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HomeMy WebLinkAboutWQ0003626_GW Monitoring - 07-2022_20220907GW-59A COMPLIANCE REPORT FORM Permit # W00003626 (Submit one each monitoring period with GW-59 forms.) I Enter date monitoring results were due. August 31,2022 2 Was any required information missing on the GW-59 report forms? YES NO X If the answer to question I or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing identification YES NO X plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Officefor guidance. 4 Are any monitored constituents equal to or above the established standards? YES X NO If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 if "YES" list the affected wells idividually with constituent(s) an ncentration(s) exceeding standards in the space provided below: MW#2- Total Ammonia Nitrogen 3.84 mg/L, MW# 4- Nitrates Tg/L, MW#5- Nitrates 13.4 mg/L, ' MW#11- Total Ammonia Nitrogen 2.81 mg/L, MW#12- Nitrates 11.3 mg/LYIN 5 For the constituents identified in question 4 above, have standards been exceede re�i sly ie same constituent(s) in the YES X NO same wells in the last two ears? ci p If the answer to question 5 is "NO", skip to section 8. c� If the answer to question 5 is "YES" list in the space provided below, each well with c16e xc t standards, concentration(s) reported, and sample collection date for each occurrence (for the last two year► JULY 2 0- M W#2 Total Ammonia 1.77 mg/L, MARCH 2O21- MW#2 Total Ammonia 2.78 mg/L, JULY 2021- MW#2 Total A-onia 2.9 mg/L, NOVEMBER 2021- MW#2 Total Ammonia 3.56, March 2022-MW#2 Total Ammonia 5.24 mg/L, MARCH 202 MW#5 Nitrates 10.7mg/L , JULY 2021- MW#5 Nitrates 14.6 mg/L, NOVEMBER 2021- MW#5 Nitrates 14.3 mg/L., March 2022- MW#5 Nitrates 15.5 mg/L 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES", a groundwater qualityproblem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. Ifthe answer is "NO", monitoring wells may be improperly located, contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this groundwater quality YES X NO problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties. Reduce spray in area of MW#5, MW#2, MW#4, & MW#11 8 The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hearby acknowledge that the above information was evaluated and the information submitted in this report (Compliance Report GW-59A) is true and complete to the best of my knowledge. �y ` Signature of Permittr Authorized Agent) Date SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: OWN W. DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES COMPLIANCE REPORT FORM INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919.807.6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 2&6 Facility Name: Campbell Soup Supply Company Non -Discharge WO 0003626 UIC A06 NPDES Other ae5 Permit Name (if different): Facility Address: 2120 NC 71 Hwy North, Maxton, NC 28364 TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery 2120 NC 71 Hwy North, Maxton, NC 28384 County Robeson 0 Spray Field ❑ Remediation: #S& Contact Person: Keith Osterman Telephone#: (910) 844-1202 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Spray Field Site No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: from PermR SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-1 Date sample collected: 7/26/22 FIELD ANALYSES: WAS Well Depth: 24 ft. Well Diameter: 4 in. pH 00400: 5.74 units Temp. 000lo: 23.5 °C DRY at Depth to Water Level 82546:17.7 ft. below measuring point Screened Interval: 19.3 ft. to 24 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, check Volume of water pumped/bailed before sampling: 15 gallons Appearance Clear here:❑ Samples for metals were collected unfiltered: ❑■ YES ,/ ❑ NO and field acidified: tJ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 08/01/22 Thru 08/24/22 Laboratory Name: Environmental Science Certification No. ENV375 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 3.83 mg/L Zn - Zinc 01092 mg/L Coliform: IMF Total 31504 /100mL Phosphorus: Total as P 00665 <0.100 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 107.0 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 1.04 mg/L Ca - Calcium 00916 mg/L Chloride 0094o 46.9 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.250 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH,as N; Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # ror Kemeolation bystems Unly (Attacn Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Keith Osterman - Environmental Manager Pennittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.3-1-2016 a;2- SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: NNL• • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM � R617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone! 919.807.6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 2P.NF S .W.Z Facility Name: Campbell Soup Supply Company Non -Discharge WO 0003626 UIC aw NPDES Other aw Permit Name (if different): Facility Address: 2120 NC 71 Hwy North, Maxton, NC 28364 TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery 2120 NC 71 Hwy North, Maxton, NC 28184 County Robeson ❑M Spray Field ❑ Remediation: 20`1 Contact Person: Keith Osterman Telephone#: (910) 844-1202 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Spray Field Site No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-2 Date sample collected: 7/26/22 FIELD ANALYSES: WAS Well Depth: 24 ft. Well Diameter: 4 in. pH oo4lo: 6.60 units Temp. 000lo: 27.1 oC DRY at Depth to Water Level 82546:15.35 ft. below measuring point Screened Interval: 18.3 ft. to 24 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 15 gallons Appearance clear here: ❑ Samples for metals were collected unfiltered: ❑■ YES � ElNO and field acidified: ER(YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 08/01/22 Thru 08/24/22 Laboratory Name: Environmental Science Certification No. ENV375 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NOA as N 00620 0.299 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 ND mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 703oo 379 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 0068o 5.11 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 135 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 3.84 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # I -or Kemediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Keith Osterman - Environmental Manager Permlttee (or Authorized Aqent) Name and Title - Please print or type Siqnature of , 8/3/ /-Z';2_ (Date) GW-59 Rev.3-1-2016 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES COMPLIANCE REPORT FORM INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807.6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 2W c3: oZ Facility Name: Campbell Soup Supply Company Non -Discharge WQ 0003626 UIC WW Permit Name (if different): NPDES Other Facility Address: 2120 NC 71 Hwy North, Maxton, NC 28364 TYPE OF PERMITTED OPERATION BEING MONITORED 2120 NC 71 Hwy North, Maxton, NC 28364' County Robeson ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: A Contact Person: Keith Osterman Telephone#: (910) 844-1202 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Spray Field Site No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-3A Date sample collected: 7-26-22 FIELD ANALYSES: WAS Well Depth: 20 ft. Well Diameter: 2 in. pH 00000: 5.30 units Temp. 000lo: 22.7 oC DRY at Depth to Water Level 82546:15.25 ft. below measuring point Screened Interval: 5 ft. to 20 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, check Volume of water pumped/bailed before sampling: 15 gallons Appearance Cloudy here:❑ Samples for metals were collected unfiltered: ❑■ YES ❑ NO and field acidified: A"YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 08/01/22 Thru 08/24/22 Laboratory Name: Environmental Science Certification No. ENV375 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 1.43 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 ND mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 106 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 1.14 mg/L Ca - Calcium 00916 mg/L Chloride 0094o 37.3 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total o1o34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 NO mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remealation toystems only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Keith Osterman- Environmental Manager Permittee (or Authorized Aqent) Name and Title - Please print or type .Z 2_ GW-59 Rev.3-1-2016 SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: 919.807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 2W S �/ Facility Name: Campbell Soup Supply Company Non -Discharge WQ 0003626 UIC 2dw NPDES Other adw Permit Name (if different): Facility Address: 2120 NC 71 Hwy North, Maxton, NC 28364 TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery 2120 NC 71 Hwy North, Maxton, NC 28384 County Robeson 0 Spray Field ❑ Remediation: JW Contact Person: Keith Osterman Telephone#: (910) 844-1202 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Spray Field Site No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-4 Date sample collected: 7/26/22 FIELD ANALYSES: WAS Well Depth: 24 ft. Well Diameter: 4 in. pH oo400: 6.5 units Temp. 00010: 21.2 oC DRY at Depth to Water Level 82546:19 ft. below measuring point Screened Interval: 19.3 ft. to 24 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 15 gallons Appearance Cloudy here:❑ Samples for metals were collected unfiltered: EYES ❑ NO and field acidified: L"'J YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 08/01/22 Thru 08/24/22 Laboratory Name: Environmental Science Certification No. ENV375 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead olo51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 11.1 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 ND mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 703oo 280 mg/L Al - Aluminum oil o5 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 1.53 mg/L Ca - Calcium 00916 mg/L Chloride 00940 95.7 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron oio45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 NO mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH, as N, Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # I -or Kemediation systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Keith Osterman - Environmental Manager Permittee (or Authorized Aqent) Name and Title - Please print or type a ;2- GW-59 Rev.3-1-2016 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Print Clearly or Type Facility Name: Campbell Soup Supply Company Permit Name (if different): Facility Address: 2120 NC 71 Hwy North, Maxton, NC 28364 2120 NC 71 Hwy North, Maxton, NC 28184' County Robeson act Person: Keith Osterman Telephone#: (910) 844-1202 Location/Site Name: Spray Field Site No. of wells to be sampled: 11 WELL ID NUMBER (from Permit): MW-5 Date sample collected: 7/26/22 Well Depth: 24 ft. Well Diameter: 4 in. Depth to Water Level 82546:14.1 ft. below measuring point Screened Interval: 18.7 ft. Measuring Point is 3 ft. above land surface Relative M.P. Elevation: Volume of water pumped/bailed before sampling: 15 gallons Samples for metals were collected unfiltered: YES ❑ NO and field acidified: 17 YES DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: 919-807-63 6 PERMIT Number: Expiration Date: 2 m .? Non -Discharge W00003626 UIC JIft NPDES Other 44 TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑M Spray Field ❑ Remediation: 206 ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: to 24 ft ft. ❑ NO Date sample analyzed: 08/01/22 Thru 08/24/22 Laboratory Name: Environmental Science PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 13.4 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 ND mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L issolved Solids:Total 703oo 261 mg/L AI -Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 <1.53 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 85.5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total o1o34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L Phenol 32730 ug/L Fe - Iron 01045 ug/L Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Specific Conductance 00095 µMhos K - Potassium 00937 mg/L Total Ammonia 00610 ND mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L TKN as N 00625 mg/L Ni - Nickel 01067 ug/L FIELD ANALYSES: pH 00400: 6.7 units Spec. Cond. 00094: Odor 00085: None Appearance clear Temp. 000lo: 22.5 oC uMhos Certification No. ENV375 Pb - Lead o1o51 ug/L Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 7873 method # method # method # method # t-or Kememation bystems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Keith Osterman - Environmental Manager Pennittee (or Authorized Apent) Name and Title - Please print or type GW-59 Rev.3-1-2016 If WELL RY at ne of impling, FEN • SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: A-W8 F 73 .Z Facility Name: Campbell Soup Supply Company Non -Discharge WO 0003626 UIC ape NPDES Other Permit Name (if different): Facility Address: 2120 NC 71 Hwy North, Maxton, NC 28364 TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon Remediation: Infiltration Gallery 2120 NC 71 Hwy North, Maxton, NC 28364 County Robeson ❑■ Spray Field ❑ Remediation: 2&8 Contact Person: Keith Osterman Telephone#: (910) 844-1202 ElRotary Distributor ElLand Application of Sludge Well Location/Site Name: Spray Field Site No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-6 Date sample collected: 7/26/22 FIELD ANALYSES: WAS Well Depth: 28 ft. Well Diameter: 4 in. pH 00400: 5.67 units Temp. 00010. 22-8 oC DRY at Depth to Water Level 82546:15.65 ft. below measuring point Screened Interval: 25 ft. to 28 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 ft, above land surface Relative M.P. Elevation: ft. Odor 00085 None sampling, check Volume of water pumped/bailed before sampling: 14 gallons Appearance clear here:❑ Samples for metals were collected unfiltered: ❑■ YES ❑ NO and field acidified: `L/ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 08/01/22 Thru 08/24/22 Laboratory Name: Environmental Science Certification No. ENV375 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 2.21 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 NO mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids:Total 7030o 212 mg/L Al - Aluminum oilo5 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 1.33 mg/L Ca - Calcium oo916 mg/L Chloride 00940 107 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 1873 method # Total Ammonia 00610 ND mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3asN, Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Keith Osterman -Environmental Manager 'e ill Permittee (or Authorized Agent) Name and Title - Please print or type 2L44M 'i (Date) Signature of Permittor Authorized Agent) GW-59 Rev.3-1-2016 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES COMPLIANCE REPORT FORM INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: 919-807.630 FACILITY INFORMATION Please PrintC/ear/yorType PERMIT Number: Expiration Date: 2" 37'917 AT Facility Name: Campbell Soup Supply Company Non -Discharge WO 0003626 UIC 20B NPDES Other 3srs Permit Name (if different): Facility Address: 2120 NC 71 Hwy North, Maxtor, NC 28364 TYPE OF PERMITTED OPERATION BEING MONITORED 2120 NC 71 Hwy North, Maxton, NC 28384 County Robeson ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: Qg'y' Contact Person: Keith Osterman Telephone#: (910) 844-1202 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Spray Field Site No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-8 Date sample collected: 7/26/22 FIELD ANALYSES: WAS Well Depth: 28 ft. Well Diameter: 4 in. pH o0400: 6.44 units Temp. 000lo: 23.3 oC DRY at Depth to Water Level 82546:15.95 ft. below measuring point Screened Interval: 25 ft. to 28 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling,check Volume of water pumped/bailed before sampling: 15 gallons Appearance clear here:❑ Samples for metals were collected unfiltered: 9YES ElNO and field acidified: LT YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 08/01/22 Thru 08/24/22 Laboratory Name: Environmental Science Certification No. ENV375 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 u 9/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 5.37 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 ND mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 91 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 1.55 mg/L Ca - Calcium 00916 mg/L Chloride oo940 28.0 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total o1034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 NO mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Keith Osterman -Environmental Manager !IM Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permi or Authorized Agent) (Date) v GW-59 Rev.3-1-2016 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES COMPLIANCE REPORT FORM INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 2" S 3 eZ Facility Name: Campbell Soup Supply Company Non -Discharge WQ 0003626 UIC efe Permit Name (if different): NPDES Other &-an Facility Address: 2120 NC 71 Hwy North, Maxton, NC 28364 TYPE OF PERMITTED OPERATION BEING MONITORED 2120 NC 71 Hwy North, Maxton, NC 28384' County Robeson ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: =M Contact Person: Keith Osterman Telephone#: (910) 844-1202 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Spray Field Site No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: M1om Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-9 Date sample collected: 7-26-22 FIELD ANALYSES: WAS Well Depth: 30 ft. Well Diameter: 4 in. pH 00400: 6.03 units Temp. 00010: 23.6 eC DRY at Depth to Water Level 825a6: 11.2 p ft. below measuring point Screened Interval: 20.3 ft. to 30 ft. Spec. Cond. 000sa: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling,check Volume of water pumped/bailed before sampling: 15 gallons Appearance Clear here: ❑ Samples for metals were collected unfiltered: ❑■ YES ❑ NO and field acidified: M YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 08/01/22 Thru 08/24/22 Laboratory Name: Environmental Science Certification No. ENV375 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 9.88 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 ND mg/L (Note Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 91 mg/L Al - Aluminum o11o5 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 1.46 mg/L Ca - Calcium 00916 mg/L Chloride 00940 16.9 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total o1o34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1o45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71 goo ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 ND mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn -Manganese 01055 ug/L ,method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # rvr rccrneoratton systems vmy (Anacn LaD Keports): mtluent I otal VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Keith Osterman- Environmental Manager Z/ @" Perms tee (or Authorized Aqent) Name and Title - Please print or type Siqn ture of Perms a or Xuthorized Aqent) (Date GW-59 Rev.3-1-2016 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: • . DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES �1617 COMPLIANCE REPORT FORM INFORMATION PROCESSING UNIT MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 2ft ,� $ Facility Name: Campbell Soup Supply Company Non -Discharge WO 0003626 UIC am NPDES Other AOR Permit Name (if different): Facility Address: 2120 NC 71 Hwy North, Maxton, NC 28364 TYPE OF PERMITTED OPERATION BEING MONITORED 2120 NC 71 Hwy North, Maxton, NC 2664 County Robeson ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑M Spray Field ❑ Remediation: 2W Contact Person: Keith Osterman Telephone#: (910) 844-1202 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Spray Field Site No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: from Perm,t SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-10 Date sample collected: 7/26/22 FIELD ANALYSES: WAS Well Depth: 24 ft. Well Diameter: 4 in. pH oo400: 5.46 units Temp. 000lo: 23.6 °C DRY at Depth to Water Level 82546:9.65 ft. below measuring point Screened Interval: 2 ft. to 24 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, check Volume of water pumped/bailed before sampling: 15 gallons Appearance cloudy here: Samples for metals were collected unfiltered: A YES ❑ NO and field acidified: [I YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 08/01/22 Thru 08/24/22 Laboratory Name: Environmental Science Certification No. ENV375 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NOZ) as N 00615 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 6.59 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 ND mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 7030o 267 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 0068o 2.15 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 113 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 ND mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Keith Osterman- Environmental Manager C�d L Permlttee (or Authorized Agent) Name and Title - Please print or type Signature of Permi (or Authorized Agent) GW-59 Rev.3-1-2016 SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 2j@&2 S i Facility Name: Campbell Soup Supply Company Non -Discharge WO 0003626 U I C ,it - NPDES Other �111e Permit Name (if different): Facility Address: 2120 NC 71 Hwy North, Maxton, NC 28364 TYPE OF PERMITTED OPERATION BEING MONITORED X Lagoon ❑ Remediation: Infiltration Gallery 2120 NC 71 Hwy North, Maxton, NC 28384` County Robeson ❑■ Spray Field ❑ Remediation: 23.2 Contact Person: Keith Osterman Telephone#: (910) 844-1202 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Spray Field Site No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-11 Date sample collected: 7/26/22 FIELD ANALYSES: WAS Well Depth: 30 ft. Well Diameter: 2 in. pH 00400: 6.45 units Temp. 000lo 23.2 eC DRY at Depth to Water Level 82546:16.2 ft. below measuring point Screened Interval: 25 ft. to 30 ft. Spec. Cond. 00094ttMhos time ofsampling, Measuring Point is 3 ft, above land surface Relative M.P. Elevation: ft. Odor 00085 None check Volume of water pumped/bailed before sampling: 15 gallons Appearance cloudy here: Samples for metals were collected unfiltered: ❑■ YES �,/- ❑ NO and field acidified: I� YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 08/01/22 Thru 08/24/22 Laboratory Name: Environmental Science Certification No. ENV375 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 21 /100mL Nitrate (NO3) as N 00620 4.85 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 ND mg/L (Note use MPN method for highly turbid Samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): ssolved Solids:Total 703oo 86 mg/L Al - Aluminum oilo5 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 <1.00 mg/L Ca - Calcium 00916 mg/L Chloride 00940 18.1 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 2.81 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH, as N, Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only . ..rts): Influent Total VOCs� I certify that, to the best of my knowledge and belief, the information submitted in this report is true, acct DWR-certified laboratory. I am aware that there are significant penalties for submitting false information Keith Osterman - Environmental Manager Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.3-1-2016 mg/L Effluent Total VOCs: of Permittee ((* #uthonzed Aqent) mg/L VOC Removal% (Date) SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Print Clearly or Facility Name: Campbell Soup Supply Company Permit Name (if different): Facility Address: 2120 NC 71 Hwy North, Maxton, NC 28364 2120 NC 71 Hwy North, Maxton, NC 26!164 County Robeson ict Person: Keith Osterman Location/Site Name: Spray Field Site Telephone#: (910) 844-1202 No. of wells to be sampled: 11 WELL ID NUMBER (from Permit): MW-12 Date sample collected: 7/26/22 Well Depth: 30 ft. Well Diameter: 2 in Depth to Water Level 82546:19.9 ft. below measuring point Screened Interval: 25 ft. Measuring Point is 3 ft. above land surface Relative M.P. Elevation: Volume of water pumped/bailed before sampling: 15 gallons Samples for metals were collected unfiltered: ❑M YES ❑ NO and field acidified: O YES DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 PERMIT Number: Expiration Date: apt Non -Discharge WQ 0003626 UIC AW NPDES Other 2p.w TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon ❑ Remediation: Infiltration Gallery Spray Field ❑ Remediation: 22.1 ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: to 30 ft. ft. NO FIELD ANALYSES: pH 00000: 5.97 units Spec. Cond. 00094: Odor 00085: None Appearance cloudy Temp. 000lo: 22.1 eC Whos Date sample analyzed: 08/01/22 Thru 08/24/22 Laboratory Name: Environmental Science Certification No. ENV375 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 u9 /L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 11.3 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 ND mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 7030o 269 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 2.31 mg/L Ca - Calcium 00916 mg/L Chloride 00940 102 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 ND mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # r-vr rcCrncurauon systems unry tAtiacn Lao Keports): Innuent I otal vOGs: mg/L Effluent Total VOCs: mg/L VOC Removal% Keith Osterman - Environmental Manager Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.3-1-2016 WAS DRY at time of sampling, here: El I acmnalXical "' ANALYTICAL REPORT August 26, 2022 EHC, Inc. Sample Delivery Group: Samples Received: Project Number: Description: Site: Report To: Entire Report Reviewed By L1518975 07/27/2022 17-M I0101-1 Campbell Soup Company MAXTON,NC Mr. Thomas Ammons PO Box 902 Red Springs, NC 28377 Heather J Wagner Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received. R *w eiiii- - +.ter 11► 4r ^k ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EHC, Inc. 17-MI0101-1 L1518975 08/26/22 11:40 1 of 36 • TABLE OF CONTENTS Cp: Cover Page 1 I Tc: Table of Contents 2� Ss: Sample Summary 3 Cn: Case Narrative 6 Sample Results 7 FSSr: MW-1 L1518975-01 7 MW-2 L1518975-02 g Fri MW-3A L1518975-03 9 FrMW-4 L1518975-04 10 MW-5 L1518975-05 11 PIC MW-6 L1518975-06 12 MW-8 L1518975-07 13 Fil MW-9 L1518975-08 14 rAl MW-10 L1518975-09 15 MW-11 L1518975-10 16 CSC MW-12 L1518975-11 17 Qc: Quality Control Summary 18 Gravimetric Analysis by Method 2540 C-2011 18 Wet Chemistry by Method 350.1 22 Wet Chemistry by Method 365.4 23 Wet Chemistry by Method 9056A 25 Wet Chemistry by Method 9060A 30 GI: Glossary of Terms 31 Al: Accreditations & Locations 32 Sc: Sample Chain of Custody 33 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EHC, Inc. 17-MI0101-1 L1518975 08/26/22 11:40 2 of 36 SAMPLE SUMMARY Collected by Collected date/time Received date/time MW-1 L1518975-01 GW Aric Clark 07/26/2209:37 07/27/22 09:00 Cp Method Batch Dilution Preparation Analysis Analyst Location date/time date/time rTC1 Gravimetric Analysis by Method 2540 C-2011 WG1903892 1 08/0112216:18 08/01/2217:14 MMF Mt. Juliet, TN Wet Chemistry by Method 3501 WG1903509 1 08/01/2213:04 08/01/2213:04 SL Mt. Juliet, TN Wet Chemistry by Method 365.4 WG1907961 1 07/29/2218:48 08/0912213:24 LDT Mt. Juliet, TN Wet Chemistry by Method 9056A WG1901570 1 07/27/22 23:31 07/27/22 23:31 LBR Mt. Juliet, TN Wet Chemistry by Method 9060A WG1908434 1 08/2412216:55 08/24/2216:55 SJF Mt. Juliet, TN Fnj Collected by Collected date/time Received date/time MW-2 L1518975-02 GW Aric Clark 07/26/22 0915 07/27/22 09 00 F qr Method Batch Dilution Preparation Analysis Analyst Location UGC date/time date/time Gravimetric Analysis by Method 2540 C-2011 WG1903896 1 08/01/2217:00 08/01/2218:51 MMF Mt. Juliet, TN Wet Chemistry by Method 350.1 WG1903509 1 08/01/2213:06 08/01/2213:06 SL Mt. Juliet, TN FG1 Wet Chemistry by Method 365.4 WG1907961 1 07/29/2218:48 08/09/2213:26 LDT Mt. Juliet, TN Wet Chemistry by Method 9056A WG1901570 1 07/27/22 23:44 07/27/22 23:44 LBR Mt. Juliet, TN Al$ Wet Chemistry by Method 9060A WG1908434 1 08/24/2217:12 08/24/2217:12 SJF Mt. Juliet, TN Collected by Collected date/time Received date/time FC M W-3A L1518975-03 GW Aric Clark 07/26/22 08:50 07/27/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location dateltime date/time Gravimetric Analysis by Method 2540 C-2011 WG1903896 1 08/01/2217:00 08/01/2218:51 MMF Mt. Juliet, TN Wet Chemistry by Method 350.1 WG1903509 1 08101/2213:07 08/01/2213:07 SL Mt. Juliet, TN Wet Chemistry by Method 365.4 WG1907961 1 07/29/2218:48 08/09/2213:27 LDT Mt. Juliet, TN Wet Chemistry by Method 9056A WG1901570 1 07/27/22 23:58 07/27/22 23:58 LBR Mt. Juliet, TN Wet Chemistry by Method 9060A WG1908434 1 08/24/2217:28 08/24/2217:28 SJF Mt. Juliet, TN Collected by Collected date/time Received date/time MW-4 L1518975-04 GW Aric Clark 07/26/22 09:45 07/27/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Gravimetric Analysis by Method 2540 C-2011 WG1903892 1 08/01/2216:18 08/01/2217:14 MMF Mt. Juliet, TN Wet Chemistry by Method 350.1 WG1903509 1 08/0112213:09 08/01/2213:09 SL Mt. Juliet, TN Wet Chemistry by Method 365.4 WG1907961 1 07/29/2218:48 08/09/2213:28 LDT Mt. Juliet, TN Wet Chemistry by Method 9056A WG1901917 5 07/27/2217:52 07/27/2217:52 LBR Mt. Juliet, TN Wet Chemistry by Method 9060A WG1908434 1 08/2412218:25 08/24/2218:25 SJF Mt. Juliet, TN Collected by Collected date/time Received date/time MW-5 L1518975-05 GW Aric Clark 07/26/2210:31 07/27/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Gravimetric Analysis by Method 2540 C-2011 WG1903896 1 08/0112217:00 08/01/2218:51 MMF Mt. Juliet, TN Wet Chemistry by Method 350.1 WG1903509 1 08/01/2213:10 08/01/2213:10 SL Mt. Juliet, TN Wet Chemistry by Method 365.4 WG1907961 1 07/29/2218:48 08/09/2213:32 LDT Mt. Juliet, TN Wet Chemistry by Method 9056A WG1901917 5 07/27/2218:06 07/27/2218:06 LBR Mt. Juliet, TN Wet Chemistry by Method 9060A WG1908434 1 08124/2218:41 08/24/2218:41 SJF Mt. Juliet, TN ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EHC, Inc. 17-MI0101-1 L1518975 08/26/22 11:40 3 of 36 SAMPLE SUMMARY Collected by Collected date/time Received date/time MW-6 L1518975-06 GW Aric Clark 07/26/2210:14 07/27/2209:00 Method Batch Dilution Preparation Analysis Analyst Location - -- date/time date/time F77 Gravimetric Analysis by Method 2540 C-2011 WG1908160 1 08/09/2217:11 08/09/2217:35 MMF Mt. Juliet, TN Wet Chemistry by Method 350.1 WG1903509 1 08/01/2213:12 08/01/2213.12 SL Mt. Juliet, TN Wet Chemistry by Method 365.4 WG1907961 1 07/29/2218 48 08/09/2213:33 LDT Mt. Juliet, TN Wet Chemistry by Method 9056A WG1901917 1 07127/2218:21 07/27/2218:21 LBR Mt. Juliet, TN Wet Chemistry by Method 9060A WG1908434 1 08/24/2218:57 08/24/2218:57 SJF Mt. Juliet, TN ° Cn Collected by Collected date/time Received date/time MW-8 L1518975-07 GWAric Clark 07/26/22 10:54 07/27/22 09 00 FSr Method Batch Dilution Preparation Analysis Analyst Location date/time date/time F Gravimetric Analysis by Method 2540 C-2011 WG1903892 1 08/01/2216:18 08/01/2217:14 MMF Mt. Juliet, TN Wet Chemistry by Method 350.1 WG1903509 1 08/01/2213:18 08/01/2213:18 SL Mt. Juliet, TN G� Wet Chemistry by Method 365.4 WG1907961 1 07/29/2218:48 08/09/2213:34 LDT Mt. Juliet, TN Wet Chemistry by Method 9056A WG1901917 1 07/27/22 19:06 07127/2219:06 LBR Mt. Juliet, TN aAl Wet Chemistry by Method 9060A WG1908434 1 08/24/2219:13 08/24/2219:13 SJF Mt. Juliet, TN Collected by Collected date/time Received date/time FC MW-9 L1518975-08 GW Aric Clark 07/26/2211:40 07/27/2209:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Gravimetric Analysis by Method 2540 C-2011 WG1903892 1 08/01/2216:18 08/01/2217:14 MMF Mt. Juliet, TN Wet Chemistry by Method 350.1 WG1903509 1 08/01/2213:21 08/01/2213:21 SL Mt. Juliet, TN Wet Chemistry by Method 365.4 WG1907961 1 07/29/22 1848 08/09/2213:36 LDT Mt. Juliet, TN Wet Chemistry by Method 9056A WG1901896 1 07/27/2218:01 07/27/22 18:01 LBR Mt. Juliet, TN Wet Chemistry by Method 9060A WG1908434 1 08/24/2219:29 08/24/2219:29 SJF Mt. Juliet, TN Collected by Collected date/time Received date/time MW-10 L1518975-09 GW Aric Clark 07/26/2211:15 07/27/2209:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Gravimetric Analysis by Method 2540 C-2011 WG1903892 1 08/01/2216:18 08/01/2217:14 MMF Mt. Juliet, TN Wet Chemistry by Method 350.1 WG1903509 1 08/01/2213:24 08/01/2213:24 SL Mt. Juliet, TN Wet Chemistry by Method 365.4 WG1907961 1 07/29/2218:48 08/09/2213:37 LDT Mt. Juliet, TN Wet Chemistry by Method 9056A WG1901896 1 07/27/2219:06 07/27/2219:06 LBR Mt. Juliet, TN Wet Chemistry by Method 9060A WG1908434 1 08/24/2219:49 08/24/2219:49 SJF Mt. Juliet, TN Collected by Collected date/time Received date/time M W-11 L1518975-10 GW Aric Clark 07/26/221155 07/27/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Gravimetric Analysis by Method 2540 C-2011 WG1904219 1 08/02/2216:08 08/02/2217:07 MMF Mt. Juliet, TN Wet Chemistry by Method 350.1 WG1903509 1 08/01/2213:25 08/01/2213:25 SL Mt. Juliet, TN Wet Chemistry by Method 365.4 WG1907961 1 07/29/2218:48 08/09/2213:38 LDT Mt. Juliet, TN Wet Chemistry by Method 9056A WG1901896 1 07/27/2219:21 07/27/2219:21 LBR Mt. Juliet, TN Wet Chemistry by Method 9060A WG1908434 1 08/24/22 20:04 08/24/22 20:04 SJF Mt. Juliet, TN ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EHC, Inc. 17-MI0101-1 L1518975 08/26/22 11:40 4 of 36 SAMPLE SUMMARY Collected by Collected date/time Received date/time MW-12 L1518975-11 GW Aric Clark 07/26/2212:20 07/27/2209:00� Method Gravimetric Analysis by Method 2540 C-2011 Wet Chemistry by Method 350.1 Wet Chemistry by Method 365.4 Wet Chemistry by Method 9056A Wet Chemistry by Method 9060A Batch Dilution Preparation date/time W G1903892 1 08/01/2216:18 W G1903509 1 08/01/2213:27 WG1910412 1 07/30/22 07:39 WG1901896 1 07/27/2219:36 WG1908434 1 08/24/22 20:20 Analysis Analyst Location date/time 08/01/22 17:14 MMF Mt. Juliet, TN 08/01/2213:27 SL Mt. Juliet, TN 08/13/2213:03 LDT Mt. Juliet, TN 07/2712219:36 LBR Mt. Juliet, TN 08/24/22 20:20 SJF Mt. Juliet, TN ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: FHC, Inc. 17-MI0101-1 L1518975 08/26/22 11:40 5 of 36 CASE NARRATIVE 1 El All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within Z the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples Tc have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form 3Ss or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. Fsr 6 QC 7G1 Heather J Wagner eAl Project Manager BSc Project Narrative Method 906OA: The TOC analysis was performed out of hold on all samples due to laboratory error. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EHC, Inc. 17-MI0101-1 L1518975 08/26/22 11:40 6 of 36 SAMPLE RESULTS - 01 IMW-1 ollected date/time: 07/26/22 09:37 L1518975 Additional Information - Results for field analyses are not accredited to ISO 17025 Result Units 17p] Analyte z pH (On Site) 5 74 su TC Temperature (on -site) 23.5 Deg C 3Ss Gravimetric Analysis by Method 2540 C-2011 Result Qualifier ROL Dilution Analysis Batch Fn Analyte mg/I mg/I date / time Dissolved Solids 107 10.0 1 08/01/202217:14 WG1903892 Wet Chemistry by Method 350.1 Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time Ammonia Nitrogen NO 0.250 1 08/01/202213.04 WG1903509 Wet Chemistry by Method 365.4 Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time Phosphorus,Total NO 0.100 1 08/09/202213 24 WG1907961 Wet Chemistry by Method 9056A Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time Chloride 46.9 1.00 1 07/27/2022 23 31 WG1901570 Nitrate 3.83 0.100 1 07/27/2022 23:31 WG1901570 Wet Chemistry by Method 9060A Result Qualifier RDL Analyte mg/! mg/I TOC (Total Organic Carbon) 1.04 B Q 1.00 Dilution Analysis Batch date / time 1 08/24/202216.55 WG1908434 ACCOUNT: EHC, Inc. PROJECT: SDG: DATE/TIME: PAGE: 17-MI0101-1 US18975 08/26/22 11:40 7 of 36 :i� t u��i�Er+i�frsd�ts F itir►t1'Rrsi���V �MlWteddate/time 07/26/220915 SAMPLE RL15ESULTS - 02 975 Additional Information - Results for field analyses are not accredited to ISO 17025 Result Units Analyte pH (On Site) 6.6 su Temperature (on -site) 271 Deg C Gravimetric Analysis by Method 2540 C-2011 Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / Lime Dissolved Solids 379 10.0 1 08/01/202218:51 WG1903896 Wet Chemistry by Method 350.1 Result Qualifier RDL Dilution Analysis Batch Analyte mg/! mg/I date / time Ammonia Nitrogen 3.84 0.250 1 08/01/202213:06 WG1903509 Wet Chemistry by Method 365.4 Result Qualifier RDL Dilution Analysis Batch Analyte mg/1 mg/I date / time Phosphorus,Total NO 0.100 1 08/09/202213:26 WG1907961 Wet Chemistry by Method 9056A Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time Chloride 135 1.00 1 07/27/2022 23:44 WG1901570 Nitrate 0299 0.100 1 07/27/2022 23-44 WG1901570 Wet Chemistry by Method 9060A Analyte TOC (Total Organic Carbon) Result Qualifier RDL Dilution Analysis Batch mg/I mg/I date / time 5,11 0 1,00 1 08/24/202217.12 WG1908434 ACCOUNT: EHC, Inc. PROJECT: SDG: DATE/TIME: PAGE: 17-MI0101-1 L1518975 08/26/22 1140 8 of 36 AMW-3A SAMPLE RESULTS - 03 Collected date/time: 07/26/22 08:50 L1518975 Additional Information - Results for field analyses are not accredited to ISO 17025 Result Units Analyte PH (On Site) 5.3 Su Temperature (on -site) 22.7 Deg C Gravimetric Analysis by Method 2540 C-2011 Result Qualifier RDL Dilution Analysis Batch Analyte mgA Mg/1 date / time Dissolved Solids 106 100 1 08/01/202218:51 WG1903896 Wet Chemistry by Method 350.1 Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/1 date / time Ammonia Nitrogen ND 0.250 1 08/01/202213:07 WG1903509 Wet Chemistry by Method 365.4 Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time Phosphorus,Total ND 0.100 1 08/09/202213:27 WG1907961 Wet Chemistry by Method 9056A Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time Chloride 37.3 1.00 1 07/27/2022 23:58 WG1901570 Nitrate 1.43 0.100 1 07/27/2022 23:58 WG1901570 Wet Chemistry by Method 9060A Result Qualifier RDL Analyte mgA Mg/ TOC (Total Organic Carbon) 1.14 B 0 1 00 Dilution Analysis Batch date / time 1 08/24/202217:28 WG1908434 ACCOUNT: EHC, Inc. PROJECT: SDG: DATE/TIME: PAGE: 17-MI0101-1 L1518975 08/26/22 11:40 9 of 36 ra yra:anum�•nnawrarira¢eexn�:r,. MW-4 SAMPLE RESULTS - 04 a Collected date/time: 07/26/22 09:45 L1518975 Additional Information - Results for field analyses are not accredited to ISO 17025 Result Units Analyte pH (On Site) 6.5 su Temperature (on -site) 21.2 Deg C Gravimetric Analysis by Method 2540 C-2011 Result Qualifier ROL Dilution Analysis Batch Analyte mg/I mg/I date / time Dissolved Solids 280 10.0 1 08/01/202217:14 WG1903892 Wet Chemistry by Method 350.1 Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time Ammonia Nitrogen ND 0.250 1 08/01/2022 13:09 WG1903509 Wet Chemistry by Method 365.4 Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time Phosphorus,Total NO 0.100 1 08/09/202213:28 WG1907961 Wet Chemistry by Method 9O56A Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg," date / time Chloride 95.7 5.00 5 07/27/202217:52 WG1901917 Nitrate 11.1 0.500 5 07/27/202217:52 WG1901917 Wet Chemistry by Method 906OA Result Qualifier RDL Dilution Analysis Batch Analyte - mg/I mg/' date / time TOC (Total Organic Carbon) 1.53 B Q 100 1 08/24/202218:25 WG1908434 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EHC, Inc 17-MI0101-1 L1518975 08/26/22 11 40 10 of 36 .MW-5 SAMPLE RESULTS - 05 Collected date/time: 07/26/22 10:31 L1518975 Additional Information - Results for field analyses are not accredited to ISO 17025 Result Units Analyte pH (On Site) 6.7 su Temperature (on -site) 22.5 Deg C Gravimetric Analysis by Method 2540 C-2011 Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time Dissolved Solids 261 10.0 1 08/011202218:51 WG1903896 Wet Chemistry by Method 350.1 Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/1 date / time Ammonia Nitrogen NO 0.250 1 08/01/202213:10 WG1903509 Wet Chemistry by Method 365.4 Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time Phosphorusjotal NO 0.100 1 08109/202213:32 WG1907961 Wet Chemistry by Method 9056A Result Qualifier RDL Dilution Analysis Batch Analyte Mg/1 mg/1 date / time Chloride 85.5 5.00 5 07/27/202218:06 WG1901917 Nitrate 13.4 0.500 5 07/27/202218:06 WG1901917 Wet Chemistry by Method 9060A Result Qualifier RDL Analyte mg/1 mg/l TOC (Total Organic Carbon) 1.53 B Q 1.00 Dilution Analysis Batch date / time 1 08/24/202218:41 WG1908434 ACCOUNT: EHC. Inc. PROJECT: SDG: DATEMME: PAGE: 17-MI0101-1 L1518975 08/26/22 11:40 11 of 36 MW-6 SAMPLE RESULTS - 06 Collected date/time: 07/26/22 10:14 L1518975 Additional Information - Results for field analyses are not accredited to ISO 17025 Result Units Col Analyte Fc pH (On Site) 5.67 su Temperature (on -site) 22.8 Deg C FS Gravimetric Analysis by Method 2540 C-2011 Result Qualifier ROL Dilution Analysis Batch Analyte mg/I mg/I date / time FCn] Dissolved Solids 212 T8 10.0 1 08/09/202217:35 WG1908160 Wet Chemistry by Method 350.1 Result Qualifier RDL Dilution Analysis Batch QC Analyte mg/I mgA date / time Ammonia Nitrogen ND 0.250 1 08/011202213:12 WG1903509 [G] Wet Chemistry by Method 365.4 e Result Qualifier RDL Dilution Analysis Batch [Al Analyte mg/I mg/I date / time Phosphorusjotal NO 0.100 1 08/09/2022 13:33 WG1907961 FC1 Wet Chemistry by Method 9056A Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time Chloride 107 1.00 1 07/27/202218:21 WG1901917 Nitrate 2.21 0.100 1 07127/202218:21 WG1901917 Wet Chemistry by Method 9060A Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time TOC (Total Organic Carbon) 1.33 8 Q 1.00 1 08/24/202218:57 WG1908434 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EHC, Inc. 17-MI0101-1 L1518975 08/26/22 11:40 12 of 36 MW-8 SAMPLE RESULTS - 07 Collected date/time: 07/26/22 10:54 L1518975 Additional Information - Results for field analyses are not accredited to ISO 17025 Result Units C� Analyte PH (On Site) 6.44 su F Temperature (on -site) 23.3 Deg C FS Gravimetric Analysis by Method 2540 C-2011 Result Qualifier ROL Dilution Analysis Batch Fln Analyte mg/I mg/I date / time Dissolved Solids 91.0 10.0 1 08/01/202217:14 WG1903892 Wet Chemistry by Method 350.1 QC r Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time Ammonia Nitrogen NO 0.250 1 08/011202213:18 WG1903509 Fil Wet Chemistry by Method 365.4 Oualifier RDL Dilution Analysis Batch FAIResult Analyte mg/I mg/1 date / time Phosphorus,Total NO 0.100 1 08/09/202213:34 WG1907961 FC Wet Chemistry by Method 9056A Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/1 date / time Chloride 28.0 1.00 1 07/27/202219:06 WG1901917 Nitrate 5.37 0.100 1 07/27/202219:06 WG1901917 Wet Chemistry by Method 9060A Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time TOC (Total Organic Carbon) 1.55 B Q 1.00 1 08/24/202219:13 WG1908434 ACCOUNT: PROJECT: SDG: DATEITIME: PAGE: EHC, Inc. 17-MI0101-1 L1518975 08/26/2211:40 13 of 36 MW-9 SAMPLE RESULTS - 08 Collected date/time: 07/26/22 11:40 L1518975 Additional Information - Results for field analyses are not accredited to ISO 17025 Result Units F P1 Analyte z pH (On Site) 6.03 su TC Temperature (on -site) 23.6 Deg C FS Gravimetric Analysis by Method 2540 C-2011 Result Qualifier ROL Dilution Analysis Batch Analyte mg/I mg/I date / time Fnj Dissolved Solids 91.0 10.0 1 08/011202217:14 WG1903892 Wet Chemistry by Method 350.1 n�C Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time Ammonia Nitrogen ND 0.250 1 08101/202213:21 WG1903509 [Gl Wet Chemistry by Method 365.4 a Result Qualifier RDL Dilution Analysis Batch A Analyte mg/I mg/I date / time r Phosphorus,Total NO 0.100 1 08/091202213:36 WG1907961 qc Wet Chemistry by Method 9056A Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time Chloride 16.9 1.00 1 07127/202218:01 WG1901896 Nitrate 9.88 0.100 1 07/27/202218:01 WG1901896 Wet Chemistry by Method 9060A Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time TOC (Total Organic Carbon) 1.46 B Q 1.00 1 08/241202219:29 WG1908434 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EHC, Inc. 17-MI0101-1 L1518975 08/26/22 11:40 14 of 36 { MW-10 SAMPLE RESULTS - 09 Collected date/time: 07/26/22 11:15 L1518975 Additional Information - Results for field analyses are not accredited to ISO 17025 Result Units 7-P Analyte pH (On Site) 546 su FC1 Temperature (on -site) 23.6 Deg C FS Gravimetric Analysis by Method 2540 C-2011 Result Qualifier RDL Dilution Analysis Batch Analyte mg/1 mg/I date / time Fn Dissolved Solids 267 10.0 1 08/01/202217:14 WG1903892 Wet Chemistry by Method 350.1 Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/1 date / time Ammonia Nitrogen ND 0 250 1 08/01/202213:24 WG1903509 Wet Chemistry by Method 365.4 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/I date / time Phosphorus,Total ND 0.100 1 08/09/202213:37 WG1907961 Wet Chemistry by Method 9056A Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time Chloride 113 1.00 1 07/27/202219:06 WG1901896 Nitrate 6.59 0,100 1 07/27/202219:06 WG1901896 Wet Chemistry by Method 9060A Analyte TOC (Total Organic Carbon) Result Qualifier RDL Dilution Analysis Batch mg/1 mg/I date / time 2.15 3 Q 1.00 1 08/24/202219:49 WG1908434 ACCOUNT: EHC, Inc. PROJECT: SDG: DATE/TIME: PAGE: 17-MI0101-1 L1518975 08/26/22 11:40 15 of 36 MW-11 SAMPLE RESULTS - 10 Collected date/time: 07/26/22 11:55 L1518975 Additional Information - Results for field analyses are not accredited to ISO 17025 Result Units Analyte pH (On Site) 6.45 su Temperature (on -site) 23.2 Deg C Gravimetric Analysis by Method 2540 C-2011 Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time Dissolved Solids 86.0 10.0 1 08/02/202217:07 WG1904219 Wet Chemistry by Method 350.1 Result Qualifier Analyte mg/1 Ammonia Nitrogen NO Wet Chemistry by Method 365.4 RDL mg/I 0.250 Dilution 1 Analysis date / time 08/01/202213:25 Batch WG1903509 Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/1 date / time Phosphorus,Total ND 0.100 1 08/09/202213:38 WG1907961 Wet Chemistry by Method 9056A Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time Chloride 27.9 1.00 1 07/27/202219:21 WG1901896 Nitrate 4.85 0.100 1 07/27/202219:21 WG1901896 Wet Chemistry by Method 9060A Result Qualifier RDL Analyte mg/I mg/I TOC (Total Organic Carbon) 2.81 BB Q 1.00 Dilution Analysis Batch date / time 1 08/24/2022 20:04 WG1908434 ACCOUNT: EHC, Inc. PROJECT: SDG: DATE/TIME: PAGE: 17-MI0101-1 L1518975 08/26/22 11:40 16 of 36 MW-12 SAMPLE RESULTS - 11 Collected date/time: 07/26/22 12:20 L1518975 Additional Information - Results for field analyses are not accredited to ISO 17025 Result Units Analyte e pH (On Site) 5.97 su TC Temperature (on -site) 22.1 Deg C Gravimetric Method 2540 C-2011 FS Analysis by Result Qualifier ROL Dilution Analysis Batch Analyte mg/I mg/I date / time FCn] Dissolved Solids 269 10.0 1 08/01/202217:14 WG1903892 0 Wet Chemistry by Method 350.1 Result Qualifier RDL Dilution Analysis Batch F Analyte mg/1 mg/I date / time Ammonia Nitrogen NO 0.250 1 08/01/2022 1327 WG1903509 F11 Wet Chemistry by Method 365.4 Result Qualifier RDL Dilution Analysis Batch FA Analyte mgA mg/I date / time Phosphorus,Total ND 0.100 1 08/13/202213:03 WG1910412 FC Wet Chemistry by Method 9056A Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time Chloride 102 1.00 1 07/27/202219:36 WG1901896 Nitrate 11.3 0.100 1 07/27/202219:36 WG1901896 Wet Chemistry by Method 9060A Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time TOC (Total Organic Carbon) 2.31 8 Q 1.00 1 08/24/2022 20:20 WG1908434 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EHC, Inc. 17-MI0101-1 L1518975 08/26/22 11:40 17 of 36 WG1903892 QUALITY CONTROL SUMMARY Gravimetric Analysis by Method 2540 C-2011 L1518975-01,04,07,08,09,11 Method Blank (MB) C (MB) R3823852-1 08/01/22 17:14 MB Result Analyte mg/I Dissolved Solids U MB Qualifier MB MDL MB RDL mg/I mg/I 10.0 10.0 L1518742-01 Original Sample (OS) • Duplicate (DUP) (OS) L1518742-01 08/01/22 17:14 • (DUP) R3823852-3 08/01/22 17-14 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/I mg/I % % Dissolved Solids 1960 2110 1 7.63 J3 5 L1518876-02 Original Sample (OS) • Duplicate (DUP) (OS) L1518876-02 08/01/22 1714 • (DUP) R3823852-4 08/01/22 17:14 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/I mg/I % % Dissolved Solids 311 311 1 0.000 5 Laboratory Control Sample (LCS) (LCS) R3823852-2 08/01/22 17:14 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I % % Dissolved Solids 8800 8400 95.5 77.3-123 ACCOUNT: PROJECT: SDG: EHC,Inc. 17-MI0101-1 L1518975 DATE/TIME: 08/26/22 11:40 PAGE: 18 of 36 a f1.9tt?tMF�'fiflrtf�llt�#3.IttFlt�ad3'�`1•c WG1903896 QUALITY CONTROL SUMMARY Gravimetric Analysis by Method 2540 C-2011 1-1518975-02,03,05 Method Blank (MB) (MB) R3824167-1 08/01/22 18:51 — - _-- Cp MB Result MB Qualifier MB MOIL MB ROL FTAnalyte mg/I mg/I mg/I Dissolved Solids U 10.0 10.0 L1518713-01 Original Sample (OS) • Duplicate (DUP) (0S) L1518713-01 08/01/22 18:51 • (DUP) R3824167-3 08/01/22 18:51 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/I mg/I % % Dissolved Solids 333 326 1 2.12 5 L1519823-02 Original Sample (OS) • Duplicate (DUP) (OS) L1519823-02 08/01/22 18:51 • (DUP) R3824167-4 08/01/22 18:51 Original Result DUP Result Dilution DUP RPD DUP Oualifier DUP RPD Limits Analyte mg/I mg/I % % Dissolved Solids 982 1070 1 8.58 J3 5 Laboratory Control Sample (LCS) (LCS) R3824167-2 08/01/22 18:51 Spike Amount LCS Result LCS Rec. Rec. Limits Analyte mg/1 mg/I % % Dissolved Solids 8800 7380 83.9 77.3-123 LCS Qualifier FS Cn Fr Fil Fil FSCI ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EHC, Inc. 17-MI0101-1 L1518975 08/26/22 11:40 19 of 36 WG1904219 QUALITY CONTROL SUMMARY Gravimetric Analysis by Method 2540 C-2011 L1518975-10 Method Blank (MB) (MB) R3824192-1 08/02/22 17-07 MB Result Analyte mg/I Dissolved Solids U MB Qualifier MB MDL MB RDL mg/I mg/I 10.0 10.0 L1518854-01 Original Sample (OS) • Duplicate (DUP) (OS) L1518854-01 08/02/22 17:07 • (DUP) R3824192-3 08/02/22 17:07 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/I mg/I % % Dissolved Solids 681 676 1 0.785 5 L1518854-02 Original Sample (OS) • Duplicate (DUP) (OS) L1518854-02 08/02/22 17:07 • (DUP) R3824192-4 08/02/22 17:07 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/I mg/I % % Dissolved Solids 806 792 1 1.75 5 Laboratory Control Sample (LCS) (LCS) R3824192-2 08/02/22 17:07 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I % % Dissolved Solids 8800 8100 92.0 77.3-123 ACCOUNT: PROJECT: SDG: EHC, Inc. 17-MI0101-1 L1518975 DATE/TIME: 08/26/2211:40 PAGE: 20 of 36 WG1908160 QUALITY CONTROL SUMMARY Gravimetric Analysis by Method 2540 C-2011 L1518975-06 , Method Blank (MB) (MB) R3825713-1 08/09/22 17:35 MB Result Analyte mg/I Dissolved Solids U MB Qualifier MB MOIL MB RDL mg/I mg/I 10.0 10.0 L1512599-01 Original Sample (OS) • Duplicate (DUP) (OS) L1512599-01 08/09/22 17:35 • (DUP) R3825713-3 08/09/22 17:35 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/I mg/I % % Dissolved Solids 1140 1170 1 2.77 5 Laboratory Control Sample (LCS) (LCS) R3825713-2 08/09/22 17:35 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I % % Dissolved Solids 8800 8300 94.3 77.3-123 ACCOUNT: PROJECT: SDG: EHC, Inc. 17-MI0101-1 L1518975 DATE/TIME: 08/26/22 11:40 PAGE: 21 of 36 WG1903509 QUALITY CONTROL SUMMARY Wet Chemistry by Method 350.1 L1518975-01,02,03,04,05,06,07,08,09 10 11 Method Blank (MB) (MB) R3821385-1 08/01/2212:39 FP1 M8 Result MB Qualifier MB MDL MB RDL 2 Analyte mg/t mg/l mg/I TC Ammonia Nitrogen U 0.117 0.250 L1518876-02 Original Sample (OS) - Duplicate (DUP) (OS) L1518876-02 08/01/22 12:46 - (DUP) R3821385-5 08/01/22 12:48 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/I mg/I % % Ammonia Nitrogen NO ND 1 0.000 10 L1518975-08 Original Sample (OS) • Duplicate (DUP) (OS) L1518975-08 08/01/22 13:21 - (DUP) R3821385-7 08/01/22 13:22 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/I mg/I % % Ammonia Nitrogen NO ND 1 0.000 10 Laboratory Control Sample (LCS) (LCS) R3821385-2 08/01/22 12:40 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I % % Ammonia Nitrogen 7.50 7.47 SIM 90.0-110 L1518876-01 Original Sample (OS) - Matrix Spike (MS) - Matrix Spike Duplicate (MSD) (OS) L1518876-01 08/01/22 12:42 - (MS) R3821385-3 08/01/22 12:43 - (MSD) R3821385-4 08/01/22 12:45 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I mg/I % % % % % Ammonia Nitrogen 5.00 ND 4.96 5.03 99.1 101 1 90.0-110 1.38 10 L1518975-07 Original Sample (OS) - Matrix Spike (MS) (OS) L1518975-07 08/01/2213:18 - (MS) R3821385-6 08/01/2213:19 Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier Analyte mg/I mg/I mg/I % % Ammonia Nitrogen 5,00 ND 4.88 97.7 1 90.0-110 ACCOUNT: PROJECT: SDG: DATE7TIME: PAGE: EHC, Inc. 17-MI0101-1 L1518975 08/26/22 11:40 22 of 36 WG1907961 QUALITY CONTROL SUMMARY Wet Chemistry by Method 365.4 L1518975-01,02,03,04,05,06,07,08,09,10 Method Blank (MB) (M8) R3824214-1 08/09/22 13:17 MB Result MB Qualifier MB MOIL MB RDL F(I Analyte mg/I mg/I mg/1 Phosphorusjotal U 0.0350 0.100 L1519045-01 Original Sample (OS) • Duplicate (DUP) (0S) L1519045-01 08/09/22 13:40 • (DUP) R3824214-3 08/09/22 13:41 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/I mg/I % % Phosphorus,Total ND NO 1 2.85 20 L1519045-02 Original Sample (OS) • Duplicate (DUP) (OS) L1519045-02 08/09/22 13:47 • (DUP) R3824214-6 08/09/2213:48 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/1 mg/I % % Phosphorus,Total 1.83 1.80 1 1.65 20 Laboratory Control Sample (LCS) (LCS) R3824214-2 08/09/22 13:18 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I % % Phosphorus,Total 3.78 3.74 98.9 83.2-116 L1519045-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1519045-01 08/09/22 13:40 • (MS) R3824214-4 08/09/22 13:42 • (MSD) R3824214-5 08/09/22 13:43 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD Analyte mg/I mg/I mg/I mg/I % % % % Phosphorus,Total 2.50 ND 2.48 2.43 95.6 93.6 1 90,0110 2.04 RPD Limits 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EHC, Inc. 17-MI0101-1 L1518975 08/26/2211:40 23 of 36 WG1910412 QUALITY CONTROL SUMMARY Wet Chemistry by Method 365.4 L1518975-11 MethOd 6ianK (MB) (MB) R3825942-1 08/13/22 13:01 MB Result Analyte mg/I Phosphorus,Total U MB Qualifier MB MDL MB RDL mg/I mg/I 0.0350 0,100 L1519049-02 Original Sample (OS) • Duplicate (DUP) (OS) L1519049-02 08/13/22 13:08 • (DUP) R3825942-3 08/13/2213:10 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/I mg/I % % Phosphorus,Total 0.177 0.169 1 4.62 20 Laboratory Control Sample (LCS) (LCS) R3825942-2 08/13/2213:02 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I % % Phosphor us,Tola1 3.78 3.48 921 83.2116 L1519049-02 Original Sample (US) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1519049-02 08/13/2213:08 • (MS) R3825942-4 08/13/2213:11 • (MSD) R3825942-5 08/13/221312 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD Analyte mg/1 mg/I mg/I mg/I % % % % Phosphorusjotal 2.50 0.177 2.57 2.50 95.7 92.9 1 90.0110 2.76 RPD Limits 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EHC, Inc. 17-MI0101-1 L1518975 08/26/22 11:40 24 of 36 WG1901570 QUALITY CONTROL SUMMARY Wet Chemistry by Method 9056A L1518975-01,02,03 Method Blank (MB) (MB) R3820440-1 07/27/22 10:13 C i) MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/I Ec Chloride U 0.379 1.00 Nitrate U 0.0480 0.100 rSS1 L1518856-02 Original Sample (OS) • Duplicate (DUP) FCn] (OS) L1518856-02 07/27/22 12:26 • (DUP) R3820440-3 07/27/22 12:40 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits s Sr Analyte mg/I mg/I % % Chloride 1.12 1.08 1 3.40 15 Nitrate 0.639 0.619 1 3.16 15 [GI L1518839-01 Original Sample (OS) • Duplicate (DUP) (0,S) L1518839-01 07/27/22 11:24 • (DUP) R3820440-4 07/27/22 16:09 FAI Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/I mg/I % % FSCI Chloride 20.9 20.4 1 2.24 15 Nitrate 5.09 4.96 1 2.64 15 L1518854-04 Original Sample (OS) • Duplicate (DUP) (OS) L1518854-04 07/27/22 22:37 • (DUP) R3820440-9 07/27/22 22:51 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/I mg/I % % Chloride 79.7 80.1 1 0.536 15 Nitrate 2.52 2.51 1 0.390 15 Laboratory Control Sample (LCS) (LCS) R3820440-2 07/27/22 10.27 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I % % Chloride 40.0 40.3 101 80.0-120 Nitrate 8.00 7.95 99.3 80.0-120 ACCOUNT: PROJECT: SDG: EHC. Inc. 17-MI0101-1 L1518975 DATE/TIME: O8/26/22 11:40 PAGE: 25 of 36 WG1901570 QUALITY CONTROL SUMMARY { Wet Chemistry by Method 9056A L1518975-01,02,03 L1518839-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1518839-01 07/27/22 11:24 • (MS) R3820440-5 07/27/22 16:22 • (MSD) R3820440-6 07/27/22 17:02 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I mg/I % % % % % ITC Chloride 50.0 20.9 72.6 70.0 103 98.3 1 80.0-120 3.66 15 Nitrate 5.00 5.09 10.2 9.81 102 94.5 1 80.0-120 3.94 15 3 L1518854-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1518854-01 07/27/22 20:23 • (MS) R3820440-7 07/27/22 20:50 • (MSD) R3820440-8 07/27/22 21:03 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I mg/I % % % % % Chloride 50.0 5.81 57.1 57.8 103 104 1 80.0-120 1.12 15 Nitrate 5.00 3.43 8.53 8.60 102 103 1 80.0-120 0.800 15 ACCOUNT: PROJECT: SDG: EHC, Inc. 17-MI0101-1 L1518975 DATE/TIME: 08/26/22 11:40 PAGE: 26 of 36 WG1901896 QUALITY CONTROL SUMMARY Wet Chemistry by Method 9056A L1518975-08,09,10,11 Method Blank (MB) (MB) R3820390-1 07/27/22 17:32 MB Result MB Qualifier MB MDL M8 RDL Analyte mg/I mg/I mg/I Chloride U 0.379 1.00 Nitrate 0,0515 1 0.0480 0.100 L1518975-08 Original Sample (OS) • Duplicate (DUP) (OS) L1518975-08 07/27/2218:01 • (DUP) R3820390-3 07/27/22 18:16 Original Result DUP Result Dilution DUP RPD Analyte mg/I mg/I % Chloride 16.9 16.9 1 0.0498 Nitrate 9.88 9.89 1 0.0991 L1518975-11 Original Sample (OS) • Duplicate (DUP) DUP Qualifier DUP RPD Limits 15 15 (OS) L1518975-11 07/27/22 19:36 • (DUP) R3820390-6 07/28/22 05:47 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/I mg/I % % Chloride 102 104 1 1.63 15 Nitrate 11.3 11.5 1 1.13 15 Laboratory Control Sample (LCS) (LCS) R3820390-2 07/27/22 17:46 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I % % Chloride 40.0 38.7 96.8 80.0-120 Nitrate 8.00 7.69 96.2 80.0-120 L1518975-08 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1518975-08 07/27/22 18:01 • (MS) R3820390-4 07/27/22 18:37 • (MSD) R3820390-5 07/27/2218:51 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I mg/I % % % % % Chloride 50.0 16.9 67.6 67.8 101 102 1 80.0-120 0.291 15 Nitrate 5.00 9.88 14.8 14.8 98.1 97.8 1 80.0-120 0.0819 15 L Ec F Fnj 5Sr �GI eAl BSc ACCOUNT: PROJECT: SDG: EHC,Inc. 17-MI0101-1 L1518975 DATE/TIME: 08/26/22 11:40 PAGE: 27 of 36 WG1901896 QUALITY CONTROL SUMMARY Wet Chemistry by Method 9056A L1518975-08,09,10,11 L1518975-11 Original Sample (OS) • Matrix Spike (MS) (OS) L1518975-11 07/27/22 19:36 • (MS) R3820390-7 07/28/22 06:02 Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier Analyte mg/I mg/I mg/I % % Chloride 50.0 102 152 99.8 1 80.0-120 Nitrate 5.00 11.3 16.4 102 1 80.0-120 ACCOUNT: PROJECT: EHC, Inc. 17-MI0101-1 SDG: L1518975 DATE/TIME: 08/26/22 11:40 PAGE: 28 of 36 WG1901917 QUALITY CONTROL SUMMARY Wet Chemistry by Method 9056A L1518975-04,05,06,07 Method Blank (MB) (MB) R3820250-1 07/27/22 1230 Cp MB Result MB Qualifier MB MDL Analyte mg/I mg/I MB RDL mg/i rTC1 Chloride U 0.379 1.00 Nitrate 0.0758 J 0.0480 0.100 FS L1518975-07 Original Sample (OS) • Duplicate (DUP) FCn] (OS) L1518975-07 07/27/2219:06 • (DUP) R3820250-5 07/27/2219:21 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits 5 $r Analyte mg/I mg/I % % Chloride 28.0 28.2 1 0.636 15 Nitrate 5.37 5.39 1 0.427 15 �Gt Laboratory Control Sample (LCS) e/al (LCS) R3820250-2 07/27/22 12:45 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I % % FSCI Chloride 40.0 40.4 101 80.0120 Nitrate 8.00 8.09 101 80.0-120 L1518975-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1518975-06 07/27/2218:21 , (MS) R3820250-3 07/27/2218:36 • (MSD) R3820250-4 07/27/2218:51 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I mg/I % % % % % Chloride 50.0 107 153 154 92.0 94.4 1 80.0-120 0.774 15 Nitrate 5.00 2.21 7.40 7.45 104 105 1 80.0-120 0.661 15 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EHC, Inc. 17-MI0101-1 L 1518975 08/26/2211:40 29 of 36 WG1908434 QUALITY CONTROL SUMMARY Wet Chemistry by Method 9060A L1518975-01,02,03,04,05,06,07,08,09,10,11 Method Blank (MB) (MB) R3830312-2 08/24/22 11:51 MB Result MB Qualifier MB MDL MB ROL Analyte mg/I mg/I mg/I TC TOC (Total Organic Carbon) 0.315 J 0.102 1.00 L1518716-01 Original Sample (OS) • Duplicate (DUP) (OS) L1518716-01 08/24/22 15:16 • (DUP) R3830312-3 08/24/2215:32 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/I mg/I % % TOC (rota) Organic Carbon) 2.35 2.67 1 12.8 20 L1518717-04 Original Sample (OS) • Duplicate (DUP) (OS) L1518717-04 08/24/22 15:50 • (DUP) R3830312A 08/24/22 16:22 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/I mg/I % % TOC (Total Organic Carbon) 5.52 4.69 1 16.1 20 Laboratory Control Sample (LCS) (LCS) R3830312-1 08/24/22 11:35 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I % % TOC (Total Organic Carbon) 75.0 74.2 98.9 85.0-115 L1518975-11 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1518975-11 08/24/22 20:20 • (MS) R3830312-5 08/24/22 20:45 • (MSD) R3830312-6 08/24/22 21:48 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I mg/I % % % % % TOC (Total Organic Carbon) 50.0 2.31 58.5 59.6 112 115 1 80.0-120 1.90 20 L1519056-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1519056-02 08/24/22 22:52 • (MS) R3830312-7 08/24/22 23:18 • (MSD) R3830312-8 08/24/22 23:44 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I mg/I % % % % % TOC (Total Organic Carbon) 50.0 1.12 58.4 58.6 114 115 1 80.0-120 0.393 20 ACCOUNT: PROJECT: SDG: EHC,Inc. 17-MI0101-1 L1518975 DATE/TIME: 08/26/22 11:40 PAGE: 30 of 36 GLOSSARY OF TERMS Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative. Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received. Abbreviations and Definitions MDL Method Detection Limit. ND Not detected at the Reporting Limit (or MDL where applicable). RDL Reported Detection Limit Rec. Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported. Successful OC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state 'ND' (Not Detected) or 'BDL' Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry) Confidence level of 2 sigma. A brief discussion about the included sample results, including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary (Qc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. This section of your report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description B The same analyte is found in the associated blank. J The identification of the analyte is acceptable; the reported value is an estimate. J3 The associated batch OC was outside the established quality control range for precision. Q Sample was prepared and/or analyzed past holding time as defined in the method. Concentrations should be considered minimum values. T8 Sample(s) received past/too close to holding time expiration. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EHC, Inc. 17WI0101-1 L1518975 08/2612211:40 31 of36 ACCREDITATIONS & LOCATIONS Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122 Alabama 40660 Nebraska NE-OS-15-05 Alaska 17-026 Nevada TN000032021-1 Arizona AZ0612 New Hampshire 2975 Arkansas 88-0469 New Jersey—NELAP TN002 California 2932 New Mexico' TN00003 Colorado TN00003 New York 11742 Connecticut PH-0197 North Carolina Env375 Florida E87487 North Carolina' DW21704 Georgia NELAP North Carolina 41 Georgia' 923 North Dakota R-140 Idaho TN00003 Ohio—VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky " KY90010 South Carolina 84004002 Kentucky 16 South Dakota n/a Louisiana A130792 Tennessee " 2006 Louisiana LA018 Texas T104704245-20-18 Maine TN00003 Texas s LAB0152 Maryland 324 Utah TN000032021-11 Massachusetts M-TN003 Vermont VT2006 Michigan 9958 Virginia 110033 Minnesota 047-999-395 Washington C847 Mississippi TN00003 West Virginia 233 Missouri 340 Wisconsin 998093910 Montana CERT0086 Wyoming A21A A21LA — ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789 A21-A — ISO 17025 ` 1461.02 DOD 1461.01 Canada 1461.01 USDA P330-15-00234 EPA—Crypto TN00003 Drinking Water ' Underground Storage Tanks ' Aquatic Toxicity ` Chemical/Microbiological `Mold 6 Wastewater n/a Accreditation not applicable Not all certifications held by the laboratory are applicable to the results reported in the attached report. ' Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical. ACCOUNT: PROJECT: SDG: DATEfrIME: PAGE: EHC, Inc. 17-MI0101-1 L1518975 08/26/2211:40 32 of 36 `. rripany Nine/Address EHC, Inc. PO Box 902 Red Springs, NC 28377 Report to Mr. Thomas Ammons Pro}ru Descnpuor-� Campbell Soup Company pnone 910-$43-4456 Colle;tby (print) 1 Cw Collected b stgn lure . f immediately Packed on Ice Sampie ID MW-2 ,Mw 3A -.. Mw to Arw• 1 ' Mairix, SS - Sod AIR Air f - falter GW Groundwater B Bioassay wW wastewater hIW Drinking )Nate( K T Other Relingashed by (Signature) Rellnqutshed oy 5%,idtute) ftr�ivgwshed by. (Signature) i fulling Information: r — .,ter : o n,,, .,, i�nr. cr tustody Vage of ' Accounts Payable LCh PO Box 902 t o ` ,Red Springs, NC 28377 I MT JULIET, TN Email To. ehctammons@gmaiLcom,ahcjjadtsorsfgmail.co '� s/swslaNs...:. Nr1�r,YrI�MaM �sY CitylState Please Grcie Collected PT MT 2 IQ Ghent Project a Lab Project N 17-MI0101-1 ENVHYD-CAMPSELL3 a 5DG +f LA i B085 t T Site/Facility ID a P 0 n MAXTON, NC Acctrum ENVHYD — .14 _ OL Z a T I artt{ylatr T55628 Rush) (Lab MUST Be Notified) Quote sosa+ _ Same Day Give Day _ _ f rerloRin: P906326 Newt Day —,-- S Day (Rad Dnlo Date Results Needed _ �. } .C® M- ' PM' i 3 Reathlr 1 Wagner , _ Two Day _ to DaY (� t'^frl NO I � I c - O PS: Three Day of ID '- I 0 r4 sal nippVia: *1' and ed Fd G ComPlGrao Matrra • Depth_ Dale Time nos � p M — = z � a r r .,, samp4 s,r,r r'n GW Z- X X X�X X GW Ct X X X I.. X X GW D D X X X X X .^ W ■- un Jim ' ' n EW Ili �! Gw X X X X X Q� Gw X X X X X ^ -- _• — r Gw i X X X X X terrtarks.. _ Gw X. X� X X X . -- ..- !� �4 !*'IPresentilntac'- t: NV L'I! 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M Client Protect N Lab Project it IPhonr 910-843-4456 17-MI0101-1 ENVHYD-CAMPBELL3 I ( SOGa Fir fl i s Cra�Ib}, Site/Facility 10 A P O h 7dhle aMAXTON, NC lt. _ 2 I 1 Asctnum. ENVHYD Cuileded v Isrgtt• Rush? (Lab MUST Be Notified) QIIOt! N i Y uJ ! Template T5562$ r0 W t1 f Sane :lay _Five Day _.( w i Q i I Prelogin. P906326 Me.t Day _ 5 Day Iliad Oniyj Rate Re.ults Needed C z 1 bM, 873 - Heather J Wagner immediately two Wv ^ 10 0a i tkad thy) No. .� l Packed on Ice N Y _ _ Y of e� Ttuee Oa Q - — a R hippedvia. Sanpk ID Comp,•'Grab Matrix • Depth pate Time ntrs rj =f rqr a I. 1 Gw Mau,, Rernarkv /1 srmn a ke'�, t jZ<:klist N SS Sots AIR - Air f hiller Lam' J\ pH _ Temp _^ CC ' Seal Praesnt 0P /Y /lnr et �/._.'�.. COO Sign /aceut:ate _ GW Groundwater B B,oas�ay ` ` / c� FION Other Na4tlee active u.taet: H W Wastewater Cotcect Cottlaa aced: X�N OW Orinkrng Water Se'ticient voluwe sRnt: NN Samples via: T�ackir m ` Q,� /f% OT Other- UPS self. —Courier (/ L//"", � OR Zeu MaedCp * { v Rel nqunhed tri . lSignawre) Gate rime r,reu r ! , r,' :... r': 77777�7 t L, screen i 7r: C.,r raottC3:ack^;1. i�1� Sctecn <0.5 _ `-- Rettoci johed by (Signature) Date T,me, Received by (Signature) Tem�'C Bottles Rece;ved; if preservation required by Login: Date/Time Re;lnywshedby (Signature) Date. `~ Tints: Reeeivedfoajsdpy 1•Slgna T+n1e Hotel: r~^� COntti n: +)rf ) �� tit, �, i w O 24-HOUR SPILL RESPONSE NUMBER (910) 843-4456 staft Water PH Tem& Lev el 77 ENVIRONMENTAL HYDROGEOLOGICALT CONSULTANTS, INC. Data 11, 5�',7't j 3, -4 _' Field Analytical ENR Certificate 55_Ts-- mw-1 Time Sampled US EPA Lab Code # NCO 1873 NjW - DATE: - MW-3A MW-4 Client: Campbell Soup- MW Juh, 2022 mW-5 MW-6 Analyst: Aric Clark mW-8 mW-9 01( 10 G tq6 MW-10 MW-12 0 Tirackin Numbers Temperature 779�1 A W-�791 H Shipping: Maillnq: 2401 W. 5th St. PO Box 589 Lumberton NC 28358 Lumberton, NC 28359 TBL EHC ENVIRONMENTAL PO BOX 902 RED SPRINGS, NC 28377 ATTN: JOSHUA BASS SAMPLE NUMBER - 33208 DATE SAMPLED - 7-26-22 DATE RECEIVED-7-26-22 TIME RECEIVED - 1300 PAGE 1 OF 11 FINAL REPORT OF ANALYSES SAMPLE ID - MW # 1 SAMPLER - ARIC CLARK DELIVERED BY - CLIENT ANALYSIS METHOD BIOCHEMICAL OXYGEN DEMAND SM5210-B TOTAL SUSPENDED SOLIDS SM2540D AMMONIA NITROGEN SM4SOONH3D FECAL COLIFORM SM9222D CONDUCTIVITY SM2510B CHEMICAL OXYGEN DEMAND SM5220D PH SM4500 H+B VOLATILE SUSPENDED SOLIDS N/R = ANALYSIS NOT REQUESTED PROJECT NAME: REPORT DATE:7-27-22 DATE RESULT N/R N/R N/R 7/26/2022 <1 N/R N/R N/R N/R SM2540E T LABORATORY DIRECTOR Phone: 910-370-0371 Pax: 910-370-0772 Email:pam.hester- tbl hotmail.com SAMPLE MATRIX - GW TIME SAMPLED - 0937 RECEIVED BY - THK QUAL DET. UNITS CODE LIMIT MG/L 2.0 MG/L MG/L 0.1 COL/100ML 1 UMHOS/CM 10 MG/L 30.0 STD UNITS 0.1 MG/L S00 NCDENR DWQ # 37, NCDENR DW # 37781 f = Y TBL Shipping: Mailing: 2401 W. 511' St. PO Box 589 Lumberton NC 28358 Lumberton, NC 28359 EHC ENVIRONMENTAL PO BOX 902 RED SPRINGS, NC 28377 ATTN: JOSHUA BASS SAMPLE NUMBER - 33209 DATE SAMPLED - 7-26-22 DATE RECEIVED-7-26-22 TIME RECEIVED - 1300 PAGE 2 OF 11 FINAL REPORT OF ANALYSES SAMPLE ID - MW # 2 SAMPLER - ARIC CLARK DELIVERED BY - CLIENT ANALYSIS METHOD BIOCHEMICAL OXYGEN DEMAND SM5210-B TOTAL SUSPENDED SOLIDS SM2540D AMMONIA NITROGEN SM4500NH3D FECAL COLI FORM SM9222D CONDUCTIVITY SM2510B CHEMICAL OXYGEN DEMAND SM5220D PH VOLATILE SUSPENDED SOLIDS N/R = ANALYSIS NOT REQUESTED SM4500 H+B PROJECT NAME: REPORT DATE:7-27-22 DATE RESULT N/R N/R N/R 7/26/2022 <1 N/R N/R N/R Phone: 910-370-0371 Fax: 910-370-0772 Email: pam.hester- tbl hotmail.com SAMPLE MATRIX - GW TIME SAMPLED - 0915 RECEIVED BY - THK QUAL DET. UNITS CODE LIMIT MG/L 2.0 MG/L MG/L 0.1 COL/100ML 1 UMHOS/CM 10 MG/L 30.0 STD UNITS 0.1 SM2540E N/R MG/L 500 LABORATORY DIRECTOR NCDENR DWQ # 37, NCDENR DW # 37781 w TBL Shipping: Mailing: 2401 W. 51h St. PO Box 589 Lumberton NC 28358 Lumberton, NC 28359 EHC ENVIRONMENTAL PO BOX 902 RED SPRINGS, NC 28377 ATTN: JOSHUA BASS SAMPLE NUMBER - 33210 DATE SAMPLED - 7-26-22 DATE RECEIVED-7-26-22 TIME RECEIVED - 1300 PAGE 3 OF 11 FINAL REPORT OF ANALYSES SAMPLE ID - MW # 3A SAMPLER - ARIC CLARK DELIVERED BY - CLIENT PROJECT NAME: REPORT DATE:7-27-22 Phone: 910-370-0371 Fax: 910-370-0772 Email:pam.hester- tbl�hotmail.com SAMPLE MATRIX - GW TIME SAMPLED - 0850 RECEIVED BY - THK QUAL DET. ANALYSIS METHOD DATE RESULT UNITS CODE LIMIT BIOCHEMICAL OXYGEN DEMANDSM5210-B N/R MG/L 2.0 TOTAL SUSPENDED SOLIDS SM2540D N/R MG/L AMMONIA NITROGEN SM4500NH3D N/R MG/L 0.1 FECAL COLIFORM SM9222D 7/26/2022 <1 COL/100ML 1 CONDUCTIVITY SM2510B N/R UMHOS/CM 10 CHEMICAL OXYGEN DEMAND SM5220D N/R MG/L 30.0 PH SM4500 H+B N/R STb UNITS 0.1 VOLATILE SUSPENDED SOLIDS SM2540E N/R MG/L �_500 N/R = ANALYSIS NOT REQUESTED LABORATORY DIRECTOR NCDENR DWQ# 37, NCDENR DW # 37781 Shipping: Mailing: 2401 W. 501 St. PO Box 589 Lumberton NC 28358 Lumberton, NC 28359 TBL EHC ENVIRONMENTAL PO BOX 902 RED SPRINGS, NC 28377 ATTN: JOSHUA BASS SAMPLE NUMBER - 33211 DATE SAMPLED - 7-26-22 DATE RECEIVE D-7-26-22 TIME RECEIVED - 1300 PAGE 4 OF 11 FINAL REPORT OF ANALYSES SAMPLE ID - MW # 4 SAMPLER - ARIC CLARK DELIVERED BY - CLIENT PROJECT NAME: REPORT DATE:7-27-22 ANALYSIS METHOD DATE RESULT BIOCHEMICAL OXYGEN DEMAND SM5210-B N/R TOTAL SUSPENDED SOLIDS SM2540D N/R AMMONIA NITROGEN 5M4500NH3D N/R FECAL COLIFORM SM9222D 7/26/2022 <1 CONDUCTIVITY SM2510B N/R CHEMICAL OXYGEN DEMAND SM5220D N/R PH SM4500 H+B N/R VOLATILE SUSPENDED SOLIDS SM2540E N/R N/R = ANALYSIS NOT REQUESTED LABORATORY DIRE Phone: 910-370-0371 Fax: 910-370-0772 Email:pam.hester- tbl(ftotmail.com SAMPLE MATRIX - GW TIME SAMPLED - 0945 RECEIVED BY - THK QUAL DIET. UNITS CODE LIMIT MG/L 2.0 MG/L MG/L 0.1 COL/100ML 1 UMHOS/CM 10 MG/L 30.0 STD UNITS 0.1 MG/L —,---S00 NCDENR DWQ# 37, NCDENR DW # 37781 Y Y u:s. TBL Shipping: Mailinq: 2401 W. Wh St. PO Box 589 Lumberton NC 28358 Lumberton, NC 28359 EHC ENVIRONMENTAL PO BOX 902 RED SPRINGS, NC 28377 ATTN: JOSHUA BASS SAMPLE NUMBER - 33212 DATE SAMPLED - 7-26-22 DATE RECEIVED-7-26-22 TIME RECEIVED - 1300 PAGE 5OF11 FINAL REPORT OF ANALYSES SAMPLE ID - MW # 5 SAMPLER - ARIC CLARK DELIVERED BY - CLIENT PROJECT NAME: REPORT DATE:7-27-22 Phone: 910-370-0371 Fax: 910-370-0772 Email:pam.hester- tbICa7hotmail.com SAMPLE MATRIX - GW TIME SAMPLED - 1031 RECEIVED BY - THK QUAL DET. ANALYSIS METHOD DATE RESULT UNITS CODE LIMIT BIOCHEMICAL OXYGEN DEMAND SM5210-B N/R MG/L 2.0 TOTAL SUSPENDED SOLIDS SM2540D N/R MG/L AMMONIA NITROGEN SM4500NH3D N/R MG/L 0.1 FECAL COLI FORM SM9222D 7/26/2022 <1 COL/100ML 1 CONDUCTIVITY SM2510B N/R UMHOS/CM 10 CHEMICAL OXYGEN DEMAND SM5220D N/R MG/L 30.0 PH SM4500 H+B N/R STD UNITS 0.1 VOLATILE SUSPENDED SOLIDS SM2540E N/R MG/L 500 N/R = ANALYSIS NOT REQUESTED LABORATORY DIRECTOR�— NCDENR DWQ# 37, NCDENR DW # 37781 Shipping: Mailing: 2401 W. 51h St. PO Box 589 Lumberton NC 28358 Lumberton, NC 28359 TBL EHC ENVIRONMENTAL PO BOX 902 RED SPRINGS, NC 28377 ATTN: JOSHUA BASS SAMPLE NUMBER - 33213 DATE SAMPLED - 7-26-22 DATE RECEIVED-7-26-22 TIME RECEIVED - 1300 PAGE 6 OF 11 FINAL REPORT OF ANALYSES SAMPLE ID - MW # 6 SAMPLER - ARIC CLARK DELIVERED BY - CLIENT ANALYSIS METHOD BIOCHEMICAL OXYGEN DEMAND SM5210-B TOTAL SUSPENDED SOLIDS SM2540D AMMONIA NITROGEN SM4500NH31) FECAL COLIFORM SM9222D CONDUCTIVITY SM2510B CHEMICAL OXYGEN DEMAND SM5220D PH SM4500 H+B VOLATILE SUSPENDED SOLIDS SM2540E N/R = ANALYSIS NOT REQUESTED PROJECT NAME: REPORT DATE:7-27-22 DATE RESULT N/R N/R N/R 7/26/2022 <1 N/R N/R N/R N/R LABORATORY DIRECTO Phone: 910-370-0371 Fax: 910-370-0772 Email: pam.hester- tbl(o)hotmail.com SAMPLE MATRIX - GW TIME SAMPLED - 1014 RECEIVED BY - THK QUAL DET. UNITS CODE LIMIT MG/L 2.0 MG/L MG/L 0.1 COL/100ML 1 UMHOS/CM 10 MG/L 30.0 STD UNITS 0.1 MG/L 500 NCDENR DWQ # 37, NCDENR DW # 37781 ;f. z TBL Shipping: Mailing: 2401 W. 51h St. PO Box 589 Lumberton NC 28358 Lumberton, NC 28359 EHC ENVIRONMENTAL PO BOX 902 RED SPRINGS, NC 28377 ATTN: JOSHUA BASS SAMPLE NUMBER - 33214 DATE SAMPLED - 7-26-22 DATE RECEIVED-7-26-22 TIME RECEIVED - 1300 PAGE 7 OF 11 FINAL REPORT OF ANALYSES SAMPLE ID - MW # 8 SAMPLER - ARIC CLARK DELIVERED BY - CLIENT PROJECT NAME: REPORT DATE:7-27-22 Phone: 910-370-0371 Fax: 910-370-0772 Email:pam.hester- tbi hotmail.com SAMPLE MATRIX - GW TIME SAMPLED - 1054 RECEIVED BY - THK QUAL DET. ANALYSIS METHOD DATE RESULT UNITS CODE LIMIT BIOCHEMICAL OXYGEN DEMANDSM5210-B N/R MG/L 2.0 TOTAL SUSPENDED SOLIDS SM2540D N/R MG/L AMMONIA NITROGEN SM4500NH3D N/R MG/L 0.1 FECAL COLIFORM SM9222D 7/26/2022 <1 COL/100ML 1 CONDUCTIVITY SM2510B N/R UMHOS/CM 10 CHEMICAL OXYGEN DEMAND SM5220D N/R MG/L 30.0 PH SM4500 H+B N/R STD UNITS 0.1 VOLATILE SUSPENDED SOLIDS SM2540E N/R MG/L 500 N/R =ANALYSIS NOT REQUESTED LABORATORY DIRECTOR NCDENR DWQ # 37, NCDENR DW # 37781 3 TBL Shipping: Mailin . 2401 W. 5th St. PO Box 589 Lumberton NC 28358 Lumberton, NC 28359 EHC ENVIRONMENTAL PO BOX 902 RED SPRINGS, NC 28377 ATTN: JOSHUA BASS SAMPLE NUMBER - 33215 DATE SAMPLED - 7-26-22 DATE RECEIVED-7-26-22 TIME RECEIVED - 1300 PAGE 8 OF 11 FINAL REPORT OF ANALYSES SAMPLE ID - MW # 9 SAMPLER - ARIC CLARK DELIVERED BY - CLIENT PROJECT NAME: REPORT DATE:7-27-22 Phone: 910-370-0371 Fax: 910-370-0772 Email: pam.hester- tbifthotmail.com SAMPLE MATRIX - GW TIME SAMPLED - 1140 RECEIVED BY - THK QUAL DET. ANALYSIS METHOD DATE RESULT UNITS CODE LIMIT BIOCHEMICAL OXYGEN DEMANDSM5210-B N/R MG/L. 2.0 TOTAL SUSPENDED SOLIDS SM2540D N/R MG/L AMMONIA NITROGEN SM4500NH3D N/R MG/L 0.1 FECAL COUFORM SM9222D 7/26/2022 <1 COL/100ML 1 CONDUCTIVITY SM2510B N/R UMHOS/CM 10 CHEMICAL OXYGEN DEMAND SM5220D N/R MG/L 30.0 PH SM4500 H+B N/R STD UNITS 0 VOLATILE SUSPENDED SOLIDS SM2540E N/R MG/L 500 N/R = ANALYSIS NOT REQUESTED / LABORATORY DIRECTOR ✓ J NCDENR DWQ # 37, NCDENR DW # 37781 Y i TBL Shipping: Mailing: 2401 W. 511 St. PO Box 589 Lumberton NC 28358 Lumberton, NC 28359 EHC ENVIRONMENTAL PO BOX 902 RED SPRINGS, NC 28377 ATTN: JOSHUA BASS SAMPLE NUMBER - 33216 DATE SAMPLED - 7-26-22 DATE RECEIVED-7-26-22 TIME RECEIVED - 1300 PAGE 9OF11 FINAL REPORT OF ANALYSES SAMPLE ID - MW # 10 SAMPLER - ARIC CLARK DELIVERED BY - CLIENT PROJECT NAME: REPORT DATE:7-27-22 Phone: 910-370-0371 Fax: 910-370-0772 Email:pam.hester- tbl(a)hotmail.com SAMPLE MATRIX - GW TIME SAMPLED - 1115 RECEIVED BY - THK QUAL DIET. ANALYSIS METHOD DATE RESULT UNITS CODE LIMIT BIOCHEMICAL OXYGEN DEMAND SM5210-B N/R MG/L 2.0 TOTAL SUSPENDED SOLIDS SM2540D N/R MG/L AMMONIA NITROGEN SM4500NH3D N/R MG/L 0.1 FECAL COLIFORM SM9222D 7/26/2022 <1 COL/100ML 1 CONDUCTIVITY SM2510B N/R UMHOS/CM 10 CHEMICAL OXYGEN DEMAND SM5220D N/R MG/L 30.0 PH SM4500 H+B N/R STD UNITS 0.1 VOLATILE SUSPENDED SOLIDS SM2540E N/R MG/L N/R = ANALYSIS NOT REQUESTED LABORATORY DIRECTOR NCDENR DWQ # 37, NCDENR DW # 37781 M k Shipping: Mailing: 2401 W. 51h St. PO Box 589 Lumberton NC 28358 Lumberton, NC 28359 TBL EHC ENVIRONMENTAL PO BOX 902 RED SPRINGS, NC 28377 ATTN: JOSHUA BASS SAMPLE NUMBER - 33217 DATE SAMPLED - 7-26-22 DATE RECEIVED-7-26-22 TIME RECEIVED - 1300 PAGE 10 OF 11 FINAL REPORT OF ANALYSES SAMPLE ID-MW#11 SAMPLER - ARIC CLARK DELIVERED BY - CLIENT PROJECT NAME: REPORT DATE:7-27-22 ANALYSIS METHOD DATE RESULT BIOCHEMICAL OXYGEN DEMANDSM5210-B N/R TOTAL SUSPENDED SOLIDS SM2540D N/R AMMONIA NITROGEN SM4500NH3D N/R FECAL COLIFORM SM9222D 7/26/2022 21 CONDUCTIVITY SM2510B N/R CHEMICAL OXYGEN DEMAND SM5220D N/R PH SM4500 H+B N/R VOLATILE SUSPENDED SOLIDS SM2540E N/R N/R = ANALYSIS NOT REQUESTED LABORATORY DIRECTOR Phone: 910-370-0371 Fax: 910-370-0772 Email:pam.hester- tbl(a)-hotmail.com SAMPLE MATRIX - GW TIME SAMPLED - 1155 RECEIVED BY - THK QUAL UNITS CODE MG/L MG/L MG/L COL/100ML UMHOS/CM MG/L STD UNITS MG/L NCDENR DWQ # 37, NCDENR DW # 37781 D ET. LIMIT 2.0 0.1 1 10 30.0 0.1 500 it �3 E TBL Shipping: Mailing: 2401 W. 51" St. PO Box 589 Lumberton NC 28358 Lumberton, NC 28359 EHC ENVIRONMENTAL PO BOX 902 RED SPRINGS, NC 28377 ATTN: JOSHUA BASS SAMPLE NUMBER - 33218 DATE SAMPLED - 7-26-22 DATE RECEIVED-7-26-22 TIME RECEIVED - 1300 PAGE 11 OF 11 FINAL REPORT OF ANALYSES SAMPLE ID - MW # 12 SAMPLER - ARIC CLARK DELIVERED BY - CLIENT PROJECT NAME: REPORT DATE:7-27-22 ANALYSIS METHOD DATE RESULT BIOCHEMICAL OXYGEN DEMAND SM5210-8 N/R TOTAL SUSPENDED SOLIDS SM2540D N/R AMMONIA NITROGEN SM4500NH3D N/R FECAL COLI FORM SM9222D 7/26/2022 <1 CONDUCTIVITY SM2510B N/R CHEMICAL OXYGEN DEMAND SM5220D N/R PH SM4500 H+B N/R Phone: 910-370-0371 Fax: 910-370-0772 Email: pam.hester- tbl�hotmail.com SAMPLE MATRIX - GW TIME SAMPLED - 1220 RECEIVED BY - THK QUAL DET. UNITS CODE LIMIT MG/L 2.0 MG/L MG/L 0.1 COL/100ML 1 UMHOS/CM 10 MG/L 30.0 STD UNITS 0.1 VOLATILE SUSPENDED SOLIDS SM2540E N/R MG/L 500 N/R =ANALYSIS NOT REQUESTED LABORATORY DIRECTOR -' NCDENR DWQ # 37, NCDENR DW # 37781 T B L ENVIRONMENTAL LABORATORY, INC. 2401 W. ST" STREET LUMBERTON, NC 28358 (910) 370-0371 Baling Information:. � H-C Fq ✓; ivy "+A-t, 0� Z Rey Sr'n`n�s, nor_ 2 S 7' ����. a, Analysls,ContalnerWreservative- \ me-�s�.L...�-� --kArem a/*A Project Description: ity/Seto ApfllC Phone: FAX: C116nt Project #: ESC Key: Collected by: Sile/Facility ID#: P.O.#:— CoCode (lab use only) TemplatefPreloyln Shipped Via: Collecled by (slgnalure): ImmediatelyPacked on Ice N Y Rush? ( lab MUST 8e Notified) Same Day ....... 200% Next Day........ 100% Two Day .........50% Date Results Needed: No. of Email? —No—Yes FAX? No Yes Sample ID CDmp(Grab Matrix' Depth Dale Time Cnlrs RemarkstConlaminant Sample It(tabonly) d ! cl /N 12 v w� Z ��- v 'Matrlx SS - SoIVSolld GW - Groundwater WW - WasleWater DW - Drinking Water OT - Other Remarks: ,17 PH Temp Flow Other Rell �hby: na�e) Relinquished by (Signature) Dale: Time; Recelved g alure Received by: (Signature) Samples returned via: ❑ UPS ❑ FedEx ❑ Courier ❑ Condllton: (lab use only) Dale: Time: Temp: Bottles Received: CoC Seals Intact: _ Y _ N _ NA Relinquished by: (Signature) Dale: Time: Recelved for lab by: (Signature) Dale: Time: pH Checked: NCF: T B L ENVIRONMENTAL LABORATORY, INC. 2401 W. 5T" STREET LUMBERTON, NC 28358 910 370-0371 BINIng Information: _. c✓i (vA �.o P,,x go z Re) S�'n`�?s�W,_ 25 7' epo o. ��o ^C�k�IC�J'►7Ci Analysls/GonlelnerlPmservalive v Project l Description: �G ity/Sate ityts d O (` Phone: FAX: Client 46roject #: ESC Key: Collected by: XY Slle/Facility ID#: P.O.#: CoCode (lab use only) late/Prelo em to p g Shipped Via: Collected (Sigr rule Immediately Pec ed on Ice N Y Rush? ( Lab MUST Be Notified) Some Day ....... 200% Next Day........ 100°/. Two Day .........50% ° Date ILesults Needed: No. of Email? —No—Yes FAX7 No Yes — Sample ID Comp/Grab Matrix' Depth Date Time Cnirs Remarks/Contamtnant Sample Ir (tab only) Gv - Z / l r b — ..- , --- •Malrlx SS - SoIVSolld GW - Groundwaler WW - WasteWaler DW - Drinking Waler OT - Other Remarks: PH Temp Flow Other Relln she by' gnat ) Relirtq> d by: (Signature) Date: Time:. Samples returned via: Received ff alure p Fedes O Courier []UPS Received by: (Signature) Temp: Bottles Received: Condltton: (lab use only) Qate: Time: CoC Seals Intact: _ Y _ N _ NA Relinquished by: (Signature) Dale: Time: I Received for lab by: (Signature) Dale: Time: pH Chocked: NCF: 41 2"OUR SPILL RESPONSE NUMBER (910) 843-4456 ENVIRONMENTAL HYDROGEOLOGICAL CONSULTANTS, INC. StationLevelWater I'll Tem Finic US EPA Lab ,.,: Campbell , , Aric Clark ='MW-8 _ - r►• -Analyst: ®rMro �y