOROETHYLENE <2.0 pg/L NA NA 0 pg/L NA NA 4 EPA 624 2.0 VINYLCHLORIDE <2.0 pg/L NA NA 0 pg/L NA NA 4 EPA 624 2.0 Use this space (or a separate sheet) to provide information on other volatile organic compounds requested by the permit writer ACID -EXTRACTABLE COMPOUNDS P-CHLORO-M-CRESOL <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 2-CHLOROPHENOL <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 2,4-DICHLOROPHENOL <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 2,4-DIMETHYLPHENOL <10.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 10.0 4,6-DINITRO-0-CRESOL <20.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 20.0 2,4-DINITROPHENOL <50.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 50.0 2-1,1ITROPHENOL <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 4-1,1ITROPHENOL <50.0 pg/L NA NA 0 pg/L NA NA 4 EPA625 50.0 PENTACHLOROPHENOL <10.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 10.0 PHENOL <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 TRIOHLOROPHENOL RIC <10.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 10.0 Use this space (or a separate sheet) to provide information on other acid -extractable compounds requested by the permit writer BASE -NEUTRAL COMPOUNDS ACENAPHTHENE <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 ACENAPHTHYLENE <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 ANTHRACENE <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 BENZIDINE <50.0 pg/L NA NA 0 pg1L NA NA 4 EPA 625 50.0 BENZO(A)ANTHRACENE <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 BENZO(A)PYRENE <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 12 of 42 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: City of Wilson - Hominy Creek WRF, NCO023906 Renewal Neuse Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE POLLUTANT ANALYTICAL MLIMDL Number Conc. Units Mass Units Conc. Units Mass Units of METHOD Samples 3,4 BENZO- <5.0 pg/L NA NA 0 Pg/L NA NA 4 EPA 625 5.0 FLUORANTHENE BENZO(GHI)PERYLENE <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 BENZO(K) <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 FLUORANTHENE BIS OROETHO%Y) <10.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 10.0 METHANE HAKE BIS (2-CHLOROETHYL)- <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 ETHER BIS (2-CHL <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 THER PROPVL)EETHER BIS (2-ETHYLHEXYL) <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 PHTHALATE 4-BROMOPHENYL <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 PHENYLETHER BUTYL BENZYL <5.0 pg/L NA NA 0 Pg/L NA NA 4 EPA 625 5.0 PHTHALATE 2-CHLORO- <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 NAPHTHALENE 4-CHLORPHENYL <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 PHENYLETHER CHRYSENE <5.0 Pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 DI-N-BUTYL PHTHALATE <5.0 pg/L NA NA 0 Pg/L NA NA 4 EPA 625 5.0 DI-N-OCTYL PHTHALATE <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 DIBENZO(A,H) <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 ANTHRACENE 1,2-DICHLOROSENZENE <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 1,3-DICHLOROSENZENE <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 1,4-DICHLOROBENZENE <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 3,3.DICHLORO- <25.0 Pg/L NA NA 0 pg/L NA NA 4 EPA 625 25.0 BENZIDINE DIETHYL PHTHALATEF<5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 DIMETHYL PHTHALATEpg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 2,4-DINITROTOLUENEpg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 2,6.DINITROTOLUENEpg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 1,2-DIPHENYL- pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 HYDRAZINE EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550.6E 7550-22. Page 13 of 42 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: City of Wilson - Hominy Creek WRF, NCO023906 Renewal Neuse Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE POLLUTANT ANALYTICAL MLIMDL Number Cone. Units Mass Units Cone. Units Mass Units of METHOD Samples FLUORANTHENE <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 FLUORENE <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 HEXACHLOROBENZENE <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 HEXA- <5.0 pg1L NA NA 0 pg/L NA NA 4 EPA 625 5.0 SUTADIENE DIENE HEXACHLOROCYCLO- <10.0 pg/L NA NA 0 pglL NA NA 4 EPA 625 10.0 PENTADIENE HEXACHLOROETHANE <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 INDENO(1,2,3-CD) <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 PYRENE ISOPHORONE <10.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 10.0 NAPHTHALENE <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 NITROBENZENE <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 6.0 N-NITROSODI-N- <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 PROPYLAMINE OSODI- <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 METHYLAMINE METH N-NITROSODI- <10.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 10.0 PHENYLAMINE PHENANTHRENE <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 PYRENE <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 1. TRIOHLOROBENZENE RIC <5.0 pg/L NA NA 0 pg/L NA NA 4 EPA 625 5.0 Use this space (or a separate sheet) to provide information on other basaneutral compounds requested by the permit writer Use this space (or a separate sheet) to provide infomlation on other pollutants (e.g., pesticides) requested by the permit writer END OF PART D. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE - EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550.6 & 7550-22, Pagr; 14 or cz kR ) .I Annual Monitoring and Pollutant Scan Permit No.: NC 0023906 Month: November Outfall: 001 Year: 2015 Facility Name: Wilson - Hominy Creek WWMF ORC: James W. Pridgen Date of Sampling 11/1712015 Phone (252)399-2491 Par. Cnalvtical Services and Citv Of Wilson WWTP Lab Parameter Sample T Analytical Method Quandtation Level Sample Result Units of Measurement Numberaf Sam les Ammonia (as N) Composite SM 4500 NH3 C 0.200 NO mg/L 1 Dissolved oxygen Grab SM 4500 O-G 0.05 9.52 mg/L 1 Nitrate/Nitrite Composite SM 4500 NO3 E 0.050 0.84 mg/L t Total Kjeldahl nitrogen Composite SM 4500 N org C 0.200 0.476 mgA 1 Total Phosphorus Composite SM 4500 O-G 0.050 0.103 mg/L 1 Total Dissolved solids Composite SM 2540 C 40.0 283 rng/L 1 Hardness Composite SM 2340 C 0.20 38 mg CaCO3/L 1 Chlonne (total residual, TRC) Grab SM 4500 CI G 10 NO ug/L 1 Oil and grease Grab EPA 1664E 5.0 NO mg/L 1 Metals (total recoverable), cyanide and total phenols Antimony Arsenic Campo Compo Compo Compo Beryllium Cadmium Chromium Compo Copper Comp Comp Lead Mercury Gra Nickel Comp Selenium Comp Silver Comp Thallium Zinc Comp Comp Cyanide Gr site EPA 200.8 1 site EPA 200.8 10 site EPA 200.8 0.10 site EPA 200.8 0.2 site EPA 200.8 5 NO ND NO NO NO 6 NO NO NO NO NO NO NO NO ug/L ug/L ug/L ug/L ug/L ug/L ug/L ng/L ug/L ug/L ug/L ug/L ug/L ug/L 1 1 1 1 1 1 1 1 1 1 1 1 N7/'4 t '. Total phenolic compounds Grab EPA 420.4 10 28 ug/L 1 Volatile organic compounds Acrolein Grab EPA 624 5.0 NO ug/L t Acxylonitrile Grab EPA624 50 NO ug/L t ,Benzene Grab EPA624 2.0 NO ug/L 1 !Bromofonn Grab EPA624 2.0 NO ug/L 1 Carbon tetrachloride Grab EPA 624 2.0 NO ug/L 1 Chlorobenzene Grab EPA 624 2.0 NO ug/L 1 Chlorodibromomethane Grab EPA 624 2.0 NO ug/L 1 Chloroethane Grab EPA624 2.0 NO ug/L 1 2-chloroethylvinyl ether Grab EPA 624 5.0 NO ug/L 1 Chloroform Grab EPA 624 2.0 5.1 ug/L 1 Dichlorobromomethane Grab EPA 624 2.0 2.1 ug/L 1 1,1-dichloroethane Grab EPA624 2.0 NO ug/L 1 1,2-dichloroethane Grab EPA624 2.0 NO ug/L 1 Trans-1,2-dichloroethylene Grab EPA624 2.0 NO ug/L 1 Parameter Sample Type Analytical Method Iluantitation Level Sample Result Units of Measurement Number of I Samples Volatile organic compounds (Cont) 1,1-dichloroethylene Grab EPA624 2.0 NO ug/L 1 1,2-dichloropropane Grab EPA624 2.0 NO ug/L 1 1,3-dichloropropylene Grab EPA624 4.0 NO ug/L 1 'Ethylbenzene Grab EPA624 2.0 NO ug/L 1 Methyl bromide Grab EPA624 2.0 NO ug/L 1 Methyl chloride Grab EPA 624 2.0 NO ug/L 1 Methylene chloride Grab EPA624 2.0 NO ug/L 1 1,1,2,2-telrachloroethane Grab EPA624 2.0 NO ug/L 1 Tetrachloroethylene Grab EPA 624 2.0 NO ug/L 1 Toluene Grab EPA624 2.0 NO ug/L 1 1.1.1-trichloroethane Grab EPA624 2.0 NO ug/L 1 1, 1,2-trichloroethane Grab EPA 524 2.0 ND ug/L t Trichloroethylene Grab EPA 624 2.0 ND ug/L 1 Vinyl chloride Grab EPA, 61-4 2.0 NG ug/L I Acid -extractable compounds P-chlcro-m-creso Grab EPA 625 5.0 ND ug/L 2-chlorophenol Grab EPA625 5.0 ND ug/L 1 2,4-dichlorophenol Grab EPA625 5.0 ND ug/L 1 2,4-dimethylphenol Grab EPA 625 10.0 ND ug/L 1 4,5-dinitro-o-cresol Grab EPA 625 20.0 ND ug/L 1 112,4-dinitrophenol Grab EPA625 50.0 ND ug/L 1 2-nitrophenol Grab EPA625 5.0 ND ug/L 1 4-nitrophenol Grab EPA 625 50.0 ND ug/L 1 Pentachlorophenol Grab EPA 625 10.0 ND ug/L 1 Phenol Grab EPA 625 5.0 ND ug/L 1 2,4,64richlorophenol Grab EPA 625 10.0 ND ug/L 1 Base -neutral compounds Acenaphthene Grab EPA 625 5.0 ND ug/L 1 Acenaphthylene Grab EPA625 5.0 ND ug/L 1 Anthracene Grab EPA625 5.0 ND ug/L 1 Benzidine Grab EPA 625 50-0 ND ug/L 1 anthracene Grab EPA 625 5.0 ND ug/L 1 pyrene Grab EPA625 5.0 ND uglL 1 oFluoranthene Grab EPA625 5.0 NDEE ug1L 1 hi)perylene Grab EPA 625 5.0 ND ug/L 1 )Fluoranthene loroethoxy) methane F(2-chloroethoxy) Grab Grab EPA625 EPA 625 5.0 10.0 ND ND uglL ug/Lloroethyl) 1 ether Grab EPA 625 5.0 ND uglLloroisopropyl) ether Grab EPA625 5.0 ND ug/L 1 Bis (2-ethylhexyl) phthalate Grab EPA625 5.0 ND ug/L 1 4-bromophenyl phenyl ether Grab EPA 625 5.0 ND uglL 1 Butyl benzyl phthalate Grab EPA 625 5 0 ND ug/L 1 2-chlcronaphthalene Grab EPA 625 5.0 ND 4-chlcrophenyl phenyl ether Grab EPA 625 5.0 ND sample Analyticat tluantitation Sample Parameter Type Method Level Result Base -neutral compounds (cont) Chrysene Grab Di-n-butyl phthalate Grab Di-n-octyl phthalate Grab Dibenzo(a,h)anthracene Grab 1,2-dichlorobenzene Grab 1,3-dichlorobenzene Grab I1,4-dichlorobenzene Grab 3,3-dichlorobenzidine Grab Diethyl phthalate Grab Dimethyl phthalate Grab 2,4-dinitrotoluene Grab 2,6-dinitrotoluene Grab 1,2-diphenylhydrazine Grab Fluoranthene Grab Fluorene Grab Hexachlorobenzene Grab Hexachlorobutadiene Grab Hexachlorocyclo-pentadiene Grab Hexachloroethane Grab Indeno(1,2,3-cd)pyrene Grab Isophorone Grab Naphthalene Grab ------ Grab Grab uglL I 1 ug/L I EPA 625 5.0 ND ug/L EPA 625 5.0 ND ug/L EPA 625 5.0 ND ug/L EPA 625 5.0 ND ug/L EPA 624 5.0 ND uglL EPA 624 5.0 ND uglL EPA 624 5.0 ND ug/L EPA 625 25.0 ND ug/L EPA 625 5.0 ND uglL EPA 625 5.0 ND ug/L EPA 625 5.0 ND ug/L EPA 625 5.0 ND uglL EPA 625 50 ND ug/L EPA 625 5.0 ND ug/L EPA 625 5.0 ND ug/L EPA 625 5.0 ND ug/L EPA 625 5.0 ND ug/L EPA 625 100 ND ug/L EPA 625 5.0 ND ug/L EPA 625 5.0 ND ug/L EPA 625 10.0 ND ug/L EPA 625 5.0 ND ug/L EPA 625 5.0 ND uglL 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 N-nitrosodi-n-prcpylamine Grab EPA 625 5.0 NO ug/L 1 N-nitroscdimethyfamine Grab EPA 625 5.0 ND ug/L iV-nitrosodiphemhamine Grab EPA 625 1D.0 ND ug/L 1 Phenanthrene Grab EPA 625 5.0 ND ug/L 1 Pyrene Grab EPA 625 5.0 ND ug/L 1,2,4,-trichlorobenzene Grab EPA 625 5.0 ND ug/L I certify under penalty of law that this document and all attachments were prepared under my direction and supervision in accordance with a system to design to assure that qualified perdonnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons that manage the system, or those persons directly responsible for gathering the information, the aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing viol Analysis for the following parameters were collected on the dates as noted: TDS Collected and Analyzed on 0612012013 and Chloride Collected and Analyzed on 0511512013. Permit Nc. Outfall Facility Name Date of Sampling Anaytical Laboratoni: Annual Mlon toriny and Pollutant Scan NC0023906 Month: August 001 Year: 2016 City of Wilson ORC James VV. Pridgen 8/9/2016 Phone 252-399-2491 City of Wilson NC 130 Pace Analytic I NC 12,40 and 667 ber of Sample Parameter Type Ammonia (as N) Composite S Dissolved oxygen Composite Composite S Nitrate/Nitrite Total Kjeldahl nitrogen Composite S Total Phosphorus Composite Composite Composite Total dissolved solids Hardness Chlorine (total residual, TRC) Grab Oil and grease Grab Metals (total recoverable), cyanide and total Antimony Composite Arsenic Composite Beryllium Composite Composite Cadmium Chromium Composite Composite Copper Lead Composite Mercury Composite Composite Nickel Selenium Composite Silver Composite Thallium Composite Zinc Composite Cyanide Grab Total phenolic compounds Grab Volatile organic compounds Acrolein Grab Acrylonitrile Grab Benzene Grab Bromoform Grab Carbon tetrachloride Grab Chlorobenzene Grab Chlorodibromomethane Grab Chloroethane Grab 2-chloroethylvinyl ether Grab Grab Grab Grab Grab Grab Chloroform Dichlorobromomethane 1,1-dichloroethane 1,2-dichloroethane Trans-1,2-dichloroethylene Analytical SM45000 SM4500CIG-2000 Quantitation Sample Units of Num Samples Method Level Result Measurement M4500NH3C-1997 0.2 0.28 mglL 1 G 2001 0.05 8.39 mg/L 1 1 M4500NO3-E2000 0.05 1.51 mg/L M400NorgC-1997 0.2 0.448 mg/L 1 SM4500PE1999 0.05 1.04 mg/L 1 SM254OC-1997 40 328 mg/L 1 SM2340C-1997 0.2 44 mg/L CaCo3 1 10 NO ug/L 1 EPA 1664B 5 ND mg/L 1 phenols 1 ND ug/L 10 ND ug/L 10.1 ND ug/L 14 WEPA200.811 0.2 ND ug/L 14 5 ND uglL 14 2 ND ug/L 1 SM3113B-2004 10 NO uglL 1 EPA 1631 E 0.5 ND ng/L 1 SM3113B-2004 10 ND ug/L 1 SM31138-2004 5 ND ug/L 1 SM3113B-2004 5 ND ugll 1 EPA 200.8 1 ND ug/L 1 SM3111B-1999 10 23 ug/L 1 EPA 335 4 0.01 ND mg/L 1 EPA 420.4 0.01 0.013 m9/L 1 EPA 624 5 NO ug/L 1 EPA 624 50 NO ug/L 1 EPA 624 2 NO ug/L 1 EPA 624 2 NO ug/L 1 EPA624 2 NO ug/L 1 EPA 624 2 NO uglL 1 EPA 624 2 ND ug/L 1 EPA 624 2 ND uglL 1 EPA 624 5 NO uglL 1 EPA 624 2 8.3 uglL 1 EPA 624 2 2 7 uglL 1 EPA 624 2 ND uglL 1 EPA 624 2 ND ug/L 1 EPA 624 2 NO ug/L 1 Parameter Sample Type Analytical Method Volatile organic compounds (Cont) 1,1-dichloroethylene Grab EPA624 1,2-dichloropropane 1,3-dichloropropylene Ethylbenzene Methyl bromide Grab Grab Grab Grab Grab Grab Grab Grab EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 Methyl chloride Methylene chloride 1,1,2,2-tetrachloroethane Tetrachloroethylene Toluene Grab EPA 624 1,1,1-tdchloroethane Grab EPA624 11,2-tdchloroethane Grab EPA 624 Trichloroethylene Grab EPA 624 Vinyl chloride Grab EPA 624 Acid -extractable compounds P-chioro-m-creso Grab EPA 625 2-chlorophenol Grab EPA 625 2,4-dichlorophenol Grab EPA 625 2,4-dimethylphenol Grab EPA 625 4,6-dinitro-o-cresol Grab EPA 625 2,4-dinitrophenol Grab EPA 625 2-nitrophenol Grab EPA 625 4-nitrophenol Grab EPA 625 Pentachlorophenol Grab EPA 625 Phenol Grab EPA 625 2,4,6-trichlorophenol Grab EPA625 Base -neutral compounds Acenaphthene Grab EPA 625 Acenaphthylene Grab EPA 625 Anthracene Grab EPA 625 Benzidine Grab EPA 625 Benzo(a)anthracene Grab EPA 625 Benzo(a)pyrene Grab EPA625 3,4 benzoFluoranthene Grab EPA 625 Benzo(ghi)perylene Grab EPA 625 Benzo(k)Fluoranthene Grab EPA 625 Bis (2-chloroethoxy) methane Grab EPA 625 Bis (2-chioroethyi) ether Grab EP Bis (2chloroisopropyl) ether Grab EP Bis (2-ethylhexyl) phthalate 4-bromophenyl phenyl ether Butyl benzyl phthalate Grab Grab Grab E E E 2-chloronaphthalene Grab E 4chlorophenyl phenyl ether Grab E A 625 A 625 PA 625 PA 625 PA 625 PA 625 PA 625 Quantitation Sample Units of Measurement Number of Samples Level Result 9 NO uglL 1 2 ND uglL 1 1 2 NO ug/L 1 2 NO ug/L 1 2 ND ug/L 1 2 NO ug/L 1 2 ND uglL 22222 NOug/L1 5 NO ug/L 1 5 Np ug/L 1 5 NO ug/L 1 10 NO ug/L 1 20 NO ug/L 1 50 NO ug/L 1 5 NO ug/L 1 50 NO ug/L 1 10 NO uglL 1 5 NO ug/L 1 10 NO ug/L 1 5 NO ug/L 1 5 NO ug/L 1 5 NO ug/L 1 50 NO ug/L 1 5 NO ug/L 1 5 NO ug/L 1 5 ND u91L 1 5 NO ug/L 5 NO ug/L 1 5 NO ug/L 1 5 NO ug/L 1 5 NO ug/L 1 5 NO uglL 1 5 NO ug/L 1 5 NO uglL 1 5 NO ug/L 1 5 NO ug/L 1 Parameter Sample Anaiy#icad Quantitation Sampis Units of Number of Samples Type Method Levei Result Measurement Sass neutral compounds (cost) Ghrysene Grab EPA 625 5 ND ug/L 1 Di-n-butyl phthalate Grab EPA 625 5 ND ug/L 1 Di-n-octyl phthalate Grab EPA 625 5 ND uglL 1 Dibenzo(a,h)anthracene Grab EPA625 5 ND ug/L 1 1,2-dichlorobenzene Grab EPA 624 5 ND ug/L 1 1,3-dichlcrobenzene Grab EPA 624 5 ND ug/L 1 1,4-dichlorobenzene Grab EPA 624 5 ND ug/L 1 3,3-dichlorobenzidine Grab EPA625 25 ND ug/L 1 Diethyl phthalate Grab EPA 625 5 ND ug/L 1 Dimethyl phthalate Grab EPA 625 5 ND ug/L 1 2,4-dinitrotoluene Grab EPA 625 5 NO ug/L 1 2,6-dinitrotoluene Grab EPA 625 5 ND uglL 1 1,2-diphenylhydrazine Grab EPA625 5 ND ug/L 1 Fluoranthene Grab EPA 625 5 ND ug/L 1 Fluorene Grab EPA625 5 ND ug/L 1 Hexachlorobenzene Grab EPA 625 5 ND ug/L 1 Hexachlorobutadiene Grab EPA 625 5 ND ug/L 1 Hexachlorocyclo-pentadiene Grab EPA625 10 ND ug/L 1 Hexachloroethane Grab EPA 625 5 ND uglL 1 indeno(1,2,3cd)pyrene Grab EPA625 5 ND ug/L 1 isophorone Grab EPA625 10 ND ug/L 1 Naphthalene Grab EPA 625 5 ND ug/L 1 Nitrobenzene Grab EPA 625 5 ND uglL 1 N-nitrosodi-n-propylamine Grab EPA 625 5 ND ug& 1 N-nitrosodimethylamine Grab EPA 625 5 NO ug/L 1 N-nitrosodiphenylamine Grab EPA625 5 ND ug/L 1 Phenanthrene Grab EPA625 5 ND ug/L 1 Pyrene Grab EPA 625 5 ND uglL 1 1,2,4,-trichlorobenzene Grab EPA625 5 ND ug/L 1 I certify under penalty of law that this document and all attachments were prepared under my direction and supervision in accordance with a system to design to assure that qualified perdonnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons that manage the system, or those persons directly responsible for gathering the information, the aware that there are significant penalties for su rmati n, cluding the possibility of fines and imprisonment for knowing violations. !: e i e . i L Name Signature fU 3�1� Date Permit No. Annuall Monitoring and Podutant Scan NIC0023906 Nlonth May ay Outfall Facility Name Date of Sampling A l t' 1 L b t' EFF A-106 HOMINY CREEKvvWMF ORC 05/16/2017 (*05116/2017) Phone PACE Anal tical and City of Wilson James W. Pridgen 252-399-2491 na y ica a ora ori. Parameter Y Parameter Code Sampie Type Analytical Method Quantitation Level Sample Result Units of Measurement Ammonia (as N) * C0610 Composite SM4500 C-1997 0.2 NO mg/L Chlorine (total residual, TRC) 50060 Grab SM2540 B-1997 10 NO ug/L Dissolved oxygen 00300 Grab SM4500 G-2001 0.01 8.9 mg/L Nitrite+Nitrate Total (as N)* 00630 Composite SM4500 E-2001 0.05 1.64 mg/L Total Kjeldahl Nitrogen* 00625 1 Composite SM4500C 1997 0.2 1.2 mglL Oil and Grease 00556 Grab EPA 1664B 5.0 NO mg/L Total Phosphorus C0665 Composite SM4500 P-1999 0.5 1.01 mg/L Total Dissolved Solids 70295 Composite SM2540 C-1997 40 356 mg/L mg/L CaCO3 Hardness 00900 Composite SM 2340B 0.662 41.4 Metals (total recoverable), cyanide and total phenols Antimony 01097 Composite EPA 200.8 1 NO ug/L ug/L Arsenic 01002 Composite EPA 200.8 10 NO Beryllium 01012 Composite EPA 200.8 0.10 NO ug/L Cadmium 01027 Composite EPA 200.8 0.20 NO ug/L Chromium 01034 Composite EPA 200.8 5 NO ug/L ug/L Copper 01042 Composite EPA 200.8 2 2 ug/L Lead 01051 Composite EPA 200.8 10 NO Mercury (Method 1631E) COMER Composite EPA 1631 0.5 NO ug/L ug/L Nickel 01067 Composite EPA 200.8 10 NO Selenium 01147 Composite EPA 200.8 5 NO ug/L Silver 01077 Composite EPA 200.8 5 NO uglL Thallium 01059 Composite EPA 200.8 1.0 ND uglL Zinc 01092 Composite EPA 200.8 10 16 ug/L Cyanide 00720 1 Grab EPA 335.4 0.010 ND mg/L Total phenolic compounds 32730 Grab EPA 420.4 0.010 ND mg/L Volatile organic compounds 5.0 NO Acrolein 34210 Grab EPA 624 NO ug/L Acrylonitrile 34215 Grab EPA 624 50.0 NO ug/L Benzene 34030 Grab EPA 624 2.0 NO ug/L Bromoform 32104 Grab EPA 624 2.0 2.0 NO ug/L Carbon tetrachloride 32102 Grab EPA 624 NO ug/L Chlorobenzene 34301 Grab EPA 624 2.0 NO ug/L Chlorodibromomethane 34306 Grab EPA 624 2.0 NO ug/L Chloroethane 85811 Grab EPA 624 2.0 5.0 NO ug/L 2-chioroethyl vinyl ether 34576 Grab EPA 624 7.6 ug/L Chloroform 32106 Grab EPA 624 2.0 3.1 ug/L Dichlorobromomethane 32101 Grab EPA 624 2.0 ND ug/L 1,1-dichloroethane 34496 Grab EPA 624 2.0 NO ug/L 1,2-dichloroethane 32103 Grab EPA 624 2.0 2.0 NO ug/L Trans-1,2-dichloroethylene 34546 Grab EPA 624 NO ug/L 1,1-dichloroethylene 334501 Grab EPA 624 2.0 NO ug/L 1,2-dichloropropane 34541 Grab EPA 624 2.0 2.0 NO ug/L 1,3-dichloropropylene 77163 Grab EPA 624 NO ug/L Ethylbenzene 34371 Grab EPA 624 2.0 NO ug/L Methyl Bromide 34413 Grab EPA 624 2.0 2.0 NO ug/L Methyl Chloride 34418 Grab EPA 624 2.0 NO ug/L Methylene Chloride 34423 Grab EPA 624 2.0 ND ug/L 1,1,2,2-tetrachloroethane 81549 Grab EPA 624 L 'Tetrachloroethylene 34475 I Grab EPA 624 2.0 Mc. I ugjL Toluene 34010 Grab EPA 624 2.0 NO ug/L 1, 1, 1 -trichloroethane 34506 Grab EPA 624 2.0 NO ug/L 1,1,2-trichloroethane 34511 Grab EPA 624 2.0 NO ug/L Trichloroethylene 39180 Grab EPA 624 2.0 NO ug/L Vinyl chloride 39175 Grab EPA 624 2.0 NO uglL Acid-extractabie compounds P-chloro-m-creso 34452 Grab EPA 625 6.0 NO ug/L 2-chlorophenol 34586 Grab EPA 625 5.0 NO ug/L 2,4-dichlorophenol 34601 Grab EPA 625 5.0 NO ug/L 2,4-dimethylphenol 34606 Grab EPA 625 10.0 NO ug/L 4,6-dinitro-o-cresol 34657 Grab EPA625 20.0 NO ug/L 2,4-dinitrophenol 34616 Grab EPA625 50.0 NO ug/L 2-nitrophenol 34591 Grab EPA 625 5.0 NO ug/L 4-nitrophenol 34646 Grab EPA625 50.0 NO ug/L Pentachlorophenol 39032 Grab EPA 625 10.0 NO ug/L Phenol 34694 Grab EPA 625 5.0 NO ug/L 2,4,6-tdchlorophenol 34621 Grab EPA 625 10.0 NO ug/L Base -neutral compounds Acenaphthene 34206 Grab EPA 625 5.0 NO ugIL Acenaphthylene 34200 Grab EPA 625 5.0 NO ug/L Anthracene CO220 Grab EPA 625 5.0 NO ug/L Benzidine 39120 Grab EPA 625 50.0 NO ug/L Benzo(a)anthracene 34526 Grab EPA 625 5.0 NO ug/L Benzo(a)pyrene 34247 Grab EPA625 5.0 NO ug/L 3,4 benzofluoranthene 34230 Grab EPA625 5.0 NO ug/L Benzo(ghi)perylene 34521 Grab EPA625 5.0 NO ug/L Benzo(k)fluoranthene 34242 Grab EPA 625 5.0 NO ug/L Bis (2-chloroethoxy) methane 34278 Grab EPA625 10.0 NO ug/L Bis (2-chloroethyl) ether 34273 Grab EPA625 5.0 NO ug/L Bis (2-chloroisopropyl) ether 34283 Grab EPA 625 5.0 NO ug/L Bis (2-ethylhexyl) phthalate 39100 Grab EPA 625 5.0 NO ug/L 4-bromophenyl phenyl ether 34636 Grab EPA 625 5.0 NO ug/L Butyl benzyl phthalate 34292 Grab EPA 625 5.0 NO ug/L 2-chloronaphthalene 34581 Grab EPA 625 5.0 NO ug/L 4-chlorophenyl phenyl ether 34641 Grab EPA 625 5.0 NO ug/L Chrysene 34320 Grab EPA625 5.0 NO ug/L Di-n-butyl phthalate 39110 Grab EPA 625 5.0 NO ug/L Di-n-octyl phthalate 34596 Grab EPA 625 5.0 NO ug/L Dibenzo(a,h)anthracene 34556 Grab EPA 625 5.0 NO ug/L 1,2-dichlorobenzene 34536 Grab EPA 625 5.0 NO ug/L 1,3-dichlorobenzene 34566 Grab EPA625 5.0 NO ug/L 1,4-dichlorobenzene 34571 Grab EPA625 5.0 NO ug/L 3,3-dichlorobenzidine 34631 Grab EPA625 25.0 NO ug/L Diethyl phthalate 34336 Grab EPA 625 5.0 NO ug/L Dimethyl phthalate 34341 Grab EPA 625 5.0 NO ug/L 2,4-dinitrotoluene 34611 Grab EPA 625 5.0 NO ug/L 2,6-dinitrotoluene C0626 Grab EPA 625 5.0 NO ug/L 1,2-diphenythydrazine 34346 Grab EPA625 5.0 NO ug/L Fluoranthene C0376 Grab EPA 625 5.0 NO ug/L Fluorene 34381 Grab EPA 625 5.0 NO ug/L Hexachlorobenzene C0700 Grab EPA 625 5.0 NO ug/L Hexachlorobutadiene 39702 Grab EPA625 5.0 NO ug/L Hexachlorocyclo-pentadiene 34386 Grab EPA625 10.0 NO ug/L Hexachloroethane 34396 Grab EPA 625 5.0 NO ug/L Indeno(1,2,3-cd)pyrene 34403 Grab EPA 625 5.0 NO ug/L Isepherone 3440E Grab EPA o"25 10.0 NO ilg/L Naphthalene 34696 Grab EPA 625 5.0 NO ug/L Nitrobenzene 34447 Grab EPA 625 5.0 ND ug/L N-nitrosodi-n-propylamine 34428 Grab EPA 625 5.0 NO ug/L N-nitrosodimethylamine 34438 Grab EPA 625 5.0 NO ug/L N-nitrosodiphenylamine 34433 Grab EPA 625 10.0 ND ug/L Phenanthrene 34461 Grab EPA 625 5.0 ND ug/L Pyrene 1,2,4,-ttichlorobenzene 34469 34551 Grab Grab EPA 625 EPA 625 5.0 5.0 ND 1 ND ug/L 41 I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Authorized Representative Name Signature Date Permit No. Outfail Facility Name Date of Sampling Analytical Laboratory: Annual Monitoring and Pollutant Scan NCO023906 Month: February EFF A-461 Year: 2018 City of Wilson - WRF ORC 02/06/2018 Phone Pace Analytical Services James M/. Pridgen (252)399-2491 Parameter Parameter Code Sample Type Analytical Method Quantitation Level Sample Result Units of Measurement Ammonia (as N) C0610 Composite SM 4500 C-2011 0.2 0.31 mg/L Chlorine (total residual, TRC) 60060 Grab SM 4500 G-2011 10 NO ug/L Dissolved oxygen 00300 Composite Sfv14500 G-2011 0 10.47 mg/L Nitrite + Nitrate Total (as N) 00630 Composite SM 4500 E 2011 0.05 0.325 mg/L Total Kjeldahi Nitrogen 1 00625 1 Composite I SM 4500 C-2011 0.2 1.41 mg/L Oil and Grease 00556 Grab EPA 1664B 5.0 NO mg/L Total Phosphorus C0665 Composite SM 4500 E-2011 0.05 0.057 mg/L Total Dissolved Solids 70295 Composite SM 2540 B-2011 2.5 253 mg/L Hardness 00900 Composite SM 2340 C-2011 662 38800 ug/L Metals (total recoverable), cyanide and total phenols . Antimony 01097 Composite EPA 200.8 1.0 NO ug/L Arsenic 01002 Composite SM 3113 B-2010 10 NO ug/L Beryllium 01012 Composite EPA 200.8 0.10 NO ug/L Cadmium 01027 Composite SM 3113 B-2010 0.2 NO ug/L Chromium 01034 Composite SM 3113 B-2010 5 NO ug/L Copper 01042 Composite SM 3113 B-2010 2 50 ug/L Lead 01051 1 Composite SM 3113 B-2010 10 NO ug/L Mercury (Method 1631 E) COMER Composite EPA 1631 E 0.5 0.518 ng/L Nickel 01067 Composite SM 3113 B-2010 10 ND ug/L Selenium 01147 Composite SM 3113 B-2010 5 NO ug/L Silver 01077 Composite SM 3113 B-2010 5 NO ug/L Thallium 01059 Composite EPA 200.8 1.0 NO ug/L Zinc 1 01092 Composite SM 3113 B-2010 1 10 25.2 ug/L Cyanide 00720 Grab EPA 335.4 0.010 NO mg/L Total phenolic compounds 32730 Grab EPA 420.4 0.010 0.011 mg/L Volatile organic compounds - Acrolein 34210 Grab EPA 624 5.0 NO ug/L Acrylonitrile 34215 Grab EPA 624 500 NO ug/L Benzene 34030 Grab EPA 624 2.0 ND ug/L Bromoform 32104 Grab EPA 624 2.0 ND ug/L Carbon tetrachloride 32102 Grab EPA 624 2.0 ND ug/L Chlorobenzene 34301 Grab EPA 624 2.0 NO ug/L Chlorodibromomethane 34306 Grab EPA 624 2.0 NO ug/L Chloroethane 85811 Grab EPA 624 2.0 NO ug/L 2-chloroethyl vinyl ether 34576 Grab EPA 624 5.0 NO ug/L Chloroform 32106 Grab EPA 624 2.0 NO ug/L Dichlorobromomethane 32101 Grab EPA 624 2.0 NO uglL 1,1-dichloroethane 34496 Grab EPA 624 2.0 ND ug/L 1,2-dichloroethane 32103 Grab EPA 624 2.0 NO ug/L Trans-1,2-dichloroethylene 34546 Grab EPA 624 2.0 NO ug/L 1,1-dichloroethylene 334501 Grab EPA 624 2.0 ND ug/L 1,2-dichloropropane 34541 Grab EPA 624 2.0 NO uglL 1,3-dichloropropylene 77163 Grab EPA 624 2.0 NO ug/L Ethylbenzene 34371 Grab EPA 624 2.0 NO ug/L Methyl Bromide 34413 Grab EPA 624 2.0 NO ug/L Methyl Chloride 34418 Grab EPA 624 2.0 NO ug/L Methylene Chloride 34423 Grab EPA 624 2.0 NO ug/L 1,1,2,2-tetrachloroethare 81549 Grab EPA 624 2.0 NO ug/L Tetrachlorcethylens 34475 Grab EPA 624 2.0 NO ug/L Toluene 34010 Grab EPA 624 2.0 NO ug/L 1,1,1-trichloroethane 34506 Grab EPA 624 2.0 NO ug/L 1,1,2-tdchloroethane 34511 Grab EPA 624 2.0 NO ug/L Trichloroethylene 39180 Grab EPA 624 2.0 NO ug/L Vinyl chloride 39175 1 Grab EPA 624 2.0 NO ug/L Acid -extractable compounds P-chloro-m-creso 34452 Grab EPA 625 5.1 NO ug/L 2-chlorophenol 34586 Grab EPA 625 5.1 NO ug/L 2,4-dichlorophenol 34601 Grab EPA 625 5.1 NO ug/L 2,4-dimethylphenol 34606 Grab EPA 625 10.2 NO ug/L 4,6-dinitro-o-cresol 34657 Grab EPA 625 20.4 NO ug/L 2,4-dinitrophenol 34616 Grab EPA 625 51.0 NO ug/L 2-nitrophenol 34591 Grab EPA 625 5.1 ND ug/L 4-nitrophenol 34646 Grab EPA 625 51.0 NO ug/L Pentachlorophenol 39032 Grab EPA 625 10.2 NO ug/L Phenol 34694 Grab EPA 625 5.1 NO ug/L 2,4,6-trichlorophenol 34621 Grab EPA 625 10.2 NO ug/L Base -neutral compounds Acenaphthene 34205 Grab EPA 625 5.1 NO ug/L Acenaphthylene 34200 Grab EPA 625 5.1 ND ug/L Anthracene CO220 Grab EPA 625 5.1 NO ug/L Benzidine 39120 Grab EPA 625 51.0 ND uglL Benzo(a)anthracene 34526 Grab EPA 625 5.1 NO ug/L Benzo(a)pyrene 34247 Grab EPA 625 5.1 ND uglL 3A benzofluoranthene 34230 Grab EPA 625 5.1 NO ug/L Benzo(ghi)perylene 34521 Grab EPA 625 5.1 NO Benzo(k)fluoranthene 34242 Grab EPA 625 5.1 NO Bis (2-chloroethoxy) methane 34278 Grab EPA 625 10.2 NO Bis (2-chloroethyl) ether 34273 Grab EPA 625 5.1 NO Bis (2-chioroisopropyl) ether 34283 Grab EPA 625 5.1 NO Bis (2-ethyihexyl) phthalate 39100 Grab EPA 625 5.1 NO lug/L 4-bromophenyI phenyl ether 34636 Grab EPA 625 5.1 NO Butyl benzyl phthalate 34292 Grab EPA 625 5.1 NO 2-chloronaphthalene 34581 Grab EPA 625 5.1 NO 4-chlorophenyl phenyl ether 34641 Grab EPA 625 5.1 NO Chrysene 34320 Grab EPA 625 5.1 NO Di-n-butyl phthalate 39110 Grab EPA 625 5.1 NO ug/L Di-n-octyl phthalate 34596 Grab EPA 625 5.1 NO ug/L Dibenzo(a,h)anthracene 34556 Grab EPA 625 5.1 NO ug/L 1,2-dichlorobenzene 34536 Grab EPA625 5.1 NO ug/L 1,3-dichlorobenzene 34566 Grab EPA 625 5.1 NO ug/L 1,4-dichlorobenzene 34571 Grab EPA 625 5.1 NO ug/L 3,3-dichiorobenzidine 34631 Grab EPA 625 25.5 NO ug/L Diethyl phthalate 34336 Grab EPA 625 5.1 ND ug/L Dimethyl phthalate 34341 Grab EPA 625 5.1 NO u9fl 2,4-dinitrotoluene 34611 Grab EPA 625 5.1 NO ug/L 2,6-dinitrotoluene CO626 Grab EPA 625 5.1 NO ug/L 1,2-diphenylhydrazine 34346 Grab EPA 625 5.1 NO ug/L Fluoranthene CO376 Grab EPA 625 5.1 ND ug/L Fluorene 34381 Grab EPA 625 5.1 NO ug/L Hexachlorobenzene CO700 Grab EPA 625 5.1 ND ug/L Hexachlorobutadiene 39702 Grab EPA 625 5.1 NO ug/L Hexachlorocyclo-pentadiene 34386 Grab EPA 625 10.2 ND ug/L Hexachloroethane 34396 Grab EPA 625 5.1 NO ug/L Inoenolt,2.3-co)pyrene 1 34+03 Grab EPA 625 1 5.1 NO I ugIL isophorone 34408 Grab EPA 525 10.2 NO NO ugiL ug/L Naphthalene 34696 Grab EPA 625 5.1 hlitrobenzene 34447 Grab EPA 625 5.1 ND ug/L N-nitrosodi-n-propylemine 34428 Grab EPA 625 5.1 NO ug/L N-nitrosodimethylamine 34438 Grab EPA 625 5.1 NO ug/L N-nitrosodiphenylamine 34433 Grab EPA 625 10.2 NO ug/L Phenanthrene 34461 Grab EPA 625 5.1 NO ug/L Pyrene 34469 Grab EPA 625 5.1 ND ug/L 1,2,4,-thchlorobenzene 34551 Grab EPA625 5.1 ND ug/L I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imp sonme for knowing violations. ��,` I j /)-2F Date FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: BASIN: City of Wilson - Hominy Creek WRF, NCO023906 Renewal :[!! Neuse SUPPLEMENTAL APPLICATION INFORMATION *Refer to previously submitted toxicity test data* PART E. TOXICITY TESTING DATA *Refer to previously submitted toxicity test data* P0TW5 meeting one or more of the following criteria must provide the results of whole effluent toxicity tests for acute or chronic toxicity for each of the facility's discharge points: 1) POT Ws with a design flow rate greater than or equal to 1.0 mgd; 2) POTWs with a pretreatment program (or those that are required to have one under 40 CFR Part 403); or 3) POTWs required by the permitting authority to submit data for these parameters. • At a minimum, these results must include quarterly testing for a 12-month period within the past 1 year using multiple species (minimum of two species), or the results from four tests performed at least annually in the four and one-half years prior to the application, provided the results show no appreciable toxicity, and testing for acute and/or chronic toxicity, depending on the range of receiving water dilution. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analyzes not addressed by 40 CFR Part 136. • In addition, submit the results of any other whole effluent toxicity tests from the past four and one-half years. If a whole effluent toxicity test conducted during the past four and one-half years revealed toxicity, provide any information on the cause of the toxicity or any results of a toxicity reduction evaluation, if one was conducted. • If you have already submitted any of the information requested in Part E, you need not submit it again. Rather, provide the information requested in question EA for previously submitted information. If EPA methods were not used, report the reasons for using alternate methods. If test summaries are available that contain all of the information requested below, they may be submitted in place of Part E. If no biomonitcring data is required, do not complete Part E. Refer to the Application Overview for directions on which other sections of the forth to complete. E.1. Required Tests. Indicate the number of whole effluent Windy tests conducted in the past four and one-half years. 23 chronic 0 acute *Refer to previously submitted toxicity test data* E.2. Individual Test Date. Complete the following chart for each whole effluent toxicity test conducted in the last four and one-half years. Allow one column per test (where each species constitutes a test). Copy this page if more than three tests are being reported. a. Test information. Test number. 1 Test number. 2 Test number: 3 Ceriodaphnia dubia Ceriodaphnia dubia Ceriodaphnia dubia Test Species & test method number EPA 1002.0 EPA 1002.0 EPA 1002.0 Age at initiation of test <24 hours old <24 hours old <24 hours old Outfall number 001 001 001 Dates sample collected 2/17114 — 2120114 515114 — 518114 814114 — 817/14 Date test started 2119114 517114 816114 Duration 7 days 7 days 7 days b. Give toxicity test methods followed. Manual title EPA-821-R-02-013 EPA-821-R-02-013 EPA-821-R-02-013 Edition number and year of publication 4th Edition, Oct 2002 4th Edition, Oct 2002 4th Edition, Oct 2002 Page number(s) 1 - 335 1 - 335 1 - 335 c. Give the sample collection method(s) used. For multiple grab samples, indicate the number of grab samples used. 24-Hour composite X X X Grab d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each. Before disinfection After disinfection After dechlonnation X X X EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 15 of 42 FACILITY NAME AND PERMIT NUMBER: City of Wilson - Hominy Creek WRF, NCO023906 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Neuse Test number: 1 Test number. 2 Test number: 3 e. Describe the point in the treatment process at which the sample was collected. Sample was collected: Eff Ouffall 001 Eff Outfall 001 Eff Ouffall 001 I. For each test, include whether the test was intended to assess chronic toxicity, acute toxicity, or both Chronic toxicity X X X Acute toxicity g. Provide the type of test performed. Static Static -renewal X X X Flow -through h. Source of dilution water. If laboratory water, specify type; if receiving water, specify source. Laboratory water Soft synthetic water Soft synthetic water Soft synthetic water Receiving water i. Type of dilution water. If salt water, specify 'natural' or type of artificial sea setts or brine used. Fresh water X X X Salt water I. Give the percentage effluent used for all concentrations in the test series. 0% & 90% 0% & 90% 0% & 90% k. Parametersmeasured during the test (State whether parameter meets test method specifications) pH Yes Yes Yes Salinity Not applicable Not applicable Not applicable Temperature Yes Yes Yes Ammonia Not applicable Not applicable Not applicable Dissolved oxygen Yes Yes Yes I. Test Results. Acute: Percent survival in t00% effluent % % LCm 95% C.I. % % % Control percent survival % % % Other(describe) EPA Forn 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 16 of 42 FACILITY NAME AND PERMIT NUMBER: City of Wilson - Hominy Creek WRF, NCO02390 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Neuse Chronic: Test number: 1 Test number: 2 Test number: 3 NOEC 90 % 90 % 90 % ICH >90 % >90 % >90 % Control percent survival 100 % 100 % 100 % Other (describe) Pass/Fail Pass Pass Pass m. Quality Control/Quality Assurance. Is reference toxicant data available? Yes Yes Yes Was reference toxicant test within acceptable bounds? Yes Yes Yes What date was reference toxicant test run (MM/DO/YYYY)? 2/18/2014 5/6/2014 815/2014 Other(describe) E.3. Toxicity Reduction Evaluation. Is the treatment works involved in a Toxicity Reduction Evaluation? ❑ Yes ® No If yes, describe: NA EA. Summary of Submitted Biomonitoring Test Information. If you have submitted biomonitonng test information, or information regarding the cause of toxicity, within the past four and one-half years, provide the dates the information was submitted to the permitting authority and a summary of the results. Date submitted: NA / NA / NA (MM/DD/YYYY) Summary of results: (see instructions) NA EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 755" & 7550-22. Page 17 of 42 FACILITY NAME AND PERMIT NUMBER: City of Wilson - Hominy Creek WRF, NCO023906 SUPPLEMENTAL APPLICATION INFORMATION PART E. TOXICITY TESTING DATA (continued) a. Test informabon, Test number: 4 Test Species & test method number Ceriodaphnia dubia EPA 1002.0 Age at initiation of test <24 hours old Outfall number 001 Dates sample collected 1113/14-1116/14 Date test started 1115114 Duration 7 days PERMIT ACTION REQUESTED: RIVER BASIN: Renewal Neuse *Refer to previously submitted toxicity test data* *Refer to previously submitted toxicity test data* Test number. 5 Test number: 6 Ceriodaphnia dubia EPA 1002.0 Ceriodaphnia dubia EPA 1002.0 <24 hours old <24 hours old 001 001 2/2/2015 - 215/2016 514/15 - 5/7115 214115 5l6/15 7 days 7 days b. Give toxicity test methods followed. Manual tille EPA-821-R-02-013 EPA-821-R-02-013 EPA-821-R-02-013 Edition number and year of publication 4th Edition, Oct 2002 4th Edition, Oct. 2002 4th Edition, Oct 2002 Page numbers) 1 - 335 1 - 335 1 - 335 c. Give the sample collection methods) used. For multiple grab samples, indicate the number of grab samples used. 24-Hour composite X X X Grab d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each. Before disinfection After disinfection After dechlorination x x X EPA Form 3510-2A (Rev. 1-99). Replaces EPA fors 7550-6 & 7550-22. Page 18 of 42 FACILITY NAME AND PERMIT NUMBER: City of Wilson - Hominy Creek WRF, NCO023906 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Neuse Test number. 4 Test number. 5 Test number: 6 e. Describe the point in the treatment process at which the sample was collected. Sample was collected: Eff Outfall 001 Eff Ouffall 001 Eff Outfall 001 I. For each test, include whether the test was intended to assess chronic toxicity, awte toxicity, or both Chronic toxicity X X X Acute toxicity g. Provide the type of test performed. Static Statio-renewal X X X Flow -through h. Source of dilution water. If laboratory water, specify type; if receiving water, specify source. Laboratory water Soft synthetic water Soft synthetic water Soft synthetic water Receiving water i. Type of dilution water. If salt water, specify 'natural' a type of artificial sea salts or bdne used. Fresh water X X X Salt water j. Give the percentage effluent used for all concentrations in the test series. 0% & 90% 0% & 90% 0% & 90% k. Parameters measured during the test (State whether parameter meets test method specifications) pH Yes Yes Yes Salinity Not applicable Not applicable Not applicable Temperature Yes Yes Yes Ammonia Not applicable Not applicable Not applicable Dissolved oxygen Yes Yes Yes I. Test Results. Acute: Percent survival in 1DO% effluent % % % LCw 95% C.I. % % % Control percent survival % % % Other(descdbe) EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 19 of 42 FACILITY NAME AND PERMIT NUMBER: City of Wilson - Hominy Creek WRF, NCO023906 Chronic: Test number. 4 NOEC 90 % Ices >90 % Control percent survival 100 % Other (describe) Pass/Fail Pass PERMIT ACTION REQUESTED: Renewal Test number: 5 90 % >90 % 100 % Pass RIVER BASIN: Neuse Test number. 6 90 % >90 % 100 % Pass m. Quality Control/Quality Assurance. Is reference toxicant data available? Yes Yes Yes Was reference toxicant test within acceptable bounds? yes Yes Yes What date was reference toxicant test run (MWDD/YYYY)? 11/412014 2/3/2016 5/512015 Other (describe) E.3. Toxicity Reduction Evaluation. ❑ Yes ® No Is the treatment works involved in a Toxicity Reduction Evaluation? If yes, describe: NA EA. Summary of Submitted Blomonitoring Test Information. If you have submitted bionwnitoring test information, or information regarding the cause of toxicity, within the past four and one-half years, provide the dates the information was submitted to the permitting authority and a summary of the results. Date submitted: NA I NA I NA (MWDD/YYYY) Summary of results. (see instructions) EPA Form 3510.2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 20 of 42 FACILITY NAME AND PERMIT NUMBER: City of Wilson - Hominy Creek WRF, NCO023906 SUPPLEMENTAL APPLICATION INFORMATION PART E. TOXICITY TESTING DATA (continued) a. Test information. Test number. 7 Test Spades & test method number Ceriodaphnia dubia EPA 1002.0 Age at initiation of test <24 hours old Outfall number 001 Dates sample collected 813115 — 816/15 Date test started 815114 Duration 7 days PERMIT ACTION REQUESTED: RIVER BASIN: Renewal Neuse *Refer to previously submitted toxicity test data* *Refer to previously submitted toxicity test data* Test number. 8 Test number: 9 Pimephales promelas EPA 1000.0 Ceriodaphnia dubia EPA 1002.0 <24 hours old <24 hours old 001 001 11/15115-11120115 11116/15-11119115 11/17/15 11/18/14 7 days 7 days b. Give toxicity test methods followed. Manual title EPA-821-R-02-013 EPA-821-R-02-013 EPA-821-R-02-013 Edition number and year of publication 4th Edition, Oct. 2002 4th Edition, Oct 2002 4th Edition, Oct. 2002 Page number(s) 1 - 335 1 - 335 1 - 335 c. Give the sample collection method(s) used. For multiple grab samples, indicate the number of grab samples used. 24-Hour composite X X X Grab d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each. Before disinfection After disinfection After dechlonnation X X X EPA Form 351 g-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 21 of 42 FACILITY NAME AND PERMIT NUMBER: City of Wilson - Hominy Creek WRF, NCO0239067 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Neuse Test number: 7 Test number. B Test number: 9 e. Describe the point in the treatment process at which the sample was collected. Sample was collected: Elf Outfall 001 Eff Outfall 001 Eff Outfall 001 f. For each test, include whether the test was intended to assess chronic trnacity, acute toxicity, or both Chronic toxicity X X X Acute toxicity g. Provide the type of test performed. Static Statio•renewal X X X Flow -through h. Source of dilution water. If laboratory water, specify type; if receiving water, specify source. Laboratory water Soft synthetic water Soft synthetic water Soft synthetic water Receiving water i. Type of dilution water. If salt water, specify "natural° or type of artificial sea salts or brine used. Fresh water X X X Salt water j. Give the percentage effluent used for all concentrations in the test series. 0% & 90% 0% & 45% 0% & 90% 67.5% & 90% 95% & 100% k. Parameters measured during the test. (State whether parameter meets test method specifications) pH Yes Yes Yes Salinity Not applicable Not applicable Not applicable Temperature Yes Yes Yes Ammonia Not applicable Not applicable Not applicable Dissolved oxygen Yes Yes Yes I. Test Results. Acute. Percent survival in 100% effluent % % % Lew 95% C.I. % % % Control percent survival % % % Other (describe) EPA Form 351 c-2A (Rev. 1-99). Replaces EPA fomu 7550-6 & 7550-22, Page 22 of 42 FACILITY NAME AND PERMIT NUMBER: City of Wilson - Hominy Creek WRF, NCO023906 PERMIT ACTION REQUESTED: Renewal RNER BASIN: Neuse Chronic: Test number. 7 Test number: 8 Test number. 9 NOEL 90 % 100 % 90 % IC25 >90 % >100 % >90 % Control percent survival 100 % 100 % 100 % Other (describe) Pass/Fail Pass ChV >100% Pass m. Quality Control/Quality Assurance. Is reference toxicant data available? Yes Yes Yes Was reference toxicant test within acceptable bounds? yes Yes Yes What date was reference toxicant test run (MM/DDIYYYY)? 8/4/2015 11/17/2015 11/17/2015 Other(desonbe) E.3. Toxicity Reduction Evaluation. Is the treatment works involved in a Toxicity Reduction Evaluation? ❑ Yes ® No If yes, describe: NA EA. Summary of Submitted Biomonitoring Test Information. If you have submitted biomonitonng test information, or information regarding the cause of toxicity, within the past four and one-half years, provide the dates the information was submitted to the permitting authority and a summary of the results. Date submitted: NA / NA / NA (MM/DDNYYY) Summary of results: (see instructions) NA EPA Form 3510.2A (Rev. 1-99). Replaces EPA forms 7550-8 & 7550-22. Page 23 of 42 FACILITY NAME AND PERMIT NUMBER: City of Wilson - Hominy Creek WRF, NCO023906 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Neuse SUPPLEMENTAL APPLICATION INFORMATION "Refer to previously submitted toxicity test data' PART E. TOXICITY TESTING DATA (continued) 'Refer to previously submitted toxicity test data' a. Test information. Test number. 10 Test number11 Test number. 12 Test Species 8 test method number Ceriodaphnia dubia EPA 1002.0 Ceriodaphnia dubia EPA 1002.0 Pimephales promelas EPA 1000.0 Age at initiation of test <24 hours old <24 hours old <24 hours old Outfall number 001 001 001 Dates sample collected 211 /16 — 214116 512116 — 5/6116 817116 — 8/12116 Date test started 213/16 514116 819116 Duration 7 days 7 days 7 days b. Give toxicity test methods followed. Manual title EPA-821-R-02-013 EPA-821-R-02-013 EPA-821-R-02-013 Edition number and year of publication 4th Edition, Oct. 2002 4th Edition, Oct. 2002 4th Edition, Oct. 2002 Page number(s) 1 - 335 1 - 335 1 - 335 c. Give the sample collection method(s) used. For multiple grab samples, indicate the number of grab samples used. 24-Hour composite X X X Grab d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each. Before disinfection After disinfection After dechlonnation X X X EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550 6 & 7550-22. Page 24 of 42 FACILITY NAME AND PERMIT NUMBER: City of Wilson - Hominy Creek WRF, NCO023906 ION REQUESTED: PERMIT ACTRenewal RNER BASIN: Neuse Test number: 10 Test number: 11 Test number: 12 e. Describe the point in the treatment process at which the sample was collected. Sample was collected: Eff Outfall 001 Eff Outfall 001 Eff Outfall 001 I. For each test, include whether the test was Intended to assess chronic toxicity, acute toxicity, or both Chronic toxicity X X X Acute toxicity g. Provide the type of test performed. Static Static -renewal X X X Flow -through h. Source of dilution water. If laboratory water, specify type; if receiving water, specify source. Laboratory water Soft synthetic water Soft synthetic water Soft synthetic water Reoeiving water i. Type of dilution water. If salt water, specify 'natural' or type of artificial sea salts or brine used. Fresh water X X X Salt water j. Give the percentage effluent used for all concentrations in the test series. 0% & 90% 0% & 90% 0% & 45% 67.5% & 90% 95% & 100% k. Parameters measured during the test (State whether parameter meets test method specifications) pH Yes Yes Yes Salinity Not applicable Not applicable Not applicable Temperature Yes Yes Yes Ammonia Not applicable Not applicable Not applicable Dissolved oxygen Yes Yes Yes 1. Test Results. Acute: Percent survival in 100% effluent % % % LCx 95% C.I. % % % Control percent survival % % % Other (describe) EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22, Page 25 of 42 FACILITY NAME AND PERMIT NUMBER: City of Wilson - Hominy Creek WRF, NC0023906 PERMIT ACTION REQUESTED:7u� Renewal BASIN: Neuse Chronic Test number: 10 Test number: 11 Test number. 12 NOEC 90 % 90 % 100 % ICzs >90 % >90 % >100 % Control percent survival 100 % 100 % 100 % Other (describe) Pass/Fail Pass Pass ChV >100% m. Quality Control/Quality Assurance. Is reference toxicant data available? Yes Yes Yes Was reference toxcant test within acceptable bounds? Yes Yes Yes What date was reference toxicant test run (MMIDDIYYYY)? 212/2016 513/2016 8/9/2016 Other (describe) E.3. Toxicity Reduction Evaluation. Is the treatment works involved in a Toxicity Reduction Evaluation? ❑ Yes ® No If yes, describe: NA E.4. Summary of Submitted Biomonitoring Test Information. If you have submitted bionrondodng test information, or information regarding the cause of toxicity, within the past four and one-half years, provide the dates the information was submitted to the permitting authority and a summary of the results. Date submitted: NA / NA / NA (MMIDDNYYY) Summary of results: (see instructions) NA EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 26 of 42 FACILITY NAME AND PERMIT NUMBER: City of Wilson - Hominy Creek WRF, NCO023906 SUPPLEMENTAL APPLICATION INFORMATION PART E. TOXICITY TESTING DATA (continued) a. Test information. Test number[ 13 Test Species & test method number Ceriodaphnia dubia EPA 1002.0 Age at initiation of test <24 hours old Outfall number 001 Dates sample collected 8/8116 — 8111116 Date test started 8110116 Duration 7 days PERMIT ACTION REQUESTED: RIVER BASIN: Renewal Neuse *Refer to previously submitted toxicity test data* *Refer to previously submitted toxicity test data* Test number 14 Testnumber 15 Ceriodaphnia dubia EPA 1002.0 Ceriodaphnia dubia EPA 1002.0 <24 hours old <24 hours old 001 001 10131116-11/03116 2/6117-219117 11/02/16 218117 7 days 7 days b. Give toxicity test methods followed. Manual title EPA-821-R-02-013 EPA-821-R-02-013 EPA-821-R-02-013 Edition number and year of publication 4th Edition, Oct 2002 4th Edition, Oct. 2002 4th Edition, Oct 2002 Page number(s) 1 - 335 1 - 335 1 - 335 c. Give the sample collection method(s) used. For multiple grab samples, indicate the number of grab samples used. 24-Hour composite X X X Grab d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each. Before disinfection After disinfection After dechlonnation X X X EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 27 of 42 FACILITY NAME AND PERMIT NUMBER: City of Wilson - Hominy Creek WRF, NCO023906 ION REQUESTED: PERMIT ACTRenewal RIVER BASIN: Neuse Test number: 13 Test number: 14 Test number: 15 e. Describe the point in the treatment process at which the sample was collected. Sample was collected: Eff Ouffall 001 Eff Ouffall 001 Eff Outfall 001 I. For each test, include whether the test was intended to assess chronic toxicity, acute toxicity, or bath Chronic toxicity X X X Acute toxicity g. Provide the type of test performed. Static Statiorenewal X X X Flow -through h. Source of dilution water. If laboratory water, specify type; if receiving water, specify source. Laboratory water Soft synthetic water Soft synthetic water Soft synthetic water Receiving water i. Type of dilution water. If salt water, specify 'natural' or type of artificial sea salts or brine used. Fresh water X X X Salt water j. Give the percentage effluent used for all concentrations in the test series. 0% & 90% 0% & 90% 0% & 90% k. Parameters measured during the test. (State whether parameter meets test method specifications) pH Yes Yes Yes Salinity Not applicable Not applicable Not applicable Temperature Yes Yes Yes Ammonia Not applicable Not applicable Not applicable Dissolved oxygen Yes Yes Yes I. Test Results. Acute. Percent survival in 100% effluent % % LCw 95% C.I. % % % Control percent survival % % % Other (describe) EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 28 of 42 FACILITY NAME AND PERMIT NUMBER: City of Wilson - Hominy Creek WRF, NCO023906 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Neuse Chronic: Test number. 13 Teat number. 14 Test number. 15 NOEC 90 % 90 % 90 % IC25 >90 % >90 % >90 % Control percent survival 100 % 100 % 100 % Other (describe) Pass Pass Pass m. Quality Control/Quality Assurance. Is reference toxicant data available? Yes Yes Yes Was reference toxicant test within acceptable bounds? Yes Yes Yes What date was reference toxicant test run (MM/DD/YYYY)? 819/2016 11/112016 2/7/2017 Other (describe) E.3. Toxicity Reduction Evaluation. Is the treatment works involved in a Toxicity Reduction Evaluation? ❑ Yes ® No If yes, describe: NA EA. Summary of Submitted Biomonitoring Test Information. If you have submitted biomonitoring test information, or information regarding the cause of toxicity, within the past four and one-half years, provide the dates the information was submitted to the permitting authority and a summary of the results. Date submitted: NA / NA / NA (MM/DD/YYYY) Summary of results: (see instructions) NA EPA Form 3516QA (Rev. 1-99). Replacas EPA forms 7550-6 & 755G-22. Page 29 of 42 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: City of Wilson - Hominy Creek WRF, NCO023906 Renewal Neuse SUPPLEMENTAL APPLICATION INFORMATION *Refer to previously submitted toxicity test data* PART E. TOXICITY TESTING DATA (continued) a. Test information. Test number 16 Test Species 8 test method number Pimephales promela EPA 1000.0 Age at initiation of test <24 hours old Outfall number 001 Dates sample collected 5114/17 — 5/19/17 Date test started 5116117 Duration 7 days *Refer to previously submitted toxicity test data* Test number. 17 Testnumber. 16 s Ceriodaphnia dubia EPA 1002.0 Ceriodaphnia dubia EPA 1002.0 <24 hours old <24 hours old 001 001 5115117 — 5/18117 7131117 — 8/3117 5/17117 812117 7 days 7 days b. Give toxicity test methods followed. Manual title EPA-821-R-02-013 EPA-821-R-02-013 EPA-821-R-02-013 Edition number and year of publication 4th Edition, Oct. 2002 4th Edition, Oct. 2002 4th Edition, Oct. 2002 Page number(s) 1 - 335 1 - 335 1 - 335 c. Give the sample collection method(s) used. For multiple grab samples, indicate the number of grab samples used. 24-Hour composite X X X Grab d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each. Before disinfection After disinfection After dechlodnation X X X EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 30 of 42 FACILITY NAME AND PERMIT NUMBER: City of Wilson - Hominy Creek WRF, NCO023906 PERMIT ACTION REQUESTED: Renewal RNER BASIN: Neuse Test number. 16 Test number: 17 Test number: 18 e. Describe the point in the treatment process at which the sample was collected. Sample was collected: Eff Outfall 001 Eff Outfall 001 Eff Outfall 001 f. For each test, include whether the test was intended to assess chronic toxicity, acute toxicity, or both Chronic toxicity X X X Acute toxicity g. Provide the type of test performed. Static Static -renewal X X X Flow -through h. Source of dilution water. If laboratory water, specify type; if receiving water, specify source. Laboratory water Soft synthetic water Soft synthetic water Soft synthetic water Receiving water i. Type of dilution water. If salt water, specify "natural° or type of artificial sea salts or brine used. Fresh water X X X Salt water j. Give the percentage effluent used for all concentrations in the test series. 0% & 45% 0% & 90% 0% & 90% 67.5% & 90% 96% & 100% k. Parameters measured during the test (State whether parameter meets test method specifications) pH Yes Yes Yes Salinity Not applicable Not applicable Not applicable Temperature Yes Yes Yes Ammonia Not applicable Not applicable Not applicable Dissolved oxygen Yes Yes Yes I. Test Results. Acute: Percent survival in 100% effluent ova % % LCw 96% C.I. % % % Control percent survival % % % Other (describe) EPA Form 3510-2A (Rev. 1-99). Replaces EPA fors 7550-e & 7550-22. Page 31 of 42 FACILITY NAME AND PERMIT NUMBER: City of Wilson -Hominy Creek WRF, NC0023906 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Neuse Chronic Test number. 16 Test number: 17 Test number: 18 NOEC 100 % 90 % 90 % Ica$ >100 % >90 % >90 % Control percent survival 100 % 100 % 100 % Other (describe) Pass/Fail ChV >100% Pass Pass m. Quality Control/Quality Assurance. Is reference toxicant data available? Yes Yes Yes Was reference toxicant test within acceptable bounds? Yes Yes Yes What date was reference toxicant test run (MM/DDNYYY)? 5116117 5116117 8I1/2017 Other (describe) E.3. Toxicity Reduction Evaluation. Is the treatment works involved in a Toxicity Reduction Evaluation? ❑ Yes ® No If yes, describe: NA E.4. Summary of Submitted Biomonitoring Test Information. If you have submitted biomonitorirg test information, or information regarding the cause of toxicity, within the past four and one-half years, provide the dates the information was submitted to the permitting authority and a summary of the results. Date submitted: NA / NA / NA (MM/DDNYYY) Summary of results: (see instructions) NA EPA Form 3579-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 32 of 42 FACILITY NAME AND PERMIT NUMBER: City of Wilson - Hominy Creek WRF, NCO023906 SUPPLEMENTAL APPLICATION INFORMATION PART E. TOXICITY TESTING DATA (Continued) a. Test information. Test number: 19 Test Species & test method number Ceriodaphnia dubia EPA 1002.0 Age at initiation of test <24 hours old Oudall number 001 Dates sample collected 11/6/17 — 1119117 Date test started 1118/17 Duration 7 days PERMIT ACTION REQUESTED: RIVER BASIN: Renewal Neuse *Refer to previously submitted toxicity test data* *Refer to previously submitted toxicity test data* Test number. 20 Test number: 21 Pimephales promelas EPA 1000.0 Ceriodaphnia dubia EPA 1002.0 <24 hours old <24 hours old 001 001 214118-2/9118 215118 — 218/18 216118 217118 7 days 7 days b. Give toxicity test methods followed. Manual fide EPA-821-R-02-013 EPA-821-R-02-013 EPA-821-R-02-013 Edition number and year of publication 4th Edition, Oct 2002 4th Edition, Oct. 2002 4th Edition, Oct. 2002 Page number(s) 1 - 335 1 - 335 1 - 335 c. Give the sample collection method(s) used. For multiple grab samples, indicate the number of grab samples used. 24-Hour composite X X X Grab d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each. Before disinfection After disinfection After dechkxination X X X EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 33 of 42 FACILITY NAME AND PERMIT NUMBER: City of Wilson - Hominy Creek WRF, NCO023906 PERMIT ACTION REQUESTED: Renewal RNER BASIN: Neuse Test number: 19 Test number: 20 Test number: 21 e. Describe the point in the treatment process at which the sample was collected. Sample was collected: Eff Outfall 001 Eff Outfall 001 Eff Outfall 001 I. For each test, include whether the test was intended to assess chronic toxicity, acute toxicity, or both Chronic toxicity X X X Acute toxicity g. Provide the type of test performed. Static Statio•renewal X X X Flow -through h. Source of dilution water. If laboratory water, specify type, if receiving water, specify source. Laboratory water Soft synthetic water Soft synthetic water Soft synthetic water Receiving water i. Type of dilution water. If salt water, specify "natural' or type of artificial sea salts or brine used. Fresh water X X X Salt water j. Give the percentage effluent used for all concentrations in the test series. 0% & 90% 0% & 45% 0% & 90% 67.5% & 90% 95% & 100% k. Parameters measured during the test (State whether parameter meets test method specifications) PH Yes Yes Yes Salinity Not applicable Not applicable Not applicable Temperature Yes Yes Yes Ammonia Not applicable Not applicable Not applicable Dissolved oxygen Yes Yes Yes I. Test Results. Acute: Percent survival in 100% effluent % % % LCw 95% C.I. % % % Control percent survival % % % Other (describe) EPA Form 3510-ZA (Rev. 1-99). Replaces EPA foram 7550-0 & 7550-22. Page 34 of 42 FACILITY NAME AND PERMIT NUMBER: City of Wilson - Hominy Creek WRF, NCO023906 PERMIT ACTION REQUESTED: Renewal RNER BASIN: Neuse Chronic: Test number: 19 Test number: 20 Test number: 21 NOEC 90 % 100 % 90 % IC25 >90 % >100 % >90 % Control percent survival 100 % 100 % 100 % Other (describe) Pass/Fail Pass ChV >100% Pass m. Quality Control/Quality Assurance. Is reference toxicant data available? Yes Yes Yes Was reference toxcant test within acceptable bounds? Yes Yes Yes What date was reference toxicant test run (MWDD/YYYY)? 1117117 216/18 216118 Other (describe) E.3. Toxicity Reduction Evaluation. Is the treatment works involved in a Toxicity Reduction Evaluation? ❑ Yes ® No If yes, describe: NA EA. Summary of Submitted Biomonitoring Test Information. if you have submitted biomonitoring test information, or information regarding the cause of toxicity, within the past four and one-half years, provide the dates the information was submitted to the permitting authority and a summary of the results. Date submitted: NA / NA / NA (MM/DDNYYY) Summary of results: (see instructions) NA EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550E & 7550-22. Page 35 of 42 FACILITY NAME AND PERMIT NUMBER: City of Wilson - Hominy Creek WRF, NCO023906 SUPPLEMENTAL APPLICATION INFORMATION PART E. TOXICITY TESTING DATA (continued) a. Test information. Test number: 22 Test Species & test method number Ceriodaphnia dubia EPA 1002.0 Age at initiation of test <24 hours old Outfall number 001 Dates sample collected 577/18 — 5110/18 Date test started 519118 Duration 7 days PERMIT ACTION REQUESTED: RIVER BASIN: Renewal Neuse *Refer to previously submitted toxicity test data* *Refer to previously submitted toxicity test data* Test number: 23 Test number. Ceriodaphnia dubia EPA 1002.0 <24 hours old 001 816/18 — 819118 818118 7 days b. Give toxicity test methods followed. Manual We EPA-821-R-02-013 EPA-821-R-02-013 Edition number and year of pubtication 4th Edition, Oct. 2002 4th Edition, Oct. 2002 Page number(s) 1 - 335 1 - 335 c. Give the sample collection method(s) used. For multiple grab samples, indicate the number of grab samples used. 24-Four composite x x Grab d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each. Before disinfection After disinfection After dechlodnation X X EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 75546 & 7550-22. Page 36 of 42 FACILITY NAME AND PERMIT NUMBER: City of Wilson - Hominy Creek WRF, NCO023906 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Neuse Test number: 22 Test number: 23 Test number: e. Describe the point in the treatment process at which the sample was collected. Sample was collected: Eff Ouffall 001 Eff Outfall 001 I. For each test, include whether the test was intended to assess chronic toxicity, acute toxicity, or both Chronic toxicity X X Acute toxicity g. Provide the type of test performed. Static Static -renewal X X Flow -through h. Source of dilution water. If laboratory water, specify type; if receiving water, specify source. Laboratory water Soft synthetic water Soft synthetic water Receiving water i. Type of dilution water. If saltwater, specify 'natural* or type of artificial sea salts of brine used. Fresh water X X Salt water j. Give the percentage effluent used for all concentrations in the test series. 0% & 90% 0% & 90% k. Parameters measured dudng the test (State whether parameter meets test method specifications) pH Yes Yes Salinity Not applicable Not applicable Temperature Yes Yes Ammonia Not applicable Not applicable Dissolved oxygen Yes Yes I. Test Results. Acute: Percent survival in 100% effluent % ova LCm 95% C.I. % % % Control percent survival % % % Other (describe) EPA Form 3510.2A (Rev. 1-e9). Replaces EPA forms 755" & 7550-22. Page 37 of 42 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: City of Wilson - Hominy Creek WRF, NCO023906 Renewal Neuse Chronic: Test number: 22 Test number: 23 Test number: NOEC 90 % 90 % lcz >90 % >90 % Control percent survival 100 % 100 % Other (describe) Pass/Fail Pass Pass m. Quality Control/Quality Assurance. Is reference toxicant data available? Yes Yes Was reference toxicant test within Yes Yes acceptable bounds? What date was reference toxicant test 518/18 8/7118 run (MMIDDIYYYY)? Other (describe) E.3. Toxicity Reduction Evaluation. Is the treatment works involved in a Toxicity Reduction Evaluation? ❑ Yes ® No If yes, describe: NA EA. Summary of Submitted Siomonitoring Test Information. If you have submitted biomonitoring test information, or information regarding the cause of toxicity, within the past four and one-half years, provide the dates the information was submitted to the permitting authority and a summary of the resuts. Date submitted: NA / NA / NA (MM/DD/YYYY) Summary of results: (see instructions) NA END OF PART E. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE. EPA Forth 3510.2A (Rev. 1-99). Replaces EPA forms 7550-6 8 7550-22. Page 38 of 42 .° Asheville, INC 23302 • T phone: (323)350.9364 1 -- Fa�c: (328) 350.9363 EnmmnmansaRosttng 5osmlons, In<. Date: March 01, 2014 Efiluent Aquatic Toxicity Report Form - Phase 11 Chronic Ceriodaphnia dubia Facility: Wilson WW'T7 N - 0023906 Pipe b: 001 County: Wilson C Comments: Laboratory Performing Test. Env nmenl9FLestin elUt ons. c. Signature of 0perator in Responsible C a 44 fi Psnjmc 9638 Signature of Laboratory Supervisor: gynp(er. 14021909, 140221 09 Mail Original To: North Ckmlina Depa Sci DWQ1 En 1621 Mail Service Center Raleigh, NC 27699-1621 Sample information sam9le I s nvironment and Natural Resources Branch Sort date: End date: Stan taut. 007335 02.19-14 02-26-14 121d Collection smt date: 02.17.14 02-19-14 Grab: Composite dmaoon: 24.5-h 25-b Alkalinity (mr/L CaCOa7 Hardness (mg(L CaC%): Cwductiviry(Whoslcm): 369 372 Total residual chimme (mr/l.): eoAo N.IO Sample Temp at Receipt CC): 24 0.8 Test Information�- Control Co.-[ Ccam Treatment: 00% 90% 90% 1.20 7.20 124 Initial PH (SU): 7.79 1.11 7.73 7.7 7. 137 71 Final pH (SU): 7.79 1.70 7.85 1,1 7.8 1.1 41 Initial DO(m,91): 8.2 8.7 85 .9 81 16 a u4 Final DO (ml;U; 8.5 8.5 It 6.7 24.9 24.7 24. ' - Initial Temp. CC): 25.2 2d.8 25.1 24.9 25. Final Temp. CQ: 24.9 25.2 24.9 24.7 Organism Number Control Organisms 1 2 3 4 5 6 7 8 9 10 11 12 .ra Number of Young Produced 29 28 29 32 29 28 29 30 31 29 28 29 29.3 Adult Survival (Live (Dkad L L L L t 1 I Effluent Percentage 90 ... ... __. 4a_.....:e,..a 1 2 3 4 5 6 7 8 9 10 l l 12 rM+. „r Effluent Percentage 4 5 6 7 8 9 10 11 12 - Treatment 3 Organisms 1 2 3 Effluent Percentage= Treatment 4 Organisms 1 Effluent Percentage= Effluent Percentage Treatment 6 Organisms 3 4 2 3 4 5 6 7 8 9 10 11 4 5 6 7 8___ 9 1_-.- 0 11 r 2 Overall Analysis: 90% ChV: '90a/° Result: PASS LOEC: >90% NOEC: 0 121 fT 4ar :. r <� Envlrvnmencal Tesaing Solutlonz,Inc. Effluent Aquatic Toxicity Report Form - Phase If Chronic C',ef2bda( Asheville,NC 23309 Phone: (828) 350-9364 Fax: (828) 350-9368 t dubia Date; May 23, 2014 i Pipe#: 001 County. Wilson Laboratory Performing Test: Environmelt tin s no, Comments: Signature of Operator in Responsible Charge Signature of Laboratory Supervisor: Pro ecf 9804 Samples: 140507.11 1401w 13 Mail Original To: North Carma Department of vironment and Natural Resources DWQ/ Envi me ces Branch 1621 Mail Service Center Standele: End date Start time: End lime: Raleigh,NC 27699-1621 os.or-w os-I4da 16oz 0636 J Sample Information Collection start date: Grab: Composite duration: Alkalinity (mg/L CaCO,) Hardness (mr/L CaCO,): Conductivity(µmhos/an): Tool residual chlorine (mgfL): Sample Temp. at Receipt(°C): �� ";E Test Information Treami Initial pH Out: Final pH (SU): Initial DO (mg(L): Final DO (mg/1.). Initial Temp. (°C): Final Temp. CQ: Organism Number 1 7 7 d [ 6 9 R 9 10 11 12 W. sun aen..11 R.M..ta Son Rnewell a�+.�3 90% 90% 90% Control Controlr24 7.68 7.57 775 777 7.69 7.60 7.77 7.65 7.52 7.69 8.1 8,2 7.9 7.8 7.9 8.0 So 8.1 8o 9.0 25.0 25.1 25.1 24.8 24.9 25.2 24.8 25.0 24.9 2/.9 __.... _. _. e_..._-.._ Number of YoungProduced 32 33 29 31 30 28 29 29 31 29 31 30 30.2 Adult Survival: (Live, (D)ead L L L L L L L L L L L L Effluent Percentage 9oz < < a a o 1n 11 17 Number of Young Produced 130129132129134311281291301301281311 29.8 Adult Survival: L)ive, Dead I L I L I L I L I L I L I L I L I L L I L.1 1 1 1.4 I - - Effluent Effluent Percentage= Treatment 3 Organisms 1 '2 d 4 J o r o > ro Number ofYow Produced Adults mi al� (L)i a (D)ead Effluent Percentage Treatment 4 Organisms 1 2 3 4 5 6 7 8 9 10 11 12 tom, Number ofYoun Produced Adult Survival: (L)ive, (D)ead %Retwion Effluent Percentage' I Treatment 5 Organisms 1 2 3 4 5 6 7 8 9 10 11 12 Nan Number of Young Produced Adult Survival L)ive, Dead xaw,<roa Effluent Percentage= n < F 7 R 9 10 11 12 aa.� Treatment o Organism, - - NumberofYow Produced Adult Survival: Live, Dkad xRmw Overall Analysis: Result: PASS LOEC: >90% NOEC: 90% ChV: >90% nwf) r .m 4 r_? (R/91) Rev. 11195 Chronic Test Results Final Control Mortality (%y 0.0 % Cannot with 3rd Broads: too Control Reproduction CV: 4.9 48 How Mortality Control: 0 °f 12 IWC: 0 lot 12 Si ificant7: No Final Mortality Significant at: No concrntration Reproduction Analyses Reproduction LOEC'. >90% Rt,roduetion NOEC: 90 Overall Method Homamdasict Normal Distribution: yes Method: shapkrc mwz Statistic: 0.967 Critical Value: 0.884 Equal Variances: yes Method: F-Test Statistic 1.456 Critical Value: 5.320 Non -Parametric Analysis (if applicable) Method: Emunnl% Rank Sum Critical Sum 90% a E�!; Asheville, NC 23302 R Phone: (823) 350-9364 (828) 350.9363 a� ` Envlronmemal Testln9solutions, Inc Date: August22, 2014 Effluent Aquatic Toxicity Report Form - Phasc 11 Chronic Ceriodaphnia dubia ---� Wilson W WTP NPDE 4: N-0023906 Pipe 1: 001 County: Wilson Facility: Laboratory Performing Test Environ ntal Testin ns, I C. Comments: Signature of Operator in Responsible Chu pmlCec 10023 signature of Laboratory Supervisor: Samples: 140806.13,140808.12 Mail Original To: North Carolina Department of Environment and Natural Resources End �e DWQIEnvironmental Sciences Branch start date: Fnddata St"ttlnl` obit 1621 Mail Service Center 08-06-Id 08-13-1d 1335 Raleigh,NC 27699-1621 Sample information Sampler Sample2 Control Test Information a+^ "^°"I` ""`ni11 a.n aae..la a Collection start date: OBA4-Id OB-OG-Ia �� �� 70S Control Cuntml Cmvo Treaunene 7.16 Grab: Initial pH (Sin: 7.62 1.71 7.68 1.70 7.64 245-h 255h r .: 7.38 Composite davation: 1.75 7.72 7 56 1.60 7.28 Alkali CaCO3) j 31. 35 Final pH MY: B.0 i.9 17 Hard,niry(nng lL Initial DO (mgd); 8.1 8.0 7.9 - 39, 38 1.1 Hardness (mrjL CaCOJ: -'8.2 19 7,g 8.1 8.0 Conductivity (Pmllaskm): 408 T a69 111.156.159 Final DO (mp/L): NO 10 4 10 Initial Temp. (`C): 25.0 25.0 25.1 24.9 25.1 24.9 Total sample Temp. at Recept cc): Final Temp. CC): 25.2 25.1 24.9 T5.1 25.1 25.2 Sample Temp. at Receipt (°Q: 0.9 0.1 - Control Effluent Percentage 90 Effluent Percentage= Treatment 3 Organisms Effluent Percentage= Treatment 4 Organisms Effluent Percentage= Treatment 5 Organisms _ Plumhrr, of Young Produced Effluent Percentage= Organism Number 1 2 3 4 5 6 7 8 9 10 Il 12 30.4 2 3 4 5 6 7 8 1 2 3 4 5 6 7 8 9 10 11 12 rMan 3� 2 3 4 5 6 7 2 3 4 5 6 7 1 l0 11 12 -FT= 9 10 It 12 �T= o In 11 12 Overall Analysis: 9o°/a ChV: Result: PASS LOEC: >90°/a NOEC: >90% r .A,h.1'il NC 3881)S Phone t328) 330.9364 A Fax. (8_8)350-9368 as FnvnontsmntM T¢sshss�SuWrrons, Inc CeriollapJrafa dubia Uma: November 17, 20I4 --r1 Efi]neaS Aquatic Toxicity Report Form -Phase it Chronic NPDES H: C- 0023906 Pipe N: 001 County -Wilson Facility: WilsonWW-fP -.l _ Comments: Laboratory Performing Test: Environmental Tesun olu' Signature of Operator in Responsible charge:"-'si. 10237 Pruizct Signature of Laboratory Supervisor Smspls; 141105.19, I411u7.17 r Mail Original To: North Carolina Department of Environment and Natural Resources date'. DWQ1 Environmental Sciences Branch stag dam. b'd date, start tune: End 1621 Mail Service Center n-0s-I4 n-a-Id 632 0828 Raleigh,NC 27699.1621 el sampk2 Coatret Sample Information Sam d -, Test Information sat vast p�nrl Cadm1 Collection scan date: II-03-14 11-0514 9p% �% gpg Cannot Como' cy _ Treatmane Grab: g _' Initial H (SU): 7.71 7,71 >�s- P 7 92 737 7.62 7.36 7.45 7.40 24 25-h 24 5 h Composim duration: 7.82 7.98 Final PH 7.95 7.43 19 7.8 42, 38 Initial W (mr/LY 7.8 7.8 Alkalinity(mg/L CaCOO: 42,38 (tag 7.8 7.9 7.9 Hardnesa(m8n-C8COt): Final DO lmBn-I: 7.8 7.9 80 7.9 7.9 25.0 5-7 iss. ise.in Conducdv(ry (ptnhosktn): initial Temp- (°C): 25.0 25.0 25.0 25.0 24.9 24.9 <0.10 <0.1a Total residual chlonne (MgM: Finil Temp. (°C): 25.2 25.1 24.9 24.9 25.1 Sample Tanp. at Receipt CC): 0.9 I4 - Organism Number 1 2 3 4 5 6 7 8 9 10 11 12 taus u an 711 28 1 29 31 29 27 28 29 27 28 28.8 Effluent Percentage Gov. I 2 3 4 5 6 7 8 9 10 Effluent Percentage= Treatment 3 Orgasi5m5 Effluent Percentage= Effluent Percentage= Effluent Percentage= z 4 9 6 7 8 9 Overall Analysis: >90% NOEC: 90% ''ChV: >90 Result: PASS LOEC: _ e iti i.33i)i 'hone: l` 3i '50-9364 x =_ r l8 S) 350-9368 Environmental Testln9 Saloons, inc. Effluent Aquatic Toxicity Report Form - Phase 11 Chronic Ceriodaphnia daoia Daze: February 20. 2015 Facility: Wilson WWTP 1NPDE."v': C-0023906 Pipe#: 001 County: Wilson Laboratory Performing Test: Envirottm tiny olut Comments: Signature of Operator in Responsible Char- a 04311 Signature of Laboratory Superrisor. pmjecr , -t- twsn?n4.t5. 150206.14 Mail Original To: North Carolina Department of Environment and Natural Resources DWQ/ Environmental Sciences Branch Stan date' End dam Sun time, a 1621 Mail Service Center 07.04-15 o2-u-Is 1333 0835 l Raleigh, NC 27699.1621 Sample Information sample) I Sample 1 Control Test Information 'an, a'""'�' � Collection son date: 02.02.15 02-04-15 90% 90% 90% Control Conn, COan4 Groh: Treatment: Initial H 5 P (U): 758 7.53 7.78 7.75 7.75 7.90 2475-h Composite duration: 24-h - 34.34 Real PH(SU): 7.82 7.82 7.73 7.65 1.73 7.61 Alkalinity(mg/L C4C%Y 7.8 7.8 7.8 7.7 7.7 7.8 Hudness(my/L CaCOr): 4 x __ 40,40 . initial DO (mg4.): 7.6 7.6 7.7 Conduc&lry (pmhos/cm): 379 380 150. ua.156 Final DO (mg/L): 7.7 7.9 7.7 24.9 25.0 247 Initial Temp. CC): 152 24.9 25 0 Total raidual ch,odne (mp/i.Y <0.10 .0.10 Final Temp. CC): 2d.9 25.2 24.9 24.8 24.9 24.8 Sample Temp. a Receipt CC) 0.7 1.3 Organism Nomber 1 2 3 4 5 6 7_ 8 9 10 11 12 31.0 Effluent Percentage 90% Treatment 2 0 anisms 1 2 3 4 5 6 7 8 9 10 I l 12 mace Number of YourProduced 36 32 37 32 38 35 33 36 37 35 30 32 34.4 iAdult Survival: (L)ive, (D)ead I L I L i L I L I L I L I L 1 1. 1 L I L I L I L xa� Effluent Percentage= Treatment 3 Organisms 1 2 3 4 5 6 7 8 9 10 11 12 may Effluent Percentage= Effluent Percentage= Treatment 5 Organisms 1 (Number of Young Produced Effluent Percentage= Treatment 6 Oreanisms I 4 5 6 7 8 9 10 11 12 ma %0.a6e 4 5 6 7 8 9 10 It 12 m.., 3 4 5 6_ 7 8 9 10 Il Overall Analysis: Result: PASS LOEC: >90% NOEC: 90% ChV: 17Wn form AT-3 (8191) Rev. 11195 >90% t0 P�-onO: (a 3; -OA364 � Fu.:: (878� 35U-9368 -Z� Ermimnmem ITIng5olutlans,1nc. Daze: iVlay 18, 2015 Effluent Aquatic Toxicity Report Form -1 ase 1I Chronic Cerfodaphnia dabsa --�" Facility: Wilson WWTP NPC S R: NC- 00^3906 Fipe l: 001 County: Win Laboratory Performing Test: Enviro a I Testin Sol I . ` Conunents. i' t7'7 Signature of Operator in Responsible Charg . prolece 10624 Signature of Laboratory Supervisor. Samplos: 150506.13. 150503 17 Mail Original To: No Carolina Department n,ir, mcnt and Natural Resources D1YQ) ences Branch 1623MailServiceCenter Son date: Enddan: Surttime. Enddmo: 05-06-15 OS-I3-Ii 1450 08d0 Raleigh, NC 27699-1623 Sample information I Simple simple control aeenbl aenr.tl sun a.esl RBI Collation start dam: 05.04-15 05-o" Test Information s �� 90N. Control Co Coma Trtmslene 717 7.21 Grab: 24-h 24.21•h Initial PH (SU): 7.34 743 1.76 7.32 Composite duration: 7 73 7,43 7.34 7.25 7.19 7.12 Alkalinity(mp(L CICOs): 32, 3I, 30 Final pH (SU): a2.44, 40 initial DO (mg/L): 8.0 8.2 82 7.9 7.9 8.0 Hardnest(mgIL CaCOs): 79 1.9 8.0 Condactivo(pedhos/cm): 403 400 Is0.lKtsr Final DO(m9fL): B.0 8.3 al e0.10 4.10 Initial TempM: 23.0 241 24.8 2a.7 25.0 25.0 Total residual ahlonne (mFJL): Final Tempi (`C): 25.2 25.1 25.2 250 25.1 II.i Sample Temp. at Recoil[ (°C): 2.3 1.1 Organism Number Control Organisms 1 2 3 4 5 6 7 8 9 10 11 12 rxm Number of Young Produced 29 26 29 26 28 29 28 �Ln Adult Survival (L)lve Dad L L L L L L L Effluent Percentage i 1 2 3 4 5 6 7 8 9 10 11 12 Id Effluent Percentage Treatment 3 Organisms 1 2 3 4 5 6 7 8 9 10 I1 12 w. Effluent Percentage= Treatment 4 Organisms Effluent Percentage) Treatment 5 Organisms Nnmher of Youna Produced Effluent Percentage= 2 3 4 5 6 7 1 2 3 4 5 6 7 1 2 3 4 567 Overall Analysis: >90% Result: PASS LOEC: >90% NOEC: 90/ ChV: Ashevi(Ie,NC 23302 > Phone: (828) 350.9364 ass x±tt fr-y= _, Fax: (SZS) 350-9368 Environmental Testing S°lutlons, Inc Effluent Aquatic Toxicity Report Form - Phase Il Chronic Cerli�aphnfa duhia Date: August2l, 2015 Facility: Wilson WWTP NPDE-Oo239o1i Pipe 4: DOI County: Wilson Laboratory Performing Test: Enviro to s C. onvnents: Signal= of Operator in Responsible ge: Signature of Laboratory Su or. Ptni«r 10821 SaoPla: 150805.19, 150807.1H Mail Original To: Carolina Departm Environment and Natural Resources DW ciences Branch 1623 Mail Service Center Stded dte: Stan tmEt ene o-0s-Is -2.15 0920 Raleigh,NC 27699-1623 E Sample Information Semple) Collection am data: 08.03.15 Gab: Composite duration: 2415-h Alkalinity (mg/L CaCO,): Ez,� - , Hudness(mg/L CaCOO: r' _ Conducdvity(pmhoa/cm): 579 Taal moduel chlorine (mg/L): No 10 Sample Temp. m Receipt (°C): La Organism t o m d Control Test Information +-, Treatment: Initial pH (SU): 32, 34, 33 Final pH (SU): 36.36,38 lninal DO(mg/L): i,s. in, 133 Final DO (mgfl: - initial Tamp. CC): Final Temp. (°C): 7 8 9 10 It 12 Sample 1 08-05.15 '-425-h _ 547 Q.10 0.9 Number t 6 l-VI441 V4 V4�a44V,,,a Number ofYoun Produced 33 33 29 30 29 29 30 29 33 32 30 32 30.8 Adult Survival: (L)ive, Dkad I L I L I L I L.1 L I L IL L L L L L Effluent Percentage 90/ c c 7 a n In 11 12 I ree[menac yr antanu Number ofYoun Produced 4 135 - 1 33 - 1 33 1 34 - 30 - 1 34 34 33 31 31 36 34 33.2 Adult Survival: L)ive, Dead I L I L ILI L I L I L L L I L L L L a -7 9 Effluent Percentage c � a o in 11 17 Treatment 3 Organisms 1 z j - - lNurnberol'Young Produced Adult Survival: (L)ive, Dkad +vase I ... t Perrenta¢el Treatment Or anisms I 2 3 4 5 6 7 8 9 10 11 12 Number of YoungProduced Adult Survival: (L)ive, (D)ead I I I I - Effluent Percentage= Treatment 5 Or anisms I 2 3 4 5 6 7 8 9 10 11 12 si— N ,mher of Youne Produced rrn,,.nt Prrrrneaoel I Overall Analysis: >9o°/a Result: PASS LOEC: >90% NOEC: 90 /° ChV: DWQform AT-3 (8/91) Rev. 11195 EffluentTusiciti Report Form-F''hr^nic Fathead Tasz F'cilhy: lAlilson - �NIPCE3.4 Pipet CC! oratory: Mentech,1¢c. !`T_ % Comment x County: Wilson MAIL ORIGINAL TO: Water Sciences Section 4 r > .Aquatic Tonicology Branch Division of Water Resources 1623 Mail Service Center Raleigh, NC 27699-1623 Test Initiation Date/Time 11/17/2015 4:27 PM %. Eff. Rapt 1 2 3 4 Avg WI/Surv. Ccntr0l 0.747 7-1 Control Surviving # Original # WUoriginal (mg) 10 101 10 1 10 10 10 10 0.731 0.765 017010 0.752 F-45--j Surviving # Original # WUoriginal (mg) 67.5 Surviving # Original# WUodginal (mg) 8 10 10 9 10 10 10 10 0.693 0.826 0.667 10.841 10 10 10 10 10 10 10 10 0.809 0.823 0.659 1 0.794 ® Surviving # Original # WUoriginal (mg) 95 Surviving # Original # WUoriginal (mg) F1-0-0-1 Surviving # Original # WUoriginal (mg) ater Quality Data Control pH (SU) InlUFin DO (mglL) InitiFin Temp (C) InillFm High Concentration pH (SU) IniUFin DO (mglL) Init/Fin Temp (C) InitiFin 10 110 10 10 0 10 10 10 0.925 1 0.141 1 0.926 0.745 10 10 10 10 10 10 10 10 % Survival 100.0 Avg IPA (mg) 0.747 % Survival 92.5 Avg Wt(mg) 0.757 % Survival 100.0 Avg Wt 09) 0. 771 % Survival 100.0 Avg WR (mg) 0.834 % SurvivalF 100.0 Test Organisms i Cultured In -House Outside Supplier Hatch Date: 11/16115 Hatch Time: 3:00 pm CT 0.788 0.813 0.862 10 10 0.823 10 10 0.984 Day Avg Vvt (mg) 0.822 % Survival 100.0 Avg WA (rng) 0.820 10 10 10 10 0.914 0.653 0 8.02 1 7.86 1 8.05 17.68 2 8.02 17.86 3 8.07 1 7.99 d 5 6 8.39 18.23 1 ! 8.13 7�.76 1 7.99 Sample Collection Start Date Grab Composite (Duration) Hardness (mg1L) Alkalinity (mglL) Conductivity (umhoslcm) Chlorine(mglL) Temp at Receipt (°C) 2 3 Survival Normal i( Horn. Var. ri. NOEL IN LOEC >100 ChV .100 Method Steel's Conc. Dilution H2O Batch # 948 949 950 P 45 Hardness (mglL) 48 44 42 [fl 67.5Alkalinity (mglL) 57 55 82 90Conductivity (umhoslcm) 218 202 239 95 1 00 Irk Growth ri ri 100 >100 >100 Dunnett's Calculated Cnucal 14 2.41 18 2.41 18 2.a1 18 2.41 Overall Result ChV >t00 Calculated -0.1496 -0.3722 4 3391 -1.1434 -1.1127 affluent ToXi Cit7 XspC_t ?J= - Work Order: on-4- =ass;`Fail and Acu=a LC50 Data: 11/30;15 NFDEs;#: MC0023906 Pipe#: 001 Councy: WT-LSON LABS, INC. Comore_^ts: MAIL ORIGINAL TO: North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test e PASSED: -7.53% Reduction�� 1NVater Sciences Section -Aquatic Toxicology Branch Division of Water Resources 1623 Mail Service Center 621 Ra eieh.N. 23 hron 9c Test Results Calculated t = -1.729 Tabular t = 2.624 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 SO 11 12 % Reduction = -7.53 % Mortality Avg.Reprod. # Young Produced - 18 27 22 19 24 22 25 28 27 28 26 26 0.00 24.33 Control Control Adult Wive (D)ead L L L L L L L L L L L L 0.00 26.17 Treatment 2 Treatment 2 Effluent %: 90 TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 contrrool CV PASS FAIL # Young Produced 25 24 26 27 26 28 26 26 26 28 24 28 % control orgs X producing 3rd brood ICheck One Adult (L)ive (D)ead L L L L L L L L L L L L 10096 1st sample 1st sample 2nd sample Complete This For Either Test pH Test Start Date: 11/18/15 Control 7.94 7.98 8.00 7.90 7.96 7.88 Collection 1: II/L6/15 Date Sample 2: 11/18/15 end Treatment 2 7.56 8.01 7.76 8.03 7.80 7.95 Sample Type/Duration 1st P/F s s s Grab Comp. Duration D S S t e t e t e a n a n a n Sample 1 X 24.4 hrs U M M r d r d r d g 23.7 hrs T P P t t t Sample 2 1st sample 1st sample 2nd sample Rardness(mg/1) 42 '••••• D.O. Control 8.19 8.14 8.07 8.42 8.26 8.06 Spec. Cond.(pmhos) 160 400 421 Treatment 2 8.51 8.15 8.54 8.49 8.42 8.19 Chlorine(mg/1) <0.1 <0.1 LC50/Acute Toxicity Test Sample temp. at receipt(°C) 0.6 0.3 (Mortality expressed as %, combining replicates) Note: Please Concentration Complete This Section Also Mortality start/end start/end EE on Control it High Conc. pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs): _ Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) Ashevdle.NC 23302 to F-- uq Phone: (3.8) 350-9364 J Fax: (828) 350-9368 �- Environmental Testing SON[lons, Inc. Effluent Aquatic Toxicity Report Form - Phase 11 Chronic Cerio pl pia dubia Date: February 22, 2016 Facility: Wilson W11'"1-P PI7ES'k"P4 02C«D,,, S906 Pipe Al: 001 County: ilson Laboratory Performing Test: Envimr Sienatlne of Operator in Responsible Signature of Laboratory Supervis Mail Original To: North tarolina Department of DWQ1'finvirommental Scienc 1621 Mai Raleigh,NC 27699-1623 Sample Information Collection start date. Grab: Composite durtiom: Alkalinity (mg/ CKC)i): Hardness (mg1L CaCO,): Conductivity (pmbos/rn1): Total residual chlorine (mgL): Sample Temp. m Receipt (°C): Comments: and Natural Resources Stan date: EM date Stan fire: End itme: 02-03-16 0_-10-16 1309 0717 sample 1 I Sample 2 = 38a M 1" Organism Number Test Information Treatment: Initial pH (SU): Final pH (SUI: Initial DO (mill): Final DO(mgl): Initial Temp. l"C): Final Temp. MY !ontrol Organisms 1 2 3 4 5 6 7 8 9 lu 11 IL M. lumber of YoungProduced 31 31 32 31 29 29 29 32 32 30 33 30.6 Ault Survival, (L)i a (D)ead L L L L L L L L L L L L L Effluent Percentage 90x Effluent Percentage= Treatment 3 Organisms Ftl)nent Percentaecl I 2 3 4 5 6 7 8 9 10 Il 12 *n. 1 2 3 4 5 6 7 8 9 10 11 12 arm Effluent Percentage Or anisms I 2 3 4 6 7 S 9 10 11 12 Treatment S nwn w�mher of Young Produced Ffflnent Percentage) I pverall Analysis: >90°/ NOEC: 90 / Chv: >90% Result: PASS LOEC: DN•'0 form AT-3 W91) Re'. 11195 y s) Environmental Teating5olutlona•Inc. Effluent Aquatic Toxicity Report Form - Phase II Chronic Cerio phnia dubia Facility: Wilson WWTP Y NC- 023906 _ Laboratory Perfonning Test: Enviro +n ntar uns nc. Comments: _ Signature of Operator in Responsible C - Signature of Laboratory Supervi pm)era: u435 .Asheville. NC 25802 Phone: (828)350-9364 Fax: (828)350-9368 2016 Mail Original To: North lina DepartmentoKnvironment and Natural Resources DWQ/ Enviro ciences Branch 1621 Mail Service Center Start data. Emi dal: Stan tune: End tine' Raleigh, NC 27699.1621 os-04-16 05-1 I.16 1222 0755 Sample Information Collection Stan date: Grab'. Composite duration Alkalinity (mg4. CaCO,): Hardness (mill, CaCOS): Cooductiviry (µmhos/c n): Toil residual chlorine (mg/L): Smnple Temp. u Receipt (°C): Sample I I Sample 2 1 Control 05-02-16 0544-16 24.25-h 26 5 h r •-+Teti, 32 ao 425 397 15L mu. in? 4.10 4010 0.5 06 Test Information Treatment: Initial pH (SU): Final pH (SU): Initial DO (mg/L): Final DO (mg/L): initial Temp. ('C): Final Temp. (°C): Organism Number < L v R Q In 11 12 Me. l:ontrot vrganisms NumberofYoun Produced 32 - 28 32 27 - 26 - 30 26 24 30 26 27 29 28.1 Adult Survival: Wive, Dead L L L L L L L L L L L L Pin neat Percentage 90Z Treatment 2 Organisms 1 2 3 4 5 6 7 8 9 10 It 12 My Number of Young Produced 32 28 30 31 29 30 31 27 28 28 29 29 29.3 Adult Survival: (L)ive, (D)ead L L L L L L 1. L L L L L -4.5 x amvewn Effluent Percentages Treatment 3 Organisms 1 2 3 4 5 6 7 8 9 l0 11 12 Mu Effluent Percentages Treatment 4 Organisms 1 Numberof Youn Produced Adult Survival: Wive, (D)ead Effluent Percentages Treatment S Organisms I Number of Young Produced Effluent Percentages Treatment 6 Organisms 4 5 6 7 8 9 10 1 2 3 4 5 6 7 8 9 10 11 12 2 3 4 5 6 7 8 9 10 11 Overall Analysis: a 90% ChV: >90% Result: PASS LOEC: >90 /a NOEC: OWO form AT-3 (R/91) Rn•. f 1i95 Mam s m i M 'as s > LI y I y Environmental Testing Solutians.inc. Effluent Aquatic Toxicity Report Form - Chronic FathepO'Ain Facility: Wilson Laboratory Performing Test: Envir Signature of Operator in Responsibl Signature of Laboratory Supmisor. Mail Original To: North Caroii DWQI Envv 1621 Mail S, Raleigh, NC Control Organisms % EMuent 46 Center 1 and Natural Resources Replicate number 3 a Survivi¢ numblarvx er ofmb. 10 10 10 10 Ori inu nuof larva I0 1 10 1 10 I 10 wei Vori nal (ma4arvx) 0.689 I 0.627 I 0.707 I0.662 Survivin number oflarvx IIO LO 10 10 i Ori Ind number aflarvx I 10 10 10 10 wei hVori inal (m arvaz)I 0.588 1 0580 0.642 V.666 PO Box 7i65 A.ihevine.NC 23802 Phone: (US)3=0-9364 Fax: (823)350-9363 E-mail, Jlm@aetsnclab.com Date: Auaust26.2016 tration Test Pipek: 001 County: Wilson Start due: Fnddue: Start time: EN time: 0g-09-16 OB-16-Ib III-<7 I103 Test Organisms Sumvd(%) 100.0 oasida tut, li. Avenge wt (mg) 0.671 ti-house C.I. Av. xgem) 0.671 Start parch: Oe-08-16 Ibld sun•iving (mg) End parch: O34946 0630 Survivd(%) 100.0 Average w (mg) 0.616 %Effluent Survw numb. o((arvxI 10 10 10 10 6T5% odgwlnumbvoflarvx 10 IO IO 10 Survive(%) 100.0 0.643 Wei heori mal(m arvae) 0.701 0.640 0.611 0.621 Averagc w(ng) % Effluent 9a % burvivin numb. o(larvu IO 10 1 10 1 10 longing numb. of larva 10 10 10 I 10 wei Vori inal(m;(larvaz) 0.658 0.623 0.634 0.638 %Effluent Survivin numb. aflarvae 10 10 IO 10 96 % Ori final numb. oClarvae 10 IID 10 10 wei hVongind (-¢!larvae) I 0.718 10.665 0.637 0.727 %Effluent Survivin¢number otlarvaz l0 10 9 l0 100% 0' iml numb. oflarvx 10 10 10 10 Wei hdori fine (mgnarvu) 0.670 0.687 0.684 O.Si7 Water Quality Data Coutr PH (: DO( Tcm Nigh PH( DO Tem Sample Ini Collectiot Grab: Compos l Analin,p Hardness Conducti Total res Sample! Survlvd(%) 100.0 Avenge vrt(mg) 0.638 Survival(%)F 'Woo Avenge vn(mg) 0.681 5wivd (%) 97 TI Avenge wgmg) 0.625 Overall Analysis: --- Result: PASS LOEC: >100% NOEC: 100% ChV: >100% lile- NC ? -8 302 Phone: t828)350-9364 FaN: (828) 350-9368 Envimrun*ntai T—Im so'ut'ons'Mc. Coriodajohnitt labia [)a,,: August 29, 2016 Effluent Aquatic Toxicity Report Form - Phase 11 Chronic C. 0o23906 pipe 9: 001 County: Wilson Facility: WilsonwwTP Comments: Laboratory Performing Test: --------------- -, , 'I Signature of Operator in Responsible Cha-rRct!--- 11704 Signature of Laboratory SuPervisaw, 16D810.14 . . . . . . . . . . Nlail original To: North& milina Depart, , d Enviroment and Natural Resources Sc, C sciences Branch Stan dale: start time: End MO. 1621 Mail Service Center OS-10-16 EEE jEnd](dWe: 0 1 7-16 08-17'� 1249 0800 Raleigh, NC 27699-1621 Sample laformation s.,*i Sample2 Control Test information S. .—a I 9.e" ARAZI6 03-10-16 C,Ilecfiw sta" date. 90% 90% muol r...i Conn] Tmarcmt: Grab: Initial PH (su): 7.80 7.75 7.60 769 772 C�mpogje duration. 24.5-h Fine PH (SU) 7.98 T93 7.54 7.62 7M 31.35 Alk,14HUY (11191L CaCol� 40 juiu.1 Do j,�#!L): 9.0 MR 8.0 7.8 7.9 7A 4, Hardnen Ma/L CaCO3): Final Do ouz"L) 9.0 8.1 7.9 7.9 9.0 ...... 5 Conducti"Y 523 Immil Temp (T) 149 24.9 24.8 24.8 24.7 24.3 T,111 midud chlorine ('911-1: <oAo <0.10 Fuel Temp. ('Q7- Sample Temp. at Receipt (*Q: 0.6 2.0 Organism Number — - - - - Chronic — - — — - Test Results g 9 10 11 12 m- 2 3 4 5 6 7 . �-_-4177777.77 'oo 27.7 Effluent Percentage EEI Treatment 2 O"ARiSMS 1 7 3 4 5 6 Effluent Percentage 1 1 3 4 5 6 7 a 9 to 11 12 Treatment 3 Organisms Effluent Percentage= 6 7 it 9 10 It 12 . - . - , 1 3 4 - Effluent Percentage 4 5 6 '7 9 9 10 11 11 5 Organisms ol'mtnl Number or Produced Adult 4 1 Adult Sun? al (L)ive. (1))e3d I I I I Effluent Percentage= 4 5 6 7 S 9 10 [1 12 -treatment 6 Organisms - Number of fount Produced Adult SurviVal; (L)im tend Overall Analysis: 90% NOEC: 90% ChV: >90% Result: PASS LOFC: 111195 \shet 'Ic NC SaL_ z1 I'houc; 11i°3} ; 5il `93u4 (82g) 3so-9368 �A 'L ' Environmental Teslmg 5olu[lana.Inc Dafc: November Effluent Aquatic Toxicity Report form - Phase 11 Chronic Ceriuduphuia dnhin , 1 1'tmn .l,• Nilson Facility: Wilson WlComments: Y'1T ,�pIN S UOv9U6 pip,: nU' i Laboratory Performing Test: Enviromiieo ul 7zstin Sul onr•,' Signature of Operator in Responsible Char ,, n s96 Signature of Laboratory Supe 'iso nai�y..a� Smap es: 161102.t9, 161104.16 Mail Original To: No Carolina Department or Gllvir0dlm pWQ nvironnic Sciences nr ch 1621 Mal arsic ' Raleigh, NC 27699-1621 Sample Information MR. Comp Collection Stan date Grab: Compo4tedaation: '_. 30,Aleatlnity (meJL CaCO;):2.4{Hardness (InF%L CaCOIr "L l'iConductivity (µlnWsoon): l'onl residwl ddorine 0nr/L): Sample Temp, at aeceipt ('C): 04 0.9 and Natural Resources Fiul due: clan lime. End tune: 5tul due: 1316 07R 11-02-16 I I-09•Ib Test Information s.' 90./. 90x 90°/. Cpnnal Cwaol Coln 7.44 7.65 1.33 7.44 757 InitlalpH(SUF 1,53 765 734 741 734 Final PH 15U1: 7.64 734 8.1 a.0 Ltilid DO UnP/U: 19 7.9 79 79 so Final D06nr/Lk 8.0 80 8.1 19 T7 N,t Initial Temp. (.C)_ 25 0 24.9 bF.B 24,8 -49 149 241 Final TrnlP. ("C): 24.7 35.0 25.1 20 0,plasin Ntmlber 1 Organisms 1 2 3 4 5 6 7 8 9 10 ll 12 hi— t ,a 77 :U 0 31 3U 26 26 29 27 30 28.Z Effluent Percentage Sox 7 4 5 7 Effluent Percentagee 4 5 6 7 8 9 10 11 12 at"' Treatment 3 Organisn 1 2 Effluent Percentage= _ < 7 g 9 10 11 1-2— Effluent Percentage 6 7 8 9 10 I I 12 nloa Treatment 50rganivns 1 2 3 4 5 nhlmher Of Yoanl; Produced Effluent Percentage= q 5 6 7 8 9 10 Treatment 6 Oreanisms l 2 Overall Analysis: >go% NOEC: 9o% ChV: >90% Result: PASS LOEC: � <.:� a >"'1 ':`. :e he•.'.I SIC ooti2 Phone: ; a- ly Fu::: 18231 »p 9.u8 Fnvlronanamal Tesrin95olunons, :nc Date: Febntarp'_1.2017 Effluent Aquatic Toxicity Report Form - Phase 11 Chronic CeriodaPhIlin ;IuBiu -"^-NRR1 S #: NC- 0023906 Pipe #: 001 Counn: Wilson 7'V NWTP - p rming TestEnvironmental Testing SOlutior�•Inc. Comments:rator in Responsible Charge:oratory' Supervisor. F--i .G samdex 170209.'-5.170210.224 Mail Original To: North Caro kina-Deperatie of Environment and Natural Resources DWQi Environmental Sciences Branch start date End daze. gran time: End tune 1621 Mail Service Center 02-08-17 0?-15-17 1341 a75g Raleigh, NC 27699.1621 ! Cuntnn Sample Information 7 Test Information Control Cpnm1 Caere Collecaon start Lau:: 90:b 90% 90% Treatment; 751 7 50 Grob: h Initial Pit 7yt 1.78 756 7.Id 736 77i 7.48 7.b3Alkalinity(myL Composite duranon.1 32. 30.31 M SM: 767 761 Final pll (SL): 80 7.9 CaCO,r d0, 40.40 Initial 00 lmg/L): S.o 80 7.7 8.0Hardness 79 (merL CaCOt); Final DO On;"LY.80 7.8 79 8.08DConductivity Inc. us. l5a Ipmhos'cml: Initial Temp. f°C): 2d.9 2 18 2;.9.0 Total residual chlorine lm�21: Final Tanp. t°CI: 25.0 2;9 2i1 23.0 '_5.1 2if Sample Temp. at Receipt CC): 0.6 0.5 Organism Number Chronic Test Results d 5 6 7 8 9 10 l l 12 stm ... _, _.,.,_,. a o Control Effluent Percentage 90% Effluent Percentage= Treatment 3 Organisms Effluent Percentage= Effluent Percentagca Treatment 5 Organisms (Number of Young Produced Effluent Percentage= 3 4 5 6 7 8 9 10 ll 12 am Overall Analysis: >90% NOEC: 90% ChV: >90% ReSdt: PASS LOEC: .. _m nuM intin9 ioiwwnxlnc Chronic Whole Effluent Tovcity Test (EPA-321-R-02-013 Method 1000.0) Species: Pintephales promelas Client: Wilson WWTP County: Wilson NPDES #: NCO023906 Outfall #: 001 Project#: %-LADb 1WC: 90% Daily feeding and renewal fnjorntatron: Day Date Morning feedin; Time Ann 0 Oi-16-17 Nos 1 05-17-17 Ot.10 1 2 0i-1s-17 0605 3 Oi-19-17 (j'10D 4 05-20-17 00 5 05-21-17 tT•l0% 6 05-22-17 ObSS 7 05-23-17 Afternoon feeding 11.10 VINQ initiation, ew renal, Simple I SSW n. r.rmination number used batch used 1 -105Zo. od oyit• 0 SOP AT20 — Exhibit AT20.3, revision I 1-01-14 - - - Fax: 1323) 350-9363 �'- :nrtronmenrat iezn,g ioltrzlons. !nc Gate: Mav 3 1. 2017 Effluent Aquatic Toxicity Report Form - Phase 11 Chronic Ceriodaphnia dubin Facility: Wilson Wl4'TP NPDLS 4;.4NC- 0033906 Pipes: 001 Coum : lti llsmr -+''-( Comments: Laboratori Performing Test Environmental Testins Solutt9nsi ne./' Signature of Operator in Responsible Chaqer:__=z.a.. Pro,, 124I4 $Igtta[ureof Ldb9[3[ory Supervisor:. i,mmles: 170511.05.17051906 Mail Original To: North Carolim'D perm, I of Environment and Natural Resources DWQ/ Environmental Sciences Branch Stan date: Etddare: Stmnmc: End time 1621tV'[all$zrviceCenter 05.17-17 05-24-17 1130 0719 Raleigh. NC 27699.1621 Sample Information e2 Conirm a="">t' any= su" nunai a nd Collection start date: 11 Test information sm 90$ Cannot CanariaGrab: - Tnaimene 90.90°L 7.70 7T- 7.82Canpasne 772 7.86 779 dtwtion: r Initial pH ISUY. 7.81 13i 7.85 7.81 7.78 781 lmg'L CaCO,)'33. 31, 3iEinai ER Phi lSl; 1: 8.0 7.5 1.8Hardness 7.3 77 ,Alkalmiry 38.10.41 ung4. CaCO,I: Initial DO ling'LI: $'1 g0 g0 77 19 7.8 Condnuiviry (pnd7os'an)o 8 na. tax. enNutt DO tm_JLI: 79 24.9 2i0+J9 Total residual cblomre (mg'L): 10 Initial Tanp.(°C1: EinalTemp.l°Cl: 24.3 '_i.l 25.0 2J.9 i. -Sample _v9 Temp. n Receipt (°Ct Organism Nnmber 1 2 3 4 5 6 7 8 9 to 11 12 >� l,t 79 32 32 33 32 30 29 33 29 31 32 313 Effluent Percentage 9o'a Effluent Percentage= Treatment 3 Organism, 1 7 Effluent Percentage= Effluent Percentage= Effluent Percentage= 3 4 5 6 7 4 5 6 7 99 10 2 3 4 5 6 7 9 l 2 3 4 5 6 7 1 2 3 456 8 Overall Analysis: ° 90 /e Chv: >90"� Result: PASS LOEC: >90 / NOEC: -_ - �� Phone lu_h) 35(1.95(r1 , ) F c (323)330-9368 Envuon n.mai Tgsrin9 5glurlona, Inc. Effluent Aquatic Toxicity Report Form - Phase 11 Chronic Ceriodnphnia dn6iu Caw: Auausc 2'_. 2017_ Factiv: Wilson R'WTP NPDES m' NC. 0023906 Pipe 4: 001 Count,,: Wilson Laboratory Performing Test: Enviranmenia4.iestina-Salutiens� Inc: Comments: Signature of Operator in Responsible Cltargea. Signature of Laboratory Supmisor: f---V vr� Project: 12609 H Similar 170802.I7. Ro8U4.17 Mail Original To: North CarotinDepartm t of Environment and Natural Resources DWQi Environmental Sciences Branch 1621 Mail Service Center FSEandase. I Ent date: I Sanumc I Fnd titm Raleigh, NC 27699.1621 0s-02-L7 1 0S.0947 1 1949 1 0736 Sample Information Coll uimt start dare: Grab: Composite duration, Alkalinin• (mgL CaCO,): Hardness (mgrL CaCO,): Conducti vi ry (pndlos en l: Total residual chlorine ImgtLl: Sample Temp. at Reccip(M): Samplel Sample2 Control 07-31-17 0&02-17 24.75-11 24.5-11 33 38 516 566 taa ua. ca <Uo s0.10 0.9 1 0.3 -rest Information Treatment. Initial PH [Sul: Final pH (Sul: Initial DO Im_L): Final DO (me0s: Initial Temp. t°Cl: Final Temp. fCl: atn Arnex�l� nrnc.n_ son n:nn.i: 90% 90% 90% Control Control Camrol 7.71 7.74 7.85 7.35 7.53 755 792 7.93 7.91 7.61 7.66 7.63 3A 8.0 8.0 7.8 7.3 7.8 8.0 3.1 8.0 77 7.8 7.6 25.1 24.9 '_S.l 'J.7 24.8 ?5.0 24.9 25A 252 f'S.0 25.1 25.1 Organism Number Control Organisms I 2 3 4 5 6 7 8 9 10 It 12 asw Number of Younp Produced 123 29 32 29 29 31 28 25 30 27 127 28 286 Adult Survival: (L)ive. (D)ead L L L L L L L L L L L L Effluent PercentageEN--] T..vt......t 7 n.... 1...,v 1 ] I 1 i 6 7 R 9 10 11 17 ua Number of Young Produced 136 33139 1 35 1 37 137 137 135 132 136 34 37 35.6 Adult Survival: (L)ive.(D)ead I L L I L L LL I L I L I L I L I L I I i 1 1 -24.5 Effluent Percentage= 'reatment 3 Organisms t 2 3 4 5 6 7 8 9 Iu It 12 lumber of Young Produced Auk Survival: (L)ive (D)ead Effluent Percentage= Treatment 4 Organisms 1 2 3 4 5 6 7 8 9 10 11 12 st, Number of Young Produced Adult Survival: (L)ive,(D)ead Effluent Percentage= reatment5Organisms 1 2 3 4 5 6 7 8 9 10 11 12 as lumber of Young Produced dult Survival: (L)ive (D)ead -wvm. Effluent Percentage= •reatment 6Ot g an isms 1 2 3 4 5 6 7 8 9 10 It 12 smn lumber of Young Produced Wall: Survival: (L)ive (D)cad Overall Analysis: Result: PASS LOEC: >90% NOEC: 90% ChV: >90% DWQ form AT-3 (8191) Rev. 11195 Chronic Test Results Final Control Ndonaliry I%I: 0.0 %Control wins 3rd Bra too Conant Repmducrion CV: &6 48 Hour llanaliry Control: 0 or 12 IWC: 0 of 12 Sienificam".: No Final Monalire Significant ac No concennalton Reproduction Analyses Reproduction LOEC: >90T Reproduction NOEC: 90% Ovesatl Method: Homonc drnxt Normal Distribution Yns Method' shaplro-\till's Statistic 0.960 Critical Value: o.8s7 Egiwl Variances: Yes N9edtod: F-Tess Statistic' 1.054 Critical Value: 5.320 Non-Pammenic Analysis of applicable) Viclhod: Effluent°/ Rall:Sam Critical Stan 90% _. M• L oo .O.1i63 i Environmental Tasting Soluilons, Inc Effluent Aqua tic To-,' city Report Form -Phase II Chronic Ceriodaphill a dubld Cate: Novamber'_2.>UI NPDES' NCI0023906 Pipe 001 Counu: R'ilsun Facility: Wilson IV1Y"CY - , Cotnmenm Laboratory Performing Test: Lnvironment9 Tasting Solutions.-1uc_.. -.i✓ Signature of Operator in Responsible Champ: `?-�' PmJeer I'_Sil Signature of Laboratory Supervisor. /r Svnides; I'.I lO3.18. 171110.16 [ail Original To: North Carolina Department of Environment and Natural Resources DWQ/ Environmental Sciences Branch Swn dote: End dnrc. Swn time'. End Mitt e: 1621 flail Service Center 11-05-17 11"13.17 16ffi Raleigh. NC 27699.1621 Sample Information Collection start date' Grab: Cwnposite duration: Aukaliniry Ung4 CaCO,r. Hardness Img'L CaC0�1: ConductiWY i µlnhos%rnn: Total residual chlntbm ImeLl: S,,Plc Tainp. at R,ceipt IT I: Control Effluent Percentage 9oi Effluent Percentage= Treatment 3 Organisms Effluent Percentage= Effluent Percentage= Treatment 5 Organisms Number of Young Produced Adult Survival: (L)ive. (D)c Test information ,en- 'rmannait: 90% 90% 901,; Cannel Contra Initial pH ISU1: 7.91 1.74 S.DI 187 182 Final P14(SU: 7.90 8.04 791 768 7.6" Initial DO lmyL): 90 3.0 SO 73 7.9 Final Do (mgtL): 9.0 3.1 So 7,7 7.6 InitInitiall'mnp. 1"C 1: 2i2 r .i -a 2e.S 24.8 2a8r Final Temp. 1"Cl: 25.1 75.2 24.9 �n Organism Nmnber t 2 3 4 3 6 7 8 9 10 it 12 s ti I 79 113, 134 1 34 1 30 131 30 29 28 30 29 30.7 7 8 9 10 1 0 3 J 3 6 7 8 9 10 11 12 alu I 7 3 y 5 6 7 8 9 10 11 12 ua k+ n i 6 7 8 9 10 I1 12 Effluent Percentages Treatment 60r anisms I 2 3 4 5 6 7 8 9 10 11 l2 Number of Young Produced Adult Survival (L)ive, (D)cad Overall Analysis: >90% Result: PASS LOEC: >go NOEC: 90% ChV: 4 �>--�; -4 -`ram-t 1 i Environmental Tasting Solutions, Inc. Effluent Aquatic Toxicity Report Form - Chronic Fath Facility: Wilson WNVT? _... NPDFi. Laboratory Performing Test: Envir Signature of Operator in Responsibl S ignature of Laboratory Supervisor: ,Mail Original To: North Carolina CA..QPartmet DWQ/ Envimnmen-31SCi 1621 Mail Service Center Raleigh. NC 27699.1621 Control Organisms %Effluent 45% Effluent 675% %Effluent 90 Effluent 95 % Effluent 200/ Pi, Lr 756i Phone: (3" d o; le) 3 ne: 3 U 9364 Fax: (373)��0 9363 E-mail:limiiietenclab.com Date: February 21. ^_013 'Minnow hfulti-Concentration Test NC-0023906 Pipe#: 00t COILING Wilson 3 and Natural Resources Replicate number 2 3 4 $rvvrvin number of arvae 10 1 10 10 10 Ongiml camber a flarvu 1 10 1 10 1 t0 i I 10 wels:ha'oneual(melarvu) 1 0.801 1 0.790 1 0.312 0.304 S,"wing number of larvae 10 10 10 1 t0 Ori fret nwnberoflarvu t0 1 I 10 1 1 10 1 10 wei dori inal (ine2tarvae) 0.808 t 0.752 1 0.775 1 0.804 Sierm.na nsanber of lance 10 10 10 1 10 Oniial mamberoflarvu 1 10 10 10 1 10 Wei9bvori ual (,ro arvati 1 0.679 1 0.312 1 0.743 1 0.316 stnivin numbaaFlarvae 10 1 10 1 10 1 10 Oriinal number oflarvu 1 10 1 10 1 IO 1 10 weiWW0n imllm,tarnel 1 0.846 1 0.811 1 0.813 1 0.337 smvivina number oFiarvae 10 t0 10 10 Oninal munbcroflarvu 10 l0 t0 10 Weiahc'wi inai (mp/larvne) 10.687 0.745 0.811 0.723 $urvs•in mm�ber of larvae l0 10 10 10 Ori roil num6eroflarvu 10 10 l0 10 weiandari anal(mal.) 0.7?8 0.695 0.739 0.750 Water Quality Data Control PH (SU): DO (mg(L): Temp. ('Q: High Cancenl pH (SO) DO (sn®'L): Temp. (Q: Smc dare: End dam: Stan time Ed time: 82-0b18 02-li-IS 1145 ( to52 Tut Organisms surviwl (K) 100.0 Oms,de rap lieo Average m l MIX) 0.807 In-harae Chhue Average ml 1 0.807 sury ivin, (aid aegmhazch: 02-05-181545 End hatcht 02 0013 0 000 survival (%) 100.0 Avenge m(1ar) 1 0.785 swvival (%) 100.0 Average mbr40 0.763 Stwivil (%) 100.0 Maiepm(na) 0.326 Survival ( e) [Ell Asmyemba3) 1 0.743 smvivi Dsl 100.0 Aamgem(rg) 0.741 7.91 1 7.55 1 7.70 1 746 1 7.70 1 7.38 1 776 1 759 1 279 1 7.39 7.73 7.58 761 7.55 80 7.6 1 7.8 1 7.7 1 So 7.2 1 9.0 7.5 1 1.9 1 6.9 77 7.5 7.9 72 24.7 24.3 1 246 1 244 1 24.8 242 1 24,7 244 1 24.7 1 243 1 24.b 11242 247 242 r a7.20 7.51 1 765 1 7. 76 6 80 79 3.0 744 1 i7b 78d . 668 S90 L7 0 6.7 25.0 1 244 1 24.7 243 1 250 1 244 1 249 1 24.6 1 25.0 1 246 1 24.6_.l 24d 1 249 1 241 Sample Information Collection Stan daze: Grab: Composite dusalion: Alkalinity (mp'L CSCOs)' Hardness (mgtL CaCO]): Conductivity 4unhoslem). Toni residual chorine (m#L): Saznple Tnnp. at Receipt CC): Sam Is I Saznple 2 sun le 3 Conhol 02.04-I8 0746.19 02.08-1 2e-h 24-h 23.75-h - 30 34 4S 30-i3 36 36 36 38-d2 391 391 466 I W-1 S7 40.10 <0.10 40.10 I.5 0.7 Analyses Nouns Hom Vat NOEL LOEC Chv Method Overall Analysis: Result: PASS LOEC: >100% NOEC: 100% ChV: >100% DWO form AT-5 4103) Sswivai Grovrth Y45 Yes Yes Yes 10% t00% >I00% >I00% >100% >100% Visual lop. Dunncn's Sur;m] Growth Ye EOluetn Cdtid Calculazed Cdriul Calalued 45% 2410 0773 675 % 2410 1554 90% 'L410 .0.658 95% 2.410 2248 100% 2..- 2327 tile, NC q qr �`�� Phone (828l 350-9=04 ai Fax' (828) 350-9368 i. Envnonmenral Tesitng Solutions.Inc. Date: February 23. 2013 Effluent Aquatic Toxicity Report Form - Phase II Chronic Ceriodaphnia dubia Facility: Wilson MNNTP--��NPDESN: NC-0023906 Pipe 8: 001 County: Wilson Laboratory Performing Test: Emnvirontal Tea4t a Solutions`I Comments: signature of Operator in Responsible Charge: - rcoieu. Signature of Laboratory Supervisor. 1+ leo7077 Mail Original To: North Carolina Department of Envirom DWQ/ Environmental Sciences Branch 1621 Mail Service Center Raleigh NC 27699-I621 Sample Information Collection Stan date'. Grab: Composite duration'. .40:aliniry (mg'L CaCOO: Hardness (mg/L CACOO: COnduttiviry(µmhoycm): Total residual chlonne(mg/L): sample Tmnp. at Receipt CC): Control Effluent Percentag 907. Treatment 2 Organisms Number of Young Produced and Natural Resources Slav dare: Ulm Sran time. End twe 02.07-18 02.14.18 1423 0758 Test Information wa R�^v' a°'n'n` Treatment: 90% 90% 909 Comroi Control Cony Initial PH(su): 743 728 772 7,70 776 767 Final PH(SU): 772 777 7.91 770 772 7.16 Initial DO(mg9.l: 7.8 9.1 79 78 9.0 79 Final DO (mg/U: 78 7a 79 7.6 7.6 79 Initial Temp (`C): 348 24a 24.9 21.7 24.3 25 ( Final Temp. (`C): 25.2 25.0 24 7 24.8 248 2d.1 Organism Number I 2 3 4 5 6 7 a 9 10 11 12 — i0 29 27 32 31 29 32 32 31 2a 2a 29 29.8 3 4 5 6 7 a 9 10 11 12 rwA EfIluent Percentages ^ 4 R 7 a 9 10 11 12 nw� Effluent Percentages 10 11 12 . tits _-_._.... A n—knna 1 2 3 4 3 6 7 8 9 Effluent Percentages Treatment 5Or a ntnisms INnber of Young Produced Effluent Percentage= __. 1 ....___:.m. 1 2 3 4 5 6 7 B 9 10 It l2 N. a: RN[I 7 8 9 10 11 12 sw�. Overall Analysis: a >90% Result: PASS LOEC: >90% NOEC: 90 /o ChV: Ca:: 13 iu it-?: o3 Envtronmental Testing Soludcns, lnc Dale; Ala\• ?i, _1118 Effluent Aquatic Toxicity Report Form . Phase I1 Chronic Cerioilaphnia dilbiu Facilin-: Wilson \\R"1'P NPDES!i: NC-0023906 Pipe 9: 001 County: Wilson r Convnents: Laboratory Performing Test Enviremr.entl "Cestinx SolutiCris.sc. Signature of Operator in Responsible Chug - t Signature of Laboratory Sup en isor-( A tsstl..��' Sander: IaoittgA4 180411.I3 Mail Original To: North Carolina Department of Environment and Natural Resources DWQ/ Environmental Sciences Branch Stan dire End dart: Stan time: Eml time: 1621 Mail Service Center 05.00-13 05-16-19 1a13 0733 Ralcigh.NC 27699-1621 Sample Information Sample t sample'_ Control�� yeni11 am,ug± o5-07-IS 05-09-t3 CoOecdon snrt dare'.,e Test Information m 90..; 90'e [wsrol Cmnrol Conval TK:1mLL'r:l: C.:mpusit. dtaasien. 71 i-L _l t Iniial PH IS" : 7.80 7.3'_ 7.80 7.73 7,66 7.56 i2.33 AlWlinisy ImgL CaC0,1: Final pH iSQ: 8.0 9i 82 Ba 7.3 8.0 HaMncss lmNL CaCO,e 40.38 Initial DC( raw 8.- 8' 7.3 7.7 3.1 Coaducticiry sunilhai:cml: J7a SO 11, u!. 1a1 Final DO ungU 8''- 2a.6 21.8 21.9 217 2a.a T,i,imidual chlorine killLr N.10 <0.10 initial T<mp. Cts: Final T,"P l'CI: 15.0 2i.1 25.0 2b.8 2i'1 2- 5.0 24.8 Sample Temp. at Receipt (-"Cl* LI 0.1 Effluent Percentage 9g/ Effluent Percentage= Organism Nutaber l 2 3 4 5 6 7 8 9 10 1112 ma,n :n :1 74 23 26 2b 29 29 23 27 26 29 27.8 7 3 4 5 6 I 7 8 9 10 11 12 . a , R n t0 11 12 n� Effluent Percentage= 7 8 9 10 11 12 c� Treatment 4 Oreanism5 I 2 6 Effluent Percentage= Effluent Percentage= 4 5 6 77 8�r 4 5 6 7 8 9 10 11 12 r.,a Overall Analysis: NOEC: 9o°/a ChV: >90% Result: PASS LOEC: >90 �° _ _ ._...... ... r r.ne „-: Enelranmenral Testing solutions. Inc Effluent Aquatic Toxicity Report Form - Phase Il Chronic Facility. Wilson WwTP �I I'C'�G` Laboratory Performing Test: Environme s SoIolut�ion,..,^Fe/t-E/ Signature of Operator in Responsible Chaff' Signature of Laboratory Supervisor: / ..het iil�. �i also; i7ac 1333) 3it1-9363 ^ioJep6ni,t;(uyp7 Uale: AueusL24.7_01 Nr. 00i tlob Pipe 9: 001 County: Wilson Comments: 180310 Mail Original To: North Carolina Coaawiedof Environment and Natural Resources DWQ/ Environmental Sciences Branch 1621 Mail Service Center Scan time End dmc Slanli,c End wed Raleioh,NC 27699-1621 os.oe-ta oa-ls-la 1520 og3a Sample Information Coliealon .tart daie: Gmtr Composite duration: Alkalinity (ng/L CaC01): Hardness (mgil CaCO,I: Canduaiviry (pmhos'atn: Total residual chlorine (mWL) Sample Temp. at Receipt("C): Sample) sample]unv•I oa-�6-1a oa-os-la 21 33, 33. 34. 34. 36 409 427 151. 14u. iP .ern' Test Information r77- sve•tl1 s,�.e- Treatment: 9P'a 90% 90% Control Control Connol Initial pH (SU1: 743 758 771 768 772 769 Final PH (Sul: 775 7.76 772 7.69 767 761 Initial DO(mg/L): 79 s0 So 7.3 7.9 S0 Final DO(mglL): 1.9 8.1 79 77 8o 7.8 Initial Temp. ("Q: 24.9 14.7 25.1 247 24.8 246 Final Tonp. l"C): 25.1 24.3 24.8 249 25.1 247 Organism Number n a 5 7 2 9 10 11 12 Mwe e.onrrol vrgamsms Number of Youne Produced it — 35 34 29 27 32 28 30 23 31 30 27 29.9 Adult Survival: (L)ive, Dead L L L L L L L L L L L L Effluent Percent2ge i e a o in 11 12 blo. t reatment4 Ur amsms NumberofYoun Produced I 1 31 < 36 I 32 - 33 - 30 - 31 I 33 - 36 - 32 35 33 35 33.5 Adult SurvivaL (L)ive,(D)ead L j L I L I L I L I L I L I L I L I L I L I L .-12.0 Effluent Percentage= Treatment 3 Orsanisms 1 2 3 4 5 6 7 8 9 10 11 12 aas Effluent Percentage Treatment 5 Or2anisms 1 2 3 4 5 ( 7 3 9 10 ll 12 ate. Effluent Percentage= 1 2 3 4 5 6 7 8 9 10 11 12 arae Overall Analysis: a >90% Result: PASS LOEC: >90% NOEC: 90% ChV: DWQ form AT-3 (8/91) Rev. 11195 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RNER BASIN: City of Wilson - Hominy Creek WRF, NCO023906 Renewal Neuse SUPPLEMENTAL APPLICATION INFORMATION PART F.INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES All treatment works receiving discharges from significant industrial users or which receive RCRA,CERCLA, or other remedial wastes must complete part F. GENERAL INFORMATION: F.I. Pretreatment program. Does the treatment works haveor is subject toan approved pretreatment program? ® Yes ❑ No F.2. Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number of each of the following types of industrial users that discharge to the treatment works. a. Number of non -categorical SIUs. 4 Total 13 are covered by a CIU classification but are not subject to CIU limits) b. Number of CIUs. 8 Total (7 Categorical Industrial Users, but one has 2 permitted categorical discharges) SIGNIFICANT INDUSTRIAL USER INFORMATION: Supply the following Information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.S and provide the information requested for each SIU. F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: 'Refer to Attachment A' Mailing Address: 'Refer to Attachment A' 'Refer to Attachment A• FA. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. *Refer to Attachment A• F.S. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): 'Refer to Attachment A' Raw material(s): 'Refer to Attachment A' F.6. Flow Rate. a. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day (god) and whether the discharge is continuous or intermittent. See attached gpd ( continuous or intermittent) b. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system in gallons per day (god) and whether the discharge is continuous or intermittent. See attached gpd ( continuous or intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: See attached a. Local limits ❑ Yes ❑ No b. Categorical pretreatment standards ❑ Yes ❑ No If subject to categorical pretreatment standards, which category and wbcategory? EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 39 of 42 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RNER BASIN: City of Wilson - Hominy Creek VVRF, NCO023906 Renewal Neuse F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU mused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years? ❑ Yes ID No If yes, describe each episode. 'Refer to Attachment A` RCRA HAZARDOUS WASTE RECEIVED BY TRUCK, RAIL, OR DEDICATED PIPELINE: F.9. RCRA Waste. Does the treatment works receive or has it in the past three years received RCRA hazardous waste by truck, rail or dedicated pipe? ❑ Yes 0 No (go to F.12) F.10. Waste transport Method by which RCRA waste is received (check all that apply): ❑ Truck ❑ Rail ❑ Dedicated Pipe F.11. Waste Description. Give EPA hazardous waste number and amount (volume or mass, specify units). EPA Hazardous Waste Number AmountUnits CERCLA (SUPERFUND) WASTEWATER, RCRA REMEDIATIONICORRECTIVE ACTION WASTEWATER, AND OTHER REMEDIAL ACTIVITY WASTEWATER: F.12. Remediation Waste. Does the treatment works currently (or has it been notified that it will) receive waste from remedial activities? ❑ Yes (complete F.13 through F.15.) ® No F.13. Waste Origin. Describe the site and type of facility at which the CERCLAIRCRAIor other remedial waste originates (or is expected to originate in the next five years). F.14. Pollutants. List the hazardous constituents that are received (or are expected to be received). Include data on volume and concentration, if known. (Attach additional sheets it necessary.) FA 5. Waste Treatment. a. Is this waste treated (or will be treated) prior to entering the treatment works? ❑ Yes ❑ No If yes, describe the treatment (provide informaton about the removal efficiency): b. Is the discharge (or will the discharge be) continuous or intermittent? ❑ Continuous ❑ Intermittent If intermittent, describe discharge schedule. END OF PART F. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 8 7550-22. 'age 1) or 2 Facility Name: City of Wilson Permit Number: NC 0023906 Attachment 0 Supplemental Application Information Significant Industrial User Information Part F Items F3 — F8 Facility Name: City of Wilson Permit Number: NC 0023906 Supplemental Application Information Page 1 of 12 Part F. Industrial User Discharges (Significant Industrial User Information) Item F3. Significant Industrial User Information - (Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary.) Name: Ardagh Glass Inc. Address: P.O. Box 1757 2200 Firestone Parkway Wilson, NC 27893 Item F.4. Industrial Processes - (Describe all of the industrial processes and raw materials that affect or contribute to the SIU's discharge.) Manufacture of glass containers from raw and recycled materials Item F.S. Principal Product(s) and Raw Material(s) - (Describe all of the principal processes and raw material that affect or contribute to the SIU's discharge.) Principal Product(s): Glass containers Raw Material(s): Too numerous to list Item F.6. Flow Rate a. Process wastewater flow rate - (Indicate the average daily volume of process wastewater discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent.) 111,300 gpd — Continuous b. Non -process wastewater flow rate - (Indicate the average daily volume of non -process wastewater discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent.) 37,800 gpd - Continuous Item F.7. Pretreatment Standards - (Indicate whether the SIU is subject to the following) a. Local Limits? - Yes b. Categorical pretreatment standards? - Yes If subject to categorical pretreatment standards, which category and subcategory? - 40 CFR Part 426, Subcategory H Item F.B. Problems at the Treatment Works Attributed to the Waste Discharged by the SIU - (Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years?) No Facility Name: City of Wilson Permit Number: NC 0023906 Supplemental Application Information Part F. Industrial User Discharges (Significant Industrial User Information) Page 2 of 12 Item F.3. Significant Industrial User Information - (Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary.) Name: Bridgestone Americas Tire Operations Address: P.O. Box 1139 3001 Firestone Parkway Wilson, NC 27894 Item FA. Industrial Processes - (Describe all of the industrial processes and raw materials that affect or contribute to the SIU's discharge.) Mixing, milling, extruding, calendaring, forming, and cutting of rubber components to assemble steel radial tires. Item F.S. Principal Product(s) and Raw Material(s) - (Describe all of the principal processes and raw material that affect or contribute to the SIU's discharge.) Principal Product(s): Steel radial tires for passenger cars and light trucks Raw Material(s): Too numerous to list Item F.6. Flow Rate a. Process wastewater flow rate - (Indicate the average daily volume of process wastewater discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent.) 67,000 gpd — Continuous b. Non -process wastewater flow rate - (Indicate the average daily volume of non -process wastewater discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent.) 66,000 gpd - Continuous Item F.7. Pretreatment Standards - (Indicate whether the SIU is subject to the following) a. Local Limits? - Yes b. Categorical pretreatment standards? No If subject to categorical pretreatment standards, which category and subcategory? 40 CFR, Part 428, Subpart A; however, no pretreatment limits. Item F.S. Problems at the Treatment Works Attributed to the Waste Discharged by the SIU - (Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years?) No Facility Name: City of Wilson Permit Number: NC 0023906 Page 3 of 12 Supplemental Application Information Part F. Industrial User Discharges (Significant Industrial User Information) Item F.3. Significant Industrial User Information - (Provide the name and address of each Stu discharging to the treatment works. Submit additional pages as necessary.) Name: Evans- Mactavish-Agricraft, Inc. Address: P.O. Box 3408 5123 Ivy Court Wilson, NC 27893 Item F.4. Industrial Processes - (Describe all of the industrial processes and raw materials that affect or contribute to the SIU's discharge.) Cleaning, etching, and powder coating of metal products Item F.S. Principal Product(s) and Raw Material(s) - (Describe all of the principal processes and raw material that affect or contribute to the SIU's discharge.) Principal Product(s): Various metal products for various local industries. Material handling equipment for tobacco, agriculture, food, and similar industries. Raw Material(s): Too numerous to list Item F.6. Flow Rate a. Process wastewater flow rate - (Indicate the average daily volume of process wastewater discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent.) 300 gpd — Continuous b. Non -process wastewater flow rate - (Indicate the average daily volume of non -process wastewater discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent.) 1,000 gpd- Continuous Item F.7. Pretreatment Standards - (Indicate whether the SIU is subject to the following) a. Local Limits? - Yes b. Categorical pretreatment standards? - Yes If subject to categorical pretreatment standards, which category and subcategory? - 40 CFR Part 433, Subcategory A Item F.S. Problems at the Treatment Works Attributed to the Waste Discharged by the SIU - (Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years?) No Facility Name: City of Wilson Page 4 of 12 Permit Number: NC 0023906 Supplemental Application Information Part F. Industrial User Discharges (Significant Industrial User Information) Item F.3. Significant Industrial User Information - (Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary.) Name: Fresenius Kabi Address: 5200 Corporate Parkway Wilson, NC 27893 Item FA. Industrial Processes - (Describe all of the industrial processes and raw materials that affect or contribute to the SIU's discharge.) Manufacturing of pharmaceutical products (prefilled drug delivery systems), Quality Control laboratory and Stability laboratory. Item F.S. Principal Product(s) and Raw Material(s) - (Describe all of the principal processes and raw material that affect or contribute to the SIU's discharge.) Principal Product(s): Prefilled drug delivery system. Raw Material(s): Too numerous to list Item F.6. Flow Rate a. Process wastewater flow rate - (Indicate the average daily volume of process wastewater discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent.) 8,800 gpd — Continuous b. Non -process wastewater flow rate - (Indicate the average daily volume of non -process wastewater discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent) 12,100 gpd - Continuous Item F.7. Pretreatment Standards - (indicate whether the SIU is subject to the following) a. Local Limits? - Yes C. Categorical pretreatment standards? - Yes If subject to categorical pretreatment standards, which category and subcategory? - 40 CFR Part 439, Subcategory D Item F.8. Problems at the Treatment Works Attributed to the Waste Discharged by the SIU - (Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years?) No Facility Name: City of Wilson Page 5 of 12 Permit Number: NC 0023906 Supplemental Application Information Part F. Industrial User Discharges (Significant Industrial User Information) Item F.3. Significant Industrial User Information - (Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary.) Name: Linamar Forging Address: P.O. Box 370 2401 Old Stantonsburg Road Wilson, NC 27893 Item FA. Industrial Processes - (Describe all of the industrial processes and raw materials that affect or contribute to the SIU's discharge.) Manufacture of bearing rings, hub rings, and forgings utilizing the following processes: forging, machining, grinding, and heat -treating. Item F.S. Principal Product(s) and Raw Material(s) - (Describe all of the principal processes and raw material that affect or contribute to the SIU's discharge.) Principal Product(s): Bearing rings, Hub rings, and Forgings Raw Material(s): Too numerous to list Item F.6. Flow Rate a. Process wastewater flow rate - (Indicate the average daily volume of process wastewater discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent.) 17,500 gpd — Continuous b. Non -process wastewater flow rate - (Indicate the average daily volume of non -process wastewater discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent.) 3,700 gpd - Continuous Item F.7. Pretreatment Standards - (Indicate whether the SIU is subject to the following) 9. Local Limits? - Yes d. Categorical pretreatment standards? - Yes If subject to categorical pretreatment standards, which category and subcategory? - 40 CFR Part 433, Subcategory A Item F.B. Problems at the Treatment Works Attributed to the Waste Discharged by the SIU - (Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years?) No Facility Name: City of Wilson Permit Number: NC 0023906 Supplemental Application Information Part F. Industrial User Discharges (Significant Industrial User Information) Page 5 of 12 Item F.3. Significant Industrial User Information - (Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary.) Name: Purdue Pharmaceuticals, L.P. Address: 4701 Purdue Drive Wilson, NC 27893 Item FA. Industrial Processes - (Describe all of the industrial processes and raw materials that affect or contribute to the SfU's discharge.) Manufacturing, packaging, and laboratory analysis of tablets, and capsulated pharmaceutical products. Item F.5. Principal Product(s) and Raw Material(s) - (Describe all of the principal processes and raw material that affect or contribute to the SIU's discharge.) Principal Product(s): Pharmaceutical tablets, caplets, and capsules Raw Material(s): Too numerous to list Item F.6. Flow Rate a. Process wastewater flow rate - (Indicate the average daily volume of process wastewater discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent.) 87,700 gpd — Continuous b. Non -process wastewater flow rate - (Indicate the average daily volume of non -process wastewater discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent.) 62,820 gpd - Continuous Item F.7. Pretreatment Standards - (Indicate whether the SIU is subject to the following) a. Local Limits? - Yes b. Categorical pretreatment standards? - Yes If subject to categorical pretreatment standards, which category and subcategory? - 40 CFR Part 430, Subcategory D Item F.S. Problems at the Treatment Works Attributed to the Waste Discharged by the SIU - (Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years?) No Facility Name: City of Wilson Permit Number: NC 0023906 Supplemental Application Information Part F. Industrial User Discharges (Significant Industrial User Information) Page 7 of 12 Item F.3. Significant Industrial User Information - (Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary.) Name: Refresco Beverages Address: 4843 International Boulevard Wilson, NC 27894-0728 Item FA. Industrial Processes - (Describe all of the industrial processes and raw materials that affect or contribute to the SIU's discharge.) Manufacture and bottling of soft drinks. Washing of plastic bottles after being formed by a plastic blow molding process. Item F.5. Principal Product(s) and Raw Material(s) - (Describe all of the principal processes and raw material that affect or contribute to the SIU's discharge.) Principal Product(s): Canned soft drinks in 12 ox size Bottled soft drinks in 1, 2, & 3 liters sizes Raw Material(s): Too numerous to list Item F.6. Flow Rate a. Process wastewater flow rate - (Indicate the average daily volume of process wastewater discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent.) 50,800 gpd — Continuous b. Non -process wastewater flow rate - (Indicate the average daily volume of non -process wastewater discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent.) 600 gpd - Continuous Item F.7. Pretreatment Standards - (Indicate whether the SIU is subject to the following) a. Local Limits? - Yes C. Categorical pretreatment standards? - No If subject to categorical pretreatment standards, which category and subcategory? 40 CFR, Part 463, Subpart B. Item F.8. Problems at the Treatment Works Attributed to the Waste Discharged by the SIU - (Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years?) two Facility Name: City of Wilson Page 8 of 12 Permit Number: NC 0023906 Supplemental Application Information Part F. Industrial User Discharges (Significant Industrial User Information) Item F.3. Significant Industrial User Information - (Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary.) Name: Sandoz Pipe 001 Address: 4700 Sandoz Drive Wilson, NC 27893 Item FA. Industrial Processes - (Describe all of the industrial processes and raw materials that affect or contribute to the SIU's discharge.) Manufacturing, packaging, and laboratory analysis of tablets, caplets, and capsulated pharmaceutical products. Item F.5. Principal Product(s) and Raw Material(s) - (Describe all of the principal processes and raw material that affect or contribute to the SIU's discharge.) Principal Product(s): Pharmaceutical tablets, caplets, and capsules Raw Material(s): Too numerous to list Item F.6. Flow Rate a. Process wastewater flow rate - (Indicate the average daily volume of process wastewater discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent.) 65,806 gpd — Intermittent b. Non -process wastewater flow rate - (Indicate the average daily volume of non -process wastewater discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent.) 17,887 gpd - Intermittent Item F.7. Pretreatment Standards - (Indicate whether the SIU is subject to the following) a. Local Limits? - Yes d. Categorical pretreatment standards? - Yes If subject to categorical pretreatment standards, which category and subcategory? - 40 CFR Part 439, Subcategory D Item F.8. Problems at the Treatment Works Attributed to the Waste Discharged by the SIU - (Has the SiU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years?) No Facility Name: City of Wilson Page 9 of 12 Permit Number: NC 0023906 Supplemental Application Information Part F. Industrial User Discharges (Significant Industrial User Information) Item F.3. Significant Industrial User Information - (Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary.) Name: Sandoz Pipe 004 Address: 4700 Sandoz Drive Wilson, NC 27893 Item F.4. Industrial Processes - (Describe all of the industrial processes and raw materials that affect or contribute to the SIU's discharge.) Pharmaceutical Quality Assurance and Stability Laboratory. Item F.5. Principal Product(s) and Raw Material(s) - (Describe all of the principal processes and raw material that affect or contribute to the SIU's discharge.) Principal Product(s): Pharmaceutical tablets, caplets, and capsules Raw Material(s): Too numerous to list Item F.6. Flow Rate a. Process wastewater flow rate - (Indicate the average daily volume of process wastewater discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent.) 40 gpd — Intermittent b. Non -process wastewater flow rate - (Indicate the average daily volume of non -process wastewater discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent.) 675 gpd - Intermittent Item F.7. Pretreatment Standards - (Indicate whether the SIU is subject to the following) a. Local Limits? - Yes b. Categorical pretreatment standards? - Yes If subject to categorical pretreatment standards, which category and subcategory? - 40 CFR Part 439, Subcategory D Item F.8. Problems at the Treatment Works Attributed to the Waste Discharged by the SW - (Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years?) IM Facility Name: City of Wilson Page 10 of 12 Permit Number: NC 0023906 Supplemental Application Information Part F. Industrial User Discharges (Significant Industrial User Information) Item F.3. Significant Industrial User Information - (Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary.) Name: Smithfield Packaged Meats Corp. Address: 2401 Wilson Boulevard Wilson, NC 27893 Item FA. Industrial Processes - (Describe all of the industrial processes and raw materials that affect or contribute to the SIU's discharge.) Processing of pork bellies into bacon. Processing consists of the injection of flavoring and pickle solution, smoking utilizing smokehouses, slicing, and packaging. Item F.5. Principal Product(s) and Raw Material(s) - (Describe all of the principal processes and raw material that affect or contribute to the SIU's discharge.) Principal Product(s): Bacon Raw Material(s): Too numerous to list Item F.6. Flow Rate a. Process wastewater flow rate - (Indicate the average daily volume of process wastewater discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent.) 75,000 gpd — Continuous b. Non -process wastewater flow rate - (Indicate the average daily volume of non -process wastewater discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent.) 20,800 gpd - Continuous Item F.7. Pretreatment Standards - (Indicate whether the SIU is subject to the following) a. Local Limits? - Yes b. Categorical pretreatment standards? - No If subject to categorical pretreatment standards, which category and subcategory? - 40 CFR, Part 432, Subpart F; however, no pretreatment limits Item F.8. Problems at the Treatment Works Attributed to the Waste Discharged by the SIU - (Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years?) No Facility Name: City of Wilson Page 11 of 12 Permit Number: NC 0023906 Supplemental Application Information Part F. Industrial User Discharges (Significant Industrial User Information) Item F.3. Significant Industrial User Information - (Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary.) Name: Sun River Services Corporation Address: 2018 Beeler Road Wilson, NC 27893 Item FA. Industrial Processes - (Describe all of the industrial processes and raw materials that affect or contribute to the SIU's discharge.) Processing of poultry, pork, and fish organs into pet food ingredients. Item F.5. Principal Product(s) and Raw Material(s) - (Describe all of the principal processes and raw material that affect or contribute to the SIU's discharge.) Principal Product(s): Pet Food Ingredients Raw Material(s): Too numerous to list Item F.6. Flow Rate a. Process wastewater flow rate - (Indicate the average daily volume of process wastewater discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent.) 27,200 gpd — Continuous b. Non -process wastewater flow rate - (Indicate the average daily volume of non -process wastewater discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent.) 4,000 gpd - Continuous Item F.7. Pretreatment Standards - (Indicate whether the SIU is subject to the following) a. Local Limits? - Yes b. Categorical pretreatment standards? - No If subject to categorical pretreatment standards, which category and subcategory? - N/A Item F.8. Problems at the Treatment Works Attributed to the Waste Discharged by the SIU - (Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years?) IM. Facility Name: City of Wilson Permit Number: NC 0023906 Supplemental Application Information Part F. Industrial User Discharges (Significant Industrial User Information) Page 12 of 12 Item F.3. Significant Industrial User Information - (Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary.) Name: United Technologies Systems/Kidde Aerospace and Defense Address: 4200 Airport Drive Wilson, NC 27896-9643 Item F.4. Industrial Processes - (Describe all of the industrial processes and raw materials that affect or contribute to the SIU's discharge.) Manufacturing and servicing of fire detection and fire suppression systems for commercial and military aircraft. The following processes are utilized: degreasing, anodizing, and phosphotizing. Item F.5. Principal Product(s) and Raw Material(s) - (Describe all of the principal processes and raw material that affect or contribute to the SIU's discharge.) Principal Product(s): Smoke detectors, heat sensors, flame detectors, electronic control units and fire extinguishing systems for aircraft and military vehicles. Raw Material(s): Too numerous to list Item F.6. Flow Rate a. Process wastewater flow rate - (Indicate the average daily volume of process wastewater discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent.) 8,115 gpd — Continuous b. Non -process wastewater flow rate - (Indicate the average daily volume of non -process wastewater discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent.) 15,040 gpd — Continuous Item F.7. Pretreatment Standards - (Indicate whether the SIU is subject to the following) a. Local Limits? - Yes e. Categorical pretreatment standards? - Yes If subject to categorical pretreatment standards, which category and subcategory? - 40 CFR Part 433, Subcategory A Item F.8. Problems at the Treatment Works Attributed to the Waste Discharged by the SIU - (Ilas the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years?) IM FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: City of Wilson - Hominy Creek WRF, NCO023906 Renewal Neuse SUPPLEMENTAL APPLICATION INFORMATION PART G. COMBINED SEWER SYSTEMS *Not Applicable* If the treatment works has a combined sewer system, complete Part G. *Not Applicable* GA. System Map. Provide a map indicating the followng: (may be included with Basic Application Information) a. All CSO discharge points. b. Sensitive use areas potentially affected by CSOs (e.g., beaches, drinking water supplies, shellfish beds, sensitive aquatic ecosystems, and outstanding natural resource waters). C. Waters that support threatened and endangered species potentially affected by CSOs. G.2. System Diagram. Provide a diagram, either in the map provided in G.1 or w a separate drawing. of the combined sewer collection system that includes the following information. a. Location of major sewer trunk lines, both combined and separate sanitary. b. Locations of points where separate sanitary sewers feed into the combined server system. c. Locations of ir0ine and off-line storage structures. d. Locations of flow -regulating devices. e. Locations of pump stations. CSO OUTFALLS: Complete questions G.3 through G.6 once for each CSO discharge ooint. G.3. Description of Outfall. a. Ouffall number NA b. Location NA NA (City or town, If applicable) (Zip Code) NA NA (County) (State) NA NA (Latitude) (Longitude) C. Distance from shore (if applicable) NA ft. d. Depth below surface (if applicable) NA ft. e. Which of the following were monitored during the last year for this CSO? *Not Applicable* ❑ Rainfall ❑ CSO pollutant concentrations ❑ CSO frequency ❑ CSO flow volume ❑ Receiving water quality f. How many storm events were monitored during the last year? NA GA. CSO Events. a. Give the number of CSO events in the last year. NA events (F_] actual or ❑ approx.) b. Give the average duration per CSO event NA hours (❑ actual or ❑ approx.) EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 41 of 42 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: City of Wilson - Hominy Creek WRF, NCO023906 Renewal Neuse C. Give the average volume per CSO event NA million gallons actual or ❑ approx.) d. Give the minimum rainfall that caused a CSO event in the last year NA Inches of rainfall G.S. Description of Receiving Waters. a. Name of receiving water. b. Name of watershed/river/stream system: United State Soil Conservation Service 14-digit watershed code (if known): C. Name of State Management/River Basin: United States Geological Survey 8-digit hydrologic cataloging unit code (if known): G.6. CSO Operations. Describe any known water quality impacts on the receiving water caused by this CSO (e.g., permanent or intermittent beach closings, permanent or intermittent shell fish bed closings, fish kills, fish advisories, other recreational loss, or violation of any applicable State water quality standard). EPA Form 3510-2A (Rev. 1-99). Replaces EPA forts 7550-6 & 7550-22, Page 42 of 42 END OF PART G. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE. EPA Form 3510.2A (Rev. 1-99). Replaces EPA fom 7550-6 & 7550-22. Page 43 of 42 f i YfTfl�fl; uV►CUJ Dlu 13 ad WJa HOMINY CREEK WATER RECLAMATION FACILITY Biosolids generated at the Hominy Creek facility are stabilized to a Class B residual by anaerobic digesters or to a Class A residual by an alkaline sludge stabilization process prior to disposal by land application or disposal to a regional compost facility. Anaerobically digested sludge (ADS) is pumped from the sludge holding tanks and conveyed to two (2) belt filter presses (BFP) located in the dewatering building. Liquid polymer feed facilities provide effective dewatering of the ADS. Dewatered sludge is discharged from the BFP directly onto a conveyor belt and then to the sludge storage pad or to the alkaline stabilization facility. The dewatered sludge cake has a solid concentration of 20 to 25 percent. Alkaline stabilization is provided in order to produce a Class A biosolids product under the 40 CFR Part 503 sewage sludge regulations. A series of conveyors deliver the dewatered sludge cake to the alkaline stabilization facility. Lime and supplemental heat are added to the sludge cake in a lime -sludge blender to raise the temperature and adjust the pH. Supplemental heat is added to boost the temperature to pasteurization levels. Temperature is maintained at or above pasteurization temperature levels during passage through a plug flow pasteurization vessel conveyor. Lime is stored in a 66-ton lime silo. Dewatered and stabilized biosolids are land applied to permitted privately -owned farmland or transported to a privately -owned composting facility. A 32,000 sq. ft. covered storage pad provides storage for periods when solids cannot be land applied. Granville Farms, Inc operates the City of Wilson land application program. The program requires full time operation,^rmally 5 to 6 days per week and 8 to 12 hours per day. Jimmy Prid9fn Water Recla#iattnt Facility Manager (Rev. 11-2018)